DISPOSABLE FILTRATION UNIT WITH RECOVERABLE FILTER

Abstract: A disposable filtration unit with recoverable filter and method of manufacturing the same, the unit (10) comprising: a) a receptacle (12) for receiving filtrate; b) a support plate (16) fixed to the receptacle 12 and having at least one opening therethrough; c) a filter membrane (18) on the support plate (16); d) an open-ended shell (14) for receiving a liquid to be filtered, the shell (14) having a lower end portion extending into the receptacle (12) and against the support plate (16) and filter sheet (18); e) seal means between the shell (14) and support plate (16); and f) breakaway means (30) connecting the shell (14) to the receptacle (12) at spaced intervals about the periphery thereof, and providing weakened rupture points which permit separation of the shell (14) and receptacle (12) for recovery of the filter membrane (18). The breakaway means can comprise vertical ribs (30) which extend between the shell (14) and receptacle (12) and which provide the sole attachment of the shell to the receptacle. These ribs (30) can be formed integrally with a necked portion (24) of the shell (14).

Description: DISPOSABLE FILTRATION UNIT WITH RECOVERABLE FILTER AND METHOD OF MANUFACTURING THE SAME The present invention relates generally to a disposable filtration unit as may be used for laboratory work and the like. In particular the present invention relates to such a filter wherein the filter medium is quickly and easily recoverable. Disposable filtration units are well known in the art. One such unit for example is identified in U.S. Patent 3,295,686. Generally the unit described in this patent is a disposable filter which is supplied to the user in a sterile package ready for use wherein the filter membrane is sandwiched between component parts of the unit. These component parts are permanently fixed together as by cementing or ultrasonic welding so that an airtight seal is formed about the periphery which prevents leakage of air into the unit at a point downstream of the filter. Other disposable units have the filter membrane permandntly afixed by cementing or by sonic welding to one element of the unit. While such units are appropriate in cases where the user is interested in recovering the filtrate, such units are not suitable in cases where the user is interested in recovering the material filtered from the liquid. In this respect the construction of disposable units of the prior art does not facilitate removal of the filter sheet. With these prior art units, attempts to recover the filter sheet often result in a destruction of the filter sheet and the loss of some of the material which the user desires to recover. The present invention may be characterized in one aspect thereof by the provision of a receptacle for receiving the filtrate and a hollow open-ended shell joined to the receptacle by a breakaway connection. Sandwiched between the shell and the receptacle is a support plate and a filter membrane wherein one end of the hollow shell clamps the filter membrane to the support plate so that when the shell is broken away from the receptacle, the filter membrane can be lifted off of the support plate. A gasket between the shell and support plate effects an airtight seal which prevents the leakage of air into the receptacle do mstream from the filter membrane. The gasket and shell also cooperate so that the gasket is removed together with the shell. Eeodlmen# of the invention will now be described by way Df example and with reference to the aaxnpanying drawings, in which: Figure 1 is a side elevation view partly broken away and in section showing the disposable filter unit of the present invention; Figure 2 is a view on an enlarged scale showing a portion of the filtration unit; and Figures 3 and 4 are views similar to Figure 2 only showing other embodiments of the invention. Referring to the drawings, Figure 1 shows the disposable filtration unit of the present invention generally indicated at 10 as including a lower cup-shaped receptacle 12 for receiving the filtrate and an upper open-ended hollow shell 14 for receiving the liquid to be filtered. The receptacle has a spout 20 which serves both as a connector for attachment of a vacuum line and as a pouring sp0'# f#r f^; filtrate received into the receptacle. Disposed between the shell and receptacle is a generally funnel shaped support plate 16. The support plate 16 has an upstanding outer rim 17 which surrounds a sheet of filter material 18 and a support pad 19 laid on the support plate (Figure 2). As shown in Figure 1 and 2, the upper end of the receptacle 12 has a rim 21 which forms an internal shoulder 22. Support plate 16 is carried on this shoulder as a customary in the art. The support plate can be permanently attached to the receptacle by Åa suitable cement or by ultrasonic welding to provide an airtight connection between the receptacle and support plate. The lower end of shell 14 has a necked portion 24 so that it can be received into receptacle rim 21. The axial length of necked portion 24 and its position within rim 21 is such that there is some axial distance, indicated at 26, between the top of the receptacle rim and an edge 28 of the necked portion. Formed integral shell 14 at spaced intervals about the necked portion are a plurality of vertical ribs 30. The length of these ribs are sufficient to bridge the distance 26 as shown in Figure 1. These ribs can be attached to the upper end of receptacle rim 21 by any suitable means such as ultrasonic welding so as to fix shell 14 to the receptacle. because the attachment of ribs 30 to the receptacle occurs only at spaced intervals about the periphery of the receptacle, it should be appreciated that these ribs 30 provide weak breakaway points so as to facilitate removal of the shell from the receptacle. Figure 2 shows in greater detail the connection between the breakaway shell and the receptacle. The lower and face of shell 14 is bifurcate, having a groove 32 which divides the lower end of the shell into an inner foot 34 and an outer foot 36 for purposes explained hereinbelow. Disposed between the lower end face of shell 14 and support plate 16 is a flat, annular gasket 38. The inner periphery of this gasket overlies the filter membrane and the outer periphery rests on the support plate rim 17. The gasket is pressed against rim 17 of the support plate 16 and against filter membrane 18 by the bifurcate lower end of shell 14. In this way the gasket provides two seals. The first seal is a liquid tight seal between shell 14 and filter membrane 18 which prevents liquid in the reservoir from being drawn around and beneath the edge of the filter membrane and into receptacle 12. This first seal is made more effective by an annular rib 40 on the gasket which is pressed into and against the filter membrane 18 by the inner foot 34 of shell 14. The second seal is an air tight seal between shell 14 and support plate 16 which prevents air from being drawn under the outer edge of the gasket. This second seal is made effective by having the outer foot 36 of the shell pressing the outer periphery 42 of the gasket against the rim 17 of the support plate. Between the gasket rib 40 and the outer periphery 42 of the gasket, is an upstanding band 44 of gasket material. This upstanding band is received in groove 32 and is slightly wiper than the groove as to provide an interference fit. With this arrangement the gasket 18 is interlocked with shell and will remain attached to the shell when the shell is broken away and removed from receptacle 12. To manufacture the filtration unit of the present invention the separate components, namely the receptacle 12, shell 14 and support plate 16, are separately molded as by injection molding. Gasket 38 is also molded from an appropriate gasket material such as thermoplastic elastomer or silicone rubber. Support plate 16 is then attached to the receptacle and against shoulder 22 by cementing, sonic welding or other suitable means. Thereafter, the filter membrane'lE and, if desired, the pad 19 are placed on support plate 16. The shell, with gasket 38 already attached to the lower end of the shell, is then placed in position by inserting the necked portion 24 of the shell into the receptacle rim 21. This simultaneously clamps the filter sheet to the support plate and compresses the gasket material to effect the two seals as described above. With the shell held in this position ribs 30 are attached as by sonic welding to the upstanding end of the receptacle rim 21. In use the liquid to be filtered is simply poured into the hollow shell 14 and the filtrate collected in receptacle 12. If desired air can be evacuated from the receptacle to speed the filtration process by attaching a vacuum line to spout 20. After the liquid has been filtered the hollow shell is simply broken away from the receptacle, the attachment of ribs 30 to the receptacle being weak, "breakaway" points which makes it easy to remove the shell from the receptacle. Due to the interference fit between the band 44 of gasket material and groove 32 in the end face of shell 14, the gasket 38 is held to the shell and is removed together with the shell to expose the filter sheet 18. With the shell and gasket removed, the filter membrane 18 can be lifted off of the support pad in order to collect or work on the materials filtered from the liquid. Alternative forms of the invention are shown in Figures 3 and 4, it being understood that parts similar to those shown in Figures 1 and 2 are identified with the same reference numeral, In the embodiments shown in Figures 3 and 4, the support plate 16 takes a slightly different form to accommodate an alternative sealing arrangement which does not utilize a formed gasket 38 as shown in the preferred embodiment of Figures 1 and 2. Figure 3 shows that support plate 16 has an upstanding tongue 50 spaced radially inward from receptacle rim 21 so the rim and tongue 50 define a space 52 therebetween. Prior to the assembly of shell 14 to the receptacle, a suitable liquid gasket material 54 such as an RTV Silicone or the like is put into space 52. Upon assembly of the shell to the receptacle, tongue 50 is received into the groove 32 so that the outer foot 36 of the receptacle extends into the gasket material 54. This displaces sufficient gasket material so that an airtight seal is formed between the shell and support plate which prevents air leaking into the receptacle downstream from filter membrane 18. The inner foot 34 of the shell presses directly on filter membrane 18 to clamp its periphery to support plate 16. An alternative construction is shown in Figure 4. In this embodiment the support plate 16 has an upstanding peripheral lip 60 in addition to tongue 50. Lip 60 and tongue 50 define the sidewalls of a channel 62 for receiving the gasket material. It should be appreciated that in this embodiment tongue 50 is higher than lip 60. This ensures that when the shell is attached to the receptacle the gasket material is not squeezed around tongue 50 so as to contact the filter sheet 18. Instead, the gasket material is squeezed over the lower lip 60 and into the space 52 between the necked portion 24 of the shell and the receptacle rim 21. In the absence of lip 60 as shown in the Figure 4 embodiment, gasket material 54 simply is squeezed around the outer foot 36 of the shell and into the space between the necked portion of the shell and the receptacle rim. Thus, it should be appreciated that the present invention provides a filter unit which permits easy recovery of the filter membrane. The unit is easily manufactured and designed to be a one-use disposable item in that the separation of the shell from the receptacle at the "break-away" points prevents reuse of the unit.

Claims: CLAIMS: 1. A disposable filtration unit having a recoverable filter membrane comprising: a) a receptacle for receiving filtrate; b) a support plate fixed to said receptacle and having at least one opening therethrough; c) a filter membrane on said support plate; d) an open ended shell for receiving a liquid to be filtered, said shell having a lower end portion extending into said receptacle and against said support plate and filter sheet; e) seal means between said shell and support plate; and characterized by f) breakaway means connecting said shell to said receptacle at spaced intervals about the periphery thereof, and providing weakened rupture points which permit separation of said shell and receptacle for recovery of said filter membrane. 2. A disposable filtration unit as claimed in claim 1, characterized in that said breakaway means comprises vertical ribs extending between said shell and receptacle, and providing the sole attachment of said shell to said receptacle. 3. A disposable filtration unit as claimed in claim 1 or 2, characterized by: a) an upstanding rim on said receptacle; b) a necked lower end portion formed integral said shell and extending into said rim; and c) vertical ribs at spaced intervals about the outer periphery of said necked portion forming said breakaway means, said ribs being shorter than said necked portion and fixed to the top edge of said rim for connecting said shell to said receptacle. 4. A filtration unit as claimed in claim 2 or 3, characterized in that said ribs are formed integral with said necked portion. 5. A disposable filtration unit as claimed in any preceding claim, characterized in that said shell has a bifurcate lower end defining an inner foot, an outer foot and an intermediate groove, i) said inner foot being adapted to press said filter membrane against said support plate, and ii) said outer foot being adapted to press said seal means against said support plate. 6. A disposable filtration unit as claimed in claim 5, characterized in that said seal means is a flat gasket having a projecting band upstanding from the upper surface of said gasket, said band being wider than said groove so as to provide an interference fit, whereby said gasket remains attached to said shell when said shell is broken away and removed from said receptacle. 7. A disposable filtration unit as claimed in claim 5 or 6, characterized in that said seal means is a flat annular gasket having a rib projecting downward from the lower face thereof, said rib being located beneath said inner foot and extending around said gasket adjacent the inner periphery thereof. 8. A filtration unit as claimed in claim 5 6 or 7, characterized in that i) said support plate is larger in diameter than said filter membrane so that the outer edge of said support plate extends out from under said filter membrane; ii) said seal means is a flat annular gasket having its inner periphery overlying said filter membrane and its outer periphery overlying the outer edge of said support plate; and iii) a band on the upper surface of said gasket interlocks with said groove to attach said gasket to said shell. 9. A disposable filtration unit as claimed in claim 5, characterized by an upstanding tongue on said support plate adapted to be received in said groove, said tongue and receptacle defining an annular space therebetween, said seal means being in said space, and said outer foot extending into said space and engaging said gasket for effecting an airtight seal between said shell and support plate. 10. A filtration unit as claimed in claim 9, characterized in that said support plate has an upstanding lip spaced outward from said tongue, said lip and tongue defining a channel therebetween for receiving said seal means, said outer foot extending into said channel to effect an airtight seal between said shell and support plate. 11. A filtration unit as claimed in claim 10, characterized in that said tongue is taller than said lip. 12. A filtration unit as claimed in claim 10 or 11, characterized in that said channel communicates with said space between said receptacle rim and tongue. 13. A disposable filtration unit having a recoverable filter membrane comprising; a) a receptacle for receiving filtrate having an upstanding rim portion which defines an internal shoulder; b) a support plate fixed to said receptacle against said shoulder and hacing at least one opening therethrough; c) a filter membrane laid on said support plate over said opening; d) a flat, annular gasket overlying said filter membrane and support plate; e) an open ended shell for receiving liquid to be filtered, said shell having a necked portion adapted to extend into said rim, the lower end face of said necked portion being adapted to press said gasket against said support plate and filter membrane to form seals therebetween; and characterized by f) vertical ribs which are formed integral with said necked portion at spaced intervals about the periphery thereof, which are shorter than the length of said necked portion, whose lower ends are fixed to the upper edge of said receptacle rim, which provide the sole points of attachment of said shell to said receptacle and which are sufficiently weak to permit manual separation of said shell and receptacle to recover said filter membrane. 14, A disposable filtration unit as claimed in claim 1X, characterized in that the end face of said necked portion has an inner foot, an outer foot and an intermediate groove, said inner foot pressing said gasket against said filter membrane and support plate to provide a liquid tight seal therebetween and said outer foot pressing said gasket against said support plate to provide an air tight seal therebetween. 15. A disposable filtration unit as claimed in claim 14, characterized by means on said gasket interlocking with said groove so that said gasket remains attached to said shell when said sheet is broken away and removed from said receptacle. 16. A method of making a disposable filtration unit having a recoverable filter comprising the steps of: a) fixing a support plate to the rim of a filtrate receptacle, said plate having at least one opening therethrough; b) resting a filter membrane on said support plate; c) placing a gasket on said support plate about said filter membrane; d) inserting one end of a hollow open-ended shell into said rim and against said gasket and support plate, said one end being bifurcate with an inner portion pressing against said gasket and filter membrane and an outer portion pressing against said gasket and support plate; and characterized by e) attaching said shell to said rim only at spaced points about the periphery of said rim.

Inventors: BAIRD, PETER K., MEHRA, RAVINDER C., RELYEA, ROBERT G.
Applicants: SYBRON CORPORATION
Application year: 1981
Main classification: B01D29
IPC codes: B01D29, B01D35, B01D36