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                            Library & Multimedia
 In situ microanalysis of organic colorants by inkjet colloid deposition surface-enhanced Raman scattering
NCJ Number
              304170
Journal

*Journal of Raman Spectroscopy* Volume: 45 Issue: 1 Dated: 2013 Pages: 123-127
Author(s)
          Dario P. Benedetti;
                        et al
Date Published

2013
Length
              5 pages
Annotation
              This article reports on a new method for the minimally invasive in situ identification of inks and colorants on documents and other objects on the basis of the deposition of silver colloid nanodroplets on a region of interest in the objects to be tested, using inkjet technology.
Abstract
              By adapting commercially available thermal and piezoelectric inkjet heads, volumes of silver colloid in the 60–220 picoliters range (corresponding to impact diameters in the range of 50–150 μm) can be delivered onto substrates with great accuracy and precision. The project demonstrated that the instantaneous superheating of the colloid in the thermal print head does not adversely affect the surface-enhanced Raman spectroscopy efficiency of the Ag nanoparticles. Furthermore, by mounting a compact piezoelectric inkjet head within a large-stage Raman microscope, the project developed an instrument in which all phases of surface-enhanced Raman spectroscopy microanalysis are integrated, with great advantages in sample handling, spatial accuracy, and colloid delivery reproducibility. The approach can be considered functionally nondestructive, since the amount of silver delivered and the area affected are too small to be detected by visual observation, and in most conditions, even by optical microscopy. The method was successfully applied to the analysis of textile fibers, gel pen ink writing on paper, and a Japanese woodblock print dating to the end of the 19th century. (publisher abstract modified)
      
  
          Additional Details
Grant Number(s)
        2006-DN-BX-K034


  
  
        
  Agencies
        NIJ-Sponsored


  
  
        
  Publication Type
        Research (Applied/Empirical)


  
  
        
  Award
        Development of Advanced Raman Spectroscopy Methods and Databases for the Evaluation of Trace Evidence and the Examination of Questioned Documents
    
  
  
Date Published: January 1, 2013
    
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