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                            Library & Multimedia
 Raman Microspectroscopic Mapping as a Tool for Detection of Gunshot Residue on Adhesive Tape
NCJ Number
              254183
Journal

*Analytical and Bioanalytical Chemistry* Volume: 410 Issue: 28 Dated: 2018 Pages: 7295-7303
Author(s)
          Justin Bueno;
                        Lenka Halamkova;
                        Alexander Rzhevskii;
                        Igor K. Lednev
Date Published

2018
Length
              9 pages
Annotation
              This article reports on validation studies that investigated the reproducibility/ruggedness and specificity of the approach of the authors' previous development of a novel method for the detection of gunshot residue (GSR) via tape lifting, combined with Raman microspectroscopic mapping and multivariate analysis.
Abstract
              The initial study achieved proof of concept for this approach. In the current validation studies, Raman mapping for GSR detection on adhesive tape was performed on an independent Raman microscope not used to generate the training set. These independent spectra were classified against the original training dataset using support vector machine discriminant analysis (SVM-DA). The resulting classification rates of 100 percent illustrate the reproducibility of the technique, its independence upon a specific instrument, and provide an external validation for the approach. In addition, the same procedure for GSR collection (tape lifting) was performed to collect samples from environmental sources, which could potentially provide false-positive assignments for current GSR analysis techniques. Thus, particles associated with automotive mechanics were collected. Automotive brake and tire materials are often composed of the heavy metals lead, barium, and antimony, which are the key elements targeted by current GSR detection technique. It was determined that Raman spectroscopic analysis was not susceptible to misclassifications from these samples. Results from these validation experiments illustrate the great potential of Raman microspectroscopic mapping used with tape lifting as a viable complimentary tool to current methodologies for GSR detection. Furthermore, current methodologies are not well-developed for automated organic GSR detection. Illustrated here, Raman microscoptrosocpic mapping has the potential for the automatic identification of organic GSR. (publisher abstract modified)
      
  
          Additional Details
Grant Number(s)
        2016-DN-BX-0166


  
  
        
  Agencies
        NIJ-Sponsored


  
  
        
  Publication Type
        Research (Applied/Empirical)
                                Report (Study/Research)
                                Report (Grant Sponsored)
                                Program/Project Description


  
  
        
  Award
        Vibrational Spectroscopy of Gunshot Residue
    
  
  
Date Published: January 1, 2018
    
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      PatentsRelated Topics
        
                Evidence collection
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        Gunshot residue
        National Institute of Justice (NIJ)



  
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