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Title:   Author  item
                                            Doll, Kenneth

                                                         - *Ken*item
                                            Biswas, Atanu
  Submitted to: Surfactants in Tribology
                                    Publication Type: Book / Chapter
                                    Publication Acceptance Date: 3/30/2012
                                    Publication  Date: 3/20/2013
                                    Citation: Doll, K.M., Biswas, A. 2013. A biobased nitrogen-containing lubricant additive synthesized from expoxidized methyl oleate using an ionic liquid catalyst. In: Biresaw, G., Mittal, K.L., editors. Surfactants in Tribology. Volume 3. Boca Raton, FL: CRC Press. p. 131-145.Interpretive Summary:
                                Technical Abstract: Utilizing an epoxidation route, an aniline adduct was synthesized from methyl oleate. An ionic liquid, 1-methylimidazolium tetrafluoroborate, was found to be the key for this catalytic system. The reaction produces a product with the aniline incorporated into the fatty chain, at the 9(10) position, and fatty amide is not produced. The product is an effective antiwear additive in polyalphaolefin lubricants, reducing the measured wear of a friction and wear test from 0.51 mm to below 0.47 mm. The material also improved the oxidation onset temperature of the lubricant solution by more than 25 deg C.


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