# Appendix D



# Draft Facility Report on Product Content

October 2010 Submission 

# ~f-,oNNon CBI



# Company Sanitized

## 2010/15 PFOA Stewardship Program



# Draft Facility Report on Product Content
I . CHEMICAL IDENTIFICATION Identify the product (e.g fluoropolymer dispersion) for which you are submitting information:

Product name: FLUOROPOLYMER Product description (including concentrations of perfluoroalkyl chemicals identified in Section IV below and year of production) : _[ ] PPM

A PFO CAS number: 3825-26-1 II . COMPANY IDENTIFICATION Identify the company and location ofthe facility submitting information:

Company name: - SOLVAY SOLEXIS, INC Site location: THOROFARE, NJ Identify a company technical contact who can respond to inquiries about the information submitted: Technical contact: VIRGINIA HUBERT

Phone: (713

) 525-6051 Address:- 10 Leonard Lane, Thorofare, NJ III . PRODUCTION Calendar year for which you are reporting: Jan 1, 2009- to Dec 31, 2009 Provide the amount of the product for the reporting year at each specific site:

Imported [ ] kgs/yr Manufactured [ 1 kgs/yr

### IV. PRODUCT CONTENT

A . CONCENTRATIONS OF RELEVANT PERFLUOROALKYL CHEMICALS Please provide the concentrations (ppb) ofvarious perfluoroalkyl chemicals in your product. For chemicals for which you do not have actual data, please provide range estimates. 

## [ ] PPM CAS# 3825-26-1 The following is a nonexhaustive list ofchemicals that should be included: PFOA and its salts " Octanoic acid, pentadecafluoro- (CAS 335-67-1) " Octanoic acid, pentadecafluoro- ammonium salt (CAS 3825-26-1) PFOA precursors " Octane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7, 8,8-heptadecafluoro-8-iodo- (CAS 507-63-1) " 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7) " 1-Decene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 21652-58-4) " 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 27905-45-9) " 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 1996-88-9) " 2-Decenoic acid, 3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-hexadecafluoro- (CAS 70887-84-2) " Decanoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 27854-31-5) Higher homologues " Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-pentacosafluoro-12-iodo- (CAS 307-60-8) " Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-l0-iodo- (CAS 423-62- 1) " Nonanoic acid, heptadecafluoro- (CAS 375-95-1) " Decanoic acid, nonadecafluoro- (CAS 335-76-2) " 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7) " Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluoro-10-iodo- (CAS 2043-53-0) " Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-12-iodo- (CAS 2043-54-1) " 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 4980-53-4) " 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12- heneicosafluorododecyl ester (CAS 17741-60-5) Part IV (cont .) 

### B . ANALYTICAL METHODS

### The surfactant content in the products imported were measured per the attached methods PF 89/110 GC E - Perfluorooctanoate and Higher Homologues in Aqueous Dispersions - Extraction for Analysis using GC-FID PF 89/110 POW

E - Perfluorooctanoate and Higher Homologues in Polymer Bulk or Sintered - Extraction and Esterification. Comments : These methods were used in 2006to obtain the data for the mass balance submittal

# U51mon-r_,=

APPROVED -COPY N° AUSIMONT S.P.A. Centro Ricerche e Sviluppo

Bollate 

### Anal yt ical Method PF 89/110 GC E Perfluorooctanoate and higher homologues

in Algoflon matrices Analysis using GC-FID
This document is composed by: 

### N° pages: 4 N° tables: N° figures : N° attachments: 

### Edition: 4 Date: Oct 2001 Laboratory: GC Author : Oriani Verification: Morandi Approval : Pace 1 Scope and application 1 .1 This method is for the analysis of extracts of perfluorooctanoate (APFO) and related homologues. 1 .2 Applicable compounds are: perfluorooctanoate (APFO) [C7FISCOO-], perfluorononanoate [C8F,7C00-], perfluorodecanoate [C9F19C00-], perfluoroundecanoate [C~oF2]C00-], perfluorododecanoate [C>>F23C00-] and higher homologues. 1 .3 Matrices : Algoflon based formulations and environmental samples compatible with esterification and GC-FIDdetermination. 2 Summary 2.1 Analysis of APFOand homologues extracted matrices is performed by injection in a packed column, glass, 2m long, 6mmo.d., 3mmi .d., packed with metylPF 89/110 GCE Page 1 of 4

# usimonT..r siloxane rubber SE 30 20% on Chromosorb W AWDMCS 80-100 mesh, isothermal run at 80°C, flame ionisation (FID) detector. 3 Definitions 3.1 APFO

: perfluorooctanoate. 3 .2 Gaschromatograph (GC) with flame ionisation detector (FID) : model 8000 top fromFisons equipped with standard packed column injector. 3.3 Data system

: Electronic integrator mod. Chromjett from Fisons or PC based acquisition systemmod. Chromcard fromFisons . 4 Safety precautions 4.1 Use caution with temperatures of GC injector and detector. When running temperatures are of about 250°C. 4.2 When handling samples or solvents wear appropriate protective gloves, eyewear, clothing and any other protective devices mandatory in your working area. 5 Interferences 5.1 To minimise interferences when analysing samples PTFE vials and tubing should not be used for sample storage or handling. 6 Equipment 

### 6 .1 GC FID mod. 8000 fromFisons 6.2 Electronic recording integrator mod. Chromjett from Fisons or PC running Chromcard software fromFisons 7 Supplies and materials 7.1 GC grade Nitrogen used as carrier gas 7.2 GC grade Hydrogen used for FID 7.3 GC grade Air used for FID 7.4 Micro-syringes glass 10 ~tl 7.5 Centrifuge tubes glass IOml 7.6 Vials lOml 8 Reagents and standards 

### 8.1 CFC 113 Fluka for IRor equivalent

PF 89/110 GC E Page 2 of 4

# UsImot'1T=~-- 8.2 Standard Typically one method and matrix blank and one continuing calibration standard S20ppmare prepared with each group of samples. 9 Quality control 9.1 Method and matrix blank Analyse a method and matrix blank prior to each group of samples . 9.2 Matrix spike Analyse a matrix spike prior to standard calibration curve. 9.3 Continuing calibration check 9.3.1 Analyse S20ppm sample first to assure the accuracy of initial calibration curve. 9.3.2 Analyse S20ppmevery tenth samples . 9.3.3 If a significant change (i .e. >25%) in peak area occurs, relative to the initial calibration curve, subsequent analysis will be invalid . 10 Calibration and standardisation 10.1 Prepare and analyse a standard calibration curve after each maintenance intervention 10.2 The r2 value for linear regression of data should be 0.98 or greater 10.3 If curve does not meet requirements change analytical column or re-prepare calibration standards . 11 Procedures 11 .1 Use a packed column, , glass, 2mlong, 6mmo.d., 3mmi .d., packed with metylsiloxane rubber SE 30 20% on Chromosorb W

AW DMCS 80-100 mesh 11 .2 Carrier : Nitrogen, flow rate: 40m1/min measured at roomtemperature connecting flowmeter to detector outlet . 11 .3 Injector : standard packed at 250°C 11 .4 Detector : FID at 250°C, Hydrogen flowrate: 30ml/min, Air flowrate 500m1/min 11 .5 Oven temperature: isothermal at 80°C 11 .6 Injection volume: liquid measured 1 pl 11 .7 APFOretention time: 3 minutes

PF 89/110 GC E Page 3 of 4

# usimcrnT_:- 12 Data analysis and calculations Calculate actual concentration of APFO, or other applicable compounds, from calibration line using an external standard method. 13 Method performances Method detection limit and method quantitation limit are referred to each matrix and reported in specific methods. 14 Pollution prevention and waste management Samples in CFC are disposed in dedicated container. Samples in water / methanol are disposed in dedicated container Solid polymer residuals are disposed in dedicated container Disposable glass vials are disposed in broken glass containers located in laboratory. 15 Records None

PF 89/110 GC E Page 4 of 4

# RU5I mO nT

_ . ~.- APPROVED -COPY N° AUSIMONT S.P

.A. Centro Ricerche e Sviluppo

Bollate Analytical Method 

### PF 89/110 POW

E Perfluorooctanoate and higher homologues in polymer bulk or sintered Extraction and esterification
This document is composed by: N° pages: 5 N° tables: N° figures : N° attachments: Edition: 3 Date: June 2001 Laboratory: GC Author: Oriani Verification: Morandi Approval : Pace 1 Scope and application 1 .1 This method is for the extraction of perfluorooctanoate (APFO) and related homologues fromAlgoflon (PTFE) polymer bulk or sintered. 1 .2 Applicable compounds are: perfluorooctanoate (APFO) [C7F15C00-], perfluorononanoate [C8F17C00-], perfluorodecanoate [C9Fj9C00-], perfluoroundecanoate [C,oFZ]C00-], perfluorododecanoate [C,IF23C00-] and higher homologues . 1 .3 Matrices : Algoflon polymer, bulk or sintered, dry (humidity lower than 5%by weight) . 2 Summary 2.1 About 500mg (I g if sintered) ofAlgoflon is weighed in a 10 ml vial . Add 2ml of methanol containing 1% Sulphuric acid. Close carefully the vial with a PTFE PF 89/110 POW

E Page 1 of 5

# RUSimof"iT- :_- capped septum, then allow APFO esterification at 70°C over night . At room temperature add I ml of CFC 113, centrifuge then transfer 2 ml of clear solution in a lOml vial . Wash out acidic methanol with 4m1 water . Close vial and allow phases separation at 40°C for 15 minutes . Inject 1 pl of lower liquid layer. Analyse using method PF 89/110 GC E. 3 Definitions 3.1 APFO

: perfluorooctanoate. 4 Safety precautions 4.1 When handling samples or solvents and hot vials wear appropriate protective gloves, eyewear, clothing and any other protective devices mandatory in your working area. 5 Interferences 5.1 To minimise interferences when analysing samples PTFE vials and tubing should not be used for sample storage or handling. 6 Equipment 

### 6.1 Centrifuge ALCCENTRIFUGETTE 4236 6.2 Shaker IKA-VIBRAX-VXR 6 .3 Balance (+/- lmg) 7 Supplies and materials 7.1 Gloves 7.2 Timer 7.3 Syringes glass 1 cc, 5 cc 7.4 Micro-syringes glass 10 p,l, 250 ~tl, 7.5 Centrifuge tubes glass lOml 

### 7 .6 Vials lOml 7.7 Glass bottles nominal 100ml 7.8 Glass volumetric flasks 100m1 volume 7.9 Athermic gloves 8 Reagents and standards 8.1 Concentrated sulphuric acid R.P.E. Carlo Erba or equivalent 8.2 Methanol R.S. Carlo Erba or equivalent 

### 8 .3 CFC 113 Fluka for IR or equivalent 8.4 Ammonia 30%R.P.E. Carlo Erba or equivalent PF 89/110 POW

E Page 2 of 5

# RUsImon°r~_r

8.5 Reagent preparation 1 % sulphuric acid in methanol : in a bottle of nominal 100m] (true volume 116ml) weigh 49.5g of methanol then add slowly 0.5 g concentrated sulphuric acid. 8.6 Standard preparation SoI .A: weigh 100mg of solid ammonium salt of perfluoro-acid, dissolve in IOOml methanol in volumetric flask. S200ppm

: transfer 100pl of Sol .A in a l Oml vial, add 1 .6m1 of methanol 1 % sulphuric acid and followthe esterification procedure. S 100ppm

: transfer 50~tl of SoI .A in a l Oml vial, add 1 .8m] of methanol 1 % sulphuric acid and followthe esterification procedure. 

### S50ppm : transfer 25u1 of SoI .A in a lOml vial, add 1 .9ml of methanol 1% sulphuric acid and followthe esterification procedure. S20ppm : transfer 10~t1 of Sol .A in a l Oml vial, add 2m1 of methanol 1 % sulphuric acid and followthe esterification procedure . S10ppm : transfer 5~1 of Sol .A in a lOml vial, add 2ml of methanol 1%sulphuric acid and followthe esterification procedure. 9 Quality control 9.1 Method and matrix blank In a lOml vial weigh 500mg of Hyflon"' MFA powder, follow esterification procedure. Note: Hyflon polymers are free fromAPFOand Surflon surfactants With each batch of samples prepare and analyse a blank as first sample. 9.2 Matrix spike In a lOml vial weigh 500mg of Hyflon® MFA powder, add 5 ~t1 of Sol .A then follow esterification procedure. Note: Hyflon polymers are free fromAPFOand Surflon surfactants. With each complete calibration prepare a matrix spike and a blank. 

### As last samples after calibration inject in triplicate blank and matrix spike. 9.3 Continuing calibration check 9.3.1 With each batch of samples prepare S20ppmcalibration solution. PF 89/110 POW

E Page 3 of 5

# usimon-r=,

9.3.2 Analyse S20ppm sample first to assure the accuracy of initial calibration curve. 9.3.3 Analyse S20ppmsample per group of 10 samples, followed by a blank (9.1) . 9.3.4 Analyse S20ppmsample last to assure the accuracy ofdata. 10 Calibration and standardisation 10.1 Prepare calibration standards 10.2 Inject 1 ~tl each at least in triplicate 10.3 Calculate concentration of APFO in dispersion from APFO concentration in solution assuming that So1 .A contains about 1 ~tg APFO/pl solution and Algoflon weight is 500mg. Correct concentration only if weighed APFO differs from nominal 100mg more that + / - 10% (namely less than 90mg or more than 110mg) . 11 Procedures 11 .1 Weigh about 500mg (l g if sintered) Algoflon in a lOml vial 11 .2 Record weight and label vial with sample ID 11 .3 Prepare S20ppmsolution and label accordingly 11 .4 At roomtemperature, add 2ml of methanol containing 1 % Sulphuric acid. 11 .5 Close carefully the vial with a PTFE capped septum . 11 .6 AllowAPFOesterification at 70°C over night. 11 .7 At roomtemperature add l ml of CFC 113, centrifuge then transfer 2 ml of clear solution in a lOml vial . 11 .8 Wash out acidic methanol with 4m1 water . Close vial and allow phases separation at 40°C for 15 minutes. 11 .9 Using a syringe take out the aqueous layer. Wash a second time with 4ml water. Close vial and allowphases separation at 40°C for 15 minutes. 11 .10 At roomtemperature, inject 1 pl of lower liquid layer. Analyse using method PF 89/110 GC E. 12 Data analysis and calculations Calculate actual concentration of APFO, or other applicable compounds, from calibration line using an external standard method. Correct data calculated from calibration line only if the amount of polymer used differ from 500mg by a quote higher than +/- 5%

using the formula: Conppm = Calppm * (Trueamt/500) Where: Conppm= Concentration in ppmof surfactant corrected for polymer weight Calppm= Concentration in ppmof surfactant fromcalibration line Trueamt = Weight in mg of polymer used PF 89/110 POW

E Page 4 of 5usimonT : :.,= .

13 Method performances Method detection limit is 4ppmAPFOin Algoflon. Method quantitation limit is l Oppm . For sintered Algoflon method detection limit is 2ppm APFO . Method quantitation limit is 6ppm . Precision and accuracy are calculated from data of calibration line; precision is percent standard deviation at each point, accuracy is percent ratio of average calculated amount to nominal concentration at each point. Recovery is percent ratio of average area of matrix spike to average area of Sl Oppmcalibration point. 14 Pollution prevention and waste management Samples in CFC are disposed in dedicated container . Samples in water / methanol are disposed in dedicated container Solid polymer residuals are disposed in dedicated container Disposable glass vials are disposed in broken glass containers located in laboratory. 15 Records None

PF 89/110 POW

E Page 5 of 5

# Appendix C



# Draft Facility Report on Emissions

October 2010 NaPFO NONCBI



# Company Sanitized

## 2010/15 PFOA Stewardship Program



# Draft Facility Report on Emissions

I . CHEMICAL IDENTIFICATION Identify the chemical for which you are submitting information:

Chemical name: SodiumPerfluoroctanooate CAS number : 335-95-5

II . COMPANY IDENTIFICATION Identify the company and location of the facility submitting information:

Company name: SOLVAY SOLEXIS, INC . Site location: THOROFARE, NJ Identify a company technical contact who can respond to inquiries about the information submitted: Technical contact : VIRGINIA HUBERT

Phone: (713)525- 6051 Address: 10 LEONARD LANE

THOROFARE. NJ

### III . ON-SITE ACTIVITIES

Calendar year for which you are reporting: Jan 1, 2009 to Dec 31, 2009 Provide the amount ofchemical identified above for the reporting year at specific site:

Imported (virgin) 0 kgs/yr Imported (externally recycled) 0 kgs/yr Manufactured 0 kgs/yr Estimate the amount of subject chemical distributed off-site:

0 %

of manufacture/import Provide the amount used (including any that was manufactured, imported [virgin or externally recycled], or internally recycled) of the subject chemical for the reporting year at specific site: 0 kgs/yr Narrative Description and Process FlowSchematic: Provide overall material balance of the chemical being reported, showing releases and products (kgs/year) . Use the following page to provide a narrative description and process flow

schematic ofon-site activities, and include information that gives an understanding of the nature and extent ofpotential exposures to the subject chemical . Attach additional pages if desired. The narrative and process flow schematic should cover major unit operations and chemical conversions for manufacturing and on-site uses, if applicable. The narrative should provide insight into why and how releases are caused by the process. The schematic should show the points of release of the subject chemical in the workplace and to the environment. In the event the subject chemical is used in many different processes, provide information on each major process instead ofeach individual process.

### Narrative Description and Process Flow Schematic: 

## Solexis ceased use of NaPFOin 2003. IV. SITE RELEASE ANDTRANSFER INFORMATION (For manufacturing and on-site processing/use if applicable) In this section, estimate the total media-specific releases after on-site treatment of the chemical from

your facility. You may estimate the releases by using monitoring data or any other method you believe appropriate. Estimates should be reported in kgs per year for the reporting period. Enter the values as whole numbers to no more than two significant figures. For example, ifyour annual releases are estimated to be 12,360 kgs, an estimate of 12,000 kgs should be reported. Estimate the number ofdays per year the release occurs . Enter a whole number with a maximum

of 2 significant figures. Insert "NA" for release activities not associated with the chemical or "0" for releases of less than 0

.5 kgs per year . For all releases, the source ofdata and/or basis for determination should be described in detail . Suggested information about the possible sources/basis includes : 1 . If the source/basis is an analytical measurement, then " Describe the method (including analytical standards used, sampling, sample treatment, analysis) . " Describe the uncertainties and assumptions made. " Give the Level of Detection (LOD)/Level of Quantification (LOQ) . 2. If the source/basis is a mass balance, then " Show

the mass balance calculation . " Show

that the mass balance closes. " If the mass balance does not close, then report the fraction of total feedstock that is not accounted for and the assumptions you made to correct the balance. Describe the uncertainties. 3. If the source/basis is other than measurement or mass balance, then " Describe the method used. For example, if engineering calculations are used, give a general description and state your assumptions. Describe the uncertainties.

### Part IV (cont.)

A . ON-SITE AIR RELEASES Estimate the total fugitive or non-point releases to air and the number ofdays per year the releases occur. These releases include equipment leaks from valves, pump seals, flanges, compressors, sampling connections, and open-ended lines; evaporative losses fromsurface impoundments and spills ; releases frombuilding ventilation systems; and, any other fugitive or non-point air emission. In addition, estimate the total releases that occur through stacks, vents, pipes, or other confined air streams as stack or point source releases. Include storage tank emissions and releases frompollution control equipment. If desired, you can provide estimates of the accuracies ofyour release estimates. Estimated Total Estimated % # Days/year Annual Releases Accuracy Release Occurs (kgs) (Optional) 

### Fugitive (non-point) 0 0 Stack (point) 0 0

Basis for each release estimate: (See discussion on source/basis in beginning of Section IV.)

Comments : (This section is available to clarify your responses. Attach additional pages if desired.)

### Part IV (cont.) B . WATER RELEASES FROM SITE N/A Estimate the total releases of the chemical leaving the fence line ofyour facility fromall discharge points to all streams or water bodies. Include all discharges from process outfalls such as pipes, open trenches, releases fromon-site wastewater treatment, and contribution fromstorm water runoff, if applicable. Do not include discharges to a POTW or other off-site wastewater treatment facilities . If desired, you can provide an estimate of the accuracy ofyour release estimate. Estimated Total Estimated % # Days/year Annual Releases Accuracy Release Occurs (lcgs) (Optional) 

### Water releases: 0 p Enter the names of the streams or water bodies to which the facility directly discharges the chemical . Also, enter the NPDES permit number for the facility. If more than one number is assigned to the facility, list each number for the appropriate discharge quantity and receiving water identified. Receiving Water Name(s) : NPDES number(s) :

Basis for each release estimate: (See discussion on source/basis in beginning ofSection IV.)

Comments: (This section is available to clarify your responses. Attach additional pages if desired.)

### Part IV (cont.) C . ON-SITE LAND RELEASES N/A Estimate the total releases of the chemical for each category of land disposal, if applicable. Estimate only on-site releases. Do not estimate leaks fromlandfills separately. This should be accounted for in your estimate of total landfill release. Releases to land treatment/land amendment include all waste containing the chemical that is applied or incorporated into soil on-site. Do not include waste that is landfilled . Surface impoundments are natural topographic depressions, man-made excavations, or diked areas formed primarily of earthen materials designed to hold an accumulation of the chemical . Underground injection is the technology ofplacing fluids underground, in porous formations of rocks, through wells or other similar conveyance systems. Other releases include any amount of the chemical that is released to land other than those listed. An example is the accidental release ofthe chemical froman underground pipeline or storage tank. Estimated Total Estimated % Annual Releases Accuracy (kgs) (Optional) 

### Landfill 0 0 Land Treatment/Land Amendment 0 0 Surface Impoundments 0 0 Underground Injection 0 0 Other (specify) : 0 0 Basis for each release estimate: (See discussion on source/basis in beginning ofSection IV.) Comments : (This section is available to clarify your responses. Attach additional pages if desired.)

### Part IV (cont.) D . OFF-SITE TRANSFERS Estimates ofoff-site transfers should be similar in accuracy and precision to previous release estimates.

DI . Transfer to Publicly Owned Treatment Works (POTW) Number ofdays/year the release occurs : - 0 Estimate the total quantity of the subject chemical , not the waste stream, transferred to the POTW . Complete section below for each POTW

to which your facility discharges wastewater containing the chemical . Enter the POTW's NPDES permit number, if known. Annual Transfer (kgs) : 0 Estimated %

Accuracy of Transfer Estimate (optional) POTW Name:_ Street Address: City: - County: - State: _ Zip Code: NJPDES number:

Basis for each release estimate: (See discussion on source/basis in beginning ofSection IV.)

D2 . Transfers to other off-site locations In this section, estimate the quantity ofthe subject chemical , not the waste stream, transferred and the accuracy of the estimate for each category listed. Ifyour facility sends

### the subject chemical in waste to an off-site location where some ofthe chemical will be

recycled and the remainder will be treated, estimate each amount separately (i .e., waste treatment and recycling activities) . Estimated Annual Estimated % Transfers (kgs) accuracy (Optional) 

### Incineration 0 Wastewater Treatment (Excluding POTW) 0 Underground Injection 0 Hazardous Waste (RCRA Subtitle C) Landfill 0 

### Other Landfill 0 Recycle or Recovery 0 (Does not include internally recycled) Internally Recycled 0 Unknown or Other 0

Basis for each release estimate:

Comments :

# Appendix D



# Draft Facility 

# Rep

# ort on Product Content

t~JT'~1F/~-D l0 ,l,/4 k) M

t

Company Sanitized

## 2010/15 PFOA Stewardship Program



# Draft Facility Report on Product Content

I . CHEMICAL IDENTIFICATION Identify the product (e.g fluoropolymer dispersion) for which you are submitting information:

Product name: FLUOROPOLYMER Product description (including concentrations of perfluoroalkyl chemicals identified in Section IV below and year ofproduction) : ZERONAPFO CAS number: 335-95-5

Pm 0 

### II . COMPANY IDENTIFICATION Identify the company and location of the facility submitting information:

Company name: SOLVAY SOLEXIS, INC Site location: THOROFARE, NJ Identify a company technical contact whocan respond to inquiries about the information submitted: Technical contact: VIRGINIA HUBERT

Phone: 713 525-6051 Address: 10 Leonard Lane, Tho rofare, NJ III . PRODUCTION Calendar year for which you are reporting: Jan 1, 2008 to Dec 31, 2008 

# Ceased use of NAPFOin 2003 Provide the amount of the product for the reporting year at each specific site:

Imported 0 kgs/yr Manufactured 0 kgs/yr

### IV. PRODUCT CONTENT

A . CONCENTRATIONS OF RELEVANT PERFLUOROALKYL CHEMICALS Please provide the concentrations (ppb) ofvarious perfluoroalkyl chemicals in your product. For chemicals for which you do not have actual data, please provide range estimates. The following is a nonexhaustive list ofchemicals that should be included: PFOA and its salts " Octanoic acid, pentadecafluoro- (CAS 335-67-1) " Octanoic acid, pentadecafluoro- ammonium salt (CAS 3825-26-1) PFOA precursors " Octane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7, 8,8-heptadecafluoro-8-iodo- (CAS 507-63-1) " 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7) " 1-Decene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 21652-58-4) " 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 27905-45-9) " 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 1996-88-9) " 2-Decenoic acid, 3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-hexadecafluoro- (CAS 70887-84-2) " Decanoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 27854-31-5) Higher homologues " Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-pentacosafluoro-12-iodo- (CAS 307-60-8) " Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-10-iodo- (CAS 423-62- 1) " Nonanoic acid, heptadecafluoro- (CAS 375-95-1) " Decanoic acid, nonadecafluoro- (CAS 335-76-2) " 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7) " Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluoro-10-iodo- (CAS 2043-53-0) " Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-l2-iodo- (CAS 2043-54-1) " 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 4980-53-4) " 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12- heneicosafluorododecyl ester (CAS 17741-60-5) Part IV (cont .)

### B

. ANALYTICAL METHODS

Comments:

# Appendix F



# Draft Company Annual Report : Summary of Reductions in Emissions and Product Content



# October 2010 NONCBI

Company Sanitizedp. 59

O

CC V 

## O a O N 

### C

V O

.O

., ., 

# w

.

. V

. .



### O 

## w 

# A 0

0 N

~. U O U 

## 0

W d 

# H 0 

## a a 

# z 0 U I

z



## x 0

to

) 

### d 00 W 0-4 to 

### - E W A M 2 

### O 

# z 0 U 

## w x

T~- 

## 0° ~zw a0~ ~oo

N 

### o U s-U~ '~ U O o O ~ v 

### o v U ~U-+ a+ U O O v b4 bA Q 

# o ~~ .~ x z o

~ C", N ~ rn c .-+

~ ° L1 ° ~; o o 0 a` ~ ~ o o N y v 0 ~ b ~ O O O b4 p

O N U M ~ ~ .~ 

# z z z t~j O



# . 0 

# o N ~n v '-' U

"" O

Q O °

~C O ~ O 

### V ~ O o a °° o a ° o ° U ,. U

### 

Q U U U U v , .C, v 

### o a :~ a a : a~ o o w Q~ . U 4 y U 'C

. ~ o :-



## ~ ° 

## o z a V V 

## U w M M M~. o °' ~ "o s o E- p" 

# z >

= b " L ,

. ° ~' o N _ ~,`~' N ~ Q . a \ `+--~ ~ b + + M >, w o~ U p . r . ° °~ O w a0 s ~ a> 3 " U ? °o N ~ o

o ~, ~

~ c ~, ° ai

~ O H O~ ~ Ri . M N

h v~ '~ ~ .cn a~ -t.3 °o o " ~ ~ ~ 3 5,

~ °

° ir" y v O 'b z' U ~ °' ra o 1~1 O +- o ° o o° 3~ a ~ i '-" `L' ° ~ O . O» 0 '4 °' 3 ° v o ° v

r . O

~ ^'

y cctsn +- U 0 ~ G

. A" a" ~ ~ o ° o ~

:5 

### U ~ ~ .," Qw"'o o ~ O'b o ~ U 

### w ~ ~ a w

a ~ ~ 

### a ' . . ~ ° b

o 

### a .~ 4 0 0 o C

p ~' 'U O U .o 

### a a O 

### ~w z~ a p. 60

dn 00 0 o *~ .g 

# 0 E L5 

# n C s I c c o 00 M . cc U 

# ° ° ¬

b0 w `1 " ~ Q O N ~ snw ,r : =0

. . . 0 O U Q 0 I to 0 . .- 0 O Y y n b x bA a; cn C q w b

L o `~ 7 L. ~ T3 I x ° ~, LC

O = .o O Y F~ U O o .~ ~ y C

.~ .-. N ^ i-' `~ O cC N = ' RS

. . ~ y U ~ y W)

ca u ° .J°w L n ° a' c0 U Q - ' ao c a~ E c o ~ x ° ° ~ c ~ E °' ¢ o Y . °~ . ~ ^o ~ ~ °' m E ~ ~o c '~ 3 E '~ ° a ' 3 cz M C V I U , 'b ~ oq Y o a, ~ ~ U vi O a~ ~ ~ a o . o . ' Y N X ° ° E ~ n ~ o .b -o -o -o

U ~ ~ 7

O O O ~ .3 l~ C O E°' .J° In V) V)

- - ° s o° ~ ~ > > >

o ~Qo U :c s 's r.c. ~ o ~ F- F- F-

-, U 3., Q C' In = M

. O

# Appendix E



# Draft Company Report : Summary of Baseline Emissions and Product Content

October 2010 

# NONCBI

Company SanitizedV V 

## 00 e C% cl W~



# .

# 2 . a 5 ""' 

## 0 0 

# O o . . r-M 4000 

### N O

U 

# A 0 

# 0 N N O U 

### 0



# H A 

# a a 

# z O 

### U 

## w I

00



## Lo °' W 

# 0

Cd 

### 0 ~g 0 

### 'REn 0 0 . 

### w 0-0 

# z A 

# z a V C) 

### O N

O U 

### w 0 H IiC l

~ U O 

# ~zQ 0 cd N 0 0 

# W z O Qw dW 0 N b ~A ~" O U "p ~ U ~ N ° O O O .~', N bA bA ~ ~_ p 

### w~ d d d d d d -d 

# w z z z z z z ~o ~

O N ~ O ~ M O ++ U 0 : ~ O .~ 4 U « ! C,~ ., . ~ ~ O ~

~ L ^' " 3-'r U 

### ~' ° ~ on d o d d d d o 

# ' o x z o z z z z ~ .p o z r ~ 0

o , o .Y 0 0 ~ U ~ Q, U ; 

# ~ ° .C



### 3 

# z z z z p A .

~ N 

# z O 

### ° p r n ~ y ~ p w 

### Ey o d ~ d ~ ~ ~ ~ ' N ~ O _O O _O ' ~ ~ o O Q' ° a ° o ,,~ ., 

### O'~ ~ ~ °' o U

~ 

### ~ r a~ V ~ .~ ~ .~ ~ ~ ~ ~ s~ -° ~ A 

### w a ~ x ~? a w a ., x ~? a 

### o 

# o ~ ° ~~ o ° ~ a~ ~, ... ~ a

C/1 O 

### ° O ~ z a d ~ H U U M w M M t /1p. 63



### 79 .° ` a " a',^~, a~ ~ p ~ -o ° ~ a ' 0 0 ° " b 

# z z o z z ~ o N O 0 M L

N M ~m N ~, 42

~ . Q ~ ~ ¢3 O C~

O `~ ~ ~o f .~. V c~ O v ~ O U s. pp"

", O ~.~+ > p o 

# ~ o z z ~ o ° o &n p U s.. '~C M ~

. p, " b~A

~ Vi Q 

### :-a b Q ; E o 0 .2, ° ~ 3 o a U 0 o 0

~. o o n,

°3 

### E 0 ~ ~ y cd w o w 

# o z z ~ ~ O Q }'~ ^ cu ~ ~ O .. c w a ~ U p ~ O ~ lz Q 73 a .~ o o >~

a .~ m

o " Q 5 O ~ L O w O 

### a ~ ~ . b Q Q Q " ~ Q tA C/1 VI ^t3 o ^c7 o ¢, '" ~ ~ ' '"

o ~ c`~

n~ 'L7 o 

### a a O ~ ~.". z ~



# - a a . O 

# T 1 IT 'IT I on °o

- o 0 E =o n 'Lo,

. . c t' t I >' o °o c'' ~ ^ U 

# ° ° ¬ I bp,~ 0 . a o O o .~ '.; '

o O U p 0 I L (~ O ~ U

Y n >> 'd X O ~ y ~ w ~ c

L o `n 7 L ~ 'C I x ~ Y c a . o o O p " -O +L-' >

~ o

_ ~a c>r^ M N 'V CC UU ~ N

. " ~ N O ~ ~ th ~ an °n x ° . .° 4 . ° ~ 0 3 o ~ o Q

., ~ U ,...

0 I ,~ o Y O o 0 .~ ~ '~oA'X O, cz. ^ o a~ Lt °' cd E o . ~o U .~ 3 E'~ .r o ,_ ° a~ _ ~ ~ 't7 N ~n "~ 4" ` cn o a"

y v~, r~n r~n U V1 O w 'O ~" L L L a~ a . n" a w ~O L ~ ~ X X X U G) N N b~fl A jo- C 7 a~ 3 t~ c a, o s .o .o U) w° o A .L on Q- ~ x c . c ".r ~ ~ o s o v c ~ o E > > > o a~ c n,~ooU o =F~-HH

.n bA O . "C