## Instructions **for completing the Fuel Material Analysis Information** 

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific**  **boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  **Data for multiple boilers should be handled by using separate spreadsheets.** Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

## Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **This spreadsheet is intended to be used for one boiler of one facility**  **but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th**  **is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units of

### EIA

**Facility Code Facility Name**  **Boiler ID Fuel Type 1**  PR5 San Juan Plant SJ 10 

## No.6 Fuel Oil (residual or bunker C)

### Fuel Type 2 **Fuel Type 3 Other Fuel Description**  

## No.6 Fuel Oil (residual or bunker C)

### EIA

**Facility Code Facility Name**  **Boiler ID Basis**  **An alyte**  

## PR5 San Juan Plant SJ 10 As Received Higher Heating Value 

## PR5 San Juan Plant SJ 10 As Received % Moisture 

## PR5 San Juan Plant SJ 10 As Received % Ash 

## PR5 San Juan Plant SJ 10 As Received % Sulfur 

## PR5 San Juan Plant SJ 10 Dry basis Higher Heating Value 

## PR5 San Juan Plant SJ 10 Dry basis % Ash 

## PR5 San Juan Plant SJ 10 Dry basis % Sulfur 

## PR5 San Juan Plant SJ 10 Dry basis Antim ony 

## PR5 San Juan Plant SJ 10 Dry basis Arsenic 

## PR5 San Juan Plant SJ 10 Dry basis Bery llium 

## PR5 San Juan Plant SJ 10 Dry basis Cadmium 

## PR5 San Juan Plant SJ 10 Dry basis Chlorine 

## PR5 San Juan Plant SJ 10 Dry basis Chromium 

## PR5 San Juan Plant SJ 10 Dry basis Cobalt 

## PR5 San Juan Plant SJ 10 Dry basis Fluorine 

## PR5 San Juan Plant SJ 10 Dry basis Lead 

## PR5 San Juan Plant SJ 10 Dry basis Manganese 

## PR5 San Juan Plant SJ 10 Dry basis Mercury 

## PR5 San Juan Plant SJ 10 Dry basis Nickel 

## PR5 San Juan Plant SJ 10 Dry basis Selenium

### An **alysis M ethod for each A**  **nalyte**

**(example: A STM D5865-04)**  

## ASTM D4809 ASTM E1064 ASTM D5142 ASTM D4239 ASTM D4809 ASTM D5142 ASTM D4239 6010B 6010B 6010B 6010B 6010B 6010B 6010B 6010B 6010B 6010B 7471A 6010B 6010B**EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## PR5 San Juan Plant SJ 10

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating Value**  **(HHV) (as received)**  **HHV Units** 

### SJ-10 Oct 18 

## 10/18/2010 10/22/2010 18453.00 Btu/lb SJ-10 Oct 22 

## 10/18/2010 10/22/2010 18407.00 Btu/lb **Fuel Testing Results % Moisture** 

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)**  

## 0.01 0.26 0.455 18453.00 Btu/lb 0.26 0.455 0.01 0.23 0.456 18407.00 Btu/lb 0.23 0.456**Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)**  

## ND mg/Kg 0.073 mg/Kg ND mg/Kg ND mg/Kg ND ND mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg ND**Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units** 

## mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg**Nickel (Dry**

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture** 

## 9.3 mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg 0.01 ND mg/Kg ND mg/Kg ND mg/Kg ND mg/Kg 0.01 **Proximate A naly** 

**ses, % by**

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur** 

## 93.55 0.26 6.19 88.19 10.58 0.34 0.455 93.64 0.23 6.13 87.89 10.90 0.38 0.456 **Proximate A naly** 

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt Oxy** **gen**



## 0.61 0.60**EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## PR5 San Juan Plant SJ 10

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating** 

**Value (HHV) (as received)**  **HHV Units** 

### Fuel Testing Results**% Moisture**

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)** **Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)** **Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units Nickel (Dry** 

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units** 

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Total Moisture Volatiles**  **As h**  **Fixed Carbon Carbon**  **Hy drogen**  **Nitrogen Total Sulfur** 

**Proximate A naly** 

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Oxy gen** **EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## PR5 San Juan Plant SJ 10

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date**  **(MM/DD/YYYY) Higher**  **Heating Value (HHV)**  **(as received)**  **HHV Units** 

### Fuel Testing Results**% Moisture**

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)** **Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)** **Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units Nickel (Dry** 

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture Proximate A**  **naly**

**ses, % by**

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur Oxy** **gen Proximate A**  **naly**

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt EIA** 

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## PR5 San Juan Plant SJ 10

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating**  **Value (HHV) (as received)**  **HHV Units** 

### Fuel Testing Results**% Moisture**

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)** **Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)** **Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units Nickel (Dry** 

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture Proximate A**  **naly ses, % by** 

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur Oxy** **gen Proximate A**  **naly**

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt**

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

**Fuel Units of Measure - HHV**  anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) **Units of Measure - Metals** sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add y our own unit of measure to the **orange** hightlighted cell, if necessary

.

**Units of Measure - Cl, Fl** % ppm