Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. 

to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific 

This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were 

tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted 

yellow are required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fi

automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865-04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If 

of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, ora

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results works

6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a m

3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you 

collected more.

7. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the uni

measure.
Information

nformation about chemical analyses of fuels 

, chlorine, fluorine, and metals, such as 

nd selenium. This spreadsheet is intended 

p to 4) fuel analyses at that specific boiler. 

esting for all 4 HAP surrogates were being 

Fields that are highlighted in 

down boxes, included. Gray fields are 

_Testing.xls).

ler on the Boiler Information worksheet.

fuel column of the Boiler Information 

 the Other Fuel Description column.

ethods worksheet. For example: "ASTM 

 Picklist worksheet (orange tab). If the units

le, please fill them in the blank, orange 

e in the Fuels Sample Results worksheet.

s worksheet. You must provide a minimum of 

re not limited to that number if you have 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Test Date

2554 Dunkirk Steam Generating Station4 4/19/2010
Fuel Type 1 Fuel Type 2 Fuel Type 3

subbituminous
Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

2554 Dunkirk Steam Generating Station 4 As Received Higher Heating Value

2554 Dunkirk Steam Generating Station 4 As Received % Moisture

2554 Dunkirk Steam Generating Station 4 As Received % Ash

2554 Dunkirk Steam Generating Station 4 As Received % Sulfur

2554 Dunkirk Steam Generating Station 4 Dry basis Higher Heating Value

2554 Dunkirk Steam Generating Station 4 Dry basis % Moisture

2554 Dunkirk Steam Generating Station 4 Dry basis % Ash

2554 Dunkirk Steam Generating Station 4 Dry basis % Sulfur

2554 Dunkirk Steam Generating Station 4 Dry basis Antimony

2554 Dunkirk Steam Generating Station 4 Dry basis Arsenic

2554 Dunkirk Steam Generating Station 4 Dry basis Beryllium

2554 Dunkirk Steam Generating Station 4 Dry basis Cadmium

2554 Dunkirk Steam Generating Station 4 Dry basis Chlorine

2554 Dunkirk Steam Generating Station 4 Dry basis Chromium

2554 Dunkirk Steam Generating Station 4 Dry basis Cobalt

2554 Dunkirk Steam Generating Station 4 Dry basis Fluorine

2554 Dunkirk Steam Generating Station 4 Dry basis Lead

2554 Dunkirk Steam Generating Station 4 Dry basis Manganese

2554 Dunkirk Steam Generating Station 4 Dry basis Mercury

2554 Dunkirk Steam Generating Station 4 Dry basis Nickel

2554 Dunkirk Steam Generating Station 4 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

D5865

D3302

D3174

D4239

D5865

D3302

D3174

D4239

SW6010B

SW6010B

SW6010B

SW6010B

SW6010B

SW6010B

SW6010B

SW6010B

D6722

SW6010B

SW6010B
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

2554 Dunkirk Steam Generating Station 4 M30B, M29, OTM 27/28

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

1 4/19/2010 8500.00 Btu/lb 27.8

2 4/19/2010 8470.00 Btu/lb 28.1

3 4/21/2010 8520.00 Btu/lb 27.7

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

4.75 0.21 11770 Btu/lb 0 6.58 0.29

4.75 0.21 11780 Btu/lb 0 6.61 0.29

4.96 0.2 11780 Btu/lb 0 6.86 0.28


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.185 mg/kg 2 mg/kg 1 mg/kg 1

0.056 mg/kg 2 mg/kg 1 mg/kg 1

0.073 mg/kg 2 mg/kg 1 mg/kg 1


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/kg 4.82 mg/kg 2.77 mg/kg 9.29 mg/kg 2.59 mg/kg

mg/kg 5.34 mg/kg 2.72 mg/kg 9.8 mg/kg 2.53 mg/kg

mg/kg 3.99 mg/kg 3.88 mg/kg 9.04 mg/kg 2.34 mg/kg


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

2 mg/kg mg/kg 1.57 mg/kg

2 mg/kg mg/kg 1.46 mg/kg

2 mg/kg mg/kg 1.22 mg/kg


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

2554 Dunkirk Steam Generating Station 4 M26, CTM033, 6C, 7E

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

1 4/22/2010 8530.00 Btu/lb 27.9

2 4/22/2010 8570.00 Btu/lb 27.4

3 4/22/2010 8520.00 Btu/lb 28.3

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

4.62 11830 Btu/lb 0 6.41 0.29

4.88 11800 Btu/lb 0 6.72 0.3

4.73 11880 Btu/lb 0 6.6 0.31


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

2554 Dunkirk Steam Generating Station 4 M6C, M10, M18, M0031 with SW-846, M0010, M0011, M25A

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

1 4/22/2010 8530.00 Btu/lb 27.9

2 4/22/2010 8570.00 Btu/lb 27.4

3 4/22/2010 8520.00 Btu/lb 28.3

 Fuel Testing Results


ith SW-846, M0010, M0011, M25A

% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

4.62 11830 Btu/lb 0 6.41 0.29

4.88 11800 Btu/lb 0 6.72 0.3

4.73 11880 Btu/lb 0 6.6 0.31


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

2554 Dunkirk Steam Generating Station 4

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm