Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10774 Southam pton Power Station 1 and 2 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

10774 Southampton Power Station 1 and 2 As Received Higher Heating Value 10774 Southampton Power Station 1 and 2 As Received % Moisture 10774 Southampton Power Station 1 and 2 As Received % Ash 10774 Southampton Power Station 1 and 2 As Received % Sulfur 10774 Southampton Power Station 1 and 2 Dry

basis Higher Heating Value 10774 Southampton Power Station 1 and 2 Dry

basis % Ash 10774 Southampton Power Station 1 and 2 Dry

basis % Sulfur 10774 Southampton Power Station 1 and 2 Dry

basis Antim ony 10774 Southampton Power Station 1 and 2 Dry

basis Arsenic 10774 Southampton Power Station 1 and 2 Dry

basis Beryllium 10774 Southampton Power Station 1 and 2 Dry

basis Cadmium 10774 Southampton Power Station 1 and 2 Dry

basis Chlorine 10774 Southampton Power Station 1 and 2 Dry

basis Chromium 10774 Southampton Power Station 1 and 2 Dry

basis Cobalt 10774 Southampton Power Station 1 and 2 Dry

basis Fluorine 10774 Southampton Power Station 1 and 2 Dry

basis Lead 10774 Southampton Power Station 1 and 2 Dry

basis Manganese 10774 Southampton Power Station 1 and 2 Dry

basis Mercury 10774 Southampton Power Station 1 and 2 Dry

basis Nickel 10774 Southampton Power Station 1 and 2 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D2015 ASTM D-3173 ASTM D-3174 ASTM D 4239 ASTM D2015 ASTM D-3174 ASTM D 4239 SW 846 7041 SW 846 7060A SW 846 6010B SW 846 6010B ASTM D4208 SW 846 6010B SW 846 6010B ASTM D3761 SW 846 6010B SW 846 6010B EPA 7473 SW 846 6010B SW 846 7740EIA Facility Code Facility Name Boiler ID 10774 Southampton Power Station 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) U1/2 Coal-027/028-1 4/26/2010 4/26/2010 12876.00 U1/2 Coal-M29-1 4/26/2010 4/26/2010 12871.00 U1/2 Coal-027/028-2 4/27/2010 4/27/2010 12821.00 U1/2 Coal-M29-2 4/27/2010 4/27/2010 13017.00 U1/2 Coal-027/028-3 4/27/2010 4/27/2010 12641.00 U1/2 Coal-M29-3 4/27/2010 4/27/2010 12603.00 Fuel Testing ResultsHAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 4.16 9.37 0.89 13400 Btu/lb 4.49 9.48 0.93 13500 Btu/lb 4.37 9.79 0.91 13400 Btu/lb 5.01 9.87 0.92 13700 Btu/lb 5.03 10.32 0.93 13300 Btu/lb 5.71 9.95 0.91 13400HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Btu/lb 9.77 0.93 1182 ppm 0.112 ppm Btu/lb 9.92 0.97 1242 ppm 0.145 ppm Btu/lb 10.24 0.95 1297 ppm 0.115 ppm Btu/lb 10.39 0.97 1300 ppm 0.138 ppm Btu/lb 10.86 0.98 1262 ppm 0.15 ppm Btu/lb 10.55 0.96 1238 ppm 0.128 ppmAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) < 0.50 ppm 3.03 ppm < 5.00 ppm < 1.00 ppm 21.9 < 0.50 ppm 3.59 ppm < 5.00 ppm < 1.00 ppm 22.7 < 0.50 ppm 3.72 ppm < 5.00 ppm < 1.00 ppm 22.7 1.33 ppm 3.34 ppm < 5.00 ppm < 1.00 ppm 23 < 0.50 ppm 5.39 ppm < 5.00 ppm < 1.00 ppm 23.2 < 0.50 ppm 3.3 ppm < 5.00 ppm < 1.00 ppm 23.7Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units ppm 17.9 ppm 12.1 ppm 21.7 ppm 4.74 ppm ppm 5.43 ppm 15.2 ppm 23.4 ppm 4.75 ppm ppm 6.95 ppm 67.8 ppm 22.8 ppm 4.65 ppm ppm 7.25 ppm 8.59 ppm 24 ppm 4.19 ppm ppm 6.84 ppm 13.7 ppm 23.4 ppm 4.22 ppm ppm 8.31 ppm 10.8 ppm 23.8 ppm 4.08 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 48.9 ppm 13 ppm 2.85 9.77 78.66 52.5 ppm 14.6 ppm 3.3 9.48 78.77 52.1 ppm 13.8 ppm 3.15 10.24 79 50.5 ppm 14 ppm 3.8 10.39 79.3 57.5 ppm 14.1 ppm 3.85 10.86 77.65 56.9 ppm 13.4 ppm 4.4 10.55 75.94 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

78.66 5.17 1.66 0.93 3.8 78.77 5.39 1.59 0.97 3.36 79 5.08 1.47 0.95 3.26 79.3 5.18 1.46 0.97 2.7 77.65 4.95 1.59 0.98 3.96 75.94 5.25 1.41 0.96 5.88 Ultimate Analy

ses, % by

wtEIA Facility Code Facility

Name Boiler ID 10774 Southampton Power Station 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) U1/2 Coal-M26A-1 4/29/2010 4/29/2010 12223.00 U1/2 Coal-M26A-2 4/29/2010 4/29/2010 12091.00 U1/2 Coal-M26A-3 4/29/2010 4/29/2010 12423.00 Fuel Testing ResultsHAPs Test Group

Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 6.22 11.66 0.94 13000 Btu/lb 6.79 12 0.91 13000 Btu/lb 5.66 11.34 1.03 13200HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Btu/lb 12.43 1 1436 ppm 0.108 ppm Btu/lb 12.88 0.97 1281 ppm 0.101 ppm Btu/lb 12.02 1.09 1256 ppm 0.159 ppmAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 0.74 ppm 3.6 ppm < 5.00 ppm < 1.00 ppm 25.5 1.01 ppm 4.08 ppm < 5.00 ppm < 1.00 ppm 25.9 < 0.50 ppm 6.18 ppm < 5.00 ppm < 1.00 ppm 25Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units ppm 8.24 ppm 9.81 ppm 20.5 ppm 3.94 ppm ppm 6.21 ppm 14.4 ppm 22 ppm 5.34 ppm ppm 10.1 ppm 8.6 ppm 20.2 ppm 5.77 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 68.8 ppm 12.9 ppm 5 12.43 76.18 74.7 ppm 12 ppm 5.55 12.88 75.29 64.2 ppm 11.9 ppm 4.45 12.02 76.78 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 76.18 5.02 1.38 1 3.99 75.29 5.03 1.35 0.97 4.49 76.78 4.9 1.35 1.09 3.78

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 10774 Southampton Power Station 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) U1/2 Coal-M10/11-1 4/28/2010 4/28/2010 12477.00 U1/2 Coal-M10/11-2 4/28/2010 4/28/2010 12542.00 U1/2 Coal-M10/11-3 4/28/2010 4/28/2010 12392.00 Fuel Testing ResultsHAPs Test Group

Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 5.77 10.45 0.94 13200 Btu/lb 6.18 9.89 0.94 13400 Btu/lb 6.13 11.2 0.93 13200HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Btu/lb 11.09 0.99 1266 ppm 0.159 ppm Btu/lb 10.55 1 1274 ppm 0.132 ppm Btu/lb 11.93 0.99 1249 ppm 0.139 ppmAn timony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 1.41 ppm 4.06 ppm < 5.00 ppm < 1.00 ppm 23.1 1.45 ppm 4.35 ppm < 5.00 ppm < 1.00 ppm 23.9 5.29 ppm 4.45 ppm < 5.00 ppm < 1.00 ppm 23.6Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units ppm 6.76 ppm 11.1 ppm 22.4 ppm 4.22 ppm ppm 10.4 ppm 13.1 ppm 24.7 ppm 5.52 ppm ppm 7.72 ppm 9.99 ppm 22.7 ppm 5.29 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon 63.8 ppm 13.6 ppm 4.55 11.09 76.99 76.99 60.7 ppm 14.5 ppm 4.95 10.55 78.11 78.11 68.5 ppm 13.6 ppm 4.95 11.93 76.95 76.95 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 4.94 1.38 0.99 4.61 4.77 1.4 1 3.65 5.1 1.38 0.99 3.65 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10774 Southampton Power Station 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm