**Instructions for using the Emission Test Reporting Template for the Primary Aluminum Test Program**

This Information Collection Request (ICR) spreadsheet is intended to be used to report emissions data from primary aluminum reduction facilities as an alternative to the Electronic Reporting Tool (ERT), as well as in cases where the test methods arenot currently supported by the ERT.**Data for multiple process units should be reported by using separate copies of the appropriate tabs of this spreadsheet.** **Please Do Not delete rows or columns , addition of rows and columns is appropriate**  **as necessary.**
**Emission Data Worksheets** The emission data worksheets are provided for each test required for this testing program, although all facilities are not required to conduct all of the tests. On each worksheet,please enter process unit operating informationduring sampling and emission test results. The emission test results to be entered depends on the constituent. **Source Operating Information** 1. Please provide the Exhaust Flow Rate (acfm and dscfm) and the Exhaust Temperature (deg F). 2. Please provide the values of all requested parametersfor each of the sample testing periods in the appropriate cells. 3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

# Primary Aluminum Testing: Filterable Particulate Matter

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**Roof 2 Duct

**Test Method Used (e.g. Method 5)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

1 4/22/2013 14:37 4/22/2013 17:50 Method 5 ADL 2 4/23/2013 8:23 4/23/2013 18:05 Method 5 ADL 3 4/26/2013 10:04 4/26/2013 13:18 Method 5 ADL

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 0.9 0.0 20.5 102 2 2.1 0.0 20.5 92.1 3 1.1 0.0 20.8 78.2

**lb/hr lb/ton of** 

**throughput Ma** **terial Rate (ton/hr)** 

1 191 18.5 Aluminum 10.3 2 131 12.7 Aluminum 10.3 3 33.1 3.21 Aluminum 10.3 **Run Number** **Calculated Emission Rate Production or Throughput**  8,919,066 7,990,026 **Filterable Particulate Emission Test Results**
**Concentration (ug/dscm)** 
7.38 4.39 0.991

**Exhaust Gas Other Supporting Information**  **Test End Date**  **Test End**

**Time**

**Flow (dscfm) 1** 

6,896,792 **Run Number**  **Run Number** **Test Start**

**Date Test Start** 

**Time**1Total Roof flow data (dscfm) provided by Noranda Aluminum, Inc.

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:**391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**Pollutant Concentration**  **(ug/dscm) Test Method Used** 

**(e.g. Method 29) Data Flag** 

**(A DL, BDL, DLL)**  **Test Method Comments**
1 Antimony 2 Antimony 3 Antimony 1 Arsenic 2 Arsenic 3 Arsenic 1 Beryllium 2 Beryllium 3 Beryllium 1 Cadmium 2 Cadmium 3 Cadmium 1 Chromium 2 Chromium 3 Chromium 1 Cobalt 2 Cobalt 3 Cobalt 1 Lead 2 Lead 3 Lead 1 Manganese 2 Manganese 3 Manganese 1 Nickel 2 Nickel 3 Nickel 1 Selenium 2 Selenium 3 Selenium 1 Mercury 2 Mercury 3 Mercury **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Filterable Particulate Emission Test Results** 

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:**391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**lb/hr lb/ton of** 

**throughput Material**  **Rate (tons/hour)** **Moisture**

**(%) CO** **2**

**(%) O** **2**

**(%) Flow** 

**(acfm) Flow** 

**(dscfm) Temp** 

**( °F)**  1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 **Other Supporting Information Calculated Emission Rate** **Production or Throughput Exhaust Gas**  **Run Number** 

# Primary Aluminum Testing: Hexavalent Chromium

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Test Method Used (SW-846 M0061)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 2 3

**lb/hr lb/ton of**  **throughput Ma** **terial Rate**  **(tons/hour)** 1 2 3 **Run Number** **Calculated Emission Rate Production or Throughput**  **Run Number**  **Exhaust Gas Other Supporting Information**  **Flow (dscfm) Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Hexavalent Chromium Emission Test Results** 

**Concentration (ug/dscm)** 

# Primary Aluminum Testing: PM and POM as MCEM
**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Rate (tons/hour)** 1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 2 3

**lb/hr lb/ton of**  **throughput Pollutant**  **Conc (ug/dscm)**  **Test Method Used (e.g. Method 315)**  PM POM as MCEM PM POM as MCEM PM POM as MCEM 1

2

3 **Production or Throughput**

**Data Flag (A** **DL, BDL, DLL) Particulate Matter and POM as MCEM Emission Test Results** 
**Test Method Comments Run**  **Number Run**  **Number Exhaust Gas** 

**Calculated Emission Rate Other Supporting Information**  **Flow (dscfm) Run**  **Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Ma** **terial**

### Page 1 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:**  391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Roof 2 Duct

**lb/hr lb/ton**  **Throughput** 1 4/22/2013 14:37 4/22/2013 17:50 1.65E-03 1.59E-04 10.3 2 4/23/2013 8:23 4/23/2013 18:05 3.12E-03 3.02E-04 10.3 3 4/26/2013 10:04 4/26/2013 13:18 9.44E-04 9.14E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.37E-04 1.32E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 1.05E-04 1.02E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.74E-04 1.68E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.36E-04 1.32E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 1.91E-04 1.85E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.09E-04 1.06E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 4.88E-05 4.72E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 4.41E-05 4.26E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 2.79E-04 2.70E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 4.85E-05 4.70E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 4.30E-05 4.16E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 6.22E-05 6.02E-06 10.3 1 4/22/2013 14:37 4/22/2013 17:50 2.43E-04 2.35E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 1.21E-04 1.17E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 3.56E-04 3.45E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 6.33E-04 6.13E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 2.28E-04 2.20E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.00E-03 9.70E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.02E-04 9.92E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 5.88E-05 5.69E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.21E-04 1.17E-05 10.3 Acenaphthene (83-32-9) **Test Start Time**  **Test End**

**Date Test End** 

**Time Calculated Emission Rate** **Throughput (ton/hr)**  **Compound Run**  **Number Test Start** 

**Date**

Anthracene (120-12-7)

Benz[a]anthracene (56-55-3)

Benzo[a]pyrene (50-32-8)

Benzo(e)pyrene (192-97-2)

Benzo[b]fluoranthene (205-99-2)

Benzo[g,h,i]perylene (191-24-2) Acenaphthylene (208-96-8)

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Test Start**  **Time Test End** 

**Date Test End** 

**Time Calculated Emission Rate** **Throughput (ton/hr)**  **Compound Run**  **Number Test Start** 

**Date**

1 4/22/2013 14:37 4/22/2013 17:50 1.30E-04 1.26E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 4.86E-05 4.70E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.98E-04 1.92E-05 10.3 1 4/22/2013 14:37 4/22/2013 17:50 7.31E-04 7.08E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 2.57E-04 2.48E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.32E-03 1.28E-04 10.3 1 4/22/2013 14:37 4/22/2013 17:50 4.17E-05 4.04E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 5.49E-05 5.31E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 7.45E-05 7.21E-06 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.63E-03 1.57E-04 10.3 2 4/23/2013 8:23 4/23/2013 18:05 9.79E-04 9.48E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 2.67E-03 2.58E-04 10.3 1 4/22/2013 14:37 4/22/2013 17:50 7.24E-04 7.01E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 1.25E-03 1.21E-04 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.93E-03 1.87E-04 10.3 1 4/22/2013 14:37 4/22/2013 17:50 7.04E-05 6.81E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 5.27E-05 5.10E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 9.19E-05 8.90E-06 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.97E-02 1.91E-03 10.3 2 4/23/2013 8:23 4/23/2013 18:05 2.26E-02 2.19E-03 10.3 3 4/26/2013 10:04 4/26/2013 13:18 3.87E-02 3.75E-03 10.3 1 4/22/2013 14:37 4/22/2013 17:50 2.83E-03 2.74E-04 10.3 2 4/23/2013 8:23 4/23/2013 18:05 2.89E-03 2.80E-04 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.55E-03 1.50E-04 10.3 1 4/22/2013 14:37 4/22/2013 17:50 1.83E-03 1.77E-04 10.3 2 4/23/2013 8:23 4/23/2013 18:05 2.39E-03 2.31E-04 10.3 3 4/26/2013 10:04 4/26/2013 13:18 1.49E-03 1.44E-04 10.3 1 4/22/2013 14:37 4/22/2013 17:50 4.24E-05 4.10E-06 10.3 2 4/23/2013 8:23 4/23/2013 18:05 3.63E-05 3.52E-06 10.3 3 4/26/2013 10:04 4/26/2013 13:18 4.97E-05 4.81E-06 10.3 1 4/22/2013 14:37 4/22/2013 17:50 3.23E-04 3.13E-05 10.3 2 4/23/2013 8:23 4/23/2013 18:05 3.43E-04 3.32E-05 10.3 3 4/26/2013 10:04 4/26/2013 13:18 4.02E-04 3.89E-05 10.3 Benzo[k]fluoranthene (207-08-9)

Chrysene (218-01-9)

Naphthalene (91-20-3)

2-Methylnaphthalene (91-57-6)

Phenanthrene (85-01-8)

Perylene (198-55-0) Dibenz[a,h]anthracene (53-70-3)

Fluoranthene (206-44-0)

Fluorene (86-73-7)

Indeno (1,2,3-cd) pyrene (193-39-5)

Pyrene (129-00-0)

### Page 3 of 8



# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

391 St. Jude Industrial Park**Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Roof 2 Duct

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** Aluminum 1 2.41E+02 Dry CARB 429 ADL Aluminum 2 4.21E+02 Dry CARB 429 ADL Aluminum 3 1.14E+02 Dry CARB 429 ADL Aluminum 1 2.00E+01 Dry CARB 429 BDL Aluminum 2 1.42E+01 Dry CARB 429 BDL Aluminum 3 2.10E+01 Dry CARB 429 BDL Aluminum 1 1.99E+01 Dry CARB 429 ADL Aluminum 2 2.57E+01 Dry CARB 429 ADL Aluminum 3 1.32E+01 Dry CARB 429 ADL Aluminum 1 7.14E+00 Dry CARB 429 ADL Aluminum 2 5.94E+00 Dry CARB 429 ADL Aluminum 3 3.37E+01 Dry CARB 429 ADL Aluminum 1 7.10E+00 Dry CARB 429 BDL Aluminum 2 5.80E+00 Dry CARB 429 BDL Aluminum 3 7.51E+00 Dry CARB 429 BDL Aluminum 1 3.56E+01 Dry CARB 429 ADL Aluminum 2 1.63E+01 Dry CARB 429 ADL Aluminum 3 4.30E+01 Dry CARB 429 ADL Aluminum 1 9.26E+01 Dry CARB 429 ADL Aluminum 2 3.07E+01 Dry CARB 429 ADL Aluminum 3 1.21E+02 Dry CARB 429 ADL Aluminum 1 1.50E+01 Dry CARB 429 ADL Aluminum 2 7.93E+00 Dry CARB 429 ADL Aluminum 3 1.46E+01 Dry CARB 429 ADL

**Compound Run** 

**Number Throughput**  **Ma terial** 

Benzo(e) pyrene

Ace naphthene

Ace naphthylene

Anthracene

Benz[a] anthracene
Benzo[a] pyrene

Benzo[b] fluoranthene
Benzo[g,h,i]peryle ne **Polycyclic A romatic Hydrocarbons Emission Test Results** 

### Page 4 of 8

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** **Compound Run** 

**Number Throughput**  **Ma terial**  **Polycyclic A romatic Hydrocarbons Emission Test Results** 

Aluminum 1 1.90E+01 Dry CARB 429 ADL Aluminum 2 6.55E+00 Dry CARB 429 ADL Aluminum 3 2.39E+01 Dry CARB 429 ADL Aluminum 1 1.07E+02 Dry CARB 429 ADL Aluminum 2 3.46E+01 Dry CARB 429 ADL Aluminum 3 1.60E+02 Dry CARB 429 ADL Aluminum 1 6.10E+00 Dry CARB 429 ADL Aluminum 2 7.40E+00 Dry CARB 429 ADL Aluminum 3 9.00E+00 Dry CARB 429 ADL Aluminum 1 2.38E+02 Dry CARB 429 ADL Aluminum 2 1.32E+02 Dry CARB 429 ADL Aluminum 3 3.22E+02 Dry CARB 429 ADL Aluminum 1 1.06E+02 Dry CARB 429 ADL Aluminum 2 1.68E+02 Dry CARB 429 ADL Aluminum 3 2.33E+02 Dry CARB 429 ADL Aluminum 1 1.03E+01 Dry CARB 429 ADL Aluminum 2 7.10E+00 Dry CARB 429 ADL Aluminum 3 1.11E+01 Dry CARB 429 ADL Aluminum 1 2.88E+03 Dry CARB 429 ADL Aluminum 2 3.05E+03 Dry CARB 429 ADL Aluminum 3 4.68E+03 Dry CARB 429 ADL Aluminum 1 4.15E+02 Dry CARB 429 ADL Aluminum 2 3.90E+02 Dry CARB 429 ADL Aluminum 3 1.87E+02 Dry CARB 429 ADL Aluminum 1 2.68E+02 Dry CARB 429 ADL Aluminum 2 3.22E+02 Dry CARB 429 ADL Aluminum 3 1.80E+02 Dry CARB 429 ADL Aluminum 1 6.20E+00 Dry CARB 429 BDL Aluminum 2 4.90E+00 Dry CARB 429 BDL Aluminum 3 6.00E+00 Dry CARB 429 BDL Aluminum 1 4.73E+01 Dry CARB 429 ADL Aluminum 2 4.62E+01 Dry CARB 429 ADL Aluminum 3 4.85E+01 Dry CARB 429 ADL

* Contains particulate filter, front half of filter holder and probe solvent rinses *** Contains condensate, impinger contents and glassware solvent rinses ** Contains XAD-2 resin tube, back half of filter holder and coil condenser solvent rinses Benzo[k] fluoranthene
Chrysene

Phenan threne

Perylene Dibenz[a,h] anthracene

Fluoranthene

Fluorene
Indeno (1,2,3-cd) pyrene

Pyrene Naphthalene
2-Methyl naphthalene

### Page 5 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Roof 2 Duct

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) 1**  **Temperature**

**( °F)**  2.41E+02 1 0.9 0.0 20.7 6,896,792 102 4.21E+02 2 1.4 0.0 20.5 7,990,026 92.1 1.14E+02 3 1.1 0.0 20.8 8,919,066 78.6 2.00E+01 1 0.9 0.0 20.7 6,896,792 102 1.42E+01 2 1.4 0.0 20.5 7,990,026 92.1 2.10E+01 3 1.1 0.0 20.8 8,919,066 78.6 1.99E+01 1 0.9 0.0 20.7 6,896,792 102 2.57E+01 2 1.4 0.0 20.5 7,990,026 92.1 1.32E+01 3 1.1 0.0 20.8 8,919,066 78.6 7.14E+00 1 0.9 0.0 20.7 6,896,792 102 5.94E+00 2 1.4 0.0 20.5 7,990,026 92.1 3.37E+01 3 1.1 0.0 20.8 8,919,066 78.6 7.10E+00 1 0.9 0.0 20.7 6,896,792 102 5.80E+00 2 1.4 0.0 20.5 7,990,026 92.1 7.51E+00 3 1.1 0.0 20.8 8,919,066 78.6 3.56E+01 1 0.9 0.0 20.7 6,896,792 102 1.63E+01 2 1.4 0.0 20.5 7,990,026 92.1 4.30E+01 3 1.1 0.0 20.8 8,919,066 78.6 9.26E+01 1 0.9 0.0 20.7 6,896,792 102 3.07E+01 2 1.4 0.0 20.5 7,990,026 92.1 1.21E+02 3 1.1 0.0 20.8 8,919,066 78.6 1.50E+01 1 0.9 0.0 20.7 6,896,792 102 7.93E+00 2 1.4 0.0 20.5 7,990,026 92.1 1.46E+01 3 1.1 0.0 20.8 8,919,066 78.6 Benzo(e)pyrene **Exhaust Gas Compound**  **Run**

**Number**

Acenaphthene

Acenaphthylene

Anthracene

Benzo[b] fluoranthene
Benzo[g,h,i] perylene Benz[a] anthracene
Benzo[a]pyrene

### Page 6 of 8

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) 1**  **Temperature**

**( °F)**  **Exhaust Gas Compound**  **Run**

**Number**

1.90E+01 1 0.9 0.0 20.7 6,896,792 102 6.55E+00 2 1.4 0.0 20.5 7,990,026 92.1 2.39E+01 3 1.1 0.0 20.8 8,919,066 78.6 1.07E+02 1 0.9 0.0 20.7 6,896,792 102 3.46E+01 2 1.4 0.0 20.5 7,990,026 92.1 1.60E+02 3 1.1 0.0 20.8 8,919,066 78.6 6.10E+00 1 0.9 0.0 20.7 6,896,792 102 7.40E+00 2 1.4 0.0 20.5 7,990,026 92.1 9.00E+00 3 1.1 0.0 20.8 8,919,066 78.6 2.38E+02 1 0.9 0.0 20.7 6,896,792 102 1.32E+02 2 1.4 0.0 20.5 7,990,026 92.1 3.22E+02 3 1.1 0.0 20.8 8,919,066 78.6 1.06E+02 1 0.9 0.0 20.7 6,896,792 102 1.68E+02 2 1.4 0.0 20.5 7,990,026 92.1 2.33E+02 3 1.1 0.0 20.8 8,919,066 78.6 1.03E+01 1 0.9 0.0 20.7 6,896,792 102 7.10E+00 2 1.4 0.0 20.5 7,990,026 92.1 1.11E+01 3 1.1 0.0 20.8 8,919,066 78.6 2.88E+03 1 0.9 0.0 20.7 6,896,792 102 3.05E+03 2 1.4 0.0 20.5 7,990,026 92.1 4.68E+03 3 1.1 0.0 20.8 8,919,066 78.6 4.15E+02 1 0.9 0.0 20.7 6,896,792 102 3.90E+02 2 1.4 0.0 20.5 7,990,026 92.1 1.87E+02 3 1.1 0.0 20.8 8,919,066 78.6 2.68E+02 1 0.9 0.0 20.7 6,896,792 102 3.22E+02 2 1.4 0.0 20.5 7,990,026 92.1 1.80E+02 3 1.1 0.0 20.8 8,919,066 78.6 6.20E+00 1 0.9 0.0 20.7 6,896,792 102 4.90E+00 2 1.4 0.0 20.5 7,990,026 92.1 6.00E+00 3 1.1 0.0 20.8 8,919,066 78.6 4.73E+01 1 0.9 0.0 20.7 6,896,792 102 4.62E+01 2 1.4 0.0 20.5 7,990,026 92.1 4.85E+01 3 1.1 0.0 20.8 8,919,066 78.6 *** Contains condensate, impinger contents and glassware solvent rinses 1Total Roof flow data (dscfm) provided by Noranda Aluminum, Inc. Benzo[k] fluoranthene
Chrysene
Dibenz[a,h] anthracene

Fluoranthene

Pyrene Fluorene
Indeno (1,2,3-cd) pyrene
Naphthalene
2-Methyl naphthalene

Phenanthrene

Perylene

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**

### Page 1 of 8 

# Primary Aluminum Testing: Dioxins and Furans

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**Roof 2 Duct

**lb/hr lb/ton**  **Throughput** 1 4/22/2013 14:37 4/22/2013 17:50 1.18E-09 1.14E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.04E-09 1.01E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 4.47E-10 4.33E-11 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 5.53E-10 5.36E-11 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 8.90E-10 8.62E-11 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 3.23E-10 3.13E-11 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 2.87E-10 2.78E-11 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 3.53E-10 3.42E-11 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.90E-10 2.81E-11 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.98E-09 1.92E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.63E-09 1.58E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 5.22E-10 5.05E-11 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.78E-09 1.72E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.85E-09 1.79E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.24E-09 1.20E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 2.05E-09 1.98E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.96E-09 1.90E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.10E-09 2.04E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.91E-09 1.85E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 3.04E-09 2.94E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.90E-09 1.84E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 2.39E-09 2.32E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 2.52E-09 2.44E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.00E-09 1.94E-10 10.3 Aluminum **Test Start Time**  **Test End**

**Date Test End** 

**Time**

1,2,3,4,6,7,8- HpCDD **Throughput (ton/hr)**  **Compound Run** 

**Number Test Start** 

**Date**

1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF
1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF
1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF
1,2,3,7,8,9- HxCDD **Calculated Emission Rate Throughput**  **Ma terial** 

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Test Start**  **Time Test End** 

**Date Test End** 

**Time Throughput**  **(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Calculated Emission Rate**  **Throughput Ma** **terial**

1 4/22/2013 14:37 4/22/2013 17:50 2.05E-09 1.98E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.56E-09 1.51E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.41E-09 1.36E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 2.08E-08 2.01E-09 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.24E-08 1.20E-09 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 3.18E-12 3.07E-13 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 6.35E-10 6.15E-11 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.22E-09 1.18E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.10E-09 1.06E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 2.19E-09 2.12E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.56E-09 1.51E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.24E-09 2.16E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 3.48E-09 3.37E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 7.57E-09 7.32E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 4.47E-09 4.33E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.57E-08 1.52E-09 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.48E-08 1.44E-09 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.49E-08 1.44E-09 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.37E-09 1.32E-10 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 3.34E-09 3.23E-10 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 9.11E-09 8.82E-10 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 8.30E-11 8.04E-12 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 8.10E-11 7.84E-12 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.48E-11 2.40E-12 10.3 Aluminum 1 4/22/2013 14:37 4/22/2013 17:50 1.74E-11 1.69E-12 10.3 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.98E-11 1.92E-12 10.3 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.90E-11 1.84E-12 10.3 Aluminum 1,2,3,7,8,9- HxCDF

1,2,3,7,8- PeCDF
2,3,4,6,7,8- HxCDF 1,2,3,7,8- PeCDD

2,3,4,7,8- PeCDF

OCDF OCDD 2,3,7,8- TCDD

2,3,7,8-TCDF

### Page 3 of 8 

# Primary Aluminum Testing: Dioxins and Furans

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park New Madrid, MO 63869 New Madrid, MO 63869 **Description of source tested:**Roof 2 Duct

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** 1 1.72E-02 Dry CARB 428 ADL 2 1.40E-02 Dry CARB 428 BDL 3 5.40E-03 Dry CARB 428 BDL 1 8.10E-03 Dry CARB 428 BDL 2 1.20E-02 Dry CARB 428 BDL 3 3.90E-03 Dry CARB 428 BDL 1 4.20E-03 Dry CARB 428 BDL 2 4.76E-03 Dry CARB 428 ADL 3 3.50E-03 Dry CARB 428 BDL 1 2.90E-03 Dry CARB 428 BDL 2 2.20E-03 Dry CARB 428 BDL 3 6.30E-04 Dry CARB 428 BDL 1 2.60E-03 Dry CARB 428 BDL 2 2.50E-03 Dry CARB 428 BDL 3 1.50E-03 Dry CARB 428 BDL 1 3.00E-03 Dry CARB 428 BDL 2 2.64E-03 Dry CARB 428 ADL 3 2.54E-03 Dry CARB 428 ADL 1 2.80E-03 Dry CARB 428 BDL 2 4.10E-03 Dry CARB 428 BDL 3 2.30E-03 Dry CARB 428 BDL 1 3.50E-03 Dry CARB 428 BDL 2 3.40E-03 Dry CARB 428 BDL 3 2.42E-03 Dry CARB 428 ADL **Run Number**  **Dioxins and Furans Emission Test Results**

1,2,3,4,6,7,8- HpCDD **Test Method Comments Compound** 

1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF
1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF
1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF
1,2,3,7,8,9- HxCDD **Separate A nalysis** 

### Page 4 of 8

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** **Run Number**  **Dioxins and Furans Emission Test Results**

**Test Method Comments Compound**  **Separate A nalysis** 

1 3.00E-03 Dry CARB 428 BDL 2 2.10E-03 Dry CARB 428 BDL 3 1.70E-03 Dry CARB 428 BDL 1 2.80E-03 Dry CARB 428 BDL 2 1.50E-03 Dry CARB 428 BDL 3 2.40E-03 Dry CARB 428 BDL 1 3.10E-03 Dry CARB 428 BDL 2 5.47E-03 Dry CARB 428 ADL 3 4.42E-03 Dry CARB 428 ADL 1 3.20E-03 Dry CARB 428 BDL 2 2.10E-03 Dry CARB 428 BDL 3 2.70E-03 Dry CARB 428 BDL 1 1.70E-03 Dry CARB 428 BDL 2 3.40E-03 Dry CARB 428 BDL 3 1.80E-03 Dry CARB 428 BDL 1 2.30E-03 Dry CARB 428 BDL 2 2.00E-03 Dry CARB 428 BDL 3 1.80E-03 Dry CARB 428 BDL 1 2.00E-03 Dry CARB 428 BDL 2 4.50E-03 Dry CARB 428 BDL 3 1.10E-02 Dry CARB 428 BDL 1 4.05E-02 Dry CARB 428 ADL 2 3.64E-02 Dry CARB 428 ADL 3 1.00E-02 Dry CARB 428 BDL 1 8.50E-03 Dry CARB 428 BDL 2 8.90E-03 Dry CARB 428 BDL 3 7.65E-03 Dry CARB 428 ADL * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses 1,2,3,7,8,9- HxCDF

1,2,3,7,8- PeCDF
2,3,4,6,7,8- HxCDF
2,3,4,7,8- PeCDF

OCDF 2,3,7,8- TCDD

2,3,7,8-TCDF

OCDD 1,2,3,7,8- PeCDD

### Page 5 of 8 

# Primary Aluminum Testing: Dioxins and Furans

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** Roof 2 Duct

**Composite A nalysis** 
**Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) 1**  **Temperature**

**( °F)**  1.72E-02 1.72E-02 1 0.9 0.0 20.7 6,900,000 102 1.40E-02 1.40E-02 2 1.4 0.0 20.5 7,990,000 92.1 5.40E-03 5.40E-03 3 1.1 0.0 20.8 8,920,000 78.6 8.10E-03 8.10E-03 1 0.9 0.0 20.7 6,900,000 102 1.20E-02 1.20E-02 2 1.4 0.0 20.5 7,990,000 92.1 3.90E-03 3.90E-03 3 1.1 0.0 20.8 8,920,000 78.6 4.20E-03 4.20E-03 1 0.9 0.0 20.7 6,900,000 102 4.76E-03 4.76E-03 2 1.4 0.0 20.5 7,990,000 92.1 3.50E-03 3.50E-03 3 1.1 0.0 20.8 8,920,000 78.6 2.90E-03 2.90E-03 1 0.9 0.0 20.7 6,900,000 102 2.20E-03 2.20E-03 2 1.4 0.0 20.5 7,990,000 92.1 6.30E-04 6.30E-04 3 1.1 0.0 20.8 8,920,000 78.6 2.60E-03 2.60E-03 1 0.9 0.0 20.7 6,900,000 102 2.50E-03 2.50E-03 2 1.4 0.0 20.5 7,990,000 92.1 1.50E-03 1.50E-03 3 1.1 0.0 20.8 8,920,000 78.6 3.00E-03 3.00E-03 1 0.9 0.0 20.7 6,900,000 102 2.64E-03 2.64E-03 2 1.4 0.0 20.5 7,990,000 92.1 2.54E-03 2.54E-03 3 1.1 0.0 20.8 8,920,000 78.6 2.80E-03 2.80E-03 1 0.9 0.0 20.7 6,900,000 102 4.10E-03 4.10E-03 2 1.4 0.0 20.5 7,990,000 92.1 2.30E-03 2.30E-03 3 1.1 0.0 20.8 8,920,000 78.6 3.50E-03 3.50E-03 1 0.9 0.0 20.7 6,900,000 102 3.40E-03 3.40E-03 2 1.4 0.0 20.5 7,990,000 92.1 2.42E-03 2.42E-03 3 1.1 0.0 20.8 8,920,000 78.6 **Exhaust Gas**
**Run Number** 

1,2,3,4,6,7,8- HpCDD **Compound**

1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF
1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF
1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF
1,2,3,7,8,9- HxCDD

### Page 6 of 8

**Composite A nalysis** 
**Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) 1**  **Temperature**

**( °F)**  **Exhaust Gas**
**Run Number**  **Compound**

3.00E-03 3.00E-03 1 0.9 0.0 20.7 6,900,000 102 2.10E-03 2.10E-03 2 1.4 0.0 20.5 7,990,000 92.1 1.70E-03 1.70E-03 3 1.1 0.0 20.8 8,920,000 78.6 2.80E-03 2.80E-03 1 0.9 0.0 20.7 6,900,000 102 1.50E-03 1.50E-03 2 1.4 0.0 20.5 7,990,000 92.1 2.40E-03 2.40E-03 3 1.1 0.0 20.8 8,920,000 78.6 3.10E-03 3.10E-03 1 0.9 0.0 20.7 6,900,000 102 5.47E-03 5.47E-03 2 1.4 0.0 20.5 7,990,000 92.1 4.42E-03 4.42E-03 3 1.1 0.0 20.8 8,920,000 78.6 3.20E-03 3.20E-03 1 0.9 0.0 20.7 6,900,000 102 2.10E-03 2.10E-03 2 1.4 0.0 20.5 7,990,000 92.1 2.70E-03 2.70E-03 3 1.1 0.0 20.8 8,920,000 78.6 1.70E-03 1.70E-03 1 0.9 0.0 20.7 6,900,000 102 3.40E-03 3.40E-03 2 1.4 0.0 20.5 7,990,000 92.1 1.80E-03 1.80E-03 3 1.1 0.0 20.8 8,920,000 78.6 2.30E-03 2.30E-03 1 0.9 0.0 20.7 6,900,000 102 2.00E-03 2.00E-03 2 1.4 0.0 20.5 7,990,000 92.1 1.80E-03 1.80E-03 3 1.1 0.0 20.8 8,920,000 78.6 2.00E-03 2.00E-03 1 0.9 0.0 20.7 6,900,000 102 4.50E-03 4.50E-03 2 1.4 0.0 20.5 7,990,000 92.1 1.10E-02 1.10E-02 3 1.1 0.0 20.8 8,920,000 78.6 4.05E-02 4.05E-02 1 0.9 0.0 20.7 6,900,000 102 3.64E-02 3.64E-02 2 1.4 0.0 20.5 7,990,000 92.1 1.00E-02 1.00E-02 3 1.1 0.0 20.8 8,920,000 78.6 8.50E-03 8.50E-03 1 0.9 0.0 20.7 6,900,000 102 8.90E-03 8.90E-03 2 1.4 0.0 20.5 7,990,000 92.1 7.65E-03 7.65E-03 3 1.1 0.0 20.8 8,920,000 78.6 1Total Roof flow data (dscfm) provided by Noranda Aluminum, Inc. 1,2,3,7,8,9- HxCDF

1,2,3,7,8-PeCDD

1,2,3,7,8-PeCDF

2,3,4,6,7,8- HxCDF

OCDF OCDD 2,3,7,8-TCDD

2,3,7,8-TCDF 2,3,4,7,8-PeCDF

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**Page 1 of 4 

## Primary Aluminum Testing: Polychlorinate Biphenyls (PCB)
**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** Roof 2 Duct

**lb/hr lb/ton**  **Throughput** 1 4/22/2013 14:374/22/2013 17:50 1.71E-06 1.65E-07 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 3.78E-06 3.66E-07 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 4.72E-06 4.57E-07 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 1.50E-05 1.46E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 2.23E-05 2.15E-06 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.32E-05 1.28E-06 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 1.09E-05 1.05E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 2.37E-05 2.29E-06 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 9.85E-06 9.54E-07 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 1.56E-05 1.51E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 4.52E-05 4.37E-06 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.48E-05 2.40E-06 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 4.41E-05 4.27E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.60E-05 1.55E-06 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.65E-06 2.56E-07 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 6.83E-05 6.61E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.26E-05 1.22E-06 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 2.57E-06 2.48E-07 10.33 Aluminum **Calculated Emission Rate**  **Throughput**

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Test Method Comments** 

Monochlorinated biphenyls **Throughput Material** 

Dichlorinated biphenyls

Trichlorinated biphenyls

Tetrachlorinated biphenyls

Pentachlorinated biphenyls

Hexachlorinated biphenylsPage 2 of 4

**lb/hr lb/ton** 

**Throughput Calculated Emission**  **Rate Throughput** 

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Test Method Comments**  **Throughput Material** 

1 4/22/2013 14:374/22/2013 17:50 5.40E-05 5.23E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 4.82E-06 4.67E-07 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 4.88E-07 4.73E-08 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 1.43E-05 1.39E-06 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 3.63E-07 3.52E-08 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 3.56E-07 3.45E-08 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 1.30E-06 1.26E-07 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 9.64E-08 9.33E-09 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 9.93E-08 9.62E-09 10.33 Aluminum 1 4/22/2013 14:374/22/2013 17:50 5.47E-08 5.29E-09 10.33 Aluminum 2 4/23/2013 8:23 4/23/2013 18:05 1.04E-07 1.01E-08 10.33 Aluminum 3 4/26/2013 10:04 4/26/2013 13:18 1.41E-07 1.36E-08 10.33 Aluminum Heptachlorinated biphenyls

Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenylsPage 3 of 4

**Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) 1**  **Temperature**

**( °F)**  0.25 0.25 1 0.9 0 20.7 6,896,792 102 0.51 0.51 2 1.4 0 20.5 7,990,026 92.1 0.57 0.57 3 1.1 0 20.8 8,919,066 78.6 2.2 2.2 1 0.9 0 20.7 6,896,792 102 3 3 2 1.4 0 20.5 7,990,026 92.1 1.6 1.6 3 1.1 0 20.8 8,919,066 78.6 1.59 1.59 1 0.9 0 20.7 6,896,792 102 3.19 3.19 2 1.4 0 20.5 7,990,026 92.1 1.19 1.19 3 1.1 0 20.8 8,919,066 78.6 2.29 2.29 1 0.9 0 20.7 6,896,792 102 6.09 6.09 2 1.4 0 20.5 7,990,026 92.1 2.99 2.99 3 1.1 0 20.8 8,919,066 78.6 6.46 6.46 1 0.9 0 20.7 6,896,792 102 2.16 2.16 2 1.4 0 20.5 7,990,026 92.1 0.32 0.32 3 1.1 0 20.8 8,919,066 78.6 10 10 1 0.9 0 20.7 6,896,792 102 1.7 1.7 2 1.4 0 20.5 7,990,026 92.1 0.31 0.31 3 1.1 0 20.8 8,919,066 78.6 Pentachlorinated biphenyls

Hexachlorinated biphenyls Monochlorinated biphenyls

Dichlorinated biphenyls **Other Supporting Information**

**Separate Analy**

**sis**

Monochlorinated biphenyls **Poly chlorinated Bipheny** **ls Emission Test Results**
**Compound Run**  **Number Exhaust Gas** 

Dichlorinated biphenyls

Trichlorinated biphenyls Trichlorinated biphenyls

Tetrachlorinated biphenyls

Pentachlorinated biphenyls Tetrachlorinated biphenyls

Hexachlorinated biphenylsPage 4 of 4

**Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) 1**  **Temperature**

**( °F)**  **Other Supporting Information Separate Analy** 

**sis Poly** **chlorinated Bipheny ls Emission Test Results** 
**Compound Run**  **Number Exhaust Gas** 

7.9 7.9 1 0.9 0 20.7 6,896,792 102 0.65 0.65 2 1.4 0 20.5 7,990,026 92.1 0.1 0.1 3 1.1 0 20.8 8,919,066 78.6 2.1 2.1 1 0.9 0 20.7 6,896,792 102 0.0 0.0 2 1.4 0 20.5 7,990,026 92.1 0.0 0.0 3 1.1 0 20.8 8,919,066 78.6 0.19 0.19 1 0.9 0 20.7 6,896,792 102 0.0 0.0 2 1.4 0 20.5 7,990,026 92.1 0.0 0.0 3 1.1 0 20.8 8,919,066 78.6 0.01 0.01 1 0.9 0 20.7 6,896,792 102 0.0 0.0 2 1.4 0 20.5 7,990,026 92.1 0.0 0.0 3 1.1 0 20.8 8,919,066 78.6 Nonachlorinated biphenyls Heptachlorinated biphenyls

Octachlorinated biphenyls Heptachlorinated biphenyls

Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenyls

Decachlorinated biphenyls

# Primary Aluminum Testing: Exhaust flow rates, temperatures, and O2/CO2 contents

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**Roof 2 Duct

**Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm)** 1 4/22/13 14:37 4/22/13 17:50 Methods 1-4 Method 5 0.9 0.0 20.5 1,852 1,728 2 4/23/13 8:23 4/23/13 18:05 Methods 1-4 Method 5 2.1 0.0 20.5 1,878 1,760 3 4/26/13 10:04 4/26/13 13:18 Methods 1-4 Method 5 1.1 0.0 20.8 1,872 1,811 1 4/22/13 14:37 4/22/13 17:50 Methods 1-4 CARB 428/429 0.9 0.0 20.7 1,440 1,343 2 4/23/13 8:23 4/23/13 18:05 Methods 1-4 CARB 428/429 1.4 0.0 20.5 1,496 1,411 3 4/26/13 10:04 4/26/13 13:18 Methods 1-4 CARB 428/429 1.1 0.0 20.8 1,483 1,433 **Test Start Date**  **Run Number**  **Exhaust Gas Simultaneous**  **with which pollutant test?**  **Test Method (e.g. Method 5)**  **Test End Time**  **Test End Date**  **Test Start Time** 

### 391 St. Jude Industrial Park

**Temp ( °F)**  102 92.1 78.2 102 92.1 78.6