Based on information and belief formed 

after reasonable inquiry, I certify that the 

statements and information in this test 

report are true, accurate, and complete. 

Permitted Facility Representative 

Name: 

Title: 

Company: 

Sign Date: 

Connie O'Neal 

EHS Administrator 

Florim USA 

Monday, June 20, 2011 

Date 

6/20/2011 

I have reviewed all testing details and 

results in this test report and hereby 

certify that the test report is authentic 

and accurate. 

Name: 

Title: 

Company: 

Sign Date: 

Troy Burrows 

Corporate Quality Manager 

Entec Services, Inc. 

6/20/2011 

Page 1 of 39 
Pho 

Fax 

Em 

ne: 

931-553-7510 

Contact:II-J

_

s

_

u

_

tt

_

on ___________ 

11 

Phone: 205-358-101 i 

Fax: 1205-358-1036 I 

ail: cjames@florimusa.com Email: sutton@entecservices.com J 

-

lndustry/SCC/NAIS f._ _____ __, AFS#: FRS#: 

Air Permit Number: Permitted Source 10/Name: 

1562538 llr-F-lo-n-.m- U- SA- , I-n-c.---- -

Permitted Maximum Process Rate: Max. Normal Operation Process Rate: Target Process Test Rate 

L I 

SCC I Description l30500812 J Industrial Processes -Mineral Products - Ceramic Clay/Tile Manufacture - Glazing 

and firing kiln** (use sees 3-05-008-45 & -50) 

The following state and federal regulations that apply to the proposed testing: 

Description of the source (including control equipment). Please see the attachments for source or 

process flow diagram: 

Spray Dryer No.2- SACMI Model ATM052, Control Equipment- Venturi Wet Scrubber 

Vertical Dryer No. 1 - EVA Model 984, no control device 

Glaze Line (GL-1)- Control Equipment -Eurofilter Dust Collector 

Glaze Line (GL- 3, 4, 5)- Control Equipment- Venturi Wet Scrubber 

Roller Kiln No. 1 - SACMI Model JMS223, Control Equipment- Eurofilter Dry Sorbent Injection Baghouse 

Sampling Location Information: 

Round 

Duct Rect.Duct Equiv. Distance-from Distance from Number of Min Trave~:s Location Diaru. Lengtb JWidth Diam upstteam dlst. downstream dist. Traverse Ports Points 

Glaze Line j 35.5 0 0 () 384 168 2 24 

(GL- 3, 4, 5) 

Glaze Line 41.5 0 0 0 240 114 2 20 

(GL -1) 

- - -

-

Roller Kiln 43.25 0 0 0 86.5 216 2 24 

No.1 May 

Spray Dryer 44 0 0 0 84 110 2 24 

No.2 

Vertical Dryer 19 0 0 0 39 -f=J,o, 2 24 No. I - Roller Kiln #I 43.25 0 0 0 86.5 2 24 

October 

------- -- - - ---

Monday, June 20, 2011 Page 2 of 39 
Glaze Line Antimony Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Beryllium Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Cadmium Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Chromium Method 29 3 240 0 

(GL- 3, 4, 5) --

Glaze Line Cobalt Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Lead Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Manganese Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Nickel Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Mercury Method 29 3 240 0 

(GL- 3, 4, 5) 

Glaze Line Filterable Particulate Method 5 3 240 0 

(GL- 3, 4, 5) -

Glaze Line !Nickel Method 29 3 240 0 

(GL - 1) 

Glaze Line Mercury Method 29 3 240 0 

(GL -1) 

Glaze Line Lead Method 29 3 240 0 

(GL -1) - -

Glaze Line Chromium Method 29 3 240 0 

(GL -1) 

Glaze Line Manganese Method 29 3 240 0 

(GL -1) - - IGlaze Line Cobalt Method 29 3 240 0 ~ 

(GL -1) 

---

Glaze Line Cadmium Method 29 3 240 0 

(GL-1) 

Glaze Line Arsenic Method 29 3 240 0 

(GL -1) 

Glaze Line Antimony Method 29 3 240 0 

(GL -1) -

Glaze Line Beryllium Method 29 3 240 0 

(GL -1) -

Glaze Line Selenium Method 29 3 240 0 

(GL-1 ) 

1-

Glaze Line Filterable 

Particulate Method 5 3 240 0 

(GL -1) -'--

----1- -- -- - - -

Roller Kiln # l 2,3,7,8-TCDD Method 23 3 240 0 

October I 

Roller Kiln #I 1 ,2,3, 7 ,8-PeCDD Method 23 3 240 1 0 October --

--

-- - - --

Monday, June 20, 2011 Page 3 of 39 
Roller Kiln #1 OCDD 

October 

Roller Kiln #I 2,3,7,8-TCDF 

October 

Roller Kiln #1 1,2,3,7,8-PeCDF 

October 

Roller Kiln #1 2,3,4,7,8-PeCDF 

October 

Roller Kiln #1 I ,2,3,4,7,8-HxCDF 

October 

Roller Kiln #I 1,2,3,6,7,8-HxCDF 

October 

Roller Kiln #1 2,3,4,6,7,8-HxCDF 

October 

Roller Kiln #I 1,2,3,7,8,9-HxCDF 

October 

Roller Kiln #I 1,2,3,4,6,7,8-HpCDF 

October 

Roller Kiln #1 1,2,3,4,7,8,9-HpCDF 

October 

Roller Kiln #1 OCDF 

October 

Roller Kiln #1 Total Dioxins 

October 

Roller Kiln #1 frotal Furans 

October 

Roller Kiln 2,3,7,8-TCDD 

No.1 May 

Roller Kiln I ,2,3, 7 ,8-PeCDD 

No.1 May 

Roller Kiln 

No. I May 

Roller Kiln 

No.1 May 

Roller Kiln 

No. I May 

Roller Kiln 

No.1 May 

Roller Kiln 

No.1 May 

Roller Kiln 

No. I May 

Roller Kiln 

No. I May 

Roller Kiln 

1,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 

1 ,2,3,7 ,8,9-HxCDD 

1 ,2,3,4,6, 7,8-HpCDD 

OCDD 

2,3,7,8-TCDF 

1 ,2,3, 7 ,8-PeCDF 

2,3,4, 7 ,8-PeCDF 

No. l May 

RollerKiln 

No. I May t------

I ,2,3,4,7,8-HxCDF 

Monday, June 20, 2011 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 Method 23 3 240 0 

Method 23 3 240 0 Method 23 3 240 0 Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

--1---+-------

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 L -+--2-4

_

0_-+ __ o _ __, __ _ 

Method 23-- 3 240 0 

-

Page 4 of 39 
Roller Kiln 1 ,2,3,4,7,8,9-HpCDF Method 23 3 240 0 

No.1 May 

Roller Kiln OCDF Method 23 3 240 0 

No.1 May 

- -

Roller Kiln Total Dioxins Method 23 3 240 0 

No.1 May 

Roller Kiln Total Furans Method 23 3 240 0 

No.1 May 

Roller Kiln Nickel Method 29 3 240 I 0 No.1 May 

Roller Kiln Mercury Method 29 3 240 0 

No.1 May 

Roller Kiln Antimony Method 29 3 240 0 

No.1 May 

Roller Kiln Arsenic Method 29 3 240 0 

No.1 May 

-

Roller Kiln Beryllium Method 29 3 240 0 

No. I May 

--

Roller Kiln Cadmium Method 29 3 240 0 

No.1 May 

Roller Kiln Chromium Method 29 3 240 0 

No.1 May 

Roller Kiln Cobalt Method 29 3 240 0 

No.1 May 

Roller Kiln Manganese Method 29 3 240 0 

No.1 May 

Roller Kiln Selenium Method 29 3 240 0 

No.1 May 

-

Roller Kiln Lead Method 29 3 240 0 

No.1 May 

Roller Kiln Filterable Particulate Method 5 3 240 0 

No. I May 

Spray Dryer 2,3,7,8-TCDD Method 23 3 240 0 

No.2 

Spray Dryer 1 ,2,3, 7 ,8-PeCDD Method 23 3 240 0 

No.2 

-- - -

Spray D1yer 1 ,2,3,4,7,8-HxCDD Method 23 3 240 0 

No.2 

Spray Dryer 1 ,2,3,6,7,8-HxCDD Method 23 3 240 0 

No.2 

Spray D1yer 1 ,2,3, 7 ,8,9-HxCDD Method 23 3 240 0 

No.2 

1-- -

Spray D1yer 1,2,3,4,6,7,8-HpCDD Method 23 3 240 0 

No.2 

·-

Spray D1yer OCDD Method 23 3 240 0 

No.2 

Spray D1yer 2,3,7,8-TCDF Method 23 3 240 0 

No.2 

1---

'---- - -- -

Monday, June 20,2011 Page 5 of 39 
Spray Dryer 2,3,4,6,7,8-HxCDF Method 23 3 240 0 

No.2 

Spray Dryer 1,2,3,7,8,9-HxCDF Method 23 3 240 0 

No.2 

-

Spray Dryer 1 ,2,3,4,6, 7,8-HpCDF Method 23 3 240 0 

No.2 

Spray Dryer 1 ,2,3,4, 7 ,8,9-HpCDF Method 23 3 240 0 

jNo.2 

Spray Dryer OCDF Method 23 3 240 0 

No.2 

--

Spray Dryer Total Dioxins Method 23 3 240 0 

No.2 

Spray Dtyer Total Furans Method 23 3 240 0 

No.2 

Vertical Dryer 2,3,7,8-TCDD Method 23 3 240 0 

No.1 

Vertical Dryer 1,2,3,7,8-PeCDD Method 23 3 240 0 

No.1 

Vertical Dryer 1 ,2,3,4,7 ,8-HxCDD Method 23 3 240 0 

No.1 

Vertical Dryer 1,2,3,6,7,8-HxCDD Method 23 3 240 0 

No.1 

Vertical Dryer 1,2,3,7,8,9-HxCDD Method 23 3 240 0 

No.1 

Vertical Dryer 1 ,2,3,4,6, 7,8-HpCDD Method 23 3 240 0 

No.1 

Vertical Dtyer OCDD Method 23 3 240 0 

No.1 

Vertical Dryer 2,3,7,8-TCDF Method 23 3 240 0 

No.I 

Vertical Dryer 1,2,3,7,8-PeCDF Method 23 I 3 240 0 No.1 Vertical Dryer 2,3,4,7,8-PeCDF Method 23 3 240 0 

No.1 

Vetiical Dryer 1 ,2,3,4,7,8-HxCDF Method 23 3 240 0 

No. l -

Vertical Dryer 1,2,3,6,7,8-HxCDF Method 23 3 240 0 

No.1 

--

Vetiical Dryer 2,3,4,6,7,8-HxCDF Method 23 3 240 0 

No. l 

Vertical Dryer I ,2,3,7,8,9-HxCDF Method 23 3 240 0 

No. I 

Vertical Dtyer l ,2,3,4,6, 7,8-HpCDF Method 23 3 240 0 

No. I 

Vertical Dryer 1 ,2,3,4,7,8,9-HpCDF Method 23 3 240 0 

No.1 -

Vetiical Dtyer OCDF Method 23 3 240 0 

No.1 l -- -

--- ---------

Monday, June 20, 2011 Page 6 of 39 
=-

___ _j 

Monday, June 20, 2011 Page 7 of 39 
Run Finish Time 

Net Run Time, minutes 

Dry Gas MeterVo1ume Sampled, dscf 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, op 

Dry Volumetric Flow Rate, dry scfrn 

Actual Wet Volumetric Flue Gas Flow Rate, acfrn 

Percent Isokinetic of Sampling Rate, % 

F-Factor, dscfrn/MMBtu@ %02 

Fw 

Fe 

Monday, June 20, 2011 

AM 

3:40:00 PM 

240 

160.202 

2.99 

5.22 

0 

20.8 

93.33 

12,736.3 

13,631.1 

101.6 

0 

0 

0 

AM 

12:36:00 5:55:00 PM 

PM 

240 240 

163.773 160.427 161.467 

2.71 2.99 2.897 

4.31 4.97 4.833 

0 0 0.000 

20.8 20.8 20.800 

87.04 91.63 90.667 

12,953.9 12,793.7 12,827.967 

13,726.0 13,709.5 13,688.867 

102.1 101.3 101.667 

0 0 0.000 

0 0 0.000 

0 0 0.000 

Page 8 of 39 
Run Finish Time 1:33:00 PM 6:28:00 12:15:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 147.329 153.752 157.914 152.998 

Moisture Content of Stack Gas, % 2.56 2.29 2.22 2.357 

Moisture Saturation at Stack Gas Temperature, % 6.58 6.39 5.97 6.313 

Carbon Dioxide, % 0 0 0 0.000 

Oxygen,% 20.8 20.8 20.8 20.800 

Average Stack Gas Temperature, °F 100.75 99.80 97.55 99.367 

Dry Volumetric Flow Rate, dry scfin 10,147.6 10,599.9 10,865.2 10,537.567 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 11,012.4 11,451.9 11,683.0 11,382.433 

Percent Isokinetic of Sampling Rate, % 103.7 103.6 103.8 103.700 

F-Factor, dscfm/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 9 of 39 
Run Finish Time 12:11:00 PM 5:25:00 11:49:00 

PM AM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 196.040 198.180 200.079 198.100 

Moisture Content of Stack Gas, % 6.47 6.09 6.56 6.373 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Carbon Dioxide, % 3 3 3 3.000 

Oxygen,% 18.3 18.4 18.2 18.300 

Average Stack Gas Temperature, °F 279.50 281.42 281.88 280.933 

Dry Volumetric Flow Rate, dry scfin 15,556.9 15,818.0 15,974.2 15,783.033 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 23,603.3 23,964.5 24,337.9 23,968.567 

Percent Isokinetic of Sampling Rate, % 100.9 100.3 100.3 100.500 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

-------

Monday, June 20, 2011 Page 10 of 39 
Run Finish Time 12:14:00 PM 8:31:00 12:08:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 202.228 198.290 205.746 202.088 

Moisture Content of Stack Gas, % 6.14 6.73 7.42 6.763 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Carbon Dioxide, % 2.5 2.5 2.5 2.500 

Oxygen,% 19.1 19.3 19.3 19.233 

Average Stack Gas Temperature, °F 265.00 267.67 265.92 266.197 

Dry Volumetric Flow Rate, dry scfin 16,185.7 16,241.5 16,668.3 16,365.167 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 23,560.5 23,878.8 24,637.8 24,025.700 

Percent Isokinetic of Sampling Rate, % 100.0 97.7 98.8 98.833 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20,2011 Page 11 of 39 
Run Finish Time 2:25:00 PM 8:31 :00 12:08:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 124.257 122.389 127.604 124.750 

Moisture Content of Stack Gas, % 6.13 6.98 7.56 6.890 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Carbon Dioxide, % 2.5 2.5 2.5 2.500 

Oxygen,% 19.1 19.3 19.3 19.233 

Average Stack Gas Temperature, oF 265.38 266.42 269.17 266.990 

Dry Volumetric Flow Rate, dry scfrn 15,657.8 15,473.0 15,972.1 15,700.967 

Actual Wet Volumetric Flue Gas Flow Rate, acfrn 22,801.5 22,770.9 23,750.3 23,107.567 

Percent Isokinetic of Sampling Rate, % 99.0 98.6 99.6 99.067 

F-Factor, dscfrniMMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 12 of 39 
Run Finish Time 12:11:00PM 5:43:00 12:18:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 152.146 130.996 131.978 138.373 

Moisture Content of Stack Gas, % 23.11 22.98 21.47 22.520 

Moisture Saturation at Stack Gas Temperature, % 22.41 21.30 21.02 21.577 

Carbon Dioxide, % 3 3 2.5 2.833 

Oxygen,% 18.3 18.5 18.3 18.367 

Average Stack Gas Temperature, oF 144.71 142.71 142.33 143.250 

Dry Volumetric Flow Rate, dry scfm 15,580.5 16,370.0 16,381.3 16,110.600 

Actual Wet Volumetric Flue Gas Flow Rate, acfm 23,301.6 24,049.2 23,884.5 23,745.100 

Percent Isokinetic of Sampling Rate, % 104.2 103.3 104.0 103.833 

F-Factor, dscfm!MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

l _j 

Monday, June 20, 2011 Page 13 of 39 
Run Finish Time 7:08:00 PM 1:52:00 7:04:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 172.081 178.973 175.714 175.589 

Moisture Content of Stack Gas, % 9.26 4.60 6.87 6.910 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Carbon Dioxide, % 2 2 2 2.000 

Oxygen,% 19 19 19 19.000 

Average Stack Gas Temperature, °F 237.71 239.58 238.04 238.443 

Dry Volumetric Flow Rate, dry scfin 4,127.5 4,433.7 4,277.8 4,279.667 

Actual Wet Volumetric Flue Gas Flow Rate, actin 6,059.4 6,151.5 6,066.5 6,092.467 

Percent Isokinetic of Sampling Rate, % 100.3 97.2 98.9 98.800 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 14 of 39 
Eglhr 3.62E-03 6.92E

03 2.89E

02 0.013 

mg/dscm 1.67E-04 3.20E-04 1.31E-03 0.001 

mg/dscm@7%02 2.32E-02 4.45E-02 1.82E-OI 0.083 

Compound: Arsenic 

Averal!e 

Run Number M29-2 M29-3 M29-1 

Mass_mg 0.0012 0.0012 0.00187 0.001 

Eg/hr 5.69E-03 5.74E-03 8.92E-03 0.007 

mg/dscm 2.59E-04 2.64E-04 4.12E-04 0.000 

mg/dscm@7%02 3.60E-02 3.67E-02 5.73E-02 0.043 

Compound: Beryllium 

Averal!e 

RunNumber M29-2 M29-3 M29-1 

Mass_mg 0.0003 0.0003 0.0003 0.000 

Eg/hr 1.42E-03 1.44E-03 1.43E-03 0.001 

mg/dscm 6.47E-05 6.60E-05 6.61E-05 0.000 

mg/dscm@7%02 8.99E-03 9.17E-03 9.19E-03 0.009 

Compound: Cadmium 

Averal!e 

RunNumber M29-2 M29-3 M29-1 

Mass_mg 0.00015 0.00015 0.000298 0.000 

Eglhr 7.12E-04 7.18E-04 1.42E-03 0.001 

mg/dscm 3.23E-05 3.30E-05 6.57E-05 0.000 

mg/dscm@7%02 4.49E-03 4.59E-03 9.13E-03 0.006 

Compound: Chromium 

Averal!e 

Run Number M29-2 M29-3 M29-l 

Mass_mg 0.345 0.15 0.154 0.216 

Eg/hr 1.64E+OO 7.18E-0 1 7.35E-OI 1.031 

mg/dscm 7.44E-02 3.30E-02 3.40E-02 0.047 

mg/dscm@7%02 1.03E+OI 4.59E+OO 4.73E+OO 6.540 

Compound: Cobalt 

Ave ra!!e 

Run Number M29-2 M29-3 M29-1 

Mass_mg 0.0147 0.0147 0.0175 0.016 

Eg/hr 6.98E-02 7.03E-02 8.35E-02 O.D75 

mg/dscm 3.17E-03 3.24E-03 3.86E-03 0.003 dscm 02 4.41E-Ol 4.50E-Ol 5.37E-01 0.476 

Compound: Lead 

Avera!!e 

---- ---

Monday, June 20, 2011 Page 15 of 39 
RunNumber M29-2 M29-3 M29-1 

Mass_mg 0.528 0.223 1.294 0.682 

Eg/hr 2.51E+OO 1.07E+OO 6.17E+OO 3.250 

mg/dscm 1.14E-01 4.91E-02 2.85E-01 0.149 

mg/dscm@7%02 1.58E+01 6.82E+OO 3.96E+01 20.740 

Compound: Mercury 

Avera!!e 

RunNumber M29-3 M29-1 M29-2 

Mass_mg 0.000706 0.000329 0.000375 0.000 

Eg/hr 3.38E-03 1.57E-03 1.78E-03 0.002 

mg/dscm 1.55E-04 7.25E-05 8.09E-05 0.000 

m~dscm

@7%02 

2.15E-02 l.OlE-02 1.12E-02 0.014 

Compound: Nickel 

Avera!!e 

RunNumber M29-3 M29-1 M29-2 

Mass_mg 0.00817 0.00629 0.0109 0.008 

Eg/hr 3.91E-02 3.00E-02 5.17E-02 0.040 

mg/dscm 1.80E-03 1.39E-03 2.35E-03 0.002 

mg/dscm@7%02 2.50E-01 1.93E-01 3.27E-Ol 0.257 

Compound: Selenium 

Avera!!e 

RunNumber M29-3 M29-1 M29-2 

Mass_mg 0.00311 0.00385 0.00302 0.003 

Eg/hr 1.49E-02 1.84E-02 1.43E-02 0.016 

mg/dscm 6.85E-04 8.49E-04 6.51E-04 0.001 

mg/dscm@7%02 9.52E-02 1.18E-01 9.05E-02 0.101 

Location: Glaze Line (GL -1)- Method 29 

Compound: Antimony 

Avera!!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.0003 0.0003 0.0003 0.000 

Eg/hr 1.24E-03 1.24E-03 1.24E-03 0.001 

mg/dscm 7.19E-05 6.89E-05 6.71E-05 0.000 

mg/dscm@7%02 9.99E-03 9.58E-03 9.33E-03 0.010 

Compound: Arsenic 

Avera!!e 

l Run Number M29-1 M29-2 M29-3 Mass_mg 0.0012 0.0012 0.0012 0.001 Eg/hr 4.96E-03 4.96E-03 4.95E-03 0.005 mg/dscm 2.88E-04 2.76E-04 2.68E-04 0.000 J 

Monday, June 20,2011 Page 16 of 39 
mg/dscm@7%02 9.99E-03 9.58E-03 9.33E-03 0.010 

Compound: Cadmium 

Averal!e 

RunNumber M29-l M29-2 M29-3 Mass_mg 0.00015 0.00015 0.000193 0.000 

Eg!hr 6.20E-04 6.20E-04 7.97E-04 0.001 

mg/dscm 3.60E-05 3.45E-05 4.32E-05 0.000 

5.00E-03 4.80E-03 6.00E-03 0.005 

Compound: Chromium 

Averal!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00281 0.00278 0.00191 0.003 

Eglhr 1.16E-02 1.15E-02 7.89E-03 0.010 

mg/dscm 6.74E-04 6.39E-04 4.27E-04 0.001 mg/dscm@7%02 9.37E-02 8.88E-02 5.94E-02 0.081 

Compound: Cobalt 

Averal!e 

RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0003 0.0003 0.00102 0.001 

Eglhr 1.24E-03 1.24E-03 4.21E-03 0.002 

mg/dscm 7.19E-05 6.89E-05 2.28E-04 0.000 

mg/dscm@7%0 2 9.99E-03 9.58E-03 3.17E-02 0.017 

Compound: Lead 

Averal!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00147 0.000986 0.000674 0.001 

Eglhr 6.07E-03 4.08E-03 2.78E-03 0.004 

mg/dscm 3.52E-04 2.27E-04 1.51E-04 0.000 mg/dscm@7%02 4.89E-02 3.16E-02 2.10E-02 0.034 

Compound: Manganese 

Averal!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00419 0.0204 0.0054 0.010 

Eg/hr 1.73E-02 8.44E-02 2.23E-02 0.041 

mg/dscm l.OOE-03 4.69E-03 1.21E-03 0.002 

mg/dscm@7%02 1.39E-Ol 6.52E-01 1.68E-Ol 0.320 

Compound: Mercury 

Averal!e 

RunNumber M29-J M29-2 M29-3 

Mass_mg 0.000631 0.000681 0.000526 0.001 

Monday, June 20,2011 Page 17 of 39 
Eglhr 5.95E-03 7.03E-03 2.45E-02 0.012 

mg/dscm 3.45E-04 3.91E-04 1.33E-03 0.001 

mg/dscm@7%02 4.80E-02 5.43E-02 1.85E-01 0.096 

Compound: Selenium 

Averal!e 

RunNumber M29-1 M29-2 M29-3 Mass_mg 0.003 0.00306 0.003 0.003 

Eglhr 1.24E-02 1.27E-02 1.24E-02 0.013 

mg/dscm 7.19E-04 7.03E-04 6.71E-04 0.001 

mg/dscm@7%02 9.99E-02 9.77E-02 9.33E-02 0.097 

Location: Roller Kiln #1 October - Method 23 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDD 

Averal!e 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.00000578 0.00000593 0.0000101 0.000 

Eglhr 2.75E-05 2.84E-05 4.84E-05 0.000 

ng/dscm 1.04E+OO 1.06E+OO 1.78E+OO 1.293 

ng/dscm@7%02 5.56E+OO 5.89E+OO 9.16E+OO 6.870 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0. 00000000812 0.00000000631 0.000000008 0.000 

Eglhr 3.87E-08 3.02E-08 3.83E-08 0.000 

ng/dscm 1.46E-03 1.12E-03 1.41E-03 0.001 

ng/dscm@7%02 7.81E-03 6.23E-03 7.26E-03 0.007 

Compound: 1 ,2,3,4, 7 ,8,9-HpCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0. 00000000444 0.00000000499 0.00000000736 0.000 

Eg/hr 2.11E-08 2.39E-08 3.53E-08 0.000 

ng/dscm 8.00E-04 8.89E-04 1.30E-03 0.001 ng/dscm@7%02 4.28E-03 4.94E-03 6.69E-03 0.005 

Compound: 1 ,2,3 ,4, 7 ,8-HxCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.000000555 0.000000616 0.00000078 0.000 

Eg/hr 2.64E-06 2.95E-06 3.74E-06 0.000 

ng/dscm l.OOE-01 1.1 OE-01 1.38E-01 0.116 

ng/dscm@7%02 5.35E-01 6.l2E-01 7.10E-01 0.619 

Monday, June 20,2011 Page 18 of 39 
Compound: 1 ,2,3 ,6, 7 ,8-HxCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.000000805 0.000000839 0.00000114 0.000 

Eg/hr 3.83E-06 4.02E-06 5.46E-06 0.000 

ng/dscm 1.45E-01 1.50E-01 2.01E-OI 0.165 ng/dscm@7%02 7.75E-01 8.34E-01 1.03E+OO 0.880 

Compound: 1,2,3,6,7,8-HxCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000496 0.00000000528 0.00000000578 0.000 

Eg/hr 2.36E-08 2.53E-08 2.77E-08 0.000 

ng/dscm 8.94E-04 9.41E-04 1.02E-03 0.001 

4.78E-03 5.23E-03 5.25E-03 0.005 

Compound: 1,2,3,7,8,9-HxCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000168 0.00000187 0.00000253 0.000 

Eg/hr 8.00E-06 8.96E-06 1.21E-05 0.000 

ng/dscm 3.03E-01 3.33E-01 4.47E-01 0.361 ng/dscm@7%02 1.62E+OO 1.85E+OO 2.30E+OO 1.923 

Compound: 1,2,3,7,8,9-HxCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.00000000148 0. 00000000 131 0.00000000327 0.000 

Eg/hr 7.05E-09 6.27E-09 1.57E-08 0.000 

ng/dscm 2.67E-04 2.33E-04 5.77E-04 0.000 

1.43E-03 1.30E-03 2.97E-03 0.002 

Compound: 1,2,3,7,8-PeCDD 

Avera!!e 

Run Number M23-1 M23-2 M23-3 Mass_mg 0.00000163 0.00000173 0.00000211 0.000 

Eg/hr 7.76E-06 8.28E-06 1.01E-05 0.000 

ng/dscm 2.94E-01 3.08E-OI 3.72E-01 0.325 

ng/dscm@7%02 1.57E+OO 1.71E+OO 1.92E+OO 1.733 

Compound: 1,2,3,7,8-PeCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000639 0.00000000643 0.00000000692 0.000 

Eg/hr 3.04E-08 3.08E-08 3.31E-08 0.000 

Monday, June 20, 2011 Page 19 of 39 
ng/dscm 7.49E-04 7.77E-04 1.05E-03 0.001 

ng/dscm@7%02 4.00E-03 4.32E-03 5.41E-03 0.005 

Compound: 2,3,4,7,8-PeCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0. 00000000801 0.00000000705 0.00000000277 0.000 

Eg!hr 3.81E-08 3.38E-08 1.33E-08 0.000 

ng/dscm 1.44E-03 1.26E-03 4.89E-04 0.001 

ng/dscm@7%02 7.70E-03 7.01E-03 2.52E-03 0.006 

Compound: 2,3,7,8-TCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000116 0.00000122 0.00000134 0.000 

Eg!hr 5.52E-06 5.84E-06 6.42E-06 0.000 

ng/dscm 2.09E-01 2.17E-01 2.37E-01 0.221 

ng/dscm@7%02 1.12E+OO 1.21E+OO 1.22E+OO 1.183 

Compound: 2,3,7,8-TCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000139 0.0000000134 0.0000000135 0.000 

Eg!hr 6.62E-08 6.42E-08 6.47E-08 0.000 

ng/dscm 2.50E-03 2.39E-03 2.38E-03 0.002 

ng/dscm@7%02 1.34E-02 1.33E-02 1.23E-02 0.013 

Compound: OCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.0000432 0.0000418 0.0000903 0.000 

Eg!hr 2.06E-04 2.00E-04 4.33E-04 0.000 

ng/dscm 7.78E+OO 7.45E+OO 1.59E+Ol 10.377 

ng/dscm@7%02 4.16E+Ol 4.14E+Ol 8.19E+Ol 54.967 

Compound: OCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000147 0.0000000127 0.0000000226 0.000 

Eg!hr 7.00E-08 6.08E-08 1.08E-07 0.000 

ng/dscm 2.65E-03 2.26E-03 3.99E-03 0.003 

ng/dscm@7%02 1.42E-02 1.26E-02 2.05E-02 0.016 

Compound: Total Dioxins 

Avern•e • 

Run Number M23-1 M23-2 M23-3 

-- -

------

Monday, June 20, 2011 Page 20 of 39 
Mass_mg 0.0000000715 0.0000000667 0.0000000848 0.000 

Eglhr 3.40E-07 3.19E-07 4.06E-07 0.000 

ng/dscm 1.29E-02 1.19E-02 l.SOE-02 0.013 ng/dscm@7%02 6.90E-02 6.62E-02 7.72E-02 0.071 

Location: Roller Kiln No.1 May- Method 23 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDD 

Averal!e 

Run Number M23-1 M23-2 M23-3 Mass_mg 0.00000791 0.00000673 0.00000668 0.000 Eglhr 3.80E-05 3.31E-05 3.25E-05 0.000 

ng/dscm 1.38E+OO 1.20E+OO l.l5E+OO 1.243 

ng/dscm@7%02 1.07E+01 1.04E+01 9.99E+OO 10.363 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000965 0.000000019 0.0000000089 0.000 

Eglhr 4.63E-08 9.34E-08 4.33E-08 0.000 

ng/dscm 1.69E-03 3.38E-03 l.53E-03 0.002 

ng/dscm@7%02 1.31E-02 2.94E-02 l.33E-02 0.019 

Compound: 1 ,2,3 ,4, 7 ,8,9-HpCDF 

Avera!!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.0000000036 0.0000000044 0.0000000068 0.000 

Eg/hr 1.73E-08 2.16E-08 3.31E-08 0.000 

ng/dscm 6.29E-04 7.84E-04 1.17E-03 0.001 

ng/dscm@7%02 4.86E-03 6.81E-03 1.02E-02 0.007 

Compound: 1,2,3,4,7,8-HxCDD 

Avera!!e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.000000401 0.000000507 0.000000448 0.000 

Eglhr 1.93E-06 2.49E-06 2.18E-06 0.000 

ng/dscm 7.00E-02 9.03E-02 7.69E-02 0.079 

ng/dscm@7%02 5.41E-01 7.84E-01 6.68E-Ol 0.664 

Compound: 1,2,3,4,7,8-HxCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000392 0.0000000048 0.00000000495 0.000 

Eglhr 1.88E-08 2.36E-08 2.41E-08 0.000 

ng/dscm 6.85E-04 8.55E-04 8.50E-04 0.001 

ng/dscm@7%02 5.29E-03 7.43E-03 7.38E-03 0.007 

Monday, June 20,2011 Page 21 of 39 
Compound: 1 ,2,3,6, 7 ,8-FixC:l)F 

Average 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000063 0.00000000717 0.00000000654 0.000 

Eg/hr 3.03E-08 3.52E-08 3.18E-08 0.000 

ng/dscm 1.10E-03 1.28E-03 1.12E-03 0.001 

ng/dscm@7%02 8.49E-03 1.11E-02 9.73E-03 0.010 

Compound: 1 ,2,3, 7 ,8,9-FixC:l)l) 

Average 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.00000164 0.00000178 0.00000161 0.000 

Eg/hr 7.88E-06 8.75E-06 7.83E-06 0.000 

ng/dscm 2.86E-01 3.17E-01 2.76E-01 0.293 ng/dscm@7%02 2.21E+OO 2.75E+OO 2.40E+OO 2.453 

Compound: 1 ,2,3, 7 ,8,9-HxC:l)F 

Average 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000033 0.000000005 0.00000000487 0.000 

Eg/hr 1.58E-08 2.46E-08 2.37E-08 0.000 

ng/dscm 5.76E-04 8.91E-04 8.36E-04 0.001 

ng/dscm@7%02 4.45E-03 7.74E-03 7.26E-03 0.006 

Compound: 1,2,3,7,8-PeC:l)l) 

Average 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000144 0.0000015 0.00000141 0.000 

Eg/hr 6.92E-06 7.37E-06 6.85E-06 0.000 

ng/dscm 2.52E-01 2.67E-Ol 2.42E-01 0.254 

ng/dscm@7%02 1.95E+OO 2.32E+OO 2.10E+OO 2.123 

Compound: 1 ,2,3,7,8-PeC:l)F 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000771 0.0000000058 0.0000000072 0.000 

Eg/hr 3.70E-08 2.85E-08 3.50E-08 0.000 

ng/dscm 1.35E-03 1.03E-03 1.24E-03 0.001 

ng/dscm@7%02 1.04E-02 8.95E-03 l.08E-02 0.010 

Compound: 2,3,4,6, 7 ,8-HxC:l)F 

Average 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000042 0.0000000046 0.00000000453 0.000 

Eg/hr 2.02E-08 2.26E-08 2.20E-08 0.000 

---------

Monday, June 20, 2011 Page 22 of 39 
ng/dscm 1.21E-03 1.66E-03 1.58E-03 0.001 

ng/dscm@7%02 9.34E-03 1.44E-02 1.37E-02 0.012 

Compound: 2,3,7,8-TCDD 

Averal!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.00000106 0.00000125 0.00000124 0.000 

Eglhr 5.09E-06 6.14E-06 6.03E-06 0.000 

ng/dscm 1.85E-Ol 2.23E-01 2.13E-Ol 0.207 

ng/dscm@7%02 1.43E+OO 1.94E+OO 1.85E+OO 1.740 

Compound: 2,3,7,8-TCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000848 0.00000000834 0.00000000965 0.000 

Eg/hr 4.07E-08 4.10E-08 4.69E-08 0.000 

ng/dscm 1.48E-03 1.49E-03 1.66E-03 0.002 

ng/dscm@7%02 1.14E-02 1.29E-02 1.44E-02 0.013 

Compound: OCDD 

Averal!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.0000684 0.0000712 0.0000635 0.000 

Eg/hr 3.28E-04 3.50E-04 3.09E-04 0.000 

ng/dscm 1.19E+Ol 1.27E+Ol 1.09E+Ol 11.833 

ng/dscm@7%02 9.19E+Ol 1.10E+02 9.47E+Ol 98.867 

Compound: OCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.000000011 0.000000048 0.0000000207 0.000 

Eg/hr 5.28E-08 2.36E-07 l.OIE-07 0.000 

ng/dscm 1.92E-03 8.55E-03 3.55E-03 0.005 

ng/dscm@7%02 1.48E-02 7.43E-02 3.08E-02 0.040 

Compound: Total Dioxins 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.000081786 0.000083977 0.000075773 0.000 

Eglhr 3.93E-04 4.13E-04 3.68E-04 0.000 

ng/dscm 1.43E+01 1.50E+01 1.30E+Ol 14.100 

ng/dscm@7%02 1.10E+02 1.30E+02 1.13E+02 117.667 

Compound: Total Furans 

Averal!e 

RunNumber M23-l M23-2 M23-3 

----- ----

---- --

Monday, June 20, 2011 Page 23 of 39 
Avera!!:e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00152 0.00131 0.00143 0.001 

Eg!hr l.l5E-02 9.94E-03 1.07E-02 0.011 

mg/dscm 4.32E-04 3.78E-04 3.96E-04 0.000 

mg/dscm@7%02 3.34E-03 3.28E-03 3.44E-03 0.003 

Compound: Arsenic 

Avera!!:e 

RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00793 0.0179 0.01411 0.013 

Eg!hr 6.00E-02 1.36E-01 1.06E-01 0.101 

mg/dscm 2.25E-03 5.17E-03 3.91E-03 0.004 

mg/dscm@7%02 1.74E-02 4.49E-02 3.40E-02 0.032 

Compound: Beryllium 

Avera!!:e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.0003 0.0003 0.0003 0.000 

Eg!hr 2.27E-03 2.28E-03 2.25E-03 0.002 

mg/dscm 8.53E-05 8.66E-05 8.30E-05 0.000 mg/dscm@7%02 6.59E-04 7.52E-04 7.21E-04 0.001 

Compound: Cadmium 

Avera!!:e 

RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00155 0.0006 0.0009 0.001 

Eg!hr 1.17E-02 4.55E-03 6.76E-03 0.008 

mg/dscm 4.41E-04 1.73E-04 2.49E-04 0.000 

mg/dscm@7%02 3.41E-03 1.50E-03 2.16E-03 0.002 

Compound: Chromium 

Avera!!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.02249 0.01904 0.0381 0.027 

Eg/hr 1.70E-01 1.44E-01 2.86E-01 0.200 

mg/dscm 6.39E-03 5.49E-03 1.05E-02 0.007 

mg/dscm@7%02 4.93E-02 4.77E-02 9.12E-02 0.063 

Compound: Cobalt 

Avera!!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00051 0.00098 0.00085 0.001 

Eg/hr 3.86E-03 7.43E-03 6.38E-03 0.006 

mg/dscm 1.45E-04 2.83E-04 2.35E-04 0.000 

mg/dscm@7%02 1.12E-03 2.46E-03 2.04E-03 0.002 

Monday, June 20, 2011 Page 24 of 39 
Compound: Manganese 

RunNumber M29-1 Mass_mg 0.01105 

Eg!hr 8.35E-02 

mg/dscm 3.14E-03 mg/dscm@7%02 2.42E-02 

Compound: Mercury 

RunNumber M29-1 Mass_mg 0.08986 

Eg!hr 6.79E-01 

mg/dscm 2.55E-02 

mg/dscm@7%02 1.97E-01 

Compound: Nickel 

RunNumber M29-1 Mass_mg 0.00531 

Eg/hr 4.01E-02 

mg/dscm 1.51E-03 mg/dscm@7%02 1.17E-02 

Compound: Selenium 

RunNumber M29-1 

Mass_mg 0.04062 

Eglhr 3.07E-01 

mg/dscm l.l5E-02 

mg/dscm@7%02 8.88E-02 

Location: Spray Dryer No.2- Method 23 

Compound: 1,2,3,4,6,7,8-HpCDD 

RunNumber M23-l Mass_mg 0.0000148 

Eglhr 9.09E-05 

ng/dscm 3.44E+OO 

ng/dscm@7%02 1.84E+01 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDF 

Run Number 

Mass_mg 

Monday, June 20, 2011 

M23-1 

0.00000000362 

M29-2 

0.0354 

2.69E-01 

1.02E-02 

8.86E-02 

M29-2 

0.12668 

9.61E-01 3.66E-02 3.18E-01 

M29-2 

0.00276 

2.09E-02 

7.97E-04 

6.92E-03 

M29-2 

0.05963 

4.52E-01 

1.72E-02 1.49E-01 

M23-2 

0.0000109 

8.17E-05 

2.94E+OO 

1.70E+01 

M23-2 

0.00000000355 

M29-3 

0.03257 

2.45E-01 

9.02E-03 

7.84E-02 

M29-3 

0.14641 

1.10E+OO 

4.05E-02 

3.52E-01 

M29-3 

0.00742 

5.57E-02 

2.05E-03 

1.78E-02 

M29-3 

0.07863 

5.91E-01 

2.18E-02 

1.89E-01 

M23-3 

0.0000123 

9.\6E-05 

3.29E+OO 

1.76E+01 

M23-3 

0.00000000396 

Average 

0.026 0.199 0.007 

0.064 

Average 

0.121 

0.913 0.034 

0.289 

Average 

0.005 0.039 0.001 

0.012 

Average 

0.060 0.450 

0.017 0.142 

Average 

0.000 0.000 

3.223 

17.667 

Avera!!e 

0.000 

Page 25 of 39 
Eglhr 2.25E-08 

ng/dscm 8.52E-04 

ng/dscm@7%02 4.55E-03 

Compound: 1,2,3,4,7,8-HxCDD 

RunNumber M23-l 

Mass_mg 0.000000605 

Eglhr 3.72E-06 

ng/dscm 1.40E-01 

ng/dscm@7%02 7.48E-Ol 

Compound: 1,2,3,4,7,8-HxCDF 

RunNumber M23-l 

Mass_mg 0. 00000000141 

Eglhr 8.66E-09 

ng/dscm 3.27E-04 

ngldscm@7%02 1.75E-03 

Compound: 1,2,3,6,7,8-HxCDD 

RunNumber M23-1 

Mass_mg 0.000000981 

Eg/hr 6.03E-06 

ng/dscm 2.28E-01 

ng/dscm@7%02 1.22E+OO 

Compound: 1 ,2,3,6,7,8-HxCDF 

RunNumber M23-l 

Mass_mg 0. 00000000139 

Eglhr 8.54E-09 

ng/dscm 3.23E-04 

ng/dscm@7%02 1.73E-03 

Compound: 1 ,2,3,7,8,9-HxCDD 

Run Number M23-l 

Mass_mg 0.0000024 

Eglhr 1.47E-05 

ng/dscm 5.57E-01 

ng/dscm@7%02 2.98E+OO 

Compound: 1 ,2,3,7 ,8,9-HxCDF 

Monday, June 20, 2011 

4.33E-08 

1.56E-03 

9.04E-03 

M23-2 

0.000000461 

3.46E-06 

1.24E-01 

7.18E-01 

M23-2 

0.00000000259 

1.94E-08 

6.98E-04 

4.04E-03 

M23-2 

0.000000719 

5.39E-06 

1.94E-01 

1.12E+OO 

M23-2 

0.00000000241 

1.81 E-08 

6.50E-04 

3.76E-03 

M23-2 

0.00000179 

1.34E-05 

4.83E-OI 

2.80E+OO 

2.12E-08 

7.63E-04 

4.08E-03 

M23-3 

0.000000387 

2.88E-06 

1.04E-01 

5.56E-Ol 

M23-3 

0.00000000473 

3.52E-08 

1.27E-03 

6.79E-03 

M23-3 

0.000000628 

4.68E-06 

1.68E-01 

8.98E-01 

M23-3 

0. 00000000 11 7 

8.71E-09 

3.13E-04 

1.67E-03 

M23-3 

0.00000165 

1.23E-05 

4.42E-01 

2.36E+OO 

0.000 

0.001 

0.006 

Averal!e 

0.000 

0.000 

0.123 

0.674 

Averal!e 

0.000 

0.000 

0.001 

0.004 

Avera!!e 

0.000 

0.000 

0.197 

1.079 

Avera!!e 

0.000 

0.000 

0.000 

0.002 

0.000 

0.000 

0.494 

2.713 

Averal!e 

Page 26 of 39 
RunNumber M23-l M23-2 M23-3 

Mass_mg 0.00000152 0.00000116 0.000000793 0.000 

Eg/hr 9.34E-06 8.70E-06 5.91E-06 0.000 

ng/dscm 3.53E-01 3.13E-01 2.12E-01 0.293 

n~dscm@7%02 1.89E+OO l.81E+OO l.l3E+OO 1.610 

Compound: 1,2,3,7,8-PeCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000143 0.0000000021 0.0000000013 0.000 

Eg/hr 8.79E-09 1.57E-08 9.68E-09 0.000 

ng/dscm 3.32E-04 5.66E-04 3.48E-04 0.000 

ng/dscm@7%02 1.77E-03 3.28E-03 l.86E-03 0.002 

Compound: 2,3,4,6, 7 ,8-HxCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000138 0.00000000259 0.00000000127 0.000 

Eg!hr 8.48E-09 l.94E-08 9.46E-09 0.000 

ng/dscm 3.20E-04 6.98E-04 3.40E-04 0.000 

n~dscm@7%02 

l.71E-03 4.04E-03 l.82E-03 0.003 

Compound: 2,3,4,7,8-PeCDF 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000138 0.00000000203 0.00000000126 0.000 

Eg/hr 8.48E-09 1.52E-08 9.38E-09 0.000 

ng/dscm 3.20E-04 5.47E-04 3.37E-04 0.000 

ng/dscm@7%02 l.71E-03 3.17E-03 l.80E-03 0.002 

Compound: 2,3,7,8-llCDD 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000129 0.000000919 0.000000603 0.000 

Eg/hr 7.93E-06 6.89E-06 4.49E-06 0.000 

ng/dscm 2.99E-01 2.48E-Ol 1.61E-01 0.236 

ng/dscm@7%02 1.60E+OO 1.44E+OO 8.61 E-01 1.300 

Compound: 2,3, 7 ,8-llCDF 

Averal!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.00000000159 0.00000000327 0.00000000432 0.000 

Eg/hr 9.77E-09 2.45E-08 3.22E-08 0.000 

ng/dscm 3.69E-04 8.82E-04 1.16E-03 0.001 

ng/dscm@7%02 1.97E-03 5.llE-03 6.20E-03 0.004 

----

Monday, June 20, 2011 Page 27 of 39 
Compound: OCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000681 0.0000000368 0.0000000532 0.000 

Eg!hr 4.18E-07 2.76E-07 3.96E-07 0.000 

ng/dscm 1.58E-02 9.92E-03 1.42E-02 0.013 ng/dscm@7%02 8.45E-02 5.75E-02 7.59E-02 0.073 

Compound: Total Dioxins 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.000488596 0.000316949 0.000396361 0.000 

Eg!hr 3.00E-03 2.38E-03 2.95E-03 0.003 

ng/dscm 1.13E+02 8.55E+01 1.06E+02 101.500 ng/dscm@7%02 6.04E+02 4.95E+02 5.67E+02 555.333 

Compound: Total Furans 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000859 0.0000000646 0.0000000758 0.000 

Eg!hr 5.28E-07 4.84E-07 5.65E-07 0.000 

ng/dscm 1.99E-02 1.74E-02 2.03E-02 0.019 ng/dscm@7%02 1.06E-01 1.01E-01 1.09E-01 0.105 

Location: Vertical Dryer No.1- Method 23 

Compound: 1,2,3,4,6,7,8-HpCDD 

Averal!e 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0.00000071 0.000000291 0.000000359 0.000 

Eglhr 1.02E-06 4.33E-07 5.24E-07 0.000 

ng/dscm 1.46E-01 5.74E-02 7.22E-02 0.092 ng/dscm@7%02 1.07E+OO 4.20E-Ol 5.28E-01 0.673 

Compound: 1,2,3,4,6,7,8-HpCDF 

Avera!!e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.00000000205 0.00000000182 0.00000000124 0.000 

Eg/hr 2.95E-09 2.71E-09 1.81E-09 0.000 

ng/dscm 4.21E-04 3.59E-04 2.49E-04 0.000 

ng/dscm@7%02 3.08E-03 2.63E-03 1.82E-03 0.003 

Compound: 1 ,2,3,4, 7 ,8,9-HpCDF 

Avera!!e 

RunNumber M23-l M23-2 M23-3 Mass_mg 0.0000000043 0.00000000225 0.00000000176 0.000 

Monday, June 20, 2011 Page 28 of 39 
Eg/hr 2.55E-08 1.28E-08 1.53E-08 0.000 

ng/dscm 3.63E-03 1.69E-03 2.11E-03 0.002 

ng/dscm@7%02 2.66E-02 1.24E-02 1.54E-02 O.D18 

Compound: 1 ,2,3,4,7 ,8-HxCDF 

Avera!!e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.00000000356 0.00000000383 0.00000000191 0.000 

Eg/hr 5.12E-09 5.69E-09 2.79E-09 0.000 

ng/dscm 7.31E-04 7.56E-04 3.84E-04 0.001 

ng/dscm@7%02 5.35E-03 5.53E-03 2.81E-03 0.005 

Compound: 1,2,3,6,7,8-HxCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000296 0.0000000138 0.0000000182 0.000 

Eg/hr 4.26E-08 2.05E-08 2.66E-08 0.000 

ng/dscm 6.08E-03 2.72E-03 3.66E-03 0.004 

ng/dscm@7%02 4.45E-02 1.99E-02 2.68E-02 0.030 

Compound: 1,2,3,6,7,8-HxCDF 

Avera!!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.00000000116 0. 000000000779 0.000000000573 0.000 

Eg/hr 1.67E-09 1.16E-09 8.37E-10 0.000 

ng/dscm 2.38E-04 1.54E-04 1.15E-04 0.000 

ng/dscm@7%02 1.74E-03 1.13E-03 8.41E-04 0.001 

Compound: 1,2,3,7,8,9-HxCDD 

Avera!!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000695 0.000000038 0.0000000489 0.000 

Eg/hr l.OOE-07 5.65E-08 7.14E-08 0.000 

ng/dscm 1.43E-02 7.50E-03 9.83E-03 0.011 

ng/dscm@7%02 1.05E-Ol 5.49E-02 7.19E-02 0.077 

Compound: 1 ,2,3, 7 ,8,9-HxCDF 

Averal!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0. 00000000 182 0.00000000116 0.00000000082 0.000 

Eg/hr 2.62E-09 1.72E-09 1.20E-09 0.000 

ng/dscm 3.74E-04 2.29E-04 1.65E-04 0.000 

ng/ds..:m@?%02 2.74E-03 1.68E-03 1.21E-03 0.002 

Compound: 1,2,3,7,8-PeCDD 

A vern•• J 

----

Monday, June 20, 2011 Page 29 of 39 
RunNumber M23-1 M23-2 M23-3 

Mass_mg 0. 00000000192 0.00000000102 0.000000000897 0.000 

Eg/hr 2.76E-09 1.52E-09 1.31 E-09 0.000 

ng/dscm 3.94E-04 2.01E-04 1.80E-04 0.000 

2.88E-03 1.47E-03 1.32E-03 0.002 

Compound: 2,3,4,6, 7 ,8-HxCDF 

Averaee 

RunNumber M23-1 M23-2 M23-3 Mass_mg 0. 00000000123 0.000000000869 0.000000000639 0.000 

Eg/hr 1.77E-09 1.29E-09 9.33E-10 0.000 

ng/dscm 2.52E-04 1.71E-04 1.28E-04 0.000 ng/dscm@7%02 1.84E-03 1.25E-03 9.36E-04 0.001 

Compound: 2,3,4,7,8-PeCDF 

Averaee 

Run Number M23-1 M23-2 M23-3 Mass_mg 0. 00000000192 0.00000000103 0.000000000886 0.000 

Eg/hr 2.76E-09 1.53E-09 1.29E-09 0.000 

ng/dscm 3.94E-04 2.03E-04 1.78E-04 0.000 

ng/dscm@7%02 2.88E-03 1.49E-03 1.30E-03 0.002 

Compound: 2,3,7,8-TCDD 

Averaee 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.0000000305 0.0000000127 0.0000000222 0.000 

Eg/hr 4.39E-08 1.89E-08 3.24E-08 0.000 

ng/dscm 6.26E-03 2.51E-03 4.46E-03 0.004 ng/dscm@7%02 4.58E-02 1.84E-02 3.26E-02 0.032 

Compound: 2,3,7,8-TCDF 

Averaee 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.00000000217 0.00000000107 0.00000000117 0.000 

Eg/hr 3.12E-09 \.59E-09 1.71 E-09 0.000 

ng/dscm 4.45E-04 2.11E-04 2.35E-04 0.000 

ng/dscm@7%02 3.26E-03 1.54E-03 1.72E-03 0.002 

Compound: OCDD 

Averaee 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.0000132 0.00000805 0.0000117 0.000 

Eg/hr 1.90E-05 1.20E-05 1.71 E-05 0.000 

ng/dscm 2.71E+OO 1.59E+OO 2.35E+OO 2.217 

ng/dscm@7%02 1.98E+Ol 1.16E+Ol 1.72E+OI 16.200 

Monday, June 20, 2011 Page 30 of 39 
Compound: Total Dioxins 

RunNumber 

Mass_mg 

Eg/hr 

ng/dscm 

ng/dscm@7%02 

Compound: Total Furans 

Run Number 

Mass_mg 

Eg/hr 

ng/dscm 

ng/dscm@7%02 

Monday, June 20, 2011 

M23-1 

0.000014086 

2.03E-05 

2.89E+OO 

2.11E+01 

M23-l 

0.000000055 

7.92E-08 

1.13E-02 

8.27E-02 

M23-2 

0.000008428 

1.25E-05 

1.66E+OO 

1.21 E+01 

M23-2 

0.0000000451 

6.70E-08 

8.90E-03 

6.51E-02 

M23-3 

0.000012178 

l.78E-05 

2.45E+OO 

1.79E+01 

M23-3 

0.0000000148 

2.16E-08 

2.97E-03 

2.17E-02 

Averal!e 

0.000 

0.000 

2.333 

17.033 

Averal!e 

0.000 

0.000 

0.008 

0.057 

Page 31 of 39 
Run Name 

BAGHOUSE Glaze Line (GL-1) 

VENTURI SCRUBBER Soray Dryer No. 2 

VENTURI SCRUBBER Glaze Line (GL 3,4,5) 

BAGHOUSE Roller Kiln No. 1 

Process Lab Run Data 

Run Name 

11anualderermined 

Monday, June 20, 2011 

Value 

0 

0 

0 

0 

Target 

UOM Value Comments 

0 

0 

0 

0 

Value UOM Comments 

0 :ons JhJ 

Page 32 of 39 
Run Finish Time 3:40:00 PM 12:36:00 PM 5:55:00 PM 

Net Traversing Points 24 24 24 

Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.255 0.255 0.255 0.255 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 0.982 0.982 0.982 0.982 

Barometric Pressure, inches ofMercury 30.21 30.08 30.08 30.123 

Average Orifice Meter Differential, inches H20 1.47 1.51 1.48 1.487 

Dry Gas Meter Volume Sampled, cubic feet 173.205 172.675 174.985 173.622 

Average Dry Gas Meter Temperature, oF 108.04 91.63 110.63 103.433 

Dry Gas Meter Volume Sampled, dscf 160.202 163.773 160.427 161.467 

Total Moisture Liquid collected, g 104.8 96.9 104.9 102.200 

Volume of Water Vapor, standard cubic feet 4.93 4.56 4.94 4.810 

Moisture Content of Stack Gas, % 2.99 2.71 2.99 2.897 

Moisture Saturation at Stack Gas Temperature, % 5.22 4.31 4.97 4.833 

Dry Mole Fraction 0.9701 0.9729 0.9701 0.971 

Carbon Dioxide, % 0 0 0 0.000 

Oxygen,% 20.8 20.8 20.8 20.800 

Carbon Monoxide & Nitrogen, % 79.2 79.2 79.2 79.200 

Fuel Factor 

Dry Molecular Weight, lb/lb-Mole 28.83 28.83 28.83 28.830 

Wet Molecular weight, lb/lb-Mole 28.51 28.54 28.51 28.520 

Flue Gas Static Pressure, inches of H20 -0.09 -0.08 -0.09 -0.087 

Absolute Flue Gas Pressure, inches of Mercury 30.20 30.07 30.07 30.113 

Average Stack Gas Temperature, °F 93.33 87.04 91.63 90.667 

Average Velocity Head, inches ofH20 0.3295082817 0.336884124 0.332992130 0.333 

09215 762715 954034 

Average Stack Gas Velocity, feet/second 33.05 33.28 33.24 33.190 

Stack Cross-Sectional Area, square feet 6.874 6.874 6.874 6.874 

Dry Volumetric Flow Rate, dry scfin 12,736.3 12,953.9 12,793.7 12,827.967 

Actual Wet Volumetric Flue Gas Flow Rate, acfrn 13,631.1 13,726.0 13,709.5 13,688.867 

Percent Isokinetic of Sampling Rate, % 101.6 102.1 101.3 101.667 

Percent Excess Air, % 19,!17.6 19,117.6 19,117.6 19,117.600 

F-Factor, dscfrn/MMBtu @ %02 0 0 0 0.000 

Round Duct Diameter, inches 35.5 35.5 35.5 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 33 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.317 0.317 0.317 0.317 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 0.982 0.982 0.982 0.982 

Barometric Pressure, inches of Mercury 30.05 30.05 30.05 30.050 

Average Orifice Meter Differential, inches H20 1.22 1.32 1.37 1.303 

Dry Gas Meter Volume Sampled, cubic feet 158.230 163.440 166.680 162.783 

Average Dry Gas Meter Temperature, op 100.95 95.35 91.50 95.933 

Dry Gas Meter Volume Sampled, dscf 147.329 153.752 157.914 152.998 

Total Moisture Liquid collected, g 82.3 76.8 76.1 78.400 

Volume ofWater Vapor, standard cubic feet 3.87 3.61 3.58 3.687 

Moisture Content of Stack Gas, % 2.56 2.29 2.22 2.357 

Moisture Saturation at Stack Gas Temperature, % 6.58 6.39 5.97 6.313 

Dry Mole Fraction 0.9744 0.9771 0.9778 0.976 

Carbon Dioxide, % 0 0 0 0.000 

Oxygen,% 20.8 20.8 20.8 20.800 

Carbon Monoxide & Nitrogen, % 79.2 79.2 79.2 79.200 

Fuel Factor 

Dry Molecular Weight, lb/lb-Mole 28.83 28.83 28.83 28.830 

Wet Molecular weight, lb/lb-Mole 28.55 28.58 28.59 28.573 

Flue Gas Static Pressure, inches ofH20 -0.04 -0.05 -0.04 -0.043 

Absolute Flue Gas Pressure, inches ofMercury 30.05 30.05 30.05 30.050 

Average Stack Gas Temperature, °F 100.75 99.80 97.55 99.367 

Average Velocity Head, inches ofH20 0.1133253953 0.122841059 0.128451490 0.122 

9107 251302 488337 

Average Stack Gas Velocity, feet/second 19.54 20.32 20.73 20.197 

Stack Cross-Sectional Area, square feet 9.393 9.393 9.393 9.393 

Dry Volumetric Flow Rate, d1y scfin 10,147.6 10,599.9 10,865.2 10,537.567 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 11,012.4 11,451.9 11,683.0 11,382.433 

Percent I so kinetic of Sampling Rate, % 103.7 103.6 103.8 103.700 

Percent Excess Air, % 19,117.6 19,117.6 19,117.6 19,117.600 

F-Factor, dscfin!MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 41.5 41.5 41.5 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 34 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.312 0.312 0.312 0.312 

Pitot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 0.983 0.983 0.983 0.983 

Barometric Pressure, inches of Mercury 29.55 29.55 29.55 29.550 

Average Orifice Meter Differential, inches H20 2.67 2.76 2.83 2.753 

Dry Gas Meter Volume Sampled, cubic feet 206.134 210.404 212.026 209.521 

Average Dry Gas Meter Temperature, oF 82.58 87.96 87.04 85.860 

Dry Gas Meter Volume Sampled, dscf 196.040 198.180 200.079 198.100 

Total Moisture Liquid collected, g 288.4 273.3 298.2 286.633 

Volume of Water Vapor, standard cubic feet 13.57 12.86 14.04 13.490 

Moisture Content of Stack Gas, % 6.47 6.09 6.56 6.373 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Dry Mole Fraction 0.9353 0.9391 0.9344 0.936 

Carbon Dioxide, % 3 3 3 3.000 

Oxygen,% 18.3 18.4 18.2 18.300 

Carbon Monoxide & Nitrogen, % 78.7 78.6 78.8 78.700 

Fuel Factor 0.87 0.83 0.90 

Dry Molecular Weight, lb/lb-Mole 29.21 29.22 29.21 29.213 

Wet Molecular weight, lb/lb-Mole 28.48 28.54 28.47 28.497 

Flue Gas Static Pressure, inches of H20 -0.22 -0.22 -0.22 -0.220 

Absolute Flue Gas Pressure, inches of Mercury 29.53 29.53 29.53 29.530 

Average Stack Gas Temperature, oF 279.50 281.42 281.88 280.933 

Average Velocity Head, inches of H20 0.3279458113 0.337879039 0.347362504 0.338 

02214 64567 618031 

Average Stack Gas Velocity, feet/second 38.56 39.15 39.76 39.157 

Stack Cross-Sectional Area, square feet 10.202 10.202 10.202 10.202 

Dry Volumetric Flow Rate, dry scfin 15,556.9 15,818.0 15,974.2 15,783.033 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 23,603.3 23,964.5 24,337.9 23,968.567 

Percent lsokinetic of Sampling Rate,% 100.9 100.3 100.3 100.500 

Percent Excess Air, % 738.9 782.8 699.1 740.267 

F-Factor, dscfm!MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 43.25 43 .25 43.25 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 35 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.312 0.312 0.312 0.312 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 1.017 1.008 1.008 1.011 

Barometric Pressure, inches ofMercury 30.08 30.08 30.07 30.077 

Average Orifice Meter Differential, inches H20 2.31 2.37 2.52 2.400 

Dry Gas Meter Volume Sampled, cubic feet 204.222 206.993 209.547 206.921 

Average Dry Gas Meter Temperature, oF 88.25 101.79 88.13 92.723 

Dry Gas Meter Volume Sampled, dscf 202.228 198.290 205.746 202.088 

Total Moisture Liquid collected, g 281.3 303.7 350.2 311.733 

Volume of Water Vapor, standard cubic feet 13.24 14.30 16.48 14.673 

Moisture Content of Stack Gas, % 6.14 6.73 7.42 6.763 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9386 0.9327 0.9258 0.932 

Carbon Dioxide, % 2.5 2.5 2.5 2.500 

Oxygen,% 19.1 19.3 19.3 19.233 

Carbon Monoxide & Nitrogen, % 78.4 78.2 78.2 78.267 

Fuel Factor 0.72 0.64 0.64 Dry Molecular Weight, lb/lb-Mole 29.16 29.17 29.17 29.167 

Wet Molecular weight, lb/lb-Mole 28.47 28.42 28.34 28.410 

Flue Gas Static Pressure, inches of H20 -0.2 -0.2 -0.2 -0.200 

Absolute Flue Gas Pressure, inches ofMercury 30.07 30.G7 30.06 30.067 

Average Stack Gas Temperature, oF 265.00 267.67 265.92 266.197 

Average Velocity Head, inches ofH20 0.3392469606 0.346541114 0.368633762 0.351 

54402 139673 949002 

Average Stack Gas Velocity, feet/second 38.49 39.01 40.25 39.250 

Stack Cross-Sectional Area, square feet 10.202 10.202 10.202 10.202 

Dry Volumetric Flow Rate, dry scfm 16,185.7 16,241.5 16,668.3 16,365.167 Actual Wet Volumetlic Flue Gas Flow Rate, acfm 23,560.5 23,878.8 24,637.8 24,025.700 

Percent Isokinetic of Sampling Rate, % 100.0 97.7 98.8 98.833 

Percent Excess Air, % 1,195.5 1,435.2 1,435.2 1,355.300 F-Factor, dscfm/MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 43.25 43 .25 43.25 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 36 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.25 0.25 0.25 0.250 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 0.973 0.973 0.973 0.973 Barometric Pressure, inches ofMercury 30.08 30.08 30.07 30.077 

Average Orifice Meter Differential, inches H20 1.06 1.05 1.13 1.080 

Dry Gas Meter Volume Sampled, cubic feet 131.837 131.660 134.240 132.579 

Average Dry Gas Meter Temperature, oF 89.42 97.04 84.67 90.377 

Dry Gas Meter Volume Sampled, dscf 124.257 122.389 127.604 124.750 

Total Moisture Liquid collected, g 172.6 195 221.5 196.367 

Volume ofWater Vapor, standard cubic feet 8.12 9.18 10.43 9.243 

Moisture Content of Stack Gas, % 6.13 6.98 7.56 6.890 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Dry Mole Fraction 0.9387 0.9302 0.9244 0.931 

Carbon Dioxide, % 2.5 2.5 2.5 2.500 

Oxygen,% 19.1 19.3 19.3 19.233 

Carbon Monoxide & Nitrogen, % 78.4 78.2 78.2 78.267 

Fuel Factor 0.72 0.64 0.64 

Dry Molecular Weight, lb/lb-Mole 29.16 29.17 29.17 29.167 

Wet Molecular weight, lbllb-Mole 28.48 28.39 28.33 28.400 

Flue Gas Static Pressure, inches of H20 -0.2 -0.2 -0.2 -0.200 

Absolute Flue Gas Pressure, inches ofMercury 30.07 30.07 30.06 30.067 

Average Stack Gas Temperature, oF 265.38 266.42 269.17 266.990 

Average Velocity Head, inches ofH20 0.3176618925 0.315308837 0.341019064 0.325 

90474 261709 065101 

Average Stack Gas Velocity, feet/second 37.25 37.20 38.80 37.750 

Stack Cross-Sectional Area, square feet 10.202 10.202 10.202 10.202 

Dry Volumetric Flow Rate, dry scfm 15,657.8 15,473.0 15,972.1 15,700.967 

Actual Wet Volumetric Flue Gas Flow Rate, acfm 22,801.5 22,770.9 23,750.3 23,107.567 

Percent Isokinetic of Sampling Rate, % 99.0 98.6 99.6 99.067 

Percent Excess Air, % 1,195.5 1,435.2 1,435.2 1,355.300 F-Factor, dscfm/MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 43.25 43.25 43 .25 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

J 

Monday, June 20, 2011 Page 37 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.275 0.25 0.25 0.258 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 1.002 1.002 1.002 1.002 

BarometJ.ic Pressure, inches ofMercury 29.55 29.55 29.65 29.583 

Average Olifice Meter Differential, inches H20 1.39 1.05 1.03 1.157 

Dry Gas Meter Volume Sampled, cubic feet 157.639 135.610 134.125 142.458 

Average Dry Gas Meter Temperature, oF 83.25 82.33 74.17 79.917 

Dry Gas Meter Volume Sampled, dscf 152.146 130.996 131.978 138.373 

Total Moisture Liquid collected, g 971.3 830.4 766.7 856.133 

Volume of Water Vapor, standard cubic feet 45.72 39.09 36.09 40.300 

Moisture Content of Stack Gas, % 23.11 22.98 21.47 22.520 

Moisture Saturation at Stack Gas Temperature, % 22.41 21.30 21.02 21.577 

Dry Mole Fraction 0.7759 0.787 0.7898 0.784 

Carbon Dioxide, % 3 3 2.5 2.833 

Oxygen,% 18.3 18.5 18.3 18.367 

Carbon Monoxide & Nitrogen, % 78.7 78.5 79.2 78.800 

Fuel Factor 0.87 0.80 1.04 

Dry Molecular Weight, lb/lb-Mole 29.21 29.22 29.13 29.187 

Wet Molecular weight, lb/lb-Mole 26.82 27.13 26.87 26.940 

Flue Gas Static Pressure, inches of H20 -0.21 -0.2 -0.17 -0.193 

Absolute Flue Gas Pressure, inches of Mercury 29.53 29.54 29.64 29.570 

Average Stack Gas Temperature, °F 144.71 142.71 142.33 143.250 

Average Velocity Head, inches of H20 0.3436517380 0.3 71538226 0.364476093 0.360 

20821 148949 807725 

Average Stack Gas Velocity, feet/second 36.78 37.96 37.70 37.480 

Stack Cross-Sectional Area, square feet 10.559 10.559 10.559 10.559 

Dry Volumetric Flow Rate, dty scfin 15,580.5 16,370.0 16,381.3 16,110.600 

Actual Wet Volumetric Flue Gas Flow Rate, acfm 23,301.6 24,049.2 23,884.5 23,745 .100 

Percent lsokinetic of Sampling Rate, % 104.2 103.3 104.0 103.833 

Percent Excess Air, % 738.9 831.8 701 .5 757.400 

F-Factor, dscfin!MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 44 44 44 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 38 of 39 
Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.25 0.25 0.25 0.250 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 1.002 1.002 1.002 1.002 

Barometric Pressure, inches of Mercury 29.65 29.92 29.92 29.830 

Average Orifice Meter Differential, inches H20 1.87 1.97 1.89 1.910 

Dry Gas Meter Volume Sampled, cubic feet 178.532 181.671 179.938 180.047 

Average Dry Gas Meter Temperature, oF 86.46 79.63 84.29 83.460 

Dry Gas Meter Volume Sampled, dscf 172.081 178.973 175.714 175.589 

Total Moisture Liquid collected, g 373.3 183.2 275.5 277.333 

Volume of Water Vapor, standard cubic feet 17.57 8.62 12.97 13.053 

Moisture Content of Stack Gas, % 9.26 4.60 6.87 6.910 

Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 

Dry Mole Fraction 0.9074 0.954 0.9313 0.931 

Carbon Dioxide, % 2 2 2 2.000 

Oxygen,% 19 19 19 19.000 

Carbon Monoxide & Nitrogen, % 79 79 79 79.000 

Fuel Factor 0.95 0.95 0.95 

Dry Molecular Weight, lb/lb-Mole 29.08 29.08 29.08 29.080 

Wet Molecular weight, lb/lb-Mole 28.05 28.57 28.32 28.313 

Flue Gas Static Pressure, inches of H20 0.41 0.45 0.43 0.430 

Absolute Flue Gas Pressure, inches of Mercury 29.68 29.95 29.95 29.860 

Average Stack Gas Temperature, oF 237.71 239.58 238.04 238.443 

Average Velocity Head, inches ofH20 0.6087614826 0.643095892 0.621221607 0.624 

24089 60242 252395 

Average Stack Gas Velocity, feet/second 51.29 52.07 51.35 51.570 

Stack Cross-Sectional Area, square feet 1.969 1.969 1.969 1.969 

Dry Volumetric Flow Rate, dry scfm 4,127.5 4,433 .7 4,277.8 4,279.667 

Actual Wet Volumetric Flue Gas Flow Rate, acfm 6,059.4 6,151.5 6,066.5 6,092.467 

Percent Isokinetic of Sampling Rate, % 100.3 97.2 98.9 98.800 

Percent Excess Air, % 1,023.7 1,023.7 1,023.7 1,023.700 

F-Factor, dscfin!MMBtu @ %02 0 0 0 0.000 

Round Duct Diameter, inches 19 19 19 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Monday, June 20, 2011 Page 39 of 39