PJGUBE +ll



## ....... WASTE MANAGEMENT DECJSION



# · .

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'· 

# ... 

# .

..

## · ' 

# · ) WliP·20



### VES 004401

# -**··~=** 

# ... ·-·· DIIC:JilOI'

1. e-eept.c ... l!!i11ty lp( o..ld• U.t.

........ .....,_. at F-ui'J



### u. D!siei• ta Dttr Ann!nl 101: 

### •e,;s tot !1ft•

• f.s ,...,... !wr!:\ 

# ·iool-

( J:) 

### C!!tt!!tJas 

### ""m Cl) !llM
... ljltph 1'" ttt"tl=


### •• IM1z:&Jel Inn ' 

# ,, 

# .... ..,....

• .

, !trd ' ' " !mlr:t!e
...

... (pd.Jat)



# . ) . ... .. l**·** • • _,. a.od...S•

------ .u.ctt. .. Dllt..-f

------ 

# -·-------------- •uta**ca~efiN"J'** Cad.•

------ - ------- 

# _,.._

....
....



# - ..

VES 004402**~.-** 

## .. . · 

## ·.·

. 

# ·) INCOMING WAS'm SBIPIIENT PJlOCZDURES 

### In a:uad&Dce 

### with 264.1 8(<) 

### IDIJ/ar 36 

### ID. Mm. Code '12Ul8 (c), 

### .:b 

### +tpment cl 'IO'a8te, 

### upco arrinJ at the facility , will be iupeeted ao cleflned b<reiD before the 

### iniUatlan oi tm1J 1\Jrtber acdvily. Tbi8

..,

...... two**~** !!rat, 

### It COlllpllreS the actual**~** ldesll.i ty wil.h that detenaiDod ill lbe prc6le**~** and that lilled 00 the

- manif est. 

## rr th e - cool orms to the apec:ttd d...,.;pt;ool a.od propertiee
.. 

### clet.eriDIMd durilllthe prollle 

### review, tbeD the 

### ilo!ormatloo 

### oblabd 

### clurinc pmllinJ 

### can ,.._ably be u.d

.. lbe 

### baoia for 

### mft!'M8inr the

- 

### which 

## a:rma at the facility. 

## Socoadb"
. it proridee a O«DDd level of

- that the coolemp!a1ed

- IDIIll8gemeu1 tec:hnique <an be utilized. Other CWM pe.--mel (or a CWM1ppl<lYed iabontory) <an pc-ovicle the**~** OIJA/or BupplosbeDtal**~ ~**  priar to or



### ....,..... rib thearrinJ ol' tbe load. WMie thip• t o thatbaff 

### armed u the 

### Cac:llity are 

### ....Wclered to be in the receiving proceoa unlll 

### such time that Facility Maoapmeot makee a 6nal dec:iolco repn!ing**~ ~**  a t IUC!I time lbe 

# -11ft c:oosideJed .....-pted. 

### If

the waste does not coof0111l to the 

### especiC!d deocriptiooa ODd properties • determined 

## cluriDi the profile 

### rniew (ja !OWICI to beiiODCOil!orminc), tbeo the 

### iDl<>rmatioll oblaiaed Uliacthe Vaivtot""7**~ad** tm1 &iftilemeolel Aoaq8es perl"ormed, will be 

### utilised to**DD~~ge** the waste . All 

### waote obipmenll which are subject to the 

### Land Dilpooal 

### RoottriciiL>os oi 40 CFR Part 268 

### ad 11...-e been 1natec1, nemptod, variaDced, or - the WGfll'iole tr 

### •••+ 4 otaodard ar prohjbjtlon wllbout**~-** 

### muet be 

## IICCOIIlll"'ll by 

### a Conn &om the s.eeter**or~ ~**  that 

### the t.reated, 

## e:rempte<\ or ....n.m.ed 

## ...8.te- the WOjliiatoo ......._.,.

### ~ 

### Jlr"b'"b!tion, ar 'fWiellce (.,..that the 1111111 'od

-

### ~ - lbe l:e&lmeotllabdanl 

### or pt 

### •4 4 11 '""1) eod i.nctudes erJif

### a~ a.oaJ;ytlcal data 

### or 

### r ot

.,......... to 8Udl dUa or 

### doouo>eol.alaoo (ID aceordanee wilb 40 CFR 268). FIJnhenoan, 61 ...- wbieh are**to** the laod**~** restrictlooo aod require lfte!mou l muot be**by** a fonn &oailbe 

## iP-ntor ( 01' • treat« ) that (1) DOtlllootl tbat 

### the
........ cm'I&IN probibitecl " 

### eoDIItitueola; (2) kleotif!eo the 

## app...,..ate" s-trneat lllaDdwdo •• • led wil.h the

- iel; and ( a) iacludel1111,1...,p;ceb!e

### ~ dPa 

### or 4m to ruth 

### cWa (lD .....,....,. with 40 

# c:FB 2118) , See SecdoD 4.U 

### for a diocu8oloo ...,.,.....the 

## inCOft!llllkm**Bod~** to**be~** by**the~-**



### WAP·21 llEVlSION 11**~**


### V E S 0 04 40 3•**~!** '-"'• - obipmeat l<leu!l' u ... bepll vpoD lll'rinl ol lhe

- 

### at lhe 

### fadllt7
. 'lba in'V"'ion, 18111pliac ead 

## IIDIIO'oia o{ 

### the 

# jn"""'"" - will be pedormed 

### in**~** rib 

### the**~** doocribod 

### in Seetiaol2.0 aDd 8.0. 

### lo the
...... o{ 

### c:ootainer ablpmenta not CO¥el-ed in 

### the e=eptloao, 

### .-h c:oot.eiDe\o in the ablpmoDi will 

### 111m! ita 

### c:ooteota vtsue11y lnlpeeled b)'**~** a IWI depth 

### -uc.l**~** 

### to YUil";y 

### that the coatePta ore similar prior 

### to C<llllj'08ilinl,**Tb~** iet:Oifiollecbnicion 

## wiJi """'pbylicalllale 

### f.w eedl clnun OCI the 

# recemoc documeDia 

# c.ee**~5o** 

### 1 , Ph,r8ic8l**~** 

### WCIIUbeet), wbidl the lob will eompue 

### to the prolllecl plvsical 

### dtwctiptioiu ol 

### the

- J.ocoming

- will bate ka fW1 depth**~rticill** sample 

# ......u.r inapected Cor 

### C<>lor

·aDd pbMe (liquid. 

### oalld, MIIIHotid) , Druml 

### oi Jllt<bpclebemicolo 1rill be**~** opeced aDd illlf 1 

### c•od 

### to ,.,.;rylhatlbe clnun 

### il packed
.. 

### idenlified in Sectico 

### 5.1.1. Upcc**~.** 10 

### pe=t o{ the <OCIIaioen frcllll eedl - p'Oiile 

### wit.blD a 8bipmeot,**~** be J'ftlldoml,y aeleded 8lld Mmpled, 

## auwcluc to Sectico 2.0.. 

### lo tho eftiDt that 

### a 

### lliDIIe drum ol 

### a apecllio .- pra!le lo J-ilod, that dNIII will be -npled A mnlrragp o{ 1M eaatainerbecl ihlpmeot •mp!oe**~** the

-- prdile m-:y be ''"di..,.;ted prior to 8D8Iyole, 

### porided the 

### iodivldual88lllpla""' 

### elmilllr ID**~ ~**  appearaoce . ... ... 

### For WMie (ecoi>ei'l 

### arer 80 drums, liD e• !if w! siop dr.- 

### p"8b**~will** be tabQ u 

# _.rt 'C,

· the 

# me.. ··c .o..t;,a Tbe**sra~>** llllljlle will be 

### lalioclto _. ,......., ... 

## JDal>dWc1**~** Tblo**pw~o** 

## wm


# . ' Whore....,bfiwrl,.,.tobeJ'8DIIoml1aeJoetedi'OfoamP'nioriutljwtiao(lo hollugpodt;ac..t.._...,,



### · drum ; ,......, ••01 ), the 

### c:oota!nen to be 

### en1uo1ec1 will 

### be eeleded 

### 1lliDc a i'8Ddom llUIIIber 

### tahle. cr a 

### .-lam

DUIDbetr 

## eeoentor oa a penooal**"""'~""«** or 

## p.,.. •"'"**~-** 

### Drum i!llillhen wiD be 

## · s '""Ito the**~** 

## . drums 

### in 

### a**~l'l!IDI** upcc**~prior** 

### to 011\l&l
. D tit 

### •"DJ"ini 'lbe ....,.,_ 

### tDiiDben wiiJ be 

## 8""*8teci to
- 

### t•h wbir:b
.. • • - wiD be**~at** tb1l time. Qed a! « .....**will~** E j'OOiled only wilh umplee film 

### the- 

## Jll'i&t wliich..., o{ timilllr eokr

### -~ lo eclcJ!tioo,

### ~~-&om**the-~** 

### abibR**~-** ioplvobl"""
......

### ~

### lhellindetc.7~izidtlioee-be•eeoMc!,!See~tbenBa•**.** 

# 'i;, t ' •aw!llle
.. 

## rbi · to

## wllleli dlnlmt!-

## ~ 

# .d.- • ·**~ ~**  be 

## D..'de

## ~ tb,. ' .,•ite!tw 'floual 

### iD!IfoectlaD. S.mpioe

### tram~.- ""ipmmt• 

### w11 be oubjod.ed 

### to Mendatory

### ~**(~** -=tioo 

### S.O). 

### All audl
....... 

### Will 

### be relltloed ' f'llr. period 

## Nlfl*'ld**to~** the- f'llr iDeiDentiDo. 'nle reeu1t1 

### oi 

## ihe v1au11 to.pectiDoa ead 

### v ..**c~at<>ry ~**  will be • • +ted 

### oo lite

- ..,.,.;pt**~do** •**-~** (WBAD), 

### tn*al !on:a attad>td • 

## Fl£ure 6- l. 

### Tblo Corm io 

### ...ed to,. , 

### •t the

### pn>~~~e**em.181ioo** 

### date. lhe 

### reea11a oilhe Mendmory

### Ana~;yeM 

# c- 8ectldli U), 

## aD.i lite 

### determluadao ol · 

# ccar..........-......,,_ <- Seetioll5.2l.



# . · IIEVIBION 11 11/2919(



### V E S 004404

### . 

# - .

: ) '!be 

## fOilowiDe**~** wblcll are 

### cle6ned in Soc:tion 

### 4.1.4, will DOt be •mp!ecl 

### upon 

### airM1 bat, 

### at 

### a mjnjmum, will be**~** to 

### a vioua1 inlpoctlon 

### as clo<!crlbed below. 

# on.- llllltcl'iolla ere DOt**~** beca1we they exhibit C8IIIIUII "" Dppractlcal sampllnc and IIDIIlytiall comp!iratiom 

### .wl beca..a 

### """ded ehemical and pbylical dote 

### bu pnMousiJ been oblalned: l) 

## Pacbce<1 cbrmicola 

### ODd clobria (-Sectloo 4-U Cor deo<ript.lon)
. 

### Thio inopectlon procedure will apply to 

## u.- drums which &nl oek!d.ed 

## ror verificatioo 

## or the drum in't'elll.or7 abeda (DIS). During the w:rillcatloo, theae drumo will be ldeoti6ed 811 coo(crming. 

### nor......,..,. wiDjc and pcoce He, or 

## DOD-C<III[arminr and diacrepeDt. '!be 

### deliniticmo end**'~** will be 

### aa fo.llon: CooCormjng 

## Pmw A c1rum that

- guidelines 

### ODd an material ;, idenlillood and 

### , wueepow!a .nth DIS. Contormiag drums will be P" t<l. PI (II! 

### hie nn,m,. A 

### drum that 

### ia DOl 

## eoofarmlnr but suffident information 

### ia 89'li1able to detetmlDe U**~.** Tbe 

## follow!nr are enmp!M 1/1 pi QC ble dnJml: 1. Mlaoin( DIS but DIS ......aab1e in 

## oOJIP"OY8l package; 2. 

### 3.
. 4. 5
. 

## e. 

# 7

:

. 8.

9. 

### Malerill ideoti6ed OD DIS but not 

## ..-m In the 

### clrvm; BrokeD bct{Je(a) rill 

### lecihle leboloW;

. &.>bsl boltle(o) and loW(I) 4Mb Ojed, but
.... •oriolld
...

HI!ob!e with 

## Joslc-1 <lec!uctica and DIS reoiew; Extra coota1nen 

## or illtulified JDaleriol; Eztra ld..,tjf!eble ODd**~** 

### moter!al;**Bxn~ ,** **•• cotPPEandjob•lJ'P'ioo** **(~ marbro,aheorbom** 

...... cardboer<l); Material on**DIS~** but q PM !eo are iDwtiectb 

### ldeoWied; 

### NCIIHIOIJiaiDeri 

# *' CADCI but jdentjf\eb!e &am 

### DIS;



### .**Wbut** 

### •al
. • • t,J?'O'oiw 

### a.ld>DIB.

. PPo

' ""' 

### ce.ab""'l!'
. drumB 

### will be aa:epted lllid pc · 

### o II. The**~** ior 

### J*br ol P'P'"'' 

### ' -abNiee
. 10. drums will be no>tiliod of the**~ww.;.** 

### . . eel with the pc He drl-. Tbe genontor 

### or piiClulr will alao be DOtilied that the ....timood

### ~ ol pr ble materia1a
.

## ·.**~ o:ont~**  wiD DOt be tolenl.od 8Dd will ;.. ln
. tbe

--- ol deteiiid



### · _...,.,Up to andlnd n d!nebennlog tbe

### ~ fnm

### aendble~­ to TWI 

# r..r treetm.,.

Bl!MSlON 11 IJ,'29,1U 

# '



# ..

. 

## ..

VES 004405

## .**:**

i. .a 

## . ... )



## . . ' 2) 

### IMgepcglL 

## Pnvrur A**~** 

### when insuftiDent iDformatioD 

### ill tmlilable to &e« wiDe**~** 

### cllbe drum 

### or lbe drum CDOiains •**._.,.,..~** maun.J. 

### 'lbe followiQe 

### are eamples 

### cl diocae!*Dt drums: 

### L ODe or more brokeD bottleo 

### wbere lbe 

### oontenta """""' be dolamioed; 2.. Unidout11iable material; 3. 

## Mlsoioe label aDd COD'•'ner does not 

### match llll,7llli:ni oo lbe 

### DIS; 4.**U~e** 

### mauriel in 

### drum; 5. DIS not &"fllilable. Tbe porticm of lbe drum wbicb is diocrcpeDt will be rejeded. All DOD direct 

### cbu&e drums will be impoct.e<1 during pc • 

### 1 in lbe 

### SpeciaiV 

### l'!c I 

### 11 Bnllcti"' !'.mpy
_ .......... deiiDed 

### at 85 lAC '72L107(b)
. 

### Tbeee- will be 'Oioually**~** upoo receipt. In odcti tlon 

### to dilrereoces In plvaical 

### appeeraoce, tbeeil wu1ea will be



### . 

### ' detamiDed 

### to be ll<lOCOII!onnlng**~** lbey 

### eooteiD meterial in**~** greater 

### 1181 3,-. cllbe**total~** otlbe contaioer or more tban one lnob of ..;due r-m. ·oolbe boUom oC lbe OOidaiDor or wben \he**~** coolabor (o nil 

### 1• t) 

### 11M &ee llquida 

### lD 

### 'mare**~** lbe above quantities. 3)

### ~ eDd

### other~ procllact.o

### ~ lD -·- queoll.tles ill their


## .,....... uu•• 1 

### "0<1 P"" 

## top,. TW1 will**~** llld

### vilualb" loopeot 5,.. ol'lbe iao• • 

## q outer 

### ''"'"'" ottboooe materiali 

### to ovl(r 

### !bat \he 

### ablpaoeot 

### ooot.m. __. 

### w prhl"' C •l":iaa 

### pioclucta 

### Or rMm!taJo 

### TWJ will opeD 6'J' but oot ._ diM. ODe of lbe lDo I Jg _...._of eacb 

## iDvninr prolile 

### to,_, tllllt 

### lbe met11 

### iBI ie 

### u dorribod 

### oolbe WPS. 6) Aeroool CIID8 mol Letture BotUes: 

# n-o-**will»~** imported upoo pr• 1 

## c

.. Into bumable**~** 

### 6) Coalrollecl•d'"'• "'
. do&ed ill 

### lll UAC Sedioo
. 802. 

### Tbeie**~** 

### otmalerialt will oot I» 

### ..-eel or •mp!oit 

### b.1 TW1 c1i1e 

### to 

### the**~** 

## il<n•ullis U... 

### material8. TWI 

### wll 

## requn ., laoeolol) "&om lbe prJrer 

### cllbeee 

### lbllleriotla 

### ee "l"" 

### 11!*1. iD tbe**~** 

## .. . 

### ·. oo•ined in 

### 8etdcll

### ~ 

# n,. maleriall""**.-..~** 

### b7**a~.[** 

### •• ' 11 

### or 

## . . .**~.,....,._;.or-..** 

### or reclenl
. ee_eac7 · · 1)

### P~ 

### lnfedloU.Medic:al WUie (P1)lW) 

### ee deliDed 

### b7 IBPA 8) 

# w- wblob ore

### ~ .. c'lleNe 

### lhroucb
... irwpectina 

### proCea 

# w- lD arigiDal


# - . 

## .

. P"" 

### • IIIP•oe will be oubjec:t to 

### 5
.. io!peCtloa 

### u per**~LL4** aboft. 

### Weetee wblch """DOt 

### in



### .....,.. P""k•oe 

### wil be 

### IUI!!oct to 

### 100'*< "¥ilouel inoprtkm 

### EnmpJes cilbeae 

# tn- ot

- ere,

### ~ cal.bode ray lubet, a"Uibed 

## &lou, pipin& lllten IIDCI filter 

## cartridp., wlrecr tubiQg. peper " producta,**~metal** sbeet!Dg ODd 

### pan.. UJ*wi•eampnr-4"0Dd

. devil& 

### Tbia 

### liit II DOt 

### -tto be 

### ell iol:bm, omd 

### 111aJ 

### t.. 1• W wi&b loe8l 

### IBPA

appro98l. 

### RBYIBlON U**~** 

## · .

VE S 0 04406

### 9) Priar 

## 1ce«:t Apprunl: 

### M.olerWo 

### wbich do oat 

### Call lato 

### oae <I 

### tbo olher noimptloa 

### = ciieo, butpnMilt

### illlp"..:ti<M 

## •"!P"n' or..,..,.,. mmpljtatlope 

### u .. <llhla 

### e:ae '' t1uu will be .,..m.ed .., 

### a pn>lile opecific bella, with iDit.ial 

### .-lew**~** the IEPA field oftlce ( CAIDorille)
. 

### PrGllle .opprova1 w!1l be IIUbject to iEPA·DLPC Permit 

### 8eetioD**~** ( e.& IU) 

### llfllli'O'IIl.

AAe.. a - bae been• ec:ehtd**~the** 

### r.:ii&J , iDipe<:tecl. Mmpltd,**~--.,..eel Ill~**  with 

### SectiaDa 5.1. 

### 2.0. aDd 3.0, Fdty 

## y_, N!N wil 

### N¥itw the pdlle iDC.......U..., the Uandat017**~** 

### 8Dd tbe IIIIIDlf• 

### to cltWnaiDe wbetber the moteriol 

### ,..,;.o;d 

## .....cor- with tbo poollle**illl~-** the 1118Di(oat, aDd wbetbtr it CIUl be**~** 

# _,pt Ill tbo lio:llity
. 

### '!be**~** flvlrt!cm• Ill the**~** ..... Cellon: 

# . .
hdlity**~** 

### w!1l 

### relY em oae or man ofthe 

## CoiJowiDc 

# """'* <I iol'onalltiGil to ...**~~·** -• · ,.

• lhe idoadty tithe 

## jntqpq mat rW tcptber with 111q olher ,_.... Dia I ' "' 

### . 

# . 

# . . 0 0 V'.....tiDopectioD <ltbo _. ...... - &unpl!rc 0 

## . lltallta**<I~~** 0**Appupiootet...d~B ·**  I kSioi>N
.........."-'Cea116
......**,.~** 

### o W..&e 

### v..;r,. '!be 

### fL1Cw 'L
... L eda- tbo 

### ilboote- ,.;o be 

## ClllllfiUed with 

### iDrormiuioo tUea a-the 

### !clklwlalr- •• !':pod 

## duriJDc J"4llal 

# c- 8octiaD 4
. 1): o 

# wa... Pre& 

### 8beeL 0
.... r4W{J 

## ,..,b
__ o

## Art~ w'JMILM 

### tk 

### a',...., ...,...,

## ~ tbo 

### II"' -· 

## .i.:b 

# .a a

## ~ nW IWe&y 

### DMa



# ............ - · ... ,,.tc.. Spedllc · crllorill 'tcr"-
. ·· .

## ~ ......... ..,tlleWJW) (Jipre 1'1). 

## CcaatW..;..willlie



## . . . """--'
... b 

### WJlAD. Ddea ' 'L I fl Q W witb
. llipldlle 

### pM '
...... be deta • lf"l M d ibeoilllAn**·w~n. .**  

## Fa:ility Va • 

### w:J1ieo4 

### iDlor!llllllaD 

### or reNia 

### <I tbo Mppcl•lory**~do** oat amfllna 

### or**~~~e:** '' mt 

# wilh.,.... flofoo , ... 

## a.., it 

### a- lo**~** Bf 

### d hd 1D Appoadi& 

### WAP-D 

### or ialu :! 

# r' tc1 1o 

# IDI,.....,. _....., bued
... eden*ifto 

### fac:ta 

### -,1 

# P.• ..->. WAJ':21i



### VES 004407

# ' ) Tbe Fadlity 

### MM..,.ent must 

## clauil7 the ..,.. aa beiQg in 

### DOD-CCDC..- il 

### it il**·jfjra~** clilferent 

### !rom the infonlllliion shown in the profile pepenoorlt 

### or oo the IIIIIDifest, 

### or di8"en 

### in quantily &om that iudicaled oo the manifest, iD**~** with 40 CFR**264.7~** atJ4/or 35 

### JD. Adm. Code 72U72.**~ ~**  <riteria 11M used to arrive at thio c!orition 

## n.e, are: 0 0 

### For 

# built-.., ..natioaa greatA!r thaD**~in** volume 

### or, For bMcb - (e.r., druml, bop, ele.), AllY 

### variaiJoo in pieee count (Le., tbe 

### nwnl>es: 

### ot pleoeto lilled 

### on the manifest 

### or drum ilm!ntoty cb!o - "'Il""' with the 

### IIWIIber of 

## p1..;,. rec:eioe<l) or, o Il iolpect.loo**or~** of AllY- 

### c1etetmi1Ms 

### oi& .,., ... , dill'.._ eDit bet......, the 

## !lll1lical pi'OpOI1ieo of the

- ad the deea ipti<w OD the prc6le tmd/or shippinr paperwork. 

### s;p;r ........ dill'.._... are: 1) Variatioao &om ccof<>nll!lllCe erileria as deoaibed 

### in AppoDdiz W AP · D or; 2)**~.-.lUI** 

### "!bicb are 

### mutullll7 e.:Juej,. hued OD ICieotific 

### facta aAd principloe 

### from the 

### waste cleecription oo the maoii'OIIt or 

### prool!le**~** 5.2
. 4 

### An Eyall!a!.!op of 

## Wbeth!!r 

## W..S" Found 

## to !je jp >!m.mqfmp'M' CI!Q 

## be A&;
....... 'l!j!l be 

## l!eleetsd Ilthe**inf~** tdlocted in (1) !IDd**~** """"' jM!reteo 

### tW """ or more 

### ot the 

## mcc.,»ngevab•tjoo <riteria io lli(poili •ool.lydllf.......t llomthe ll*lireot or pro6le Wormetlon, Fadllty**~must** undatake to IOCI:O\ID1 

### fw the**appare~~t** oboened diii......,.,.. 

### 'lblo 

## .,.,...&a will · IDdude ooe or mont ol the 

## follow!n&: 0 ll!Mew 

### of •mpliog metboda 

### to 

## -111**~** ••q>lb>g; 0 

### Supp!m>enta!**~** 

### .. !lj>OOClilied in Sectioa 3.8; 0**~** 8ft!uatloG 

## ri the
- · poofile 

## ..m ·;. . ..**~** 

## ... cJjoco....._ with the



### . gooert!&ar

I! 

### intor-'ba 

# r" · e4 

# cbi.c thio 

# ....,pitlm ...., reeoa.. the · dllctepme 1 , the 

## · neolut:ioG 

## iL tht 

### cliiJoepomi;y Will be docupwp t 

### ciR 

# ihe 

# WBAn lllooig with the reoulla 

### ill the Incoming 

## wUie ..,.qiie. .:

## I!~in!pci.nlng- .-.aluatio.ocriterlaCIIIIDOt bereooiYed, the- 

# ..m boi •• ..; ed 

### DllD'<lOIIII'OI'JI>ixc ad the reou1t11 clocumeD&ed on the 

### WRAD aloag 

### with the reou11a 

### ot the •• 

## ic

- &ll!llytea.
. 

## w- fOIIDd to be 

### in 

### IMH!Gilf'""""""" will either be rejected 

### w**~pro&led** 

### f or J)C*iblo**~** 

## bJ the lilcility cleepile the
........ . 

# w- tW
..... 

# reJec:ted <luriag 

### •mloeding 111111 be placed 

# ""'*
... the trudt 

### f or tranoportelloD. 

### as 

### !· ) 

# • • ....-1 with the 

## ...,..u.:r. 

# w- u.t
- "!Jacte<l 

# an. the lnal8parter '- depertecl 

### the 

### facDit7 -WI
WAP-26



### V ES 004408!.•



# " ] in

### a~ area 

## bolclillc 

## 01117 """'P*Oie. materiala, baled CIG the MaDdalory ADalyees 

### ieaJ11a. A 

# record.; kept oC 

### the loatlioo oC 1111 druml OIHita a1
.. tin>eL**Al~.** 

### TWl 

## mar re-ealua1e 

### the- to dillermlDe wlletber 

### the- 

### materialaa Gpped



### · (Le. 

### !,..,;.cent rib 

### WPS rmd/at: 

### mamr..t dac.) CIID be handled a1 the 

### Fac:ilny. It the 

### r.cwty c1etermi1o1M tba1 the - can be 

### IIIIUlllpCI c<lCIIIisteni rib permit rtqa&emeots, the lblpmeot will be 

# """""'ied Tbe prollle information w111 be ameoded prior 

### to '"""""""' 

## or lbe DO:U 

### abipmes>t. 

# w- to be ,...proliled 

### w111 be 

### .,q..,t to 

### the pro6le proce88 

### requiremeota
... aet forth 

### in 

### Seotioo 4.0• .If the 

### r&-eV111uatioa proeedule indicates !.bat tbe - ClOD be IOOCepled aod 

### the geoerator ........, 

### a l"f:flaed WBBt.e**~t** decisloo will be**pr_.,c~** by Fadllly 

# Mm•e '""'• if lbe metbod 

## or DIOIIJIII'IIIII tbqet. 

### It**a~** 

### eminot be 

### '""""ed within 

### 16 • oC 

### ""ipnm• 

### rec:e!pt, 

### the IBPA wtl be IIOdlled, 

### in 

## writinc. 

## or the dilcn!peDcy and 

## or attemp.. to l'fl<Xll>l:ile iL 

## w- will be 

### n¥cted 

## row the 

### fcillowinr """""'"' 0

0

0
0
0 

### . 

### , Fadllly**~** Cor 11111 .._ determinml tW 

### it CIODDOt _,.. the 

### -rW in Mmpliaooe**withal~** permjt**~** 8Dd llaodudl**or~** ODd 

### ..cety. A 

### 111811!Ceot cliaorepanl::r (or llOII"COilfOi-) CIIIIDCt be ,.....,ed 

### to the aeoentor'e and TWl's satloCactloo 

## 1llliDr the pcu4taeo oulliDed above. Tbe**~'e/t.n\oopcrter'l** popes ....... il DOt iD
..... aDd 

### the pi I I If caDII<It be 

### coiTec:led upon 

### llft'iotal. Stonge opooce 

### in ...,te!ner atonge 

### areoa at: 

### In 

# oo«w balk lqo!ld atonge 

### IIDb le DOt uailoble to provide 

### ...,•ptloa of incompatible "W'm'IIIL 

### A liquid - 

### 1a 

### DOt compatible (piS" the Liquid 

# w- CompeHNiily 

### Tootl wilh - lllreel!y 

### In 

### atonce and no """' gatiw. or otber " ; 

### w •t motbod le**~** · 

### Rejecl.cl- will be pickecklp by the 

## aenftator at: by

### ~**~** 

# lr..,.. 1..- 

### to be 

### relolrDed to lhe 

### 8'lll'"ftlor '• r.dlity
... tnmoported 

### to an altemata huardous - tu,;, tent, 

### ot<n;e. at: diopoeol r.cillt)'
.



### WAP-27 BBVIBION 11 9fJ9J94 

# ·.

,.

V E S 004409

# .... .. 

# , ' • 1



## . .. ." 

### FIGUBEIH PRY81CAL DE8CIUP'l10N WOBBflfiEKl 

### AND WA81'B KBCED"l' ANALYSIS I)()CUMENT
.



### . 

# ·.**w~ 28**  

## .. 

## ·**.**



# . '

# t

' ( 

# - i •• ' ·



### VES 004410M'M EBIND .



# -- l'iiOCESI CCIII: 

# ( , __ ..._"P'J_ ( )WIFfii-UCUNI I (**--&lkMCILY** ( 

# , 

# ........ -. 

# ........ 

# - ( ) DIOUI 

# -·--..III!CUIIED**~Dar!NMOQAA:** -- -
Reiii.TS:

### ~-- FAll;.,_ · --

-YIICAI.CI • c:.J1111-'I:I:

- --------------
MlfU - B

# JIOII~~N::··=II~I~t-~;,~C~C>~CM~i~ii~IB~Ifl~wt~**: ::::::** **:::::::::~lllll~ifl:~===** .-E&iWClMIOc HBITI: ---------:--------------

-.....--_...........**--.~---** .. 0
... , .., ....... 

# -· ' 

# .. ....., 

# .... ___ _.... 

# .... ____ .._.

# ________ ......._**~-**



### VES 004411

### ' ,; ·' J



### - " PHYSICAL DESCR:X:P ' T:X:O N WOR:KSHEET



### DRUM I 1 2 3 4 

### 5 6 

### 7 8 9 

### 10 ll 

### 12 13 14 15 16

" 

### 17 18 

## 19 20 

### 21 22 

### IDI'III , __ PIOriLI ' -- 

### SIZE COLOR/OESCRIPriOH

' 

## . . nm __ _ 1 

# or aJrJAIJDS
__ 

### tFULL tSOL tLIQ

..

" 

### • \



## . "



### •

VES 004412:--· 8 .. 0 

### P RO CESS OP J!:RA110NS PllOCEDORES



# )
. Each IXICI'Iei:Dent ol 

### a 

### waate within the r.cility, 

## durinc which 

## arrr eboalp 

### in i1a**~** IDIIJ oceur , meba it aullject to addit.ionel inapecUon. umplincand analyses 

### to determine 

## "''Jl""lFlaF**~and ~**  ol the waate.. Many of the aoalysea needed Car the tft&tmalt, 1ton1ge, and 

### dioposal f\wcllOIIIi are perlormed durizlg iocom!ne waste shipment ideDt.ffication. These are not**~** uole8s it is known or bellevecl that the wute dlaracteristlcs bave cllanpl during**~** Ezlstlog and anUoipated opetalions •t the**focili~.** for which current and pedodjc oampling and analyses is importaut, indode the following:**~** 

### Doc:antiDi Incinenldon 

### The**~** procedure& for eocl> ol these are described separately below
. 

### 8. 1 Stonge 

### Before au.y - 

### are placed 

### into a storage unit, Facility 

### Management will- the compoollbility of the

- with the**~** unit mat.eriala ol eonatrudioo and with W1IStes**~** stored therein. 

### 6.Ll W.pe in Ccmtaine[s 

### Ccotainerlud 

### .....tes ue stored with mpec:t 

### to lgnitlbift\y, 

### reactmt.y and 

### """P'*'uftl.y
. CompaUI>ility sball be
.cletennined .,...,....;,! with DOTHM·181 guldellnea 

### aa 8\lmlllllrbod 

# m the 

### "Scggep'ion Table b 

## iJa.ardoua Materials" listed ill 49 CFR 177.MS (.see Apperulix 

### WAP.O)
. Baood on the initial DOT 

### l>aJerd dooo delermineliou and .,..qaio ollhe waMe, the drummed waste 

### will be 

### aeerepted 

### wdizic to**eompa~.** 

### ,_ D>lllerials will be 

### oepueted 

### from inercnpatible 

### maU!rlala by 

### &tOrap in oogrepted • within the drum storap OO!!ctinp Tblo is oecomjillabed by the data from the 

### WPS, Manclatoey**~** and

### ~AnalYse& 

## requetted by the Padity 

### Manogtmvm\. 

### Compat>1lility
. iqreption will

### not~ to · '

· material ...tUcb 

### luive been •epacbafid,**~** 

### or aolidilled at 

### TWI.

• • + l • • • • •• • . \

. To fllrtber veri(Y that
. _... ate 

## beloc ' properlY ·c:atA!goriied. 

### 'l'Wl Wilt Institute a 

## P!cl8a.., of · 

### · ·Omtamerisod Stonge Compet.ibility

## ~**~** will be · 1 soeci

## ~ perfonn!ng a liquid : Willllte '

· oompatlhility oil 

### the waate>eeeivod forcon+•iller

## t;~Qoage oooulline<lin 

### Appelldix WAP·A. '!'be 

### t.eotin& will 

### not apply 

### to 

### soi.on qti!IDiity patbaed 

### cbemirels or other 

### material .-npted under 

## ._U and 5.1.1

- 

### In the



# . nmt that 

### a compalib!My is performed
... -' lab 

### which
..... 

# "''*' ' eel
. . lneompatlble per Dql', the
· COIIlpatlllility teet will toke PJecedeoee """' the DOT
............**~** 

### 8.1.2 

### Wtste jn 

### Thnp 

### Liquid Wllltel 

### deli'med 

### in 

### balk Ccrm 

### (e.g., taDk !nJI:b, railr<>ed 

### taDk 

### con), or pouiiPod 

### from clruma, 

### are**~** placed in bulk t;IQoage taDb prior 

### to inciDeratioo. 

### Prior 

### to tnnsrerrlog 

### ""1 Waste into 

### a 

# '*""""'
WAP · 211 

### •·

V E S 0 04 413

### •.• t.aDir, 

### lbe Ml!!p••iJ:·''itJcllbe 

### -wi*h tbe 

### ID8&eriaJ**~ill** !be 

### iaaltmd lbe iaak...amallcl**~** will be 

### determiDod 

### 11J a liquid

- 

### """P""l · ;ft7

- ( M 

### AI'P"W'iz WAP-A:J
. lA ec!c!jtlm 

### laalt 

### W1ll rompeliN!fty 

### wiD 

### be •-odd 

### 11J porformiac a liquid.- • pe+ibi*y- aa 

### lbe liquid wule n>ceioed fcJr bulk 

### -.pwith**a~** OOiiipClliit.t 

### cllbe laDb 

### wilbilllbe -' •" I 

### 1J11em to wbidl tbe 

# DeW- will 

### be added. 6.1 .8 

## Jbd!s 8e'i" S tonft Bulk oaicla will be w" I'd ao fallon for nnlnadi"' 

### into the bullr. 

### liOIIdo pile 1}**~** .......... which paaooot 

### lbe p6iDt. 

## miAII" - can 

### be**~** into 

### the 

### lllolnllle pil& 2) 

### The 

### BTU ODd cbloriDe CDIII&ellta uood orill 

### be either: (II) 

### Tbe 

## hill- 'IBbae cllbe CUI"1U1 pit or 

### tbe 

### Qwnlnc DIIIUirial, or (b} Tbe**-~** 

### W wil be 

### •mp!ed after lllildog 

### aDd 

### lbe oample will be 

### oaalJud for 

### BTU md 

### dlloriDe , 

## u o-tttlq 

### In tbe<le<enq**~liquid-** are dr.can!ed rraatdnm. cral.bor ..,....,....._...,.,.... 

### bulk
...... tmil&. Tbe 

## "i'P'k"""" Manc!atory 

# ADaiJoiea will be ptil\1iaoad
... Wllllealo be
.. . '



### . Prlorto........,t!nJ,aLiquidWI!IIeCc.,'l' llljlii)Teetllld opec:ille_.,._
... . ......,. • .**~soc!** 

### II8II1JIIe will be perf..--.1 lo..,..,... tW


### - to 

### be balbd 

### t.csootJ- ue piLe 

# A.,.._ a 

### '&fta4

, . :)
.......... io 

### A
........... p<Ji>o."tioDM.t 

### 0 i 

### C qh cltbe jnte 1 

### '"--liqaidt.



## ·: 

# )'


# ·- u**~** lil the h · : non 

### .--lquld,**~** md 

### IOiid- ue 

### dotott..,...IIJ 

## bicb**~** thermal 

### owic!etlnn 

### Tbe 

### realllbll - indude ........,.... .- 

### t11.t
... lt:I'IIIIIJeclto resDO'N 

# sa """
. putletllteo, 

### mf otba 1¥ • •• 1 • •- (I.a., 1111!,
..

### aDd~ llwlp, 

### oorubller IOidl (bee bc8e clult)



### . 

# . . '

. that Me 1\utber I I II. 

### 'l'bebttl 4 ,, , .**r;;,·,..-~;** 

### b 

## lh··-.bediYideclilliotwo4 $ 

### ;-=b willl • opec;&


## . . .**~** 

### a 

## Pitb · f I

### wCII.IbllnatWibe-**a.DJ.riliiD.~...,peniil&a** ' ' 

### 2' 1 I 

### '• •llllli
...... . liall 

## timiDt cllbe 

# s-- opaliliao:wl.,...olnlioto;



## . . o 

### TI 9 w!B**i'ei!.i!t•"""coallrm~b** 

## , '"'*..Stlllitbe t rt 5 

### 'iceGf 

### !bot ...,._ 

# .m... are mch t.bU 

### It**tao;~** 

### be

- 

### to the 

## .;...c *P**~** 1 1 .., .....,..., 

### or 1\zrtMr 

### a·• ••M) -.- 

### apoo permit 

### ar**~** 

### , . 4 • . 

### 1 5 , 

### &c. CD1Ite 

### tz•• · Mnat 

### ot 

### lllld**~** ..-ncted

### ~ wtl be

### ~sad 

# ...r- mmh-iect. • oeeded. · ajpoii>R lbe appapioe.e 

## w·**=-~or** 

### 14 I 

### 3 .,. • 

### 1v1t a ., 

### w or ...... - off lite fw st.onp, 

### further b •• ..... 

### rJDt.flar 

## L4 1 

### will**~aft** ..,.o;zjate 

### r-•i" tj n 

### 1'orma 

### 011-.duJce wi*h .c) CPil
.... 21111),



# . . : 

### WAP·80

V ES 004414

# . )



# ... 6.3.1 

### Ptt-tne•meJtt Ana!y!ee AD 

### .....te. red to the indoerator are blended to 

### meet permit .....traiD1a aod to maintain 

## ote.!7 lt8te ( normal) cperaiXm of the 

### iDciDentor
. Liquid

- is**~** 

### in bulk laDb prior to inciDeralica. J>ro. tnatmenl**~** ( 6.8.1 numbers Hl) 

### are optiooaJ Car liquid 

### waate in taob wllicb will 

### IJIIdarao furlber 

## blmclins prior to incinentloo. 

### Priclc to iDc:ineralioo, 

### a sample 

### i.s drawn 

# mm the bllllt to 

### be fed aod**~ed** for lhe foilowixlr**~** 1. Heat 

### Ya!ut - Heet 'Niue io III<80III'ed to c:ootrol U.. feed ratea of - fed into the incilloraton. 'lbe 

### ...amum beat Yllloe wbicb 

### can be buraed 

### per bDw ia 

### "''blished ill the opel&liDQ permit. 2
. Aah Ccl!!le!Jt - Aah conle!Jt is**~** to control per<:eot. 

### aoh of wiate 

### fed**the ~**  

# cbem*- bumen of the 

### izlciDeraton. Tbe 

# ma..m...m aoh C<JilkDt forfed into tbe aecoodoay cbamM is "*b!jebrd 

### in 

## u.,; ...... tillc permk. 

### Wbere the permit baa

- eatablbbed 

### a limit, 

## lhio**~** will DOt be perlbrmed. 

### t 3
. 

### Total Qllorine Qmtmt

- CbloriDe coole!Jt is 

### -.red to c:oo!rol the percea1

### ~ iD

- fed into the illoioeraton. 'lbe 

### mezimnm dlb iDe CXJDtesrt 

### far waate led into -the**~** is etllabllobed 

### in tbe 

### opaaliue permit. 4
. fhp1pt 

### Qm!m' lo

### ~ aod
. 118ed

### in~ with 

## c:blorliM 8Dd

### bromiDe~ to delenaiDe the 

## haloaen 

# eon- in- feedo to the 

### ......Mory t "w -"""*-of the illdDenton. Tbe mnfmum balopn eootalt 

### far- fed iDto theM du) 

### dwn'* 5
. Bl • 

## .,Qmt
.....**ia-...claad118ediD~wllbdllorb>eaad~~..,** cfet I
.. tbe 

## IJoioeeD -"'- feed& to 

### the ...........,. ...._._ -"""*-of

·the illdDeraton. Tbe

### _.......,~"""*"~~~c 

## ........... fed IDto

### ~(II> ...., .... t
...



## . pHII!nt!l!i' 1Md**to~ the~**  cltaali; 

## tan. 

## -r:rioll**tif~aad** 

### poorid& 

# "* a - •at 

### cteu 

# rar . JII'OPer hie 

### rM 

### !I 7
. 

### Bprslfir Gmjtx

- 

### 'l'bio iDM 

### D.tiuu lo 1l8ed to _.. lhd 

# d.. apedllc 

## ......,uy 

## oC bulk or**~** c:ompooite liquid is -. 

# u- the 

## cJeaien lpedfic 

### lf8Yit1 

# fc!r the 

### otorace taob 

## <o.r. - U). 'lbe permit cpenlinawluee......, meNt""ed 

## tbnJush a trial bum. 

### The penail operalinc........, 

### me,y be d>Mpcl 

### lilt is domaootnted 

## tbnJush a trial burn that the

### """'permit~ 

## .iow tbe iDdnontor to operale 

### will*l the penlllt 

# = · ii1ait 8Dd a&**a~** lt8te (IIOlmel)**opa~**


### WAP-31 

### I!BVJSlON U 9{29/94



### VES 004415:; "-"' · Tbe 

### 1'acili9 vi. 8 ..,. ' will 

### rme..lbe 

# bleod"""""""' to......, 

# permit""""""""' aod.to _,...



## . 

# ") ·
_ .... 

### · .


### . 

## , 

## . .

· . that 

### lbe 

### bleDd willllloor 

## ICeM\r etate 

# c--o operation 

## or · the iDciDeralor. 

### Tbe blood will be 

# .....-e-1

. 

## . wheoenr 

### ..-ryto
- oil permit opecihtim• Tbie 

### le accomplillbed through 

### taak-to-lllllk**~** wllh additiooal W118te8. 

### A Uqul<l 

### W- C<wnpotibil!ty 

### Teot will be perfOI'IIICd prior to all taak•to-tanlt ttauol'en
. of Hquid 

### -e. This new blend io !ben**~** 

### fer lbe blood polr'lmeten. wblcb 

### are uoed to determiDo optimum bleod ebanocteristlcs as mentioned 

### iD tbe 

### Jft'riaul pncnpb. Containeri<od - ia aeqlleiiOod fer iocioenlt!ca 

## tbJoouch careful iodezios ol 

### CODialoer 

### teed. Tbe 

### parameter•,.. 7 far oeleelioo 

### otpoperfeed MqUODOe 

## ar- Value, 

## Cblorioe 

# eo-> are**evaluated'-<~** on tbe Malldatory 

### ADoiJoeo. Fcrlbe

- riall jdrntif!od iD 

### Seetioa 

### 6.U. \be """""' ol tbe above paaaeten 

### are 

### cateaoriJed bued OD**~** eod • .... I i W """''''"jm idormatloD obtaloed pel' 

### 8ec:lioo 

### U eod 

### 5
. L CootaJner feed 

### eequmcee reflect 1D 

## onpz.g enheetion ofcpentiDs e:peri.eoce.

6.3.2 

## 'l'mtment H+'l!e 

## Enlua!ioa Poet-tzoea-**"""""""'ODd~** will 

## C0116rm....,.,.,..,.. _.,..,, aod 

### that 1be c:baraderilllal ollbe**pro<e~~~** 

### ellluent 

### uewch that it
.... be

- to lbe Dl!li otap 

### (clio<:buae, dilpooalcr 1\aiber 

### treo-ot) bued 

### oo permit 

### or pro<eee 

### eo-.inl&. lo**~with~** CI'R 288.?(b) , reoiduM 

### (or...-...) 

### ..-.Jllor ftoom OIHite 

### tn-i- ollaod diopooaJ roetricted

### ~**~ ~**  tt>d/cr evaluated, 

### u oeecled, 

# ...,.._:u,.. apptoprl•lla
..... ,_... lll.oDdanl (e.g., 

### Cwotitueut 

### Coooeotration 

### io W..., 

### Extno<t (CCWE) "f8!uee) or 

### pdUb!tiaa Tbe iadoentloD proeell 

### reeulta io tbe
. &O t 1 jm oltbe f
.... 

### lie 

## i ' I

- 

### ub,
.. aod 

### 8l:l'llllber .,.temlollda. Each reooidlle bel beOD**~~to** 

### deO-elop. , . . ..**~** thai, 

### ia ......!stet)t aod iDdependerrt ot 

### lbe original-**fer** iA:ioer 

# *" w- ... trw-**~** 

## - oiJ'-oite 

# r

.... furtber

-- will be
.... ,q>MJie<l tiy \be llp!II'CIIIriot 

# ,.. · e ... 1**or~** forma. · locizleniar ub 

### aod 

## alas**~** 

### io the 

### rolar1 kim 

### ODd ""' oerubl>or ICIIido**~** 

### lo



## . 

## . · i• !- !' •• uoita numben 2, 3 

### ar 4 ani •mpled, 

## lllllb'Ad aod**~** 

### oo a......- bMio (See**~** 

### WAP·B, 8eclloo 2..2.1) 

### in """""""" wilh 

## -tYtia11**p~** ""''*ed to 

## ..,.q.e ...,._ tbe

## ~ . . . 

### tnat • Uodard or 

### Jll""'ltAtion (See Appendix 

### WAP-B) : Iodoent«
.. . 

## fi-nlecl · k>**~** lb
..



# l
.

lleuth. , · ll'!l'iciD.;;..

## ~ eilhor

- l ""'d. 

### ttt\ll....t aod

## ~ ....

## ~~criazetz**led ..;d** **~en;** 

## eele.t. · · · Tbe Fadlir;y**~** -d 

### ievfew the 

## aDeO
. ticol
..... aod**~D>ioe** 

### tbe 

## ill "'i!L"' 

### ol the 

### troeet •l'fllidue. It

### !be~**.-.~Umeet** 'tbe
... 

### op-..tresh•••**~** 

# ce:,.. CCWE
...... 

# >.Ibe

. bMI w •

### reo~c~ue il !ben lpplOY8Il for o!ripnwrt 

### Bilch •' · , lflll ill ;,.,...,P.Oniec! wllb · the 

## folowbic


# . . . doc, a M
..ef t • Laud ])jape-' 

## a-ictkm Treet!!Wit Certfl!cetlm; 

### Aoa\lltice!Beport or 

### re!- to 

### 8IIOb**~data.** 

### WAP-82 . ,



### V E S 00 44 16:•':



# r'' ) ' 

### .

. 

## . 

## .



# .. In the 

### omoat thet 

### tbe 

## ca171ia doel DOt meet the 

### "''JJI''Olriellnw._,t staDdlad (Le., 

### CCWE ..,._), tbe 

## FociiV**~** 

### will ionr'lpk the illlllllpliDc 

### procedure aDd the**~** 

### pruc:eduro to
....... . DO 

### cootaminetion Two et!d!tjmelllalplool 

### will be 

### ••tmi«e-1 for 

### anal1* ol 

### the panmotere wldch • 

### W lftelmos# lllalldarcls iD 

### the firot 

### I'OUIId of

## ...,.q.;.. rt the**~** 

## aoaq- plll8, the 

### re8due 

### wil be ""'*Oted for 

### &po.l 

### fllhe..,..... of the**""""minetlo:~C** '*"be 

### ciMenDioed, it will be clocui:Deuted. 

## H- , if the



## . --s**~** c!oee not 

### meet the 

## 8JIP"'P'iate lnw•ment IIW!dard**(~e.,** 

### CCWB nluee), 

### TWI will- 

### the reelduee in order 

### to 

### meet the appoprlote 

### -•ment l&aDdud 

### (l.o., 

### OCWE**~. ~.**  

### TWI

-**r~** 

### adclltiona1 IIID!pliaa and ...,.... I!Dd chooooo to rell'ellt the raidue 

### wblch did - 

### iDiliall;r - the

- lltandiJrd.



### . •'



# . - :



### · . REVIBlONU 

### 912111114



### VES 004417

# ) '7.0 QUAU'JT 

### cONmoL POLICY TWI 11M dee 

### akped a prO!Jim 

### <L quelky 

### CDIItr<ll pndi:ei....S**~** to OIIOUI'e that 

### prec:Mdon ....Srma) ...,_ . liiiODedthr<JucbauiaDaCilalabor8iorieL ABiite)obonltorieureK;Uktd to l*' ' · : • e 

### In !bit

### ~ Coou.:t labcniGrieo 

# .......,eel by 1M 

# '"""'*" .,.. aubject to ioopectiOD 

### ODd audit 

### w hile 

### pa!Drlllillc .....,... Cor 

### CWM. A review aC 1M coalnll:t loboralory Ia coaduu:ted to eaoure tbet 1M quality ecotral aC 

### CWM data ia 11•1111 1 

### +i Tbe quality CUIIlnll jAO!Jim Ia buecJ Oil "ffepclbook for ADaiJtice) Quality Control io**w~** 

### ODd**w~** 

### Lahontorieol' EPA, lUrch 19'79
. Good lobcntooy ,.. 

## r .. whicb '"" 

### _,.po hii!IC!tin& bcuoekeepillc 

### IID<I oofety - maintolne<l Ill aD laborat.orlee. 

### Tbe 

### followillc praot.lteo - be**in~Jolonw"od** a&
.. lite loborotcrioc All iDotnlmealaliol - be

### ~ tbroagb 1M

- a(""

### ~ 

### c:beck lll8lldud. Dh ag • • froaucceplallle 

# """"" nwlt criteria 

## nqu;r. couection. Tbe ..__**~** ataudood 

### resalle-
......deoi Tbe .-d 

## mit, ... CODtliD =hwtion
... • .... beodwnert criterio aDd 

### rneim
......... reeords. ' 

## a...,.m bUb 

### are tn*:aDJpepatd with M<h blldl aC...,... aDd 

## -'>'sed to -...


# - oample coolemlne'ioo bao""' OCCUiftd. Ilblmlt IIIIAI,y.- do 110t 

## ran wtlhiD acceptable 

### laiito, 

# A...,.. 1o 

# -o-s ;., +'f 5
,**~;r: ·**  

## .,_**~«** M<h 

## t-.r wi>plrio 

### boiac**~** 

## ror • puticq1or 

### permet« . A 

### bliDd 

## ""P""e'a BDple 

### will be
.........td to 1M 

### i1bon14rJ lXI 

## a IDC.'IQtbb't.lis.**ltelllll&a~tbeee** 

## "ali ••-.lJ-ewilbetavicwut.&:r · t )· 

### A qudl:y conuu oolution 

### ar oompJe ..-terial will be**~** a& leMt .,.,.,. ror M<h doy or 

### .-11 Web i\IQ to ... tbet eeljj I ' aDd -- 5 • • I a( ill '
.... __ ..., B ftbiD ao:ceplabie limlla. ,. 

### prOcedure ..,.,._ 1M 

### laboretoi:J' !hat 

### preocrihed pro I i= 

### ODd



## ... .., n boiar nwiD • einowi**a-.t~o** aCtbeee 

### a:wob-
.... . 

# epcww ror review
. 

### Few•• •L " are**~** to 

## .-mr neue ia 

### md M t • 

### exbcticu.**rDJ/r~** I illlw tee!1u4ipw 

### at ............. lewela. 'lbit**~** potitle& 

### ilaC« l h 1 aluout 

### ilie e&ct 

## ot**tli....p~e ~**  

## .. lbe

### ~ill 

# q I' 

### T;i
. ., .. . 

### nlllci**of ~**  

## ruu ·s •• I t« 

# eid.**~.,.ilea~** wil be wiintalaed 

### u.U.U:,,Ihe
_ _... 

## ....r ... tbe
.......... ...,.. wil be 

### forti6ocl.



### . W.AP-34 &BVJlliOH 

## u 9.121119' ' ,.



### VES 004 4 18

# . .' 

# ')

' WbeD 8'l8ilohle,

### ~ maiA!rWo &om the Nadobal 

## lmlitm or**~** aDd 

### Tedmnkv, 

### or 

## re.r- ll>llllerlall**&om~** other 

## recosolsed -, will be 

### obtained aDd**~** 

## ..... dine to 

### DOI'DI8!**W>ara~ary** metboclolagy 

### to 

### IDdi<ale 

### eceunq 

## or the methods. 

## n- maleriolo will be iaal;yud 

### ot -- . quarler!y il' the Jl"l''IIDeler baa been perfi>amed 

## duriar that quarter. Reference ma1eria1o are not required Cor acretitlog metboda. AD CWM laboratoriea partlclpate in ' rcuwl robin ' sample**~** 

### 'n-. oamplea will be IIUbmittecl by the 

### QAIQC Group and will be for the anel}llia 

## or1101111a1 perameten. s-.!ta

### ~ 

### muot be reported to the group . 

## Dfei uklol fnmlthe 

### norms -bhbed by the**Ulljar~** 

## or labonl.ories particlpeliog will be inftlllpled aDd**~** 

### At**~** 

### cme llllllple per month 

### Is eeo.t to 

### a CWM d 

## · a n '"" labonl<lry 

### or a .............. ODd appl'O'Yed C0111l11cllaborat.ory 

# rer porallel-"-' Tbeee op11t oamplee 

### or a 

### J'8PCrl 

## or bolll reouJ&o ..., eeo.t to t.be Quality CooQoJ. Unit wileD. an OUUide loboralllry io ewplojed. Samplelaent 

### to the**~** lohoratory 

### wil be 

## J.aaled in ODd analyzed**without~·** knowleclp 

## or lite lab Naill&

- Tbe fllcilily nporUo the 

## followlnc iDI'armatiaD
... 

### •IIIOOIIIb- be* 0 0 0 0 0 Nlllllber 

## or """''>'e8**~eel** Numhor aDd reoW1a oC d •q.Y. "" Nlllllber aDd,...... cl fart!flcellgns Illlb 

## ...a.t ..eel**~or** 

### OCX:WniiCe for qualt:y 

### CCIIIIlol dledl:
........ 

### wit.biD ecceptllble Jimila o M
... 

### aDd lllaDcWd deolatiaD 

## or en.oJ;Jte in quetitioo. 

# n.e · lilclll*>' allo reporta 

### iDtra-
. lab """ I'OIIIId robin reoulla
.. 

## lbo7 - ead ,..,_

--- anel}llia ot 

### Jeut quarter\y. A written ""PY ' cl 

### q third puty 

### ccintow:t IUJontory' o**~** ecatrc1 

### p......tateo 

### Is 

## •"'"'ftted to 

### CWM 

# '*" ' to lpP,IOIIl.
. 

### A 

### qu.ik, 

## -w- IDopeo:liou
.. oqgdoded to ..... 

## tll!o* prilpor
. ftoOC>Idi ead

· @ 

### ++ 

### i

# are...;..~ 

# DllliD......t**All~** .....

# ~ to 

### 1w> t 

# liouaD<I-***of~** pi'OCOCJaree

while 

### 'UIIdor contno:L 

### to CWM. A reriew of tbe - 

### labcwai<Wj Is .....;....eel 

### to _, t.bot the 

### q.iality OO!Iitl'ol II 

### beiDa miint..;.,..s,



### WAP-86 

### :



### VES 004419

# . .



# )

. . . 

### ... 

## . 

# .

. . 

# .

. . 

### •' :'\ 

## "' / APPENDIX WAP-A



# . .. .

. ·,'



# . ' 

## . - • . 

# . -

.· 

## . . .

VES 004420

# .-:,

. : . 

### }**'n>efollowiog..qtblpr~** 

### are deelped 

### to iclenti(y 

### oroereen -· 

### '1'blo' an:-.-! 

### b7C'Nli, baed**~** ita opentiQg expe leoce, aa rllpid but elroc:tive a>....,. for estaNi•hing 

### kfl7 decioico 

### per-. perllnes>.t 

### to proper- 

## -rite me•• Tbe _.,_ 

### cleecribecl 

### iD tbe 

### eec:t1ao1 below 

### ore t.oec1 

### oa ASTil md 'SI.alldard 

### lletbocll'**~** 

### b7 EPA 

### or are hued 

### cc 

### procodureo aod**~** CormuJa&ed by 

### CWll aod 

### a>eet CWM perf""""""" 

## -...m.. Aoaqtbl procedunls DOt 

## lisliocl below 1111\Y be added
.. 

### neo r ry with prior 

### IEPA appnwaL It 

### IObould be 

### noted tbet tbe inrormatioo 

### .,.-..1 Ill th!e 

### appendix II pocric in ebenlo:ter. TllenCore, 

### oertaiD- a>ethoda are clillo.-d wblcb llllll7 pertain 

### to tz ' em or dilpoea1 pre c - tbat ere 

### eoa:luded 

### I':JIIP lbe cadllty for wbicb !.be**fo~** WBIIIe**~** plm il )>reooDted. 

### J
. 

### UNIQUE ANALYnCAL 

### PROCEDUR&'J

DOt lmlilol>le ' fioom 

### "SSaDccord**·** in 8ecticm 

## n wblcb**ro~owo.** 

## m**ot~>w-.** 

## u... - are ••lwtihtted for 

### 'Staiodtact .w.tbod8" where they prvoide 

## .,,&..... equMioDt infonDIIUoa. 

### Bmsb sc;r-TJ=••••11!rh ... 

## km · &anp&- 

### olWM'teaarectBDbinedwit& JMnplee olotber 

### ..-.err 

# a 4• 

### at

### ~ ratic:& 

### hrthi::r t.estlng 

### iDay be requirecl in 

## cWder to CODllnD tbat tbe cleeirect ..-... - 

### ocewrect. 

### Qb,,,, 

## 'Mr vlkrh+ '" bfiPetrPglbc•'*'••LimMQ:rte•• 1 

# '"*' lBPLCl ·Tbiamethod(CWK&?8)**lll'ortbe.....q.uoC2,~aclcl** t2,4-D),2,4,6-tricbloi ipl
..

• )acAtii:ldd CZ,4,6-T), ..t2,4,6-



### . •. . trichlot .,.. ... .. , ..**~** 

### llelct 

### (l!iha:) ill**~-** eolilll
....... 

### BPLC/tJV. Tbe eblr:lropbeDollli<kle 

### SDcl



### ........

# ~**to~••li••** Mila 

### b.r

# heatillcdllirr!DJibe~'rilt...- olkali. 'l'lle
... 

### . 

## . 

# -

) IIJ'e 

# u-.o....n..a**~** 1oepee\tte ..- 

### b.r the 

### eddi!ion oCHCL. 

## 'ibe "qqleO'JI 

### ri'*ime oilbefiee"..a are 

### thea**~** 

### uob!r HPLC 

### Wlin« 

## ullrimolet clotedlao. 

## Ill

......**&!~Met** 

## . An llllquot oClfBBie is a>idcl with cli8llllecl 

### -ter. 'l'lle

### ~ ;S 

### fllt.arecllhrouJb IIIIer """"'aod tbe 

# ,.....,..ent flltl8!e 

### il then 

### anai.Y-1 

## r ... sul6cl& 8omnoled
.. • ·**~pot** • 

### rm - 11114 1:1 hjdroeblaric ' ldd 

### are added 11114 the eiJior 

# Proctuoec! is olsuallj COIIIp&led 

### with ataDdM elL



### WAP-A·l 

### JIBVJSION U

. 9129194



### V E S 004 4 21

## . 

# ) Heel l1eh1t br XsiDO:wed 

## &At• 

## !NlRl Sr 2 1


### - Bat 

### m ........m.;, io defemlnod 

### b.r 

# xluftued il*b.-.pj ill a 

### dillllle Nftertarre 

### mode 

## bJ pAoeillc a 

### paoperb' 

# miud....,.. ill ,a 

## c1i1fua**~** cell. 'lbe ..,...._ podweo NIB 

# .mo. ....... tpeetnc 

### whi<h- c:oonet.od to 

# a._ m ................. wiDe a preoloolly deflaed aolibultiw -. Tbe 

### motbocl lint ..,_ far ampleo to estreot qn•litatift 

## apeet>.....pe f- &em the NIB op«tno and then j»>OIoces quantit8ti'fe dot& 

# Car._ m mmt.notjre....., 

### multivariate talibratioDL Mota!f!!qeep btX·Bay1'lyon "' IXJ!F)- W•uapleo 

### mqbe p ; al,il'= -,. l>JeriD<Iolctoa_ 

### "'""'iDed mnhllise. 

### 'lbe p...,ed 

# .......-ill placed illaemple bolder and poeitloaecl far 

## .-line-**~** oatp.lt irfentj6ee tbl p M f Clf lt'fWIIl**~!or** Li**~** C pGJ I I Semi-p• f& r**~** I ) Hted 

### .IDitiall ill then pooolble 

# .-a... to Dl:riz 

### -"bed lluldudo. 

# ""'"""..,,.....,..,
......... ,.r.., -Aportiwoflllmjlleia ,.. · ; 

### •IDtomwqaiatewiuowwdi& ,. ... ._... 

### die ted uolag a mizlwe of aitric Uld**~** od<loL 

### 'lbe 

# .-1• baited ill a 

### wiaow&N

- ..... IJCOJII +4 llepo to ft"linkniae the 1 ee:Ji'ly of--., 

### A.tt.**~** the

- dilaAd**to~ ~**  filtered aDd 

### -'1>ed 

## bJ the 

### appooptW..**~** 

### <BW.ete 4010) 

## bJ ..., wu;aiate**oepn~~ao** pcoc:edxa• 

### < .. ,., 

## ema:tiaa, flllz 

## r ,**~** tbia**~ovw ~).** **Tbeestreotiothenllliadalld~illalltep** wiw......-illlideodi>od;r< 2adtuba 

### 'lbe • •• 0
• of 

### milia&**~** Uld 

# _,..,taboo about 80 ,.,_ 8lld ,_..ill a CGior 

### cbulp ill**~tube.** 'lbe eolar 4eu l'f w 2 io iuuuwly popcatiwal to the _,.,..,.,. . .. -til

. ., of the enti' 

### t.J • o r**~)of""-,e.g.,baul:lkldw,J** 2 ,.**opbeool(PCI?,pw2•~~** et!eb,)ch-booaCPABII),

... tolal petl .._ 

## JoG- t - ('l'P&j. PCB 

# s.re.. bd I

- 4 partiaa oCthe**~.....pe** io PEl 

### , al,... 101
. 

### i
.. 

### (CWM9HllllillJN·«01>Jr.s1 , -> 

## rm- '8

### ,~,· }Ill 

## cdbJ
.. :1 

## 'lbe-.-Cm.s
. . 

## . . 

## .., . .is theia 

### llhi:led 

## IPi!d i ' I 2 

## ft:J ill 

# air., ,... pr-ooei. iDIIde 

## tie.**Metlboc~i** m'ed tuba 

### 'lbe · - Nmlu

### of~ ... 

### a-b&dar Uld , . .. 

## li!l tabo 

### !ibau'* 80 miDulee Mid ,._.. iD 

### a eolar
.... 1D

## ~ tube. 

# -D.·C111cr •**derelopmeotileiDta~pcopcalicuoltothe** •,. • :1**ofPCBuadiodefectedl>Ja~o** • 0 • 

## fmnt Aci4jty

- 

# a-.. are 'EjiOtlul a 

### JIOI"'IIl ol 

### OoOO, ...,Do 

### hot or the JW :1 

# *' opeci6e opeciea if ·



# ......... ; 

# '

VES 0 044 2 2**~** Qn!clr 

## 'ri !S•IIP:tioo 

## Pn!cec!ur! • Adeoignated-**c.--.mp~e** io llliDcl wllh 

### tbe lf'l*qwiate eatrodJoo J]Qjd aDd fl!rred 

## rcw ad ·petecl time period. Afterl!ltndloo, tbe pH 

### udl
. ar-.. CXIIIteDt
... det 

### JmiDed llling lbe 

### appropriate !lppi'O'IIld 

### me!hod:i.



# .·· )

. .



## . 

# . Wnec<jy!ty 

### 5cmn ·A llllmpie oCwaote -erial io**~by a~**  CIIIUDter or 8U1'W17 

## mew .**~ty** Ieveii aboft**~** ... DOled, 

# •-dod ad iaftetip'ed

'1'lpk 

### lB!Il <;qppetjhi'ily • A.•-I!Odd by per!ormiQc a Liquid Wute Compatibility Teot oo 

### tbe liquid

-

- will be added. 

### CantaiDment area 

### muter eompooke 

### wiD be made up OD<e per week. matm.l will be cbe<kecl ......,. , tbio- eompooite.. Tbe 

### ill 

### ic

. . 

### ' 

## \l!emo!tt • Tbo**~** of the mat.erial 

### 1a vWually 

### ....._ted**mint~-** 

## .. 

# a..,_ rcw 1ow**~·** 

### " 

### • 

### r.mtejp=jze4 

## S!mn fgmte!j!!!jty. 

## wm be --"'by 

## perf...,.. a liquid 

# w- CmvpotiWI!y 

### Tea"" 

### fhe waate 

### a Gifelted 

### tor 

### amtafner ..... M CoDon; 

### a. 'lbe 

### teot PI 

### OJ"- 

### llfJPiieo 01:117 

### to
- ;.! 

### tW &llo tbe p&illt lllle U:& b. 

### A muter ..,....,.. for each ol tbe 

### DOT buad cltue cetepieo will be me!ntajnec! 

### d tbe llil:e. c. Tbo IJIMier 

### o JjiOiite will be 

### made**up~** by 

## acidiz>c 100 

### miL of each 

## ......m.r in the 

### co' &"J 

### to 1111
......... , 

### tab' lioad --. •

. d
. 

### W'- tbe 

## ..i.ect 

## rcw " , oa.ffity Wlli&elloo hao

### been~ 

### a eompMibDIIJ**~** w11 

### b;e
· pel'cwuioe4 

## :..U, tbe
..............

### DOT~ oW COIUgdry. 

### e. 'l'be : 

### t '' · .,. - 

## Will be pe:formeclao 

### ftlllon: · · · · L · .

### lA**ilrcier:tA>~IIiutlle JIIilltecaqullu,:P** **olu.~** ...... ldolu 

### JlD

. · 

## , )

. ·,; 

## .**=etc** 

## ,. 

# the --.er «•tp 

### -.Will be 

### maiDtalaed 

## m .a 

## w · +i , i;,liied ••· e .

. 2. 

## A ,: llJO lllil eomple ..,. the 

### ir•n,lng

## ~ will be
. tbeokeol

## ~ a 100 lllil -.pie ol the iljiP.qwia&e 

### DOT 

### baiard clue 

### maoter eompc>lite
...... 

## U..liqu6d • ••tiJjty
. teK. 8. 

### If tbe ...,.._ pa-. the 

## OOIJJil'lliblli teot, tbe 

### eDtire liOO 

### lllilllll:dure II edde4 

### to the

. ........ eompool.te. Tbo ......,._ ia UleD apptO+Ed 

### to be IIGred widliD**~** oltbe 

## aioelue**~** 

### """''inin&**~** 

# oe tbolt 

### DOT**~oa.on~c:~ooe.,.** 

# a , .

If tbe .-..... 

### raila the competiiJillly teet, the
..... will 

### IJ<It be adlleol to tbe

- 

## COIJIIlOI& ; .



### V E S 0044238. 

### U'the..........., il

### DOt~,.,. wKII 

### eay 

## eziotiar DOT 

### ha.d 

## doio- he, the clr=- will 

### I» ...., 1 'ad ID 

### olof:lrCe UDtllllll:b time tbat they com 

### I» moved cllreclq 

### to a**~-tar** 

### 11-..t.
'!'be 

### teotinc 

# '*""'- wil not 

### IJIPlJ to 

# -a qou>tity**~** 

### t!.emlrolo, materiallhelbM been 

## re!*b&ed ar ooljc!ified, 

### ar other materiol 

## " "'"P""' UlldeJ: UA la16.ll. In 

### the_,. 

### 11:.- a e , .. a**~** ilpa f'oi awd 011 

### ma&erieis wbioh- in<lialled
.. ..._polible I* 

## oor bual'cl clua, 

### the """'P"tJM!Iy- will take 

# '*
....... u.e 

## oor**~** 

## .- .,._,

PAB..UIBTER Sample 

### Wed Up Techlliqueo:



### Irmz ·**~** Acid 

## dia<**.,,_~for** 

### flome lllomk: aboarpllan opa:ti....., 

### Add
......... jii'<U<Iln 

### tar 

# a.r# Add~~~;""" Add 

## 4
. ... olcilt, 

# .,_ortH.oludoa 

## ,....,..u. tar ... .. ,_



# ... 

# - Acid 

### di8
...... c(
........ Alb6De 

### di8 ,, ( tar eolldt)
. 

### Orgimie Teclullquee**~** bmelliquid-llqald 

### -aDa Omt,imra**·** • 1 

### ' k •

. Af:id..bue dea-1ip
. ... • ..

. Badllet 

### -idila .MBTBOD BEPBKBHCB

8-8«17; 1-8020

### &91~ ·- !1128; &-BalltiD 

### .746 l.aoaG 1:3040 

### 8-M-08; 1-liOiiO 1:3080



### &r+

## ·~··~ .
..!tje.jM 

## CGiillm 

# o ' Aiit ..i**ss,.~-·t~~ ·**  

# .. otP ••etalnlli " ioaaw
.... llarooitC Y
. 

# a ' ,. IHU-22; 

### 14510 

### 1-3620 1:3580 1...0 

### l-86GO • t-liSU



### . Bib 

### Gel 

# ao-..p . SulbO 

### wp 

### L>ao
......**~** 

### W..bocllo:**~Coupled** 

### 1"'-- AIAlmic
.. !!mi

..

. _, .. 

## BJa t 

### » ,., UCPJ 

# A••' J Ala:Dio abicapdau, 

### clirec:t I I " " metbod A1Allllic 

### abicaptioa, furmce .-hod

. ArMDic Ala:Dio abicapdau, 

## rur..ce -*bod
. A1Allllic abearptiarl,
........ 

## tvdride IDOitbod 

### WAP-A-4 8:114-22;

-1-ae:IO

. 1:S830**IHW-22:1~**

1-«110 1-7 0 40;
.. 20U**1-'!0U;~** IHU-10; 1-'1080;
.. 2CU
. 

### 1-'1081;
.. 306.8 

### RBVIBlONU 9121119' 

## ,.

V E S 0 044 2 4

# ..

. 

# "

)'


# ·- PA!WIB'lD
BoaizD
. Alomie abootptiw, direc:t ..,.Uotiou -u.od AIGmie abootptiuu, 1\unaoe -u.od Beryllium

. Alomie abootptiuu, dlreet
.......... -u.od Alamie abuptiw. Nrnac:e -u.od Cadmjen

. A*omic
.abearptioll, dir«t
.... otiou method Atomic abootptiw. fia'naa! -u.od caJeium A-* 

### aboptiw. dlreet upiratico -*bod Al=lo abouo ptloo, 

## runwe -u...d Cbraaoium Aloalit abootptiw. clir<ct
............ method Atomic abouoptloo,**rum.:.~** He:aataluat**~** 

### C&pc fg 

## ·· .me Besa"fllilllt c:lllomham: 

### Cc.looi&Mril! BeoamiJeat 

## c:m-lum:..,....**~** 

# eow- . Iroo. Alomie**~** clir<ct
..... otiou -'lwei Alcmlc lot 

## t*• ' filn>oce 

# -w AtCIIDio lobeotpduu, clinct 

## MJ*IIdun .-bod 

### AScall: abootpduta, 

### &-. 

# -w

. . PbalaolhrcliDo 

### melhocl (f--.) 

### I.-I Al<mic abouoptiw, dite:t
......... -*bod At.amle abearpdaa, furriaDt 

### Jadhod 

### Mp wo Mea 

### Atcalic el+ I ,; "• direct I '
. . ' 

### met.hiocl
.

. Alomie IIIMwptiLcl, filn>oce 

# -w Y ; 

### f....a tHo 4"* t. 1 

### +r-l 

### IA
. Jcrdrlwae

-- ·IA:..JIIlw 

# r n.....,. N"dool**.~** .. .**ASclllic:~jijiw,** cllnct 

## ""''irirdun -*bod 

### Alcmlc • ; . • ' """'- aoi$bod**sse~o· -.** **·** Atomic alaaptiw, funloo:e**~** "*--o el j ' h \
........ .**~** 

### melhocl

# saAtomic abuptiw, 

### direct
............ metbod Alomie a.lwpiou, 

### Nri.ce IMihocl 1-7080; 4- liOB.l 1 -'ro81; 4- 208.2 1-70110; 4- 110.1 

## ' 1-7081; 4- llo..t 1-'1'130; 4- 21!.1 1· 718 1; 4-213.2 1-71«1; 4-m.l +21.6.2 1-7190; 4-118.1 l-71111; +11&.2 l-'7UIIi**1·1196;~D** 1-'1187;**+~** 

# .**1-7210;4-~** 

### HID.2 1·'1380; +21111.1 +2:1U 

### :.i..s&OOFeD 1-'TCO; +2311
. 1 

### 1-7W; ._.DI.i 1-'7460;
.. :H2-1**1.17~ .-MS.l**  

### +-J4U

.**~12;** 1·7470 &34-05;**~12;** 1 • '7471

. 1-7630;
.. 

### 249
. 1

. 1"7611; + 248.2

. "'"18; 1-7740; oH7D.2 ' 1.17741; +270..8

1-7780;
.. 

### 272.1 1-'1'181; +272.2



### VES 004425

## ..**~** 

## .... ..**p~ ·** 



# . ·

.. ·,?\

.. . !I Gu Qli I "' , .... )&thoda 

### B•' ; ....., Volatile OrpDicl

### N~ Volalile 

### OrpDico 

### Aromatic Vclali)e 

### Orplliol 

### A<rUeln.

### ~ ...

### ~ PbeDOia**~Eaten** 

### ()rpDOCh1orioe Peotkideo aDd pCIIo 

## NitroaJ'OdiSiict aDd Cyclic Kei<IOM

## p~~~ Cb)orill&ted**~** 

### ()rpnOPh
....... Peeljdc!M 

## CbJoriDatedHer,. r• 

# ocs- . GM

## ~ Bpt<b 'P11(ethoclo 

### GCIMS )(dbal 

### fOI' 

### DiolcliD GCIMS )(etba<t!or 

### VoiU!Ie OrpDicl 

### GCIMS 

### Yatbad fOI' 

### s.m>-VoiU!Ie ()rpDica 

### Infrsred Speeb"""""' )lelllodl 9a ' 4 

# c lo{elbodo:



### WAP·A-8 1· 7840; '-2711.1 1-784.1;
.. 2711.2 

### 1·'19150:
.. 2811.1 • 2811.2

1-801B Hl015 

### 1-8020 1-80110 1-8040 

### 1-8080**8-84-22;1~** 

# 1...,**1~00** 

## 1-6i21r 1-8Wl 

### 1-8150 H&O'J; a.B21!0 

### 1-8280. 8280**1~7~ 1~**  8S'IO; .,. 

### a.D'J621, l)tOiS; 6-



### BBVISION 11 

### 9129/94 ' : · 

### .



### VES 004426. :-:• 

### p}.RAYE'l'ER**~~Methods:**



# '"""' ; .J

. . .. .... ·. ::)


## . Acidity 

### AlkalinitY 

### AmmoDia AnioDB by 

### Ion**~pby** 

### Aab CoatAA' 

### Bromidee Cblorideo**~~** Ext;ractioo 

### J>rccedure Flalb point 

### Penaky·MarteoS cJoeed-cup method 

### Selailosh clooed-cup 

### m.elbod 

### ClevelaDd opeD'CUP 

### l'luoride 

### Pr8e c,ao;dee 

### HaJoceD CcoleDt 

### Heat Value 

### Oil aDd Grease ()Diedon-)ledul:tloo (Jiedos) 

### Po\ellllll (OBP) Pel;relkum 

### HJdrocUbolla, Total 

### Recoverable**p~** 

### . pH:M..-ent 

## Pbooi>""""**~Screen** 8otidl 

### METHOD REFERENCE

8-9H8; 2·2310 

### 2 · 2320 

### 4-850-3 

## s.sNo: a-D482'1; ..aoo . o**8-91~** 

### S.D482. DS1 7 4 

### 2-4600Br '; 4-SOO.O. S20
. 1 

### 2-41i00Cl'": 4-900

- 0. 

### 826.3 S.D1125; 4-1.20.1 HSI,O &8H9; 

### 1-1 010; &-D9S**t-1020;3-~** 

### s-D92 2...000F"; 4-SOO.O, 340.2, 

### 340.8 

## 2-4600CN1U &-))808, D2861. D4S27 &87-3 7• S.D240. D2016 

# 2-6520; 4-413.1, 

## 4ia.2 &-DU98 2-652QF; 4-418.1 2-6630, 8420; 

### 4-420
. 1 1-\lOA 9041., 

### eoci; ;**~;** 8-E'IO; 

### 4-160.1**2~F:** 

## ..aoo.o, S61U"' 8-87-38

· 2-2540B; Heo.3



### 2·2Ml!C; 4-160.1 2-aMoD;4-160.2 

### 2-2640E. 2540G; 

### HeM ll-2710F; 3-D71l.
. D8111. "Dl2l'l, Dlol29 

## 240080.'·: 

# 4-300.0. s'IU**8-87~** 

### s-D129. DS17'1, D4827 

### 1.0010A; WSOOCN'"C,G; +3S6.l
.**&-l).608.~ ·**  

### U$10; s-D26'19
. .**1-9030;~** 

### HSU 

### 8-86-815: &-D88, D446, 

### Dll98S

. &-1)96, DSl'IS, B208



### VES 004427

## .. . ..**~**



# ·,·' ) --·

. '



# ·· )**'!be~~** 

### are cleiecllbed In the 

## folowioi puN•
.. ._ 'lbe 

### lint 

### dicit fll lbe 

## ree .......... IIUIDI>en above**ore~** to the numbed..._, 

### below: 

### 1- "''eot Mel.bodo 

### l'ar 

## EYaluatincSolid Waste,**P~** 

### Methodio', SW-846, 

### Tbird Ectitlca, 

### 1986 u IIDODded 

### 11.1 UpdaU I 

### Co1ub' 1992), 

### 0.8. Butb 

# *'"'"' Prot...uan**~.** 

### Oftiee fll &61 

### Woet.e (N'l'IS, 68 Pert Ro,al 

### s-1, Springfield, VA 22161) 

### or - .-nt edita 

### or revilioo (GPO, 

### Supt. fll IloeumeDU, 

### Wl!llblngton, DC 20402). 

## ·.

'Stadord 

### Methodt f« Ilia 'Enm!n•!lm <I

### Water and 

### Wulewoter', l8lh**~** 

### AmerlceD Puhllc**~** 

### H!!flllh
....... t!an 

### (1015 FifteeDt.h 

### Street, NW, Weal>inctoa. DC 200()6), Amerioan 

### Waler Worb

7-**~klo,** Watet 

### En•il->t Fodonltica, 1992, 

### cw more recent 

### odiUoo 

### cw upclale. "AI!Dual Book fll ASTM 

### Standotda', Amerioan Society 

### for 

### Te8tlnJ ODd 

### Ma• e zWa (1916 

### Rltce Street, Pbiladelpbia, PA 

### 19013-118'1), 

# 1992,..,- recent edltico 01' 

### re"rillon. 

### "Metbodt 

# r ... Cbemleal 

### A:oaiJiia ., 

# w- and 

### WIIJfW, BPA-«X!/4-'19-020, 

# u.s. Bawb I noeuta! :, Prol«tioa 

## Joaerx:1,**~** 

### Mr.aitcrinc ODd Support 

### l.olbarai<:1r7 (Cinrirmati, 

### OH 46288),
.. reorioed 

### .Man:h 1963,
... mare recent .........., or f«<miMI ediUcn.
.. , Inbond**~** 

### Melboclln IEJU,B'I'P Prooedurell**Yam.~:** 

### Levell En>io--'IMDtal ).

- (2D4 Bdl!lm) ,**EPA~ -7** **&-201,** 

### Oct4ber, 1978, 

### « II!OI'e 

### receot edltioD.



### " hid Digeotioa 

### Bombe-", Bulletin 

### 4 7.S,

### Parr~ C'hnP"V (Moline, 

## n. 61266), or mare 

# .....,;.m buldln. 

### "Met.hoda 

## r ... Orpme C))emicel**~** 

### fllllunit:IFel IIIII lDdwolrial 

### Wlllllewaler', 

### Appmdk A fll '1\lle 40 Code ol Fedora! 

## BecuJaticmo Part 186, 

## ti. S. 

### 'Butihll .., Prolectiocl l!emq,**~MoaltoriJJclllll8uppart~Mpme** 

### r!edJimta1980
...marencellll l'1l'liol<m. 

### 'CWM

### ~ Metboclo Mauuar, Q.rmjre! 

# w..te**~** Ine.. Anal,ytbl 

### J>roeramo, September 

### 1992-



### .**at-lani-~Jtb~** 

### .. oeedweelioled ben 

## wiueh ...,l'l!'tiMcleon be**lmplemen~** upo11 

### the 

### etrectlft elate fll 

### t.he 

### 1et'
. o, wilb Mlll!ce"ah
. to 

### t.he IEPA-DLPC Permit 

### 8eetloi>. 

## ·.

WAP-A-8 BBVJSION U 

### 9129/94.



### VES 004428

### ,' 

## ...,

APPENDIX WAP · B ASH AND DRY SCRUBBER SOLIDS



# ..

. I. ' •I. • 

### - .. •



# . ..

' ··.: 

# .

VES004429' · "':' · "•



## . :' 

### 1 .0 PURPOSE 

### APPENDIX WAP-B ASH AND DRY**SCRUBB~** 

### SOLIDS SAMPLING PROTOCOL The TWI lnc:llloftll.cl destto)' huardoaa waatea in 

### bigb**temper~~ture** tberma1 cuidation J>i" Tblo procedure proricleo --..ce lbat 

### a repr....,tat!ve 181:Dple oC 

### ash or dry**~~:n~bber** 

### ooiida (DSS) io colleded 

### for**~** 

### 2.0 SAMPLING 2.1 

### Sample ldeDtlfleatlon



### 2.1.1 Each sample 

### '"""alner ia labeled with date, time oC cla,y, tompltr, and 

### con ••i- jdentjfbtjm JIWIIber. 

### Tbe IUiJpleoare 

## Joaed into lbo laboratory 

### Produetion**~** lc¢ook 

### upon 

### c1e11wrJ to lhe laboral<>ry
. 

## u Sample Collection

2.2.1 Aolt aod DSS IIIUIIpleo 

### are ccllected, aaoolyud aocl ewluoled 

### on a quuteo1y t.oio to 

### oaaure lbe ; 

### 2..2..2 &mp!ee 

### are collected 

### aa outlined in 

### Section 2.2.1 oC tbe W AP. An ...,... ia**~** uaeci to obUin**a~** aample oC lbo ash 

### or DSS. Each oemple jlr- be filled 'lrilh IOih 

### or 

### DSS.**~** 

### 2...2.8
. Trained 

### opentiooa**~** 

### .,.;n ccllect 

### tbo lllllpie ud**~** ....,., ..**~ec~p** c:ustocl,y by 

### oowpJeem, lippllcahle eediooa oCibo

_ lohoNI<>ry 

### Pmll....... 0
.**'n~-<:uolody** qbooiL 

### Sample preperation ud**~** wil be por!ormed •...., .. p '!rwNe Colowiog wbidllbo 

### l!eJ ..,.,., oC the lllh .(Sectian 4 .0) will be dete7minod. 2.3**Sam~1** 

### PC5RWbiid



### 2.S.l I\ io 

### the**~** 

### oCPedlil7 

# v..,..,..... to 

### 1111118J> 

### CllllJ qullifled pei.....el to perform lbo 

### Mh or D68 IRII2pllne 

### p....,...,a tbet 

### haft**~** lnliiiW 

### in the irnple"*Diation of lhio proceclure 

### are COIIIidt!Jed to be quolillod. 

### 3.0 SAMPLE 

### ANALYSJ8

8.1' 

### 'Each
..... wil j)o leDI to 

### a CWK or CWK iifiPIOIEd lab tor
... oC 

### IJlB 

### ccw"'>_.,; b,r 

## tbt
. "''P'vl*iiie

### ~ . 3.2 

### Tbe 

## triddua at- codoa 

# tbiousii tbtt 

### lockaeralir:ID .,.._..to 

### the incineratar reaiduala 

## wil be .._ 

## . . 

# . 

# . .in**~** wilh 

### TWI 

### St.Dderd Dl-risloc 

### Practice 161SL

WAP

- B- 1 

### .RE.VISION U



### . . W29/94 

## '· 

## '

VES 004430. · ·U 4.0 

## u 4.2 

## u


## u



# · ·· ')



# . .



# . .



# . •



# -· J. DJSP08l'J'ION OF A8R AND DRY SCJWBBER SOUD8 (1)88) 

### ADr ..,....,, of

### Mh
... DS8 Lbat wu IOJilpled for 

### tetotiDtr 

## In........,.. to the**app~opla&oe** 

### lt'""•ment standard 

### or probibitloo, will be 

### mained by lbe facility 

### until nUia 

### ere 8\01Iillollle for -··m Tile aoaq.ia 

### .-.Ita are 

## ='reel ap!Dot 

### the LDR 

### ll"h"""''lltaDcluda for lbe cocleo inthe 

## ooat•'""•· The 

### ..,.,t.Ome, ia**~if'** al t-ee'nep! 

### llmdordo ue met. Tbe**~** 

### .-.11. .,.**~** 

### .,..mot lbe 

### LDR -tii&Ddatda 

### for all cocleo IIC<epted by TWt 

## Meetiltc the

- st.oodarda Ia de.maDsltaled lhrwgb 

### the procea 

### When eompliMce with 

### the LDR 

### lltaDdards 

### bill been demoostrated, 

### the 

### 11111terio1 will be etabilill"' aud ouboequ<miJ.yclisp-" oial CWJollqlproved 

### '-nloua-**~t** f 

### =· ;,., Tbe DIIIDir..t aud 

### I.encl**~** 

### ReaVictioo 

### Tratmeol Cettj;f\eetieoo will be 

### 1 1 -ted prior 

### to 

### .t.ipnen•

WAP·B-2 

### / ( 

### V E S 004431

### APPENDIX WAP.C WABTE A CCEPTABIL1'l'Y 

## CB1'l'BBlA



# . . .

,• 

## ··. 

## . \



### · :· . · 

## . · .



# .. .

. .. VES 004432

# .. . : .



### . '



# :·.·: )

..... . ... WASTE ACCBP1'ABlLI'IY ClU'IBJliA
Tbe 

### r ollowlog Nettietiuw apply 

### to the acx:epC&oce 

### vi- exbibi*ine certain properties 

### or apecillc

- 

### u 

## T.WL Prior 

### to**eccepU~nce** 

## c- Seaion 

### 6.2>. the 

### Mandet

### 017**ADa~yMo** 

### ODd the 

# w- Prollle 8beet 

# ..m be e'f8luo&ed opiDot tbio appeudiL Alq reotrictiaos ldmt!l!ed will be doou11....,ted Oil the

- 

# ..,..,..._.t deci... Tbe 

### !itt viitem8 under eech vilheoe h
........ 

# io--

to be e:xhauortift. Tbe pUIJiLc**~** will iacble 

### a re.lew 

### vi the 

### MBDSa 

# a a -.cb 

### vi the other 

### blbliosnPhle -- 

# <- Appendix 

### W AP·P> fllr 

### o,wouw, product- common -.. 

### The ll&lure 

### ol tbe 

### .-tri<Uona are 

### aa**ro~~owc** 

## Bf.JICT
.. 7hete 

## Met - ,.... may 

### J10t be 

### proc
Thorium 

### C«DpooJOda 

# u..-um Compoonde 

### d at the 

### t •@ty.

R eclnec!m 

### materWa aa dellued by the TWI Part B RCBA Permil, ar 

### .,-er U.. jU millinda J* bour (per 8ecticn S
. U) .Perjzjt !:!spits! Wi !



### WAP .(}l ' REVIBION 11 

### MMN

VES 004433

## .... . D008 NlCd 

### J!atteriee D008 

### Leed acid 

### BaUeriee K069 Non-Calcium 

### Sulfate

Pboopboi<><IO 

## Metial }Vdllcla



## . iJIIooe6.i-roomateo
.



## i.) ·
. .-· WAP-0-2 

### BEVJSIONU 9/29194

VES 0044 3 4

## . .. , 

### ...

. 

## '· ' )

. 

## ' · 

## . : Wti/IU 

### wlDeh eahibila 

### es>e!J"tlc d>anlcteriatlca 

### (e.g., poc>pe!lmta, exploaiv-.**~** Omruneble 

### llquida, elc.) will either be**~** per \he Smell Quootity Cbemicalgolidelirww or will be 

### ..,.pte<! per tbt 

### UowJuc proc:ed\ft. When \he 

### -.olume o/a- lltl'OIIIIl or 

## c:lwla'ee ill illcinerator per!cnDIIIlCO indbteelhoi a ...... chwge 

## me io ...-...Jtecl, 

### TWI will follow the following proceclqn : l) Tbe material will be reviewed 

### U1inJ re!....,_IDCormatlou, MSDSt whee available, geaerator di"''tO'IrGo or pnvioua 

## -ieu::e
. :a-d Oil thio 

### review, 

### TWI will 

### determlne it 

### a ...... 

### eharte 

## me ia**~** 2) When It baa been deletwille<llhoi alllrger charp 

# m io**~.** 

### TWI will 

### ei1.ber. 

# ->**~** ifthio type o/materiol 

### 11M**been~** pro 

### d at 

### TWlill larger dllqe 

## "!- aDd 

### lhonbJ ••bljob a ebargoe lile; or b) c-hri 

# a- barn o/the -*'ial**to~** 

### wW dlolrp 

### .U. would 

### IMi -.pteble. 'l'llia 

### teot barn willslarhrilh !tie qtlADtll;r tlpOCi6ed in \he BQCG'o of the 

## ""'"'rile"'' 4**t~~•eot** aDd be inn ' by 

### co more Ibmdoubla the preoloue 

### c:barJo ftoGm lbia 

### " atMt!nc pciDt 

### '-"4 em lha 

### iocineo"*"'" ope.atlmd.. Tbe iM - Mor operatlooa**~** 

### whioh will be enlao&ed to det«miDo 

### if dlolrp
.. ""' be inn ! ! d will be
.. . 

## r..uo- > Y8CUl;!Dl cleCI t Ill \he prlmaq or """ 

### oodo•1 

## dw,.,;,.
. > Temperature 

### lila'' ••• ill the primary tbaber ol 

### > lOO'T 

### > . V".....t IDenupdon of the 

### l'riD*7IIMM > 

### N-otea.V o1a1A1 pia 

### flow
. 

### NOI'B: 'l'llia 

### teet pmocol OliV be utilbed to • 

### Hfeh re'fiood <Drp.., fw 

### .U**~** preoioiJob' 

# llmlleci in 

### \he SQCG ; a. 

### Teet barn 

# , ....,,_!Migj. wil be 

### potided to 

### lbe 

### IEPA-DLPC priar 

### to 

### hnrw• 

# •••.r

........ <Drge
....



### WAP.C.S BEVISIONll**~** 

## . ,

V E S 004435

### · · . DIOXIN l f.i llNG • lrute.,.tdcll Clllltaln

### ~than 

### Mlsotu.-Coa.citoe..ta requlredlmdn

### ~ IIi 

### a 1 ppm 

### tau.bDid before 80C8ptaDce.**Erbcn (2-<2.4~>-et11112,2odichloropropanale))** **R~ ~Jene.bio**  (8, 4 ,&-tric:hJOI'OI'bes>ol}) 2,4,11-t.riehlorophenc**2,4,6-~** 2,4,5-T**c; •.~-&**  

### adell**2,~TP (2·(2,~)**  propaooic: 

### acid. Silvex) 2,3,4,6-tetnd1lcropbmol Pentecl>L• opbeuolll'CP) BOJ>Del (0 ,0-dimelll;yl**Q- ~~)**  Debria 

# er..n fire 

### imol•iuc PCBo**~** the 

### rompnnnd!o lilted above Some Clltheoe- (lliMm. 2,4,6-T , ond PCP) are doteeted by**the~-** wbicb will**be~** OD diozin IIUip<!Ct 

# --per the TWl Diasio Suapeet Wute PollcJ. Additb>al - Ji8ted 

# .-..if jnc!lreted "'the**~** Oil the pro6lit iDI'OI"ID81ioQ. 

### wiD be 

# terted...., pa**~ph** It> I .,_ .



### . The 

### !<lAowi:ue are bnmd name 

### JlO'OCiuolll wbicb iDclude the 

## """'J>'U>ldalialed abaft ( 1!111 lilt 

### It DO& i · 

### WI tAl : ' -: ) be all illclllme) :



# .. 

# .,.,**'~** 

### . J
• ....

1> 

### AWCHBM AMINE 2,4,5-T 

### AQUA· VEX 

### BRUSR·BHAP 

### BRUSH.TOX DACINB 

### : · DED-WBBD

DOUBLE 8'l'B.ENGTB

. DOWCIDBS

. DOWCIDB8 D6WCIDB ' 28 DOWCIDE 

### BC-7

. DOWCIDE 

### G-8'1' ENVE!n'DT ENVI!lln'T 

### EMUI.8AMINE BK 

### F..STBBONB FAIWCO FENCE RIDER 

## FENOPROP FOBRON FRUITONET INVERTON 

### 24!>

. KUBON

KUROSAL 

### LlNBRIDD 

### PZNCBI.OR PENTACON



### . PENWAll PRILTOX 

### REDDON 

### SANTOBRITB SANTOPBBN 

### SILVl · RAP SINlTUHO 

### SPONTOX 

### SUPER D WEEDONB 

### T·NOX TORMANA 

## TaAN!wo:NB TlUBt1l'ON 

### TBINOXOL U48**VEON~** 

### VE!lTONzr VlSXO BRAP LOW VOLA'ltLE E8l'.l!3 

### WEEDAil WEJm.&GONB WEEDBBADS 

### WEEDONB 

## . . 

## .

BEVISlON 11 

## wwc

VES 004436

## . . ;:

### ..

APPENDIX WAP-D DE'I'BBMlNATION OP INCOMING WASTE

CONJ'OJtMANCEINONCONFOftMANCB

:

,.



### . 

## ..

. 

# .. ''.)

_,

VES 004437

### APJ'iENDU: WAP-D INCOMING WASTE OONPORMANCE/NO N.CONPORMANCE 

### Imwnine

- Dll\1 _, from the iDCOI'IIIIItion determined 

## durini the pro6JiDc pbue clue to the 'flll'W:Iility ID the 

## ...-.o**~** the waste or ID eo!!.,.. ion of the wule 

### DllllerW. lD CC'der to cletenDiDe wloelher a partloulat iDcoming woste stream ccofCrmll to the ia'ofiJe, the 

## folll>winc oitaia wil be U8ed. 

### AI other Mandatory 

### IUid Supplemeotal**~** dala colloeted ..;a be 

### .-1 to allow TWI to 

### c1eUnDioe the t.e.t metbod 

### for ...-;ng tho W8lte material. 1.

2.



### 3. pB &neg: A**~** 

### in the p H 

### from the """" oped6ed 

### in the profile docwDenta ms,y 

### iodi<:aSe a 

### eiJance ID the - ......,. Jt a pH 

### variation**~** the 

## ranc- opec:i6ecl on the tiquld pro6le sboel, the procedures 

## outJiDed in Sectioo 5.2.4 will be IDitlatecl (e
. g., a - which ;. td 1111111:1 neutral ;. fOund to be corrooive ).**Material~** will be eva1uatec1 for oonrarmance oo 

### toOowr. 

## PrnCWnc t\nehrtim' 

## RaWi Acceotable 

## Brmm <2 <2 

### 2-12.5 

### 2-12.6 > 1.2.5 > 12.5 

### W- prdlled aa pH 

### 2 to pH 

### 12.6 but 

### ahiwed with

### an~ LDR 

## filrm for IlOQ2 

## wli be CGDII<Jeled coofonning 

### at pH <2 or pH > 12.6 

### i! 

## oawortoc1 b)' the prc&cl 

# + · e! 

### caaotlh_., nMnmnbi!jb Poteptla! &mq; 

### A variatiOil in the lbermaiiii:!Mty from the fndiretrn OJ*.;IIed ID the prollle**~will** indleate 

### a 

### +a,.. in the -..,-. If the ....atian 

### ...,_a change ID the buard .-. of the -, the poocedures outlined in Seclbl 5.2.4 will be IDitlatecl (e.g. a



### . mot ill wllitb did DOt ezbiiJil n """tty potertW ID the 

### prallllo, pbMo doea 

## ciur1D1 the 1,;.,..m,l l!bipDeDt**.**



# -- rit ladlii.te
....**~the-** oiHaa, will+ 

### ....,lid 

## llillwe
.the
.. oc:eoturo. .oulbd


### '
. ' 1D 

## Sec:dooi U.f. 

### Twi ;. Dot 

# P!"'JJ''lted to accept 

### PC8e > 

### 110 ppm or 

### TSCA deriYed 

### PCB -. 4
. 

## Bed! ·"viti 8cqea.; 

### Tbe preaenoo**of~malerialaMdelermloedi'JtheriOdio«tiwit)o­** (- Seedoa

### 8.1;~ wllllal&te the procedureo M 

### aullined 

## lza 

# 8eclloo! 6 . U, 

## leedint to rej 

### z 

## :fiC n cltbe
. 

# --

WAJ>.l)·l 

### RIM8lON 11**~** 

### ...

V E S 00443 8

## . . •'

' 

# ..**bnnmnt~** A 

### oi«P' 6 •rrl. 

### -wion ill tbe appareul 

### cis :oity 

### 6:<D that 

### optOIIed ill tbe 

### profile docuii'Mt.a 

### will 

### iDdii::IHe a cUnp 

### ill tbe wut.e 

### -lhat wwld 

### iDidate tbe

# ~ outlioecl ill 

### SectioD &.U.



### BBVISION 11 

### II/29/IK ' 

# I

VES0044 3 9', :



### APPENDIX WAP·B



## .. ... 

# .. . : 

# .**·** 

# . .

VES 004440

### ·-


# · ·) APPENDIX WAP·E CONTAJNEIUZED WASTE: SPECIAL 8.UIPIJNG PROCEDUIUI:S 

### 1.0 PURPOBE This procedure providee --=e that 

### r c po eeectoU.c.......,. oCihe 

## fallowiae ecmtaiDerilrllcare 

### colle<:ted for 

### Specifioo!lr, thMe are 

### CODiai:oerised

- oC 

### delft aDd 

### llU IDII&erilll, adhO&iveo and other 

### bigbly elootie IIUbNDces, 

### aDd 

# ....ma 8lld other bard lllll&erial&**~** 

### sam p

leo ..,.. eonee\ed by 

### llliDe rou1tipoiat 

### •"tiline
2.0 DEPINlTIONS

8
. 0 2.1 Debria and 

### like 

### moteriaJ • inclo.W wood, 

### briob. <.OQOI'et.e,**~** 

### pioollc 

## ebeoq 2.2 Adbeoioea aod other 

### hicbi.Y elut.ic tt>IOteriall· otlck;y, 

### cJue-like, IUil>IIV', otretdlab6lt • iolll. 2.8 Reoinl aDd other bard maleri8lo. piMtice aDd 

### pla8tlo OOIDj)OIMDtl, 

### epoDes IIDcl otiMr jll;
. 

## 111 llmDar me1erlala that 

### ba-fe hardened 

### or eured 

### t

. 2.4

## U.,JUpoiot...upie·Atample~oC.,,._ , .... 

### .,.,u..tedtr-tbe......, 

# ib.t

INSPECl'ION 

### Eech eonta!Mr ..nl be ....w.ted prlor 

### to opeaiDg 

### to detenDiDa it ' a 

## illl.ecri*7. Mter opening. 

### tbe cooteiDer'o c:aatente wiD be viauolly ;. 

### It 

### r led lo c1etermiDe 

### wbother

- cr - it ....rormo with it.f proliled deou iptiuu. 4.0 J'ERCENT 8AMPLBD See WNte**~** PIIID ' Sedioo U.



### ·. G.O 

### 8AMPLI1fG • 

### .Multip.mt

_ lllliliploe ce i apeo 

### lh• 

## -rir be 

# cohtec! · tram

### coo~ eelee!ecl 

### for 

## i'"'c
.

. 8 

## •"'1"'nr-eirit 

# *"* wiJ be aeleeted 

### beeecl 

### ce .-.Ita oC tbe inopecticn 

### Rw11qM will 

### be Ia 

### CWM



### c:uolod7 &,. tBmple enl!ectjon 

### UDiil t.raDoiCer 

### oC cuetod,y lo 

### tbe**~** 

### flea · ..... . 

### . .



### RBVISlONll 

### 9lllllr9' 

# '

V E S 0044 41

# ... : \

.. I


# ... · 6.1 

### HIGHLY ELASTIC SUBSTAI'fCES Allbelliftl 

### IDd 

### odw 

## biabl7 elaatlo
..... •• .. 

### will 

### be -mp!ed wilb • 

### acoop at**~** -' ocioeon 

### or l(qL The pr<x:edure ia to: 6.1.1 dip tbe obovel at 

### acoop inl<> the material I<> the cleptb of the blade and 

### .-e; 6.1
. 2 Ill\ tho acoop at ebovel with the oample aDd 

### cut with the ......., 

### or taop, _ • appropriate; 6.1.:1 wind the boqiiJc partloD ol the S8IQple 

### cato tbe acoop "

### ar......,. 

### aDd lnllllfer 

### the**~** 1<> 

### the 

## -.pie....,..,;._ 

# by.......,. tbe maWial 

### &om the abarel 

### or acoop into



### 6.2 DEBIUB AND LIKB MATERIAL Delrio """ · lite JDIIierials will be Mmplecl with
........ hammer , c:biloel 

### aDd**~clap** .. 

### appoplase. The procedure io to: 

### 6.2
. 1

- hammer 

### 81111 chioelt<> coiled IIIIDJ)Iea 

### ol wood, lllicl< at otba- bard ma&md 

## froc>mitbe
. 1<>p of 

### the ......,mer 

### IDd pl-. 

### iD the lilmple 

# cmtn- with 1a11p; 6.2.2

- ........ 14 

### cut 

## -DJ!Ie ofc,.ekead 

### GdlerflMiib' cublble
_ ....... 

### (pw!dfnc rubber , piMIIe
... 

# ·&.., ece.)-' plaee 

### ill 

### IISQille.. !ol rl with l<lap. 6.3 

### RE81NS AND/OR OTHER HABD MATERW..S Reodos IIDd/or other bard**material~** will be _..ped 

### witb a 

## a-, c:biloelllllllt.qp at 

### acoop. Tbe procedure la to: 

### u.t 

## u .. .

## ~ 

## ..i4 cblid 

## w redDce 

## lllliterioi1W ibe

## t~t"i&:~**.** 

# -or be piloi:ed 

### iDa '



## . 

# .**~** 

### •elMo 111111 plaee**the~** 

### iD 

### the'""'' • • 

### w1t1i )""P 

### or 

## oooap.

· · 8.0 

### SAMPLiNG'PBBSONNBL · It io 

### the '"I • Ulty of. Fedlity Mr 

### J • I 1<>
...... aoly qualilled periOilll!!l 14 perflip" 

### I • • jili 

### C ofCGI!IIIIilwiJed-.**P~** tbatblrfe beeD tniDedin 

### the implementation oftblo 

## JII'CIC8CliiN

- ,.c edt<> be 

### qualillecl. 7.0 SAMPLE ANALYSIS Samples 

### will**be~** • 

### rptcifled in 

### Seetlom 

### s.t, 

### U. *>II 

### S.S. &Ill! 

## l'IJure 3-1 ot . the 

### WAP
. Ml*boal**~** 

### wil 

### be 

## per{armid !It 

### the nque1t of**the~** Vmpnnl 

### REVISION 11 

### 9/29194

VES 004442

## . . 

# ·- ·

' ' '>.



### . "

I



# ... : 

## .·· :' 

# . . '.•.}·· 

## ·. • 

# .. 

# . .

..... . ..

... APPENDIX WAP ·F \

·"



### V E S 004443

### APPJ!INl)IX WAP·F BJBLI()GBAPBY 

### OF 

## 8'l'ANDARD CHDIICAL JtEFEJlENCE MAT"Rxa.LS

2.

# ~Properties of 

## :IJiduslriol Clw- • h, 

### CurRDt 

### Bdltim 1989, V111 N-d 

### Relllbold. NY NY.

5
.



### WAP ·F·l 

## · .

VES 004444

# , .·

APPENDIX WAP -G BM

- 18 1 CO MPA'n,BILlTY 

## CLASSES**'~~** 

# .. ' )

. · 

# .. • • > > ' I ' , • 

## . .
' • '' . ' ' 'I 

## . 

# .. . 

# . ....

. :. \



# . ,/



### VES 004445: t'••

1.1

- 1.6 

### :U-2-2 8 

### (. 1**.2** 

# • .

s ' 

## J 5'.1 6.2 

### 2.3



# .. 6. 1 8



### , . .**~** 

### II 

## ..·: ,



# .) :APPENDlX WAP

- G
ml

- 181 COMPA'l'IBILTIY 

## CLASSES

., 

## . . . Jl\ali,mable Solids**~** ()ombustlblel 

### J>aocerous When 

### Wet

P....,...... G8s 

### z..,., A & B



### Couosi ves

. ·

## N.O.S. nebrll
. . ·' Nl"'!Hazar'4louiollaleri81
.

. 

## .**~** • ••• ','
. -¥ '

### :·**·.~:· ~.:**  : : ·:

### ;.**;~**

### ;-**~.** 

## . 

# :**:~·~~.** 

# . ..

BEVISION · 11 

### lll'l9J9'

VES 004446

# . '



# ... @

")



# ) CHEMICAL WASTE MANAGEMENT PCB SCREENING 

## POUCY



# . .

. '

R evis1 Qf11 October 

### 1991 :;**~ ~**  

# .. ... · 

## . .

• : ._. 

### VES 004447

# , .)



# ..

. . •



# ... . )

. 

# . . CWM P CB SCREEN I NG POUCY

L I NTROD UCDOii 

### -rhe Toxic Substances Control

### ~ 

### (TSCA) is 

### the 

## prirniry SOUI'ce of federal 

### regulations affecting the 

### management of Polychlorinated 

### Biphenyls (PC Bs). Most of 

### the 

## provisions of 

### the 

### TSCA 

## reg!Jialion$ specified 

### In 

### 40 CFR Part 761 

### apply to PCBs 

## cx*'f if PCBs are 

### present in 

### concentrations 

### above specified 

### levels. 

### The 

### 40 CFR Part 761 subpart 

### 0 Storage and 

### Disposal 

### provisions apply 

### generally to materia l at 

### c:oncentratlons of 

### 50 

### parts per 

### mllion 

# tppm) aile! above , However, no provision specifying a PCB concentration 

## may ba avoided 

### by

_ diluting PCB containing 

### materials unless otherwise speclficaly provided
.



## . 

# . Furthe rm ore. 

### the Resource Conservation and Recovely 

## Act (RCRA) is 

### an ' 

### additlonal source of fedefat 

## regu l ations affecting 

### the management of
. hazardous 

### was te containing 

### PCBs
. 

### The land 

### disposal of liquid 

### hazardous wastes c:ontanng PCBs 

### at ccincentrations greater than 

### or equal 

### to !50 

## PPf:11 is 

### prohibited 

## i.ndec' the provisions of 

### 40 CFR Part 268
. 32 (a)(2). 

### The land 

### cbPosal of 

### liquid or 

## nonliquid 

### hazardous waste containing halOgenated 

### aganJC**~** 

### (Hoes) including PC B s (see 40 CFR Part 268 Appendix 

### 111
. for 

### a 

### listing of 

### H OCs) at 

## concentrations equal to or greater than 

### 1 000 mgiL. 

### or 1 000 mglkg , respectively, is prohibited 

### under the pr!Wislons of 

### 40 CFR P art 268.32 (a)(3) ; (e)(1)
. 

### and (e)(2) the 

### "Callfcma 

### Ust.• In addition, 

### the management 

## of liquid 

### hazardous waste


## . . . . 

### containing PCBs 

## at coocenlralions 

## of 50 

### ppm or 

### above as wei
. 

### as liquid 

### or non 

## licjuid h;llardous wastes 

### containing HOes 

# lnC:IudihQ PcBs (see 

# 40 CFR P art 268
.

. Appendix Ill for 

## 1st d HOCs ) 

### in ICtal 

### c:oncentralions equal10 

# ar gre at er 1han



### 1000 

### mg/l 

# Or 1000 

### rng,1<g 

### lor liquid or 

### eoid, relpiG1Ivefy, 

# n apeci a, d under
. 

### !he
.

## pr~ d 

# -.o CFR P art

## ~42. 

# ·Flrialy; 

# the land 

### dispo s al 

## d 

# haiar.oous 

# waSte c:ontan1g 

## • PC8s IWld identified


### . by 

# hi listed 

### hazardous 

# waSte cede fUilbeis



### · K065 IWld 

# F 009 (multi-Gouice leachate) 

### Is regulated under Specific Land Disposal 

## Restrictions (LDR) prcMslons under 

### 40 

## cAA Part 

# 268. 43
. Th ese regWilion$



### - require 

## PCBs to 

## b8 treated 

### to 

## the folowing levels 

### (Table 

## Q 

# Prier tO land 

### clspo!ial
.



### 2 

## Re.vislon

. 1 

### October 

### 1991 > t



### . -

VES004448

## .......

' 

### )

I •") 

# . .
I • • • 

### PCB Screening 

### Policy 

### TABLE I Wast e Water Non-Waste Water 

### K085 & 

### F 039 mg/L

### ~ Aroclcf 

### 1 016 0 .0 13 0.92 Aroclcf 

### 1221 0.014 0.92 Arodoc 

### 1232 0
. 013 0.92 Aroclcf 

### 1242 0
. 017 0 .92 

## Arodoi 1248 0
. 013 0. 92 Arodor 

### 1254 0.014 1.8 

## ArOdcx 1260 0
. 014 1.8

State and 

### local agencies and 

### permits 

### may also 

### regulate the management ol 

## PCBs
. 

## Conllfiance with 

### these regulations is 

### recjuir ed 

### wflerSYef IIley**~** 

### more

. stmgent 

### than federal regulations (e. g . , certain states 

### req&n that 1he PCBs b8

reported 

### on a 

### dry 

### weight 

### basis ). Additionaly, 

### TSCA 

### adchisses 

## PCBs , 

## rlot Arcc:lora:
. This 

### irdldes Flti\ieillalty .produced 

## PCBa ..:1 foreign prOduced 

## mate dall 

## that inclJCfe Clophtu • . 

# f'henodor •.**Pyra.e.,..~** 

# Kaiilctilor •. ainct fflllCior-
. . . In 

# cxder to assure that 

### the appropriate 

## praCtices are 

### beiilg 

# appied 

# c:oniislently

. . 

## . 1hrougllotA

_ ChelniE:al Waste 

### Management, 

### Inc. ( CWM) JIIQ8idi 

### .g the management 

## or wastes 

# which. may**potentia~~)'** 

## Contain PCBs , · 

### It Is

## ~ 

# tO 

# der.ne**pr~** to be 

## 8fTlliOyed 

## ihrougllQUt the

# G!Pi**i~ IY-**  

# lherifore, the 

## tobw iug Policy and 

### P rocedur es 

### has been develope d.



# . · Re\<iSion 

## 1
·**Octo~1991** 

### :



# . .



### VES 004449i 

### '



## . ..



# ) PCB 

### ScreeriRg Policy
, 

## . . D

. POLICY
. A. 

### The trealmeri, 

## swrage, and 

### disposai 

### of f1n1 

### TSCA regulated 

### waste 

### shaD OCCU' 

# ort-t at a 

### TSCA apprOYed 

### treatment. storage, or c:isposal facilly. 

### B
. AJ 

### PCB analy$8$ 

### required as a 

### result

_ of the appk:ation of 

### !his policy
. shal 

### be performed 

### by a CWM 

### laboratory 

### or a CWM 

### apprCMid waste 

## liboralory
. C
. 

### ArTy waste 

### !hat 

### will 

### be analyzed for 

### PC8s 

# r. acc:crdanc:e with 

### thil policy
. 

### shal 

### not be accepted 

### for storage, treatment. or 

### disposal 

## IXIIi 

## PCB analyses 

### have been 

### complet ed and 

### evaJuatad. D
. 

### ArTy 

## non- TSCA waste 

### which meets 

### the 

### following 

### criteria shal be 

### treated as 

### a PCB suspect 

### waste uoti demonstrated otherwise, 1hrough cnemlqll 

### analysis
. 

### II/. 

### PCB SU SP E

C T**WASTE~ ·**  

### The following

## ~ have

## ~ deYeloped 

### by 

## Cheri lical 

## Wast8 

## r.l'anagemeri.. 

# nc. through 

### its 

### extensive opel 

### atiiiQ 

### experiences as 

### wei aa 

## thrOugh r eview of various 

### &ources of 

### literature for 

### deli ling 

### a 

## WIISte as being 

### PCB Suspect 

# n-e aleria 

### are intended to

### ~existing 

### requirements which 

## may 

## have 

# beeO Imposed through pennlt COIIdifloc IS ,

## ~inlstraliYe orders , or 

### CJiher

## ~ill 

# Mh 

# federal or state 

### regUatory 

### agencies
. ·


## krf 

# wasta for 

# which the 

### genetator 

## hits**~ed** on 

## th8**"Getierator'~** Waste
.. 

## Material Profile 

### Sheet" 

## -0!**~n~ '**  octllf 

## MJppOf1ilg doc:umlnralion ' 1hat 

## Pees are J)fesent 

### below 

## regt.Aated levels. ·**Re~ision** 

### 1 

### 4 October1991 :



### VES 004450

## . ... ... . 

# , ·



# ( )

( 

## .; .)

,> 

### PCB Screening 

### Po licy
B
. 

### Oi Bearilg Waste NOTE: • 

### Oi bearing 

### was1es are defined as 

### any material (Tquid, sofld, organic, or 

### aqueous) 

### conlai!Wlg 

# oa as descri)ed 

### on 

### the "Genetator:'s Waste Material 

## Profile Sheer (other supporting documentation) OR 

### any material which 

### exhibits the 

### visual presence 

### of oil. 

## The visual pre sa nee 

### of ol 

## may include, but is 

### not limited 

### to , an oil 

### emulsion, oil 

### film , oil 

### phase, or water soluble oil
. 

### It 

### is the responsibity 

### of 

### the laboratory Manager at 

### each divis ion to use sound 

### judgment based 

### on their analytical 

### experience 

### to make 

### the final determination 

### I a 

## waste stream 

### exhibits 

### the 

### visual 

## presence of 

### oi. C
. . Municipal Waste W ater Treatment Facility Sludge 

# D

. E. 

# F

. G.

; 

### Bulk Laboratory 

### Wastes BaghoUse Dusts from Secondaly 

### Smelters (e
. g.! copper, aluminum) 

## Afr.J Waste 

## as Designated 

### by**~** 

### L.aboretory Manager All 

### Wastes , liql 

### ids or 

### Solids, from 

### the following: 

### 1
. 

### Electrical UtJiity Company 

## 2. Ncltural 

### Gas Pipeb Transmission Company 3. Solvent Recovery , 

### ReuSe or Recycling 

### Unit 

# 4

: Oi Recovery, 

### Reuse 

## a R8eycling Unit 

### 5. Oi 

## Maintenance 

## CenJcn 8. Pond Cloel.res**[~** 

### Pond SludgN 

# n Dredg iu

gs)



### . 7.
.**Remedial~ ~Sites**  

### · 

# a RCRA 

# Corrective Adion Prci;eete 9
. . . Trrtler/I..Lmber Treating Facility 

### 10. Hydraulic 

### Equipment 11. ENAAC 

# Remedial Action 

## PrOtects *

• Unless demons1rated 

### non-TSCA



### 5 Revision 1 {)c;tobe( 

### 1991 

# . .

\ VES 004451

### P C B S cr een ing P olicy
12. 

## Heat Transfer 

### Un its 13
. 

### Me tal Machiring (Cutting) Ope ra tions 

### 14
. 

## P esticide /Herbicid e Manufacturing 

### 15
. Ink a nd Pig m e nt Manufactur i ng 16
. Oil 

### Based Pai nt Manufacturing 

### 17
. P aper Recycling 

### Oper ations 18
. Roofin g 

### Felt Manufacturing or Processing 

### 19
. Auto 

### FJull 20
. Non-WMI Waste Tr eaters 

### 21
. Chlorobenzene 

### Manufacturi1g 

### IV. F'ROCEDURES 

### A. P r e-Acceplance Samples 

### Pre-acceptance samples are 

### to be 

### analyzed for PCBs 

### by a 

### laboraloly 

### i f
· ' ) 1tle 

### wast e stream 

### meets any of the criteria 

# spec&ci in 

# aectlori Dl 

# aboVe :

..



# ..J B
. Incomin g Was t e Shipment 

### Samples 

### The need t o analyze 

### incom ing waste 

### shipment samples for PCBs 

### wil 

### be



### ..

estabished by the

## resu~~~ of 

### the


### . sales 

## sample Wlllyais 

## and**·~** of 

### the sales 

### sample Waste Profile 

## Sheet
. i lfounatiOil against 

## 1tiis policy
. Table R d es c riberithe 

## overaD 

## requirements discussed 

### below
.

· I( 

### a waste

### ~ 

### doel 

### ncit meet 

### 11f1J of 

### the P.CB
. auspect 

# crit,rta; 1l)en



### there 

### is 

## no specific

## ~.tll'l'llri to 

# Perform PCB ' analysj!S 

# on the : rnco.,)i,g
. 

# shiPmet 11s 

### of 

### this 

### wast e 

# stream uliless spec:ilicaly required 1n:1tr 

### a Waste
. . .**AnalYSis~** 

### (WAP)
. . . .

6 

## f!evisior\ 1 

### Oct ober 199 1 

## . '

VES 004452

# . .... ,



# .J PCB 

## Screening Policy If a waste stream meets 

## any of the 

### PCB Suspect Crheria and the sales sample 

### analysis indicates PCBs 

### are less than 

## 5 

## ppm ' or the 

### regulatOf)' limit (The**EP.~** 

### TSCA office has 

### recently specified coricentrations of 

### less than 2 

### ppm PCBs 

### in treatment r esidues for 

### approval and refer to 

### Table I for listed code 

### specifications}, wtlichewf 

### iS lowef, 

### then the 

### laboratoryJtec;hnical manager 

## must specify on the Waste 

### Management 

### DecisiOn (WMO) 

### whether PCB analyses on incorring waste 

### shipments are required 

### and, If so, 

### the 

### frequency of 

### analyses
. If a waste stream meets any 

## 0! the 

### PCB Suspect 

## Critlfla and
. 

## tO. sales sample analysis indicates PCBs are above 5 ppm ' 

### or the 

### regulatory 

### imil, whichever 

### is lo wer, then 

### the**laboratory~echnical** 

### manager must specify on the WMO lh!ll 

### P CB analyses on 

# incoming waste shipments 

### are required and 

### the frequency at which that 

### analysis 

### is to 

### be performed
. 

### It 

### the receipt matenal demonslrates a change 

### in 

### the waste from the 

## preacceptance sample and It**now~** 

### the 

### PCB suspect cr11eria, 

### then PCB analys i s 

## must be performed before treab neut. 

## atorage, or 

## dispoUJ
.



# . · 

## ·.

• · The specific c;rilerlon of 

### 5 ppm is the**~** 

### laboratory repol'ting · 

### Umit for 

### PCB analysis. 

### II is a 

# conServative approach to protecting 

### the integrity of 

## non- TSCA 

## facilities
.

Revision 1 

### 7
. · October 

### 1991. 

## \ VES 004453

### ?CB screening 

## PolicY



# .. )



# - . TABLE II



# . WPS

# ~

1WMDI N

o ActiOn llequir • d



### Meets PCB Suspect 

### C riteria * Sales Sample 

### P C B Anults 

# No Yes 

### < . 5 

## ppm



# .. Yes 

## >5ppm . PCB Suspect 

# • UI> D•• 

# c_.,o....,..., .......-' 

# -- >!i-PCI 

### <IIIP"'tcl I Yos • N o I I Yosl 

# ' ...,- IWMDI IWMDIIIY II**Fr~Cl'** 

# ,,_....., ol TutinO of Tutlnll



### R eceiving P r ocedures

No 

### specific actiOnS 

### required. Specify in 

### Waste Managem8nt [)eclsion 

## ·**~** 

## Whethtf 

## PCB. · analyle& 

## on**~** wa5te
. 

## shlpineniS are 

## required '

and. if 

## so , the 

## frequency of 

### ii\alyseS. WMD 

## must specify that 

## PCB

## ~ses are required on intX)mk'lg

# wasta~ ilnd must 

## specifY the frequency of 

## thO$& analyseS
. .
• or the r egulatory 

### limit.

## w~ is 

### loWer
.



### 8 Revision 1 October 1991 

# ..

VES 004454

## ·.· '\



## ...



# . .

. , :


# )

•' 

# ..... ' 

# .. ·.



# .,

# ~· WU'I'Il

# :~•curaaa:~xOII D:IOX:I. 

## SOSP&cr
.. aLYSXS pOL:ICY

. ... 

## .·

' ·: 

## . .. . . · ..



# . . ''

' 

### · . · 

# ..

. 

## ' '
.



# · e ,..... ..**~** 

# ...
. . 

### VES 004455

# ,,

\

'.



# ' ) I
. !WI DIOXJB AalLYSIS POLICY lJftJIOIICJC! lOll 

### Trade Waste Incineration ia impl...atinv thia policr for the screening of waatea which mar contain dioa.ina. This
. policr wil l i den tif r the trpea o f waatea vbicb .u.t be 

### analraed for dioaina or dioain
. preouraora prior to a.,roval for ac c eptance aa a vaate atre- a t 

## • nu . IIIPl-tatiOA of Wa p o licr wU 1 P

. roYide a -aaa o f ensuring that potential.lr clioain contlllllinated vaatea are analJ&ed for dioun content aad**suba~ nt** **lr** 

### .anaged appropriatelJ a c: cordinv to applicable state and federal regulat i ons. The final deciaiOD to -.nave a dioain bearing waate**~~~&at** 

### be ucla aocorclia.g to _ the co nditions and restrictions of the goveruing facilitJ**W~e** 

### AnalJaia Plan and
. 

### o perat i ng per.ita
. 

## 7 , 

# . . II. POLICY A
. Waate atre- oont aplated for ..n.g-t a t TWi Ifill be 

### aub j e ct ed to the Dioain suspect. Wute Criteria during the deciaion evaluation proceaa of the profiling procedure
. B. lfailtu vbich are d eterained to .. et the Dioliin Slulpeot Waate Criteria will**r~re** 

### analraia tor dioain precur.ora prior to acceptance and 

### -.nav-t tor treat.ent aa.d cliapoaal at th e taoilitJ
. .**~** 

### . 

### c . · wutea vhioh
. ara fou.nd to**conta~** 

### dloain**precurao~a** 

### at or above tbe aita**a~i-** 

### level for prec:uraora vill require clioain .a.alraia prior to a ccapt&Dc e &Del 

### -.nav-t for treaa.., , -8nd · fia;oa&l at tlae ·**faaili~J ·**  

### • . . · 

## . . . D. Wutea 

## vbich are found to cont aia. cUoJ!ina at or

# ~**tli~** rite actiOD level will not be 

### accepted for winav-t for treat.&Dt and
. 

### diapoaal at the facil!tr UDtil auoh ti
.. that**t~ea~t** 

### and cliapoaal
. are allowed accorclint to the conclitiilna &Del 

### rutdcticiu of the govemia.t facilitJ Waate AD&lJaia Plan and 

### operating perait.a. ; 

### '

VES 004456' ' 

## . .

. 

# ..

. 

# .

.. 

# . . 

## ·•



# . J

· . The f o ll o wing cri teria has been devel o ped for defining a waste u di o .dn au.pect. Theae crit eria ere inteaded to a u pp l -u t niating 

### requir-ta which •l' 

### have been**i~oaed** 

### through**pe~t** 

### conditiona , adminiatrative orders , or other agre ... nta w

it h f · ede r al or sta te authorities
. Waataa c -.idered under these crit eria**r~n** 

### . subject to all eaistin9 con diUoua i mposed bJ Chemical Waate

- MaDav-t polioiu aDd 

### anv iro a.antal directives. A.



# • •• OaDarator Defined Di o zin Was t a. ADJ waate for whi c h the 9BDerator baa indicated OD 

### the " Generator's Waate Material Profile 8haat" or &DJ othat supportiD9 docn.entation that diOUDa Or diOJI!i!!la precuraora are prea-t · at &D7 level -. 

### < r 

## .. . 

# . lfaataa PrOia the P o llowiuv : Thea• waataa · will be couid!ared u 

### suspect if 

### theJ
.. , · have beaD 

### subject to historical oonhaiDation frdiodna o r di o :r.bi precursors , or if the waatea c ontain a 

## known dio:r.in or dio:r.in preouraor aatarial
. 1. 

### T i mber/Lu.ber Traat in 9 Pacilit i
.. .**~** 

### P_.ticide / Berbioide**Nanufao~urinv rao~litiaa**  

### • 3. 

### HaDufaeturara

_ or Prooua.- 

# u.-inv t

. ...... <:": '-.



## ..·, 

# ..... . .

, 

### . .. 

## · . .



## .**~ ··~** **:** 

## . a ) · 

# aciiao- , di- ; tri- , or tetrachlorophenola , aDd · 

### their chloro-pbno:r.y
. dedvativa aoida,
.. tara , 

## ·**~** 

## :' ui4l otllft 

## ·. S.lta
. · · · · · · ' · · 

# b

)**..-ta hloropal** **·.** 

### · · · · · · · ·· o), ·· lllillo-
. . 

### di '"; 

### trl -, · tetra- , PBilta -, . o r**bauclal oro** **beluaD~ .**  

### . , .· . d )'
... ,· tdchloropheDo:r.nro pionio acid
. (ailve:r.) ·. . ... a) 

### '' trtch.or 0 

### pb.eoaJaoeUo acid (2,
... 

### ,5-T) f ) · · lae:r.achl orophene ·



# . • .**c~ucia** 

### · prodlac:ta fr- aoucaa**ciu~aide** 

### of the 

## Clfll/lllli 'l'a o lmo lovha faailJ of c 

## :ct .. where •11ch cotlbutioa o

_ courr:ad 'lllldar**acontt~lled** 

### conditiou and 

### the for.atiOD of dioaina or: dioain related cOIIPOUDda ia 

### auapeotlicl · to 

# Jaave · oonned ( i
. e . the : ootlbution of PVC , Cl'VC , 

### 'etc. ). · ·

· C
. · 

### Wutu

## ~dil9 

## u&**baser~** nata 

## nililben r032 , P039 ,

· ltO
. Ol , lt015
. &011 , .K030 , · JtOU , lt043 ,**ltOI~,** 

### JtOt9 , UOS ,'
. UU ,' · ltUO , aDd 

### ltl51
. 

# . . '**~** :-:. I '



### . 

# . - 

# .

. 

# .. , 

## , , •,



### VES 004457'·;.**.~ \** 


### . . · . t lV
. PROCalftU 

## &. Precursor Analysis :

'•, 

### Dioxin precurs o r analysis -Y be c ondu c ted by llPt.C ; CC or CC/ MB , or i-oassay scr- techDiquas follow i ll9 •pprove4 ID'A •thocls o r CMK -difications of aueh •thocls. 1
. Profile Approval
. Samples : Profile approval s ... laa are to be analysed tor diodn precursors if the waste stre- -ts any of the eritar:ia apecified • :hl section Ill above
. Wastes which are beipg nprofiled or raeertified dua to ohanvaa ill 

## U... process gaaaratill9 the wasta , or u a raault ot generator**iafo~Uon** 

### gathered duriag t!l. 

## ajp-**onfo~ce** 

### resolution duriJW ' iDcc.Uag aulyaia 

## !iF• also subject to the cr:itada specified in saotJiGa 2 . Ill
. · '1 

### Illoc.Uag Wuta 8biPMDt
.... 1
.. : a) t'ba 

### need to ualr•• 1Dcoii1D9 · vuta ahii-aat

.... les for dioaill prac:Uraora will be



### .. tablial:aed by tl:aa r .. ul ta 

### of tl:aa profile approval s ... l• &Dalyais aDd 

# aa avalU.tiOD of tJ:aa
. wuta profile abaat
.**illfo~UOD** 

### agdut · tl:aa criteria
.. tabUabacl ill this poUcr ·. ....



### _ b ). If 

### a vuta str.- cloaa·
. 11o
. t .._.t ,_ aar ot · the
. ·.criteria
.. tabUabacl- ia secUOD til 

### ot . this policy , thaD 

### tl:aera
. 1a 

### llO jpaoitic raquit...at**~** 

### pedom 4i!)alll
. pHCII&fPr -1-raia Oil the



### ·- ,f.Ac..Ua• · shi
. ,._t. s ... laa · ot

## the**tl~tla atr._,** **.** : . 

# ;::'J --:'·

• ' ' I, • ••• • , ' ': • • ' '',· ''·. ' • ' ' • ::



### c)
. ·.**i~ ·**  

## tJ:aa**~ecetpt** 

# -ter.tiil

_ ci..,..trat 'aa**.: ctiallt•** **#-1-fr: ~** 



### . . iJi.
. tl:aa vuta fr• tM · profile approval
.... le •.**~**



### d ) 

### · u . a. intonation prodded
. br t

_ ll8 eaaerator · .. ·:. during
. the aOD-COilfOIWU.Clt r .. ohatioa**pro~aaa) .**  

### allll 

### . it aow ._ts tb criteria

· -..tablisha4
. ill sactloa Ill of this policr , thaD 

### -dioaill · precursor ealrs
. ia aat be



### · parfomad u · part of the inc.tQg aulr•i•
. Wastes**vhi~** 

### Mat the criteria eatablisiMcl · iD lfaotiOil Ill of this poUor
. aDd 

## ti.hiC:rh a:ahibitad negative screen results
. for dioain precuraora darbg profile
.**appr~val** 

### anahaia will not bil · ·.



### · ., acr . aaaed lQIOil
. ncaipt.



# .. . 

# .

VE S 004 4 58

## ...**·** 

# ) e) Nut
.. which
... t tbe cri'teda ••tabliahecl in ••ctioD Ill of thia policJ and which eahibited positive screen results for dioaio precursors duriD9 profile approval analJ&ia will 

## be screened upon receipt if the profile approval screen indicated dioaio precursors above the**~** 

### precursor threahold value, and 

### aubaequeot dioxin analJaia coofir:.ed dioaiu beloti the dioaiD thr
.. hold value (or Dot present). The · inca.iD9 screen will be liai ted to onl J those

preouraora which were detected duriov ' profile approval analJsia. · 

## If the ioco.in9 acreeo indicat
.. 

## the pr .. ence of diodn precuracJra, incca1D9
. · diaat'D**coafi~ticm** 

### aD&lJ&ia wi 11 be conducted if 

### the level& of precursor& iD the iDca.iov soreaceed the leYels of preGUrsors in the profile approval analJsia with the**toll~** 

### guidelines: 

# : · ! · i)

H) ' 

### Profile approval precursor ac:r- 

## na · posiu..,e
. dioain**confi~tiDD** 

### aD&hsh

wu**~atiye,** 

### none dateoted. · -ad - 

### The 1Dcca1D9 scr- iDdicatu precursor levels vreater than a**fao~or** 

### of 10 

### ti
.. s above the profile approval result&. ·



## .· 

## . Prcifile approY&l pr-uraor sc· re• wu . I'Oaithe ;' dioain ' c:OilfiraatiOil analJaia · vu U,athe,**~t** 

### dioaili wu**detec ~ed**  

### below tueabol4 nlu
. · ·



# .. - u4-
. 'fba ·· 

### iDCcainv aor . e-**~cat** 

### .. . premsor 

# ·.**J••~•** 

# ·. gJ:-,

_ ter**'\~** 

# .**· p.t** **ci~fi~ed .**  

### 1
. ..**.** 

### abOY!I 

### tll.e: pz'Ofile mtoYal raault8. · fte · ' ::. '''
. '.;
.. . ·**p~orated** 

### ..leV.l ia · deteraiawt u fallCiws:**·~ ·**  . J. ' • . . . .• . . ..**~** 

## (lm • . 

## 1 or.il) x 

## nt. · · · · .. .. . · ' f
.. 

## · ?.

" wh;re: D'rL '" ·

# di~aill**': t~e~~ld** **. l~~~i**  DtJ) a 

### ' dioah leve1 cleteet.d · · · (pr!lfU'e ap•ronl) PPL ::: profile qpro•al precursor level 

# a. Dioain ,llla}Jaia:
. Dioaill anal pia
. will 

## be perfol.ed, 

# with the concurrence

. of the g•erator of
. the waste , · foUoviDv
.. a cli
. oaiD
. . ' .;· ..**:·,' li•~iftiii~** **.>;,! cireeD** **w.hi~** 

### indicat
..**;:: pr~a** **or ·** **pre~\. --'** **'t:, ~•·** **·** 

### · or 

# aboYe o .01_. ' br ve'iv\lt · ; ' 

## l)et'aetioa ··· u.m til ·· foi' · 

## cuoil.'i'**":~"'~;** 

### aD&lJsia will be aet at a , l put per . ail\ioa**hrubold ~**  

### VES 004459

## A
.


# a.

c.
p ,



# • •

' •

: 

# .. .) Diplip: General · hailr u ... for ca.polllleb known •• 

### polrchlorinatecl dibemo

- p-diozilul ( PCDOa). Specificallr, "dioxin " ia tJpicallJ u.ecl to refer to 2,3 ,7, 1- tetrachlorodiben•o-p-dioain, or 2 ,3,7, 1-TCDD
. · Diolip precunora: Cheaicab vbicb vho NDUhcturad 

### have been ahowu to contain dioriu u a wute or bJ'- product. Diozin precn&raon ,. are of aiailar obeaical**c~o aition**  

### to diorlu.s
. aaae ea ... lea**~re** 

### 2 ' ,4,5 • trichlorophenol, ailvea, and
. haaacbloropboe
.**.** 

## UJ&: High Pn
.. ure · Liquid ChrOIUtographJ'
.. . ' ualJ'aia teclllli'lue ia 

### uecl in alii 

### -thad lt2
. •71, ADalJaia of Chloropheno&J' lerbiciclu uaiue BfLC• • 

### 'l'bia**"~** 

# ..**.; ~**  

## • • · OC· 

## cciKS: Gaa Chr_.tographf, GC/Kua Spectro.copJ'.

&nalraia**inat~tati u**  

### uecl
. for the ·**~peciJ!ic** 

### identi
. Ucatioll of J:i-roua oreanic CCIIIPOI&Dda. 'fJ'picaliJ', the -t)ocla 

### tor .'l\l&lltUicaUoil !If apecUic dio&iua' : or ·. dio&in pUCI&riOl'!J. uae GC OK; 

### GC/
..**te,olllli~ .**  

### . I"'Pol"" IC(IM : 

### A 'lUiCk, a.ai•'l\l&lltitathe -thad of**ide~:~tUtin9** 

### the pruoce · of a apecifio**o~cal** 

### . or ch.aical fUiilf , · ap.Oi • ficallr
. •·146 lletbo<l , 4010 , . I'PR"oaaa.,. Tut for the Prea,oce of PeatachlotoPb*Do) : .



# .....

. . · '• 

### ·. ' ::: 

### · 

### .. .



# :: ..**~·- ~:::**  . • :. 

# :-·

# ..**~-~:- ,**  

## .**~** 

### ..

### "'
. 

## .

·.)



### ... • 

# ..**~~-. ~**  

# . ' 

### .. 

## ..**-~** ·'

• '

• , 

### '
. .• 

### . . , 

### . .'.

•'



# . . "' 

# .



# ... 

# .. '·



## .·. -·. 

## ---. ,**~:** 

## .

• . , I



### . 

# . ,

V E S 004460**~ .~.** 



### . 

# . )

· , <1. • 

## .. . 

# ...... POLl CY
. REVIEW Of' PROf' I

## L~**CoNST i-** **tf tli** **:** '**~** 

### . .**~** : .**~** 

## . . 

## . . : ."'

. • 

## . ,**~** 

## . . . . . 

## . · Suap.Ct per poI icy : Not
.. _, •**.,~ per:**  

# · pO'f' WY <--..a.,...:.... - > . ·. . .**,.---""'-~~...,** 

### .**·~ ~**  

### I
. . . . · . , . 

### COnduct dioxin Proeeelt'w{tll**~bi ln** **·** 

### · precuraor analyaia proceaa, no pre• cur.or analyafa

• .. J, • • .. . . • 

### Dioxin precuraora Precuraora not found

fou n d 

# « 

# > >----------. No 

### No dloxi
. n t .. ttne Doea generator want to have dioxin teat
- int parforwed? 

## »**O~y** 

### dectaion No 

### precuraor teatintJ on in-intJ waate V 

### Yea Conduct dioxin analyeia ... 

### :. . 

# .. . I 

# .-------,...;.,
. . · 

# wu dioxin detected? Ye • Waa the dioxin Y.ea 

# Deny deciaion «' ': , 

### level > 1 ppm? 

### >>-reject ahfpaerit 

## . t 

## -> I 

### VHo Approve dectaton, conduct · preeuraO.r analyata on inc-ine waate ahfpaMnta I 

### Ia in-c-•ne w•• . t• ahfPIMIIt
. pr-.or la
. v el 

# > . Jo tt-• 

## tM.
. prof.fle
. ..,a1yafa ;**pre-~** 

### 1evel t! '

. ...



### . ·**~Yea ·** 



## Yea · 

# • Conduct di
. oxtn analysts 

# ..:..... : No 

### APtH-ove dMfeton (or uc-..t wute**ahf~),*****~pre- ·**  

### c:uraor**t~t~ia1yitie** 

### on t-tne w .. 

### t ·

e ahf.:...nta ·

'.



# ...

. . ttod1 

# ;y · chic ta tdft < 

## ,.,..._.;...._,__ ____ ...._..,v.a · ·**~lyeia re•~t1U**  

## ,



## . > fO#t ratto 

## · -of ' lilr'f-· · : · 

# 1.,..---r-----___. curaorw · . to cfJoxil'l' l , :·

. if neca8earv


# .. . '• 

# •

. . . Accept the weat · e · aht.-.nt · .,

## L-**----- --** **--------~-J ------------~~..1**  .....**~** 

## . · . 

## . · .

VES 004461

# v

VES 004462Prot 11• . , 02f l0 7**af;OC' r**  snACOS& 1Xiw:uiTY 0\LlD Oe.c:rlptioa : KIUD COUOSIVU/SOLVJ:Vn a.c.Jver I • UU10

--- - -- 

### (\
. Q "\ Dna I Iii • I Type 

### o I 

### r W.igb t COlor I o.adipd OJl ' P'u ll \ loUd ' LtCI'J.!d 

# 8 55 

# C'P 

# l lJl'-rk bf'Wl
..

## ""~..rd 

# r.s let;)

2 3 

# • 

# I 

# re:os l**~,** 5

# A~**::Jl~f()o{l/,)** 

# ' 7


# . I 

# • 10 1l 

# L_
u u

# ~ 

# .. · .A I 

# - """' u 

# ... \1\-**~** 

### -' !"iil**~\** 16



## .. 

# "'**,~** 17 

## g
l8 

### u 20 

# ffWSliL!-.::1&/uj..t ....,

·,_ __ .... I- 

# 3 /

- 

# Cli

Loeatioa

### ----~**--** ,_,.,,. --------- - - ------- - ---
Wdgh t
----- - -- 

# . ...

• . i.

VES 004463

# w

VES 004464UNITED STATES ENVIRONMENTAl. PROTECTION AGENCY REGION5 71 WEST JACKSON BOU\.EVAAD CHICAGO,l.ll0604-3590



## CERTJFIED 

## MAlL IEIURN 

## RECIIPI RWUISTED**~glas** 

### Hurls, Oenml 

## MaDa8cr VooliaES Tec}prirM Solutioos, LLC. 

### 7 Mobile Avenue Sauget, lll!nois 62201 o-M r .HeMs: 

## l«lV212008

A ·ISJ

As 

### you 

### know , on February 22, 2008, the U:S. Envirenmeatal Protection 

### Agency 

### issued 10 

### Veolla**ESt~** 

### Solutions, L.L.C. (Veolia) a 

### Cl![all Air 

### Act Soction 114 Request for lofQrmalion. 

### EP' A revised 

### lbe n:qaest on June 

### S, 

### 2.008, and 

### Sep4lmber 

### 12, 2oo8. Pursu.oitt 

### 10 Item II c, 

### the tostnport 

### must 

## ilJdude an e• empie 

### ofeach 

### calculalion pcrlormed. On 

### October 

### 14, 2008, £PA received theteat 

### report 

### for Unit& 2, 3, aJ1(i 

### 4. 

### Appendix 

### B ofeach r.epor1 is 

### titled 

### "Refm:nce 

### Medlod Field Ollla 

### ond 

### Calcrulllioo&.• Weha¥e.localed the 

### field data 

### fur each lest ND 

### tiDd 

### the results ofENSR.'s calculations. Ho wever, ENSR failed to 

### include an example of each calcul ation. 

### Wo eitpected the 

### test ):q)Olt to show 

### each equadoo 

### from the 

### R'*"euce**Mctho~** 

### in 40 

### C.P.R. 60 ; 

### AI'J'CD(IU A, that ENSR used
. ln 

### per!i<ular, we expccted
.to iOe 

### the oxamp! e calculaliOIIl for each of 

### tho following peramciCr5 

### for one test nm for each incinerator; l!qUalioo 

### Panmeter 

### 2-6 

### ll!olccular Weillbt ofthe Stack Gas 

### 2-7 Average Sblcl( o..-Vclocitv 2-8 

### Avera ' "" Stack Gu 

### Drv Volumctrie**Flow~** 

### 3·1 

### DrvMolccu1arWciaht 4-1 Y!>lume ofWater Varxir**~ed** 

### • 4-2 Volume ofWIIIer COllected in 

### Silica Gel 4-3 

### Sanole Gu Volume 4-4**~! tore**  

### Coot eat · 5-7 or 

### S-8 bokinetic Variation from 

### Raw Data 

### or Intermedi ate Values

29·1 

### In-Stack Olltectlon Limits 29-2 An.alvtical Proc1ion I 

### A. Front·fWf. McQis 

# e Men:uni) 29-3 

### Aoalvtical Fraction 

### 2A. 

### '&.c:.k-Half. Metals xca>t Men:urvl 29-4 

### T otal Train Metals (Exceof Memcr¥) 

### 29-S Analvtical Fnl<:tioo 

### IS; Fro)li·HalfMel(:urY 29-6 

### Amount ofMCR:IUY Collected in Sample FIIetioa 

### 2 

### :

VES 004465

### l!!nualim> Parameter 29-7 

### Back-HalrMcrcuiY Values for AniMical Fractidils 3A. 3B
. And 3C
. 29-8 Total 

### Am<fWlt

## of~ Collected in the 

### Bid<-Fialfoflhe

## Sm~~>llnlt Ttain 29-9 To tal Train**M~** 

### Catch 29-10 

### !JidMdual Mellll**Conc:e~~tratlons** 

### in Sticlc Ou 1'umant 

### to Sectioo 114 oflhoClean Air Act, 42 U.S.C 'S 

### 7414, wi1hin20 da)'l ofrecolp t of

Ibis 1etter. V eolia must 

### eitb<c

## ~ App«<dix B ofeach tCSI "'IJC)rt to 

### includb lhese calculaliollS Ed to · make any noc:es$lf)' 

### revisions to the 

### em\ssi011 concentratioas ot 

### subm i t a compact 

### disc wilhd!e 

### S!JCeadsbeet 

### propm wcx\Sbeell 

### tblt COIIl8in the 

### ealculalionll
. 

### I!)'Oll have my questions reprding 

### the letter_, pi- 

### contact Cbar!CI!I Hall of .my 

### staff a! (312) lSJ-.3443. 

### SineeR l y yours, .

# ~~ ewton 

### Acting DireClOr 

### Air and Raclfalion Division



### VES 004466

### • 

# .. !

UMI TED STATES £NVIRONMEN'tAL l'ROTE<;tiON A GE NCY REGIONS 

## n WEST JACKSON BOU!fVARD ClilCAGO, ll jl0604-3590



# · -

. CERTIFIED MAIL



## RETURN**~q rrr** **~UESIED** Douglas' Hams ; Oco:cql 

### M anager Veolia ES 

### Technical Solulio.is, L.LC. 

### 7 Mobi le Avenue ·**~auget,** 

### lllioois 

### 62201 ;



# .. . Dear 

## Mr. Hurls : .



## . . 

# ·. A-181

· · As 

### you lcndw, on februaty22, 2008, the U, S. Environmental Protectio n Agency issued to VeoliaES 

### Techn.icafSolutiom, L. L C. (Veolia) 

### a Clean Air 

### A\'lSection 114 Request for · lnfo mif.tio n. 

## E? A revued the 

### request on June 

# s, 2008, and , SeptCmbq
. J.2, 2008. 

### Pursuant to Item li e; the 

## teSt 

## report must include an e:xample of eac;h 

### cal culation 'pcrfonned. On 

## October 14 , 2008, EPA received the 

### test**r~** 

# for**Unit ~**  

### 2, 3, and 

### 4.' 

### Appeod,ix B ofeach 

### rejxlrt is titled · 

### "R:eference Method Field Data an d Calculations." W e have located the 

### field data for each test nm and 

### the resullll ofENSR's c8!c:uJatioos
. Howevc:i-, ENSR failed to in<:Jvde an**~ple** 

### of · each calculation
.. We Cl(j,ec ted the test repott to ·show each equation from the Reference Methods in 

### 40 C.F ;R. 

## 6o, Appendix 

### A, that ENSR used. 

### · Jn particular, we 

### expeCted to see the txlllllp l e calculatioi,)S.for each ofthe'followil).g 

### parameters
- for'one iest 

### nm for 

### e*:h incinerator:
_


## . 

# ..

_ Eg\llltiOtl Parametet 

# .. 

# . .. 2-6 Molecular Wi:W>t of the Stack Gas 2·7 Average Stacie Gas 

### Velocity .. 

### 2-8 Aveilllte Stack
. Gas 

## Drv V olumetri c Flow Rate 3-1 

## Drv Molecular Weigbt
. 4-1 Vobune ofWntcc Vapor Condensed 4-2 Volume ofWater Collected in Silica Gel 

## . 4-3
.**~e** 

### Gas Volume 4-4 · · Moisture Content 

## . 5-7**or~ ·**  

### ! so kin etic V 

### ariatiO.. 

### from Raw Data or ln
. tatmdiaie V aloes 29-1 

### ln-Stacl: Detection 

### Limits 29- 2 ' cal Fraction lA, Front-Half. Metals (Except 

### Mercury) · .. . 

### 29

- 3
. Analytical FJactioo 2A**Ba~k-Hal!** 

### M etals (Except M 29-4 

### Total Train, Metals (El!cept 

### M 29

- S Anal}'!ical Fraction tB · Front-HalfMercur)t 29..(; Am01mt ofMctCWY Collected in S8uwle Fraction 2

VE S 004467

### l &!uation PaJlllllete:r 

### 29-7 Back

-Half 

# MercurY Values for Analvtical Ftactlons 3A 3B 

### And 3C 29-8 Total Ainount

## of~ Collect ed in the Back-Half 

### of the S amDlina 

### Train 29-9 Total Train 

### Mefciiry Catch 29- 10 

### Individual Metal Concentrat ions in Stack 

# Gas

· Pursuant to Section 114 of the Clean Air 

### Act, 42 U.S.C. § 

### 7 4 14, within20days ofreceipt of thi s 

### Jetter, 

### V eolia 

### must either revise Appendix B ofeach test report to include

# ~ calcul ati ons and 

### to make any 

### necessarY revisions to the emission concen1n1tions or submit 

### a compact disc with 

### the 

## spreadshecl prnSJMl worksheets that 

### contain 

### the 

### calculations
. 1 fynu have an y questions

# re~ing the letter, please 

### cnntact Charles Hall ofmy 

### mtf at (312) 353-3443. Sincerely ymn,**~l(br'f'( L.**  

### ewto ri Acting Directo r 

### Air ond Radiation Division 

## '

i 

# \

'· 

## I
. l
. .**~** 

### .



### VES0044 68

# X

VES 004469

### . USPS • T racll 

### &. 

## CoDlinn



# Trac.k& 

# "Contion**Siiil'i:i~ '** **~~ 70\)\~Qll01;91M** **.fl!l2**

# ~~~uaod a12>d 1'111 on . F"ebi\J*y 

### 3
. :2008 t> 

### EAST"S'AOO Page I 

### c>fl

# -~-**~** EnW**~cti9t** ..... . (



### NiJiifir .... 

## ilfli!'"" .**TIUil.~IJ1I** 

### Pi lft\lili 'Gill

## :i!ll'elillr\li;;matiQ<1 0( lljidili t · !Or y\>11< ilom soi1110 you 

## bcolb!lis by...- .(
.. . )


# - _.......,. I

http://trkcntiml.smi.usps.com!PTSlntemet Webllntetlabellnquiry .do 

### 2/1212009 i !'



## · . ..

,_

l



### VES 004470

## y

VES 0044711 2 3 4 

## s 5 1 8 9 10 11 1 2 13 14 lS 16 11 18 19 20 2 1 22 23 24 2S ILLiliOIS EPA' PUBLIC
. IIEARIKG DIIIIFT CMPP and RCAA PEFMIT S 

### for ONYX ENVIRONMENtAL SERVICES, 

### SAUGET

### T~N**.** Ju ly 22, 

### 2oo3 Cahoki• Vill a ge Ball C.-bOkia, IUino i. s.

SEARING OFFtctR: Charl es tsatoesia.n
COURT R£POR$R: Cynthia A. Kyers, CSR, OCR



### VES0044721 2 3 

# • 5 6 1 B 9 10 11 12 13 14 15 16 17 1 8 19 20 21 22 23 

### 2

4 25 CHARLES

### W.TOESI~ • . lllinoil EPA Hearing Officer
.
Ladi•• and Gent leme n,

### ~Y name is Charle3 tor.atoeai&Jh I'a tb• hea:riog officer toniqbt. Th
. 1 • bear in9 ia be.it\9 held by the Illinois sv-ironmental Protection l\9ency : This is the joint bearin.q of the eure.au s of ldr and Land

- 1be purpose of the 

### hear1nq is to receive comments a nd data &nd

### ans~or questions

### fr~ the public concGrnin; two dxafe pOtlnita. Ony)[

### E.nvi~onst.entAl serv ice-S , fortaally 

### known as Trade Mast s Incine ration, haU 

### requeated tvo petu'i t5 from th&

### Illi~ois &nvironmenta.l Protection Aqency. The faci l ity is located at 1

### ~il• Avenue io

### Sauqe~,**llinO s.**  fbe facility bAa
. N.qVeated a Clean Air**~t** Pet:Rit Pa:oqrUI Per:ait for its e.ir eaission.s and renewal of their 

### Resource conoerv&tion and Recovery Act and Saxardous and Solid W aste

### Amen~ot · Pepmit for the man39ement 

### ot haz•rdous waste on b ite.

### ~h**e** faci l ity eecepts, stores, and**nei~atao h~za~doul**  waste. 'this

### ht!a~inq is being held on the pz:oviaione
o f 3S Illinois

## ~niS~rative Code Section 166



### VES 0044731 2 3 

# • 5 6



# . , 8 9 10 11 12 13 14 15 16 11 18 19 20 21 22 23 

### 24 25

### s~bpart A, and 35 Ill inois Administrative code S e ction 105.182. tf you do no t wish to speak at the

### h~rinq you

### ~Y**au~it ritten** **nts,** and in lndeed lenqtby

### c~nt**e o~**  questions sboutd be subMitted and the lllinola EPA v ill answer in vritinq. Written c0«11'18nts -.ast be postma-r-kect by aidniqb.t Au9uet 22, 2003-

### ~Y need not be notar11ed but ahou1d be 8ent to myse lf, Charles Katoes i an, that 1 S H-A-T-O·E

- S-t-A -N, as in Nancy, tllinoia EPA Heating Ot'fic:or
. at 1021 No rth Grand 11.ve. nuo east, 

## v..o. Bo• 19276, Sprin9fi e ld , Illinois , 62194-9216. Tni• infoooation is a ll avoi lable in the notice that va s placed in the newspape r . . to addition,

### rest**r~** axe on either aide 

### ot the rooa anc.t tbe.t' e • s a drinki.nq fouotaU ju.:st outside 

### ot the close d

### doo~s, and also a aoda

### mac~ne. wo vill seart w ith 

### some presenta tions by staff

### fr~ the Il l inoi$ EPA and United States &PA, then w e w ill take written
. -- or comments

### fr~ the pubU
. c , and after people have Spok.en we w i ll tak.e general questions from the public
. ln addition, I wil l note that there a£• II'JIUibe.tl !rocrt t.he CQII'IPa.nY involved who uy answer que.ations as vell. Please com up to the



### VES 0044741 2 3 4 5 6 1 8 9 10 11 12 13 14 15 16 17 18 19**~0** 2 1 22
. 23 24 25 u tiotop h ono t he re w he n you spe ak your COI'IIMnte and also p laase clearl y state and spel l y our last name for the r e cord because the court reporter JW St Q at**e~erythin9** down on**~ne** record fo r i t to be presetved. I' U start th en wi th 1'ed oraqov ieh f<oa the 11llnols BP A
.
1'80 OR.AGOVICH, Pea\it Uni t t'.anaq er . (BY MR. OAAGOVICH) : Tban l< you . Good cveninq, AIY name is Ted. D rag ovich
. I am t he manage r of th@ Oieposal**Alt erna** **~iv os**  Un it for the Bureau of Land. Before we d i scuss the specifics ()f these pennJ.ta, I voulO. li ke**~** expl ain a little. bit abo ut JtCAA, ""tu:RA• is an ac.ronp for the Resource C onservation and Reco11e.ry Ac t.. That w u a law v hich**~• ~ssed**  by Congress in 19 16
. Ita purpose ia to deal w ith hazardous w aste iasuaa. 

### R.CilA if!\POees requll"eme n ts on p eople w ho IM-:'&90 

### hazardous
. w aete f rom the time i t 

### is qenerat e d through ita ator a9o,**eat~nt 1**  or**piace ~on** **t** i n o lat>dflll. Facilities that man age**haza~douo** wasto mus t tir•t obt.o. in a permit, un le$S t hey wutt ozut o f the permit**x~ti ona**  in the regula tiona. Peoaits aro very specific abO u t w hat types. of



### VES 004475l 2 3 4 5 6 1 8 9 10 11 12 13 14 l
.

S 16 11 18 19 20 21 22 23 24 25

### cti**itiea** a ro • l l owed a t tho facil i ty .

### Pe**r~ite** arc u . sually is s ue d fo r t en

### year~**.** Prior to 

### exp iration t he facility operator must submit & ren e v al application. It the

### appl**atio~** is cocQlete, the facility s&y co n tinue to o pera te afte r tl' ut petcit baS e xp ired,

## unti**~** the n:PA ..akea
a final deei
. sion on the app lication
.

## Ton**i9h~** we

## a~e here

## ~o discuss • dzaft

## pe~**lt** tor tho rcne w&l of

### e**pe~ ~**  to r the O nyx incinerato r . xn thiS casa th e app li c a ti O n va s five volumM ! of information. A s w e go through th e application
w

e

### ~ke 5Ut0

### th**~t** their desiqn and operatin9 procedures will

### ~et the feder al RcRA regul a tions
as ve.l l a a any

### ~C~Cte sc r inqest. state re9Ulatlona. 1fe send a lilt of de ficien-cie s to the applicant 'W

ho then 111\llt respond w ith a..ddi tioo.al 1nfoce.at1on.

## ~fte**r** w o go tbtouqh this

## p~ss a couple of

## ti~s, we have epou9h

## nf**o~t io** **n** to

## kc a porait 

### clecis1on. I n t hl. a -pa r tictJlar

## a~e, regulato ry c:M.ngos .' w

ee• 

### occurring at th e same time ve w ere rovie w in q 

### t ho application. thes e changes we re de Si gned to 

### coordlnat. e t he

## miss**~on.s requireMfl~$**  betti'Gin

## RC~ and ebe Cle f.n Air: Act.. As a result •

### complian~

VES 004476

## • . l 2 3 4 5 6

' 1 8 9 1 0 

### u 12 13 14 15 16 11 1 8 19 

### 20 21 22 23 24 25 schedule w a..a tncl ud od i n the dr aft permit to

### unsu~:o t h at appl icant complied with ne w air eats sio n atandarde as soon &s possib le. The draft**~t** also includeS a schedule and procedure to restrict eaiatio;ll o f meuls before the f inal emiselone etanda rd s a : re achieved- &ecause. o f tho ch&nqin9 r69Ulaeions .,nd the ceqvired coordination

### bet**vo ~n**  the various Aqeneies and progr&ma involved wi th this faelity, it has been a lonq prooeJe; but w

e have developed a dra ft per.tt . It ie our ob liq at io n as the lse u in9 Agen cy . to prapare a · d%aft

### pe~it and ca l l a pub lic h earing. That is wh y ve arc here ton iqht; to**g~t** your

### ~nta on the dc.a.ft petmlc:. We · a :Ce requixed to issu e a public notice of our draft decis i on and tbe t.i.M and loe.-tio n of the b0arin9 at l.N&t 4 5 

### dat• btlfor• the hearing is he.lcL A!t.er the he.acing the record is lef t open for thirty days t.O allo " all intere a · t ed

### cit.iu**~s** .a . nd the

### ~-.ny t.0**~nt** on the draft**pe~t.** A t that point ve

### Ul consolidate the col'llflents and address tben1.

### ov that may lead to chanqes to the

### d~A**ft** permit or the pcrtnit may sta y tbe same . Our reaponao and final decieion will take a t least thirty days to pcepa._ce, depe.nctin9 on**~o v**  extf!flSiv• the COCIIIMlDtS



### VES 0044771 2 3**~** 

## s 6 7 8 9 1 0 11 12 13 14 lS 16 

### 11 18 19 20 2 1 22 23 2 4 25 are. At tbia timd 1 w oul d like t o introduce**ry .**  

### Riegle who wi l l 91ve yo u

### s~ spe cific technical

### 1nfo~tion o n th• requirements in the propO, ed paudt
.

(HS. artGLI!I: Good eveninq, my 

### rwoe is Ma %Y Rieqle. I all an enviro.nmental engineer with the ll).i u oia tnvirorunental P r o tectio n Aqe nc y . On NOVQmber. 4 # 1991 , Onyx E n v i roruaental Secvic
. ae aubm,l.ttad a Pu t B r ene wal &pplieation to etore and incin erate wa seea . Onyx is an

### exil~~ facUlty that has been opera ting since 1919. No

### e~iona or significant ch4P90S to the operat ion axe proposed. Tbe et.

_ ppUcat.ion consiata o f a Part A app licatt.o · n, a descri.ptioo of' the faci lit y, and**~3 aie** **mana~~nt** operations, 

### a contingency 

### or

### ~r9ency**re ~ponse** **~n ,**  a tr aining p1an for

### ~loyees, a cloauro pl a n, a w a s te a n alyaia plan , and detailed process informat i on .. the ap pl i cation w as reviewed by both the tedctr:al and state Environment
. a.l Prote c tion Aqenc1es to

### dete~ne w hether the

### ~&nY**ha~**



### VE S 00 4 4781 2 3**~** 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19

· 20 21 22 23 2( 25 d Monstrate.d that it can h an dl e specific b.a

_ tardoua waat¢8 w ithin t h e strin9ent requ ixements of RCRA. S ince

### ~be IEPA aod O SZPA found th e opplicat ion IM!et• tbe technical requixemants, the Aqeneies were t'ti<(Ui.ted to dealt or propose a peoait for the facility. on June 3, 2001, a draft perai.t v a.a lseu.ed to onyx. Today, the Aqencies are going to the pul)llc: with · thi• tentative decision and r aqucstioq inP,Ut
on thO dr•ft permit. Onyx raciev es h &zaroou' and non-hazardous wasteo for repac kaginq, bUlki ng, and i nc ineratio n . These w a•tes

### ~y either be so li ds ,

### lL~ids, or sludCJ••. fh•Y ean be r e cei ved i o t.a.nk truckS, ca1l carl, or conuiners. W astos. ftOIIl bul k trUCks a.re puiDPOd into t.e . nks for storage or

### f~ directly**to~** incine r ator. A ll**~oadin9** and atorage
ueas

### ~MJSt**~~-v• aecood~ry** **contai~t** systeaa, consiating of lealcp roof co ncrete structures 

### desiqned to collect spills.

### ~e~e areaD w ill be inspected routinel y tor spills or damage. The ' v o lutae or these cont.ainrwant systeM mu st be equal to tba largest t3nk in the area of 10 percent of th• total

### vol~ ot the containers stored in tbc
a.re.a.



### VES 004479l 2 3 4 5 6 1 8 9 10 ll 

### 12 13 l< 15 1 6 17 18 19 20 21 22 23 24 25 ThO Onyx facility has a

### ~otal of tbree operating nazatdou•

### ~aste incineration units. Uni. ta N o. 2 and No • . 3 u :e f ixed baarth, duel cbaq')e.r 

### type i ucinerators
. Unit No. 4 i& a transport&ble rotary k iln. Thi:l pondt. would requir e we tac:i.li.ty to foUov apael.tlc procedUres in order to operete safely. These procedure& i nclude tbe wa ste analysts procedu
. re. e he employee training proqram, and

## ~rqency reDponse plan. The vast• analy•1• plan e.nour.es that onlY wastes w hich ca.n be properly handled

### ~re accepted at the faoil1ty.

## wa~to**~hich** do not meet the

## acc~ptab**lG** criteria aro refused. · Once a w aste haa been evaluated and

## de~ accepu.ble, it

## ~ be. transported

## f~ the

## 9enc~atot to

## ~e facility. At

## th~ tac11lty, the "'a•t• il a9aio ana.lyt.ed to ensure that lt 

### 1• the sA*! a . • tbe approftd. waste .

### tt**~tos** 111 hicb do not

## ~et the facilit y's acceptance crit•ria or conform to tho initial p re-•cc eptanoe analysis,

## ~us**t** be 

### rejecte d. The training plan and numerous safety syatema and deviseS at the facility ensure tbat tbe

## e~loyHI u• pro-per ly t.raio.td fo.c their jobl and in .-erqency proce(!ureS, and that the 

### b.a<U<Ia



### VES004480l 2 3 

# • 5 6 1 8 9 10 ll 12 13 l4 1 5 16 l.1 1 8 1 9 

### 20 21 22 23 24 25 asaoo1A tc d w i th b4ndl i ng hazardous wastes aLe rniniJld 7 .0 d 0 The facility ' • contingency plan i s dotiqned to provide guidance tor a quick, efficient respon 14 i n the event of a $p i ll , fire, or o thar 

### t ype of _,.rqen cy. The eont-inqency plan is p.covid.ed to

## 1~ -rqoncy response lJ<(>Ut>S to provide local

## autbori~iel w ith the

## nfo~tio~ necessary to deal w

i tb •n

## ~mergency**~h ic** **h** may impac t areas off -ait•· onyx hal provided a copy 

### of tba 

### contingency p lan to t h e local police

### ~ fire departwents, 

### emorqenc y te aponae teams . and 

### some araa ho s p ite \5
. Onyx muat revie w the contingency plan w lth each

· gro up annuallY ' to ensure that all peraonne l ln\fol v e-cl in an

### ~rq:ency s .itu a tioo a

_ nt f-.il i &t:
w

i.tb the {a.cility, ctte types of wastes

## ba.l'ldl~ by t.be fa cili ty, and the eonti..ngeney p lan.. 

### u · part. 

### of tbe review o f the faci lit y's

## ~rgencY roapona•

· p.rocedu.reo, 1:he "9e.ncy requ i red the

### faci~ity to

model an

## ~rt-a1te air

## re~e**ase** so that 

### lPC&l omerqancy response

## t~s can ev•luate the

## ~act

· tbia typo of'

## sl~uat**ion** m2ty haW on the c;oaaun it y. The coii!Pany JM.l.St

## p~perly .aintetn record# of

· vaate t r ack11\9 doCU."'IIents tor u.nifeat
. s}, .,ploy•• ua.ini.nq, inspect i on reeordsr · recoxd.s of opera.t1fl9



### VES 0044811 2 3 4

1

8 9 10 ll 12 13 14 15 16 11 18 19 20 21 22 23 24

. 25 co n ditione, and any i n ci dents. · and tbc

## ~int**enAnce** r ecord s of th& co nt ai nmen t systemS and eq u ipment. T

h s c ompany must

## ~lao pexform an tnvest19ati? n

## in~ a ll va ate manaqement activ ities, pa$t and present, to

### dcte**ne** if thes e ac tivities hav e imp a cted the

### enviro~nt.**(eitbe~** th e land or groun4 w

.tterl
. tbi.s i-S c&lled corrective action

## ~nd addr•aaea the en ti re taci1ity , tneludin 9 thOse ateas vb ich are n ot cove red through thi&**pe~ 1t** **n9** 

### a ctio n. ThO re newal perm it conta i nS 

## &**li ance**  s chedule. the purpose of th e compl i ance aehedu lo i s to btinq

## h~ facility in to compliance w ith

## ~~ n8

w HA C1' au.ndards a.s soon as possib le. Th• tiM: f .ta-8• have been K ep-c to a adni.&u:m con41de .rinCJ t.be a_aount atKl CQIIPlexi ty of liOrk. It w ill r:esult in tut !.n?' .nd eJtiss1.ons aonitorin9 to be ua.naterred tree the RCRA perlli t

## ~ the Clean " i.r Act pat11li t.. l t w i ll Al.SO reS u.lt io ne w motal5

## i~ta and other constituents cons istent w it

h the C lean 7\it "ct Permit. · A

it 

### oroiss ion s are controlled thr ough w aste feed l i m itat i ons, e•is s ions

## .oni**to~inq,** and oir

## po~luti**n** control equipment- Wa a te taed is liaite.d by bOth amount of waste fN 

### peX hour and



### VES 0044821 2 3 4 

## s 6 7 8 9 1 0 11 12 13 l4 15 16 17 1 8 19 20 21 2 2 23 24 25 concantration of

### cont~inants in tho wa st e . Ths

### c~t also cequ1tes ·

### ~ waste teed cut·off 

### ayatem

### ~hich would atop • n Y waste feed ineo the i nc inerator wh en certain opei a t inq condition& are not aet.. Onyx 18

### ~:ec;ulred to sonito r

### ocu~ta_in ea1a11on U.its. 'l'he facility operates a d%y scrubber

### sys~. cadbon injection

### unl**~.** and

### 1~ tojectlon unit to oonero l •ir**~is ions** **.** I n addition to Onr-'s o wn inspeetion l , th e factlity w ill be

### nspect~d routinely by our in8poctoro to & naure the f4cility's

### ~Li**~n ce**  w

it

h all RCRA

### requira~ents**.** The

### ll**lin~ia** &PA baa the authority to inspect the fa cility at any

## ti~ withOUt advance notice.

### ~ purpose of

### t~ia public bearin9 ie to gather the public' •

### ~n**s** on tbe drAft poxelt. Aft.er tho bea
. df\9, the record i s le.ft open for 30 days to al lo w all interest ed ci tize .ns, as w ell •• the c;:oanpany , to aubtait c()fi':IMinU on tl\e pe:D'11ta. 1\fte .r the

### ~nt period ia cloa o .d , thft Aqepcy will consolidat e the comments

### ~nd addre s s eac h one. Ch anges . v i ll b6 eade to the

### ~af**t** pendt if t he J19etlcy receives COf'l'oentl v hicll identlfy technical l5sues 

### that were oot

## adOqua~~Y

V ES 004483

## .: 

# . 1 2
. 3**~** $ 6 1 8 9 10 ll 12 l3 

### u 1$ 1 6 17 18 19 20

. 21 22 23 2. 25 a.ddJ:O&GGd· If no technical issues are i dent ified , no chal\9&8 to the Gta. f t pextnit vil l be made. 'the reaponua eo

## e~nta**~ill** probab l Y t•k• 

### abOu e 30 days, d epending on how extensive t he

### c~t**•** oto and hOW .uch w o rk is invol ved for th e

### cy. 'tb&n k you.

(BY MR
. Jill BUJUG!Il: Gootl evenin g, "'Y n.,.. le JLin Blouq h, I ,.lift a pe:ooit W ' riter i n

### tb~ W as te

### Maoag**e~ t**  Divisi on of

### th~ United States &nv1 ro nment4 l P ' rot8ct ion Agency located ln Cbic a ;o , IllinoiS , My purpose berc todaY ia to cUaCU.SS the. uSEf:A portion of the P.CAA peralt fo r the OOVX facilit y $.J\ S-.uq e t, llli.nOiS AS you ha ve prevlou.a
. ly been told, the ReM. Act of 1976 v as

## ~a**oded** i n 1 984. rhe 198 4

## R&~o%doUS an d Solid w aste

## ~n&oents, kn own as BS'MA
. . i.lftPOSed further r•quirecaent.a for the unaqQl\\f!.Q , t of**hazardOu~** wa6te
- Tha State of tl l. inois bas re.cei"ed

## aut**ori~ at** **ion** to

## ~inister several b ut no t all HS •A proviaions.

## ~hose conditions for w hi c h the st

•to has no t. 't)ee!l yet autbo.r i z . ed ll\USt be issued



### VES 004484l 2 3 4 5 6 1 5 9 10. 11 1 2 13 14 15 16 11 18 19 20 21 

### 22 23 24 25 

### by the 

### USEPA. At the preeene time tha State of I lli no is ia not

## &ut~o**ized** for tne i mp l emen t4t1on

· of cequlat ion s found in 40 CFR Par t 264 Subpart

CC
. Onyx EnvlrCM'UI'Ont al service s bave three

## r~ulated units tb<lt fa ll under Subpart cc . The unlts are contalnera,

### ~an**ts,** an d miscellaneousunitsThO fir1t set. of the fede ral cooditiona du.l. w

it

h eontainer s toraqe which falls u nder w ha t la kn o wn as x..vel 1 controls and requ i re on pt. to JI.Ht t h e a.pp U.ce.ble o. s.

## oepart~~ent of 1' ran sport , a tio n rcqulat to na. The second part o f the p erMit daals w lt

b Tanka Requ.i xtlfl6nts
. orw:ter thi s condit io n· tbe tank• dASitp\ capacit y of e.ach t ank eust be l. esa tban 15 a3 and t he uxiftrU.m vapor pres sure aust be less tb aa 16. 6kP4. '!'he h a.:.a.t: doUS was te in the: t.a.nk eball not be heAted to a eemperature that is qre ater than the t emperat ure at w hich t be

## d&X~ va.por preoaure of 1 6.6kPa is de termined. The

## ha~atdoua wante i , n the tank shall not be treated by any w aBte stabiliza ti o · n process. The condit ion also has a

## los**~** vent

## sto~ and control devise xequirements wh ich 11 co n trollad by the ca,_rbol\ N:tsorpt ion Systea. The par ait requires



### VES 0044851 2 3**~** 5 6 1 8 9 10 

## n 12 1 3 14 15 ].6 11 18 19 20 2 1 22 23 24 25 that onyx

## cOP~l**y** w it

h the Applicable waste testing 

### and atoraqe caquireMents pr ior to all oft-sl to ahiptM-nt of w aste and prohib
. ited 

### troa h&vinq bypaes devla•• that co uld be used to

## dl~ert the qa,s oc vapor atc· e.U\ to the at;.ospbere t>cfoce e.nterin9 the contco l device. 'fbe fi.tLa.l sot of Fecteral

## condi~ion& •dd
. ress t;be Kiscell.Aoe<>US Oni.t O.tu. ancl t.a.bP•cJc &oxes

## bqui**r~ 't-S.**  t'he pe.rait requ . lres Onf" to: 1. Maint..iP these areas at a. s l iqhtly neqa.t i ve

## pr~eauro un¢or bo t h ventil atio n an d inexting 

# modO•• 2. Hainte.i n an oxyqen defi c ien t condition of 

### leos than 5 percent

## oxyq~**Under** the inertin9

## mo~a ud: 3. TlW b.n d.iscbaJ:q:e CllS t be incinerated in the 

### peautted on-site !Jleioeratot (Onit No. 31
. At tl'lil t . iJie I would J..i.ke to introdUce Gary Vi.ct.orLne.

### G~Y V I CTORINE, I ncin erator Specialist
( BY MR. 'IICTORINEI: c;ood evening. My """"' is Gary Victorine
. I

## ~ a n

## enginee~ with the

## USEP~ a.qion S up in CRicag O. Up at Re91oo 5 t



### VES 0044861 2 3 4 5 6 7 8 9 10 11 1 2 ll 1 4 15 16 11 18 19 20 21 22 23 24 25 coordinate and

### ~r**ck** t hft R CRA perwitting of hazardOUS

### aate**incine~a ors**  and othe c d e v ico& t hat**born ha~ardous**  wa •te. I'd like to focus on se v eral issues tb1a e<Veni.ng. First,
.1 ' d l ike to provide a bit of biator:y on the requladons requc1i.n9 ha
. zUdo\lS vasto incinecator s. and al.so t ell you about bow those ru l es are currently in transition. And second, I ' d like to taL k aboUt how risk as aesaecnt ha• been 9art of the requlatory picture , both in qcneral a"d in th e specific case of t h o onyx facility. tbe Reaou

_ roe conservAtion and Re covery A ct (RCAA) -requ.is:es the OSSP A to . develop national standatda Cor

### ~z~**dous** waste combustion tacllitiea that are protective of hl.IIPAB bOalth and the en,iroNDOnt. In a ddition , S•ction 3005 (c) (3) of RCRA contains lanquager we c01¥00DlY ref« to as the • omnibus prov - is i on•, v b ich qives tho OSEI?A and the authorized Stat es tbe

### authO~iey to include addi
. tional te.r. m.s and condi tions in oacb RCM facilit Y permit. a$ necessary, to pz:oteet buma
. n h eolth and the erwiro_mMn t . In 1981 tbe USRPA is &ue d

### ~ CQObuot ion standards foe Lncinerators
. Since that

### t~,



### VES 0044871 2 3 4 5 6 1 B 9 10 

### u li 13 14 15 1 6 17 lB 

## i9 20 

### Z

l 22 23 24 25 howeve r , additionAl

### info~ti**o** h as

### beco~ available wh icn euggested th a t those sta.oda.t"dl may not have fully addreeaed the potential riak ftom i ndirect expo.sures to emissions. Now incli.rect expoautu can occur as a resul t . of contact wi tb contarainat.ed eoil. plants, water, o%" food. sec•uso 

### ot ou.r coaoern rega..rd.i-09 i.ndi«ct

## oxpOSU~ds, ebe US£PA strongly r •oomdended in ita 199 4

## lla~ardOUS waste tU.nlr:U.zation and COIIIbUttlon stxateqy that site-specific risk aA&easaent• be

### co**nd~ctod** tor. each combUstion f a cility aee k in9 a RCI\l\ ?ormJ.t
. Permit tin9 a\\tborities could the n

### ua~ th.o result• of thfi Site.-specitic Risk Asaessaent.s to deteaal.ne, on & case-by

- <:.aS* basi&, wbethe t the opcr&t ion of the i.ftcinerator in accoxd&nee w i tt\ t.be atand..erds vould be protective of huaa.t\ bl.a.lth
an d t he e.l'lviro ...-.nt. In tbe>Se casu wh.ere a RC:J\A peorltt l. ng •uworl.ty identified a pOtentiallY
. siQnificant riek, it could invoka the

## ft~ibus aothor:it.y• and a'Uq:ment cbe R CAA pe.J:IIIit \l ith additional conditions. In 1999 toe OSEPA

### re~ised**~d** updated ito nation•l atandar<1S 

### tor hazardOUS waste-bUrnin; i,ncinon.tor• and other devices. Tbe USEP A • 1 f i na l



### VES 0044881 2 

## 3 4 5 6 7 8 9 1 0 11 1 2 13 H 15 16 17 lB 1 9 20 21 22 23 24**2~** 

### standaXds y ete

## p~~~l9ated on september

## 30~ 1999,

## 1nc~eas1n9 control over

## e~iss**ons** of ha%atdous air pollutants at 172 inct.n erat.orsr

## ~~nt kilns, and l iqhtwe ight

### aggrega~e ki lo s operating in the · 

### United States. Thea• !aci1ltles burn aboUt 80

### per~t of the 4 million tons of

## ha~ardou.s was te being ca.buated each year. 'the ,;.-aini.nq 1 5 to 20 percent of waste 1• butned in industrial bo i lers and othe r types 

## Of induetrlal furoac•s th a t w i l l be addresecd l n a future rulem&kin9· 1he

## n~w**•tanda.rd~** are based on the concept of

### ~i~**chievable** control

### ~ecbno~oqy**(~A -c~** **,** or "MAC'l'""), an

## •w~oac;h required by tlle eM. HA.CT "C"8f1ecu the

### m~&Xblua deqree 

### ot hazardous air pollutlon

### ~eduction that can be achieved considerinq the a-qailabUit:y, eur-re. . nt use, co•t . s, snd

### env**ironme n~** **~cts** of

### ar~ous**eai~sionl** c ontrO l tech nologies. The MAC!' still\daXd.e 11Jait ettlasione of dioxins and turan.s, mercury,

## t~ se m l-volatile · metals

### caa.i~ and lead; tho lo w-volatile metals,

### are~enic,**be rylli** **~,** and ch

:romiUJ:I; particulate ro.a.tter, hyd.rochlocic ac id and chlorine, hydroca.d>On&, and cubon monoxide. 

### 'l'be nev rule wa.s 

### unusual- under tbe joint.



### VES 0044891 2 3 4 5 6 1 8 9 10 11 12 13 1 4 15 16 17 18 19 20 21 22 23 24 25 author it y of

### th~ Clean Ail' ACt and the h&O\ltce conserva tion and Recovery Act. The final role

## onsu~es that combustion facilities will b• able to

### ~void t wo potentially different regu l atory co=pliance

### sche**~s** by integratinq

### ~e mooito rinq , cQdPliance testing,

### ~0 record keepin9 requ i reDenee of the Clean Air Act and Resource conservation · and Recovery Act in to oAe

## t~ the Titlo V Clea. n

## ~r .Act per:ade. t'be: nev lo'_,.C'f rule and the Title V

## pe~t**il~ ~eplaee**  tho RCSA permit ae t ho p r imarY regu l atory tool

## r.e;~Ld**ng ha~ardou~**  v4stc inci n era to rs. Ces:taiJ\ly , RCAA perad' ts w ill continue to b e

### reqU~red, but once a

### facil~ty**~nstra tes**  c,OIIIpll&nce w it

b the MAC'l' rule, it maY petit ion to ro..ove pendt conditiOnS

## f~ its RCi<A pedlit covorin9 the cQIIIbusto r. Generally, the only exce.ption vou.ld be the s i tuation w he.re addi tional, aite-sp&c 1tlc

## pe~it COnditions re9ardUlq

## ~a**i~cinerator** are needed to . protec t hU11'AO health and

· the Mvirorwent, in which case those c:oncU.t
.iona would reM i n i1\ the RCAA peadt or coold bo added to the RCAA peroait.

## SiD~**~~** MACT

## s~dards are

## technol~y**b&eed** ina te&d of bei.DC] risk-based. the OSBPA parfomcd a



### VES 0044901 2 3 4
6 1 8 9 10 ll 12
1 4 15 16

1 8
. 19 20 2 1

24 25 nati onal or n atio nw i de ris k ass e ssment to

### dot~~**ine** wh ether ot not the s tan d ard s al so s atisfi ed the RCRA mandate to protect human he,lth 

### and · the

### -enviro**mM~nt.** 'Tb.is nationa l ri s k

eaaed on thi.S national. risk

### usess~nant, the 

### osEPil coocludoed thae t he te<:hn<>lOCJY -b&se d HIIC T standard.l Mt t.be protect:i'l/ e n e ss requi r - ement of R

C

RA· aecauee of tbis, th e Agency

### co**nclude~** thbt i i o Jr. tta:sesame . nta tJOu l d, in 9eneral, no longe r be n eeded foz: hazar;doul

### wil:st~**co~ustion** fa_c;
. il,ltics. Althougb comp rehens i ve, tho national riek aasaaement did contain

### ~ev**~al** unoert•intlos &nd 1Laitatloas, 3od a s a r esult , the

### os&P~ could not
protact L ve o f hua&n he<b and the

## vir~nt in


### . 

## . •ll cuea. Thu-a. i n some oases,. a siee-apec1fic ' riak aae •a em.nt

## ~Y still be neoessa FY to

## confi~ w

hether operat io n of a partic u l ar baz&rdoUS w• ste comb us tor in accOrdance w i th th e HA C

T standards w1 ll be protecti ve. In order to a..s si
. st the Illinol• £PA i
. n evaluating wh ether or oo t the new

## ~T standards



### VE S 0044911 2 3 4 

## s 6 1 8 9 10 11 12 13 14 15 16 17 1 8 19 20 21 22 23 24 

### 25 wil l bo cu . lly protective 

### tor t h is par:ticuuu : .bcil.ity in this particula r l oc a tio n, the USEPA 

### conduce•d a acreen1n9 r i a k analy s i s. l n addition , beeitUSO onyx

### ~111 not have to coll'lPlY with the new MACT stand4rdl 

### until Jun e JO, 2004, thG scxeeoinq

### ~atassaeot**~s** alao u s ed to develop oartain eal.s.slon restrictions vbich could be included in thtt RCAA permit in the short term

### we rcfcz to 

### this risk an a lysis as a screenin9 f i r st , it 

### focused only
on thoao pollu tants w h ich t . he U SEPio. belie v es at this time to have a li ke lihoo d of excQeding 

### aceeptGle levels for chronic toxicity or ine1'e.&aod cancor ci.sk. And second , it is a**sc~eening ~**  tho aonsa that several si.Jq>lifyi.nCJ

### a.sSU~~Ptiona haVe been m.CS. in tbe proce&s of condUccinq the uaeaaGent, ca.uoinC) lt. to en· on the side of' over--pxedic t1"9 ri.sk. A

### mo~ datal le d

### eva~**a.ti on**  w ou l d generally be
. expect'&d to result. i n l ow er .

### pt:edi<::t~ ria\:.

### screen1n~ analyses are g: en erallY

### us~d as a first step 1n

### ~he ' ris k eval uat i on 

### process and can be 

### ueed to determi ne - w h e th er

### ~ more 4etailed 

### rla k analysis ia called for.



### VE S 0 0 44921 2 3 4 5 6 

# , 8 9 1 0 11 1 2 13 14 15 16 l? 18 19 20 2 1 22 23 24 25 At thi:d ti me , . baaed on our experi e n ce w ith the ftndinqa of si•Uar risk assessments,

## uSBP~ Region 5 has cboaeri to focu

_ s specificallY on the potential health !.pacts of polychlorinated 

### dfbenzodioxlna and polychlorinated

### dibeD~ofur**ana,**

## ~re coaDQnlY ce lled dioxins and 

### tu rans, plu a tb• specific

## co**ic/c&LCin09 enic**  aetals

## ~equla~ und• r tbe new USE'PA re.qulat.iODS.

### ~he generel .oQal tor the r i s k

### assas~nt

· analyais ia containe d in 

### the OSEPA 1 

### S 19 98 Draft ttutt\an He alth Ris lt Assess d nt Protocol for u.az3rdou S Wsste combostion

## F~**cilities .**  · w tuch ls**a~a labl~**  

### on our website. secauae the evaluation of multip lo chemic&ls,
a u ltipl.e expo suc e path v a . ys, and UNl tiplo fate anci

### tranlpo~**t p~sses**  is a very . chall engln g exes:ci••· • c:.ocmM:t'cial

### CC~~DPUtu softvAre px09't'61' vaa

## ~tilize4 to run the ris k assessma . ot aQdel. Por t bia pxojeet , we

### us~ the softva...re ayst• c & lled Integr•ted Risk

## Assts~nt Protocol tot " 11Ul.e" ) ,' dQveioped by Lakos Environmental 

### softw are of waterloo, Ontario. tRAP wa s expres s ly dos iqn e d

## ~o c1osely follo w the

## e~ndationa, cbeaical-apeclfic parasaters, and fat• and tnllllpo rt

## a1god.~ q i ven ill the U S&PA ' • 1998



### VES 0044931 2 3 4 $ 6 

# , 8 9 10 

### n 1 2 13 l4 1 5 16 l1 18 

### 19 20 2 1 22 23 24 25 combust ion risk

### assoss~ent gu idan ce·

### ~ toE th e finding s o! the r isk serQ•nin9 , fix&t w ith 't · •apec t to clio x. in.s and )urane: osinq actual esd
. ssiot\ data provi&!:d by the facllity, pre ,LiJai.na.ry ca.lcul&tions predicted that. the potentiAl iocx- eased ti$k o.f cancer ftoa dioxina/furans would be - ell belov the Agency's typical action level of l e ve l 

### ot l in 100f000. tba OSEPA is not at th is t ime recoa.aendinq any 

### f u rther reductions in dioxins/furans emissions. W

it

h 

### respect to t oxic/carcinQ9eDiO

### ~tala, the tta_z . otdous waste eow>ustion-MACT

### ~u**le** regulates 

### emisaion concenttations o f t.be metals 

### arsenic, bct:yU Lull, chrOilium, le ad , ca&niwn
. a.nd Mtcury, beca
. u.se of the Agency" s findings, as discussed ln the p..:eaable 

### ot 1:bat rule, is tbese aet&la prcaent a qruter potenti
. al threat than other• 9ene.ra.llY 0111-lttod from a b.at.a ,dou. s waste iocine.t•tor. 'the preamble futther oonelud&S that omissions 

### ot tbe 

### other eo x ic an d carci nogenic

### eeta**~s ~11**  be 

### adequate l y

### ro#t~iceod via

### t~ now

### par~**icut •e•**  e.iesion limit contAined i n th at rule. H owever , because tnc

## BWC~'t Ru le sinqle:s out these ai x 

### oetala, we 

### singled them out

## n**tbi• ris~**  sc«ent.nq.



### VE S 004494l 2 3 

# • s 6 7 8 9 10 ll 12 13 14 15 16 17 18 19 20 21 22 23 24 25 SOJH of**thet~e** met.als have potential toxic effects, and others are con sidered to b4 carcinogenic. For those that are toxic, the total caLculAted impacts of**~** m•tal were compared to a va.lue of 25**percen~** 

### ot th e e.u.a .r d I.o.ct.x • . . T'M. t is , only a llo wi ng the incineration facility to subject a person to 25 percent or le3S of · the. ma..d..um .xpoaure t hou ght to be s.Ue. tor those aetalo thoug h t to cause ca.ncer, the result• v cre c:ompa_r.CS to • ru.xi.mwn increased uncer riak tarqet valuo oe 1 in 1,000,000. .t ' vo got. a little bit on l ead here but I
won ' t qo into it in the interest of time- Lead needs to bo**loo~od** at a li tUe bit differently
. And a leo for metals, rat her th&n**st.o.~:tlng •**  vith caiuiona and tben ealculatinq**~to** and r1aks, we condocteO the assessment in reve%ae . Region 5 star · ted w ith t.he iq>acts .and risk& considered. aceeptabl · e, and then worked tbe risk model backwards to detemine what eais sio ns would reSult in t hose**qro~nd-level** concentrations and i• pG cta. tn this way, th e analysiG eventually re sultad in a set of suqqasted A'l.eta.l& m1
. sa1on li

..

ito. Now, because ac tual ae tals emissions
. conin9 out



### VES 0044951 2 3 4 5 6 7 8 9 10 ll 12 13 14 15 16 17 18 1 9 20 21 22 23 

### 24 25 the ateck are difficult to measure on a routine basis, RCRA por•lto have generally, instead,**i~po~e d**  

### ceatriotio na on tbe quantity of**~atala** 

### ted i nto the 1nci ner•tor. The relati onship between wb4t is fed into the incinera to r and v h&t ia emitted out the stack is es tab li shed vi& testing which seaaures both feed and**~ssions** si.Utoneou!llY- In the case of the onyx fa cility, feed l iaits vece 6eveloped based. on removal effic i -.ncies demon-strated du

_ rinq pr evious stac . k. te3tinq for tho vari ous re guLated metals. Wb en the Ony x facility complies wi tb t h o HA CT rule, cU£rently scheduled**fo~** June 30 of next year, the teod rates of these**~etalt** wi ll be pEecisely tr3ekad ' and averaged continuo usly by COIIIPUter. Until th•t. time , th e P..CP.A pendt illpOSe& u.nual techniques ancl a.dlainistra.tl.vo cootrola to achieve the appxopriate teed Uait
. e. Aft•r onyx begins cOifiPlying with the MA CT standards an<l conducts it.s KACT QOq)liance t•at, and after it eUb=ita th6 resul t s of the compliance test, the regu lat ions state that it ca n petit ion t.ho I ll inois EPA to remove MOst of the incin erator condition• fr ora the RCAA permit. Tile Illinois EPA w

ill •t t hat time evaluate the test ;eeults 

## tO

VES 0044961 2 3 4 5 6 7 8 9 10 ll 12 13 14 15 1 6 17 1 8 19 

### 20 21 22 23 24 25 determi ne if so me conditio ns should remain in the RCRA permi t . Thank you very**mu~h** tor coming out and parti cip ating in this**~ting** tonight.


### RO BER T W. BERNOTEI T, CAAPP, Onit Manager**Permi~** Sect ion , B ureau of Air
(.BY MR.. BE:R.NOTEIT}: Good evening, · ladies a.nd qe.ntlomen, my name is Bob e.e.znoteit, an acting
. Onit Manag er in th e Division of**~ir** P ol l ution Control Permit Section. I w i1l now gi ve a brief auavaary of ' the t ype of permit we ar4t here to p r ovid e informatio n to you . on. 

### W e, Of course,



## . . are also h ere t o lis t e n to youx conce rn s and to answer an y questions that you may have. But**tirst~** some bac kground on the per. i t. The 19 90 Clean Air Ac t ameoc::bents created a federa l operating permit p r;og ram knoWn**~ation~ly** 

### as Title V. 

### This
. program, knovn in Illinois as the Clean A i r A ct Permit Prog ram, (CAAPP}, focuses
on the**indu~trial** so-u r ces 

### ot ai r po llu t i on of greatest . concern. Aga tn , CAAPP is an acronym for 

### Clean Ai.r l\ct Pennit 

### Program. CAAPP and Title V are synonymous teens and are interchanqeable in



### VES 0044971 2 3 ( 5 6 1 8 9 1 0 11 12 13 14 lS 16 11 18 19 20 2 1 22 23 2 4 2S IUinoi.D. 1:hat

### ie~**,** we refer to tlle pen•ita: th:a.t r esult

## fro~ thia program as both T itle v patmits and CMPP perlllita. The CA,P.PP r11quire.s th a t a si.t\9 1 8 petmit be i s sue d to each offacted source tbat covers all emission unit• and

### ac~vities a t tbe souxeo. Detore a source could have a&nY as tOO penU.t• i , n sooe cas••. ony x. has bad as eany as 18 stat• s&pa.x:a.te &1r

### ope~atlnq**pe~iti.** 1!his often cauaoa confusion and

### pe~it conflic ts. The sinqle,

## a~l-ln**cl uaive** **pe~it stra~egy**  required by Title V oiq>ll.od the process down to a .single, en fo rc eable do cuMent. Thea• C AAPP

## per~ts a r e very detailed in scope and ran9e in siz e from 50 to 1,000 p49••· the typical ai:o ot an operat ing

## per~it before the CAAPP w aa only l to 5 pages. onyx • s clr& f t peEeit i s 165 pac;as. 'the state ope t . a ting permit• t:or onyx•s Unite 2 &nd 3

### ~ere 5 pages eacb. The tEPA

### haa**oomai ~d**  in writing to

### US**EP~** to iaaue ita

## r~inio9**~P** permi ts by the end of**th ~O**  ye&r -- 2003. The i ; as uonce of a

### t-~**e** V

### per~~oit trig9ers

## R~ny**benefi~** that assis t in tbe compliance aod 

### Some of**enforce~~ent** of applicable requ ire.enta. thel6 benctits· are:



### VES 0044981 2 3 4 5 6 1 8 9 10 11 12 13 14 15 16 11 1 8 19 20 21 22 23 

### 2 4 25**~11** 

### requirement s ace consoli dated in a single**~mit ;**  All 

### oondit , ioos i n the peroit, with the exception of those**to~** fees, are t edec&lly ento.cceable, et•t• enforceabl e, and enforceable by the publiCI Oft;en**t~• .q~**  .onitori..ncJ i .s requi.red, if not, the**pc~lt** at**~east** provides a check that current monitoring is appropriate. Th s more**repo~tinq** r e qu ire d

-- al lov s a periodic eelf-ehec k 

### by t he $Ou rc e of**~OP pl** **ianoe.** Tho b 19 4 r.eporti nq req ui reme nts: 1. Reportin9 of Devi&tions. 2. Soai- Mnual Honi tor i ng Report; 3 _ Annual C a.pl.iance. certification, w hich ia
ono of the aain tooLs for compli..ance and it only beCOMS required a .fter the 'title v pemit 1• 1asued. Thi,s is one of
. the pr imarY drawbac k s of CAAPP permi&l not bei nq is sued 

### as quickly as poniblt. 4. A nnual e.iss io ns Report

-- many may S4Y thla is · alrea dy required , and i t is, but onco t h e CAA.'PP permit l.s i
. ssue d there
. becomes avaiLable t.o 

### the tEPA o ainqle document to c to s a-c b eck w ith 

### tho ·Annual &aU-saions Report nUllllber s for coapUance.



### VES 004499