J1SPECIALTYTheLDSTANDARforAirTestingComplianceTestProgramAlcoalntalcoWorksFerndale,WashingtonSource:187BakeOvenBaghouse(BO)AirOperatingPermitNo.000295-0ReportNumber:NW11ALINT109DatesTested:June29-30,2011DatePrepared:September9,2011PREPAREDFORMs.KathrynMitchellAlcoalntalcoWorks4050MountainviewRoadFerndale,WA98248Phone360.384.7206Air Quality Test Report Compliance

Test Program Alcoa lntalco Works Ferndale, Washington Source:

187 Bake Oven Baghouse
(80) This report

is supported

by GOLDEN's
Quality Assurance Manual

and ASTM 07036 Interim Accreditation

as an Air Emission Testing Body.

The information included

in the report

is authentic and accurate

to the best

of our knowledge.

tan
B. Moye

, Ql (Groups

1-111} Project Supervisor

I Onsite

QlTABLE

OF CONTENTS

Air Quality Test Report EXECUTIVE SUMMARY ................................................................................................................................................

1 TABLE 1-1. SUMMARY

OF RESULTS ..................................

.. ..........................................

. ..........................................

1 INTRODUCTION ..........................................................................................................................................................

2 PURPOSE

OF TEST .............

.. ....... ..... .........................

. ....................................................................................

. .. ...
.. 2 PROBLEMS, DEVIATIONS AND/OR EXCEPTIONS ..................•......................................................................................

2 PERFORMANCE

TEST PROCEDURES ...........................................................................................................................

3 USEPA REFERENCE METHODS ..............................................................................................................................

3 USEPA METHOD

1: SAMPLE
AND VELOCITY TRAVERSES

FOR STATIONARY SOURCES ...............................................

3 USEPA METHOD

2: DETERMINATION

OF STACK GAS VELOCITY

AND VOLUMETRIC
FLOW RATE (TYPES PITOT TUBE)

3 USEPA METHODS

3: MOLECULAR WEIGHT (INTEGRATED

BAG) ...............................................................................

3 USEPA METHOD

4: DETERMINATION

OF MOISTURE CONTENT

IN STACK GASES .......................................................

3 USEPA METHOD

5: DETERMINATION

OF PARTICULATE EMISSIONS
FROM STATIONARY SOURCES ..............................

4 TESTING EQUIPMENT .......................................................

.. ..........................................

...... .....................................

4 PREPARATION

OF SAMPLE TRAIN COLLECTION ..........................................................

........ ......................................

.4 SAMPLE TRAIN OPERATION ..............................................

... .....................................

.

. ...... .......................................

5 SAMPLE RECOVERY .........................................................................................

························· ..............................

5 FIGURE
1-1. US EPA METHOD

5 SAMPLING TRAIN .....................................................................................................

7 METHOD 315: FILTERABLE PARTICULATE MATTER
AND METHYLENE CHLORIDE EXTRACTABLE MATTER (MCEM)
.......

8 FIGURE
1-2. USEPA METHOD
315 SAMPLING TRAIN ......................................................................................

..... ....
9 ALCOA METHOD 4075A-
TF: PARTICULATE, GASEOUS

AND TOTAL FLUORIDE ..........................................................

9 FIGURE
1-3. ALCOA METHOD 4075A-

TF SAMPLING TRAIN .....................................................................................

1 0 SOURCE INFORMATION

........ ............ ................................

.......... ...............................................................................

11 FIGURE
1-4. DIAGRAM

OF TESTING LOCATION

FOR THE BAKE OVEN BAGHOUSE ......................................................

11 SAMPLE CALCULATIONS

......

...

.. ..............................................

... ...............................................................................

12 ABSOLUTE STACK GAS PRESSURE

(P

5 ) ............................

..... ................................................................................

12 GAS VOLUME SAMPLED

AT STANDARD CONDITIONS (VM(sTo)) ...................................................................................

12 WATER VAPOR COLLECTED

AT STANDARD CONDITIONS (Vw(sm)) ............................................................................

12 MEASURED STACK GAS MOISTURE CONTENT

(8w

5 ) ...............................................................................................

13 WET MOLECULAR WEIGHT

OF STACK GAS .............................................................................................................

13 STACK GAS VELOCITY ..........................................................................................................................................

13 VOLUMETRIC
FLOW RATE (ACTUAL CUBIC FEET PER MIN) ................. ............................

.... ......................................

13 VOLUMETRIC
FLOW RATE (STANDARD CONDITIONS,

DRY BASIS) .............................................................................

14 PARTICULATE MATTER SAMPLE
AND EMISSION RATE CALCULATIONS ......................................................................

14 ISOKINETIC SAMPLING
RATE ..................................................................................................................................

14 STACK GAS PARTICULATE CONCENTRATION
(GRAINS
PER DSCF) ............................................................................

14 STACK GAS PARTICULATE EMISSION RATE (LB/HR) ................................................................................................

15 TOTAL METHYLENE CHLORIDE EXTRACTABLE MATTER (GRAMS) .............................................................................

15 TOTAL FLUORIDE CONCENTRATION (MG/DSCM} ......................................................................................................

15 EMISSION RATE (LB/TON) ......................................................................................................................................

16 TEST RESULTS

...

. ............... ............................................

. .................

. ......................

. ... ... ....

. ....................................

17 TABLE 1-2. METHOD

5 AND METHOD
315 TEST RESULTS ......................................................................................

17 TABLE 1-3. ALCOA METHOD 4075A-

TF TEST RESULTS .........................................................................................

18 APPENDIX

A- TESTING EQUIPMENT .......................................

. .....................................

. .........................................

A TABLE 1-4. TESTING EQUIPMENT
USED

IN THE COMPLIANCE TESTING .....................................................................

A APPENDIX

B- RESUMES ........................................................................................................................................

B APPENDIX

c- CALIBRATION

DATA ....................................................................................

. .....................................

c APPENDIX

D- FIELD DATA .....................................................................................................................................

D APPENDIX

E- REFERENCE METHOD DATA .............................................................................................................

E APPENDIX

F- PROCESS DATA ...............................................................................................................................

F APPENDIX

G- LABORATORY

DATA

. ............................

......

. ..... ............ ........

. ......

. ....... ...... ................................

.... ... G4 of90 **~** OLDE I **~-'SPECIALTY**

Air Quality Test Report EXECUTIVE SUMMARY On June 29- 30, 2011, Golden Specialty,
Inc.'s (GOLDEN) Northwest Regional Office was contracted

by Alcoa lntalco Works

to perform

air testing

at their facility located

in Ferndale, Washington. GOLDEN performed

a compliance

test program

on the exhaust

of the Bake Oven Baghouse.

The test was conducted

in accordance

with

all appropriate United States Environmental Protection Agency (USEPA) Methodologies

as well as all requirements outlined

in Alcoa lntalco's

Air Operating permit
No. 000295-0. For the compliance

test program, three

(3) 5-hour test runs were performed

by experienced

test personnel in accordance

with United States Environmental Protection Agency (USEPA),
Code

of Federal Regulations,

Title 40, Part 60 (40CFR60), Appendix

A Methods

1, 2, 3, 4, and

5, 40CFR63 Method
315 and Aluminum Company

of America (ALCOA) Source Sampling Method 4075A-TF.

The methods

are discussed

in the Performance

Test Procedures section

of this report. Included

in this test report are sections detailing

the Test Program, including Executive Summary, Introduction, Sampling Procedures, Source Information, Sample calculation

and Test Results Sections;

with Appendices
which include

all resumes

of key personnel, calibrations,

field data, calculated
data, and process data. Table

1-1 presents

the compliance results

of the test program performed

on the Bake Oven Baghouse. Emission Source Methods

Three Run Compliance Unit No. Name Perfonned

Test Date(s) Analyte, Units Average

Limit FPM, gr/dscf

0.0002 FPM, lb/hr

0.16 Bake Oven

US EPA Methods

1, 6/26.
MCEM, gr/dscf 0.00025 187 Baghouse

2, 3, 4, 5, 315

& 6/30/2011 Alcoa 4075A·

TF

MCEM, lb/ton

*0.015

0.18 Total Fluoride,
ppm
0.256 Total Fluoride, lb/ton *0.0055

0.20 • Lbl!on

of Green Anode placed

in the Anode Bake Furnace. Table 1·1. Summary

of Results

11Page5 of90

Air Quality Test Report INTRODUCTION Purpose

of Test The purpose

of the test program
was

to demonstrate compliance

for mass emission concentrations

of filterable particulate matter (FPM), Total Fluoride,

and Methylene Chloride Extractable Matter (MCEM) from the exhaust

of the Bake Oven Baghouse.

Mr. Stan Moye served

as Project Supervisor,

and performed

the testing with the assistance

of Messrs.
Paul Clark, Pete Hilty and Daniel Farwell.

Ms. Patricia Bilskis was the point

of contact

for Alcoa lntalco Works during
the testing.

All documents

and data relating

to this test program

are presented

in this report. Airflow was determined
using USEPA Methods

1 and

2. Testing

for

0 2 and C02 was performed
using USEPA Method

3. The moisture content

of the stack gas was measured
using Method

4, which was performed inclusively

with Method
315 and Alcoa Method 4075A-

TF for the Bake Oven Baghouse. Testing procedures

are discussed

in more detail

in the test methods section.

All calculated reference method data is provided

in Appendix

E, and examples

of all calculations

are presented

in the Sample Calculation section of this report. Process Data

is provided

in Appendix

F of this report. Problems, Deviations and/or Exceptions No problems encountered
during this test program.

21 Page6 of90 UD I **~) PECIALTY** 

Air Quality Test Report PERFORMANCE

TEST PROCEDURES USEPA Reference Methods This section provides

a detailed description

of the individual USEPA Reference Methods employed

in this test (40 CFR 60, Appendix

A).

A schematics

of the various sampling systems used

to perform

the test program

on the different sources

can be found

in Figures

1-1 through

1-4. Specifics

for the test equipment utilized

in this program

are presented

in Appendix

A. USEPA Method

1: Sample
and Velocity Traverses

for Stationary Sources Sampling traverse points were determined based

on the ratio

of the stack diameter

to the upstream

and downstream distances

of the sampling plane

to the closest disturbances. The minimum number

of traverse points

on the sampling plane

is determined

from Figure 1-2 and Table
1-2 of 40CFR60, Appendix

A, Method

1. USEPA Method

2: Determination

of Stack Gas Velocity
and Volumetric

Flow Rate (TypeS Pitot Tube) Velocity

and volumetric

flow rates were determined

from the measurement

of the stack gas velocity head with

a Type-S Pitot tube and inclined manometer.

The Pitot tube was constructed

per USEPA Method

2 design specifications.

Based

on the face opening alignments, external tubing diameter,

and base-to-opening

plane distances,

a coefficient value

of 0.84 was assigned

to the Pitot tube. USEPA

M ethods

3: Molecular Weight (Integrated

Bag) USEPA Method

3 was performed

to determine

the molecular weight

of the gas based

on measurements

of the concentration

of oxygen
(02) and carbon dioxide (C02)

in the stack gas. Method

3A analyzers
were used

in lieu
of the Orsat analyzer.

02 was measured using

a paramagnetic analyzer.

C02 was measured
using

a non-dispersive
infrared (NDIR) analyzer. During each test run an integrated

bag

of the sampled

gas stream was collected. Method

3 was performed

at any site that gaseous emissions testing using direct interface sampling

was not being performed.

The samples were analyzed onsite the same day. Molecular weight data was collected during

all emission

test periods. USEPA Method

4: Determination

of Moisture Content

in Stack Gases USEPA Method

4 was performed inclusively

with Methods

5, 315 and 4075A-TF

to measure

the moisture content

of the stack gas for calculating

the volumetric

flow rate and molecular weight

on

a dry basis. The impingers

for each high-flow sample train were weighed before and after each run to determine moisture weight gain. 3IPageliDLDE/\17of90AirQualityTestReportUSEPAMethod5:DeterminationofParticulateEmissionsfromStationarySourcesTestingEquipmentAbuttonhookprobenozzlemadeofstainlesssteelwithasharp,taperedleadingedgewasused.Theangleofthetaperwas<30°,andthetaperwasontheoutsidetopreserveaconstantinternaldiameter.Arangeofnozzlesizessuitableforisokineticsamplingfrom1/8to1/2inchwasavailablethedayoftesting,andeachnozzlewascalibrated.Theprobelinerwasmadeofstainlesssteeltubingwithaheatingsystemcapableofmaintainingagastemperatureattheexitendduringsamplingof120±14°C(248±25°F).ATypeSpitottubewasattachedtotheprobe(asshowninFigure1-1)toallowconstantmonitoringofthestackgasvelocity.Theimpact(highpressure)openingplaneofthepitottubewasevenwithorabovethenozzleentryplaneduringsampling.TheTypeSpitottubeassemblyhasacorrectioncoefficient,typically0.84whenphysicalcriteriaaremet.Adualinclined/verticaloil-guagemanometerwasusedforvelocityheadandorificedifferentialpressurereadingsAborosilicateglassfilterholder,withaglassfritfiltersupportandaTeflon®coatedgasketwasused.Theholderdesignhasapositivepressuresealagainstleakagefromtheoutsideoraroundthefilter.Theholderisattachedwithconnectingglasswaretotheoutletoftheprobe.Thefilterheatingsystemutilizedforthistestwascapableofmaintainingatemperaturearoundthefilterholderduringthesamplingof120±14oc(248±25°F).Atemperaturegaugecapableofmeasuringtemperaturetowithin3°C(5.4°F)isinstalledsothatthetemperaturearoundthefilterholdercanberegulatedandmonitoredduringsampling.Theimpingertrainusedtoremovemoisturefromthegassampleconsistedoffourimpingersconnectedinserieswithleak-freegroundglassfittingsoranysimilarleak-freenon-contaminatingfittings.Thefirst,thirdandfourthimpingerswereoftheGreenburg-Smithdesignthathavebeenmodifiedbyreplacingthetipwitha1.3em(1/2in.)IDglasstubeextendingtoabout1.3em(1/2in.)fromthebottomoftheflask.ThesecondimpingerwasoftheGreenburg-Smithdesignwiththestandardtip.Athermometer,capableofmeasuringtemperaturetowithin1oc(2°F)wasplacedattheoutletofthefourthimpingerforexittemperaturemonitoringpurposes.Themeteringsystemwasmadeupofthefollowing:vacuumgauge,leak-freepump,thermometerscapableofmeasuringtemperaturetowithin3°C(5.4°F),drygasmeter(DGM)capableofmeasuringvolumetowithin2%,andrelatedequipment,asshowninFigure1-2.PreparationofSampleTrainCollectionDuringpreparationandassemblyofthesamplingtrain,allopeningswherecontaminationcanoccurwerekeptcovereduntiljustpriortoassemblyoruntilsamplingwasabouttobegin.100mlofdistilled,deionizedwaterwasplacedinthefirsttwoimpingers,thethirdimpingerwasleftempty,andsilicagel,preweighedtothenearest0.5gwasplacedinthefourthimpinger.Usingtweezersorcleandisposablesurgicalgloves,alabeled(identified)andweighedfilterwasplacedinthefilterholder.Theprobewasmarkedtodenotethesamplepoint41Page8 of90

Air Quality Test Report locations,

and crushed

ice was placed around

the impingers

just before
the start

of sampling. Sam ple Train Operation The sample ports were cleaned prior

to the test run to minimize

the chance

of drawing deposited material

into the sample when removing

or inserting

the probe. During
the sampling

run, an isokinetic sampling

rate was maintained, and

a temperature

of 248

± 25°F was maintained around

the filter.
For each run, pertinent
data was recorded

on the appropriate

data sheet.
The stack cross-section

was traversed,

as required

by Method

5, being careful

not
to bump
the probe nozzle
into the stack walls when sampling
near the walls, which minimizes

the chance

of extracting deposited material. During

the test run, periodic adjustments

were made

to maintain

an isokinetic sampling

rate, and additional

ice was added

to the impinger
train

in order

to maintain

an impinger outlet temperature

of 68°F

or lower. Also, periodic checks of the manometer

were made

to insure

it was level and zeroed. At the end

of the sample
run, the coarse adjust valve was closed,

the probe and nozzle were removed
from the stack,
the pump was turned

off, the final DGM meter reading
was recorded,

and

a post-test leak-check

was conducted.

Also, the pitot lines were leak-checked.

The lines must pass this leak-check

in order to validate

the velocity head data. Finally,

the percent isokinetic

was calculated to determine whether

the run was valid

or another

test run should

be performed. Sam ple Recovery Sample collection procedures began

as soon

as the probe was removed
from the stack

at the end

of the sampling period.
The probe was allowed

to cool
so

it could

be safely handled,

all external

PM near the tip of the probe nozzle was wiped
off, and

a cap was placed over

it to prevent losing

or gaining
PM. The probe was removed
from the sample train, any silicone grease
was wiped clean, and the open outlet

of the probe was capped. Care was taken
not
to lose any condensate

that might

be present.
The umbilical
cord was removed
from the last impinger,

and the impinger

was closed

off with Teflon® tape. The selected cleanup area was clean and protected
from the wind

so that the chances

of contaminating

or losing
the sample
was minimized.

A 200 mL portion

of the acetone used for cleanup
was directly taken from the wash bottle being used and placed

in a glass sample container labeled "acetone blank.

• 5I PageI

.

**~** OLD£ **-'SPECIALTY**

9 of90 The samples were recovered

as follows:

Air Quality Test Report Container

No.

1. The filter was carefully removed
from the filter holder and placed

in its original identified
petri dish and sealed with Teflon® tape.

A pair of tweezers and/or clean disposable surgical gloves was used

to handle

the filter. Container

No.

2. The recovered

PM
or any condensate

from the probe nozzle, probe fitting, probe liner, and front half

of the filter holder was collected by washing

the inner surfaces

of these components

with acetone

and placing the wash

in
a sample container.

The probe liner was rinsed and brushed

a minimum

of six times

as required

for stainless steel probes.
This container was properly labeled, sealed with Teflon® tape, and the sample level was marked with

a permanent marker prior

to transport

to the lab. lmpinqers

1, 2, and

3 Using

a graduated cylinder,

the liquid contained

in the impingers

was measures

to the nearest

1 ml and the volume recorded

on the field data sheet.

All liquid contained

was then discarded
since

no back half analysis
was required

for this test program. Using

a top loading balance, each of the impingers

was weighed

to within
0.5

g and the weight recorded

on the field data sheet. This data was used

in the stack gas moisture calculation. Silica Gel. The color

of the indicating
silica
gel was noted

to determine whether

it had been completely spent, and

a notation

of its condition

was made. Using

a top loading balance,

the impinger
was weighed

to within
0.5

g and the weight was recorded

on the field data sheet. Reagents:

The reagents
used

in sampling

are as follows:

(1) Glass fiber filters, without organic binder, exhibiting

at least
99

. 95 percent efficiency (<0.05 percent penetration)

on 0.3- micron dioctyl phthalate smoke particles.

The filter efficiency

test

is conducted

in accordance with ASTM Method

D 2986-71.

(2) Silica Gel, Indicating
type,

6- to 16-mesh.

If

it has been previously
used,

it is dried

at 175°C (350°F)

for

2 hours. Since analysis

of the material caught in the impingers

is required,

(3) deionized distilled water was used. Analysis

of deionized water

is run prior

to field use
to eliminate

a high blank

on test samples.

61 Page10of90__:__""''DLDEl\1AirQualityTestReportTEMPERATURESENSORPitOtTUb8IMPINGERTRAINSENSORNoz!!.!,_THERMOMETERiHEATED/AREA_j>-----1-,1_______- - --OILMANOMETERORIFICEMANOMETER\----111"--Figure1-1.USEPAMethod5SamplingTrain71Page11 of 90

Air Quality Test Report Method 315: Filterable Particulate Matter and Methylene Chloride Extractable Matter (MCEM) The sample train used
for particulate matter and methylene chloride extractable matter (MCEM) sampling

was
an USEPA Method
315 design,

as shown

in Figure
1-2. The sample train consisted

of
a quartz nozzle
and quartz probe liner,

a quartz fiber filter, followed

by an impinger train. The glass filter assembly

was enclosed

in a temperaturecontrolled heated sample
box. The average

box temperature

is maintained

at 248°F

± 25°F. The nozzle, probe liner, pre-filter connective glassware,

and filter are referred

to as the "front-half"

of the sample train. Following

the filter was

a condenser section, which,

by convention,

is referred

to as the "back-half."

The condenser section consisted of
a modified Greenburg-Smith
bubbler containing

100 milliliters
(mL)

of deionized water, a second impinger containing

100 mL

of deionized water,

an empty bubbler,

and

a bubbler containing indicating
silica
gel desiccant.

The back-half

was maintained

at
a temperature
below 68°F

by adding

ice to the condenser section during sampling.
After sampling,

the filters were recovered, desiccated,

and weighed

to constant weight.
The same weighing procedures

were followed

to obtain
the tare weights

for the filters after

a sixteen-hour extraction

in methylene chloride (CH2Cb)

and drying. The nozzle and probe liner were recovered

with acetone

as sample portion

"2," for the gravimetric determination,

then they were given

a final rinse with CH2Cb
and the rinsate was quantitatively transferred

to

a separate glass storage container labeled, "2M." The acetone rinse was evaporated

and weighed

to constant weight (same protocol

as the filters).
The impingers
were recovered

with deionized

(DI) water into one container, labeled "3W, and then they were rinsed with
25 mL
of acetone

into another container. They were rinsed again with three

25 mL portions

of CH2CI2
into the container

with the acetone rinse. The back-half aqueous samples were then extracted

with
50 mL
of CH2CI2 that had been used

to rinse the sample bottle. The CH2CI2 portion was drained into

a beaker.
The extraction

was repeated twice more with
50 mL portions

of CH2CI2. The aqueous portion was archived.

The CH

2 CI 2 sample, called "3X," was evaporated almost

to dryness

and transferred

to

a tared aluminum

dish and was then dried and weighed.

The combined acetone/CH

2 CI 2 rinse, sample portion "3S," was evaporated almost

to dryness, transferred

to

a tared aluminum
dish, dried, and weighed.

This analysis
was the methylene chloride extractable matter (MCEM) portion

of the back-half. A gravimetric particulate matter analysis
was not performed

on the back-half.

After gravimetric analysis
was complete,

the front-half sample portions (including filters and probe rinse residues)
were analyzed

for MCEM.

The filter was placed

in
a beaker

to which 100 mL CH2Cb was added.
The beaker was sonicated

for three minutes
and was allowed

to stand

for twenty minutes.

The solution
was filtered, then transferred

to

a BOchner funnel
and vacuum-filtered

into

a beaker.

The beaker
was placed

in

a temperature-controlled

oven

at less than 40°C and evaporated almost

to dryness

. The contents
were transferred

to

a tared aluminum

dish, evaporated

to dryness,

and weighed.

25 mL of CH2CI2 was added

to the acetone beaker residue.

The beaker was sonicated

for three minutes
and was allowed

to stand
for twenty minutes.

The solution was combined

with the CH2CI2 probe rinse and the combined sample
was filtered then transferred

to

a BOchner funnel
and vacuum-filtered

into

a beaker

. The beaker
was placed

in
a temperature-controlled

oven

at less than 40°C and evaporated almost

to dryness.

The contents were transferred

to

a tared aluminum
dish, evaporated

to dryness,

and weighed.

The filter residue, front-half
rinse residue,

the back-half extract residue,

and the back-half solvent rinse residue represent

the total MCEM

for the sample.

BI Page12 of90 r

liD DEN **-~)SPECIALTY**

Air Quality Test Report TEt.IPERATURE SENSOR -------- PROBE Oil MANOMETER ORIFICE t.IANOt.IETER

VACUUt.l PUt.IP Figure
1-2. USEPA Method

315 Sampling Train Alcoa Method 4075A-

TF: Particulate, Gaseous

and Total Fluoride Alcoa Method 4075A

- TF was performed

to measure

the fluoride content

of the stack gas.
Use

of this method requires

that the analyses

be performed

per Alcoa 4076TF/914F,

which was devised especially

for this sampling method.

The sample train consisted

of
a stainless
steel nozzle mounted

on

a 47mm in-stack stainless
steel filter holder containing

a 47mm Teflon® filter. The filter holder was connected

to
a series

of four impingers

by means

of
a stainless
steel probe.
The first two impingers contained 125 ml of
a 0.1

N sodium hydroxide (NaOH),

the third

is empty,
and the fourth indicating silica gel desiccant. Following sample collection

and the post test leak check,
the filter was transferred

to petri dishes labeled with the sample date, client name, and run number.

The contents

of the nozzle and filter holder inlet section were quantitatively transferred

to

a storage container. Several rinses

of acetone were used
for the front-half clean-up.
After the 9IPa
ge!
liOL

£ **-~)SPECIALTY**

13 of 90

Air Quality Test Report particulate gravimetric determination

was made,
the particulate sample was rinsed

off the Teflon® filter, evaporated

to dryness

and fused with NaOH.
The fusion was dissolved

in water and distilled. Fluoride
was determined directly using the fluoride selective

ion electrode. The contents

of the impingers containing condensed moisture

and the water solutions were quantitatively transferred

to
a graduated cylinder using

0

. 1 N NaOH and
01 water

. The solution
was transferred

to
a separate labeled sample container

for fluoride analysis. Sample blanks

of the filter and reagents were prepared

and analyzed along with the samples. Stack WaU In-Stack Finer Holder lncUned Manometer ·s· Type Pilot Tube

125 mL O.INNaOH

Empty

T e m pe

r a
t u r e Se
n sor Silica Gel Figure
1-3. Alcoa Method 4075A-TF Sampling Train
Vacuum Gauge 10

I Page14 of 90

Air Quality Test Report SOURCE INFORMATION The sample ports

on the Bake Oven Baghouse

are located 85.5 inches downstream

and

> 120 inches upstream
from the nearest disturbances.

The Bake Oven Baghouse

has an inside diameter

of 84.0-inches. A diagram

of the Bake Oven Baghouse

is shown below

in Figure 1-4. TRAVERSE POINTS:

16 NUMBER

OF PORTS:

2 POINTS/PORT:

8 STACK

ID: 84.0 ln. PORT LENGTH:

6.0 ln. TRAVERSE POINT NO. 1 2 3 4 5 6 7 8 DISTANCE FROM INSIDE WAll,

ln

. 2.7 8

. 8 16

. 3 27.1 58.9 67.7 75.2 81

. 3 Baghou• Figure
1-4. Diagram

of Testing location

for the Bake Oven Baghouse

11I Page15 of 90

Air Quality Test Report SAMPLE CALCULATIONS The following calculations

were used

in the determination

of emission rates for the unit's exhaust. Absolute Stack Gas Pressure

(Ps)
p = P.

+ psratic s
bar
l3.

6 Where:

Pba,

= Barometric pressure

(in. Hg) Psratic =Static pressure

of stack gas (in.
H 2 0) Gas Volume Sampled

at Standard Conditions (Vmtstd)) Where:

V.n(srd)

= **(~)xVmx**
**Y[~ar +(~)]**  29.92

Tm Vm =Actual
gas volume sampled

(ff) Y = Gas meter calibration factor Pba,

= Measured barometric pressure

(in. Hg) !JH =Average differential pressure

(in H 2 0) Tm =Absolute average meter temperature

COR) Water Vapor Collected

at Standard Conditions (Vw(std)) Vw(std)

= 0.04715

X **~c** Where:

V,c
= Liquid collected

in impingers

(g)

121 PageliDLDE/\116of90MeasuredStackGasMoistureContent(Bws)vB=w(std)ws()V+Vw(std)m(std)WetMolecularWeightofStackGasStackGasVelocityWhere:v,=(85.49)(cpXavgW)(i)P.M,Cp=Pitotcoefficient(0.84)Ts=Averagestacktemperature(0R)P5=Absolutestackgaspressure(in.Hg)AirQualityTestReportMs=Molecularweightofstackgas(lbllb-mole)VolumetricFlowRate(Actualcubicfeetpermin)Where:Oaw=Volumetricflowrate(acfm)V8=Stackgasvelocity(ftlsec)As=Stackarea(tf)131Page17 of90 f:

6 DEN **,~)SPECIALTY**

Air Quality Test Report Volumetric

Flow Rate (Standard Conditions,

dry basis) Where:

Qsd =Volumetric

flow rate (dscfm) Ps =Absolute
stack gas pressure

(in. Hg) T 5 =Average stack temperature

( 0 R) Bws

= Stack moisture content Particulate Matter Sample
and Emission
Rate Calculations lsokinetic Sampling
Rate Where:

I=

( 0.0945xT. xVm(srdJ

J **~X**

v, X An x() x(l- Bws) T 5 =Stack temperature

("R) Vm{stdJ =Sample volume (dscf) Ps =Absolute
stack gas pressure

(in. Hg) Vs = Stack gas velocity (fps) An= Area
of nozzle opening
face (tr) 8 = Run time (minutes) Bws

= Stack gas moisture content Stack Gas Particulate Concentration
(grains
per dscf) Where:

Cs =0.01543 **X~** vm(srd) Cs
= Particulate concentration (gr/dscf) mn =Total particulate collected

in sample (mg) Vm{stdJ =Sample volume

at standard conditions (dscf)

141 Page18of90AirQualityTestReportStackGasParticulateEmissionRate(lb/hr)Where:P,,,=xQsrdx60Pmr=Particulateemissionrate(lblhr)Cs=Particulateconcentration(grldscf)Ostd=Stackgasflowrate(dscfm)60=minlhrTotalMethyleneChlorideExtractableMatter(grams)mmcem=Im,o,al-wa-w,-tbmmoem=TotalMethyleneChlorideExtractableMatter(grams)'l_miDial=SumoftheCH:!JI2fromeachcontainer(grams)W8=Weightofresidueinacetoneblank(grams)w1=Weightofresidueinmethylenechlorideblank(grams)fb=Weightoffilterblank(grams)TotalFluorideConcentration(mg/dscm)cif=cfp+cfgCtt=TotalFluorideconcentration(mg!dscm)=TotalParticulateFluorideconcentration(mg!dscm)=TotalGaseousFluorideconcentration(mg!dscm)15IPageEmissionRate(lb/ton)Where:19of90AirQualityTestReportEb=EmissionRateofTF(lblton)ofgreenanodeproducedCs=ConcentrationofTF(mg/dscf)Osc1=VolumetricFlowrate(dscfh)K=ConversionFactor(453,600mgllb)161PageGOlDE. **-~)SPECIALTY** TEST RESULTS

20 of 90

Air Quality Test Report A comprehensive summary

of results

for the testing perfonned

on the sources

are listed below

in Tables

1- 2 and 1-3.

All supporting calibration, process, laboratory

and field data collected

for this project

are provided

in the following Appendices. l Plant

1 AlCoa ntalco Works

I Address Ferndale,

W1<

Job

I NW11AUNT109

I I Location

1 Balle oven Bll!lhDuse IPersonne

1Da18

6129. &'3012011 Run Number

I

,

2

3

I Avoraao

Com lilian
.. Date

Test Date

612912011 6129/11-6130111
&'3012011 Start

Run Start Time

15:36:00 21:59:00
4:15:00 Run Finish nme

20:55:00
3:23:00 9:29:00 Net Traversing Points

16

16

16 9

Net Run Tome, min.

300

300

300

300 DN
Nozzle Diameter.

in.

0.188

0.188

0.188

0.188 c,

**P~ot** Tube Coeficient

0.84

0.84

0.84

0.84 y

Dry Gas Meter Calibration Factor

1.007

1.007

1.007

1.007 Par Barometric Pressure,

ln

. Hg

29.70

29.80

29.75

29

. 75 411 Average orifiCe meter Differenbal,

on. H,O

1.19

1.27

1.43

1.29 v,.

Dry Gas Meter Volume Sampled,

tr 195.346 196.587

202.568 194.834 t, Average

Dry Gas Meter Temperature,

F

74.5

68.9

64.6

69.3 v_d

Dry Gas Meter Volume Sampled,

dscf 183.555 197.448

204.864 195.289 **V~e**

Total Moisture Liquid collected,

g

202.8

259.6

257.7

240.0 Ywatcl Volume

of Water Vapor,

scf

9.56

12.24

12.15

11.32 %H20 Moisture Content

of Stack Gas,

%

4.95

5.84

5.60

5.46 %C02 Carbon Dioxide,

%

1.50

1.60

1.20

1.50 %02 Oxygen,%

18.50

18.00

19.10

18.53 Md

Dry Molecular Weight, lbllb-Mole

28.98

29.01

28.96

28.98 M,

Wet Molecular weight. lbiJb..Mole

28.44

28

. 37
28.34

28.38 P,

Aue Gas Static Pressure,

in

. H,O

.0.16

.0

. 16

.0.20

.0

. 17 P, Absolute
Flue Gas Pressure,

on. Hg

29.69

29.79

29.74

29.74 t. Average Stack Gas Temperature,

F

217.3

215.6

211.9

214.9 1/I!.P,

•• Average Square-Root Velocity Head,

in H 2 0

1.145

1.190

1.273

1.203 v, Average Stack Gas Velocity, fVsec

73.64

76.43

81.65

77.24 A.

Stack Crossectional

Alea,

If

38.48

38.48 38.48 38.48 Qod

Dry Volumetric
Aow Rate, dry sclm

125,030
129,304 139,005 131,113 a_

Actual Wet Volumetric

Aue Gas Flow Rate, aclm

170,044
176,474 188,537 178,352 %I Percent lsoktnetic

of Sampling Rate,

%

97.7

101.6

98.1

99.1

90. 110 pb Quantity

of green anode material placed

in fumace, tons/In

18.02

18.02

18.02

18.02 w, Filterable Particulate Matter,

g

0.0054

0.0000
0.0000
0.0018 c, **A~erable** Particulate Concentration,
gr/dscf

0.0005

0.0000

0

. 0000 0.0002 E, **Fi~erable** Particulate EmoSSion Rate, lblhr

0

. 48

0.00

0.00

0

. 18 E, Filterable Particulate Emission Rate, lb/day

11.60

0.00

0.00

3.97 WuceM

Total Methylene Chloride Extractable Matter,

g

0.0052

0.0016

0

. 0024 0.0031 CuceM

Total Methylene Chloride Extractable Matter Concentration,
gr/dscf

0.00044
0.00013 0.00018 0.00025 EucEII

Total Methylene Chloride Extractable Matter Emission Rate, lblhr

0.469

0.139

0.215

0.274 EucEII

Total Methylene Chloride Extractable Matter Emission Rate, lb/day

11.24

3.33

5.17

6.58 EucEII

Total Methylene Chloride Extractable Matter Emission Rate, lblton

"0.028

"0.008

*0.012
*0.015

0.18 • lblton

of Green Anode placed

on the Anode Baka Furnace. Table 1-2. Method

5 and Method
315 Test Results
171Pagef OLD£ =.:>)SPECIALTY Plant

I Alcoa lnta co Works
Addreas L Location

I Bake Oven Baghouse

I Personnel Run Number Date

Test Date Start

Run Start Tome Run Finish r.ne Net Traversing Points 8

Net Run Time. m11. ON
Nozzle Diameter,

in

. c.

**P~ot** Tube Coelicient y

Dry Gas Meter Calibration Factor Par Barometric Pressure,

ln. Hg 4H Average orifice meter Differential,

in. H,O v,.

Dry Gas Meter Volume Sampled,

tr t, Average

Dry Gas Meter Temperature,

F v_d

Dry Gas Meter Volume Sampled,

dscf v ..

Total Moisture liquid collected,

g Vwa1d Volume

of Water Vapor,

sci %H20 Moisture Content

of Stack Gas.

% **%C~**
Carbon Dioxide.

% %02 Oxygen,% Md

Dry Molecular Weight, lb/1b-Mole M,

Wet Molecular weiglt. lbllb-Mole P,

Flue Gas Static Pressure.

ln.
H 2 0 P, Absolute
Flue Gas Pressure.

in. Hg t. Average Stack Gas Temperature,

F **"~** ... Average Square-Root Velocity Head,

in H 2 0 v, Average Stack Gas Velocity, fVsec A.

Stack Crossectional

Area,

It' old

Dry Volumetric

Flow Rate, dry scfm o ...
Actual Wet Volumetric

Flue Gas Flow Rate, acfm %1 Percent lsolonetic

of Sampling Rate,

%

21 of90 Ferndale

WA HIDDF

I pb Quantity

of green anode material placed

in furnace, tonslhr Fp Particulate Fluoride Concentration. mg/dscm Fp Particulate Fluoride Concentration,

ppm Ep Particulate Fluoride EmissiOn Rate, lblhr Ep Particulate Fluoride Emission Rate, lblday Eb Particulate Fluoride Emission Rate, lblton F, Gaseous Fluoride Concentration, mg/dscm Fa Gaseous Fluoride Concentration,

ppm E, Gaseous Fluoride Emission Rate, lblhr E, Gaseous Fluoride Emission Rate, lblday **~** Gaseous Fluoride Emission Rate, lbllon F,

Total Auoride Concentration, mg/dscm F,

Total Auoride Concentration,

ppm E,

Total Auoride Emission Rate,lb/hr E,

Total Fluoride Emission Rate, b'day Eb

Total Fluoride EmiSSJOO Rate, lblton • Lblton

of Green Anode placed

in the Anode Bake Furnace

Air Quality Test Report Job

I NW11AUNT109

I !Data

I

11129

• 613012011

J 1

2

3 Average Compliance 11/2!112011 11129. 1113012011 1113012011 15:25:00 21:541:00
4:12:00 20:53:00
3:20:00
9:28:00 111

111

18 300

300

300

300 0.113

0.113

0.113

0.113 0.84

0.84

0.84

0.84 1.043

1.043

1.043

1.043 29.70

29.110 29.75 29.75 0.17

0.111

0.19

0.17 71.6110

611.533

72.6113
70.292 78.7

74.2

68.3

74.4 72.821

611.345

75.225
72.064 56.7

72.4

87.8

72.3 2.67

3.41

4.14

3.41 3.55

4.78

5.22

4.51 1.5

1

. 11

1.2

1.50 18.5

18.0

19

. 1 18.53 28.98

29.01

28.98

28.98 28.59

28.48

28.38

28.49 .0.16

.0.15

.0.18

.0.16 29.69

29.79

29.74

29.74 219.9

215.1 212.5 215.8 1.179 1.133 1.235

1.182 75.75

72.58

78.13

75.82 38.48

38.48

38.48

38.48 130,002
124,284
135,142 129,813 174,913
187,800
182,718 175,077 102.1

101.3

102.5

102.2 i0·110 18.02

18.02

18.02

18.02 0.0107

0.0000

0.0000
0.0038 0.0135

0.0000

0.0000
0.0045 0.0052

0.0000

0.0000
0.0017 0.125

0.000

0.000

0.042 *0.0003
*0.0000
•o.oooo *0.0001 0.062

0.161

0.371

0.198 0.078

0.204

0.000

0.084 0.030

0.075

0.188

0.098 0.73

1.80

4.51
2.347 *0.0017
*0.0042
*0.0104 *0.0054 0.073

0.181

0.371

0.202 0.092

0.204

0.470

0.258 0.038

0.075

0.188

0.100 0.85

1.80

4.51

2.39 *0.0020
*0.0042
*0.0104 *0.0055

0.20 Table 1-3. Alcoa Method 4075A-TF
Test Results

181 PageliOLDEN22of90AirQualityTestReportAPPENDIXATestingEquipment23 of 90

Air Quality Test Report T esting Equipment Provided

in the Table
1-4 below

is a list of all testing equipment

used

in the emission

test

at Alcoa lntalco Works

.

Golden Specialty,

Inc. Trailer
No.
11 Constituent

Make/ Model Operating Range
Serial Number Velocity

I Pitot Environmental
Supply

00
P003NW Velocity

I Pitot Environmental
Supply

00

P0029 Moisture/ Environmental
Supply

00

1696 Meter Box Moisture/ Environmental
Supply

00

1729 Meter Box FPM/Nozzle

Apex

NA

0.113

& 0.188 02
& C02

CAl Model 602P 0-25%

& 0-20% W02022M Table 1-4. Testing Equipment
Used

in the Compliance Testing"'""''liCJLDEN24of90AirQualityTestReportIGOLDENI25of90AirQualityTestReportSCOTTB.SWIGGARD,Ph.D.QSTIPRESIDENTITECHNICALDIRECTORProfessionalExperienceSummary•Broadbackgroundinenvironmental complianceandregulatoryissues.Hasdirectedprojectsassociatedwithairpermitting,groundwatercontamination,airtoxinsemissionscontrol,hazardousmaterialscontrolandreporting,wastewaterprocesscontrol(metalsremoval),energyconservation,industrialventilation,noisecontrol,bioremediation,andstormwatercontrol.•Extensivebackgroundinemissiontesting,withover1,600testspersonallyconductedand/orsupervised.•Responsibleforthecontinueddevelopmentoftestingcapabilitiesandtheirresearchanddevelopment.•Providesprojectmanagementfortestingatassignedclient'sfacilities.Providesfieldsupporttotheprojectmanagersontestingprotocolsandmethods.•ResponsibleforverificationandvalidationontestdataaspartofaQualityAssurance/QualityControlProgram.SelectedPubIications/PresentationsSwiggard,ScottandSpellicy,Robert,PhD.,FTIRMonitoringinHighWaterandCarbonDioxideEnvironments.Presentedatthe2003AirandWasteManagementAssociation96thAnnualConferenceandExhibition,SanDiego,CA,June22-26,2003.Swiggard,ScottB.,ComparativestudyofNH3analysisandmethodsforSCRSlippage.PresentedatSourceEvaluationSocietyAnnualMeeting,KiawahIsland,NorthCarolina,2004Swiggard,ScottB.,IdentifyingIn-StackDetectionLimitsandHandlingofNon-DetectData,PresentedatSourceEvaluationSocietyAnnualMeeting,RohnertParkCalifornia,2005Swiggard,ScottB.,WhyCoolingTowersandVentsmatterinTexas!,PresentedatSourceEvaluationSocietyAnnualMeeting,HiltonHeadNorthCarolina,2006Swiggard,ScottB.,Howaccurateareyourstandards?,PresentedatSourceEvaluationSocietyAnnualMeeting,HiltonHeadNorthCarolina,2006Swiggard,ScottB.,BonnetteSidney,PhD.,andPalomarezJorge.,GasChromatography(GC)AnalysisofHAVOC'sinCoolingTowersandVents;includingdegradation1,3-ButadieneinthepresenceofNOxcompounds,PresentedattheGAS2006Conference,Galveston,Texas,April2006Swiggard,S.,McCulloch,R.StackTestingforDummies®.GoldenSpecialtyEdition.Indianapolis:WileyPublishing,2011.ProfessionalAffiliationsSourceEvaluationSociety(SES)-QSTII-IV#2006-025AirandWasteManagementAssociation(AWMA)SourceTestingAccreditationCouncil(STAC)-MemberandBoardofDirectorsASTMInternational,VotingMemberD22,#39569126of90KARENL.SWIGGARDAirQualityTestReportVICEPRESIDENTIDIRECTOROFQUALITYASSURANCEProfessionalWorkSummary•Broadbackgroundinsafety,environmentalcomplianceandregulatoryissues.HasmanagedprojectsassociatedwithHazardCommunication,Bloodbornepathogens,TuberculosisInfectionControl,RespiratoryProjection,PersonalProtectiveEquipment,LifeSafetyCode,FireSafety,ElectricalSafety,BackInjuryProtection,WorkplaceViolence,EmployeeInjuryandIllnessReporting,EmergencyResponse,HazardousDrugs,VentilationandIndoorAirQuality,andJointCommissiononAccreditationofHealthcareOrganizations(JCAHO).•ExtensivebackgroundinemployeeTraininginareasof:HazardCommunication,Bloodbornepathogens,TuberculosisInfectionControl,RespiratoryProjection,PersonalProtectiveEquipment,FireSafety,ElectricalSafety,BackInjuryPrevention,EmergencyResponse,andComputerErgonomics.•DevelopedandpresentedintensivetrainingcoursesforHealthandSafetyprofessionalsatallNASAcentersincluding:OccupationalErgonomicsandBloodbornePathogens.•WhileworkingforTexasWaterCommission(nowTexasCommissiononEnvironmentalQuality,TCEQ),shewasresponsiblefortheenforcementofRCRAprograminTexasincludingtheinspectionandevaluationofRCRAprogramsatvariouschemicalplantsandotherfacilitieshandlinghazardouswaste.Wasakeymemberforemergencyresponseforchemicalspillsandaccidents.•ExtensiveexperienceinQualityAssuranceprogramsincludingservingasQualityAssuranceOfficerfortheEnvironmentalHealthLaboratoryforNASA-JohnsonSpaceCenterfor5years,andmanagingtheenvironmentofcareaccreditationprocessofKelsey-Seybold,HoustonTexas,forJCAHOinwhichitwasawarded.WorkExperienceGoldenSpecialty,Inc.(February1999-present)Position:VicePresidentIDirectorofQualityAssuranceKelsey-SeyboldClinic(June1995-February1999)Position:ManagerofEnvironmentalHealthandSafetyNASA-JohnsonSpaceCenter(April1986-June1995)Position:Health&SafetyTrainingSpecialist/IndustrialHygienist/QualityAssuranceOfficerTexasWaterCommission(February1984-April1986)Position:EnvironmentalQualitySpecialistProfessionalAffiliationsSourceEvaluationSociety(SES)NationalEnvironmentalLaboratoryAccreditationCommission(NELAC)AirandWasteManagementAssociation(AWMA)AmericanIndustrialHygieneAssociation(AIHA)EducationStudiestowardsMastersinScienceinEnvironmentalScience,UniversityofHoustonBachelorofScienceinEnvironmentalManagement,UniversityofHouston,1984SourceSamplingandCEMSWorkshop,WalterSmith&Associates,2002NIOSHQualityAssuranceOfficerTraining,1990-AI27of90AirQualityTestReportRONALDB.McCULLOCH,M.S.,MBA,QSTIBUSINESSDEVELOPMENTMANAGER/DEPUTYTECHNICALDIRECTORProfessionalWorkSummary•ManagesoverallbusinessoperationsforGoldenSpecialtyoperationsoutsidetheU.S.GulfCoast•Accomplishedteamleaderwithatrackrecordofincreasingfinancialandoperationaleffectivenessbyapplyingsoundbusinessstrategyprinciplesandadiverseindustrialbackground.•Experiencebasespanscommerciallaboratory,stategovernmentandenvironmentalconsultingforcommercialandmanufacturingclients.•Corecompetenciesincludefinancialprojectmanagementandreporting,budgetmanagement,programdirection,strategicplanningandprocessimprovement.WorkExperienceGoldenSpecialty,Inc.(October2010-Present):BusinessDevelopmentManagerIDeputyTechnicalDirectorURSCorporation(July2000-October2010):AccountManagerISeniorScientistNorthCarolinaDivisionofAirQuality(December1994-July2000):QAAuditorILeadScientistCompuchemLaboratories(August1991-December1994):StaffChemistSelectedPublications/PresentationsRobarge,W.P.,Walker,J.T.,McCulloch,R.B.andMurray,G.2002.AtmosphericconcentrationsofammoniaandammoniumatanagriculturalsiteinthesoutheastUnitedStates.AtmosphericEnvironment.36:1661-1674.McCullochRB,ShendrikarAD.2000.Concurrentatmosphericammoniameasurementsusingcitric-acid-coateddiffusiondenudersandachemiluminescenceanalyzer.AtmosphericEnvironment34:4957-4958.McCulloch,R.B.,IManufactureWidgets;WhyShouldICareAboutAgriculturalEmissions?EM,August1999,27-28.McCulloch,R.B.,G.S.Few,G.C.Murray,andV.P.Aneja,1998,"Analysisofammonia,ammoniumaerosols,andacidgasesintheatmosphereatacommercialhogfarmineasternNorthCarolina,USA,"EnvironmentalPollution,Vol.102,pp.263-268.Swiggard,S.,McCulloch,R.StackTestingforDummies®.GoldenSpecialtyEdition.Indianapolis:WileyPublishing,2011.ProfessionalAffiliationsSourceEvaluationSociety(SES):QSTII-IV#2007-098AirandWasteManagementAssociation(A&WMA)EducationMasterofBusinessAdministration(MBA),ColoradoStateUniversity,FortCollins,Colorado,2009M.S.,AtmosphericScience,NorthCarolinaStateUniversity,Raleigh,NorthCarolina,1999B.S.,Chemistry,UniversityofCentralFlorida,Orlando,Florida,1991TotalQualityManagementEffectiveLeadership-NCPublicManagementProgramOSHA40-hrHealthandSafetyTrainingWin-WinNegotiationsSarbanes-OxleyComplianceRCRAHazardousWasteTrainingforManagersClientAccountManagersBootcampProfessional

W o rk Summary

28 of90 PAUL

J. CLARK, QSTI PROJECT MANA GER

Air Quality Test Report • Responsible

for planning

and managing sampling programs,
daily assignments

of field testing crews, sample analysis,
data reduction, QA/QC reviews,

and reporting activities. Services

and maintains instrumental analyzers. • Supervised and/or participated

in thousands

of source tests across
the Western United States and Alaska. • Sampling experience includes

trial burns
for

a Metal Parts Furnace (MPF), Liquid Incinerators
(LIC), and Deactivation Furnace System (DFS).

Mr. Clark has designed

and built

a continuous mercury monitoring system including

two analyzer based continuous monitors

and three Appendix

K systems. Some trial burns required supervision

of up to 25 testers

on site. • Participated

in several test aboard marine vessels,
both

at sea and dockside. • Managed

the largest mercury (Hg) project performed

by

a stack testing company

to date

in Oregon. Work Experience Golden Specialty,

Inc. (July 2011 ·Present) Position: Project Manager URS Corporation
(June 2010-July 2011) Position: Senior Project Manager- Measurement
Group TRC (September

2001 -July 2009) Position: Western Regional Manager -Air Measurement Division Emission Technologies

Inc. (August 2000- August 2001) Position: Stack Testing Division Manager Am Test LLC. (January
1995 -August 2000) Position: Senior

Air Quality Specialist Penberthy Electromelt International

Inc. (1990

- 1995) Position: Safety

& Regulatory Compliance Manager Airo Services,

Inc. (1987- 1990) Position: Project Manager US Navy (September

1980

- March 1987) Position: Chemistry-Radiological

Controls Division Professional Affiliations Source Evaluation Society (SES)

- QSTI HV #2008-229 Air and Waste Management Association (AWMA) Education Naval Nuclear Engineering School, 1982 OSHA 80-hr Hazardous Waste Training, 1993

& 2006 QSTI Certification, December
200829 of 90 STANLEY

B. MOV

E, Ql PROJECTSUPERW

SOR Professional

Work

S ummary

Air Quality Test Report • Responsible

for planning

and managing sampling programs,

daily assignments

of field testing crews, sample analysis,
data reduction, QA/QC reviews,

and reporting activities. • Supervised and/or participated

in thousands

of source tests across
the Western United States and Alaska. • Sampling experience includes almost
the entire gamut

of EPA wet and instrumental

test methods

as well
as several toxic organic (TO) methods

and solid waste (SW-846) methods

to quantify hazardous

air pollutants (HAPS). • Experienced

in the maintenance

of in-house continuous emissions monitoring systems (CEMS), performed particulate matter (PM) and total reduced sulfur (TRS) testing
and analysis,

as well
as data reduction

and report generation. • Conducted testing with respect

to wet and dry Kraft recovery precipitators

and hog fuel boiler precipitators, and performed quality assurance procedures

of ITT Barton total reduced sulfur instruments,

as well
as the maintenance

and repair

of NCG system. Work Experience Golden Specialty,

Inc. (October 2009

- Present) Position: Project Supervisor Am Test Air Quality (July 1992

- October 2009) Position

: Senior

Air Quality Specialist/Chemist Simpson Tacoma Kraft Paper and Pulp Mill (February 1977- July 1992) Position:
Shift Chemist; Waste Water Operator; QA/QC

for Paper and Pulp, Waste Water and Air Quality Professional Affiliations Source Evaluation Society (SES)

- Ql Groups

1-111 Education Coursework completed towards B.S., Mathematics, Chemistry, Central Washington University Course 450- Source Testing

for Particulate Matter (August 1992) Continuous Emission Monitoring Systems (CEMS) WorKshop, taught

by Mr. James Jahnke (April1993) CSTOP Training,
WAliOL.DENProfessionalWorkSummary30of90PETERHILTY,QlPROJECTSUPERWSORAirQualityTestReport•Directed,supervisedandscheduledandprovidedstacktestingasrequiredfornearly119permittedairsources.•MaintainedandcalibratedambientPSDmonitors.•Trainednewemployeestoinsurecompliancewithair,water,andRCRApermits.•AsRadiationSafetyOfficer,insuredproperoperationofradiologicalmonitoringsystems,performedsurveysforsuspectedradioactivescrap,andtrainedemployeesonpersonalexposurerisks.•Performedrequiredoperationalchecksandleakagechecksofsealedsources.•Reviewedandinterpretedregulationsforvariousairprograms(Part40,Part63,Part70,andPart75)todeterminetestingrequirements,appropriatetestmethods,andreportingrequirements.•Compiled,reviewedandrevisedtechnicalenvironmentalreportsandensuredcompliancewithappropriateStateandFederalrequirements.•CoordinatedtestingandsecuredapprovaloftestprotocolsfromStateandFederalAgencies(KDEP,OEPA,USEPA)WorkExperienceGoldenSpecialty,Inc.(April2011-present)Position:ProjectSupervisorIndependentEnvironmentalContractor(2008-2011)NorthAmericanStainless(2007-2008)Position:EnvironmentalTechnicianFBT,Inc.(1996-2007)Position:Director,EnvironmentalServicesUnitedStatesArmy(1987-1991);ArmyReserve(1991-1999)Position:AvionicsICommunications-ElectronicsRepairEducationUniversityParallelEngineeringCoursesSinclairCollege,Dayton,OhioCertificationsQl,GroupsI,IllandIVNRCcertifiedRadiationSafetyOfficer(RSO)31of90AirQualityTestReportPAULAM.METZ,QSTIREPORTSDEPARTMENTMANAGERProfessionalWorkSummary•ExperiencewithEPAtestingregulations,including40CFR,Part60,Part75,andPart266,andTCEQtestingregulations,including30TAC115,30TAC117,andTCEQSamplingProceduresManual.•Over6yearsofexperienceandparticipationinover500testsinTexas,Arkansas,Ohio,Mississippi,SouthDakota,Iowa,Kansas,andLouisiana.•CEMinstrumentationprojectsincludecontinuousanalysisforcarbonmonoxide(CO),totaloxidesofnitrogen(NOx).oxygen(02),carbondioxide(C02),totalhydrocarbons(THC),andsulfurdioxide(S02).•Samplingexperienceincludesflowstreamcharacterizationandmonitoringofanumberoftypesofflowstreamsforengineeringpurposes;includinganalysisusing3-DsphericalprobesperMethod2F,emissionssamplingforregulatorycompliancedemonstration;emissionssamplingforsystemsauditrequirementsofcontinuousemissionmonitoringsystems(CEMS).•ConductedisokineticsamplingandcalculationsforMethods1,1A,2,2A,2F,3,3B,4,and5,includingsamplerecovery,preservation,andstorageatthetestsitewithassociatesamplecustodyrequirementsforthemethodslisted.•KnowledgeableinthetestingrequirementsandproceduresforthetestingandanalysisofPredictiveEmissionsMonitoringSystems(PEMS).Participatedinseveralnewsourceperformancestandards(NSPS)fordevelopmentofnewPEMS,includinginitialdatacollectionofemissions.•ExperiencedinmodifiedElPasoMethod,AppendixP,(CoolingTowerSamplingforVolatileOrganicCompounds);applicabletomonthlysamplingandtroubleshootingleaksinProcesssystems.•Experiencedinreportwriting,review,andfinishedproduct.WorkExperienceGoldenSpecialty,Inc.(February2001-Present)Position:ReportsDepartmentManagerProfessionalAffiliationsSourceEvaluationSociety(SES)-QSTII-1112006-026EducationAssociateofArts-Chemistry,SanJacintoCommunityCollege,December2010VisibleEmissionsCertified(EPAMethod9),2004-200712HourBasicInstrumentationTraining,CaliforniaAnalyticalInstruments,January2003SourceSamplingandCEMSWorkshop,WalterSmith&Associates,2002,2003and2004PreparationfortheSESQSTIExamWorkshop,WalterSmithandAssociates,2005SkiiiPath®Seminars,EmployeeManagementandSupervisionWorkshop,2003HazardousMaterialsShippingQualified,2006Man-LiftTraining,August2006FredPryor®:TeamBuildingSeminar,2007FredPryor®:Excel:BeyondtheBasics"Seminar,2007QualifiedIndividual-CylinderGasAuditsQualifiedIndividual-EPAMethod30BQualifiedIndividual-PortableCombustionAnalyzerGOLDENI32of90AirQualityTestReportBARBARAL.SCHMElTZRECORDSCOMPLIANCEANALYSTProfessionalExperienceSummary•Proficientinoperatingandmaintainingambientairqualitysamplingequipment.•Proficientincollection,processingandanalysisofmeteorologicalandchemistrydata.Speciesincludecarbonmonoxide(CO),totaloxidesofnitrogen(NO.),oxygen(02),carbondioxide(C02),andsulfurdioxide(S02)·•Proficientinmaintaining,preparingandlaunchingofmeteorological,ozone(03),andsulfurdioxide(S02)samplingequipment.•Responsiblefordocumentingandmaintainingthetrackingofprojectdataandtestreports.•IntrainingfordataimportationforPEMSandCEMSRATAs,aswellasmultiplecompliancetestprojects.•Intrainingforreportwriting,reviewandfinishedproduct.•ProficientinMicrosoftWord,Excel,PowerPointandAccess.•ProficientinEsriGISsoftwareArcMAP,ArcGISandArcView.•ExperiencedinWaveMetricsscientificgraphing,dataanalysis,imageprocessingandprogrammingsoftwareIGOR.•ExperiencedinC++andMATLABprogramming•FluentinDutchandEnglish,experiencedinGermanandFrench.WorkExperienceGoldenSpecialty,Inc.(February2011-Present)Position:RecordsComplianceAnalystUniversityofHouston,IMAQS-InstituteforMulti-DimensionalAirQualityStudies(January2009-February2011)Position:ResearchTechnicianC.Hecht&Co.(Netherlands)(November2002-November2004)Position:Sales&ProductionCoordinatorGrafico(Netherlands)(October2000-October2002)Position:Sales&ProductionCoordinatorGrafico(Netherlands)(August1997-October2000)Position:EngraverEducationBachelorsofScience-EnvironmentalScience,EnvironmentalSystems&Modeling,UniversityofHouston,May2010AssociatesofScience-EngineeringIEnvironmentalScience,HoustonCommunityCollege,August2007EN33of90AirQualityTestReportIDANIELD.FARWELLENVIRONMENTALTECHNIC/CANProfessionalWorkSummary•Intrainingforinstrumentationmethods:carbonmonoxide(CO),totaloxidesofnitrogen(NO.),oxygen(02),andcarbondioxide(C02).•IntrainingofEPAtestingregulations,including40CFRPart60andPart75.•Intrainingforsourcecompliancetestingandemissionsamplingmethodologiesforstackgasvelocity,moisture,andavarietyofisokinetic(wetchemistry/particulate)testing.•Intrainingforperformingmaintenanceandcalibrationsonavarietyofairtestingequipment.•Computerskillsinclude:Windows9x,Windows2000,Excel,WordandAccess.WorkExperienceGoldenSpecialty,Inc.(April2008-present)Position:EnvironmentalTechnicianEducation8-hrCSTOPTraining,WA,2008BasicPlusTrainingliOLDEN34of90AirQualityTestReportAPPENDIXCCalibrationDataFORM#GSC-TM003-002REV2010-01,EFF11/1/1035of90P£TOTTUBEINSPECTfONDATASHEETCompe:nyName:Pre-sc?.mplePostSampleDateC.-Vf-ZotlDatev>rrYe..,;,l?2._£,1NOobstructions?/Vt7J./vda1:1aged?#cJ0-10°<Cl)<+100<3I0-10°<\)2<+10°C)I0-50<gl<+50C)0-5"<Bz<+500M:,tcIt•e•t••U•ll•l'ltl,,.lOt"·1•1•Cl.l&.a:!nC,I.00••••,.....c__,•••::!oo•;•:r,........··-:11·;;;..,::;.-·-·'-·Co[ffilents:u;•u...,...,,.un:c.•n••...••Kt1.-..•a4•I_..Ifuo.9t.foo_'·noC)•'-110XX'(Xy8C/Ao.C\4o1.OSDt<Pa<1.5DtIo.l...\161.OSDt<pb<1.5Dt0ffi03/16"'"'<::Dt'<3/8"xAtany<0.125")(AtanE<0.03125"X-Pa=Pb±0.063"vPitottube/probenumberfe-003;l'y.}meetsorexceedsall,specificationscriteriaand/orapplicabedesignfeatures*andisherebyassignedapitottubecalibrationfactorof0.84.Signature!:>ate&.-2?-Z..or/•see4GCFRr.o,Vol.4Z,Ho.160,Z.themin;...,,.Rev:-A-:266tZinchStlbickofthelhenooc011Plelndthtmini....,)/4inchsepar-•tionbttwnnthepitottubelftdlhenoulcushownHthetopofthisPI9C.

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# -- Aal>ient Tecparature

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••••••••••••••••••••••••••••••••••••••••••••••••••• •tsULTS •·•••••••••••••••••••-•••••••••••••••••••••••••••••



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--



# VOLUME VOW<E 

# VOLUME VOLU>!I VOL'-"! I 

# Co\LIBilATION nCTOR


# CORRECTED 

# COIU<EC'rED COIUtl'CTED 

# CORU'CT!D 

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# Value
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# tolerance of indivictu.l value• ha.

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# Box Units. English 

# K' Factor

Version 2 3

Model #: 

# C-5000 Serial 

# # 1696 Date

· ---------> Barometric Pressure: ---> 07/01/11 Annual Factor of 

# Dry Gas Meter 

# I 1.o43 

# I 30.10 (m. 

# Hg)

IMPORTANT: Select the Post-Test orif1ce serial number that closely assimilates measured

**~H** 

# during the last test

.

----DRY GAS METER READINGS---- ..CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. OrifiCe 

# K' Orifice Actual -Ambient TemperaturedH Time Initial Final Total Inlet Outlet Inlet OuUet (in H20) (min) (cult) (cult) (cull) (deg F) (deg F) (deg F) (deg F)
0.28 32

. 00 512.359 521.976 9.617 70.0 70.0 72.0 71.0
0.28 36.00 521.976 532.731 10755 72.0 71.0 75

. 0 74.0 0.28 50.00 532

. 731 547.702 14.971 75.0 74.0 77.0 77

. 0

1 I..

.. ... • 

# ----RESULTS

--- • •

.... • •

- DRY GAS METERVOLUME VOLUME ;ORRECTECORRECTED Vm(std) Vm(std)

(CU 

# II) (liters) 9.627 272.6 10 721 303.6 14 847 420.5 ---ORIFICE--

VOLUME VOLUME CORRECTECORRECTE[

Vcr(std) Vcr(std) (cu Ill (liters) 9952 2819 11

. 175 3165 15 492 438 7 VOLUME NOMINAL

Vcr (cull) 9.953 11 218 15

. 610 - DRY GAS METER

--

CALIBRATION FACTOR y 

# Value (number) 1.034 1.042 1043 Vanation (number) -0.006 0.003 0004 Serial# Coefficient Vacuum Initial (number) (see above) (in Hg) (deg F) XF44 XF44 XF44 0.2381 24.0 69.0 0.2381 24

. 0 73

. 0 

# 0.2381 24.0 73.0

--ORIFICE--

CALIBRATION FACTOR dH@ Value (in H20) 1.630 1.630 1.627 Value Variation (mm H20) (in H20) 41

. 41 0.001 41.41 o.oot 41.33 -0.002 Final (deg 

# F) 73.0 73

. 0 77.0

Average Y --> 

# 1

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# 38 <--Average dH@

Note: DGM Calibration Factor must not deviate more than

SIGNED:_ S 

# Moye 

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# I% Error

O/ 

# E ( y """"'""

- 

# Y,,;fic.) I 0 -,o 

# rror= x 

# Y,,!ftc•

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# Date: 7/1/2011 Average (deg 

# F)

71.0 73.0 75.0



# w (X) 

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# muabe-01 English oris, 

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# mnm•

--- DRI'GAS METER READINGS---
--- CAI1'1CAI.OAIFICE R£.-o o NGS

---



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**------------------~n-----------------**

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# --ORIFICE--



# IIOI.UME IIOI.UME VOWME 

# IIOWMI: IIOWME 

# CORRECTEO 

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# COARECTBI NOMINAL

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# (did)

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# 5.2811 148

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# 5.288
5.3518 152.8 5.4Sl 

# 154

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# 5.483 1547 

# 5.482 155.5 

# 5.419 

# 8.544 115.3 

# uoo 111.9 

# 8.8011
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# 5

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# 5.411



# -

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CALIIRATION FACJOA


# v 

# - lnumborl
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# 1

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# 1.003 

# -.g.v-•D¥:1 

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# 0

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# .(1.002 

# 0

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# w

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# z~A:£~ llt!f!!
Value 

# r

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# I.S51 

# 1

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# ·- --.g&T-- 

# DGM DGM 

# - Outlol Ooerll 

# T- ('A) I"R) 

# ("II)


# 527$ 

# 528.0 

# 528.0 528.5 528.1 lllll.5 

# 5211.0 

# 5211

. 3 5:!9

. 0 5211

. 0 529.$ 

# 5:!9.0 530

. 0 Sl0.8 

# 5211

. 0

--ORIFICE---



# CAUBRAnON FACTOR

lloluo 

# - -/Fol (INn 

# H20) 

# r"H20l 

# m

- .0.070 

# 38

. 44 

# .0

. 0811 42.17 0.011 41.84 0.11011 45.04 0

. 131 

# I 41.10



# 0.0.: 

# 9- 

# 3- '2.-o/o

DeorPooi<.T- (..) 

# co 0


# - co 0

# EPA Method 5 Meter Box Calibration Post- Test OrifiCe Method English Meter Box Units, English K' Factor

Version: 2.3

Model #' 

# C-5000 Serial 

# # 1729 

# Date:- 

# ·-----> 07/01/11 Annual Factor of 

# Dry Gas Meter 

# I 1. 

# oo1 

# I Barometric Pressure: 

# ---> 30.10 

# (in.Hg)

IMPORTANT: Select the Post-Test orifice serial num b er that c l ose l y assimilates measured 6H during the last test.



# ------DRY GAS METER READINGS--- -CRITICAL ORIFICE READINGSVOlume Volume Volume Initial Temps. Final Temps OrifiCE! 

# K' Orifice 

# Actual -Ambient TemperaturedH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial (in H20) (min) (cu It) 

# (cull) (cu Ill (deg 

# F) (deg F) (deg F) (deg F) (number) (see 

# above) (in Hg) (deg 

# F)

1.10 10.00 638.598 645.210 

# 6.612 67.0 67.0 69.0 68.0 XF44 0.4665 22.0 69.0

1.10 10.00 645.210 651.826 

# 6.616 70.0 68.0 71.0 69

. 0 XF44 0

. 4665 22.0 72.0

1.10 11.00 651.826 657

. 526 

# 5.700 71.0 69.0 73.0 71.0 XF44 0.4665 22.0 72

. 0



# -·-- RESULTS- ---

- DRY GAS METER- -----ORIFICE----

VOLUME VOLUME VOLUME VOLUME :ORRECTEGORRECTED CORRECTECORRECTEl Vm(std) Vm(std) Vcr(std) Vcr(std)

(cu It)

**~iters)** 

# (cu ft) 

# (liters) 6.670 188

. 9 6.102 172.8 6.652 188.4 6.088 172.4 5 715 161.8 6703 1898 VOLUME NOMINAL

Vcr (cull) 6.085 6.100 6.703 - DRY GAS METER

-
CALIBRATION FACTOR y 

# Value (number) 0.915 0.915 1173 Variation (number) 

# -0.086 -0.086 0

. 172 --ORIFICE--

CALIBRATION FACTOR dH@ Value (in H20) 1.673 1.678 1.670 Value Variation (mm 

# H20) (in H20) 42.50 -0.001 42 62 0.004 42.42 -0.004 Final (deg 

# F) 70.0 72.0 70

. 0



# Average Y ---> 

# 1.001 1.674 42 51 <--Average dH@

Note: DGM Calibration Factor must not deviate more than



# SIGNED:_ S Moye IQ.60%

**l~t** 

# Error

0/ 

# E

**(Y,..,a~-** Y,,fi"') 10 "/o 

# rror= x 

# Y.,..,fiu

**5'.~----~-----~-~**



# Date: 711/2011 Average (deg F)

69.5 72.0 71.0

**~** 

# 0 0


# - co 0

# 41 of 

# 90 

# EMISSION RATE CALCULATIONS FACILITY

: 

# Al tp(.&.



# l"" 

# \.J c..o **l.Ut>.A~** CITY, STATE: 

# ~~

I 

# Will SOURCENAME:



# &b. £N..eM., **~~** DATE

:



# (,l 'ZA\ **~**
l \

RUN NO.

:. ___ 

# ___;__-.-.L;ij(..;.;5::..;1~~- MOISTURE



# (~,)

= __ 

# _.Q._

• **..;:.O_~.:...Q....;~'-----**

(See Moisture Sample Data) GAS ANALYSIS:

% 

# cq_..:..\

_. 

# S __

% 

# ~

%CO __

. __

_ MOLECULAR WEIGHT,



## dry basis ('4) 

## g/g mole

: Md

= (0.440

x **%C~)**



## + (0.320

x **%~)**



## + (0.28

X **(%~**



## + %CO)) Md= (0.440

x 

# \.~

) + (0.320

x 

# \$.S"

) + (0.28

x

( 

## g'l).O

+ ___

))
= 

# ~~.q~D M,

= Md

(1

- B.,.,)

+ 

## (18.0

x 

## 8,.,) M.

= 

# u,.'ltlo

(1

- 

# o.O'f5S

> 

### + 

## (18.o

x 

# o. 

# ~~

> 

## = 

# zgA3c.,S"



# .v" VELOCITY TRAVERSE DATA: AVG.f

t:.P = \

• \"' ..;' 

# ~AVG.= 

# \,11.3 •RP.= 

# 1fi.(,fj STACK DIAMETER= __ -6.%..,..!.({_.



## 0 ____

f.,= __ 

# ....;3.:...i~.'\»._.CS..__ 

# ___

**~** = 

# 1--~

· 

# '4-3<,-~ CALCULATIONS:

v,
= 85.49

X 

## Cp
X AVG

. 

# ..;;p-

X .J{T, AVG./

( 

# M. X P,))

= ACFM

= 

## V. X 60

X 

# 1\
= Q,d=(1.00-B.,.,)

X ACFM

X **(528/~AVG.)**



## X (P,/29.92)= ISOKINETIC DATA:

(If 

## applicable) Vm(std)



## = 

# \~'?>



# · '!) 

# 5S NOZZLE
DIA.

= 

# O·l



# 'i \ PERCENT ISOKINETIC



# = o.09450



# x
T,


# x vm(std)

= 

# q;.13

./ 

## P,
X V,
X 

# 1\.
X


# 8 X (1-S,..)

# 42 of 

# 90 

# /~/

....J



# II.. ::l"'tJ 

# ·· 

# ~)SPECIALTY PROJECT: 

# M@: \nk\ca \.9cw" 

# ~ 

# /t3@.. <6Kn. **~(.** PROJECT

NO.: 

# tJVJll 

# A£..I.tJT\oq Equations:

I 

### USEPA Method
315 Spreadsheet Calculation Quality Assurance POMIMCEM USEPA (Front half Catch) grldscf



## = (Residual Probe Wash Weight

+ Residual Filter Weight,

in g)
x 15.43 grlg IV m(std)



### in dscf lblhr



## = (grainsldscf

x Volumetric

Flow Rate, Qsd



### in dscflhr) 17000 grllb POMIMCEM grldscf



## = (Residual
Filter Weight+ Residual Weight

of Containers

2, 2M, 3W, and 35,

in g)
x 15

. 43 grlg IV m(std)



### in dscf lblhr



## = (grldscf

x Volumetric

Flow Rate, Oad



### in dscflhr)



### I 7000 gr/lb Example: Source: 

# ~~ **~ ~**  **~** Run No.:

\ USEPA (Front half 

# Catch~

((). 

# o·~•L

D 

# ·OOOO: grldscf



## =

...,l 

## ~.:=--:--v-'--<7""1.;__-t_-:-;....:...;~'_J.~_,)C-'--_.\-=S;....;._~...:.;3,..__



# I'&
'1

. S'5'S lblhr



## = POMIMCEM



# fl\;)


# < grldscf



## = lblhr



## = **O.Q>Q~**



## X



# 1

1 

# 50t,33S.

IrS' (,000 

# O.QQQ'i4

**~** 

# 11 '50\, 

# '33S. ¥'5 

# \ i>3 .55'5'



# - ..

::

;: 

# o.ooot.ts ;::. 

# Q. 

# ooo 

# 'fZ:!:.

o...- Calc QA 

### Perfonned

by 

# ?- :z/.ul£1

## 43 of 90 

# EMISSION RATE CALCULATIONS FACILITY 

# :_-~..A



# ........ **l!L:C«A:%..:---i~~~~:..,_~IM=..;.;..LS** ________

_ CITY, STATE: 

# f~~

1 

# tV~ SOURCE NAME:


# &Ju. **~ ~ata**  **~** DATE: 

# c,('ll11h

RUN NO.

: __ 

# .._I_-.....:U...:..:.......1:...1.f_-4....;..0_1~51:\~ MOISTURE



# (~.)

= __ --...JoC;Q.....;. 

## 0=:..3::;..9.;;...')" __

_ (See Moisture Sample Data) GAS ANALYSIS:

% 

# cq \.SO

%CO ___

_ MOLECULAR WEIGHT,

dry basis 

## (1'4) g/g mole

: Md

= (0.440

X 

### %C~)



### + 

## (0.320

X 

## %0.!)

+ 

## (0.28

X 

### (%~



### + 

## %CO)) Md= (0.440



# x t,<;

) + (0.320



# x



# K

.. **~**



# ) + (0.28 

# x ( ,.()

+ ___

))
= 

## =z.tR~o M, 

# = Md

(1

- 

## S.,.)

+ (18

. 0 

# x E\.s) 

## M, 

# = ze.qso

(1

- 

## o.o3ff

) + 

## (18.0

X 

## 0·03S]'

) 

# = Z.f. S'7oz

""' VELOCITY TRAVERSE DATA: AVG.f



# 6P 

# = \ 

# .(1q
l;AVG

. = 

# (,JjoJ

•R 

# P.= 

# 2'1°1-'1 STACK DIAMETER



## = ___ 

# <l~~,_.O 

# ___

f-.= 

# _.........;:;3....:..7_·

'fCi_;.;;_ ____



# ~ = 

## 2.<(

o 

# 910Z.. CALCULATIONS:

v
5 

## =85.49

X 

# Cp
X AVG. 

# ~X ./(T,AVG

. /(M.XP,))=



# 1~ **17**



# v ACFM



## = V. X 60

X 

## A,.= Qsd 

## = ( 1.00- 

## 8,,)

X ACFM
X ( 528 

# I~ AVG. ) X (

P, /29.92) = ( 

# '2Jo,<rz.

... C,

o 

# .PJ

./ ISOKINEllC DATA:

(If applicable)

I

_{

?- 

## NOZZLE
DIA.

= 

# _.....;0::....;...,

0 

# lu..l **~-=----**

**~=**

1p 

# A(.'#

JC 

# \0 8= __ 

# .;;)V;::;..;;..:l>.___ PERCENT ISOKINETIC



## = 0.09450

X
T,

X Vml•ldl



## = P,
X V,
X 

# An
X 

## 0 X (1-E\.s)

Calc QA Perfonned

by 

# &< d11e{t44of90Facility:Source:TestDate:TotalFluorideCalculationQAFlowDataDateSampleVolume(Vm(otdJ:---=.2'"::'....,Qt51......,....______dscmVolumetricFlowRate(Q.J:\'301Ol'i,CjdscfmCt(V\lllParticulateFluoride(Filter)AnalysisandCalculationsParticulateFluorideTotal(1)(2)ManPM,FluoridePM,FluorideRunPM1FluorideCone.Cone.No.BlankConectad(malma/dscmppmvd(1)PM1Fluondemg/dscm=M101(mg)IVm(s"'l(dscm)(2)PM,Fluondeppm=PM,Fluoride{mg/dscm)x22.414118.998x293.151273.15(3)PM1Fluoridelblhr=PM1Fluoride(mg/dscm)135.31xa...1453,600x60(3)PM,FluorideEmis.RatalblhrParticulateFluoride(Front-HalfRinse)AnalysisandCalculatlonsk'ParticulateFluorideTotal(4)(5)MassPM,FluoridePM,FluorideRunPM,FluorideCone.Cone.No.BlankCorrected(malma/dscmppmvd\vvO·Ol01().Ol35"(4)PM,Fluoridemg/dscm=M101(mg)IVrn(S1dl(dscm)(5)PM,Fluorideppm=PM,Fluoride{mg/dscm)x22.414118.998x293.151273.15(6)PM,Fluoridelblhr=PM,Fluoride{mg/dscm)135.31xa...1453,600x60GaseousFluorideAnalysisandCalculationsGaseousFluorideTotal(7)(8)MassGasFluorideGasFluorideRunGaaFluorideCone.Cone.No.BlankCorrectad(mg)mgldscmPDmvdlo.\v,;().Ob:l-"Z..O·O"l<li(7)GasFluoridemg/dscm=M101(mg)IVm(..,l(dscm)(8)GasFluorideppm=GasFluoride(mg/dscm)x22.414118.998x293.151273.15(9)GasFluoridelb/hr=GasFluoride(mg/dscm)135.31Xa...1453,600X60!TotalFluorideCalculationsProcessData(10)(11)TotalFluorideTotalFluorideRunOperatingHoursEmis.RateEmls.RateNo.hourslblhrtonalvr(tJIA-v(10)TotalFluoridelblhr=PM,Fluoride+PM,Fluoride+GasFluoride(11)TotalFluoridetons/yr=(TotalFluoride(lblhr)xOperatingHours)12,000lblton(6)PM,FluorideEmis.Ratelblhr..o.oo52.(9)GasFluorideEmis.RatelblhrvO·'t>'303%......TimetS":1,.(CalcQAPerformedby"'SPECIALTY45of90AirQualityTestReportAPPENDIXDFieldDataUncontrolled

Valid Only

@ Time

of Print Refer

to Master

on Network Client/Plant
Name 1/LCoA P.//-A-1

('c46 of90 FIELD DATA SHEET

1 Sampling Velocity Traverse Points Job#

FORM# GSC-TM002·001 REV 2010-01,

EFF ll/1/10 City/State **----<-h__;_""'..;..:.v--=:..ob~'l+u/._,e**
___ **(.M.;__~'-------** Date/Time **--~=:...._-_Z..__:?_-_-z.._o_** _______

_ Test Location

B1y Ov&V
**&.~ 1~-s** 

.._ 5Tflc-l<-- Personnel

_ **_..:.'3:..!:tf{;::.:':.......,...:...........:f'~H_.,.....!.:.,7....:C:.......__:..12~;::.------** Port I.D. Distance from Fall Wall
to Outside

of Port

90 Nipple Length and/or Wall Thickness

" Stack/Duct

( J) Blue Print

(

) Measured

( ) Depth/Diameter

( >12 in.?)

?'f Width

(if rectangular) Equiv. Diamter

(if rect.) De=

2 DW/(D+W) Area (A)

( >1131n.

2 ?) A=

n D2/4
or D W

554/-1:f I>

b Distance

De

No. Pts* Updstream

( > 2 Dz?)

t4S.sff-

(1._ Downstream

(?. O.S De?)

)114#

**I~** Cyclonic Flow Checked?

Yes

No

NA Rectangular Matrix **~--------------------** *Circle larger

of two

Pt. %Duct

Dlst from Depth Inside Wall* 1 J.l.
l.b'l 2 ;o.)
**Y-~'** 3 **~~--~**

'(,_j

0 4 Jt.3 1.."\.13 5

t. 7.7 5<o.R1 6 !oC. G,l.)l.l 7 5'15

1 J,f
g 8 **1'-~ ~~.~'**  9 10 11 12 13 14 15 16 17 18 19 20 •oo not place closer

to stack walls than: 1.0 in. for stack dia

> 24 in. 0.5 in. for stack dia 12 **to~** 24 in.

Dist from Oustide

of Port **_8~9 I'-\-.~** 

1. 1 '-.3o ) 3.\) 6'2..81 rl.1o **~I.\~ ~l.')** 

I Sketch

of Location:

In the space above, sketch

a flow diagram

of the test location; show the distance from the ports

to the distrubances before

& after. Sketch the cross-sectional

area; show sampling
port locations.

In honzontal ducts, check
for dust buildups

& measure

or estimate

the depth. OA/QCCheck Completeness

Accuracy____::::"" Specifications
__ **~Reasonableness**

__

- Checked

by: **-~b"~~'-1--~......=./).;...Pf"__**

**~** Team Leader (Signature/Date)**-~** .......
_

} 1: **~ruu.rv** l

: acilit) **~lc.o** Location: **~...-.vdA(e...**

t..vATeq

'I cam:

}l u.J Page

of

l'(lllll I ;1 \' CIIII

47 of90 Unit: **~ke** OVeN Test No:

I Date:

(,- Z."J

- l.O

I I I ,·st Sullllll:tl'): Nott·s:

315 Method

) Source

' I t.:\l Dct

1 :-,hct.:l l'rt·-tcst **~-0"**

{ Port cha11gc

- chn11
(L. ct'nt

11

-

r'

I nit Purl change

- ct'111

11 ....-

I nil.

- Post Test ji. oo

1 cfm

11

( l.''

I nil. Pitntl.t·nt.. Ch.:cl..

: 1'1c t.-- Po,t **~**

# 48 of 90 

# r/

"JEIW 

# / 

# ~)SPECIALTY Facility: ItVf,.{c_

'-' 

# Test No:

Date:

(., -'2..."\-
-z..o;o

1



# I 

# Imp_
Til!_ Style Volume 

# I Modified

IOOmL 2



# GIS
IOOmL 3 

# Modified

Empty 4 

# Modified



# -200

g 5 

# 6 V

_ Vm



# * Y


# * 5 

# 28



# * [Pbar



# + 

# &l m(std)

- (Tm



# + 460)



# * 29.92 Vw(std)



# = 0.04706



# * (Vr-
Vi) Vw(std)



# = 0.04715



# * (Wr- Wi) 

# B _ ( Vw(sttl)

) ws

- Vw(std)



# + Vm(std) 

# %Moisture=

100



# * Bws



# Contents 

# Dl Water Dl Water Empty Silica Gel 

# Md


# = 0.440(%C0

2 ) 

# + 0.320(%0

2 ) 

# + 0.280(%N

2 

# +%CO) 60



# * (1

- Bws)



# * v 5 

# * A
5 

# * 528



# * P 5 

# Oscfm



# =

(T

5 

# + 460)



# * 29.92 . .

(T

5 

# + 460)



# * Vm(std)



# * 29.92



# * 100



# * 144 % 

# lsokmetzc



# =

rr 

# 528



# * V 5 

# * () 

# * P 5 

# * 60



# * (1

- Bws)



# * **D~**



# * 

# 4

Page_of_ ;'" 

# Method:~



# 3

I '::1 Post



# Pre 

# q 

# 3 .f. 

# 3 -??.7 **·J~J.L**



# J'-.•1.

**~-** (o'fl.t'>

(, 

# ~~'

I 

# '1 __t-t


# 'B

. .;


# So :..t.) 

# As ------Stack

area (ftz) Bws 

# ----Gas moisture (fractional) 

# Cp ------Pi

**to~** 

# correction factor 

# Du -----Nozzle diamter (inches)

Net 

# (&4'5".1 

# _g_s 

# £.i.q '-\H

GJ 

# '}.0]_.~ 

# Md -----Dry molecular weight (lb/lb-mole) M,. -----Wet molecular weight (lb/lb-mole) PbJr 

# ----Barometric Pressure (inches
Hg) P 8 

# ------Stack static pressure (inches water) P s 

# ------Stack Pressure (inches

of Hg) 8 ------Sample

time (minutes) V; ------Initial impinger volume (ml) Vr 

# ------Final impinger volume (ml) V m 

# -----Dry

gas meter volume
(ft3) Vs 

# ------Stack

gas velocity (ft/s) V w(std;-- 

# Meter volume

at STP W; -----Initial impinger weight (grams) W



# r -----Final impinger weight (grams) Y 

# ------Dry

**~as** 

# meter correction factor 

# Ps



# Oz COz

Nz 

# co

As 

# Ts

Tm 6P.,.



# Vm Vm(.<td

Bws %Moisture

Md M,.

Vs 

# Qsdm

Qacfm % lsokinetic.......·SY........2Ai"'l"'!J.t:vi!iFacility:_rA.J\-:o..\Tl:slTl'<Hn:tJc.VPageor•loj-.__.'.-'',Point49of90Unit:.9TestNo:L..t.."ill·stSummar):Nllll"S;315'-5Shl'l'tl're-te>lC>.C/OG;,c1"11111(""L.Init.l'nrtchange_.cfm11-Init.-Pnrtchangt--dn1:a-Init.-PostTesto.txRermIIt()Inti.GJ!-PitotLeal..C'hed.Pre.___.·r--·-------------------·-.·:;:----,,-1-r:>.kt.-1.-·tlltn'"'t'1\ktc·r---,...-1\'nlullll'St:•l·l-l'l\\lk'ChenI\IIl.\.1!InC)ut',ll.1...1ft.J.li__UJ.._·..-·--1:_'1£---IA11...z48-':J--,I(_:].J_""2..__-·-1-·k.-r.oJ3)21l__Q._Jo_____]_'2.,.__L_i..1.,11.£roI.-b.s__-=-:.r-lil-!__,ol'--_zf---\:7P.:.Q.._1_.\!..1.'?'"__kl::t.<)1o.Iv:s1s..L.1.______u_::J.._7JL.l.-1(qzg_fJJ:YJ.:Ql__3_-z..!.:)__lJg__LI'L!I!J.5__i____1____._______tx,__-__Jo.1.·l__!_J.t.J!:l_'__tJ..k11-:':L]'1o___2.l&___'l.{o__-__iL__(___jL')j_-_L_)_]____1_1]__ltt_S_--=-_0Y-___{_\·!J\..._11.o.___-__.4S_______7...___L..!&.__lw____L___...._l_L(.go___2\8}N.__UC,-__!,j__L_____t(_jz.25.a..___]__1]_,_l(u_r-1.51-r--:-__(,.]___1.__-__"1.t8..__li'1--__1__z._____'J;:L](.,l,.)..J_J_Q__...:.lt3_!__Q_:\1."Lt]___1\(,J(_(\__c-____!_L:zJIJ____1.<;\---t.)10.----___··--r--------------------·---··-r-----------·--1---t------

# ~ **~\** GUL./JJIEN 

# · **~JSPECIA**

**TY** Facility: 

# .T~cu

50 of 

# 90

Page_of_ Test No:



# 7- __ ____c....::::;_ __

_ 

# Date:

_ 

# __;:_'-_-_z._f.._-_,_1 ___

_ Method:



# ~

3

1 

# 5' Imp_

Tip Style Volume I 

# Modified



# IOOmL 2

G/S



# 100 mL 3 Modified

Empty 4 

# Modified



# -200g 5 

# 6

Vm



# * Y 

# * 528



# * [Pbar 

# +&] Vm(std)



# = (Tm



# + 460)



# * 29.92 Vw(std)



# = 0.04706



# * (Vr-
Vi) Vw(std)



# = 0.04715

• (Wr- Wi) Bws 

# = ( Vw(std)

) Vw(std)



# + Vm(std) 

# %Moisture=

100



# * Bws



# Contents Dl Water DI Water Empty Silica Gel 

# Md 

# = 0.440(%C0

2
) 

# + 0.320(%0

2
) 

# + 0.280(%N

2 

# + %CO) M

5 

# = Md(l-

Bw

5
) 

# + 18(Bw

5
) 

# V 5 

# = 85.49



# * Cp



# * 

# J I:J.Pavg



# * 60



# * (1

- Bw

5 ) 

# * V 5 

# * A 5 

# * 528



# * P 5 

# Qscfm



# =

(T

5 

# + 460)



# * 29.92 Qacfm



# = 60



# * Vs 

# *As 

# .

.
(T

5 

# + 460)



# * Vm(std)



# * 29.92



# * 100



# * 144 % 

# lsokmettc



# =

2



# rr 

# 528



# * v 5 

# * () 

# * P 5 

# * 60



# * (1

- Bw

5
) 

# * Dn



# * 

# 4

Post

Pre

Net 

# C..1..~~7_


# 1l4.1
**l.Ql.~** 

# l3cJ"



# 7 J..5.j



# ·5.0 

# uS""'1.

\ 

# (.,51.1-

·7_

. I 

# 'it~.



# { q25".6



# 41ct **~~'**



# 2..5,

. \D As ------Stack

area (ft2) 

# Bws ----Gas moisture (fractional) Cp 

# ------Pi
tot correction factor 

# Dn -----Nozzle diamter (inches) 

# Md -----Dry 

# molecular weight (lb/lb-mole) 

# Ms -----Wet molecular weight (lbjlb-mole) Pbar 

# ----Barometric Pressure (inches
Hg) P 8 

# ------Stack static pressure (inches water) P s 

# ------Stack Pressure (inches

of Hg) 8 ------Sample

time (minutes) 

# v, ------Initial impinger volume (ml) V r 

# ------Final impinger volume (ml) V m 

# -----Dry



# gas meter volume
(ft3) 

# v_. ------Stack

gas velocity (ft/s) 

# Vw(stdrMeter volume

at STP 

# Wi -----Initial impinger weight (grams) W

r 

# -----Final impinger weight (grams) Y ------Dry



# gas meter correction factor 

# Ps

Oz COz

Nz 

# co

As Ts

Tm I:J.Pavl;'



# Vm Vm(std

Bws %Moisture

Md Ms

Vs Qscfm

Oacfm 

# % Isokinetic**~)SPECIAL~ Facility:~\._,,¥-¥---~**  **Location:_fut-~**

S:\

, v-J ll Test Team:

N ..J --'---'-'---- Page __

of __

51 of 90 Unit: t1.t.:c **Q,~.u** Test No:

t:. 'l D

.

• l' ate:
**"~** '\c:>

- ..... **.~**

3\( Methodr-5"'Source

Test Data Sheet Pre-test (;).oc>l cfm@

\ '('

I nit. **(~** Port change-==-.
cfm@ **~**

I nit.

- Port change----==-
cfm@ __:::::::._

I **nit.~** Post Test

P .o.o.>-cfm@

1:)

I **nit.~**

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Pre **~Post _.r:._~-**  PRETEST DATA:

Meter No. _j 11

c; **~~~q;,vt.)**

02 **II-~ 2~::1;** 

Meter Factor

]. 00]

Pi tot Factor

0. jq

I.?' P Bar:

C02 Sample Time lou

P static

.- (} .1.()
Filter Tare ,}\>v

Mole Ambient

F **~()**
6H@ **~.l,\j:Z**

Filter No. **~~I**

Bws
O· uuq K Factor

o jou
Nozzle

dl:

.I fi_d2:...11L_d3:..Jit_Avg:

**~~~~**

Stack Diameter:

£Y Stack Doagram /n

Start Time:
Cl>'-1

\ ( Stup Time: OCfJ,.

Cf **~v**

Tesl Summary: E

Note

s:

- roont **.~**

Lavout

-

---- - :\Ieier **Condouon~**

lcmpcmlurc p,,uu
rome

ar

611

Meter

Stack
**rro~**
Oven
Foltcr

Imp 1\.kter
Meter

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E"t

hot

In

Out l....r.l

()

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219
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g **"1."\~**

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i.\a_"L

li 1.1

.

. {ut.(.tJ

# 52 of90 

# /~

**~,**
**.u** Lfi!EI 

# · **~/SPECIALTY**

Page_of_ 

# Facility: 

# .zwAe/c..v

Location: 

# ~k

**W~** Test No: 

# ---"""'3'------

Date:



# b -}o-

\
\ **-~=-~~~'------**



# Method:

**~**


# 3 **I~** 

# Imp

Tip Style Volume I Modi tied IOOmL 2



# GIS
IOOmL 3 Modified

Empty 4 

# Modified

-200



# g 5 

# 6

_ Vm



# * Y 

# * 528



# * [Pbar



# + 

# &J Vm(std)

-


# (Tm



# + 460)



# * 29.92 Vw(std)



# = 0.04706 *(VI-

Vi) Vw(std)



# = 0.04715

• (W

1

- Wi) B _ ( Vw(std)

) ws

- Vw(std)



# + Vm(stcl) 

# %Moisture



# = 100



# * Bws



# Contents 01 Water 01 Water Empty Silica Gel 

# Md


# = 0.440(%C0

2 ) 

# + 0.320(%0

2
) 

# + 0.280(%N

2 

# +%CO) Vs 

# = 85.49



# * 

# cp

* Jt..Pavg



# * 

# 60



# * (1

- Bws)



# * v 5 

# * A
5 

# * 528



# * P 5 

# Qscfm



# =

(T

5 

# + 460)



# * 29.92 Qacfm



# = 60

• Vs *As . .

(T

5 

# + 460)

• Vm(std)



# * 29.92



# * 100



# * 144 % 

# lsokmettc



# =

rr 

## 528



# * v 5

• 

### (J

• 

## P 5 

# * 60



# * (1

- Bw

5
) 

# * **D~**



# * 

# 4

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# ~ 

# '-1.
**~**



# 1.\o **~ 'i~-** 



# "L **yc;~.'}**



# S}.:> 

# "l..5l."7 As ------Stack

area (ftZ) 

# Bws ----Gas moisture (fractional) Cp 

# ------Pi
tot correction factor 

# Dn -----Nozzle diamter (inches) Md -----Dry molecular weight (lb/lb-mole) Ms -----Wet molecular weight (lb/lb-mole) P bar 

# ----Barometric Pressure (inches
Hg) Pc ------Stack static pressure (inches water) P s 

# ------Stack Pressure (inches

of Hg) 8 ------Sample

time (minutes) Vi 

# ------Initial impinger volume (ml) V r 

# ------Final impinger volume (ml) 

# Vm -----Dry

gas meter volume
(ft3) v_. ------Stack

gas velocity (ft/s) V w(srrl;-- 

# Meter volume

at STP 

# Wi -----Initial impinger weight (grams) W



# r -----Final impinger weight (ghms) Y ------Dry

gas meter correction factor 

# Ps

02 C02

N2 

# co

As 

# Ts

Tm AP avg.



# Vrn Vm(std

Bws 

# %Moisture

Md Ms

Vs 

### Q~·cfm

Oacfm 

# % lsokinetic53 of90 htl'ilit). **]:~lc**

o

lJ 11

i
l
: /JI.,I:<

0 ..; e..rv

4o7.;- Method **-~source**

Test Data Sheet- ,-------·-------··----, l'rl

· -tcsta.oo3

dm

' a 12.• lnit.s:d'1of t\lrt chang_e

- cf111

II

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I nit.

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U/14

"I **c~l** No

:

{

Port **chan~c**

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11

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I

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° **~ample** Time 30

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I

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... (

Date:

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·,

t
l'it<)t l.ca" Chcd.:

l'rc ,..-- l'nst ,_.....- Meter

No

. l(oq"'
**'"~~c** f'oo1...Cf Mctl·r

I :tt"l(ll

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# 54 of90

Page_of_ Facility: 

# _r:w/-tJ

I<

o Test No: 

# __ __._ 

# ___

_ Date: __ 

# Co.::._~...:...;t..=-ct-=---1.._c

_, '---

Unit: 

# f;4.te

o v eA.-' 

# Method:~~

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) 

# L(o

1 

# ~ Imp

Tip Style Volume I 

# Modified



# 100 mL 

# 2

G/S



# 100 rnL 3 Modified

Empty 4 Modified



# -200

g 5 

# 6

Vm



# * Y


# * 528



# * [Pbar 

# +&] Vm(std)



# = (T,n



# + 460)



# * 29.92 Vw(std)



# = 0.04706

• (Vr-
Vi) Vw(std)



# = 0.04715

• (Wr

- Wi) 

# B _ ( Vw(std)

) ws

- Vw(std)



# + Vm(std) 

# %Moisture=

100

• Bws



# Contents 

# 9-t~''" 

# OJ tV

91 Wat« **WM)~** 

# f).t

.,) **{).~.** 

# Weter **~~>.DU** 

# Empty Silica Gel 

# Md


# = 0.440(%C0

2 ) 

# + 0.320(%0

2 ) 

# + 0.280(%N

2 

# +%CO) 60

* 

# (1

- Bw

5
) 

# * V 5 

# * A
5 

# * 528



# * P 5 

# Qsc[m



# =

(T

5 

# + 460)



# * 29.92 . .

(T

5 

# + 460)



# * Vm(std)



# * 29.92



# * 100



# * 144 % 

# lsokmetlc



# =

rr 

# 528



# * V 5

• (} 

# * **P.~**


# * 60



# * (1- Bw

5 ) 

# * **D~**



# * 

# 4

Post

Pre 

# 7t)"i.

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# 1\&
**.~** 

# (f,o.3.

**~~~.**



# 2 **'"'~.v G~g.'-1_**  

# _S')$.

I 

# 2\b',c, 

# '"'~' As ------Stack

area (ftZ) 

# Bws ----Gas moisture (fractional) Cp ------Pi

tot correction factor 

# Dn -----Nozzle diamter (inches)

Net 

# 31-~ 

# 1.1 **0~** l(n 

# ~ 

# 51o-1 Md -----Dry molecular weight (lbjlb-mole) Ms -----Wet molecular weight (lb/lb-mole) P bar 

# ----Barometric Pressure (inches
Hg) P g 

# ------Stack static pressure (inches water) P s 

# ------Stack Pressure (inches

of Hg) 

# e ------Sample

time (minutes) 

# V; ------Initial impinger volume (ml) V r 

# ------Final impinger volllme (ml) 

# Vm -----Dry
gas meter volume
(ft3) v .• ------Stack

gas velocity (ft/s) 

# V w(srdr· 

# Meter volume

at STP W; -----Initial impinger weight (grams) W



# r -----Final impinger weight (grams) Y ------Dry

gas meter correction factor 

# Ps

Oz COz

Nz 

# co

As 

# Ts

Tm .1Pav



# Vm l!,n(std



# Bws %Moisture

Md 

# M,.

Vs Q\·cfm



# Qacfm % lsokinetic

# /.... GCJL.CJEN / 

# ~)SPECIALTY Facility: **.I"'~o-lc..c** 

# Location:

**F~-**



# ..... **d4t~**


# t..A

# Test Team:



# N- W, Page __

of __ PRETEST DATA: 

# P Bar: 

# 2'1."&

**~** Sample Time 

# .?,ou Ambient

F 

# ..;-c;. K 

# Factor 

# ().fl..~ Stack 

# 01agr~~



# 55 of90 

# Unit: 

# [3Hk:e.. Oue......, Test No: __
'- __ Date:

**~** 

# -L-1-l-P



# II



# Yol5 Method **~ource**



# Test Data Sheet Pre-test **.-.e~jl71l** 

# cfm@



# I L lnit. __ Port change__:::::::::

cfm


# @J -=:.. lnit.-=- Port change--==

cfm


# @J 

# _..=-

I nit.

- Post Test(.)

, 

# oto cfm@ 

# _l2_
lnit. 

# ----p(_ Pitot Leak Check:

Pre (./'"' Post **~** 

# 02 **1~.5'** 

# C02



# I. 

# S::: Mole __ Bws


# o. 

# o<-( Stack Diameter:



# ~ "'{: Test 

# Summary:

Start Time: "1..\ 

# 51o Stop Time

: 

# C"11..(.) 

# w~~

Notes:

_________________

_ 

# 5 l'omt

I une

tll' 

# ~~

0 **13~** 

# l. 

# i5.5 1-35" ) 

# 375 \."3,o 4 

# 5'~:6 

# !.lv ) 

# 7'i.v 1.1.( (, 93.8



# \, 1u 1 //1.

. 5 

# lt l1 

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# c; **22~()** 

# l.1( 

# ~
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# l. 1.\ 

# -1 **1~1.5'**



# 1-1

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# 'b

l 

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# I , ,,g


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Pomt 

# Lavout Meter Condmons 

# Ml

Meter Volume 

# 0-\1 **~<-1.£.1~0** 

# O-llc1



# .% **-a.~·vo** 

# (A'"

''1).
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# L\7.7.
**-~-l**



# r .- 

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# l..\~ 

# '1..19-. 

# . 2t& '2..

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# v" "")

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# '2 \1 

# 'l \) ll1 

# 'lll ll) 

# 7.r'i **ll~** /tL 

# _1\l **ll~** 

# 2../<:o-}

Temperature Probe
Oven 

# ~~lle_!..t(

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# ~ 

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# In

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# ~ 78


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- 

# 2.- **~- z.~** 

II 

# Imp

Tin Style Volume I 

# vlodified

100 

## mi. 2

G/S

100 mL 

# "' Modified

Empty .) 

## -l 

# Modi lied



# -200

g 

# 5 (i



# [

llH



# J V

- V,n



## * 

## Y 

# * 528



# * p/Jar



# + I3]j m(std)

- 

# (Tm



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# * 29.92 VwrstdJ



# = 0.04706



# * 

# (V 1

- Vi) Vw(std)



# = 0.04715

• 

# (w

1

- Wi) B 

# = ( Vw(stcl)

) ws Vw(std)



# + Vm(std) 

# %Moisture



# = 100 "'Bws



# Contents 

# oJII

.Gl W8ter 

# 11..071- b.fll **~lltll'tttc:r 11/~0H**  

# Empty Silica Gel 

# Md


# = 0.440(%C0

2
) 

# + 0.320(%0

2 ) 

# + 0.280(%N

2 

# +%CO) V 5 

# = 85.49



# * Cp



# * jllPavg



# * 60



# * (1

- Bws)



# * V 5 

# * A 5 

# * 528



# * P 5 

### Qscfm



# =

(T

5 

# + 460)



# * 29.92 . .

(T

5 

# + 460)



# * Vm(std)



# * 29.92



# * 100



# * 144 % lsokmetzc



# =

rr 

# 528

• V 5 

# * () 

# * P 5 

# * 60



# * (1

- Bws)

• D;

* 

# 4

Page_of_ Method

: • l{o,.) 

# Post

t•rc

l'ict - 

# ~((~



# 7z.8



# c ;?7 **/1'1.~** 

# 711.3 **("OJ~**



# 7 **~1'/.l** 

# 1u~-



# 3

**~** 

# ~'l~ <r
... 

# h..' A.< ------Stack

area (ftZ) 8..,_,. ----Gas moisture (fractional) 

# C" ----·-Pi
tot correction factor D" -----Nozzle diamter (inches)



# Ia \ 0 

# 11..'1 1_2.-"'

- Md 

# -·-··Dry molecular weight (lb/lb-mole) M.< ----- 

# Wet·molecular
weight (lbflb-mole) P tw· 

# ····Barometric Pressure (inches

Hg) P g 

# ------Stack static pressure (inches water) P_,. ------Stack Pressure (inches

of Hg) 8 ------Sample

time (minutes) V, 

# ------Initial irnpingervolume

(ml) V 

# r ------Final impinger volume (ml) Vm 

# -----Dry

gas meter volume
(ft>) v_, ------Stack

gas velocity (ft/s) V wt•·tt!;--Meter 

# volume

at STP W, -----1 nitial impinger weight (grams) Wr-----Final impinger weight (grams) Y ------Dry

gas meter correction factor 

# p<

Oz COz

Nz 

# co

A, 

# r..

Tm llP "''"



# Vm 101/(Sit/)



# B..,, %Moisture

**Mr~** 

# M,.

If, Q.,

· cfm



### ,ctin 

# % 

# lsokinetic57 of90

'"{a1( I **~)s~EcfA**

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,Method ,8'Source
Test Data Sheet Pre-test cl.OuS cfm@ iL_

In it. _BL Port change- cfm@-==-

I nit.-=:.._ Port change--===. cfm@--=-

I nit.-==- PostTest.P,Oo6

cfm@ /5' **lnit.~** Pi tot Leak Check:

Pre

v
Post

V Facility:

i tJ kl
'<•

Unit: fkkt **c>.~t..J** Location: C:urJ.

... **~,** vlA

Test No:

3 **-~--** Test Team:

,J 1\) Page __

of __ PRETEST DAT)\: P Bar: "Z."-1\ Sample Time **_.,.JU>~­** Ambient

F --c;:iv.-0 __ K Factor

CJ ./ 2 t. Stack D•agram l'omt Tnne

,\I' ' . ,) 9

0 \.&o ' ) **\~.~**

\ t l.l 6 S1.) **\.'~'1** ( ..;-t,

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t

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Date: ___(g..:..3Q

-

I

I Meter
No

.

I (tt;

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fo

o '2.. Of Meter Factor

t
1 C)'{J

Pitot Factor

0 ,3'\ P static

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0

\ **~**
Filter Tare tJ. H@ **-"""=J~t==**

Filter No

. --=-

c. -- Nozzle **dl:~d2**

__ **tt~d3:**

**Avg** .113

02 ?(?

<:.. C02

/. '?- Mole- Bws

o .uq Stack Diameter: Test Summary:

Start Time:
6i.\ •1.. Stop Time: 0?

z. <.,. Notes: _________________

_ Po•nt Lavout Meter Conditions
Meter .'\II Volume 01 \S 41.\ 5"::-\ 0 l'i **4~~-l{O** 0 ',c, ct-to, c.,sq (J

.

I **~ ~f.{C**  **1(,~** l) ll 4L.\'\ '17\ 0,11 **~\(** ,'\>o (J,\1

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70 ; :. {)·/ 21'-l "· ':i

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Probe lu, 7'11 z \$ ("to **-z.,~** 7.--\0 **~\C\**

'1'-4

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**lo~'**58of90,/;!rJ'[jtLE:'!\1/Page_of_Facility:1.-..J)lr-,;Location:t<./14-Unit:_/2&/:eOue...JTestNo:..3---=:::::.______Date:_--.:::(o=---·)c.?"----_l_l___Method:rJt+l(''-\ol..;(t3b)Imp_VolumeContentsIModifiedIOOmLlt.>.UVQlrJtJ>U2G/SIOOmLlo.lrJWa:terfJ"-0H3ModifiedEmptyEmpty4Modified-200gSilicaGel56V_Vm*Y*528*[Pbar+-&lm(std)-(7;n+460)*29.92Vw(std)=0.04715*(w1-Wi)B= (Vw(std))wsVw(std)+Vm(std)%Moisture=100*BwsMd=0.440(%C02)+0.320(%02)+0.280(%N2+%CO)V5=85.49*Cp*jAPavg*60*(1-Bws)*Vs*As*528*PsOscfm=(Ts+460)*29.92Oac{m=60*Vs*As. .(Ts+460)*Vm(std)*29.92*100*144%lsokmettc=rr528*Vs*()*Ps*60*(1-Bws)**4PostPre30.?f{,l).q7;?.,.q_I'12.Q:t(,'\8.?gn.'2.As------Stackarea(ft2)Bws----Gasmoisture(fractional)Cp------PitotcorrectionfactorDn-----Nozzlediamter(inches)Net"Jf'.qQ.C\oSJ5_1R\.SMd-----Drymolecularweight(lb/lb-mole)M,.-----Wetmolecularweight(lb/lb-mole)PbJr----BarometricPressure(inchesHg)P8------Stackstaticpressure(incheswater)Ps------StackPressure(inchesofHg)8------Sampletime(minutes)Vi------Initialimpingervolume(ml)Vr------Finalimpingervolume(ml)Vm-----Drygasmetervolume(ff1)Vs------Stackgasvelocity(ft/s)Vw(strl;--MetervolumeatSTPWi-----Initialimpingerweight(grams)Wr-----Finalimpingerweight(grams)Y------DrygasmetercorrectionfactorPsDzCDzNzcoAsTsTmVmVm(std)Bws%MoistureMdM..VsQscfmOacfm%lsokineticI59 of 90
FORM# GSC-TM012-004 REV 2011-01,

Eff 7/1/11 GAS BAG SAMPLE DATA SHEET Client: Location: Sample
Site

: C-LJ-Z.otl Date Samples Collected:

'=-

**~** z.ct

**~** >v

**0** 11 Date Samples Analyzed:
'--yo -ZcJ

•' Number(fype

of Tests

: Number

of Bags:

3 Collection Method

: Sample Bag Identification

Time ts-z..l;) rer

1.. o-.> > **~2.**

2.1 **~"'** -o 3t }'[)

**C~** 4 n.

- o q 'LSo Fuel Factor (Fa) where

%0

2 and %C0

2 are by volume on

a dry bas1s and 20.9

1S the percenl

by volume

of amb1ent air Notes:

Sampled

By: Subm1tted

By Analyzed

By: 02
C02

co %

%
ppm

Fa /S.-5"" /.) o/8.0
/.6 /1,

(

;, '2- F 0 Faclors

for Selecled Fuels Coal Anlhracile

and ilgnote

1 016·1 130 811Uminous

1 083·1.230 Ool Distillate

1

. 260·1 413 Res1dua1

1.210·1
370 Gas Natural

1.600·1
836 Propane

1.434·1
586 Butane

1.405·1
553 Wood

1

. 000·1 120 Wood Bark

1.003·1
130__ ..A_

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Mid Nitrogen

Zero Nitrogen Dioxide

n/a High Carbon

Mid Monoxide

Zero #tkr

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4 **(..}#{~)**

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Zero ANALYZER INFORMATION Analyzer

SYSTEMI1 Type
Model NOx co 02 C02 **SO:~** voc Form

# GSC·WP007-00S REV 2010-01,
EFF 11/1/10

Serial

#I

60 of 90 REFERENCE METHOD Analyzer Calibration
Error Test Date:

**Analyst: ~**  C

- Z-'9-
t..o
I' Trailer Unit:
Analyzer **S~m:** " Assigned
Data

: Analvzer ResPOnse

Actual Cone. Cylinder System

1 System2

Exp. Date ppm ppm ppm ppm ppm ppm ppm 2..1..,
1.....
2'2..'L

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Serial

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ppm ppm

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ppm ppm

ppm Page __

of __...A."IiOLOENI61of90,AirQualityTestReportAPPENDIXEReferenceMethodDataPlantAlcoalntalcoWorksAddressFerndale,WAc,LocationBakeOvenBa9housaP,.In"H9PersonnelSBM/PH/PCIDDFPatatlcInH,ODistancefromFarWalltoOutsideofPort,InchesWidth(IfRectangular)NipplelengthandforWallThlcknesa,InchesDiameter,InchesEquivalentDiameter(onlywhenrectangular)AreaInequarefeetStreightDistancebeforesamplinglocation,InchesNumberofDiametersBeforeLocation•StraightDistanceattarsamplinglocation,InchesNumberofDiametersAfterLocation•Enter•p•forParticulateor•v•forvelocityMinimumNumberofTotalPointsNumberofTotalPointeChosenNumberofPortaNumberofPointsperPortDrawsamplinglocation,plan&topview.ONOCChecYJ=.IJCompletenessLegibility__AccuracyCheckedBy:.,\--ft..,/)()pPersonI{Sianatura/Oatalv'OKOKOK62of90Method1DataSheetMethod1DataSheetITimeIIDateI6129/201tIJobIINWltALINTtoe90.06.084.038.4845.5NA>121.01.4p121628________FoDistanceStackYaw&VelocityData%DucttromOutsideYawAngle41'TempVelocityPointsDepthofPortOagreesInchH20°FFeet/sec.3.2%8.7·----·-------·-1-----_10.5%___...11:.L__----·--·--·---·-·-·-----19.4%.__.22.3·-·-------·--·-·------.....32.3%.._33.1·-----·-----____,.__------·---..--.67.7"LA680.6%73.7-·"A7-89.5%·-81.2---..9&.8%-·----·------818.7--8210.5%14.8.83--·22.3·--·-84--32.3%=-_-n1___858687.7%62.9---·80.6%73.7......89.5%·-·-81.2--......J!8_.96.8-'!..____,_!!.:!.__,___,_......._.,__,_____,___,_...._..__------------..--·-----·--·----·--------·--·-·------------·-·--..---,_____-------·------_,_,_,___-----·-------.................._...._..___---·----·----·-----------···-·----.--___,.,__-------------i------·-·------·______,,1--·----·------·----·--·---------_,___""'1-------·------·_,__,___------------·---·-------------------------·----_,____,..---···-----------·--------__.,___------,,____-------·------------------.--..-·.......____,_------__,___--·-·-___..__.............____--·---·-------·-----------___,_..___AverageldacfmI1_IJ_A_J'_v/'·rLeader(Sionatura/OateIE·1I I Plant Location Date Start e DN c. y Per 4H Vm t... v,...d Vac v_d %H

2 0 %C02 **%~** Md M. Pa Pa t. "AP••• v. A. a ad a_ %1 pb w, c, E, E, WIICEII C..ce11 EIICEII E..ce11 EIICEII

I Alcoa lntalco Work& I Bake Oven BaghouH Run Number

63 of 90 Bake Oven Baghouse USEPA Methods

5 & 315 Summary

of Test Results IAddresa

I Ferndale,

WA

IJobt I Personnel

I SBMIPHIPCJDDF

I Date L

1

I I 2 Test Date

6121112011 61211111·6130111 Run Start Time

15:36:00 21:59:00 Run Finish Time

20:55:00
3:23:00 Net Traversing Points

16

16 Net Run Time, min

.

300

300 Nozzle Diameter.

in

.

0.188

0.188 Pitot Tube Coelicient

0.84

0.84 Dry Gas Meter Calibration Factor

1.007

1.007 Barometric Pressure,

rn. Hg

29.70

29.80 Average orifiCe meter Differential,

in. H,O

1.19

1.27 Dry Gas Meter Volume Sampled,

ti'

185.346
196.587 Average

Dry Gas Meter Temperature,

F

74.5

68.9 Dry Gas Meter Volume Sampled,
dscf

183.555
197.446 Total Moisture Laquid collected,

g

202.8

259.6 Volume

of Water Vapor,
sci

9.56

12.24 Moisture Content

ol Stack Gas,

%

4.95

5.84 Carbon Dioxide

. %

1.50

1.80 Oxygen,%

18.50

18.00 Dry Molecular Weight, lbllb-Mole

28.98

29.01 Wet Molecular weight, lbllb-Mole

28.44

28.37 Aue Gas Static Pressure,

ln.
H 2 0

.0.16

-o.16 Absolute
Flue Gas Pressure,

ln. Hg

29.69

29.79 Average Stack Gas Temperature,

•F

217.3

215.6 Average Square-Root Velocily Head,

in H 2 0

1.145

1.190 Average Stack Gas Velocity, It/sec

73.64

78.43 Stack Crossectional

Area,

If

38.48

38.46 Dry Volumetric

Flow Rate. dry scfm

125,030
129,304 Actual Wet Voh.metric

Aue Gas Flow Rate, acfm

170,044
176,474 Percent lsokinetlc

ol Sampling
Rate,

%

97.7

101.6 Quantlly

of green anode material placed

in furnace, tonslhr

18.02

18.02 Filterable Particulate Matter,

g

0.0054

0.0000 Filterable Particulate ConcentratiOn,
gr/dscf

0.0005

0.0000 Filterable Particulate Emission Rate. lblhr

0.48

0.00 Filterable Particulate Emission Rate, lblday

11.60

0.00 Total Methylene Chloride Extractable Matter.

g

0.0052

0.0016 Total Methylene Chloride Extractable Matter Concentration,
gr/dscf
0.00044
0.00013 Total Methylene Chloride Extractable Matter Emission Rate, lb/hr

0.469

0.139 Total Methylene Chloride Extractable Matter Emission Rate, lblday

11.24

3

. 33 Total Methylene Chloride Extractable Matter Emission Rate,lblton

"0.026

"0.008 • Lblton

of Green Anode placed

In the Anode Bake Furnace.

E·2

NW11ALINT109

I 6129

• 6131112011

I 3

J Avera_110_ **~nee** 6131112011 4

: 15:00 9

: 29:00 16 300

300 0

. 188
0.188 0.84

0.84 1.007

1.007 29.75 29.75 1.43

1.29 202.568 194.834 64.6

69.3 204.884 195.289 257.7

240.0 12.15

11.32 5.60

5.46 1.20

1.50 19.10

18.53 28.96

28.98 28.34 28.38 .0.20

-o.17 29.74

29.74 211.9 214.9 1.273

1.203 81.65

77.24 38.48 38.48 139,005 131,113 188,537 178,352 98.1

99.1

90. 110 18.02

18.02 0.0000
0.0018 0.0000
0.0002 0.00

0.16 0.00

3.87 0.0024
0.0031 0.00018 0.00025 0.215

0.274 5.17

6.58 "0.012
"0.016

0.1864of90AlcoalntalcoWorksFemdale,WAFilterableParticulate&MCEMDataRun1FIHerable<Front-Half<FHllParticulateMatterMassFilterNumber969TareWeightofFilter,g0.3543FinalWeightofFilter,g0.3541NetWeightofParticulateMatterfromfilter,g•o.ooooTinNumber1112TareWeightofTin,g2.6406FinalWeightofnn,g2.6460NetWeightofParticulateMatter,g0.0054VolumeofAcetone,mL72.0NetWeightofBlank,g**0.0001VolumeofAcetoneBlank,mL198.0Wt.Nol.ofAcetoneBlank,mg/mL0.0005NetWeightofPMDuetoAcetone,g0.0000NetWeightofParticulateMatter(BlankCorrected),g0.0054TotalFront-HalfParticulateMatter,Jl0.0054Methv!eneChlorideExtractableMatter(MCEMlPortion"1"Section(extractedfiltercatch)NetWeightofParticulateMatter,g0.0003FilterBlankWeight,g0.0000"2A+2M"Sectionprobewashes)NetWeightofParticulateMatter,g0.0031VolumeofSample,mL52.0WtNo!.ofDCMBlank,mg/mL0.0000NetWeightofPMDuetoDCM,g0.0000NetWeightofParticulateMatter(BlankCorrected),g0.0031"3W"Section-lmplngerWaterNetWeightofParticulateMatter,g0.0000VolumeofSample,mL320.0WtNol.ofDCMBlank.mg/mL0.0000NetWeightofPMDuetoDCM,g0.0000NetWeightofParticulateMatter(BlankCorrected),g0.0000"3S"Section-Solvent(lmplngerAcetone/DCMRinse)NetWeightofParticulateMatter,g0.0018VolumeofSample,mL98.0WtNol.ofAcetoneBlank,mg/mL0.0000Wt.Nol.ofDCMBlank,mg/mL0.0000NetWeightofPMDuetoAcetone,g0.0000NetWeightofPMDuetoDCM,g0.0000NetWeightofParticulateMatter(BlankCorrected),g0.0018TotalMCEMParticulateMatter(BlankCorrected),g0.0052*ForFPMresultsreportedaslessthan(<)zero,zerowasusedforthecalculations.••forresultsreportedbelow(<)thedetectionlimit,thedetectionlimitwasusedforthecalculations.E-3Run29700.35460.3539•o.oooo11102.63512.63460.0000102.0••o.ooo1198.00.00050.00010.00000.00000.00010.00000.000252.00.00000.00000.00020.0000410.00.00000.00000.00000.0013100.00.00000.00000.00000.00000.00130.0016BakeOvenBaghouseJune29•30,2011Run39710.35360.3535·o.oooo11112.57522.57510.000078.0··o.ooo1198.00.00050.00000.00000.00000.00030.00000.000150.00.00000.00000.00010.0000480.00.00000.00000.00000.0020142.00.00000.00000.00000.00000.00200.002465of90USEPAMethod5/315Run1Method51315DataSheetPlan!Alcoaln1alcoWorksIRunNo.1IDateI612912011IIJobINW11AUNT109AddressFerndale,WAEqutpmontIDCalLocationBakeOvenBaghouseRaag.Bo>SampboxMeterbox1729CReadoutPersonnelSBPNPHIPCIDDFUmbocalParln"Hg_29._70_r-odarl!agPilotP003NW"--'yAHoc.ConatantaChocks38.48y_.,...1.!X17InitialOGM1.642AnalDQM0.11-tLeeknoteP-lc1nK,O_-o_._11_1EOr;;;sa=tPum=.:;.P________I::K::::;;tacto7r__-::::------------------------I:Es=l:::Moistu::::'=ra:::,___-tgmH,O202.8M31.5%C011-•MidPoat12120.0040.001FilterI969B,.meas5.018.5%0,!stackTCFtnorwt.0.3543B,.satTraversaElapsedlimeClockGasVelocityVelocitySlackPointInMinytesTmeMeterTemp.No.BeginEnd24hrReadingM'•FW-1..---063.600·-._1._38_1..1!.__2_15_•.__,L__...!!1.8_37.5____065.720_....!:B.._....:!·.!.L337.556.3078.180135116218--4---;;r;:;;+---;;,.2,0··-1:12_!!?_--;::=--;;8+-·:_1 -2186___!!;!.!._112.5J1129751·-__,_42171112.s131.3I124.385_801135.715-s-a150.01688147040-7-"168.82,87.5.158626_____"187.55206.32250182754_...!25.024383___•.243.81281.33000··----·-f----r--f-·--r----·--r-·---·-+--------------·····-·------··-------------·-·-·-------·----··--·-----·--Final20:55193996205.340-216.5522785238948----2389461 .02181 . 72211-.__._1.!_2181___:_02161··-,__,_62161.42181218__._1-·--'-'.16218216216DryGasMeterTemperaturaOnbcePressuroInletOutletM!anH,O_2!_._,_.E.,_.,E__1.241.18r--1.211.13._.!.L_74_7575-75-76-..!!.__._!L....757&77!J.._r-74_--f----74___1!!!!._74___,_f--l.:..lL741.2074__75_._._1.31!_.-'!.:.tO75___1.1C!_76-_.......!:.!.!..75_..__74-----Sumoravg185346l131e11144I217I48I1uI1.185I97.71.014183.555IP'IIIIISlblhrgrlacflbiMIIIB1u5.11180.00540.48330.00045Flow73.64125,030.30.00540.48330.00045170044.31ProbeTemp•F2522482492492532482492512482472532542512512502411OvenTempF246250249248-250-247248_2472411250248248-245249248248-----ConeentaH,OIH20.4SGFiherExtlmpngTemp TempF•FNANANANANANANANANANANANANANANANA50_5456-5657_57-59-506259_62I_!!_62626261PympVacHg5.05.05.06.0504040405050505050505050Maxc::!IJVol.PostPre(mUg)(mLig)(mLig)100933.8788.71007532764.40697.0692.120094859045QA/QCCheckCompleteness//Leg<biityCheckedBy-+>J/tSIQnawreiDate)AccyracyJL./fs/)a#1---J;;.mL;;'ader(Sognature/Oate)ReuonablanessE·4Noles-Netpin145.1884944.0vPlantAlcoalntalcoWorka66of90USEPAMethod51315Run2Method5/315DataSheetIRunNo.2IDateI6129111-6130111IAdclreuFerndale,WAEquipmentIDColConstantsChecksLocationBakeOvenBaghouseRoagBoxSampboxA.-·38.48VacuumPersonnelSBMIPHIPCIDDFUmbir:alMelerbo><17291.001tnnDGMt;%,=;;,M::;;als;;;t;;;ure;,;.;..--==..:.;.:..;5.:;:84F--.,.M:-eaa----15tackTC!TcReadout-1.842FinalDGMIJoblNW11AUNT109PreMidPost12100.0080.008pllttn"Hg28.80TedtorBagP1totP003NW<,.0.84LNlrnoteP-tnH,O.0.18H,O259.81131.8%CO,NozzleFiltert970B,.moas5.8.,______FilterWL0.3546B,.satF""IF.-IM.28.371M.29.01TraversoElapsedlimoClockPointInMinutesTimeNo.BeginEnd24hrGasMotorReadingVeltx:•tyVeloCityStackTemp•FDryGasMotorOrificeProbeOvenRiterExitlmp1ng.PumpTemperaturePressureTemp.Temp. Temp. Temp.Vac.InletOuUotinH2(•F•F•F•FHg.239.6481.501.22212727!______________1___1___1.so1.22212111-73______...m__!iL._..!:!!..__!____37"!__58.3-1-----269.1751.501.222137072_____-·248______249__N.!..._____50____..!.__75.o.J___277.8501.361.112131011____M!_____ill______!!'_J..:!!___!._______ps_....l.:!L_____....§!!____!:!L250250NA482_____L___93.8____t..:.l!L____f!l!____Lo_........!:!L_250250NA482 o__112.s.J..E.!.:LJ-.______.312.880.1___!E__..!.:!L___!!!.___ro-·1.19248_2soNA482 o1__1_!!_::1__150.0.324.780___1.301.14__!!!!..___88____!!____1.1!248_250NA4820W-8__!50.0_____1.5!___!!!.____!!____88249NA4920___!..._____188.8_!_!7..:!._1---------348.320____!£____.1!!_._.!!!____!!____251250NA492L_____!_____187!._1-----·--362.355_____l!L_._.!!!_____68____250250NA492L____!__-------375.341-__!.60-·___88__250249...!!___20-:i::::___=j::-=-;!!==--;:----:---::::::::::-__..!___---·---r-·-413.092___t!?.__!!____250251NA4201281.3300.0424.5111.301.1421486 861.18250251NA4!._2--:j=_3:2;:00.:=--=:===·-=------==-·----____1__·1--1----------·1---·-·--t··----------1----J.....__------·-·!-·-+··--·----·j--·----- ----------1-----------Final3:23438.233Sumoravg198.5871.4200!11902!215.688.889.31.270Max[TIJ101.8187.448Particulate1.022gramslblhrarlsc:flbiMMBtuContentaVatPoetPnl(mUg)(mUg)(mUg)5.5920.00000.00000.1100001H,O10092877191Flow2"HO1007301725178.43065936572129,304.1TOIIII96859256QAIQCChockCompletenessLegibilityvReasonablenoStChockedBy:9nrPersonnelv(S>Qnaturo/OatolE·5Notes-------Netgain20985.021429PlantAlcoalntalcoWorksAddressFemdsle,WALocationBakeOVenBaghousePersonnelSBMIPHIPCIDDF%Moisture5.60.....---P•ln"Hg28.75P...ueonH,O----41.20---KtaaorFlltorI871FilterWI.0.3531TraverseElapsedTimoClackGasPoinlInMinutesTIIT1aMeterNo.SaginEnd24hrReadingS·10.018.8I4:15:oo436.490r-·--_37.5!_)_8..:!._r-!.___37.556.3__r-......!____75.0-....473.271..._r·_s_..?.!·.!!....__II:!JI_----484115·--·-r-....L-_IIi!:!...·---497.87r-....I.__..!!!!..131.3·---5099·---r--L-..m:!.-·-·-·-·--521632·---W·1_!50.0534.360r--·-·------·--r-___!..-.188.8187.55411.585-.......L.....!!!H...1_08.3r:==--=...-r--..!___225.0i572.58----r----r-.....L...584105--......,l!J.8599420--__]___F==-----__!__300.0'628.2-839.0--·-----·---L-------------w-•-·•-----1---·-_._.,__=r-=--=--·----·--f--.----·----··-__.._L_r-------__J___._I··----------·---..-j..-Ir··----------·-r---1·-----------..-1-·--I1------..-r--t-----------·--·----FinalI9:20639.058SumoravgI3oo.oII202.568%lloldMIIo98.1Ytfl1.011!I......VoLdiOi204.8114..._Vol.cbclll5.802Flow.MieoI81.85dl!:fmI139,004.8...I,1f8,537.1Complotonoss•.:jLegibilioy67of90USEPAMethod5/315Run3Method5/315DataSheetIRunNo.3IDateEquipmentIDCelConstantsR.BoxSampbollublcalMetarbox1729skTCTCRoadoutBagPilOtPD03NWc.Or&alPumpllozzlo0.111DNinlt'ChMEsMoisturegmHz()257.71131.2B,.meas5.619.1I613012011IIJobItNW11ALINT109ClleckaPreMidPoot38.48Vacwm15151.007lnltDGM1.1142AnalDGM0.114Leakr11te0.0070.0050.181Pilat%CO,Nozzle%OzStockTCB,satFO•IF.-IM,28.341...2696locityVolocityStackDryGasMeterOriiiC8ProbeOvenFilterExitlmping.PumpTampTamparalurePressureTamp.Tamp. Temp. Tamp.Vac.NotesAP11AP•FInletOuUelH2C•F•F•F'FHg1.501.226060245,..247__525.0·-.•.....!.:!!........!:212176181-·--__,24!_..1.182188182_...!.:!L248,_,ill_NA485.0--....ldL1..::!52!88262··--·_,J.:!fL____.!"..!.__!!.....,....Ji.:!!..........:!9_...!:262186363-·-_!:!12441-.lliL...495...._,_o_1182181141-114,____...!.:!32472.!!.._NA5050......:............116r-..!!L6564......J..:!L249248-NA515-......:!'!.......-1.222196885__..!,E_248247-NA515.520785114......!:.4!....246l_lli_NA505·--....1.3419885114--·__!.£__249248_NA525.....:fL.-13719068__1.50248248NA5460...-=.!!!....-13819168 65248248NA5560.......:!!.....1.3720768___1,!!.8251248NA586-·---.821352..!1:_6866___...!:'!:'246249_NA586......68__1.37221L..6657__........!.!L245 248NA596.827067249 249818.,_,_____-----....___--------·-----------r-......-·--------1--------------1----1--- -----1---f1-1--1--,_..1-.......--I1.8281lu73412119I851I84.1I1.428IMuCIT]hid-ParticulateContentoVol.PoolPnlNatgaingramalbllvarlllcflb/MMI!1u(mLJg)(mLJg)(mLJg)A'ilnl0.00000.00000.000001H,O100963.7789.3194.4e.clc2H20100770.476327.21........3M,0697.4694826TGiil4SG2009462892.753.5JA-./V'--In,L.f!11J=-_RoasonablenossChockedBy-!_1DDf¥-D"-Lea/or.......loamPersonISIQnature/DatelE-6IIPlantLocationDateStart9ONc.yPIITAllVmt.nvmatdv..Ywatd%C02%02MdMoPePot.'IAJ>•••v.A.Qoda.."'olpbFpF,E,E,EbFeFeEgEgEbF,F,E,E,Eb68of90BakeOvenBakeOvenBaghouseAlcoaMethod4075A·TFSummaryofTestReauhsIAlcoalntalcoWorksIAddressIFerndale,WAIJobtIIBakeOvenBaghouseIPersonnelISBMIPCIPHIDDFIDateIRunN1611ber12TestDate612!1120116129•6/3Cit'2011RunStartTime15:25:0021:56:00RunFinoshTime20:53:003:20:00NetTraversingPoints1616NetRunTome,min.300300NozzleDiameter,in.0.1130.113PrtotTubeCoeficient0.840.84DryGasMeterCalibrationFactor1.0431.043BarometricPressll'e,in.Hg29.7029.80AverageorificemeterDifferential,ln.H,O0.170.16DryGasMeterVoll611eSampled,II'71.66066.533AverageDryGasMeterTemperatll'e.'F79.774.2DryGasMeierVollJ'neSampled,dscf72.62168.345TotalMoistureLiquidcollected.g56.772.4Voll611eolWaterVapor,scf2.673.41MoistureContentofStackGas,%3.554.76CarbonDioxide,%1.51.8Oxygen,%18.518.0DryMolecularWeight,lbii>-Mole28.9829.01WetMolecularweight,lbllrMole28.5928.48AueGasStaticPressure,ln.H20-11.16-o.15AbsoluteFlueGasPressure,in.Hg29.6929.79AverageStackGasTemperatll'e,'F219.9215.1AverageSquare-RootVelocityHead,inH,O1.1791.133AverageStackGasVelocity,It/sec75.7572.58StackCrossectionalArea,If38.4838.48DryVOI1611elrlcFlowRate,dryscfm130,002124,294ActualWetVolunetricFlueGasFlowRate,aclm174,913167,600PercentlsoklnetlcofSamplingRate,%102.9101.3Quantityofgreenanodematerialplacedintumace,tonsntr18.0218.02ParliciAateAuorideConcentration,mg/dscm0.01070.0000ParliciAateAuorideConcentration,ppm0.01350.0000ParticulateAuorideEmissionRate,lblhr0.00520.0000ParticulateAuorideEmissionRate.lblday0.1250.000ParticulateAuorideEmissionRate,lblton"0.0003•o.ooooGaseousFluorideConcentration,mg/dscm0.0620.161GaseousFluorideConcentration,ppm0.079D.204GaseousFkJorideEmissionRate,lbiiY0.0300.075GaseousFluorideEmissionRate,lb/day0.731.80GaseousFkJorideEmissionRate,lblton*0.0017*0.0042TotalFluorideConcentration,mgldscm0.0730.161TotalAuorideConcentration,ppm0.0920.204TotalAuorideEmissionRate,lblhr0.0360.075TotalAuorideEmissionRate,lblday0.851.80TotalAuorideEmissionRate,lblton"0.0020*0.0042•LbllonofGreenAnodeplacedIntheAnodeBakeE·7NW11AUNT109I6129•6131112011I3IA-.QoComIIIIanco6/30120114:12:009:26:00163003000.1130.1130.840.841.0431.04329.7529.750.190.1772.68370.29269.374.475.22572.08487.872.34.143.415.224.511.21.5019.118.5328.9628.9828.3828.49-o.18.0.1629.7429.74212.5215.81.2351.18279.1375.8238.4838.48135,142129,813182,718175,077102.5102.290·11018.0218.020.00000.00360.00000.00450.00000.00170.0000.042"0.0000"0.00010.3710.1980.0000.0940.1880.0984.512.347"0.0104"0.00540.3710.2020.4700.2560.1880.1004.512.39*0.0104"0.0055Q.20AlcoalntalcoWorksFerndale,WA69of90FlourideDataParticulateFluorideEmissions,.,,...·'ft'&Front-HalfRlnselAuorideDetectionUmlt,mg/LTotalVolumeofSample,mLTotalVolumeofBlank,mLFluorideDetectionUmit,mgFluorideConcentrationinSample,mg/LFluorideConcentrationinBlank,mg/LFluorideConcentrationinSample,mgFluorideConcentrationinBlank,mgFluorideConcentrationinSample(lessblank),mgFluorideConcentrationinSample,mg/dscmAuorideEmissionConcentration,ppmGaseousFluorideEmissionsllmalnaerContents\AuorideDetectionUmit,mg/LTotalVolumeofSample,mLTotalVolumeofBlank,mLAuorideDetectionUmit,mgAuorideConcentrationinSample,mg/LAuorideConcentrationinBlank,mg/LAuorideConcentrationinSample,mgAuorideConcentrationinBlank,mgAuorideConcentrationinSample(lessblank),mgFluorideConcentrationInSample,mg/dscmFluorideEmissionConcentration,ppmE-8Run10.062002000.0120.17<0.060.0340.0120.0220.01070.01350.064002000.0240.35<0.060.1400.0120.1280.0620.079Run20.062002000.012<0.06<0.060.0120.0120.0000.00000.00000.063152000.0191.03<0.060.3240.0120.3120.1610.204BakeOvenBaghouseJune29-30,2011Run30.062002000.012<0.06<0.060.0120.0120.0000.00000.00000.064272000.0261.88<0.060.8030.0120.7910.3710.470PlantAlcoalntalcoWorksAddressFerndale,WALocationBalatOvenBaghousePeraonnetSBM/PCIPHIDDF%Moisture3.55Meu---Patln"ttg211.70---P-1n11,0-o.16---KRiterIAFllterWt.TraverseElapsedTimeClockGasPointInMonutesTomeMeterNo.BeginEnd24hrReadingS-815:25:00I--28G.448--_]__•..!JI.8__17.5.__&___37.556.3..""'303.51570of90BakeOvenBaghouseAlcoaMethod4075A-TFRun1Method4075A-TFDataSheetIRunNo.1IDateEqulpmentiDCalConstantaReag.Bo><Samp.box"'-·UmblcalMeterbox1696yStackTCTCReadout411.BagPatot1'0029"'OrsalPLmpNozzle0.1130,InInchesEstMolstumgmH.o58.7M31.5B,meas3.618.5B,.sal100.0Fo..VelocltyVelocityStackDryGas1.4eterOriliceTemp.TemperaturePressureM'•FInletOuUett.HinH201.701.3021673720.21-·-----·-1.55-75-74·-·0.18_!£__1.271--220rr-7L___....l,!i2p23-22076__0.19---"-··-...!!&..93.8_-·--·-308.255--1.28·-pl.L22079770.18......!.12.5_-----312.840______!.:!L..J.E22280780.152_112:!,1_131.3_,_,___318.9881.301.1422180790.181-;-Et.:1=-321.1501.32....!:..1_L22381_!!__1-0.17__W-fl__325.412--1.411.112198080I-0.18t--·-L0329.950.....!:...."L.80_!!!_0.18___!._._334.430·---___1_.g_,_8281-0.19____5__338.170-1.40...!.:!!8382_0.18_...!___;*;:F=-343.930______,..h!Lr-Wr--22184820.14__1___348.280-1.281.1322185830.16352.550--___Lli._22184840.181281.3300.0358.8701.35..!.:1!..22'!._83 830.17·------------___,.20:53:00381.108--·-------=::·I==-·-·-----·-------------·-·----·---·----·---·-----·--···-·---1----,___----·-------1-r----------__,____--------------·-----·--------·--·-------- -----·----·-----·---I---·-·---l---·--·------·--··-------·-··-----------·------····----·---·--- ----··---··-----1---Final20:53361.108SumoravgI300.oII71.880I1.393111.17881219.9I80.3I78.1I0.174%......SC102.9Yga1.051Particulate1-.......VoLdlct72.821aramslblhrarlacflbiMMB1u......VoLci.clll2.057l'rantFlow8ltcktlfteC75.751-.....130,002.0TCICitl....)14,913.4AI612912011IIJobtNW11AUNT109PreMidPool31.48Vocuum12121.1143lniU.IDGM1.688FlnaiDGMOA4Leakrate0.0030.0050.113PHot%CO,Nozzle%0.StackTCIF.-IM.28.511Mo28.98ProbeOvenFilerExitlmplllgPumpTemp.Temp.Temp.TempVacNotes•F•FF"FHg240NA582.0----·----241NA....!L.2.0NANA..2!.,_2.0..lli...__M___-.,_562.0_245NANA572.0I-245-NANA572.0246-NANA562.0245NANA612.0246NANA812.01---244NANA822.0_1--240NANA_57_2.0_-241NANA582.0-248_NA582.0-248_NA602.L1--245NA61__bLr-246NA NA622.0---1----1------- -------- ----------IMu[2:]lmpiDIIII'8c_,.VDI.PostPreNe1gain(mUg)(mUg)(mUg)10.1NNaOH10079437569374I0.1NNaDHtOO73037282213M,06490648406..SG20087518585166PA10CChecka{;LegibilityvReasonablenessvCompletenessCheckedBy:\{.L¥Z'i"72_Personnel((S;grtature/Date)E-9PlantAlcoalntalcoWortcaAddressFemdale,WALocationBakeOwnBaghousePeraonnelSBMIPCIPHIDOF"'Moisture4.76MPar"'"H!I29.80p_.,H,O---·0.15---KtoctarFln.tIBArterWI.TraverseElapsedllmelClockGasPcintInMinutesTlmeMeterNoBegnEnd24hrReadingW·1I21:56:00__!64.480--_o::-41e.e218.8.J-.!!:!.-3373.100-·-----4---5r-1-5.093.8·-__6,_!3·8_j12.5385.533-7112.5_1131.3389.515-8131.3_j_1500393.510__--J.168.8S-1-397.5352-'i'401.8853206.34225.04_10.505-5--414.700__6262.5418.8027_w.s281.3-422.815-8300.0--=-1.3·20"00-----------------·-------·----r-----IFlnaI0431013rr:JI66.533'!(,llc*bllct101.3Tep1.047I-.-Vol.diet68.345Vol....1.936FlowI72.581124,294.31167,600.4OAIQCCheckCompletenessL.egllliltyCheclledBy/Personnel((SiQnature/Date)71of90BakeOvenBaghouseAlcoaMethod4075A-TFRun2Method4075A·TFDataSheetIRunNo.2IDateIEqui_.IDColCanslontlReagBoxSamp.bollA,-'UmbocalMotetbox16116ySlaCkTCcReadotneclitBagPilOt1'0029c,OrsatPumpNozzle0.113o"..-EstMoisturegmH,O72.4M31.8B,.meas4.818.06129-613012011IIJobtNW11AUNT109c-p,.MidPOol38.411Vacuum12121.043lnMDGM1.6811FlnaiDGM0.14Leoll-0.0100.0100.113!Pnot%C01%0,ist.ckTCB,.satFo-IF.-IU.28.481...29.01VelocityVelocityStackOryGuMeterOnliceProbeOvenFdterEx1tlrnplng.PumpTempTemperalUrePressureTemp. Temp.TempTe""4'.VacNotes&P•FInletOutletHinH2(•F•F•F•FHg1.38 1.17...!!!__78780.17240NANA512.0-·---------------------r--!,;1§__!:)_!;__r-21877770.16___lli__.J!A_,2.01.301.142187777--0.16NANA502.0__1.12_7576__!1-..!L_.••.•.241__!!L__.!:!!__2157475,.____!!,_!!i__......ML...__NA_2.0-11021473740.14240NA_NA502-1.1710821473_740.14240NA_21--11021373740.15240NANA4 21.40118r-2127474_0.17241NANA4_2-1.3911821274_740.17239NANA4!_2.-__El_117213_7374!-0.17240NANA492......!d!!__11421473730.16240NANA52.11221472730.15241NANA492.__!J.l_110216_73 73!-0.15240NANA42..._H.L11321772720.16240NANA5-2.-.11221872 720.1.!_240NANA_4- --·--------·-··------1-·--·M-------·-·----·-----·-···----··-----M··-·---------·--------·-·-·-·-----·--·--------·-1----------·---·---·--··--·----··---I-1-----------·--------··------------------·-·---·--·r----·------·------·---·_,__--r-----------·---·---·---··-·--·-----·------r-·--·-------------------r----------I-·-------·-----------·-----------------·------·---1---·-----Iuesol11331I2151I739I74.4I0.156IMaxm:JPar1lculateConteniSVol.-Pre.-.gainlaramslblhrarfscllb/MUIIU(mUg)(mUg)(mUg)flail10.1NNaOH100785.9728.257.7....20.1NNaOH100779.3778.31.0'-*,M,0592.7591.71.0T_.4SG200902.3889.812.7fAV__Reasonablenes!v--E•10PlantAlcoaWorksAddressFemdale,WALocationBakeOvenBaghouaePersonnelSBMIPC/PHIDDF%Moisture5.22Meas---Pa."'"'lg29.75P...JetnH,O----(1.18---KtKtorFiltertcAltarW\.TraverseElapsedTomeOockGasPointInMinutesTimoMetorNo.BeginEnd24hrReadongW-110.018.84:12:00431.531--------··--·-·-L·--·436.750637.556.3440.659__s__....1!:.0445.18947509384495753938]112545393021125j131.345818911504825106-111500188848878271888187.5-471480-61875208347615552063225481000-422502434654113243.8_28248998922825281495210--12813311!!._4995103000r504214I-t-i--·---------1-----------+------.----·--·--·-----------·-------·----1--·-----FinalI8:28504.214SumoravgI3oo.oII72o883.......102.5Yqa1.057l,..._v....-.i"75.2250cilcln2.130FlowM.-oI79.13.,.1135,142.0I1OA/OCCheck/IILegibilityChockedI/1Ib:.....D/272of90BakeOvenBaghouseAlcoaMethod4075A-TFRun3Method4075A-TFDataSheetIRunNoo3(DateIEquipmentIDCalConotantaRoagBoxSarnpboxA,tod.'lumbocalMaterbo•1696yfStackTCcReadOutTodlarBagPrtotP002Vc,Iars••PumpNzze0.113DNinlnchMEslMoisturegmH,O87.81131.2B,.maas5.218.1613012011JIJobIJNW11ALINT109ChocksPreMidPost38.41Vacwm15151.043lniiDGMueaFinalDGM0.84LHI<role0.0090.0050.113,Ito!%CO,Nozzle%0,TCB,salFO=IF..IM.28.381...2B.MVelocilyVelacllyStackDryGasMolerOrifoceProbeOvenFiherElcitlmping.PumpTempTemporaturoPressureTemp.Temp.TempTemp.VacNotesb.P'FInletOuUel1M!inH,C'F'F 'F•FHg1.601261-21863630.19242NANA501.0i----·-1.821.272188463___N_L___ll!_480__!.01.571252186464-__240NANA481.01.501.222196584--...._0.18-_NA481.0145_____h!_986,_O,.!L.......___.....£_r-!,!!..139-.....!.L.08889___9.:.!!....•.0__NA.•_...£__!:!!_,.-01.1--...17089_cg?_____NA__NA481.0140-__.!:.L_-72690.17241NA NAr-!:!!160-....!:.L37071.__!!:!L.....NA_!I!__r-!:!!r161!1.27.!__73_!!.20___i-..,1!1____NA491.01-1.50-7271·--·___!!:.!.!____ill____M.___r-!:Lr--1.51.247271,__...!!.:!!._241NANA50......!:!!.....1o60107472__,1.01.5274 73__!)....!!.___!:9.1.50..097473____g..J!........___NA___..l!L._.....§L_1:9.r1601.237573---·_.....245NANA59__!:!'-r-·-------·M_M_··----_.._____-·------r--r----w•••----··--·-·-·--··---·-·--·--·--·---·-·--·-r---1-----__.._··-·-·--------·-i-------·----·---r---··-·---------·-·-------·--t-··------r----------r-----r------Iu2solu34s12125I698I69.0I0.186IMax[TI]mDinValPaatPreContentaNetgaingramslblltrgr/scflbiiiiiiBtu(mUg)(mUg)(mUg)Frvnt10.1NNaOH100830.8760.470.4·a.ct20.1NNaOH1007291728.20.9a""0649.664880.84SG200892.9877.215.7IIAccuracy-fJn,'i/1u-'--'J.---Reasonableness'Ak_j£-fteam...-E-11OLDEN73of90AirQualityTestReportAPPENDIXFProcessData

## 74 of 90 

# Paula Metz From: Sent:



## Bilskis, Patricia

A. (Patricia.Bilskis@alcoa

. com] Tuesday,

July 26, 2011

10

: 33 AM To:



## Paula Metz Subject:



## FW: Production

data for June 2011

# PaulaBelow

is the production

data for the source tests that was conducted

at Intalco's Bake Oven Scrubber

at the end of June. Thanks Trish 

# From: Nordlund, Roger

A. 

# Sent: Friday, July 22, 2011 9:04AM 

# To: Bilskis, Patricia

A. Cc: Morgan, Scott 

# Subject:

RE: Production

data for June 2011 Patricia, During

the compliance

test on C7, we had

7 fires going.

To feed these

7 fires,
we introduce green anode into the furnace

at

a rate of: 608.7lbs/green carbon*

216 carbon/fire*

0

. 94 (fraction actually packed)*

7 fires/day

= 865,133 lb/day

= 25,953,994 lb/month

or 12,977 tons/month for 30 day month (June) We operated

30 days/June

* 24 hours/day=

720 hours

in June 1""'GOLDEN75of90AirQualityTestReportAPPENDIXGLaboratoryData76of90GoldenSpecialtyLabNo.:Project:GSL110666AlcoaIntalcoPreparedfor:PaulClarkGoldenSpecialty931SeacoCourtDeerPark,TX77536931SeacoCourtDeerPark.TX7'75361of11ReportDate:7/27/2011(II)Ph:(281)476-4769Fax:(281)476-9876/PaulClark931SeacoCourtDeerPark,TX7753677of90GoldenSpecialtyProjectID:AlcoaIntalcoGSLOrderID:GSL_110666ReportDate:7/27/2011ThesamplessubmittedundertheabovereferencedprojectnameandidentifiedbyourGoldenSpecialtylaboratoryordernumberhavebeenanalyzed,andthedataisenclosed.OnlyresultsforsampleslistedontheoriginalChainofCustody(atendofreport)areincludedinthisreport.Rawdataandsubcontractdata,ifapplicable,areattachedtothisreport.Resultsprovidedinthisreportrelateonlytothesamples.Allsampleswillbeproperlydisposedofwhenfinalreportissubmittedunlessotherarrangementshavebeenmade.Samplesputonholdorheldincanistersduetoclientissueswillincurweeklycanisterrentalfees.GoldenSpecialtyreservestherighttoreturnanyunusedsamplesduetohazardoussamplematrices.Rawdataandfinalreportswillbefiledforfiveyearsunlessotherwiserequestedbyclientorregulatorymandates.Toprotecttheintegrityandcompletenessofthisreport,itmustremainattachedtothiscoverletter.Icertifytothebestofmyknowledgeallanalyticaldatapresentedinthisreporthasbeencheckedforcompletenessandaccuracy,andisfreeoferrors.Anydeviationsfromthestatedanalyticalprotocolsduetosamplematrixhavebeendocumentedinthelaboratorynarrativeofthisanalyticalreport.Unlessotherwisenoted,anyanalysisperformedbyGoldenSpecialtyfallswithinthescopeofourNELACaccreditationandmeetsallNELACrequirements.WethankyouforselectingGoldenSpecialtytoserveyouranalyticalneeds.Ifyouhaveanyquestionsconcerningthis report,pleasefeelfreetocontactusatanytime.Respectfully,ScottSwiggardLaboratoryDirectorTlusanalyhadrtpOrtanddataIISS«IIJitdluubttnrrorrwedandpupartdsptcrficailyforyoudatapackstgtrtprtstntstiltbtstaualyhcalar1dltchnrcaljudgmnllandmtnprrtahon5ofourpnsmurri,rnaccordanctwrththtGoldmSpmaltyl.slboratoryQu11htyAssuranctMmrualGoldrnSptcialtyInc.assumtsnorrsponsilnlrtyfortilttndustoftinsdoeurntntoranypornontxtractrdfrmnrtUnltssrtr·othrrw!Stagrttdupon.111wntmg,andpnortoaualyhcalwork,GoldtnSptcialtyInclrabilitymaynotacttdtiltarnountmvorctdforthrsordtr931SeacoCourtDeerTX'77596GSL_tt0666Ph:(281)476-Fax:{281)476-98762of11I78of90ReportDate:7/27/2011LaboratoryNarrativeEPAMethod315:VolumesreportedfortheMCEMportionsofContainer2aretakenfromtheContainer2Mvolumesofthesamerun,andvolumesreportedfortheMCEMportionsofContainer1reflectthevolumeofmethylenechlorideusedforthefilterextraction.TheWashingtonDepartmentofEcologydoesnotcurrentlyofferaccreditationforEPAMethod315.Respectfully,ScottSwiggardLaboratoryDirector17rrsanalyhcalrtporlanddtltaassocr11ttdluubttnrtvitwtdandprtpartdspecificallyfor11wdab!pGclcslgttlztbtstttntllyticalandttchnictzlandintnprttationsofourmaccorrlmretwrtlrthtGoldnrSpmaltyLAboratoryQu11lityAssurGnaMDnualGoldnrSpmtdtyIncass&nnN110rrsponsrbdrtyfortltttndustofthisdocumtutorauyportio11t:rtracttdfromit.UnltSsrfuagrttd11pon.111wnhng,audpnortoanalyhcalwork.Goldtl1SprcudtyIncliabrhtymaynotacmlllrtamountmvorctdfortinsordtr931SeacoCourtDeerPark,TX17536GSL_ll0666Ph:@)476-4769Fax:(281)476-98763of11

# 79 of 

# 90



# Report Date: 7/27/2011 

# Laborat0ry Analysis Report Client Name: Golden Specialty 

# Source Sampled:

Bake Oven Baghouse Stack 

# Test: Order
ID: Determination

of PM and MCEM

by EPA Method

315 GSL

_ 110666 

# Sample Analyst:

Hari Pandi 

# Date Sampled: 6/29/2011 Date Analyzed: 7/25/2011 Analytical
SOP: GSL

_ TM030 

# Instrument

ID: QCBatchiD:

Balance

#1 -Sartorius QC

_ 02811 SampleiD Run

1 Filter

- Cont.

1 Run

1 Filter- Cont.

1 Run

1 Acetone Rinse- Cont.

2 Run

1 Acetone Rinse

- Cont.

2 Run

1 BH D1 Rinse

- Cont. 3W Run

1 BH Ace/DCM-
Cont.

35 

## Sample Number -001 -001 -002 -002 

### -004 -005 

## Parameter PM MCEM PM MCEM MCEM MCEM 

## Container Filter 969 Tin 1129 Tin1112 Tin 1132 Tm 1116 Tin 1119



### PM

• Particulate Matter MCEM

"' Methylene Chloride Extractable Matter 

## Sample

Tan



## Post Test Result



# (g) Volume
(ml) 

## Weight



## (g) Weight



## (g) N/A

0

. 3543

0

. 3541

< 

### 0

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2

. 6204

2

. 6207

0.0003 

### 72
2.6406

2

. 6460

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2.6348

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. 6379

0.0031 320
2.6579

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. 6574

< 

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### 1180of90ReportDate:7/27/2011La}!)oratoryAnalysisReportClientName:GoldenSpecialtySourceSampled:BakeOvenBaghouseStackTest:OrderID:SampleAnalyst:DateSampled:DateAnalyzed:AnalyticalSOP:InstrumentID:QCBatchID:SampleJ!DDeterminationofPMandMCEMbyEPAMethod315GSL_110666HariPandi6/30/20117/25/2011GSL_TM030Balance#1-SartoriusQC_02811SampleParameterContainerSamplePM=ParticulateMatterMCEM=MethyleneChlorideExtractableMatterTarePostTestResult(g)NumberVolume(ml)Weight(g)Weight(g)Run2Filter-Cont.1Run2Filter-Cont.1Run2AcetoneRinse-Cont.2Run2AcetoneRinse-Cont.2Run2BHDIRinse-Cont.3WRun2BHAce/DCM-Cont.35-006-006-007-007-009-010PMMCEMPMMCEMMCEMMCEMFilter970NfATin1128100Tin1110102Tin113052Tin1117410Tin11211000.35460.3539<0.00012.63702.63710.00012.63512.6346<0.00012.61562.61580.00022.62372.6235<0.00012.66582.66710.0013TiristnJQlyhcalrtporttmddsltDllSSOCJtJkdluzsbmrmntwtdandprtpllrtdsptcificallyforyouTittdatapacbgtrrprtSenfstilebtst11nalyhcalandttcJnuctJIJ''dgmentandmtnprtrationsofourprrsmmtl,inaccordsmctuntlrthLGoldnrSpmaltyUbortlloryQualityA..ssuranctManualColdnrSptcrllltyIncrnurntSnortsponSlbtlrtyfortlwtndofthl$d«umnrt01'anyporhontxtrGcttdfromit.Unltssitisllgrttdupon,mwrihrrgandpriOrtoamzlyhcalwork.ColdtnSptcialtyInclrabthtymaynottXcttdtlttamountrnvozudfort/usordtr931SeacoCourtDeerPark,TX77536GSL_l10666Ph:(281)!76-4769Fax:'(281)4116-98765of1160DE81of90LaboratoryAnalysisReportClientName:GoldenSpecialtyReportDate:7/27/2011SourceSampled:BakeOvenBaghouseStackTest:OrderID:SampleAnalyst:DateSampled:DateAnalyzed:AnalyticalSOP:InstrumentID:QCBatch10:SampleiDDeterminationofPMandMCEMbyEPAMethod315GSL_110666HariPandi6/30/20117/25/2011GSL_TM030Balance#1-SartoriusQC_02811SampleParameterContainerSmlplePM"ParticulateMatterMCEM"MethyleneChlorideExtractableMatterTarePostTestResult(g)NumberVolume(ml)Weight(g)Weight(g)Run3Filter-Cont.1Run3Filter-Cont.1Run3AcetoneRinse-Cont.2Run3AcetoneRinse-Cont.2Run3BHDlRinse-Cont.3WRun3BHAce/DCM-Cont.35-011-011-012-012-014-015PMFilter971MCEMTin1127PMTin1111MCEMTin1131MCEMTin1118MCEMTin1124N/A0.35360.3535<0.00011002.63002.63030.0003782.57522.5751<0.0001502.62792.62800.00014802.63352.6331<0.00011422.63362.63560.0020Tinsanalyhalrrportandd12taassoaattdl1asbm1rtVJtwedandprtpartdsptcrficaUyforyouTiltdatapacblgtrtprtSt'tlfstJJtbtstmuzlyha:Jandtuhr1rctJIJUdgmntfandrt1trrprttahonsofourptrsonntl111accord4nctw1thtlztColdtnSptCUZityLAboratoryQualrtyAssurauctManualColdn1Sp«1altyIncassumtsnorrsponsrb:l1tyfortilttndofthasdocumCJtoranyportrontxtracttdfrom11Unless1ft.sagrudupm1,inwnhng,tzndpnorto12nalyhc11lwork,ColdmSptCJaltyInclttJbllztynottxutdtht«mountmvozctdforthiSorder931SeacoCourtDeerPark,TX'7'7536Ph:(ml476-4769Fax:476-98766of11Test:OrderID:SampleAnalyst:DateSampled:DateAnalyzed:AnalyticalSOP:82of90LaboratoryAnalysisReportClientName:SourceSampled:GoldenSpecialtyField BlanksDeterminationofPMandMCEMbyEPAMethod315GSL_110666HariPandi6/30/20117/19/2011GSL_TM030ReportDate:7/27/2011InstrumentID:Balance#1-SartoriusPMaParticulateMatterQCBatchID:QC_02811MCEM=MethyleneChlorideExtractableMatterSulpleiDFieldReagentBlankAcetoneFieldReagentBlankDCMSulpleParameterNumber-016PM-017PMContainerSampleVolume(ml)Tin1125198Tin1120200TareWeight(g)2.62772.6527PostTestWeight(g)2.62782.6521Result(g)0.0001<0.0001ThiSanalyhcalrtporland.UtaassoetaltdIUJSb«trmlitwtdQndprtpartdspmfictJIIyforyouThtdAtap12cbgtrtprnt'nf..thtbtsttn112lytiadandteclnzrctJIand1nkrprdahmrsofourptrsonntl.inaccordanctwrththtGoltknSpmaltyl.i:boratoryQualrtyAssuran«Maru.urlColdnzS/HcudtyIncIIS5umtsnorrsponsrbdrtyforthtoftlusdocurntntoranyportiontXtrtJcttdframrtUnitS$11ISotlwrwistagrttdupon,mwnhng,andpnortotmalyhCtJIwork.GoldnaSptcittltyInclitlbtlrtymaynottxcttdamountmvorctdfortimordtr931SeacoCourtDeerPar}<,TX77536GSL_l10666Ph:(281)476-4769Fax:(281)476-98767of1183of90LaboratoryAnalysisReportQualityControlInformationMethodBlankAnalysisTest:Analyst:DateAnalyzed:Instrument10:QCBatch10:Mahix:ParameterAcetoneBlankDichloromethaneBlankDe-ionizedwaterBlankFilterMCEMBlankDeterminationofPMandMCEMbyEPAMethod315HariPandi7/19/2011Balance#1-SartoriusQC_02811LiquidVolume(ml}505050100Tare,WeightPostTestWeight(g)(g)2.62642.62592.5830258232.62202.62222.629726297ReportDate:7/27/2011BlankResult(g)<0.0001<0.00010.0002<0.0001Tinsanalyhcalrqxn-t4nddAtaas50CUittdhasbMrrnntWtd11ndsptet.ficalfyforyou.Utapacbgttlrtbt-stamzlyhclllaudttclmiC41andmtnprtttJhonsofourptrsmmtl,inaccordanuwrthtlrtGoldnrSptctaltylAboratoryQutdrtyAssurarraManualGoldtuSpteudtyInca55urntsnortsponsrf"lltyfaTthentdIJJeofth15documnrtoranyporhont:rtnlcttdfromtlUnit$$ttrsagrttdupon,mwnhngandpnortoanalyticalworlGoldmSptcuzltyInclu1btlrtymt1!fr1ott:xcttdtlaeamountmootctdfortlusordtr931SeacoCourtDeerPark.TX7'1536Ph:(281)476-4769Fax:@)476-98768of1184of90ILal!JoratoryAnalysisReportDataQualifiersandFlagsoMQL-MethodQuantitationLimitoJ 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