Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis

Location: Mountaineer Plant Report Date: 3/5/2012

Sample Number:120833-001 Date Collected:02/22/2012 07:45 Date Received:2/22/2012 

## CPS Effluent

Units Parameter Result RL Analysis By Analysis Date/TimeMethod MDL Data Qual mg/L Ammonia, NH3, as N 4.00 0.05 DMM EPA 350.1 0.01 02/27/2012 mg/L Alkalinity, as CaCO3 228 5 WKE SM20 2320B 1 02/23/2012 mg/L Chemical Oxygen Demand, COD 48.8 5 WKE SM20 5220D 1 02/24/2012 mg/L Nitrate, NO3 as N 19.9 6 KLG EPA 300.1 1 02/23/2012 mg/L Orthophosphate, PO4 as P < 5.00 20 KLG EPA 300.1 5 02/23/2012 U



### Sample Number:120833-002 Date Collected:02/22/2012 07:45 Date Received:2/22/2012 

### Leachate Effluent

Units Parameter Result RL Analysis By Analysis Date/TimeMethod MDL Data Qual mg/L Ammonia, NH3, as N 4.05 0.05 DMM EPA 350.1 0.01 02/27/2012 mg/L Alkalinity, as CaCO3 550 5 WKE SM20 2320B 1 02/23/2012 mg/L Chemical Oxygen Demand, COD 27.1 5 WKE SM20 5220D 1 02/24/2012 mg/L Nitrate, NO3 as N 9.05 6 KLG EPA 300.1 1 02/23/2012 mg/L Orthophosphate, PO4 as P < 5.00 20 KLG EPA 300.1 5 02/23/2012 U



### Sample Number:120833-003 Date Collected:02/22/2012 07:45 Date Received:2/22/2012 

### 1st Stage Feed

Units Parameter Result RL Analysis By Analysis Date/TimeMethod MDL Data Qual ug/L Selenium, Se 404 0.5 DPC EPA 200.8 0.1 03/01/2012 11:23 mg/L Ammonia, NH3, as N 3.77 0.05 DMM EPA 350.1 0.01 02/27/2012 mg/L Alkalinity, as CaCO3 129 5 WKE SM20 2320B 1 02/23/2012 mg/L Chemical Oxygen Demand, COD 26.8 5 WKE SM20 5220D 1 02/24/2012 mg/L Nitrate, NO3 as N 14.2 6 KLG EPA 300.1 1 02/23/2012 mg/L Orthophosphate, PO4 as P < 5.00 20 KLG EPA 300.1 5 02/23/2012 U

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### Sample Number:120833-004 Date Collected:02/22/2012 07:45 Date Received:2/22/2012



### 2nd Stage Feed

Units Parameter Result RL Analysis By Analysis Date/TimeMethod MDL Data Qual ug/L Selenium, Se 37.9 0.5 DPC EPA 200.8 0.1 03/01/2012 11:37 mg/L Ammonia, NH3, as N 4.43 0.05 DMM EPA 350.1 0.01 02/27/2012 mg/L Alkalinity, as CaCO3 171 5 WKE SM20 2320B 1 02/23/2012 mg/L Chemical Oxygen Demand, COD 30.9 5 WKE SM20 5220D 1 02/24/2012 mg/L Nitrate, NO3 as N < 1.00 6 KLG EPA 300.1 1 02/23/2012 U mg/L Orthophosphate, PO4 as P < 5.00 20 KLG EPA 300.1 5 02/23/2012 U



### Sample Number:120833-005 Date Collected:02/22/2012 07:45 Date Received:2/22/2012 

### Bioreactor Effluent

Units Parameter Result RL Analysis By Analysis Date/TimeMethod MDL Data Qual ug/L Selenium, Se 320 0.5 DPC EPA 200.8 0.1 03/01/2012 12:25 mg/L Ammonia, NH3, as N 3.69 0.05 DMM EPA 350.1 0.01 02/27/2012 mg/L Alkalinity, as CaCO3 475 5 WKE SM20 2320B 1 02/23/2012 mg/L Chemical Oxygen Demand, COD 28.3 5 WKE SM20 5220D 1 02/24/2012 mg/L Nitrate, NO3 as N 16.9 6 KLG EPA 300.1 1 02/23/2012 mg/L Orthophosphate, PO4 as P < 5.00 20 KLG EPA 300.1 5 02/23/2012 U

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.com Tel. 614-836-4224 Fax 614-836-4168 Audinet 210-4224

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