## Testing Data - Inlet

Copy this worksheet as necessary for pollutants/compounds sampled on different dates. For multiple facilities, process units, or control devices, users may copy this worksheet within this workbook. Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.

**PVC Facility Name:**

**Process Unit ID:** P-1 **Process Equipment ID / Control Equipment ID:** VGA **Process Equipment / Control Equipment Description:**

**Parameter CAS Number**  **Sample #1 Sample #2**  **Sample #3 Units**  **Test Method Used PVC Process Only**  **Note(s)**

Enter the CAS number for each pollutant/compound. Do not include dashes. Select appropriate unit from list. Enter the name of the Test Method used. Indicate whether the inlet to the control device and where the inlet sampling occurred is from the PVC process only (dedicated) or from the PVC process and another process unit (non-PVC) (shared) For all pollutants/compounds, provide any other information supporting information you think is necessary about this test report.

Sample Date (mm/dd/yy) 01/08/10 01/08/10 01/11/10 **Required Operating Parameters During Test** Total Heat Input (MMBtu/hr) MMBTU/hr (select) Fuel 1 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) Fuel 2 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) Fuel 3 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) **Other Inlet/Outlet Stream Operating Parameters During Test** Flow Rate 0.093 0.0869 0.0903dscmm Temperature 0.83 0.28 

### -2.2deg C Moisture 0.0063 0.006 0.0049% O2 2.82 2.7 2.4% CO2 29.4 26.3 34.8% CH4 

### [<3.23E-02] [<5.72E-02] [<3.28E-02] ppmvd @ 3% O2 **Testing Data** Compound (list) CAS Number Chloromethane 74-87-3 8.12E+04 7.59E+04 1.02E+05ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90 (select) Vinyl Chloride 75-01-4 5.28E+05 5.62E+05 4.33E+05ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90 (select) Chloroethane 75-00-3 1.07E+03 1.67E+03 6.85E+02ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90 (select) VOC - Other 592-27-8 1.90E+02 1.48E+00 5.63E-01ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90 (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

(e.g., [< 0.010]). Polyone Corporation--Pedricktown, NJ

## Testing Data - Outlet

Copy this worksheet as necessary for pollutants/compounds sampled on different dates. For multiple facilities, process units, or control devices, users may copy this worksheet within this workbook. Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.

**PVC Facility Name:**

**Process Unit ID:** P-1 **Process Equipment ID / Control Equipment ID:** VGA **Process Equipment / Control Equipment Description:**

**Parameter CAS Number**  **Sample #1 Sample #2**  **Sample #3 Units**  **Test Method Used PVC Process Only**  **Note(s)**

Enter the CAS number for each pollutant/compound. Do not include dashes. Select appropriate unit from list. Enter the name of the Test Method used. Indicate whether the inlet to the control device and where the inlet sampling occurred is from the PVC process only (dedicated) or from the PVC process and another process unit (non-PVC) (shared) For all pollutants/compounds, provide any other information supporting information you think is necessary about this test report.

Sample Date (mm/dd/yy) 01/08/10 01/08/10 01/11/10 **Required Operating Parameters During Test** Total Heat Input (MMBtu/hr) MMBTU/hr (select) Fuel 1 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) Fuel 2 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) Fuel 3 (select) Feed Rate MMBTU/hr (select) HHV BTU/scm (select) **Other Inlet/Outlet Stream Operating Parameters During Test** Flow Rate 0.0435 0.0373 0.0501dscmm Temperature 0.83 0.28 -2.2deg C Moisture 0.0063 0.006 0.0049% O2 19.2 18.6 18.4% CO2 0.0947 0.44 5.45% CH4 [<3.96E+02] [<4.36E+02] [<4.47E+02]ppmvd @ 3% O2 **Testing Data** Compound (list) CAS Number Chloromethane 74-87-3 [<3.33E+00] [<2.36E+00] [<2.23E+00]ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90(select) Vinyl Chloride 75-01-4 [<3.36E+00] [<2.38E+00] [<2.25E+00]ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90(select) Chloroethane 75-00-3 [<1.50E+00] [<1.07E+00] [<1.00E+00]ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90(select) VOC - Other 592-27-8 3.05E+04 1.87E+04 2.63E+04ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90(select) Hydrochloric Acid 7647-01-0 [<1.51E+00] [<1.24E+00] [<1.21E+00]ppmvd @ 3% O2 EPA Method 18/ASTM Method 1946-90(select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) (select units) (select) Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

(e.g., [< 0.010]). PolyOne Specialty Resins Group - Pedricktown Plant

# Testing Data (Dioxins / Furans) - Outlet

Copy this worksheet as necessary for pollutants/compounds sampled on different dates. For multiple facilities, process units, or control devices, users may copy this worksheet within this workbook. Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.



# PVC Facility Name:

**Process Unit ID: Process Equipment ID / Control Equipment ID:**  **Process Equipment / Control Equipment Description:**

**Parameter CAS Number**  **Sample #1**

Enter the CAS number for each pollutant/compound. Do not include dashes.



# Sample Date (mm/dd/yy) **Required Operating Parameters During Test** Total Heat Input (MMBtu/hr) Fuel 1 Feed Rate HHV Fuel 2 Feed Rate HHV Fuel 3 Feed Rate HHV **Other Inlet/Outlet Stream Operating Parameters During Test** Flow Rate Temperature Moisture O2 CO2 CH4 **Testing Data** Compound (list) CAS Number 2,3,7,8-TCDD Other TCDD 1,2,3,7,8 PeCDD Other PeCDD 1,2,3,4,7,8 HxCDD 1,2,3,6,7,8 HxCDD 1,2,3,7,8,9 HxCDD Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

# Other HxCDD

1,2,3,4,6,7,8 HpCDD Other HpCDD 1,2,3,4,6,5,7,8 OCDD 2,3,7,8-TCDF Other TCDF 1,2,3,7,8 PeCDF 2,3,4,7,8 PeCDF Other PeCDF 1,2,3,4,7,8 HxCDF 1,2,3,6,7,8 HxCDF 1,2,3,7,8,9 HxCDF 2,3,4,6,7,8 HxCDF Other HxCDF 1,2,3,4,6,7,8 HpCDF 1,2,3,4,7,8,9 HpCDF Other HpCDF 1,2,3,4,6,5,7,8 OCDF TOTAL

## Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.



# Sample #2 **Sample #3 Units**  **Test Method Used**

Select appropriate unit from list. Enter the name of the Test Method used.



# MMBTU/hr

MMBTU/hr BTU/scm

MMBTU/hr BTU/scm

MMBTU/hr BTU/scm

dscmm deg C % % % ppmvd @ 3% O2

ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

(e.g., [< 0.010]).

# ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2

# PVC Process Only **Note(s)**

Indicate whether the inlet to the control device and where the inlet sampling occurred is from the PVC process only (dedicated) or from the PVC process and another process unit (non-PVC) (shared) For all pollutants/compounds, provide any other information supporting information you think is necessary about this test report.



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# Testing Data (PCBs) - Outlet

Copy this worksheet as necessary for pollutants/compounds sampled on different dates. For multiple facilities, process units, or control devices, users may copy this worksheet within this workbook. Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.



# PVC Facility Name:

**Process Unit ID: Process Equipment ID / Control Equipment ID:**  **Process Equipment / Control Equipment Description:**

**Parameter CAS Number**  **Sample #1**

Enter the CAS number for each pollutant/compound. Do not include dashes.



# Sample Date (mm/dd/yy) **Required Operating Parameters During Test** Total Heat Input (MMBtu/hr) Fuel 1 Feed Rate HHV Fuel 2 Feed Rate HHV Fuel 3 Feed Rate HHV **Other Inlet/Outlet Stream Operating Parameters During Test** Flow Rate Temperature Moisture O2 CO2 CH4 **Testing Data** Compound (list) CAS Number 3,3',4,4'-Tetrachlorobiphenyl 3,4,4',5-Tetrachlorobiphenyl 2,3,3',4,4'-Pentachlorobiphenyl 2,3,4,4',5-Pentachlorobiphenyl 2,3',4,4',5-Pentachlorobiphenyl 2,3',4,4',5'-Pentachlorobiphenyl 2,3,3',4,4',5-Hexachlorobiphenyl Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

# 3,3',4,4',5-Pentachlorobiphenyl

2,3,3',4,4',5'-Hexachlorobiphenyl 2,3',4,4',5,5'-Hexachlorobiphenyl 3,3',4,4',5,5'-Hexachlorobiphenyl 2,3,3',4,4',5,5'-Heptachlorobiphenyl TOTAL

## Facility names, Process Unit IDs, Process Equipment IDs, and Control Equipment IDs must match those used in your section 114 survey response. When completed, submit this workbook containing reporting spreadsheets for all process units and control devices according to the instructions in the section 114 letter, Enclosure 1.



# Sample #2 **Sample #3 Units**  **Test Method Used**

Select appropriate unit from list. Enter the name of the Test Method used.



# MMBTU/hr

MMBTU/hr BTU/scm

MMBTU/hr BTU/scm

MMBTU/hr BTU/scm

dscmm deg C % % % ppmvd @ 3% O2

ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 Enter numerical value when available. If the test results are below detection limit, please note the detection limit in brackets

(e.g., [< 0.010]).

# ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2 ng/dscm @ 3% O2

# PVC Process Only **Note(s)**

Indicate whether the inlet to the control device and where the inlet sampling occurred is from the PVC process only (dedicated) or from the PVC process and another process unit (non-PVC) (shared) For all pollutants/compounds, provide any other information supporting information you think is necessary about this test report.



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