Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

April 2009 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 6

1.1 Project Objective .............................................................................................................. 6

1.2 Previous Reports .............................................................................................................. 6

1.3 Background ...................................................................................................................... 7

1.3.1 Site Description ......................................................................................................... 7

1.3.2 Facility Information .................................................................................................. 7

1.3.3 UST Information ....................................................................................................... 7

1.4 Previous Environmental Investigations ............................................................................ 7

1.5 Regulatory Updates .......................................................................................................... 9

2.0 Sample Collection and Analyses ........................................................................................ 11

2.1 Monitoring Well Purging ............................................................................................... 11

2.2 Groundwater Sample Collection .................................................................................... 11

2.3 Groundwater Sample Analyses ...................................................................................... 11

3.0 Groundwater Sample Analytical Results ........................................................................... 12

3.1 February 2009 Sample Analytical Results ..................................................................... 12

3.2 Groundwater Contaminant Trend ................................................................................... 14

3.3 Results of Oil/Water Interface Measurements ............................................................... 15

3.4 Groundwater Status ........................................................................................................ 15

4.0 Summary and Conclusions ................................................................................................. 18

5.0 References .......................................................................................................................... 22

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..13 

Table 2 Oil/Water Interface Measurements ..............................................................................15 

Table 3 Action Levels for Compounds of Concern ..................................................................16 

Table 4 Responses to Groundwater Monitoring Results ..........................................................16 

List of Figures 

Figure 1 TPH Trends in Groundwater, Round 14 (February 4, 2009) .......................................20 

Figure 2 PAH Trends in Groundwater, Round 14 (February 4, 2009) ......................................21 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
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Red Hill Fuel Storage Facility April 2009 

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Executive Summary 

This Quarterly Groundwater Monitoring Report presents the results of groundwater sampling 

conducted on February 4, 2009 at the United States (US) Navy Bulk Fuel Storage Facility at Red 

Hill, Oahu, Hawaii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) 

for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This report is part of 

a series of quarterly groundwater monitoring reports provided by the US Navy to the State of 

Hawaii Department of Health (HDOH) in accordance with HDOH’s release response 

requirements. Currently, there are 18 active and 2 inactive, 12.5 million gallon, field-constructed 

underground storage tanks (USTs) located at the Facility. 

Background 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility had migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. The US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from 

the Red Hill Fuel Storage Facility and provides approximately 24 % of the potable water to the 

Pearl Harbor Water System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility lower access tunnel, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility at ground surface adjacent to the US 

Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 

infiltration gallery (RHMW2254-01). 

All five wells were sampled twice as part of a comprehensive environmental investigation and 

risk assessment (TEC, 2006). For this investigation, groundwater samples were analyzed for 

petroleum constituents and compared against HDOH Drinking Water Environmental Action 

Levels (EALs) (HDOH, July 2005). In addition, a three-dimensional (3-D) groundwater model 

was developed to produce site-specific risk-based levels (SSRBLs) for compounds of concern. 

The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest 

risk to the US Navy water supply, due to its mobility and toxicity. Finally, the model indicated 

that a non-aqueous plume (free product) of JP-5 must migrate to within 1,100 feet of the US 

Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded within the gallery. 

Based on this, free-product must be observed at RHMW01 for EALs to be exceeded at the US 

Navy Well 2254-01. 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was each previously 240 g/L, assuming they were not carcinogens. 

Evidence that they are carcinogenic to humans has now been accepted by the US Environmental 

Protection Agency (USEPA), and HDOH adopted more rigorous EALs of 4.7 g/L for 1-

methylnaphthalene and 24 g/L for 2-methylnaphthalene (HDOH, 2008). 
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The drinking water EAL for naphthalene was also updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels (HDOH, 2008). 

Finally, the drinking water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, 

although the gross contamination EAL for TPH-DRO remains 100 g/L. 

Groundwater Protection Plan 

In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater 

Protection Plan (TEC, 2008), which specified SSRBLs for each well, and actions that would 

occur for the pertinent cases, based on categories for each groundwater monitoring well 

(Categories 1 through 4). The main object of the Plan is to protect groundwater quality entering 

the US Navy Well 2254-01, which provides potable water to the PHWS. This is accomplished 

by comparing petroleum concentrations in the Facility wells (RHMW01, RHMW02, and 

RHMW03) to the SSRBLs and taking the corresponding action. A secondary, but important 

objective of the Plan is to identify leaking USTs by evaluating increasing concentration trends, 

or the sudden and lasting presence of free product in one or more groundwater monitoring wells. 

This quarterly report compares the water quality to these categories and recommended actions. 

Current Results 

On February 4, 2009 four groundwater samples were collected from RHMW01, RHMW02, 

RHMW03 and the US Navy Well 2254-01, along with the required quality control samples 

(duplicate, matrix spike, spike duplicate, trip blank). Samples were analyzed for Total Petroleum 

Hydrocarbons (TPH) quantified as Diesel-Range Organics (DRO) and Gasoline Range Organics 

(GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic Hydrocarbons (PAHs), and 

lead. 

TPH-DRO

TPH-DRO was detected at 387 micrograms per liter (μg/L) in RHMW01, 2,840 μg/L (i.e., the 

average of normal and duplicate samples) in RHMW02, and at 207 μg/L in RHMW03. The 

HDOH Drinking Water EAL and SSRBL for TPH-DRO are 210 μg/L and 4,500 μg/L, 

respectively. 

TPH-GRO

For TPH-GRO the HDOH Drinking Water EAL is 100 μg/L. In samples collected at RHMW01, 

RHMW02, RHMW02D (i.e., the duplicate sample collected), RHMW03, and RHMW2254-01 

estimated values (i.e., values below the laboratory reporting limit, but above the method 

detection limit) were observed at the following respective levels: 14.4 μg/L, 52.3 μg/L, 54.3 

μg/L, 16.1 μg/L, and 14 μg/L. The estimated value of 14 μg/L of TPH-GRO detected at 

RHMW2254-01, which is well below the HDOH Drinking Water EAL of 100 μg/L and just 

above the method detection limit of 10 μg/L was unexpected. Therefore, analytical results will 

be closely monitored during future quarterly groundwater sampling events at RHMW2254-01 to 
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assess whether the detection of trace quantities of TPH-GRO from the February 2009 sampling 

event represents an anomaly or an apparent analytical trend relative to RHMW2254-01. 

Other Parameters

At RHMW02, average concentrations between the normal and duplicate samples were 

determined to be above the HDOH Drinking Water EALs as follows: naphthalene at 42.9 μg/L 

(HDOH EAL is 17 μg/L) and 1-methylnaphthalene at 22 μg/L (HDOH Drinking Water EAL is 

4.7 μg/L). 

The average analytical values of the normal and duplicate samples for 2-methylnaphthalene at 

RHMW02 were 10.8 μg/L. This value slightly exceeds the HDOH Drinking Water Ceiling EAL 

for 2-methylnaphthalene of 10 μg/L. 

It is noteworthy that 1-methylnaphthalene, which was detected at trace quantities (i.e., estimated 

to be 0.03 μg/L) at RHMW2254-01 during the October 2008 sampling event, was not detected 

during the February 2009 sampling event. 

Trend Analysis 

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005, but less than 25 percent of the SSRBL of 4,500 g/L. In February 

2009, TPH-DRO was lower in concentration than the October 2008 sampling event. Prior to the 

October 2008 event, TPH-DRO concentrations had decreased for three consecutive sampling 

rounds. 

At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 and greater than 50 percent of the SSRBL of 4,500 g/L over that 

same period. The average TPH-DRO concentration from the October 2008 sampling event 

increased to above the SSRBL (estimated solubility limit). However, the February TPH-DRO 

concentration dropped below the SSRBL of 4,500 g/L (i.e., average of normal and duplicate 

samples of 2,840 g/L). Three parameters (i.e., naphthalene, 1-methylnaphthalene, and 2-

methylnaphthalene) also have exceeded EALs since September 2005. In October 2008, these 

parameters decreased in concentrations following increasing trends over three previous rounds 

(since January 2008). During the February 2009 sampling event, the decrease continued as all 

three parameter concentrations were less than the respective October 2008 values. There are no 

SSRBLs established for these parameters. 

At RHMW03, concentrations of TPH-DRO have fluctuated around the HDOH EAL since 

September 2005 and are significantly lower than corresponding values observed at RHMW01 

and RHMW02. During the February 2009 sampling event, TPH-DRO at RHMW03 (i.e., 207 

g/L) slightly decreased from the observed October value (i.e., 244 g/L) and was slightly less 

than the newly established HDOH Drinking Water EAL value of 210 g/L. Prior to the 

February 2009 event, TPH-DRO has been increasing in concentration since April 2008. 
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Current Groundwater Status 

Based on the monitoring event that occurred in February 2009, no free product was observed at 

RHMW01, RHMW02, or RHMW03. 

Although TPH-GRO was detected at US Navy Well 2254-01 during the February 2009 sampling 

event, it does not place the well into the Category 1 status. Since no contamination trend (i.e., 

two or more consecutive sampling rounds) has been observed at US Navy Well 2254-01, the 

well does not meet the Category 1 definition. 

Category 1 Status Locations

Based upon the February 2009 sampling event, RHMW03 is presently in Category 1 status, since 

the TPH-DRO value (i.e., 207 g/L) dipped slightly below the HDOH Drinking Water EAL (i.e., 

210 g/L) and this represents a slight decrease in the concentration as compared with the 

October 2008 concentration. Category 1 response for RHMW03 requires: 

1. Quarterly reports to be sent to HDOH. 

Category 2 Status Locations

Results from the February 2009 sampling event indicate that RHMW01 is presently in Category 

2 status, since the TPH-DRO concentration of 387 g/L is greater than the HDOH Drinking 

Water EAL (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated solubility limit of 

JP-5). Category 2 response at RHMW01 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 Status Locations

Results from the February 2009 sampling event indicate that RHMW02 is presently in Category 

3 status (i.e., downgraded from Category 4 status observed during the October 2008 sampling 

event), since TPH-DRO [2,840 g/L and 2,840 g/L (duplicate)] is greater than the HDOH 

Drinking Water EAL (210 g/L), but is between one half and the established SSRBL value of 

4,500 g/L (estimated solubility limit of JP-5). In addition, the HDOH Drinking Water EAL of 

4.7 g/L for 1-methylnaphthalene was exceeded [i.e., 21.2 g/L and 22.8 g/L (duplicate)]. 

Category 3 response at RHMW02 requires: 

1. Send quarterly reports to HDOH; 

2. Initiation of a leak determination program to identify if tanks are leaking; 

3. Increase free product monitoring frequency to once per month (if concentrations 

increasing); 

4. Notify HDOH verbally within 7 days and follow with written notification in 30 days; 

5. Remove sampling pumps, measure product in pertinent wells with interface probe, reinstall pumps if product is not detected; and 

6. Immediately evaluate tanks for leaks. 
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Conclusions and Recommendations 

There is no indication of an imminent threat to the US Navy Well 2254-01 water resources based 

on this report, since petroleum concentrations at RHMW01 remain less than half the SSRBLs. 

Additionally, based upon the February 2009 sampling event, the groundwater status at RHMW02 

is Category 3 (i.e., downgraded from Category 4 status observed during the October 2008 

sampling event) since the concentration of TPH-DRO was greater than the HDOH Drinking 

Water EAL (210 g/L), but was between one half and the established SSRBL value of 4,500 

g/L. The Groundwater Protection Plan requires specific responses to Category 3, which should 

be conducted. 

Although 1-methylnaphthalene was detected at trace quantities (i.e., estimated to be 0.03 μg/L) 

at RHMW2254-01 during the October 2008 sampling event, it was not detected during the 

February 2009 sampling event. An unexpected estimated value of 14 μg/L of TPH-GRO was 

detected at RHMW2254-01; however, this concentration is well below the HDOH Drinking 

Water EAL of 100 μg/L and just above the method detection limit of 10 μg/L. 

 

The US Navy plans to install an additional monitoring well in the Facility lower access tunnel 

and dedicated oil/water interface probes in four lower access tunnel wells in the coming year to 

better monitor contaminant migration in the basal drinking water aquifer. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead will 

continue as previously scheduled until such time that new data indicates that a different schedule 

is warranted. It is recommended that future quarterly analytical results be closely monitored at 

RHMW2254-01 to assess whether the detection of trace quantities (i.e., 14 g/L) of TPH-GRO 

from the February 2009 sampling event represents an anomaly or an apparent analytical trend. 
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1.0 Introduction

This report presents the results of the 14th groundwater sampling and analysis event, conducted 

in February 2009 at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as 

“the Facility”). The Facility consists of 18 active and 2 inactive underground storage tanks 

(USTs) operated by the Fleet and Industrial Supply Center (FISC), Pearl Harbor. The 

groundwater sampling and analysis event is part of a groundwater monitoring program for the 

UST site in response to past UST releases, previous environmental investigations, and 

recommendations from the State of Hawaii Department of Health (HDOH). 

1.1 Project Objective 

This groundwater sampling and analysis project was performed to evaluate the presence of 

chemicals of potential concern in groundwater underlying the Facility. The project was 

conducted to ensure the Navy remains in compliance with HDOH UST release response 

requirements as described in Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release 

Response Action. The groundwater sampling and analysis procedures generally followed the 

procedures described in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan [TEC 

Inc (TEC), 2008 also referred to as “the Plan”]. 

This groundwater sampling and analysis event was conducted by TEC under United States (US) 

Navy Contract Number N47408-04-D-8514, Task Order No. 54. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); and 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009) 
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1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24% of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter sentinel well RHMW01 (previously known as MW-V1D) to 

monitor for contamination of the basal aquifer underlying the Facility. The well was installed 

and completed at approximately 100 feet below grade within the underground access tunnel. At 

the time of well completion, depth to water in RHMW01 was measured at 86 feet below grade 

(Dawson, 2006). 

In February 2001, groundwater samples collected from sentinel well RHMW01 contained total 

petroleum hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (g/L) to 

1,050 g/L and total lead ranging from 10.4 g/L to 15 g/L. The maximum total lead 

concentration in the samples was equal to the primary drinking water standard of 15 g/L for 

lead and exceeded the HDOH Tier 1 groundwater action level of 5.6 g/L (Dawson, 2006). 
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2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 g/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility 

construction material (TEC, 2007). 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically 

upgradient of the USTs to provide geochemistry for water moving through the basal aquifer 

beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of 

approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of 

approximately 300 feet below ground surface outside the tunnel. Groundwater samples were 

collected from the three newly installed wells and two existing wells (RHMW01 and US Navy 

Well 2254-01) in September 2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 

samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs are current and provide action levels for more chemicals, and are 

much more useful for conducting screening risk assessments. Since the HDOH (HDOH May 

2005) Policy Letter stated that the two sets of action levels should not be mixed, the Tier 1 
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screening levels presented in HAR Section 11-281-78 would no longer be used to evaluate 

environmental impact at the Facility. 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

 No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

 TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

 1-methylnaphthalene and 2-methylnaphthalene exceeded HDOH Drinking Water EAL 

for taste and odor at RHMW02 during all three sampling events; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January, April, July, 

and October 2008. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace detections of 1-methylnaphthalene and naphthalene prompted a resample event in 

December at US Navy Well 2254-01, no chemicals were detected above the method 

detection limit (MDL); 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in October. 

1.5 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was previously 240 g/L, assuming they were not carcinogens. 

Evidence that they are carcinogenic to humans has now been accepted by the US Environmental 

Protection Agency (USEPA), and HDOH adopted more rigorous EALs of 4.7 g/L for 1-
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methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding to a residential tap 

water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels, a Hazard Index of 2.7 

(HDOH, 2008). 

Finally, the drinking water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, 

although the gross contamination EAL for TPH-DRO remains 100 g/L. 
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2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on February 4, 2009. 

Groundwater samples were collected from three monitoring wells located inside the Facility 

lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. 

Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility 

Groundwater Protection Plan (TEC, 2009). A total of seven samples were collected; one normal 

environmental sample from monitoring wells US Navy Well 2254-01, RHMW01, RHMW02 and 

RHMW03, one duplicate sample from RHMW02 (Sampled as RHMWA01 and reported as 

RHMW02D), and one matrix spike and matrix spike duplicate from US Navy Well 2254-01. 

2.1 Monitoring Well Purging 

The groundwater monitoring wells were purged and sampled using a dedicated pump system. 

Well purging was considered complete when no less than three successive water quality 

parameter measurements had stabilized within approximately 10 percent. Field parameters were 

measured at regular intervals during well purging and included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. Purge water was disposed in the Facility oil/water 

separator system. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system. Samples were placed into sampling 

containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile organic 

analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in the field 

and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, 

polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C SIM, and dissolved lead by 

EPA Method 6020. 
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3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

three monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring wells 

RHMW02 are reported in this document as RHMW02D. A summary of groundwater analytical 

results is included in Table 1. Complete analytical laboratory reports are provided in Appendix 

A. 

3.1 February 2009 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The results for each groundwater monitoring well are discussed below. 

RHMW01

TPH-DRO at 387 μg/L exceeded the HDOH Drinking Water EAL of 210 μg/L. Trace 

concentrations of TPH-GRO, fluorine, and naphthalene were detected well below HDOH EALs 

(Table 1). All other constituents were not detected. 

RHMW02

Eight petroleum constituents were detected at RHMW02: TPH-DRO, TPH-GRO, 1-

methylnaphthalene, 2-methylnaphthalene, naphthalene, acetone, benzene, and ethylbenzene. 

TPH-DRO was detected at RHMW02 in the normal and duplicate samples, at 2,840 μg/L. This 

result exceeded the HDOH EAL of 210 μg/L, but not the site-specific risk based level (SSRBL) 

of 4,500 μg/L. TPH-GRO was detected at an estimated average concentration of 53.3 μg/L, well 

below the HDOH Drinking Water EAL of 100 μg/L. 

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. USEPA 

Method 8260B produced the highest naphthalene concentrations, which averaged 42.9 μg/L from 

the normal and duplicate sample (HDOH EAL is 17 μg/L). In addition, 1-methylnaphthalene 

and 2-methylnapthalene were detected by USEPA Method 8270C SIM in the normal and 

duplicate samples. The average result for 1-methylnaphthalene was 22 μg/L, greater than the 

HDOH toxicity EAL of 4.7 μg/L. The average result for 2-methylnaphthalene was 10.8 μg/L, 

less than the HDOH drinking water toxicity EAL of 24 μg/L, but slightly greater than the HDOH 

drinking water taste and odor EAL of 10 g/L. All other petroleum constituents, including trace 

concentrations of acetone, benzene, and ethylbenzene, were well below HDOH Drinking Water 

EALs at RHMW02 (Table 1). 

RHMW03

Two constituents were detected at RHMW03: TPH-DRO and TPH-GRO (Table 1). TPH-DRO 

was detected at an estimated 207 μg/L, slightly below the HDOH Drinking Water toxicity EAL 

of 210 μg/L, but greater than the HDOH Drinking Water taste and odor EAL of 100 μg/L. TPHGRO was detected at an estimated 16.1 μg/L, well below the HDOH Drinking Water EALs of 

100 μg/L. All other constituents were below HDOH Drinking Water EALs at RHMW03. 
Table 1. Red Hill Analytical Results for Quarterly Groundwater Monitoring Release Response Report (February 4, 2009)

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result 

TPH as DIESEL RANGE ORGANICS 210 100 387 F 89.9 449 2840 89.9 449 2840 88.4 442 207 

TPH as GASOLINE RANGE ORGANICS 100 100 14.4 F 10 100 52.3 F 10 100 54.3 F 10 100 16.1 1-METHYLNAPHTHALENE 4.7 10 ND U 0.0165 0.0549 21.2 0.161 0.538 22.8 0.163 0.543 ND 

2-METHYLNAPHTHALENE 24 10 ND U 0.0165 0.0549 10.5 0.161 0.538 11.1 0.163 0.543 ND 

ACENAPHTHENE 370 20 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND ACENAPHTHYLENE 240 2000 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND ANTHRACENE 1800 22 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

BENZO(a)ANTHRACENE 0 092 4 7 ND U 0 0165 0 0549 ND U 0 161 0 538 ND U 0 0163 0 0543 ND 

RHMW02

UG/L

RHMW02D

UG/L

February 4, 2009 February 4, 2009 February 4, 2009 Fe

HDOH Residential 

Drinking Water EALs1

UG/L

HDOH Drinking 

Water Ceiling 

EALs2

UG/L

Chemical 

8015B (Petroleum)

Method

RHMW01

UG/L

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

BENZO(a)PYRENE 0.2 0.81 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

CHRYSENE 9.2 1 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND FLUORANTHENE 1500 130 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND FLUORENE 240 950 0.0235 F 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

NAPHTHALENE 17 21 0.173 0.0341 0.11 15.2 0.333 1.08 16.6 0.337 1.09 ND PHENANTHRENE 240 410 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

PYRENE 180 68 ND U 0.0165 0.0549 ND U 0.161 0.538 ND U 0.0163 0.0543 ND 

1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND 

1 2-DIBROMOETHANE (EDB) 0 0065 50000 ND U 0 31 1 ND U 0 31 1 ND U 0 31 1 ND 

8270C SIM 

(PAHs)

1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,2-DICHLOROETHANE 0.15 700 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

1,3-DICHLOROPROPANE 0.4 50000 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND 

1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND ACETONE 22000 20000 ND U 3.1 10 8.51 F 3.1 10 8.59 F 3.1 10 ND BENZENE 5 170 ND U 0.12 0.4 0.26 F 0.12 0.4 0.24 F 0.12 0.4 ND 

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND 

CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 

ETHYLBENZENE 700 30 ND U 0.31 1 0.49 F 0.31 1 0.52 F 0.31 1 ND 

HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

8260B (VOCs)

HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND 

METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND 

METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND 

METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND 

NAPHTHALENE 17 21 ND U 0.62 2 42.8 0.62 2 43 0.62 2 ND 

STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method 

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

12

Toxicity-based environmental action levels, Table D-1b, Screening For Environmental Concerns At Sites With Contaminated Soil and Groundwater, HDOH, 2008Taste, odor and solubility thresholds, Table G-1, Screening For Environmental Concerns At Sites With Contaminated Soil 

and Groundwater , HDOH, 2008

200

13
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

14 

US Navy Well 2254-01

TPH-GRO was detected at US Navy Well 2254-01 at 14 μg/L estimated value (i.e., the value is 

below the laboratory reporting limit, but above the method detection limit). The HDOH 

Drinking Water EAL for TPH-GRO is 100 μg/L. 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 

shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without fill) represent the method detection limit for 

chemicals that were not detected. 

RHMW01

TPH-GRO has only previously been detected in April 2008 at 13.6F μg/L, which is below the 

HDOH Drinking Water EAL of 100 μg/L. In February 2009, TPH-GRO was detected at 14.4 

μg/L. TPH-DRO was detected above the HDOH Drinking Water EAL during all groundwater 

sampling events. The concentration of TPH-DRO observed during the February 2009 sampling 

event decreased after showing an increase in October 2008. 

RHMW02

TPH-GRO was detected in all but one of the sampling rounds since September 2005, and 

exceeded the HDOH Drinking Water EAL of 100 μg/L three times during 2006 and 2007. The 

maximum concentration detected has been 148 μg/L. 

The concentration of TPH-DRO was relatively stable at RHMW02 until July 2008, ranging from 

2,250 to 2,995 μg/L. However, during the July and October 2008 sampling events, these average 

concentrations increased (i.e., average between the normal and duplicate samples). Specifically, 

the July 2008 average concentration was 4,055 μg/L and the October 2008 average concentration 

was 5,420 μg/L. Both of these values were well above the HDOH Drinking Water EAL of 210 

μg/L, with the October 2008 average also exceeding the SSRBL of 4,500 μg/L. The average 

concentration of TPH-DRO observed during the February 2009 sampling event (i.e., 2,840 μg/L) 

decreased relative to the July and October 2008 sampling event concentrations to approximate 

levels not observed since the April 2008 sampling event. This decrease in the February 2009 

sampling event downgraded RHMW02 to a Category 3 status from the previous Category 4 

status that followed the October 2008 sampling event. 

PAHs at RHMW02 remain above the HDOH Drinking Water EALs for naphthalene and 1-

methylnaphthalene. Concentrations decreased in the October 2008 and February 2009 sampling 

events after showing a slight increasing trend since the April 2008 sampling event. 

RHMW03

TPH-GRO has never been detected prior to February 2009. The February 2009 sampling event 

detected TPH-GRO at an estimated value of 16.1 μg/L, well below the HDOH Drinking Water 

EAL of 100 μg/L. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

15 

TPH-DRO had shown a slight increasing trend peaking at 244 μg/L during the October 2008 

sampling event. During the February 2009 sampling event, TPH-DRO concentrations decreased 

to 207 μg/L. Generally, the concentrations of TPH-DRO have remained relatively stable, near 

the DOH Drinking Water EAL of 210 μg/L. Concentrations of petroleum-related compounds at 

RHMW03 have normally been the lowest of the three wells located within the Facility. 

3.3 Results of Oil/Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

free product, released from the USTs were measured during this sampling event using a 300 ft 

Heron Oil/Water Interface Meter. The static water levels were measured to a precision of ± 0.01 

ft and fuel thickness was measured to a precision of ± 0.01 ft with this equipment. 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of < 0.01 ft, but has not been observed in other monitoring wells as of this document. 

Measurements to determine the presence and thickness of fuel were conducted at RHMW01, 

RHMW02, and RHMW03 prior to the current sampling round. At the end of February and the 

end of March subsequent rounds of oil/water interface measurements were conducted. In 

February, a measurement at RHMW01 was planned but was not completed due to extensive 

work being performed by Tank 02, making RHMW01 inaccessible. No free product was 

observed in any of these wells before and after this event (see Table 2). 

Table 2. Oil/Water Interface Measurements 

        

Date 

RHMW01 RHMW02 RHMW03 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT NT 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 

October 2008 18.61 0.00 18.56 0.00 18.82 0.00 

November 2008 18.50 0.00 18.45 0.00 18.51 0.00 

January 2009 19.28 0.00 19.22 0.00 102.04 0.00 

February 2009 NT NT 18.66 0.00 18.75 0.00 

March 2009 18.59 0.00 18.57 0.00 18.67 0.00 

 

SWL Static water level, elevation above mean sea level 

LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater 

ft Feet 

NT Not Taken 

3.4 Groundwater Status 

Constituents of concern are defined as those petroleum-related chemicals that have been 

observed in the groundwater samples above the HDOH EALs. In accordance with the Red Hill 

Bulk Fuel Storage Facility Final Groundwater Protection Plan (TEC, 2008), Table 3 defines the 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

16 

constituents of concern in groundwater at the Facility and the SSRBLs and updated EALs for 

each (HDOH 2008). 

Table 3. Action Levels for Constituents of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 210 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 4.7 NA 

2-Methylnaphthalene 24 NA 

Naphthalene 17 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, and RHMW03 

EALs are applicable at US Navy Well 2254-01 

In addition, the Plan defines four results categories of groundwater status for the Facility, based 

on concentrations of constituents of concern in RHMW01, RHMW02, RHMW03 and the US 

Navy Well 2254-01, and requires specific responses when these categories are observed during 

quarterly groundwater sampling. Table 4 describes each of the four results categories and 

identifies response actions to be taken in accordance with the Plan. 

 Table 4. Results Categories and Response Actions to Changes in Groundwater Status 

Results Category RHMW02 or 

RHMW03 

RHMW01 US Navy Pumping 

Well 2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E,P 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

Specific Responses: 

A. Send quarterly reports to HDOH 

B. Begin program to determine the source of leak 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report (see box below) to HDOH 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

17 

F. Send Type 2 Report (see box below) to HDOH 

G. Increase monitoring frequency to once per month (if concentrations increasing) 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately determine leaking tank 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 

L. Provide alternative water source at 2254-01 

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

O. Install additional monitoring well downgradient 

Report Types 

HDOH Type 1 Report 

 Re-evaluate Tier 3 Risk Assessment/groundwater model results 

 Proposal to HDOH on a course of action 

HDOH Type 2 Report 

 Proposal for groundwater treatment 

In response to the previous Category 3 conditions at RHMW02, oil/water interface 

measurements were collected in October 2008, November 2008, January 2009, February 2009, 

and March 2009 at Red Hill tunnel monitoring wells (Table 2). To date, there is no evidence of 

fuel on groundwater at any of these wells based on oil/water interface measurements. 

Although TPH-GRO was detected at US Navy Well 2254-01 during the February 2009 sampling 

event, it does not place the well into the Category 1 status. Since no contamination trend (i.e., 

two or more consecutive sampling rounds) has been observed at US Navy Well 2254-01, the 

well does not meet the Category 1 definition. 

Category 1 Status Locations

Based upon the February 2009 sampling event, RHMW03 is presently in Category 1 status, since 

the TPH-DRO value (i.e., 207 g/L) dipped slightly below the HDOH EAL for drinking water 

(i.e., 210 g/L) and this represents a slight decrease in the concentration as compared with the 

October 2008 concentration. Category 1 response requires: 

1. Quarterly reports to be sent to HDOH. 

Category 2 Status Locations

Results from the February 2009 sampling event indicate that RHMW01 is presently in Category 

2 status, since the TPH-DRO concentration of 387g/L is greater than the HDOH EAL for 

drinking water (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated solubility limit 

of JP-5). Category 2 response at RHMW01 requires: 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

18 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 Status Locations

Results from the February 2009 sampling event indicate that RHMW02 is presently in Category 

3 status (i.e., downgraded from Category 4 status observed during the October 2008 sampling 

event), since TPH-DRO [2,840 g/L and 2,840 g/L (duplicate)] is greater than the HDOH EAL 

for drinking water (210 g/L), but is between one half and the established SSRBL value of 4,500 

g/L (estimated solubility limit of JP-5). In addition, the HDOH Drinking Water EAL of 4.7 

g/L for 1-methylnaphthalene was exceeded [i.e., 21.2 g/L and 22.8 g/L (duplicate)]. 

Category 3 response at RHMW02 requires: 

1. Send quarterly reports to HDOH; 

2. Initiation of a leak determination program to identify if tanks are leaking; 

3. Increase free product monitoring frequency to once per month (if concentrations 

increasing); 

4. Notify HDOH verbally within 7 days and follow with written notification in 30 days; 

5. Remove sampling pumps, measure product in pertinent wells with interface probe, reinstall pumps if product is not detected; and 

6. Immediately evaluate tanks for leaks. 

4.0 Summary and Conclusions 

Summary

At RHMW02, the concentration of TPH-DRO in groundwater exceeded the EAL of 210 g/L 

and was between one half and the established SSRBL value of 4,500 g/L, which indicates 

Category 3 groundwater status at RHMW02. This represents a downgrade from Category 4 

status, which was prompted by the October 2008 sampling effort. Although 1-

methylnaphthalene which was detected at RHMW2254-01 during the October 2008 sampling 

event, it was not detected during the February 2009 sampling event. An unexpected estimated 

value of 14 μg/L of TPH-GRO was detected at RHMW2254-01; however, this concentration is 

well below the HDOH Drinking Water EAL of 100 μg/L and just above the method detection 

limit of 10 μg/L. 

Conclusions

 Oil/water interface measurements were collected in October 2008, November 2008, 

January 2009, February 2009, and March 2009 from Red Hill tunnel monitoring wells 

and no free product was measured (Table 2). 

 The concentration of TPH-DRO measured at RHMW01 in February 2009 was less than 

one tenth of the SSRBL. RHMW01 is down-gradient from RHMW02 and between 

RHMW02 and the US Navy Well 2254-01, an important drinking water source for the 

Pearl Harbor Water System. 

 The US Navy Well 2254-01 is not imminently threatened at this time; however, 

conditions should be monitored closely to determine if any USTs in the Facility are 

currently leaking fuel into the subsurface and whether or not the unexpected value at 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

19 

RHMW2254-01 of 14 g/L of TPH-GRO from the February 2009 sampling event 

represents an anomaly or an apparent analytical trend. 

 Category 4 activities should continue due to the October 2008 analytical results. These 

activities include: 

 Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both 

are valid and protective of human health and the environment under the existing 

conditions and provide a report describing the results of this re-evaluation to the 

HDOH; 

 Evaluate potential requirement for groundwater treatment and provide a report 

describing the results of this re-evaluation to the HDOH; 

 Implement monthly oil/water interface measurements at RHMW01, RHMW02, 

and RHMW03, and provide monthly letter reports of the results; 

 Evaluate tanks associated with the middle section of the Facility (Tanks 5, 6, 7, 8, 

9, 10, 11, 12, 13, and 14); 

 Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and 

OWDF MW01; 

 Prepare for alternative water source at US Navy Well 2254-01, as necessary. 

The US Navy plans to install an additional monitoring well (RHMW05) in the lower access 

tunnel of the Facility between RHMW01 and the US Navy Well 2254-01 to better monitor the 

quality of the groundwater moving from the Facility to the US Navy Well 2254-01. 

It is recommended that RHMW01, RHMW02, RHMW03, and RHMW05 (once installed) be 

evaluated monthly for the presence of fuel on groundwater, in accordance with the Plan. The 

US Navy plans to install dedicated oil/water interface probes in each of these wells to facilitate 

these measurements. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead will 

continue as previously scheduled until such time that new data indicates that a different schedule 

is warranted. The quarterly collection and analysis of groundwater samples will continue to 

monitor the quality of the groundwater located beneath the Facility. Groundwater monitoring 

reports will be submitted to the HDOH upon receipt and evaluation of laboratory analytical 

results. It is recommended that future quarterly analytical results be closely monitored at 

RHMW2254-01 to assess whether the detection of trace quantities (i.e., 14 g/L) of TPH-GRO 

from the February 2009 sampling event represents an anomaly or an apparent analytical trend. 
The HDOH toxicity EALs were updated •TPH-DRO Residential Tap Water EAL •TPH-GRO Residential Tap Water EAL (HDOH 2008)(HDOH, 2008).
The HDOH toxicity EALs were updated • Naphthalene Residential Tap Water • 1-methylnaphthalene Residential Tap • 2- methylnaphthalene Residential Tap (HDOH 2008)(HDOH, 2008).
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2009 

 ____________________________________________________________________________________________ 

22 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Volume 1: Summary Tier 1 Lookup Tables. Interim Final. May 2005. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

The Environmental Company, Inc. and AMEC. Red Hill Bulk Fuel Storage Facility Work Plan, 

Pearl Harbor, Hawaii. June 2005. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii. 

August 2007. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

Red Hill BFSF

The Environmental Company, Inc. (TEC)

1090476
Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1090476 Red Hill BFSF

Customer:

Project:

NPDL WO:

SGS Environmental Services Inc.

Refer to the sample receipt form for information on sample condition.

1090476005 PS RHMW02-WG14

8015C - DRO - The pattern is consistent with a weathered middle distillate.

8270D SIM - PQLs are elevated due to sample dilution. Sample analyzed at a dilution due to matrix interference 

with internal standards.

8270D SIM - Surrogate recovery for terphenyl-d14 doe snot meet QC criteria (biased high) due to sample dilution.

1090476006 PS RHMWA01-WG14

8015C - DRO - The pattern is consistent with a weathered middle distillate.

1090476002 BMS RHMW2254-WG14 MS

8260B - BMS recoveries for dichlorodifluoromethane, chloromethane, vinyl chloride and trans-1,2-dichloroethene do 

not meet QC goals (biased high). Refer to LCS for accuracy.

8260B - BMS/BMSD RPD for trans-1,2-dichloroethene does not meet QC goals (biased high). Refer to LCS/LCSD 

RPD for precision.

1090476003 BMSD RHMW2254-WG14 MSD

8260B - BMSD recoveries for dichlorodifluoromethane, chloromethane and vinyl chloride do not meet QC goals 

(biased high). Refer to LCS for accuracy.

8260B - BMS/BMSD RPD for trans-1,2-dichloroethene does not meet QC goals (biased high). Refer to LCS/LCSD 

RPD for precision.

883392 LCS VXX/19212]

8260B - LCS recoveries for dichlorodifluoromethane, chloromethane and vinyl chloride do not meet QC goals 

(biased high). These analytes were not detected above the PQL in the associated samples.

883393 LCSD VXX/19212

8260B - LCSD recoveries for dichlorodifluoromethane, chloromethane and vinyl chloride do not meet QC goals 

(biased high). These analytes were not detected above the PQL in the associated samples.

883395 CCV VMS/10380]

8260B - CCV recoveries for dichlorodifluoromethane, chloromethane, vinyl chloride and trichlorofluoromethane do 

not meet QC goals (biased high). These analytes were not detected above the PQL in the associated samples.

8260B - ICV recoveries for several analytes do not meet QC goals (biased high). These analytes were not detected 

above the PQL in the associated samples.
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1090476

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike (Duplicate)

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 2/19/2009

Notes: All DRO/RRO analyses are integrated per SOP.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: Red Hill BFSF

Workorder No.: 1090476

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 2/19/2009 10:58 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1090476001 RHMW2254-WG14

1090476002 RHMW2254-WG14 MS

1090476003 RHMW2254-WG14 MSD

1090476004 RHMW03-WG14

1090476005 RHMW02-WG14

1090476006 RHMWA01-WG14

1090476007 RHMW01-WG14

1090476008 TB01-WG14

S G S N orth A m erica Inc . A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5820 MXX21362

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5820

Analytical Method: SW6020

Analysis Date/Time: 02/17/09 11:41

Prep Batch: MXX21362

Prep Method: SW3010A

Prep Date/Time: 02/12/09 12:00 Container ID:1090476001-G

Dilution Factor: 5 Analyst: SCL

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 14.0 J 100 10.0 ug/L 1 VFC9351 VXX19194

4-Bromofluorobenzene <surr> 85.2 50-150 % 1 VFC9351 VXX19194

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9351

Analytical Method: SW8015C

Analysis Date/Time: 02/10/09 12:33

Prep Batch: VXX19194

Prep Method: SW5030B

Prep Date/Time: 02/10/09 09:30 Container ID:1090476001-A

Dilution Factor: 1 Analyst: HM

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.460 0.0920 mg/L 1 XFC8449 XXX20585

5a Androstane <surr> 79.6 50-150 % 1 XFC8449 XXX20585

Batch Information

Initial Prep Wt./Vol.: 870 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8449

Analytical Method: SW8015C

Analysis Date/Time: 02/11/09 15:55

Prep Batch: XXX20585

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476001-H

Dilution Factor: 1 Analyst: KDC

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 98 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 17:18

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476001-D

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW2254-WG14

SGS Ref. #: 1090476001 Collection Date/Time: 02/04/09 09:20

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Acenaphthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Fluorene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Phenanthrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo(a)Anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Chrysene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[b]Fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[k]fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[a]pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Indeno[1,2,3-c,d] pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Dibenzo[a,h]anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[g,h,i]perylene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Naphthalene ND 0.108 0.0333 ug/L 1 XMS4825 XXX20586

1-Methylnaphthalene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

2-Methylnaphthalene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Terphenyl-d14 <surr> 92.7 50-135 % 1 XMS4825 XXX20586

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4825

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/10/09 22:34

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476001-J

Dilution Factor: 1 Analyst: JDH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5820 MXX21362

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5820

Analytical Method: SW6020

Analysis Date/Time: 02/17/09 11:48

Prep Batch: MXX21362

Prep Method: SW3010A

Prep Date/Time: 02/12/09 12:00 Container ID:1090476004-G

Dilution Factor: 5 Analyst: SCL

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 16.1 J 100 10.0 ug/L 1 VFC9351 VXX19194

4-Bromofluorobenzene <surr> 85.4 50-150 % 1 VFC9351 VXX19194

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9351

Analytical Method: SW8015C

Analysis Date/Time: 02/10/09 13:28

Prep Batch: VXX19194

Prep Method: SW5030B

Prep Date/Time: 02/10/09 09:30 Container ID:1090476004-A

Dilution Factor: 1 Analyst: HM

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.207 J 0.447 0.0894 mg/L 1 XFC8449 XXX20585

5a Androstane <surr> 88.9 50-150 % 1 XFC8449 XXX20585

Batch Information

Initial Prep Wt./Vol.: 895 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8449

Analytical Method: SW8015C

Analysis Date/Time: 02/11/09 16:23

Prep Batch: XXX20585

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476004-H

Dilution Factor: 1 Analyst: KDC

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 98.8 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 17:52

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476004-D

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW03-WG14

SGS Ref. #: 1090476004 Collection Date/Time: 02/04/09 11:10

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Acenaphthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Fluorene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Phenanthrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo(a)Anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Chrysene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[b]Fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[k]fluoranthene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[a]pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Indeno[1,2,3-c,d] pyrene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Dibenzo[a,h]anthracene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Benzo[g,h,i]perylene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Naphthalene ND 0.108 0.0333 ug/L 1 XMS4825 XXX20586

1-Methylnaphthalene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

2-Methylnaphthalene ND 0.0538 0.0161 ug/L 1 XMS4825 XXX20586

Terphenyl-d14 <surr> 85.2 50-135 % 1 XMS4825 XXX20586

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4825

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/11/09 00:11

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476004-J

Dilution Factor: 1 Analyst: JDH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5820 MXX21362

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5820

Analytical Method: SW6020

Analysis Date/Time: 02/17/09 11:50

Prep Batch: MXX21362

Prep Method: SW3010A

Prep Date/Time: 02/12/09 12:00 Container ID:1090476005-G

Dilution Factor: 5 Analyst: SCL

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 52.3 J 100 10.0 ug/L 1 VFC9351 VXX19194

4-Bromofluorobenzene <surr> 116 50-150 % 1 VFC9351 VXX19194

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9351

Analytical Method: SW8015C

Analysis Date/Time: 02/10/09 13:46

Prep Batch: VXX19194

Prep Method: SW5030B

Prep Date/Time: 02/10/09 09:30 Container ID:1090476005-A

Dilution Factor: 1 Analyst: HM

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 2.84 0.449 0.0899 mg/L 1 XFC8449 XXX20585

5a Androstane <surr> 69.3 50-150 % 1 XFC8449 XXX20585

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8449

Analytical Method: SW8015C

Analysis Date/Time: 02/11/09 16:32

Prep Batch: XXX20585

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476005-H

Dilution Factor: 1 Analyst: KDC

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.260 J 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene 0.490 J 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene 2.37 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene 8.60 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone 8.51 J 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene 7.67 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene 42.8 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene 0.400 J 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene 1.19 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) 6.48 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 98.4 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 101 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 18:26

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476005-D

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW02-WG14

SGS Ref. #: 1090476005 Collection Date/Time: 02/04/09 12:40

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Acenaphthene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Fluorene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Phenanthrene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Anthracene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Fluoranthene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Pyrene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Benzo(a)Anthracene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Chrysene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Benzo[b]Fluoranthene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Benzo[k]fluoranthene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Benzo[a]pyrene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Indeno[1,2,3-c,d] pyrene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Dibenzo[a,h]anthracene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Benzo[g,h,i]perylene ND 0.538 0.161 ug/L 10 XMS4828 XXX20586

Naphthalene 15.2 1.08 0.333 ug/L 10 XMS4828 XXX20586

1-Methylnaphthalene 21.2 0.538 0.161 ug/L 10 XMS4828 XXX20586

2-Methylnaphthalene 10.5 0.538 0.161 ug/L 10 XMS4828 XXX20586

Terphenyl-d14 <surr> 162 * 50-135 % 10 XMS4828 XXX20586

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4828

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/12/09 19:57

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476005-I

Dilution Factor: 10 Analyst: JDH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5820 MXX21362

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5820

Analytical Method: SW6020

Analysis Date/Time: 02/17/09 11:52

Prep Batch: MXX21362

Prep Method: SW3010A

Prep Date/Time: 02/12/09 12:00 Container ID:1090476006-G

Dilution Factor: 5 Analyst: SCL

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 54.3 J 100 10.0 ug/L 1 VFC9351 VXX19194

4-Bromofluorobenzene <surr> 116 50-150 % 1 VFC9351 VXX19194

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9351

Analytical Method: SW8015C

Analysis Date/Time: 02/10/09 14:05

Prep Batch: VXX19194

Prep Method: SW5030B

Prep Date/Time: 02/10/09 09:30 Container ID:1090476006-A

Dilution Factor: 1 Analyst: HM

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 2.84 0.442 0.0884 mg/L 1 XFC8449 XXX20585

5a Androstane <surr> 73 50-150 % 1 XFC8449 XXX20585

Batch Information

Initial Prep Wt./Vol.: 905 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8449

Analytical Method: SW8015C

Analysis Date/Time: 02/11/09 16:42

Prep Batch: XXX20585

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476006-H

Dilution Factor: 1 Analyst: KDC

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.240 J 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene 0.520 J 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene 2.46 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene 9.00 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone 8.59 J 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene 7.81 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene 43.0 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene 0.470 J 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene 1.14 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) 6.88 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 99.7 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 99.8 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 99.5 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 18:59

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476006-D

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMWA01-WG14

SGS Ref. #: 1090476006 Collection Date/Time: 02/04/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Acenaphthene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Fluorene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Phenanthrene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Anthracene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Fluoranthene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Pyrene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Benzo(a)Anthracene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Chrysene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Benzo[b]Fluoranthene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Benzo[k]fluoranthene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Benzo[a]pyrene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Indeno[1,2,3-c,d] pyrene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Dibenzo[a,h]anthracene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Benzo[g,h,i]perylene ND 0.0543 0.0163 ug/L 1 XMS4825 XXX20586

Naphthalene 16.6 1.09 0.337 ug/L 10 XMS4828 XXX20586

1-Methylnaphthalene 22.8 0.543 0.163 ug/L 10 XMS4828 XXX20586

2-Methylnaphthalene 11.1 0.543 0.163 ug/L 10 XMS4828 XXX20586

Terphenyl-d14 <surr> 87.2 50-135 % 1 XMS4825 XXX20586

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4825

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/11/09 01:16

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476006-I

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4828

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/12/09 20:29

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476006-I

Dilution Factor: 10 Analyst: JDH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5820 MXX21362

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5820

Analytical Method: SW6020

Analysis Date/Time: 02/17/09 11:54

Prep Batch: MXX21362

Prep Method: SW3010A

Prep Date/Time: 02/12/09 12:00 Container ID:1090476007-E

Dilution Factor: 5 Analyst: SCL

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 14.4 J 100 10.0 ug/L 1 VFC9351 VXX19194

4-Bromofluorobenzene <surr> 85.5 50-150 % 1 VFC9351 VXX19194

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9351

Analytical Method: SW8015C

Analysis Date/Time: 02/10/09 14:23

Prep Batch: VXX19194

Prep Method: SW5030B

Prep Date/Time: 02/10/09 09:30 Container ID:1090476007-A

Dilution Factor: 1 Analyst: HM

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.387 J 0.449 0.0899 mg/L 1 XFC8449 XXX20585

5a Androstane <surr> 77.9 50-150 % 1 XFC8449 XXX20585

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8449

Analytical Method: SW8015C

Analysis Date/Time: 02/11/09 16:51

Prep Batch: XXX20585

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476007-F

Dilution Factor: 1 Analyst: KDC

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 99.1 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 19:33

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476007-C

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: RHMW01-WG14

SGS Ref. #: 1090476007 Collection Date/Time: 02/04/09 14:55

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Acenaphthene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Fluorene 0.0235 J 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Phenanthrene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Anthracene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Pyrene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Benzo(a)Anthracene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Chrysene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Benzo[b]Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Benzo[k]fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Benzo[a]pyrene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Indeno[1,2,3-c,d] pyrene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Dibenzo[a,h]anthracene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Benzo[g,h,i]perylene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Naphthalene 0.173 0.110 0.0341 ug/L 1 XMS4825 XXX20586

1-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

2-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4825 XXX20586

Terphenyl-d14 <surr> 86.2 50-135 % 1 XMS4825 XXX20586

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4825

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/11/09 01:48

Prep Batch: XXX20586

Prep Method: SW3520C

Prep Date/Time: 02/10/09 10:50 Container ID:1090476007-H

Dilution Factor: 1 Analyst: JDH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: TB01-WG14

SGS Ref. #: 1090476008 Collection Date/Time: 02/04/09 08:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

Toluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Styrene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Acetone ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10380 VXX19212

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10380 VXX19212

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

Chloroform ND 1.00 0.300 ug/L 1 VMS10380 VXX19212

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Chloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromomethane ND 3.00 0.940 ug/L 1 VMS10380 VXX19212

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 2/19/2009 10:58 am

Client Sample ID: TB01-WG14

SGS Ref. #: 1090476008 Collection Date/Time: 02/04/09 08:05

Project ID: Red Hill BFSF Receipt Date/Time: 02/06/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10380 VXX19212

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10380 VXX19212

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

Naphthalene ND 2.00 0.620 ug/L 1 VMS10380 VXX19212

o-Xylene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Bromoform ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10380 VXX19212

1,2-Dichloroethane-D4 <surr> 101 73-120 % 1 VMS10380 VXX19212

Toluene-d8 <surr> 102 80-120 % 1 VMS10380 VXX19212

4-Bromofluorobenzene <surr> 98.9 76-120 % 1 VMS10380 VXX19212

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10380

Analytical Method: SW8260B

Analysis Date/Time: 02/16/09 16:45

Prep Batch: VXX19212

Prep Method: SW5030B

Prep Date/Time: 02/16/09 11:48 Container ID:1090476008-A

Dilution Factor: 1 Analyst: DSH

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882405 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20585

SW3520C

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.0800 mg/L 02/11/09

Surrogates 

5a Androstane <surr> 77.3 60-120 % 02/11/09

Instrument

Method

Batch XFC8449

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882440 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20586

SW3520C

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 02/10/09

Acenaphthene ND 0.0500 0.0150 ug/L 02/10/09

Fluorene ND 0.0500 0.0150 ug/L 02/10/09

Phenanthrene ND 0.0500 0.0150 ug/L 02/10/09

Anthracene ND 0.0500 0.0150 ug/L 02/10/09

Fluoranthene ND 0.0500 0.0150 ug/L 02/10/09

Pyrene ND 0.0500 0.0150 ug/L 02/10/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 02/10/09

Chrysene ND 0.0500 0.0150 ug/L 02/10/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 02/10/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 02/10/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 02/10/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 02/10/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 02/10/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 02/10/09

Naphthalene ND 0.100 0.0310 ug/L 02/10/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 02/10/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 02/10/09

Surrogates 

Terphenyl-d14 <surr> 90.6 50-135 % 02/10/09

Instrument

Method

Batch XMS4825

8270D SIMS

HP 6890/5973 MS SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882496 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19194

SW5030B

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics ND 100 10.0 ug/L 02/10/09

Surrogates 

4-Bromofluorobenzene <surr> 85.6 50-150 % 02/10/09

Instrument

Method

Batch VFC9351

SW8015C

HP 5890 Series II PID+HECD VBA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882936 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21362

SW3010A

02/12/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 02/17/09

Instrument

Method

Batch MMS5820

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883391 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007, 1090476008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883391 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 02/16/09

Toluene ND 1.00 0.310 ug/L 02/16/09

Ethylbenzene ND 1.00 0.310 ug/L 02/16/09

n-Butylbenzene ND 1.00 0.310 ug/L 02/16/09

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 02/16/09

1,2-Dichloroethane ND 0.500 0.150 ug/L 02/16/09

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 02/16/09

4-Chlorotoluene ND 1.00 0.310 ug/L 02/16/09

Chlorobenzene ND 0.500 0.150 ug/L 02/16/09

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 02/16/09

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 02/16/09

4-Isopropyltoluene ND 1.00 0.310 ug/L 02/16/09

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 02/16/09

n-Propylbenzene ND 1.00 0.310 ug/L 02/16/09

Styrene ND 1.00 0.310 ug/L 02/16/09

Dibromomethane ND 1.00 0.310 ug/L 02/16/09

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 02/16/09

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 02/16/09

Acetone ND 10.0 3.10 ug/L 02/16/09

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 02/16/09

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 02/16/09

Methyl-t-butyl ether ND 5.00 1.50 ug/L 02/16/09

Tetrachloroethene ND 1.00 0.310 ug/L 02/16/09

Dibromochloromethane ND 0.500 0.150 ug/L 02/16/09

1,3-Dichloropropane ND 0.400 0.120 ug/L 02/16/09

1,2-Dibromoethane ND 1.00 0.310 ug/L 02/16/09

Carbon tetrachloride ND 1.00 0.310 ug/L 02/16/09

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 02/16/09

Chloroform ND 1.00 0.300 ug/L 02/16/09

Bromobenzene ND 1.00 0.310 ug/L 02/16/09

Chloromethane ND 1.00 0.310 ug/L 02/16/09

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 02/16/09

Bromomethane ND 3.00 0.940 ug/L 02/16/09

Bromochloromethane ND 1.00 0.310 ug/L 02/16/09

Vinyl chloride ND 1.00 0.310 ug/L 02/16/09

Dichlorodifluoromethane ND 1.00 0.310 ug/L 02/16/09

Chloroethane ND 1.00 0.310 ug/L 02/16/09

sec-Butylbenzene ND 1.00 0.310 ug/L 02/16/09

Bromodichloromethane ND 0.500 0.150 ug/L 02/16/09
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883391 Method Blank

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 02/16/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 02/16/09

Methylene chloride ND 5.00 1.00 ug/L 02/16/09

Trichlorofluoromethane ND 1.00 0.310 ug/L 02/16/09

P & M -Xylene ND 2.00 0.620 ug/L 02/16/09

Naphthalene ND 2.00 0.620 ug/L 02/16/09

o-Xylene ND 1.00 0.310 ug/L 02/16/09

Bromoform ND 1.00 0.310 ug/L 02/16/09

1-Chlorohexane ND 1.00 0.310 ug/L 02/16/09

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 02/16/09

tert-Butylbenzene ND 1.00 0.310 ug/L 02/16/09

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 02/16/09

1,1-Dichloroethane ND 1.00 0.310 ug/L 02/16/09

2-Chlorotoluene ND 1.00 0.310 ug/L 02/16/09

Trichloroethene ND 1.00 0.310 ug/L 02/16/09

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 02/16/09

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 02/16/09

2,2-Dichloropropane ND 1.00 0.310 ug/L 02/16/09

Hexachlorobutadiene ND 1.00 0.310 ug/L 02/16/09

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 02/16/09

1,2-Dichloropropane ND 1.00 0.310 ug/L 02/16/09

1,1-Dichloropropene ND 1.00 0.310 ug/L 02/16/09

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 02/16/09

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 02/16/09

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 02/16/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 101 73-120 % 02/16/09

Toluene-d8 <surr> 101 80-120 % 02/16/09

4-Bromofluorobenzene <surr> 103 76-120 % 02/16/09

Instrument

Method

Batch VMS10380

SW8260B

HP 5890 Series II MS1 VJA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882441 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20586

SW3520C

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.259 52 ( 50-105 ) 0.5 ug/L 02/10/2009

Acenaphthene LCS 0.253 51 ( 45-110 ) 0.5 ug/L 02/10/2009

Fluorene LCS 0.271 54 ( 50-110 ) 0.5 ug/L 02/10/2009

Phenanthrene LCS 0.288 58 ( 50-115 ) 0.5 ug/L 02/10/2009

Anthracene LCS 0.282 56 ( 55-110 ) 0.5 ug/L 02/10/2009

Fluoranthene LCS 0.374 75 ( 55-125 ) 0.5 ug/L 02/10/2009

Pyrene LCS 0.364 73 ( 50-130 ) 0.5 ug/L 02/10/2009

Benzo(a)Anthracene LCS 0.363 73 ( 55-120 ) 0.5 ug/L 02/10/2009

Chrysene LCS 0.360 72 ( 55-120 ) 0.5 ug/L 02/10/2009

Benzo[b]Fluoranthene LCS 0.382 76 ( 46-130 ) 0.5 ug/L 02/10/2009

Benzo[k]fluoranthene LCS 0.357 71 ( 60-125 ) 0.5 ug/L 02/10/2009

Benzo[a]pyrene LCS 0.364 73 ( 55-120 ) 0.5 ug/L 02/10/2009

Indeno[1,2,3-c,d] pyrene LCS 0.361 72 ( 45-125 ) 0.5 ug/L 02/10/2009

Dibenzo[a,h]anthracene LCS 0.361 72 ( 41-140 ) 0.5 ug/L 02/10/2009

Benzo[g,h,i]perylene LCS 0.361 72 ( 46-125 ) 0.5 ug/L 02/10/2009

Naphthalene LCS 0.252 50 ( 42-100 ) 0.5 ug/L 02/10/2009

1-Methylnaphthalene LCS 0.243 49 ( 46-115 ) 0.5 ug/L 02/10/2009

2-Methylnaphthalene LCS 0.233 47 ( 45-105 ) 0.5 ug/L 02/10/2009

Surrogates 

Terphenyl-d14 <surr> LCS 84 ( 50-135 ) 02/10/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882441 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20586

SW3520C

02/10/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4825

8270D SIMS

HP 6890/5973 MS SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882497 Lab Control Sample

882498 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19194

SW5030B

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 192 96 ( 79-108 ) 200 ug/L 02/10/2009

LCSD 191 95 1 (< 20 ) 200 ug/L 02/10/2009

Surrogates 

4-Bromofluorobenzene <surr> LCS 91 ( 50-150 ) 02/10/2009

LCSD 90 1 02/10/2009

Batch

Method

Instrument

VFC9351

SW8015C

HP 5890 Series II PID+HECD VBA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882788 Lab Control Sample

882789 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20585

SW3520C

02/10/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.47 90 ( 75-125 ) 5 mg/L 02/11/2009

LCSD 4.27 85 5 (< 20 ) 5 mg/L 02/11/2009

Surrogates 

5a Androstane <surr> LCS 88 ( 60-120 ) 02/11/2009

LCSD 84 4 02/11/2009

Batch

Method

Instrument

XFC8449

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

882937 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21362

SW3010A

02/12/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 986 99 ( 80-120 ) 1000 ug/L 02/17/2009

Batch

Method

Instrument

MMS5820

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

QC results affect the following production samples:

1090476001, 1090476004, 1090476005, 1090476006, 1090476007, 1090476008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 31.1 104 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 29.2 97 7 (< 20 ) 30 ug/L 02/16/2009

Toluene LCS 30.7 102 ( 77-120 ) 30 ug/L 02/16/2009

LCSD 30.6 102 0 (< 20 ) 30 ug/L 02/16/2009

Ethylbenzene LCS 32.9 110 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 32.1 107 2 (< 20 ) 30 ug/L 02/16/2009

n-Butylbenzene LCS 33.0 110 ( 80-124 ) 30 ug/L 02/16/2009

LCSD 31.9 106 3 (< 20 ) 30 ug/L 02/16/2009

1,4-Dichlorobenzene LCS 30.9 103 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.9 103 0 (< 20 ) 30 ug/L 02/16/2009

1,2-Dichloroethane LCS 31.5 105 ( 80-129 ) 30 ug/L 02/16/2009

LCSD 29.8 99 6 (< 20 ) 30 ug/L 02/16/2009

1,3,5-Trimethylbenzene LCS 32.6 109 ( 80-128 ) 30 ug/L 02/16/2009

LCSD 31.9 106 2 (< 20 ) 30 ug/L 02/16/2009

4-Chlorotoluene LCS 31.2 104 ( 79-128 ) 30 ug/L 02/16/2009

LCSD 31.2 104 0 (< 20 ) 30 ug/L 02/16/2009

Chlorobenzene LCS 32.5 108 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.8 106 2 (< 20 ) 30 ug/L 02/16/2009

4-Methyl-2-pentanone (MIBK) LCS 91.4 102 ( 69-134 ) 90 ug/L 02/16/2009

LCSD 86.8 97 5 (< 20 ) 90 ug/L 02/16/2009

cis-1,2-Dichloroethene LCS 32.5 108 ( 80-125 ) 30 ug/L 02/16/2009

LCSD 31.5 105 3 (< 20 ) 30 ug/L 02/16/2009

4-Isopropyltoluene LCS 32.5 108 ( 80-125 ) 30 ug/L 02/16/2009

LCSD 32.0 107 2 (< 20 ) 30 ug/L 02/16/2009

cis-1,3-Dichloropropene LCS 32.2 107 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.8 103 4 (< 20 ) 30 ug/L 02/16/2009

n-Propylbenzene LCS 32.0 107 ( 80-129 ) 30 ug/L 02/16/2009

LCSD 31.8 106 1 (< 20 ) 30 ug/L 02/16/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 33.3 111 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 32.7 109 2 (< 20 ) 30 ug/L 02/16/2009

Dibromomethane LCS 32.8 109 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.2 104 5 (< 20 ) 30 ug/L 02/16/2009

trans-1,3-Dichloropropene LCS 29.1 97 ( 80-124 ) 30 ug/L 02/16/2009

LCSD 29.2 97 0 (< 20 ) 30 ug/L 02/16/2009

1,2,4-Trichlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.6 105 2 (< 20 ) 30 ug/L 02/16/2009

Acetone LCS 100 111 ( 50-135 ) 90 ug/L 02/16/2009

LCSD 89.3 99 12 (< 20 ) 90 ug/L 02/16/2009

1,1,2,2-Tetrachloroethane LCS 30.7 102 ( 76-123 ) 30 ug/L 02/16/2009

LCSD 30.3 101 1 (< 20 ) 30 ug/L 02/16/2009

1,2-Dibromo-3-chloropropane LCS 30.5 102 ( 73-130 ) 30 ug/L 02/16/2009

LCSD 29.7 99 2 (< 20 ) 30 ug/L 02/16/2009

Methyl-t-butyl ether LCS 38.7 86 ( 80-120 ) 45 ug/L 02/16/2009

LCSD 39.3 87 1 (< 20 ) 45 ug/L 02/16/2009

Tetrachloroethene LCS 32.9 110 ( 79-122 ) 30 ug/L 02/16/2009

LCSD 31.6 105 4 (< 20 ) 30 ug/L 02/16/2009

Dibromochloromethane LCS 29.9 100 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 29.5 98 1 (< 20 ) 30 ug/L 02/16/2009

1,3-Dichloropropane LCS 32.1 107 ( 80-121 ) 30 ug/L 02/16/2009

LCSD 31.8 106 1 (< 20 ) 30 ug/L 02/16/2009

1,2-Dibromoethane LCS 32.2 107 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.6 105 2 (< 20 ) 30 ug/L 02/16/2009

Carbon tetrachloride LCS 35.2 117 ( 80-126 ) 30 ug/L 02/16/2009

LCSD 33.2 111 6 (< 20 ) 30 ug/L 02/16/2009

1,1,1,2-Tetrachloroethane LCS 29.7 99 ( 80-120 ) 30 ug/L 02/16/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 30.1 100 2 (< 20 ) 30 ug/L 02/16/2009

Chloroform LCS 31.5 105 ( 80-124 ) 30 ug/L 02/16/2009

LCSD 29.8 99 5 (< 20 ) 30 ug/L 02/16/2009

Bromobenzene LCS 29.9 100 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.6 102 2 (< 20 ) 30 ug/L 02/16/2009

Chloromethane LCS 48.5 162 * ( 67-125 ) 30 ug/L 02/16/2009

LCSD 56.4 188 * 15 (< 20 ) 30 ug/L 02/16/2009

1,2,3-Trichloropropane LCS 32.2 107 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.3 104 3 (< 20 ) 30 ug/L 02/16/2009

Bromomethane LCS 25.3 84 ( 30-140 ) 30 ug/L 02/16/2009

LCSD 30.5 102 19 (< 20 ) 30 ug/L 02/16/2009

Bromochloromethane LCS 34.1 114 ( 77-129 ) 30 ug/L 02/16/2009

LCSD 32.4 108 5 (< 20 ) 30 ug/L 02/16/2009

Vinyl chloride LCS 44.4 148 * ( 72-145 ) 30 ug/L 02/16/2009

LCSD 44.4 148 * 0 (< 20 ) 30 ug/L 02/16/2009

Dichlorodifluoromethane LCS 56.6 189 * ( 62-153 ) 30 ug/L 02/16/2009

LCSD 55.0 183 * 3 (< 20 ) 30 ug/L 02/16/2009

Chloroethane LCS 30.3 101 ( 67-133 ) 30 ug/L 02/16/2009

LCSD 27.6 92 9 (< 20 ) 30 ug/L 02/16/2009

sec-Butylbenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.4 105 1 (< 20 ) 30 ug/L 02/16/2009

Bromodichloromethane LCS 34.1 114 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 32.0 107 7 (< 20 ) 30 ug/L 02/16/2009

1,1-Dichloroethene LCS 35.1 117 ( 76-130 ) 30 ug/L 02/16/2009

LCSD 32.0 107 9 (< 20 ) 30 ug/L 02/16/2009

2-Butanone (MEK) LCS 103 115 ( 66-136 ) 90 ug/L 02/16/2009

LCSD 93.7 104 10 (< 20 ) 90 ug/L 02/16/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 32.9 110 ( 63-131 ) 30 ug/L 02/16/2009

LCSD 31.4 105 5 (< 20 ) 30 ug/L 02/16/2009

Trichlorofluoromethane LCS 37.7 126 ( 68-145 ) 30 ug/L 02/16/2009

LCSD 33.9 113 11 (< 20 ) 30 ug/L 02/16/2009

P & M -Xylene LCS 68.1 113 ( 80-120 ) 60 ug/L 02/16/2009

LCSD 66.4 111 2 (< 20 ) 60 ug/L 02/16/2009

Naphthalene LCS 31.0 103 ( 75-120 ) 30 ug/L 02/16/2009

LCSD 30.9 103 0 (< 20 ) 30 ug/L 02/16/2009

o-Xylene LCS 33.4 111 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 32.7 109 2 (< 20 ) 30 ug/L 02/16/2009

Bromoform LCS 31.9 106 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.9 103 3 (< 20 ) 30 ug/L 02/16/2009

1-Chlorohexane LCS 49.9 111 ( 70-125 ) 45 ug/L 02/16/2009

LCSD 47.8 106 4 (< 20 ) 45 ug/L 02/16/2009

1,2,4-Trimethylbenzene LCS 31.6 105 ( 80-125 ) 30 ug/L 02/16/2009

LCSD 31.3 104 1 (< 20 ) 30 ug/L 02/16/2009

tert-Butylbenzene LCS 31.4 105 ( 80-122 ) 30 ug/L 02/16/2009

LCSD 30.9 103 1 (< 20 ) 30 ug/L 02/16/2009

1,1,1-Trichloroethane LCS 32.7 109 ( 80-122 ) 30 ug/L 02/16/2009

LCSD 31.0 103 5 (< 20 ) 30 ug/L 02/16/2009

1,1-Dichloroethane LCS 32.6 109 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.7 102 6 (< 20 ) 30 ug/L 02/16/2009

2-Chlorotoluene LCS 30.7 102 ( 80-125 ) 30 ug/L 02/16/2009

LCSD 31.0 103 1 (< 20 ) 30 ug/L 02/16/2009

Trichloroethene LCS 30.8 103 ( 80-125 ) 30 ug/L 02/16/2009

LCSD 28.8 96 7 (< 20 ) 30 ug/L 02/16/2009

trans-1,2-Dichloroethene LCS 31.8 106 ( 79-132 ) 30 ug/L 02/16/2009

LCSD 31.1 104 2 (< 20 ) 30 ug/L 02/16/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 30.5 102 0 (< 20 ) 30 ug/L 02/16/2009

2,2-Dichloropropane LCS 33.4 111 ( 80-132 ) 30 ug/L 02/16/2009

LCSD 31.9 106 5 (< 20 ) 30 ug/L 02/16/2009

Hexachlorobutadiene LCS 28.4 95 ( 77-125 ) 30 ug/L 02/16/2009

LCSD 28.6 95 1 (< 20 ) 30 ug/L 02/16/2009

Isopropylbenzene (Cumene) LCS 33.4 111 ( 80-121 ) 30 ug/L 02/16/2009

LCSD 32.3 108 3 (< 20 ) 30 ug/L 02/16/2009

1,2-Dichloropropane LCS 33.0 110 ( 80-121 ) 30 ug/L 02/16/2009

LCSD 31.4 105 5 (< 20 ) 30 ug/L 02/16/2009

1,1-Dichloropropene LCS 33.0 110 ( 80-122 ) 30 ug/L 02/16/2009

LCSD 31.5 105 5 (< 20 ) 30 ug/L 02/16/2009

1,1,2-Trichloroethane LCS 32.1 107 ( 77-120 ) 30 ug/L 02/16/2009

LCSD 31.7 106 1 (< 20 ) 30 ug/L 02/16/2009

1,3-Dichlorobenzene LCS 31.4 105 ( 80-120 ) 30 ug/L 02/16/2009

LCSD 31.1 104 1 (< 20 ) 30 ug/L 02/16/2009

1,2,3-Trichlorobenzene LCS 30.9 103 ( 77-120 ) 30 ug/L 02/16/2009

LCSD 30.2 101 2 (< 20 ) 30 ug/L 02/16/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 02/16/2009

LCSD 95 3 02/16/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 02/16/2009

LCSD 101 1 02/16/2009

4-Bromofluorobenzene <surr> LCS 95 ( 76-120 ) 02/16/2009

LCSD 99 4 02/16/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Prep

883392 Lab Control Sample

883393 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19212

SW5030B

02/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS10380

SW8260B

HP 5890 Series II MS1 VJA
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

MXX21362

3010 H20 Digest for Metals ICP-MS

02/12/2009

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 877 88 ( 80-120 ) 1000 ug/L 02/17/2009

BMSD 922 92 5 (< 15 ) 1000 ug/L 02/17/2009

Batch

Method

Instrument

MMS5820

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS 14.0 J 423 91 ( 79-108 ) 450 ug/L 02/10/2009

BMSD 411 88 3 (< 20 ) 450 ug/L 02/10/2009

Surrogates 

4-Bromofluorobenzene <surr> BMS 45.2 90 ( 50-150 ) 02/10/2009

BMSD 46.0 92 2 02/10/2009

Batch

Method

Instrument

VFC9351

SW8015C

HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 4.9 88 ( 75-125 ) 5.56 mg/L 02/11/2009

BMSD 5.23 95 6 (< 30 ) 5.49 mg/L 02/11/2009

Surrogates 

5a Androstane <surr> BMS .0984 89 ( 50-150 ) 02/11/2009

BMSD 0.0985 90 0 02/11/2009

Batch

Method

Instrument

XFC8449

SW8015C

HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

VXX19212

Volatiles Extraction AFCEE 3.1 8260 (

02/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS ND 31 103 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 29.4 98 5 (< 20 ) 30.0 ug/L 02/16/2009

Toluene BMS ND 31.7 106 ( 77-120 ) 30.0 ug/L 02/16/2009

BMSD 29.6 99 7 (< 20 ) 30.0 ug/L 02/16/2009

Ethylbenzene BMS ND 33.9 113 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.8 106 6 (< 20 ) 30.0 ug/L 02/16/2009

n-Butylbenzene BMS ND 33.8 113 ( 80-124 ) 30.0 ug/L 02/16/2009

BMSD 31.8 106 6 (< 20 ) 30.0 ug/L 02/16/2009

1,4-Dichlorobenzene BMS ND 32.2 107 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.8 103 5 (< 20 ) 30.0 ug/L 02/16/2009

1,2-Dichloroethane BMS ND 30.9 103 ( 80-129 ) 30.0 ug/L 02/16/2009

BMSD 29.5 98 5 (< 20 ) 30.0 ug/L 02/16/2009

1,3,5-Trimethylbenzene BMS ND 33.7 112 ( 80-128 ) 30.0 ug/L 02/16/2009

BMSD 31.6 105 6 (< 20 ) 30.0 ug/L 02/16/2009

4-Chlorotoluene BMS ND 32.6 109 ( 79-128 ) 30.0 ug/L 02/16/2009

BMSD 31.0 103 5 (< 20 ) 30.0 ug/L 02/16/2009

Chlorobenzene BMS ND 32.7 109 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 5 (< 20 ) 30.0 ug/L 02/16/2009

4-Methyl-2-pentanone (MIBK) BMS ND 97.8 109 ( 69-134 ) 90.0 ug/L 02/16/2009

BMSD 90.2 100 8 (< 20 ) 90.0 ug/L 02/16/2009

cis-1,2-Dichloroethene BMS ND 33.5 112 ( 80-125 ) 30.0 ug/L 02/16/2009

BMSD 31.6 105 6 (< 20 ) 30.0 ug/L 02/16/2009

4-Isopropyltoluene BMS ND 33.7 112 ( 80-125 ) 30.0 ug/L 02/16/2009

BMSD 32.3 108 4 (< 20 ) 30.0 ug/L 02/16/2009

cis-1,3-Dichloropropene BMS ND 32.1 107 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.4 101 6 (< 20 ) 30.0 ug/L 02/16/2009

n-Propylbenzene BMS ND 33.3 111 ( 80-129 ) 30.0 ug/L 02/16/2009

BMSD 31.6 105 5 (< 20 ) 30.0 ug/L 02/16/2009

Styrene BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.5 105 6 (< 20 ) 30.0 ug/L 02/16/2009

Dibromomethane BMS ND 32.1 107 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 02/16/2009

trans-1,3-Dichloropropene BMS ND 30.3 101 ( 80-124 ) 30.0 ug/L 02/16/2009

BMSD 27.6 92 9 (< 20 ) 30.0 ug/L 02/16/2009

1,2,4-Trichlorobenzene BMS ND 32.2 107 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 02/16/2009

Acetone BMS ND 95.7 106 ( 50-135 ) 90.0 ug/L 02/16/2009

BMSD 92.0 102 4 (< 20 ) 90.0 ug/L 02/16/2009

1,1,2,2-Tetrachloroethane BMS ND 32.3 108 ( 76-123 ) 30.0 ug/L 02/16/2009

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 02/16/2009
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

VXX19212

Volatiles Extraction AFCEE 3.1 8260 (

02/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 31.4 105 ( 73-130 ) 30.0 ug/L 02/16/2009

BMSD 30.5 102 3 (< 20 ) 30.0 ug/L 02/16/2009

Methyl-t-butyl ether BMS ND 50 111 ( 80-120 ) 45.0 ug/L 02/16/2009

BMSD 43.6 97 14 (< 20 ) 45.0 ug/L 02/16/2009

Tetrachloroethene BMS ND 34.3 114 ( 79-122 ) 30.0 ug/L 02/16/2009

BMSD 31.6 105 8 (< 20 ) 30.0 ug/L 02/16/2009

Dibromochloromethane BMS ND 29.5 98 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 27.1 90 8 (< 20 ) 30.0 ug/L 02/16/2009

1,3-Dichloropropane BMS ND 32.8 109 ( 80-121 ) 30.0 ug/L 02/16/2009

BMSD 30.9 103 6 (< 20 ) 30.0 ug/L 02/16/2009

1,2-Dibromoethane BMS ND 32.5 108 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.5 102 6 (< 20 ) 30.0 ug/L 02/16/2009

Carbon tetrachloride BMS ND 35.2 117 ( 80-126 ) 30.0 ug/L 02/16/2009

BMSD 32.7 109 7 (< 20 ) 30.0 ug/L 02/16/2009

1,1,1,2-Tetrachloroethane BMS ND 30.6 102 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 28.7 96 6 (< 20 ) 30.0 ug/L 02/16/2009

Chloroform BMS ND 31.1 104 ( 80-124 ) 30.0 ug/L 02/16/2009

BMSD 29.4 98 6 (< 20 ) 30.0 ug/L 02/16/2009

Bromobenzene BMS ND 31.7 106 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.0 100 5 (< 20 ) 30.0 ug/L 02/16/2009

Chloromethane BMS ND 54.3 181* ( 67-125 ) 30.0 ug/L 02/16/2009

BMSD 50.5 168* 7 (< 20 ) 30.0 ug/L 02/16/2009

1,2,3-Trichloropropane BMS ND 33.1 110 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 6 (< 20 ) 30.0 ug/L 02/16/2009

Bromomethane BMS ND 37.6 125 ( 30-140 ) 30.0 ug/L 02/16/2009

BMSD 39.7 132 5 (< 20 ) 30.0 ug/L 02/16/2009

Bromochloromethane BMS ND 34.1 114 ( 77-129 ) 30.0 ug/L 02/16/2009

BMSD 32.1 107 6 (< 20 ) 30.0 ug/L 02/16/2009

Vinyl chloride BMS ND 47.5 158* ( 72-145 ) 30.0 ug/L 02/16/2009

BMSD 45.0 150* 5 (< 20 ) 30.0 ug/L 02/16/2009

Dichlorodifluoromethane BMS ND 56.3 188* ( 62-153 ) 30.0 ug/L 02/16/2009

BMSD 52.8 176* 7 (< 20 ) 30.0 ug/L 02/16/2009

Chloroethane BMS ND 30.1 100 ( 67-133 ) 30.0 ug/L 02/16/2009

BMSD 27.4 91 9 (< 20 ) 30.0 ug/L 02/16/2009

sec-Butylbenzene BMS ND 32.6 109 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 5 (< 20 ) 30.0 ug/L 02/16/2009

Bromodichloromethane BMS ND 33.8 113 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 32.0 107 6 (< 20 ) 30.0 ug/L 02/16/2009

1,1-Dichloroethene BMS ND 33.1 110 ( 76-130 ) 30.0 ug/L 02/16/2009

BMSD 31.7 106 4 (< 20 ) 30.0 ug/L 02/16/2009
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

VXX19212

Volatiles Extraction AFCEE 3.1 8260 (

02/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 104 115 ( 66-136 ) 90.0 ug/L 02/16/2009

BMSD 97.8 109 6 (< 20 ) 90.0 ug/L 02/16/2009

Methylene chloride BMS ND 32.7 109 ( 63-131 ) 30.0 ug/L 02/16/2009

BMSD 31.2 104 5 (< 20 ) 30.0 ug/L 02/16/2009

Trichlorofluoromethane BMS ND 35.6 119 ( 68-145 ) 30.0 ug/L 02/16/2009

BMSD 32.4 108 9 (< 20 ) 30.0 ug/L 02/16/2009

P & M -Xylene BMS ND 68.3 114 ( 80-120 ) 60.0 ug/L 02/16/2009

BMSD 64.6 108 6 (< 20 ) 60.0 ug/L 02/16/2009

Naphthalene BMS ND 33.1 110 ( 75-120 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 6 (< 20 ) 30.0 ug/L 02/16/2009

o-Xylene BMS ND 33.8 113 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 8 (< 20 ) 30.0 ug/L 02/16/2009

Bromoform BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 28.6 95 6 (< 20 ) 30.0 ug/L 02/16/2009

1-Chlorohexane BMS ND 50.7 113 ( 70-125 ) 45.0 ug/L 02/16/2009

BMSD 48.2 107 5 (< 20 ) 45.0 ug/L 02/16/2009

1,2,4-Trimethylbenzene BMS ND 33.1 110 ( 80-125 ) 30.0 ug/L 02/16/2009

BMSD 31.1 104 6 (< 20 ) 30.0 ug/L 02/16/2009

tert-Butylbenzene BMS ND 33 110 ( 80-122 ) 30.0 ug/L 02/16/2009

BMSD 31.2 104 5 (< 20 ) 30.0 ug/L 02/16/2009

1,1,1-Trichloroethane BMS ND 33 110 ( 80-122 ) 30.0 ug/L 02/16/2009

BMSD 31.5 105 5 (< 20 ) 30.0 ug/L 02/16/2009

1,1-Dichloroethane BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.5 102 9 (< 20 ) 30.0 ug/L 02/16/2009

2-Chlorotoluene BMS ND 32.5 108 ( 80-125 ) 30.0 ug/L 02/16/2009

BMSD 30.6 102 6 (< 20 ) 30.0 ug/L 02/16/2009

Trichloroethene BMS ND 31.1 104 ( 80-125 ) 30.0 ug/L 02/16/2009

BMSD 29.5 98 5 (< 20 ) 30.0 ug/L 02/16/2009

trans-1,2-Dichloroethene BMS ND 48.4 161* ( 79-132 ) 30.0 ug/L 02/16/2009

BMSD 32.2 107 40 * (< 20 ) 30.0 ug/L 02/16/2009

1,2-Dichlorobenzene BMS ND 31.2 104 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 02/16/2009

2,2-Dichloropropane BMS ND 35.3 118 ( 80-132 ) 30.0 ug/L 02/16/2009

BMSD 33.0 110 7 (< 20 ) 30.0 ug/L 02/16/2009

Hexachlorobutadiene BMS ND 29.4 98 ( 77-125 ) 30.0 ug/L 02/16/2009

BMSD 29.0 97 1 (< 20 ) 30.0 ug/L 02/16/2009

Isopropylbenzene (Cumene) BMS ND 33.3 111 ( 80-121 ) 30.0 ug/L 02/16/2009

BMSD 31.5 105 6 (< 20 ) 30.0 ug/L 02/16/2009

1,2-Dichloropropane BMS ND 33.4 111 ( 80-121 ) 30.0 ug/L 02/16/2009

BMSD 31.8 106 5 (< 20 ) 30.0 ug/L 02/16/2009
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

VXX19212

Volatiles Extraction AFCEE 3.1 8260 (

02/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 34.1 114 ( 80-122 ) 30.0 ug/L 02/16/2009

BMSD 31.6 105 8 (< 20 ) 30.0 ug/L 02/16/2009

1,1,2-Trichloroethane BMS ND 33.3 111 ( 77-120 ) 30.0 ug/L 02/16/2009

BMSD 31.3 104 6 (< 20 ) 30.0 ug/L 02/16/2009

1,3-Dichlorobenzene BMS ND 32.6 109 ( 80-120 ) 30.0 ug/L 02/16/2009

BMSD 30.7 102 6 (< 20 ) 30.0 ug/L 02/16/2009

1,2,3-Trichlorobenzene BMS ND 31.8 106 ( 77-120 ) 30.0 ug/L 02/16/2009

BMSD 30.5 102 4 (< 20 ) 30.0 ug/L 02/16/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 28.9 96 ( 73-120 ) 02/16/2009

BMSD 29.1 97 1 02/16/2009

Toluene-d8 <surr> BMS 29.9 100 ( 80-120 ) 02/16/2009

BMSD 29.4 98 2 02/16/2009

4-Bromofluorobenzene <surr> BMS 29.9 100 ( 76-120 ) 02/16/2009

BMSD 29.9 100 0 02/16/2009

Batch

Method

Instrument

VMS10380

SW8260B

HP 5890 Series II MS1 VJA

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

XXX20586

3520 Liquid/Liquid Ext for 8270 SIM

02/10/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .345 60 ( 50-105 ) 0.575 ug/L 02/10/2009

BMSD 0.313 58 10 (< 30 ) 0.538 ug/L 02/10/2009

Acenaphthene BMS ND .332 58 ( 45-110 ) 0.575 ug/L 02/10/2009

BMSD 0.311 58 7 (< 30 ) 0.538 ug/L 02/10/2009

Fluorene BMS ND .351 61 ( 50-110 ) 0.575 ug/L 02/10/2009

BMSD 0.326 61 7 (< 30 ) 0.538 ug/L 02/10/2009

Phenanthrene BMS ND .348 61 ( 50-115 ) 0.575 ug/L 02/10/2009

BMSD 0.332 62 5 (< 30 ) 0.538 ug/L 02/10/2009

Anthracene BMS ND .352 61 ( 55-110 ) 0.575 ug/L 02/10/2009

BMSD 0.329 61 7 (< 30 ) 0.538 ug/L 02/10/2009

Fluoranthene BMS ND .42 73 ( 55-125 ) 0.575 ug/L 02/10/2009

BMSD 0.395 73 6 (< 30 ) 0.538 ug/L 02/10/2009

Pyrene BMS ND .41 71 ( 50-130 ) 0.575 ug/L 02/10/2009

BMSD 0.380 71 8 (< 30 ) 0.538 ug/L 02/10/2009

Benzo(a)Anthracene BMS ND .413 72 ( 55-120 ) 0.575 ug/L 02/10/2009

BMSD 0.383 71 8 (< 30 ) 0.538 ug/L 02/10/2009

Chrysene BMS ND .409 71 ( 55-120 ) 0.575 ug/L 02/10/2009

BMSD 0.375 70 9 (< 30 ) 0.538 ug/L 02/10/2009

Benzo[b]Fluoranthene BMS ND .411 72 ( 46-130 ) 0.575 ug/L 02/10/2009

BMSD 0.389 72 6 (< 30 ) 0.538 ug/L 02/10/2009

Benzo[k]fluoranthene BMS ND .426 74 ( 60-125 ) 0.575 ug/L 02/10/2009

BMSD 0.386 72 10 (< 30 ) 0.538 ug/L 02/10/2009

Benzo[a]pyrene BMS ND .432 75 ( 55-120 ) 0.575 ug/L 02/10/2009

BMSD 0.391 73 10 (< 30 ) 0.538 ug/L 02/10/2009

Indeno[1,2,3-c,d] pyrene BMS ND .435 76 ( 45-125 ) 0.575 ug/L 02/10/2009

BMSD 0.387 72 12 (< 30 ) 0.538 ug/L 02/10/2009

Dibenzo[a,h]anthracene BMS ND .445 77 ( 41-140 ) 0.575 ug/L 02/10/2009

BMSD 0.395 73 12 (< 30 ) 0.538 ug/L 02/10/2009

Benzo[g,h,i]perylene BMS ND .422 73 ( 46-125 ) 0.575 ug/L 02/10/2009

BMSD 0.390 73 8 (< 30 ) 0.538 ug/L 02/10/2009

Naphthalene BMS ND .334 58 ( 42-100 ) 0.575 ug/L 02/10/2009

BMSD 0.307 57 9 (< 30 ) 0.538 ug/L 02/10/2009

1-Methylnaphthalene BMS ND .332 58 ( 46-115 ) 0.575 ug/L 02/10/2009

BMSD 0.301 56 10 (< 30 ) 0.538 ug/L 02/10/2009

2-Methylnaphthalene BMS ND .32 56 ( 45-105 ) 0.575 ug/L 02/10/2009

BMSD 0.289 54 10 (< 30 ) 0.538 ug/L 02/10/2009

Surrogates 

Terphenyl-d14 <surr> BMS .456 79 ( 50-135 ) 02/10/2009

BMSD 0.425 79 7 02/10/2009
Matrix

SGS Ref.# Printed Date/Time 02/19/2009 10:58

Batch

Method

Date

Original

Prep

1090476002 Billable Matrix Spike

1090476003 Billable Matrix Spike Dup.

1090476001

Water (Surface, Eff., Ground)

XXX20586

3520 Liquid/Liquid Ext for 8270 SIM

02/10/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4825

8270D SIMS

HP 6890/5973 MS SVOA