November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC General Company and Facility Information

Instructions

Please complete this worksheet for your parent company and PVC production facility.

Parent Company General Information

Parent Company Name:

Address:

City:

Country: USA

Size of Company (approximate number of employees including all subsidiaries, branches, and related establishments 

PVC Production Facility General Information

Facility Name:

Facility Address:

Facility City:

Facility Technical Contact Name:

Technical Contact Telephone Number:

Technical Contact Email:

Number of employees attached to the PVC production facility: 80

Avon Lake

33857 Walker Rd

PolyOne Corp

856-299-8413

otis.sistrunk@polyone.com

Pedricktown

Rt 130 & Porcupine Rd

Pedricktown

Otis Sistrunk
ers (PVC) Production Process Wastewater

State: OH Zip Code: 44012

hes, and related establishments owned): 7000

State: NJ Zip Code: 8067
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC Production Process Wastewater Treatment System Information Update

Instructions

2. Also complete the additional supplemental questions to Form C-1-c.

FORM C-1-c

PROCESS EQUIPMENT - WASTEWATER STEAM STRIPPER

Process Unit ID: P-1

Process Equipment ID: U-17

Wastewater Feed Rate (lb/hr): 37,350

Feed Temperature (°F): 100

Feed Inlet Pressure (psia): 64.5

Liquid Loading Rate (liters/m2):

Steam Feed Rate (lb/hr):

Steam to Feed Ratio (kg steam/liter of wastewater):

Operating Temperature (°F): 185

Operating Pressure (psig):

Total Number of Stages: 2

Overall Calculated Tray Efficiency:

Stripping Factor:

Flow configuration (countercurrent, cocurrent): Countercurrent

Number of Actual Trays: 0

Column Height (meters): 8.08

Year Equipment Installed: 1978

Equipment Currently Regulated Under (cite regulations):

1. A copy of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included w

below.
mers (PVC) Production Process Wastewater

Form C-1-c Supplemental Questions

Please also provide the stripper feed rate in liters per hour, or liters for batch strippers:

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, plea

ection 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous respons
 batch strippers: 17744 liters/hour

 liters

m design rate or capacity, please provide those values:

 liters/hour (max design)

 liters (max design)

eview those previous responses and update if necessary
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC Production Process Wastewater Stream Information

Instructions

1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production fa

2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wa

3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for e

Table 1. Process Wastewater Streams Not Treated by a PVC Process Wastewater Treatment System

1 3

U20 8

U31 25

Permeate (North)

Permeate (South)

2

PVC Process 

Unit ID Name of PVC Process Wastewater Stream

PVC Process 

Wastewater 

Stream ID
Table 2. Process Wastewater Streams Exiting a PVC Process Wastewater Treatment System

1 2 3 4 5 6

Min

U17 Steam Stripping Continuous 44 30000

Table 3. PVC Process Wastewater Destination Codes Table

Wastewater treatment system

Discharge without treatment by pipeline, sewer, or other conveyance to surface water

Discharge to POTW, no treatment

Discharge to PrOTW, no treatment

Zero discharge or alternative disposal method

Recycle to process

Other

Table 4. Non-PVC Production Process Wastewater Streams Entering a PVC Process Wastewater Treatment S

2 3

Min Max

PVC Process Wastewate

1

Process Wastewater Stream Flow Rate 

Source of Process Wastewater Stream (gallons per day)

Destination Description

PVC Process 

Wastewater 

Treatment 

System ID

PVC Process 

Unit ID

PVC Process 

Wastewater 

Stream ID

Is this 

process 

wastewater 

treatment 

system batch 

or continuous 

operation?

Type of Process 

Wastewater 

Treatment System

VC) Production Process Wastewater

hin the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process waste

VC production process wastewater treatment system.

ter treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC prod

tment System

4 5 6 7 8

Min Max Average

0 43000 15000 Measured 12

0 43000 15000 Measured 12

Flow Rate 

Determination 

Method

PVC Process Wastewater Stream Flow Rate 

(gallons per day) Operating Days Per 

Year
7 8 9 10 11

Max Average

90000 45200 Measured 360 WWT

Code

WWT Provide name of the wastewater treatment system

SW Provide name of outfall

POTWRAW Provide name of POTW

PrOTWRAW Provide name of PrOTW

ZEROALT Describe method

RECYC Describe where in the process the stream is recycled

OTHER Describe

Wastewater Treatment System

4 5 6 7

Average

Flow Rate 

Determination 

Method

PVC Process 

Wastewater 

Treatment 

System ID

VC Process Wastewater Stream Flow Rate 

(gallons per day)

Flow Rate 

Determination 

Method

Operating Days 

Per Year

water Stream Flow Rate 

ons per day)

Process Wastewater Destination D

PVC Process 

Wastewater Stream 

Destination Code

(Refer to Table 3 below)

Operating Days 

Per Year

eated by a PVC production process wastewater treatment system.

hat does not originate from the PVC production facility.

9 10

Fil 1N/Fil 2N UF System (North)

Fil 3N/Fil 4N UF System (South)

Originating PVC Process 

Equipment ID

Originating PVC Process 

Equipment Description
12 13

Yes

e of the wastewater treatment system

ere in the process the stream is recycled

Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2

Associated Destination 

Information

(Refer to Table 3 below)

Is this PVC process wastewater 

stream exposed to the atmosphere 

at any point between the outlet of 

the PVC process wastewater 

treatment system and its 

destination?

11 12

WWT

WWT

PVC Process Wastewater Stream 

Destination Code

(Refer to Table 3 below)

Associated Destination Information
able 1 and Column 11 of Table 2

14

If your response in Column 3 is "Other" then please provide a description of the process wastewaetr 

treatment system

13

Yes

Yes

Is this PVC process wastewater 

stream exposed to the atmosphere 

at any point between the 

originating PVC process equipment 

and its destination?
de a description of the process wastewaetr 
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Process Wastewater

PVC Production Process Wastewater Sampling and Analysis Data

Instructions

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Complete one worksheet for each single stream (make copies of this worksheet if necessary).

2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet.

3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed.

4. Enter any other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below.

4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column.

5. Enter any notes or additional information relevant to the sampling or analysis.

Company PolyOne Corp

Facility Pedricktown

PVC Process Wastewater Treatment System ID P-1

CAS No. HAP Analysis Method Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

107211 Ethylene glycol SW-846-8015C 10 Non-detect U 10 Non-detect U 10 Non-detect U 10 Non-detect U 10 Non-detect U 10 Non-detect U 10 Non-detect

67561 Methanol SW-846-8015C 75.2 55 37.4 46.4 39.5 20.4 29.1

75070 Acetaldehyde SW-846-8315A 4.53 8.77 7.1 6.04 6.3 6.23 8.64

50000 Formaldehyde SW-846-8315A 0.0755 0.241 0.0619 0.361 0.0669 0.158 0.217

51285 2,4-dinitrophenol SW-846-8270D 0.17 Non-detect U 17 Non-detect U 0.17 Non-detect U 0.17 Non-detect U 1.7 Non-detect U 1.7 Non-detect U 1.7 Non-detect

98862 Acetophenone SW-846-8270D 2.69 3.52 0.966 1.39 1.57 1.24 0.683

117817 Bis(2-ethylhexyl) phthalate (DEHP) SW-846-8270D 0.0059 Non-detect U 0.59 Non-detect U 0.0059 Non-detect U 0.0059 Non-detect U 0.059 Non-detect U 0.059 Non-detect U 0.059 Non-detect

123319 Hydroquinone SW-846-8270D 0.05 Non-detect U 5 Non-detect U 0.05 Non-detect U 0.05 Non-detect U 0.5 Non-detect U 0.5 Non-detect U 0.5 Non-detect

108952 Phenol SW-846-8270D 0.013 Non-detect U 1.3 Non-detect U 0.013 Non-detect U 0.013 Non-detect U 0.13 Non-detect U 0.13 Non-detect U 0.13 Non-detect

79345 1,1,2,2-tetrachloroethane SW-846-8260B 0.0011 Non-detect U 0.0011 Non-detect U 0.011 Non-detect U 0.0021 Non-detect U 0.0011 Non-detect U 0.0043 Non-detect U 0.0011 Non-detect

106990 1,3-butadiene SW-846-8260B 0.0095 Non-detect U 0.0095 Non-detect U 0.095 Non-detect U 0.019 Non-detect U 0.0095 Non-detect U 0.038 Non-detect U 0.0095 Non-detect

540841 2,2,4-trimethylpentane SW-846-8260B 0.0011 Non-detect U 0.0011 Non-detect U 0.011 Non-detect U 0.0023 Non-detect U 0.0011 Non-detect U 0.0045 Non-detect U 0.0011 Non-detect

71432 Benzene SW-846-8260B 0.0012 Non-detect U 0.0012 Non-detect U 0.012 Non-detect U 0.0024 Non-detect U 0.0012 Non-detect U 0.0047 Non-detect U 0.0012 Non-detect

108907 Chlorobenzene SW-846-8260B 0.0011 Non-detect U 0.0011 Non-detect U 0.011 Non-detect U 0.0023 Non-detect U 0.0011 Non-detect U 0.0046 Non-detect U 0.0011 Non-detect

67663 Chloroform SW-846-8260B 0.001 Non-detect U 0.001 Non-detect U 0.01 Non-detect U 0.002 Non-detect U 0.001 Non-detect U 0.0041 Non-detect U 0.001 Non-detect

126998 Chloroprene SW-846-8260B 0.001 Non-detect U 0.001 Non-detect U 0.01 Non-detect U 0.0021 Non-detect U 0.001 Non-detect U 0.0042 Non-detect U 0.001 Non-detect

98828 Cumene SW-846-8260B 0.0022 Non-detect U 0.0022 Non-detect U 0.022 Non-detect U 0.0045 Non-detect U 0.0022 Non-detect U 0.0089 Non-detect U 0.0022 Non-detect

75003 Ethyl chloride (Chloroethane) SW-846-8260B 0.4 0.252 1.39 0.208 0.148 0.361 0.159

100414 Ethylbenzene SW-846-8260B 0.0011 Non-detect U 0.0011 Non-detect U 0.011 Non-detect U 0.0023 Non-detect U 0.0011 Non-detect U 0.0046 Non-detect U 0.0011 Non-detect

107062 Ethylene dichloride (1,2-Dichloroethane) SW-846-8260B 0.0158 0.0139 0.0499 J 0.0087 J 0.0102 0.0302 0.0086

75343 Ethylidene dichloride (1,1-Dichloroethane) SW-846-8260B 0.00053 Non-detect U 0.00053 Non-detect U 0.0053 Non-detect U 0.0011 Non-detect U 0.00053 Non-detect U 0.0021 Non-detect U 0.00053 Non-detect

74873 Methyl chloride (Chloromethane) SW-846-8260B 0.869 0.777 4.92 0.694 0.433 1.11 0.579

75092 Methylene chloride SW-846-8260B 0.0035 Non-detect U 0.0035 Non-detect U 0.035 Non-detect U 0.007 Non-detect U 0.0035 Non-detect U 0.014 Non-detect U 0.0035 Non-detect

110543 n-Hexane SW-846-8260B 0.0023 Non-detect U 0.0023 Non-detect U 0.023 Non-detect U 0.0046 Non-detect U 0.0023 Non-detect U 0.0093 Non-detect U 0.0023 Non-detect

108883 Toluene SW-846-8260B 0.0011 Non-detect U 0.0011 Non-detect U 0.011 Non-detect U 0.0023 Non-detect U 0.0011 Non-detect U 0.0045 Non-detect U 0.0011 Non-detect

71556 Methyl chloroform (1,1,1-Trichloroethane) SW-846-8260B 0.0012 Non-detect U 0.0012 Non-detect U 0.012 Non-detect U 0.0024 Non-detect U 0.0012 Non-detect U 0.0047 Non-detect U 0.0012 Non-detect

79005 1,1,2-Trichloroethane SW-846-8260B 0.0014 Non-detect U 0.0014 Non-detect U 0.014 Non-detect U 0.0029 Non-detect U 0.0014 Non-detect U 0.0057 Non-detect U 0.0014 Non-detect

108054 Vinyl acetate SW-846-8260B 0.0056 Non-detect U 0.0056 Non-detect U 0.056 Non-detect U 0.011 Non-detect U 0.0056 Non-detect U 0.022 Non-detect U 0.0056 Non-detect

593602 Vinyl bromide SW-846-8260B 0.0013 Non-detect U 0.0013 Non-detect U 0.013 Non-detect U 0.0027 Non-detect U 0.0013 Non-detect U 0.0054 Non-detect U 0.0013 Non-detect

75014 Vinyl chloride EPA Method 107 3.818 4.082 9.281 4.477 0.019 5.766 2.405

75354 Vinylidene chloride (1,1-Dichloroethylene) SW-846-8260B 0.00096 Non-detect U 0.00096 Non-detect U 0.0096 Non-detect U 0.0019 Non-detect U 0.00096 Non-detect U 0.0038 Non-detect U 0.00096 Non-detect

1330207 Xylenes (isomers and mixtures) SW-846-8260B 0.0012 Non-detect U 0.0012 Non-detect U 0.012 Non-detect U 0.0024 Non-detect U 0.0012 Non-detect U 0.0048 Non-detect U 0.0012 Non-detect

JB25234 JB25235 JB25236 JB25238 JB25239

See Lab Report

22 20 21

01/08/13 01/09/13

6

01/10/13 01/14/13

Measured

2

01/15/13

Measured Measured Measured Measured Measured

1

185

25

01/07/13

3 4

185 185 185

Lab Sample ID -->

Lab Report ID -->

Analysis Date -->

Stream Temperature (degrees F) -->

JB25233-1 JB25234-1 JB25235-1 JB25236-1 JB25238-1 JB25239-1

JB25233

See Lab Report

185

See Lab Report

JB25237

JB25237-1

See Lab Report See Lab Report

Stream Flow Rate (gallons per minute) -->

Resin Type (suspension, dispersion, bulk, etc.) -->

185

See Lab Report

20

See Lab Report

Flow Rate Determination Method -->

21

Measured

Sample Date -->

Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion

5

01/11/13

Suspension/Dispersion
Note(s) Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

U 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detect

24.9 22.8 27.5 56.6 3.49 18.2 25 17.5 22.8 30.5 46.9 26.4 16.1 19.6 14.4

8.29 8.5 7.03 6.14 7.93 7.45 6.22 6.77 2.98 7.93 7.33 6.22 7.22 4.49 5.19

0.556 0.31 0.254 0.214 0.455 0.228 0.321 0.432 0.106 0.171 0.212 0.217 0.193 0.14 0.122

U 1.7 Non-detectU 1.7 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.17 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.083 Non-detectU 0.017 Non-detectU 0.17 Non-detectU 0.17 Non-detectU 0.083 Non-detectU 0.017 Non-detect

0.291 0.18J 0.0652 0.54 0.687 0.899 2.38 0.731 0.479 0.3050 0.395 0.795 0.808 0.376 0.584

U 0.059 Non-detectU 0.059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.0059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.0029 Non-detectU 0.00059 Non-detectU 0.0059 Non-detectU 0.0059 Non-detectU 0.0029 Non-detectU 0.00059 Non-detect

U 0.5 Non-detectU 0.5 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.05 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.0025 Non-detectU 0.005 Non-detectU 0.05 Non-detectU 0.05 Non-detectU 0.025 Non-detectU 0.005 Non-detect

U 0.13 Non-detectU 0.13 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0022 0.0013 Non-detectU 0.013 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0064 Non-detectU 0.0013 Non-detectU 0.013 Non-detectU 0.013 Non-detectU 0.0064 Non-detectU 0.0013 Non-detect

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0054 Non-detectU 0.0021 Non-detectU 0.0011 Non-detectU 0.0021 Non-detectU 0.011 Non-detectU 0.00021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.0011 Non-detectU 0.0011 Non-detect

U 0.0095 Non-detectU 0.0095 Non-detectU 0.0095 Non-detectU 0.0095 Non-detectU 0.0095 Non-detectU 0.048 Non-detectU 0.019 Non-detectU 0.0095 Non-detectU 0.019 Non-detectU 0.095 Non-detectU 0.0019 Non-detectU 0.019 Non-detectU 0.019 Non-detectU 0.0095 Non-detectU 0.0095 Non-detect

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0056 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0023 Non-detectU 0.011 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0011 Non-detect

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0059 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0024 Non-detectU 0.012 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0012 Non-detect

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0057 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0023 Non-detectU 0.011 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0011 Non-detect

U 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.0051 Non-detectU 0.002 Non-detectU 0.001 Non-detectU 0.002 Non-detectU 0.01 Non-detectU 0.0002 Non-detectU 0.002 Non-detectU 0.002 Non-detectU 0.001 Non-detectU 0.001 Non-detect

U 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.001 Non-detectU 0.0052 Non-detectU 0.0021 Non-detectU 0.001 Non-detectU 0.0021 Non-detectU 0.01 Non-detectU 0.00021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.001 Non-detectU 0.001 Non-detect

U 0.0022 Non-detectU 0.0022 Non-detectU 0.0022 Non-detectU 0.0022 Non-detectU 0.0022 Non-detectU 0.011 Non-detectU 0.0045 Non-detectU 0.0022 Non-detectU 0.0045 Non-detectU 0.022 Non-detectU 0.00045 Non-detectU 0.0045 Non-detectU 0.0045 Non-detectU 0.0022 Non-detectU 0.0022 Non-detect

0.186 0.235 0.0769 0.23 0.288 0.477 0.168 0.215 0.234 0.426 0.103 0.235 0.21 0.163 0.126

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0057 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0023 Non-detectU 0.011 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0011 Non-detect

0.0107 0.0129 0.0058 0.0119 0.0139 0.0268 0.0088J 0.012 0.0136 0.0167J 0.0151 0.0149 0.0148 0.0075 0.0129

U 0.00053 Non-detectU 0.00053 Non-detectU 0.00053 Non-detectU 0.00053 Non-detectU 0.00053 Non-detectU 0.0027 Non-detectU 0.0011 Non-detectU 0.00053 Non-detectU 0.0011 Non-detectU 0.0053 Non-detectU 0.00011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.00053 Non-detectU 0.00053 Non-detect

0.605 0.727 0.268 0.712 0.928 1.62 0.652 0.712 0.863 1.4 0.296 0.922 0.825 0.535 0.425

U 0.0035 Non-detectU 0.0035 Non-detectU 0.0035 Non-detectU 0.0035 Non-detectU 0.0035 Non-detectU 0.018 Non-detectU 0.007 Non-detectU 0.0035 Non-detectU 0.007 Non-detectU 0.035 Non-detectU 0.0007 Non-detectU 0.007 Non-detectU 0.007 Non-detectU 0.0035 Non-detectU 0.0035 Non-detect

U 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.012 Non-detectU 0.0046 Non-detectU 0.0023 Non-detectU 0.0046 Non-detectU 0.023 Non-detectU 0.00046 Non-detectU 0.0046 Non-detectU 0.0046 Non-detectU 0.0023 Non-detectU 0.0023 Non-detect

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0057 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0023 Non-detectU 0.011 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0011 Non-detectU 0.0011 Non-detect

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0059 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0024 Non-detectU 0.012 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0012 Non-detect

U 0.0014 Non-detectU 0.0014 Non-detectU 0.0014 Non-detectU 0.0014 Non-detectU 0.0014 Non-detectU 0.0072 Non-detectU 0.0029 Non-detectU 0.0014 Non-detectU 0.0029 Non-detectU 0.014 Non-detectU 0.00029 Non-detectU 0.0029 Non-detectU 0.0029 Non-detectU 0.0014 Non-detectU 0.0014 Non-detect

U 0.0056 Non-detectU 0.0056 Non-detectU 0.0056 Non-detectU 0.0056 Non-detectU 0.0056 Non-detectU 0.028 Non-detectU 0.011 Non-detectU 0.0056 Non-detectU 0.011 Non-detectU 0.056 Non-detectU 0.0011 Non-detectU 0.011 Non-detectU 0.011 Non-detectU 0.0056 Non-detectU 0.0056 Non-detect

U 0.0013 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0067 Non-detectU 0.0027 Non-detectU 0.0013 Non-detectU 0.0027 Non-detectU 0.013 Non-detectU 0.00027 Non-detectU 0.0027 Non-detectU 0.0027 Non-detectU 0.0013 Non-detectU 0.0013 Non-detect

3.758 3.009 2.224 1.837 6.352 3.206 3.436 5.026 1.917 9.631 3.943 4.58 4.23 2.86 2.78

U 0.00096 Non-detectU 0.00096 Non-detectU 0.00096 Non-detectU 0.00096 Non-detectU 0.00096 Non-detectU 0.0048 Non-detectU 0.0019 Non-detectU 0.00096 Non-detectU 0.0019 Non-detectU 0.0096 Non-detectU 0.00019 Non-detectU 0.0019 Non-detectU 0.0019 Non-detectU 0.00096 Non-detectU 0.00096 Non-detect

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.0012 Non-detectU 0.006 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0024 Non-detectU 0.012 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0012 Non-detectU 0.0012 Non-detect

Measured

185 185 185 185 185

25

Measured Measured Measured Measured Measured Measured

JB25243-1 JB25244-1 JB25245-1 JB25247-1

JB25251

185

02/11/13

185

JB25252

JB25248-1 JB25249-1 JB25250-1 JB25251-1 JB25252-1

See Lab Report See Lab Report

JB25248 JB25249 JB25250

See Lab Report See Lab Report

JB25253-1 JB25254-1 JB25255-1

JB25253 JB25254

02/13/13 02/14/13

22 23

Measured

See Lab Report See Lab Report See Lab Report

JB25255

24 20

JB25239 JB25240 JB25241 JB25242 JB25243 JB25244 9 10 19

02/04/13

12

20 22 22

Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion

22

Suspension/Dispersion

13 14 15

22 20 20 23

16

See Lab Report See Lab Report See Lab Report See Lab Report See Lab Report See Lab Report See Lab Report See Lab Report See Lab Report

185 185 185 185

01/15/13

Measured Measured

185

Measured Measured Measured Measured

01/23/13

185 185 185

78

JB25239-1

JB25245 JB25247

JB25240-1 JB25241-1 JB25242-1

Suspension/Dispersion Suspension/Dispersion

Measured Measured

20 212 21

Suspension/Dispersion Suspension/Dispersion

01/16/13

Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion

01/17/13 01/20/13 01/22/13

20

02/08/13 02/12/13

17 18

02/05/13 02/06/13 02/07/13
Note(s) Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

U 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU 10 Non-detectU

17 31.8 13.4 7.78 7.33 44 50.9 50.9

5.13 2.28 4.6 7.72 4.56 3.9 2.88 2.88

0.0386 0.102J 0.0875 0.447 0.128 0.112 0.2 0.2

U 0.017 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.083 Non-detectU 0.017 Non-detectU 0.017 Non-detectU 0.017 Non-detectU

2.45 1.11 1.02 3.2 1.19 0.497 1.18 1.18

U 0.00059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.0029 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU 0.00059 Non-detectU

U 0.005 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.025 Non-detectU 0.005 Non-detectU 0.005 Non-detectU 0.005 Non-detectU

U 0.0013 Non-detectU 0.0013 Non-detectU 0.0013 Non-detectU 0.0027 Non-detect 0.0064 Non-detectU 0.0022 0.0032 0.0032 Non-detect

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0043 Non-detectU 0.00021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU

U 0.0095 Non-detectU 0.0095 Non-detectU 0.038 Non-detectU 0.0019 Non-detectU 0.019 Non-detectU 0.019 Non-detectU 0.019 Non-detectU 0.019 Non-detectU

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0045 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0047 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0046 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU

U 0.001 Non-detectU 0.001 Non-detectU 0.0041 Non-detectU 0.0002 Non-detectU 0.002 Non-detectU 0.002 Non-detectU 0.002 Non-detectU 0.002 Non-detectU

U 0.001 Non-detectU 0.001 Non-detectU 0.0042 Non-detectU 0.00021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU 0.0021 Non-detectU

U 0.0022 Non-detectU 0.0022 Non-detectU 0.0089 Non-detectU 0.0013 Non-detectJ 0.0045 Non-detectU 0.0045 Non-detectU 0.0045 Non-detectU 0.0045 Non-detectU

0.13 0.693 0.868 0.151 0.0635 0.0821 0.178 0.178

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0046 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU

0.0174 0.0393 0.0508 0.0606 0.005J 0.0088J 0.01J 0.01J

U 0.00053 Non-detectU 0.00053 Non-detectU 0.0021 Non-detectU 0.0013 Non-detect 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU 0.0011 Non-detectU

0.344 3.41 3.29 0.32 0.186 0.182 0.394 0.394

U 0.0035 Non-detectU 0.0035 Non-detectU 0.014 Non-detectU 0.0007 Non-detectU 0.007 Non-detectU 0.007 Non-detectU 0.007 Non-detectU 0.007 Non-detectU

U 0.0023 Non-detectU 0.0023 Non-detectU 0.0093 Non-detectU 0.00046 Non-detectU 0.0046 Non-detectU 0.0046 Non-detectU 0.0046 Non-detectU 0.0046 Non-detectU

U 0.0011 Non-detectU 0.0011 Non-detectU 0.0045 Non-detectU 0.00023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU 0.0023 Non-detectU

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0047 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU

U 0.0014 Non-detectU 0.0014 Non-detectU 0.0057 Non-detectU 0.0018 Non-detect 0.0029 Non-detectU 0.0029 Non-detectU 0.0029 Non-detectU 0.0029 Non-detectU

U 0.0056 Non-detectU 0.0056 Non-detectU 0.022 Non-detectU 0.0011 Non-detectU 0.011 Non-detectU 0.011 Non-detectU 0.011 Non-detectU 0.011 Non-detectU

U 0.0013 Non-detectU 0.0013 Non-detectU 0.0054 Non-detectU 0.00027 Non-detectU 0.0027 Non-detectU 0.0027 Non-detectU 0.0027 Non-detectU 0.0027 Non-detectU

2.73 8.56 8.41 5.27 1.74 1.15 2.09 2.09

U 0.00096 Non-detectU 0.00096 Non-detectU 0.0038 Non-detectU 0.00019 Non-detectU 0.0019 Non-detectU 0.0019 Non-detectU 0.0019 Non-detectU 0.0019 Non-detectU

U 0.0012 Non-detectU 0.0012 Non-detectU 0.0048 Non-detectU 0.00024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU 0.0024 Non-detectU

33 35 36 37 38 39 40

03/19/13

Suspension/Dispersion

50

Measured

185

See Lab Report

JB31445

JB31445-1

32

03/18/13

Suspension/Dispersion

21

Measured

185

See Lab Report

JB29350-1 JB31145-1

31

03/12/13

Suspension/Dispersion

21

Measured

185

See Lab Report

JB31069

JB31069-1

27

03/04/13

Suspension/Dispersion

22

Measured

185

29 30

03/06/13 03/08/13

21 20

185 185

See Lab Report

Measured

See Lab Report

Suspension/Dispersion Suspension/Dispersion

JB29490

25 20

185 185

Measured

See Lab Report

JB29350

JB25262-1 JB29487-1 JB29490-1

See Lab Report See Lab Report

JB25262 JB29487

Measured Measured

JB29488-1

JB29488

28

02/28/13 03/05/13

JB25255-1

20

02/14/13

24

185

Measured

25

See Lab Report

JB25255

Suspension/Dispersion Suspension/Dispersion Suspension/Dispersion
Note(s) Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

41 42 43 44 45 46 47 48 49 50 51 52 53 54 55
Note(s) Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect? Note(s)

56 57 58 59 60