Table	1

Summary	of	Filterable	Particulate	Matter	Test	Results

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Run	Identification Run	1 Run	2 Run	3 Average

Run	Date 30Apr13 30Apr13 01May13

Start/Stop	Time 1043/1501 1610/2026 0825/1230

Process	Rate

tons	of	Aluminum	produced/hr 5.12 5.12 5.12 5.12

Exhaust	Gas	Conditions

Temperature	(deg.	F) 83 85 87 85

Moisture	(volume	%) 0.8 0.6 1.0 0.8

Oxygen	(dry	volume	%) 20.90 20.90 20.90 20.90

Carbon	Dioxide	(dry	volume	%) 0.00 0.00 0.00 0.00

Volumetric	Flow	Rate

acfm 2,685 2,736 2,660 2,694

dscfm 2,568 2,613 2,531 2,571

Total	Particulate	Matter

gr/dscf 0.0012 0.0015 0.0029 0.0018

	lb/hr 0.03 0.03 0.06 0.04

lb/	ton	of	Aluminum	produced 0.01 0.01 0.01 0.01

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
Table	2

Summary	of	Multiple	Metals	Test	Results

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Run	Identification Run	1 Run	2 Run	3 Average

Run	Date 30Apr13 30Apr13 01May13

Start/Stop	Time 1043/1501 1610/2026 0825/1230

Process	Rate

tons	of	Aluminum	produced/hr 5.12 5.12 5.12 5.12

Exhaust	Gas	Conditions

Temperature	(deg.	F) 83 85 87 85

Moisture	(volume	%) 0.8 0.6 1.0 0.8

Oxygen	(dry	volume	%) 20.90 20.90 20.90 20.90

Carbon	Dioxide	(dry	volume	%) 0.00 0.00 0.00 0.00

Volumetric	Flow	Rate

acfm 2,685 2,736 2,660 2,694

dscfm 2,568 2,613 2,531 2,571

Arsenic

mg/dscm 2.46E-03 2.25E-03 3.34E-03 2.68E-03

	lb/hr 2.37E-05 2.20E-05 3.17E-05 2.58E-05

lb/	ton	of	Aluminum	produced 4.63E-06 4.30E-06 6.18E-06 5.04E-06

Antimony

mg/dscm <1.69E-04 <1.68E-04 <1.69E-04 <1.69E-04

	lb/hr <1.63E-06 <1.65E-06 <1.60E-06 <1.63E-06

lb/	ton	of	Aluminum	produced <3.18E-07 <3.21E-07 <3.13E-07 <3.17E-07

Beryllium

mg/dscm <4.23E-05 <4.20E-05 <4.23E-05 <4.22E-05

	lb/hr <4.07E-07 <4.12E-07 <4.01E-07 <4.06E-07

lb/	ton	of	Aluminum	produced <7.94E-08 <8.04E-08 <7.83E-08 <7.93E-08

Cadium

mg/dscm 6.02E-05 7.99E-05 9.09E-05 7.70E-05

	lb/hr 5.79E-07 7.82E-07 8.62E-07 7.41E-07

lb/	ton	of	Aluminum	produced 1.13E-07 1.53E-07 1.68E-07 1.45E-07

Chromium

mg/dscm 8.57E-04 7.72E-03 6.68E-03 5.08E-03

	lb/hr 8.24E-06 7.55E-05 6.33E-05 4.90E-05

lb/	ton	of	Aluminum	produced 1.61E-06 1.47E-05 1.24E-05 9.58E-06

Cobalt

mg/dscm 2.04E-04 3.01E-04 4.04E-04 3.03E-04

	lb/hr 1.96E-06 2.94E-06 3.83E-06 2.91E-06

lb/	ton	of	Aluminum	produced 3.83E-07 5.75E-07 7.47E-07 5.68E-07

Lead

mg/dscm 1.27E-03 1.34E-03 1.43E-03 1.35E-03

	lb/hr 1.22E-05 1.31E-05 1.35E-05 1.30E-05

lb/	ton	of	Aluminum	produced 2.39E-06 2.56E-06 2.64E-06 2.53E-06

Manganese

mg/dscm 8.98E-04 3.47E-03 3.38E-03 2.58E-03

	lb/hr 8.64E-06 3.40E-05 3.21E-05 2.49E-05

lb/	ton	of	Aluminum	produced 1.69E-06 6.63E-06 6.26E-06 4.86E-06

Mercury

mg/dscm 4.12E-06 6.73E-06 4.86E-06 5.24E-06

	lb/hr 3.96E-08 6.58E-08 4.61E-08 5.05E-08

lb/	ton	of	Aluminum	produced 7.74E-09 1.29E-08 9.00E-09 9.87E-09

Nickel

mg/dscm 1.02E-02 2.21E-02 2.20E-02 1.81E-02

	lb/hr 9.83E-05 2.16E-04 2.08E-04 1.74E-04

lb/	ton	of	Aluminum	produced 1.92E-05 4.22E-05 4.07E-05 3.40E-05

Selenium

mg/dscm <4.23E-04 <4.20E-04 <4.23E-04 <4.22E-04

	lb/hr <4.07E-06 <4.12E-06 <4.01E-06 <4.06E-06

lb/	ton	of	Aluminum	produced <7.94E-07 <8.04E-07 <7.83E-07 <7.93E-07

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
-Please	note	that	"<"	indicates	result	is	below	analytical	detection	limit

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
Method	29-Data	Summary

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Run	1 Run	2 Run	3

Traverse Stack Delta Delta Tm(F) SQRT Stack Delta Delta Tm(F) SQRT Stack Delta Delta	 Tm(F) SQRT

Point Temp(F) P H in out Delta	P Temp(F) P H in out Delta	P Temp(F) P H in out Delta	P

1 80 0.57 1.46 71 66 0.7550 84 0.52 1.33 79 77 0.7211 85 0.58 1.48 72 65 0.7616

1 80 0.57 1.46 70 64 0.7550 84 0.52 1.33 79 76 0.7211 85 0.58 1.48 72 65 0.7616

1 80 0.57 1.46 73 65 0.7550 84 0.52 1.33 78 75 0.7211 85 0.58 1.48 72 65 0.7616

1 80 0.57 1.46 73 66 0.7550 84 0.52 1.33 84 76 0.7211 85 0.58 1.48 72 65 0.7616

1 80 0.57 1.46 75 67 0.7550 84 0.52 1.33 84 77 0.7211 85 0.58 1.48 74 66 0.7616

1 80 0.57 1.46 75 67 0.7550 84 0.52 1.33 84 77 0.7211 85 0.58 1.48 75 67 0.7616

2 80 0.54 1.38 75 68 0.7348 84 0.55 1.41 84 77 0.7416 85 0.52 1.33 75 67 0.7211

2 80 0.54 1.38 76 68 0.7348 84 0.55 1.41 84 77 0.7416 85 0.52 1.33 77 68 0.7211

2 80 0.54 1.38 77 69 0.7348 84 0.55 1.41 84 77 0.7416 85 0.52 1.33 78 69 0.7211

2 80 0.54 1.38 77 69 0.7348 84 0.55 1.41 85 78 0.7416 85 0.52 1.33 78 69 0.7211

2 80 0.54 1.38 77 69 0.7348 84 0.55 1.41 85 78 0.7416 85 0.52 1.33 78 69 0.7211

2 80 0.54 1.38 78 70 0.7348 84 0.55 1.41 84 78 0.7416 85 0.52 1.33 79 70 0.7211

3 80 0.50 1.28 78 70 0.7071 84 0.48 1.23 84 78 0.6928 85 0.49 1.25 79 71 0.7000

3 80 0.50 1.28 78 71 0.7071 84 0.48 1.23 84 78 0.6928 85 0.49 1.25 79 71 0.7000

3 80 0.50 1.28 79 72 0.7071 84 0.48 1.23 85 79 0.6928 85 0.49 1.25 80 72 0.7000

3 80 0.50 1.28 79 72 0.7071 84 0.48 1.23 84 79 0.6928 85 0.49 1.25 80 73 0.7000

3 80 0.50 1.28 79 72 0.7071 84 0.48 1.23 85 79 0.6928 85 0.49 1.25 80 73 0.7000

3 80 0.50 1.28 79 72 0.7071 84 0.48 1.23 84 79 0.6928 85 0.49 1.25 81 73 0.7000

4 80 0.60 1.54 79 72 0.7746 84 0.56 1.43 85 79 0.7483 85 0.52 1.33 82 73 0.7211

4 80 0.60 1.54 80 73 0.7746 84 0.56 1.43 85 79 0.7483 85 0.52 1.33 82 74 0.7211

4 80 0.60 1.54 81 73 0.7746 84 0.56 1.43 85 79 0.7483 85 0.52 1.33 82 74 0.7211

4 80 0.60 1.54 81 74 0.7746 84 0.56 1.43 85 79 0.7483 85 0.52 1.33 82 75 0.7211

4 80 0.60 1.54 81 74 0.7746 84 0.56 1.43 84 79 0.7483 85 0.52 1.33 82 75 0.7211

4 80 0.60 1.54 80 74 0.7746 84 0.56 1.43 85 79 0.7483 85 0.52 1.33 82 75 0.7211

1 85 0.54 1.38 80 74 0.7348 85 0.57 1.46 82 78 0.7550 89 0.48 1.23 79 76 0.6928

1 85 0.54 1.38 80 74 0.7348 85 0.57 1.46 83 78 0.7550 89 0.48 1.23 79 76 0.6928

1 85 0.54 1.38 80 74 0.7348 85 0.57 1.46 83 78 0.7550 89 0.48 1.23 80 76 0.6928

1 85 0.54 1.38 81 74 0.7348 85 0.57 1.46 84 78 0.7550 89 0.48 1.23 80 76 0.6928

1 85 0.54 1.38 81 74 0.7348 85 0.57 1.46 83 78 0.7550 89 0.48 1.23 82 76 0.6928

1 85 0.54 1.38 82 75 0.7348 85 0.57 1.46 84 78 0.7550 89 0.48 1.23 82 76 0.6928

2 85 0.59 1.51 82 75 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 76 0.7280

2 85 0.59 1.51 82 75 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 76 0.7280

2 85 0.59 1.51 82 75 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 76 0.7280

2 85 0.59 1.51 81 75 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 77 0.7280

2 85 0.59 1.51 82 76 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 77 0.7280

2 85 0.59 1.51 81 76 0.7681 85 0.50 1.28 84 78 0.7071 89 0.53 1.36 83 77 0.7280

3 85 0.50 1.28 81 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

3 85 0.50 1.28 81 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

3 85 0.50 1.28 82 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

3 85 0.50 1.28 82 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

3 85 0.50 1.28 82 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

3 85 0.50 1.28 82 76 0.7071 85 0.62 1.59 84 78 0.7874 89 0.59 1.51 83 77 0.7681

4 85 0.44 1.13 82 76 0.6633 85 0.63 1.61 84 78 0.7937 89 0.47 1.20 83 77 0.6856

4 85 0.44 1.13 82 77 0.6633 85 0.63 1.61 84 78 0.7937 89 0.47 1.20 83 77 0.6856

4 85 0.44 1.13 82 77 0.6633 85 0.63 1.61 85 78 0.7937 89 0.47 1.20 83 77 0.6856

4 85 0.44 1.13 83 77 0.6633 85 0.63 1.61 85 79 0.7937 89 0.47 1.20 83 77 0.6856

4 85 0.44 1.13 83 77 0.6633 85 0.63 1.61 85 79 0.7937 89 0.47 1.20 83 77 0.6856

4 85 0.44 1.13 83 77 0.6633 85 0.63 1.61 85 79 0.7937 89 0.47 1.20 83 77 0.6856

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

0.0000 0.0000 0.0000

Average 83 0.54 1.37 79 73 0.7306 85 0.55 1.42 84 78 0.7434 87 0.52 1.34 80 73 0.7223

Laboratory	Data Run	1 Run	2 Run	3

Filter	ID

Front	Half	Sample:

Filter	wt,	g 0.0107 0.0066 0.0178

Acetone	rinse	volume,	ml 120 150 150

Acetone	wt,	g 0.0026 0.0096 0.0134

F.H.	Total,	g 0.0133 0.0162 0.0312

Back	Half	Sample:

B.H.	Total,g

Acetone	Blank	Sample:

Acetone	blank	volume,	ml 160

Acetone	Blank	weight,	g 125.632 125.632 125.632

Acetone	weight	gain,g 0.0003 0.0003 0.0003

Acetone	Blank	concentration 0.00000 0.00000 0.00000

0.001%		of	Acetone	Blank	Weight 0.0009 0.0012 0.0012

Weight	of	Sample	in	Acetone	Wash,	g 0.0002 0.0003 0.0003

Corrected	Acetone	Blank	Value,	g 0.0002 0.0003 0.0003

(F.H.	Total+B.H.	Total-Blank):

Total,	g 0.0131 0.0159 0.0309

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
	Test	Data	Summary	and	Calculations

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Parameter Run	1 Run	2 Run	3

Run	Date 30Apr13 30Apr13 01May13

Start/Stop	Time 1043/1501 1610/2026 0825/1230

Duration	of	Run,	Minutes 240 240 240

Ave.	Nozzle	Diameter,	inches 0.227 0.227 0.227

Pitot	Calibration	Factor,	CF 0.84 0.84 0.84

Meter	Gamma 1.027 1.027 1.027

Meter	Delta	H,	inches	of	H2O 1.61 1.61 1.61

Stack	Diameter,	inches 14 14 14

Rectangular	Width,	inches

Rectangular	Length,	inches

Stack	Area,	sq.ft. 1.07 1.07 1.07

Barometric	Pressure,	inches	of	Hg 30.2 30.2 30.37

Static	Pressure,	inches	of	H2O -7.7 -7.7 -7.9

Dry	Gas	Meter	Sample	Volume,	(VM)ft3

Initial 892.344 55.782 221.484

Final 1055.46 221.223 383.903

Difference 163.116 165.441 162.419

Ave.	Stack	Temperature,		Ts(F) 82.5 84.5 87.0

Ave.	Meter	Temperature,	Tm(F) 76.1 80.9 76.8

Ave.	Run	Delta	H,	inches	of	H2O 1.37 1.42 1.34

Ave.	Square	Root	of	Delta	P 0.7306 0.7434 0.7223

Moisture	Data

Volume	of	water	collected,	mls 4 -4 12

Silica	Gel,	grams 24.3 24 22.9

Total	Collected,	mls 28.3 20 34.9

ORSAT	Data

%O2 20.90 20.90 20.90

%CO2 0.00 0.00 0.00

%CO

Calculations

Vw(std),	scf	= 1.332 0.941 1.643

Vm(std),	dscf	= 167.103 167.980 167.079

Bws= 0.008 0.006 0.010

Md= 28.84 28.84 28.84

Ms= 28.75 28.78 28.73

Vs,	ft/sec	= 41.9 42.7 41.5

Qs,	acfm	= 2,685 2,736 2,660

Qs(std),	dscfm	= 2,568 2,613 2,531

Isokinetic	Sampling	Rate,	% 103.1 101.9 104.6

Where:

Vw(std)	=	volume	of	water	vapor	in	gas,	standard	conditions	=	0.04707*Vlc

Vm(std)	=	vol.	of	gas	sampled,	standard	conditions	=	17.647	x	Vm	x	gamma	x	[Pb	+	(dH/13.6)]/Tm(R)

Bws	=		water	vapor	in	gas	stream,	proportion	by	volume	=	Vw(std)/(Vm(std)	+	Vw(std))

Md	=	molecular	weight	of	stack	gas,	dry	basis	=	(0.44	x%CO2)	+	(0.32	x%O2)	+	[0.28	x	(%N2	+	%CO)]

Ms	=	molecular	weight	of	stack	gas,	wet	basis	=	[Md	x	(1-Bws)]	+	(18.0	x	Bws)

Vs	=	stack	gas	velocity	=	85.49	x	Cp	x	(avg.	Sq.Rt.	dP)	x	[Sq.Rt.	(Ts(R))/(Ms	x	Ps)]

Qs	=	stack	gas	flow	rate	=	Vs	x	As	x	60

Qs(std)	=	stack	gas	flow	rate,	standard	conditions	=	Qs	x	(1-Bws)	x	(528/(Ts(R))	x	(Ps/29.92)

Isokinetic	sampling	rate	=	{(Ts(R))	x	[(0.00267	x	Vlc)	+	(Vm(std)/17.647)]	x	100}/(Time	x	vs	x	Ps	x	An	x60)

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
Particulate	Results	Summary

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Test	Results: Run	1 Run	2 Run	3 Average

Particulate	Emission	Concentration:

	grains/dscf 0.0012 0.0015 0.0029 0.0018

grains/dscf	@	7%	O2 #DIV/0! #DIV/0! #DIV/0! #DIV/0!

grains/dscf	@	15%	O2 #DIV/0! #DIV/0! #DIV/0! #DIV/0!

	lb/dscf 1.72E-07 2.09E-07 4.08E-07 2.63E-07

Particulate	Emission	Rate:

grams/minute 0.20 0.25 0.47 0.31

	lb/hr 2.66E-02 3.28E-02 6.20E-02 0.04

fuel	F-factor,	dscf/MMBtu 0 0 0

	lb/MMBtu #DIV/0! #DIV/0! #DIV/0! #DIV/0!

Where:

Particulate	Emission	Concentration:

grains/dscf		=		(15.432	grains/gm		x		gms	of	particulate	collected)/sample	vol.,	standard	cond.	(29.92"	Hg,	68°F,	dry)

grains/dscf	@	7%O2		=		grains/dscf		x		[(20.9	-	7.0)/(20.9	-	%O2)]

grains/dscf	@15%O2		=		grains/dscf		x		[(	20.9	-	15.0	)/(	20.9	-	%O2)]

lb/dscf		=		grains/dscf/7000	grains	per	pound

Particulate	Emission	Rate:

grams/minute		=		(grams	of	particulate	collected/sample	vol.,	standard	cond.)		x		stack	gas	flow	rate,	standard	cond.		

lb/hr		=		lb/dscf		x		stack	gas	flow	rate,	standard	conditions		x		60	minutes/hr

lb/MMBtu		=		(	Fuel	F-factor,	dscf/MMBtu	)	x	(grains/dscf)	x	(1	lb/7000	grains)	x	[	20.9/(20.9	-	%O2)]

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb
Multiple	Metals	Results	Summary

Total	of	Front-Half	and	Back-Half	Analyses

ALCOA	Massena	-	East	Plant

Line	1	Exhaust

Massena,	New	York

Run	1 Run	2 Run	3 Average

Parameter: (Total	ug) (mg/dscm) (g/min) (lb/hr) (Total	ug) (mg/dscm) (g/min) (lb/hr) (Total	ug) (mg/dscm) (g/min) (lb/hr) (mg/dscm) (g/min) (lb/hr)

Arsenic 11.65 2.46E-03 1.79E-04 2.37E-05 10.7 2.25E-03 1.66E-04 2.20E-05 15.8 3.34E-03 2.39E-04 3.17E-05 2.68E-03 1.95E-04 2.58E-05

Antimony <0.80 <1.69E-04 <1.23E-05 <1.63E-06 <0.80 <1.68E-04 <1.24E-05 <1.65E-06 <0.80 <1.69E-04 <1.21E-05 <1.60E-06 <1.69E-04 <1.23E-05 <1.63E-06

Beryllium <0.20 <4.23E-05 <3.07E-06 <4.07E-07 <0.20 <4.20E-05 <3.11E-06 <4.12E-07 <0.20 <4.23E-05 <3.03E-06 <4.01E-07 <4.22E-05 <3.07E-06 <4.06E-07

Cadium 0.29 6.02E-05 4.38E-06 5.79E-07 0.38 7.99E-05 5.91E-06 7.82E-07 0.43 9.09E-05 6.51E-06 8.62E-07 7.70E-05 5.60E-06 7.41E-07

Chromium 4.06 8.57E-04 6.23E-05 8.24E-06 36.7 7.72E-03 5.71E-04 7.55E-05 31.6 6.68E-03 4.79E-04 6.33E-05 5.08E-03 3.71E-04 4.90E-05

Cobalt 0.97 2.04E-04 1.48E-05 1.96E-06 1.43 3.01E-04 2.22E-05 2.94E-06 1.91 4.04E-04 2.89E-05 3.83E-06 3.03E-04 2.20E-05 2.91E-06

Lead 6.01 1.27E-03 9.24E-05 1.22E-05 6.37 1.34E-03 9.91E-05 1.31E-05 6.75 1.43E-03 1.02E-04 1.35E-05 1.35E-03 9.79E-05 1.30E-05

Manganese 4.25 8.98E-04 6.53E-05 8.64E-06 16.5 3.47E-03 2.57E-04 3.40E-05 16.0 3.38E-03 2.42E-04 3.21E-05 2.58E-03 1.88E-04 2.49E-05

Mercury 0.02 4.12E-06 3.00E-07 3.96E-08 0.032 6.73E-06 4.98E-07 6.58E-08 0.023 4.86E-06 3.48E-07 4.61E-08 5.24E-06 3.82E-07 5.05E-08

Nickel 48.35 1.02E-02 7.43E-04 9.83E-05 105 2.21E-02 1.63E-03 2.16E-04 104 2.20E-02 1.58E-03 2.08E-04 1.81E-02 1.32E-03 1.74E-04

Selenium <2.00 <4.23E-04 <3.07E-05 <4.07E-06 <2.00 <4.20E-04 <3.11E-05 <4.12E-06 <2.00 <4.23E-04 <3.03E-05 <4.01E-06 <4.22E-04 <3.07E-05 <4.06E-06

Where:

Total	ug=	Total	sample	collected,	micrograms

mg/dscm	=	grams	of	pollutant	per	dry	standard	cubic	meter	=	(ug/dscf	)	x	(35.314	cubic	feet/cubic	meter)	x	(1	mg/1.00E+03	ug)

g/min	=	grams	per	minute,	emission	rate	=	ug/dscf		x		DSCFM	x	1	gram/1.00E+06	ug

lb/hr	=	pounds	per	hour	emission	rate	=	g/min	x	60	min/hour/(453.59	g/lb)

C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\4760309437670059524\09000064819454fb