Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

130 Santee Cooper-Cross Unit 1 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

130 Santee Cooper-Cross Unit 1 As Received Higher Heating Value 130 Santee Cooper-Cross Unit 1 As Received % Moisture 130 Santee Cooper-Cross Unit 1 As Received Antim ony 130 Santee Cooper-Cross Unit 1 As Received Arsenic 130 Santee Cooper-Cross Unit 1 As Received Beryllium 130 Santee Cooper-Cross Unit 1 As Received Cadmium 130 Santee Cooper-Cross Unit 1 As Received Chlorine 130 Santee Cooper-Cross Unit 1 As Received Chromium 130 Santee Cooper-Cross Unit 1 As Received Cobalt 130 Santee Cooper-Cross Unit 1 As Received Fluorine 130 Santee Cooper-Cross Unit 1 As Received Lead 130 Santee Cooper-Cross Unit 1 As Received Manganese 130 Santee Cooper-Cross Unit 1 As Received Mercury 130 Santee Cooper-Cross Unit 1 As Received Nickel 130 Santee Cooper-Cross Unit 1 As Received SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D 240 ASTM D 2216 SW846 3050B/6020A SW846 3050B/6020A SW846 3050B/6020A SW846 3050B/6020A SW846 5050/9056A SW846 3050B/6020A SW846 3050B/6020A SW846 5050/9056A SW846 3050B/6020A SW846 3050B/6020A SW846 7471B SW846 3050B/6020A SW846 3050B/6020AEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 130 Santee Cooper-Cross Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units RUN 1 5/2/2010 5/2/2010 12600.00 Btu/lb RUN 2 5/3/2010 5/3/2010 12000.00 Btu/lb RUN 3 5/3/2010 5/3/2010 12400.00 Btu/lb Fuel Testing Results% Moisture

(as received) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units 5.8 874000 μg/Kg 15.3 μg/Kg 114 μg/Kg 10300 μg/Kg 6.36 1040000 μg/Kg 16.4 μg/Kg 98.3 μg/Kg 5280 μg/Kg 6.09 631000 μg/Kg 11.3 μg/Kg <100 μg/Kg 3800 μg/KgBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 727 μg/Kg 109 μg/Kg 6470 μg/Kg 3960 μg/Kg 16400 677 μg/Kg <96 μg/Kg 5850 μg/Kg 3620 μg/Kg 14400 716 μg/Kg 104 μg/Kg 14300 μg/Kg 3450 μg/Kg 11700Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 8940 μg/Kg <2460 μg/Kg 197000 μg/Kg 2640 μg/Kg μg/Kg 6160 μg/Kg <2400 μg/Kg 104000 μg/Kg 2200 μg/Kg μg/Kg 9290 μg/Kg <2500 μg/Kg 69400 μg/Kg 2600 μg/KgEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 130 Santee Cooper-Cross Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units RUN 1 5/4/2010 5/4/2010 12300.00 Btu/lb RUN 2 5/4/2010 5/4/2010 11000.00 Btu/lb RUN 3 5/4/2010 5/4/2010 12200.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units 6.05 978000 μg/Kg 18.6 μg/Kg <96.9 μg/Kg 6810 μg/Kg 5.56 882000 μg/Kg 16.5 μg/Kg <97.8 μg/Kg 4890 μg/Kg 5.77 1040000 μg/Kg 20.2 μg/Kg <100 μg/Kg 3490 μg/KgBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 691 μg/Kg <96.9 μg/Kg 5930 μg/Kg 3740 μg/Kg 20700 698 μg/Kg <97.8 μg/Kg 5730 μg/Kg 3290 μg/Kg 10600 865 μg/Kg <100 μg/Kg 6130 μg/Kg 4100 μg/Kg 12300Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 8820 μg/Kg <2420 μg/Kg 94900 μg/Kg 3390 μg/Kg μg/Kg 7160 μg/Kg <2450 μg/Kg 67000 μg/Kg 2630 μg/Kg μg/Kg 7020 μg/Kg <2500 μg/Kg 72900 μg/Kg 3010 μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/Kg