2714 Exchange Drive 

Wilmington, NC 28405 

Ph.: 910-794-1613 

1 / 2 

 

 

18 October 2010 

 

Bill Kissel 

ATC, Inc. 

1630 Dale Earnhardt Blvd 

Kannapolis, NC 28083

Ph.: 800-733-3193 

Email: bkissel@atc-net.net 

Subject: Certificate of Results 

Dear Bill; 

Attached to this narrative are the analytical results you requested on samples submitted 

for the determination of polychlorinated dibenzo-p-dioxins and dibenzofurans. The insert 

below summarizes the relevant information pertaining to your project. In particular, QC 

annotations bring to your attention specific analytical observations and assessments made 

during the sample handling and data interpretation phases. A brief description of the 

report’s components is provided. 

Project Information Summary When applicable, see QC Annotations for details

Client Project No. P-10124

AP Project No. P2694

Analytical Protocol Method 23

No. Samples Submitted 10

No. Samples Analyzed 10

No. Laboratory Method Blanks 1

No. OPRs / Batch CS3 1

No. Outstanding Samples 0

Date Received 27-Sep-2010

Condition Received see below

Temperature upon Receipt (C) 4

Extraction within Holding Time yes

Analysis within Holding Time yes

Data meet QA/QC Requirements yes

Exceptions see below

Analytical Difficulties see below
2714 Exchange Drive 

Wilmington, NC 28405 

Ph.: 910-794-1613 

2 / 2 

 

Analytical Perspectives remains committed to serving you in the most effective manner. 

Should you have any questions or need additional information and technical support, 

please do not hesitate to contact us. Thank you for choosing Analytical Perspectives as 

part of your analytical support team. 

Sincerely, 

Heather Steele, Ph.D. 

Project Manager 

QC Annotations: 

1. Please see the attached appendices for a list of data qualifiers and lab identifiers 

that may be contained in the report.

2. The recoveries for the extraction standards (ES) OCDD and OCDF were below 

15% for Sample 007. This will have a negligible effect on the TEQ and totals.
APPENDIX A: DATA QUALIFIERS / DATA ATTRIBUTES 

* The reported concentration exceeds the calibration range (upper point of the calibration 

curve).1

> Indicates high recoveries. Shown with the numeric value at the top of the range.1

B The analyte is found in the method blank, at a level that is <=10x the sample 

concentration.

C 

Two or more congeners co-elute. In EDDs C denotes the lowest IUPAC congener in a 

co-elution group and additional co-eluters for the group are shown with the number of the 

lowest IUPAC co-eluter. 

E The reported concentration exceeds the calibration range (upper point of the calibration 

curve). 

EMPC 

Represents an Estimated Maximum Possible Concentration. EMPC’s arise in cases where 

the signal/noise ratio is not sufficient for peak identification (the determined ionabundance ratio is outside the allowed theoretical range), or where there is a co-eluting 

interference. 

ETH Indicates the presence of a diphenyl ether that appears to interfere with the quantitation of 

a furan. The reported concentration is the maximum. 

H/h If the standard recovery is below the method or SOP specified value “H” is assigned. If 

the obtained value is less than half the specified value “h” is assigned.1

J Indicates that an analyte has a concentration below the reporting limit (lowest point of the 

calibration curve). 

ND Indicates a non-detect. 

NR Indicates a value that is not reportable. 

PR Due to interference, the associated congener is poorly resolved. 

QI Indicates the presence of a quantitative interference. 

Ra The new ratio – [Ra] -- for 2,3,7,8-TCDD following the 37Cl4-2,3,7,8-TCDD correction is 

shown between squared brackets in the DL column.1

SI 

Denotes “Single Ion Mode” and is utilized for PCBs where the secondary ion trace has a 

significantly elevated noise level due to background PFK. Responses for such peaks are 

calculated using an EMPC approach based solely on the primary ion area(s) and may be 

considered estimates.1

U The analyte was not detected. The estimated detection limit (EDL) may be reported for 

this analyte. 

V The labeled standard recovery was found to be outside of the method control limits. 

X Indicates results reported from reinjection, refractionation, or repeat analyses. 

APPENDIX B: LAB ID IDENTIFIERS

AR Indicates use of the archived portion of the sample extract. 

CU Indicates a sample that required additional clean-up prior to MS injection/processing. 

D Indicates a dilution of the sample extract. The number that follows the “D” indicates the 

dilution factor. 

DE Indicates a dilution performed with the addition of ES (extraction standard) solution. 

DUP Designation for a duplicate sample. 

MS Designation for a matrix spike. 

MSD Designation for a matrix spike duplicate. 

RJ Indicates a reinjection of the sample extract. 

S Indicates a sample split. The number that follows the “S” indicates the split factor. 

1

Denotes data qualifiers/attributes whose use will be phased out over time 
 P2694 - TEQ

Project ID: P-10124 

Sample SummaryPart 1 

Analyte 0_8209_ MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet- R1 Plant 4 Outlet- R2 Plant 4 Outlet- R3 Plant 4 Oven-R1 P

Ov

pg pg pg pg pg pg pg pg 

2,3,7,8-TCDD (5.83) (3.27) (2.18) (3.37) (4) (3.66) (3.73) (3.05) (1,2,3,7,8-PeCDD (5.77) (3.65) 3.34 (4.24) (4.05) (3.23) (4.12) (2.86) (1,2,3,4,7,8-HxCDD (5.56) (2.67) (2.2) (3.44) (3.74) (3.41) (3.92) (2.45) (1,2,3,6,7,8-HxCDD (5.59) (2.57) (2.32) (3.14) (3.64) (3.36) (3.55) [3.43] (1,2,3,7,8,9-HxCDD (6.35) (2.76) (2.5) (3.9) (4.32) (3.79) (4.12) [4.47] (1,2,3,4,6,7,8-HpCDD (7.09) [29.3] 13.6 [9.52] (5.42) (4.97) (3.8) 41.2 [OCDD (9.71) 148 63.2 42.4 [19.7] 17.3 (7.51) 284 2,3,7,8-TCDF (3.59) 9 [7.53] 4.56 (2.83) (2.11) (2.36) (2.3) (1,2,3,7,8-PeCDF (3.39) 11.3 20.2 7.73 (2.19) (2.25) (2.37) (1.42) 2,3,4,7,8-PeCDF (3.23) 9.67 10.5 [6.36] (2.23) (2.15) (2.05) (1.31) (1,2,3,4,7,8-HxCDF (3.6) 9.72 13.8 9.07 (2.26) (2.24) (2.39) (1.54) (1,2,3,6,7,8-HxCDF (3.18) 10.4 [10.7] [7.78] (2.18) (1.98) (2.15) (1.41) (2,3,4,6,7,8-HxCDF (3.38) [11.9] 9.45 [6.39] (2.32) (2.2) (2.29) (1.43) (1,2,3,7,8,9-HxCDF (4.65) (2.68) (1.97) (2.92) (3.03) (3.2) (2.94) (1.99) (1,2,3,4,6,7,8-HpCDF (3.28) 29.4 23.1 21.5 [1.52] [1.71] 5.97 5.03 (1,2,3,4,7,8,9-HpCDF (4.34) (3.14) [2.36] (2.96) (4.23) (3.06) (3.18) (3.15) (OCDF (8.04) 14.1 11.2 19 (5.81) (3.95) [7.79] (22) (ITEF TEQ (ND=0; EMPC=0) 0.00 8.77 10.7 2.03 0.00 0.0173 0.0597 0.746 0ITEF TEQ (ND=0; EMPC=EMPC) 0.00 10.3 12.6 6.72 0.0349 0.0344 0.0675 1.54 0ITEF TEQ (ND=DL/2; EMPC=0) 7.13 12.0 12.4 6.18 4.91 4.41 4.75 4.18 ITEF TEQ (ND=DL/2; EMPC=EMPC) 7.13 13.3 14.1 10.2 4.93 4.42 4.76 4.72 ITEF TEQ (ND=DL; EMPC=EMPC) 14.3 16.4 15.6 13.6 9.82 8.81 9.45 7.90 Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 31Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P269

( ) = DL[ ] = EMPC
 P2694 - WHO-2005-TEQ

Project ID: P-10124 

Sample SummaryPart 1 

Analyte 0_8209_ MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet- R1 Plant 4 Outlet- R2 Plant 4 Outlet- R3 Plant 4 Oven-R1 P

Ov

pg pg pg pg pg pg pg pg 

2,3,7,8-TCDD (5.83) (3.27) (2.18) (3.37) (4) (3.66) (3.73) (3.05) (1,2,3,7,8-PeCDD (5.77) (3.65) 3.34 (4.24) (4.05) (3.23) (4.12) (2.86) (1,2,3,4,7,8-HxCDD (5.56) (2.67) (2.2) (3.44) (3.74) (3.41) (3.92) (2.45) (1,2,3,6,7,8-HxCDD (5.59) (2.57) (2.32) (3.14) (3.64) (3.36) (3.55) [3.43] (1,2,3,7,8,9-HxCDD (6.35) (2.76) (2.5) (3.9) (4.32) (3.79) (4.12) [4.47] (1,2,3,4,6,7,8-HpCDD (7.09) [29.3] 13.6 [9.52] (5.42) (4.97) (3.8) 41.2 [OCDD (9.71) 148 63.2 42.4 [19.7] 17.3 (7.51) 284 2,3,7,8-TCDF (3.59) 9 [7.53] 4.56 (2.83) (2.11) (2.36) (2.3) (1,2,3,7,8-PeCDF (3.39) 11.3 20.2 7.73 (2.19) (2.25) (2.37) (1.42) 2,3,4,7,8-PeCDF (3.23) 9.67 10.5 [6.36] (2.23) (2.15) (2.05) (1.31) (1,2,3,4,7,8-HxCDF (3.6) 9.72 13.8 9.07 (2.26) (2.24) (2.39) (1.54) (1,2,3,6,7,8-HxCDF (3.18) 10.4 [10.7] [7.78] (2.18) (1.98) (2.15) (1.41) (2,3,4,6,7,8-HxCDF (3.38) [11.9] 9.45 [6.39] (2.32) (2.2) (2.29) (1.43) (1,2,3,7,8,9-HxCDF (4.65) (2.68) (1.97) (2.92) (3.03) (3.2) (2.94) (1.99) (1,2,3,4,6,7,8-HpCDF (3.28) 29.4 23.1 21.5 [1.52] [1.71] 5.97 5.03 (1,2,3,4,7,8,9-HpCDF (4.34) (3.14) [2.36] (2.96) (4.23) (3.06) (3.18) (3.15) (OCDF (8.04) 14.1 11.2 19 (5.81) (3.95) [7.79] (22) (WHO-2005 TEQ (ND=0; EMPC=0) 0.00 6.5 9.83 1.83 0.00 0.00518 0.0597 0.548 0WHO-2005 TEQ (ND=0; EMPC=EMPC) 0.00 7.98 11.7 5.25 0.0211 0.0223 0.062 1.34 0WHO-2005 TEQ (ND=DL/2; EMPC=0) 8.2 10.6 11.5 6.84 5.67 4.97 5.55 4.55 WHO-2005 TEQ (ND=DL/2; EMPC=EMPC) 8.2 12.0 13.2 9.74 5.68 4.98 5.55 5.08 WHO-2005 TEQ (ND=DL; EMPC=EMPC) 16.4 16.0 14.7 14.2 11.3 9.93 11.0 8.83 Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 31Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P269

( ) = DL[ ] = EMPC
 P2694 - Totals

Project ID: P-10124 

Sample SummaryPart 2 

Analyte 0_8209_ MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet- R1 Plant 4 Outlet- R2 Plant 4 Outlet- R3 Plant 4 Oven-R1 P

Ov

pg pg pg pg pg pg pg pg 

TotalsTCDDs 0 35.5 15.2 11.1 0 5.97 6.79 7.69 PeCDDs 0 18.1 58.2 23.8 0 0 0 33 HxCDDs 0 26.2 31.3 11.7 0 0 0 44.3 HpCDDs 0 0 30.1 11.3 7.75 0 0 97.9 OCDD 0 148 63.2 42.4 19.7 17.3 0 284 TCDFs 0 84.7 76.7 21.9 0 0 0 22.5 PeCDFs 0 78.7 105 25.7 0000HxCDFs 0 57.4 63.9 24.4 0000HpCDFs 0 37.4 23.1 26.4 0 0 5.97 5.03 OCDF 0 14.1 11.2 19 0 0 7.79 0Total PCDD/Fs (ND=0; EMPC=0) 0.00 500 478 218 7.75 23.2 12.8 494 Total PCDD/Fs (ND=0; EMPC=EMPC) 0.00 710 575 325 29.0 25.0 20.5 576 Total PCDD/Fs (2378-X ND=DL; EMPC=EMPC) 86.6 731 586 349 81.2 70.5 71.0 621 Total 2378s (ND=0; EMPC=0) 0.00 242 168 104 0.00 17.3 5.97 330 Total 2378s (ND=0.5; EMPC=0) 43.3 256 177 121 31.6 41.1 34.2 355 Total 2378s (ND=1; EMPC=0) 86.6 269 185 138 63.1 64.9 62.4 380 Total 2378s (ND=0; EMPC=1) 0.00 283 189 134 21.2 19.0 13.8 338 Total 2378s (ND=0.5; EMPC=1) 43.3 294 195 146 47.3 41.8 39.0 360 Total 2378s (ND=1; EMPC=1) 86.6 304 200 158 73.5 64.5 64.2 383 Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 31Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P269

( ) = DL[ ] = EMPC
 P2694 - Others

Project ID: P-10124 

Sample SummaryPart 3 

Analyte 0_8209_ MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet- R1 Plant 4 Outlet- R2 Plant 4 Outlet- R3 Plant 4 Oven-R1 P

Ov

pg pg pg pg pg pg pg pg 

Other PCDD/Fs (ND=0, EMPC=0)Other TCDD 0 35.5 15.2 11.1 0 5.97 6.79 7.69 Other PeCDD 0 18.1 54.9 23.8 0 0 0 33 Other HxCDD 0 26.2 31.3 11.7 0 0 0 44.3 Other HpCDD 0 0 16.5 11.3 7.75 0 0 56.7 Other TCDF 0 75.7 76.7 17.4 0 0 0 22.5 Other PeCDF 0 57.8 74 18 0000Other HxCDF 0 37.2 37.5 15.3 0000Other HpCDF 0 7.98 0 4.94 0000Other PCDD/Fs (ND=0, EMPC=EMPC)Other TCDD 0 35.5 27.3 15.1 0 5.97 6.79 41.1 Other PeCDD 0 36.4 60.6 23.8 0 0 0 45.3 Other HxCDD 0 36.9 41.6 25.3 0 0 0 64.8 Other HpCDD 0 37.4 16.5 11.3 7.75 0 0 56.7 Other TCDF 0 142 94.2 47.1 0 0 0 26.4 Other PeCDF 0 84.5 80.5 33.3 0000Other HxCDF 0 39.5 52.2 24.7 0 0 0 4.09 Other HpCDF 0 14.6 10.2 9.78 0000Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 31Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P269

( ) = DL[ ] = EMPC
 P2694 - DLs

Project ID: P-10124 

Sample SummaryPart 5 (DLs) 

Analyte 0_8209_ MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet- R1 Plant 4 Outlet- R2 Plant 4 Outlet- R3 Plant 4 Oven-R1 P

Ov

pg pg pg pg pg pg pg pg 

2,3,7,8-TCDD 5.83 3.27 2.18 3.37 4 3.66 3.73 3.05 1,2,3,7,8-PeCDD 5.77 3.65 2.54 4.24 4.05 3.23 4.12 2.86 1,2,3,4,7,8-HxCDD 5.56 2.67 2.2 3.44 3.74 3.41 3.92 2.45 1,2,3,6,7,8-HxCDD 5.59 2.57 2.32 3.14 3.64 3.36 3.55 2.55 1,2,3,7,8,9-HxCDD 6.35 2.76 2.5 3.9 4.32 3.79 4.12 2.53 1,2,3,4,6,7,8-HpCDD 7.09 4.61 2.57 3.5 5.42 4.97 3.8 3.24 OCDD 9.71 6.83 4.5 5.49 8.29 5.59 7.51 62 2,3,7,8-TCDF 3.59 1.95 1.71 2.52 2.83 2.11 2.36 2.3 1,2,3,7,8-PeCDF 3.39 2.01 1.82 2.23 2.19 2.25 2.37 1.42 2,3,4,7,8-PeCDF 3.23 1.75 1.75 2.02 2.23 2.15 2.05 1.31 1,2,3,4,7,8-HxCDF 3.6 2.14 1.6 2.14 2.26 2.24 2.39 1.54 1,2,3,6,7,8-HxCDF 3.18 1.95 1.49 1.93 2.18 1.98 2.15 1.41 2,3,4,6,7,8-HxCDF 3.38 2.06 1.61 2.04 2.32 2.2 2.29 1.43 1,2,3,7,8,9-HxCDF 4.65 2.68 1.97 2.92 3.03 3.2 2.94 1.99 1,2,3,4,6,7,8-HpCDF 3.28 2.46 1.5 2.08 2.62 2.09 2.35 3.37 1,2,3,4,7,8,9-HpCDF 4.34 3.14 2.07 2.96 4.23 3.06 3.18 3.15 OCDF 8.04 5.1 2.69 4.8 5.81 3.95 5.92 22 Total TCDD 5.83 3.27 2.18 3.37 4 3.66 3.73 3.05 Total PeCDD 5.77 3.65 2.54 4.24 4.05 3.23 4.12 2.86 Total HxCDD 5.82 2.66 2.34 3.48 3.89 3.51 3.85 2.5 Total HpCDD 7.09 4.61 2.57 3.5 5.42 4.97 3.8 3.24 Total TCDF 3.59 1.95 1.71 2.52 2.83 2.11 2.36 2.3 Total PeCDF 3.31 1.87 1.78 2.12 2.21 2.2 2.21 1.36 Total HxCDF 3.66 2.19 1.65 2.23 2.42 2.37 2.42 1.58 Total HpCDF 3.75 2.76 1.76 2.48 3.32 2.5 2.72 3.26 Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 31Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P269
14.3

16.4

15.6

13.6

9.82

8.81 9.45

7.90

9.14

02468

1012141618

pg

0_8209_MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet-R1 Plant 4 Outlet-R2 Plant 4 Outlet-R3 Plant 4 Oven-R1 Plant 4 Oven-R2 Plant 4 Oven-R13 

ITEF-TEQ

Project ID: P-10124

P2694

NNNNN
16.4

16.0

14.7

14.2

11.3

9.93

11.0

8.83

11.0

02468

1012141618

pg

0_8209_MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet-R1 Plant 4 Outlet-R2 Plant 4 Outlet-R3 Plant 4 Oven-R1 Plant 4 Oven-R2 Plant 4 Oven-R13 

WHO-2005-TEQ

Project ID: P-10124

P2694

NNNNN
86.6

731

586

349

81.2 70.5 71.0

621

447

0

100200300400500600700800

pg

0_8209_MB001 Plant 4 Inlet-R1 Plant 4 Inlet-R2 Plant 4 Inlet-R3 Plant 4 Outlet-R1 Plant 4 Outlet-R2 Plant 4 Outlet-R3 Plant 4 Oven-R1 Plant 4 Oven-R2 Plant 4 Oven-R13 

Totals

Project ID: P-10124

P2694

Total PCDD/Fs (ND=0; ETotal PCDD/Fs (ND=0; ETotal PCDD/Fs (2378-X N
Method Specification Limits: Tetra-Hexa ES: 40-130%, Hepta-Octa ES: 25-130% (F = fail)

76-90

76-89

74-92

78-94

74-93

70-86

5-85 F

72-88

72-85

73-88

71-89

72-90

73-91

72-87

53

0

102030405060708090

% Rec.

13C-TCDD

13C-PeCDD

13C-HxCDD

13C-HxCDD

13C-HxCDD

13C-HpCDD

13C-OCDD

13C-TCDF

13C-PeCDF

13C-PeCDF

13C-HxCDF

13C-HxCDF

13C-HxCDF

13C-HxCDF

13C-HpCDF

Mean Recoveries of Extraction Standards (N=11)

Project ID: P-10124

P2694 M
Method Specification Limits: Tetra-Octa SS: 70-130% (F = fail)

91-102

94-103

96-105

95-101

95

0

20406080

100120

% Rec.

37Cl-TCDD

13C-PeCDD

13C-PeCDF

13C-HxCDF

13C-HpCDF

Mean Recoveries of Sampling Standards (N=11)

Project ID: P-10124

P2694 M






Sample ID: 0_8209_MB001 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID MB1_8209_DF_SDS Date ExtDate Collected: n/a QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 5.83 ES 2378-TCDD 8512378-PeCDD ND 5.77 ES 12378-PeCDD 82123478-HxCDD ND 5.56 ES 123478-HxCDD 91123678-HxCDD ND 5.59 ES 123678-HxCDD 94123789-HxCDD ND 6.35 ES 123789-HxCDD 931234678-HpCDD ND 7.09 ES 1234678-HpCDD 86OCDD ND 9.71 ES OCDD 842378-TCDF ND 3.59 ES 2378-TCDF 8612378-PeCDF ND 3.39 ES 12378-PeCDF 8423478-PeCDF ND 3.23 ES 23478-PeCDF 82123478-HxCDF ND 3.6 ES 123478-HxCDF 89123678-HxCDF ND 3.18 ES 123678-HxCDF 89234678-HxCDF ND 3.38 ES 234678-HxCDF 90123789-HxCDF ND 4.65 ES 123789-HxCDF 871234678-HpCDF ND 3.28 ES 1234678-HpCDF 861234789-HpCDF ND 4.34 ES 1234789-HpCDF 86OCDF ND 8.04 ES OCDF 81

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 91

Total TCDD ND 5.83 ND SS 12347-PeCDD 98Total PeCDD ND 5.77 ND SS 12346-PeCDF 95Total HxCDD ND 5.82 ND SS 123469-HxCDF 96Total HpCDD ND 7.09 ND SS 1234689-HpCDF 96

AS 1368-TCDD 83

Total TCDF ND 3.59 ND AS 1368-TCDF 84Total PeCDF ND 3.31 NDTotal HxCDF ND 3.66 NDTotal HpCDF ND 3.75 ND

Total PCDD/Fs ND NDITEF TEQsTEQ: ND=0 0 0 

TEQ: ND=DL/2 7.13 7.13 TEQ: ND=DL 14.3 14.3 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 823-702 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Inlet-R1 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_001 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.27 ES 2378-TCDD 7712378-PeCDD ND 3.65 ES 12378-PeCDD 75123478-HxCDD ND 2.67 ES 123478-HxCDD 82123678-HxCDD ND 2.57 ES 123678-HxCDD 83123789-HxCDD ND 2.76 ES 123789-HxCDD 821234678-HpCDD EMPC 29.3 J ES 1234678-HpCDD 78OCDD 148 ES OCDD 722378-TCDF 9 J ES 2378-TCDF 7712378-PeCDF 11.3 J ES 12378-PeCDF 7323478-PeCDF 9.67 J ES 23478-PeCDF 74123478-HxCDF 9.72 J ES 123478-HxCDF 76123678-HxCDF 10.4 J ES 123678-HxCDF 78234678-HxCDF EMPC 11.9 J ES 234678-HxCDF 8123789-HxCDF ND 2.68 ES 123789-HxCDF 771234678-HpCDF 29.4 J ES 1234678-HpCDF 761234789-HpCDF ND 3.14 ES 1234789-HpCDF 73OCDF 14.1 J ES OCDF 73

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 95

Total TCDD 35.5 35.5 SS 12347-PeCDD 10Total PeCDD 18.1 36.4 SS 12346-PeCDF 98Total HxCDD 26.2 36.9 SS 123469-HxCDF 96Total HpCDD ND 66.6 SS 1234689-HpCDF 99

AS 1368-TCDD 83

Total TCDF 84.7 151 AS 1368-TCDF 80Total PeCDF 78.7 105Total HxCDF 57.4 71.5Total HpCDF 37.4 44

Total PCDD/Fs 500 710ITEF TEQsTEQ: ND=0 8.77 10.3 

TEQ: ND=DL/2 12 13.3 TEQ: ND=DL 15.2 16.4 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 901-690 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Inlet-R2 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_002 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 2.18 ES 2378-TCDD 8512378-PeCDD 3.34 J ES 12378-PeCDD 84123478-HxCDD ND 2.2 ES 123478-HxCDD 87123678-HxCDD ND 2.32 ES 123678-HxCDD 8123789-HxCDD ND 2.5 ES 123789-HxCDD 891234678-HpCDD 13.6 J ES 1234678-HpCDD 85OCDD 63.2 J ES OCDD 812378-TCDF EMPC 7.53 J ES 2378-TCDF 812378-PeCDF 20.2 J ES 12378-PeCDF 8223478-PeCDF 10.5 J ES 23478-PeCDF 84123478-HxCDF 13.8 J ES 123478-HxCDF 84123678-HxCDF EMPC 10.7 J ES 123678-HxCDF 86234678-HxCDF 9.45 J ES 234678-HxCDF 85123789-HxCDF ND 1.97 ES 123789-HxCDF 831234678-HpCDF 23.1 J ES 1234678-HpCDF 801234789-HpCDF EMPC 2.36 J ES 1234789-HpCDF 8OCDF 11.2 J ES OCDF 80

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 9

Total TCDD 15.2 27.3 SS 12347-PeCDD 98Total PeCDD 58.2 63.9 SS 12346-PeCDF 9Total HxCDD 31.3 41.6 SS 123469-HxCDF 95Total HpCDD 30.1 30.1 SS 1234689-HpCDF 10

AS 1368-TCDD 8

Total TCDF 76.7 102 AS 1368-TCDF 81Total PeCDF 105 111Total HxCDF 63.9 89.2Total HpCDF 23.1 35.6

Total PCDD/Fs 478 575ITEF TEQsTEQ: ND=0 10.7 12.6 

TEQ: ND=DL/2 12.4 14.1 TEQ: ND=DL 14.1 15.6 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 058-218 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Inlet-R3 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_003 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.37 ES 2378-TCDD 7612378-PeCDD ND 4.24 ES 12378-PeCDD 76123478-HxCDD ND 3.44 ES 123478-HxCDD 80123678-HxCDD ND 3.14 ES 123678-HxCDD 79123789-HxCDD ND 3.9 ES 123789-HxCDD 71234678-HpCDD EMPC 9.52 J ES 1234678-HpCDD 83OCDD 42.4 J ES OCDD 782378-TCDF 4.56 J ES 2378-TCDF 7212378-PeCDF 7.73 J ES 12378-PeCDF 7123478-PeCDF EMPC 6.36 J ES 23478-PeCDF 73123478-HxCDF 9.07 J ES 123478-HxCDF 79123678-HxCDF EMPC 7.78 J ES 123678-HxCDF 80234678-HxCDF EMPC 6.39 J ES 234678-HxCDF 79123789-HxCDF ND 2.92 ES 123789-HxCDF 781234678-HpCDF 21.5 J ES 1234678-HpCDF 71234789-HpCDF ND 2.96 ES 1234789-HpCDF 8OCDF 19 J ES OCDF 74

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 10

Total TCDD 11.1 15.1 SS 12347-PeCDD 10Total PeCDD 23.8 23.8 SS 12346-PeCDF 10Total HxCDD 11.7 25.3 SS 123469-HxCDF 99Total HpCDD 11.3 20.8 SS 1234689-HpCDF 10

AS 1368-TCDD 73

Total TCDF 21.9 51.7 AS 1368-TCDF 70Total PeCDF 25.7 47.4Total HxCDF 24.4 47.9Total HpCDF 26.4 31.2

Total PCDD/Fs 218 325ITEF TEQsTEQ: ND=0 2.03 6.72 

TEQ: ND=DL/2 6.18 10.2 TEQ: ND=DL 10.3 13.6 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 555-716 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Outlet-R1 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_004 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 4 ES 2378-TCDD 8012378-PeCDD ND 4.05 ES 12378-PeCDD 84123478-HxCDD ND 3.74 ES 123478-HxCDD 85123678-HxCDD ND 3.64 ES 123678-HxCDD 85123789-HxCDD ND 4.32 ES 123789-HxCDD 841234678-HpCDD ND 5.42 ES 1234678-HpCDD 79OCDD EMPC 19.7 J ES OCDD 812378-TCDF ND 2.83 ES 2378-TCDF 8012378-PeCDF ND 2.19 ES 12378-PeCDF 7723478-PeCDF ND 2.23 ES 23478-PeCDF 78123478-HxCDF ND 2.26 ES 123478-HxCDF 82123678-HxCDF ND 2.18 ES 123678-HxCDF 82234678-HxCDF ND 2.32 ES 234678-HxCDF 82123789-HxCDF ND 3.03 ES 123789-HxCDF 801234678-HpCDF EMPC 1.52 J ES 1234678-HpCDF 81234789-HpCDF ND 4.23 ES 1234789-HpCDF 77OCDF ND 5.81 ES OCDF 77

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 99

Total TCDD ND 4 ND SS 12347-PeCDD 10Total PeCDD ND 4.05 ND SS 12346-PeCDF 10Total HxCDD ND 3.89 ND SS 123469-HxCDF 9Total HpCDD 7.75 7.75 SS 1234689-HpCDF 96

AS 1368-TCDD 81

Total TCDF ND 2.83 ND AS 1368-TCDF 78Total PeCDF ND 2.21 NDTotal HxCDF ND 2.42 NDTotal HpCDF ND 1.52

Total PCDD/Fs 7.75 29ITEF TEQsTEQ: ND=0 0 0.0349 

TEQ: ND=DL/2 4.91 4.93 TEQ: ND=DL 9.82 9.82 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 246-880 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Outlet-R2 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_005 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.66 ES 2378-TCDD 8312378-PeCDD ND 3.23 ES 12378-PeCDD 84123478-HxCDD ND 3.41 ES 123478-HxCDD 82123678-HxCDD ND 3.36 ES 123678-HxCDD 81123789-HxCDD ND 3.79 ES 123789-HxCDD 811234678-HpCDD ND 4.97 ES 1234678-HpCDD 79OCDD 17.3 J ES OCDD 762378-TCDF ND 2.11 ES 2378-TCDF 812378-PeCDF ND 2.25 ES 12378-PeCDF 7923478-PeCDF ND 2.15 ES 23478-PeCDF 79123478-HxCDF ND 2.24 ES 123478-HxCDF 78123678-HxCDF ND 1.98 ES 123678-HxCDF 79234678-HxCDF ND 2.2 ES 234678-HxCDF 78123789-HxCDF ND 3.2 ES 123789-HxCDF 761234678-HpCDF EMPC 1.71 J ES 1234678-HpCDF 781234789-HpCDF ND 3.06 ES 1234789-HpCDF 72OCDF ND 3.95 ES OCDF 74

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 99

Total TCDD 5.97 5.97 SS 12347-PeCDD 10Total PeCDD ND 3.23 ND SS 12346-PeCDF 10Total HxCDD ND 3.51 ND SS 123469-HxCDF 96Total HpCDD ND 4.97 ND SS 1234689-HpCDF 94

AS 1368-TCDD 82

Total TCDF ND 2.11 ND AS 1368-TCDF 79Total PeCDF ND 2.2 NDTotal HxCDF ND 2.37 NDTotal HpCDF ND 1.71

Total PCDD/Fs 23.2 25ITEF TEQsTEQ: ND=0 0.0173 0.0344 

TEQ: ND=DL/2 4.41 4.42 TEQ: ND=DL 8.81 8.81 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 601-566 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Outlet-R3 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_006 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.73 ES 2378-TCDD 8912378-PeCDD ND 4.12 ES 12378-PeCDD 8123478-HxCDD ND 3.92 ES 123478-HxCDD 81123678-HxCDD ND 3.55 ES 123678-HxCDD 82123789-HxCDD ND 4.12 ES 123789-HxCDD 841234678-HpCDD ND 3.8 ES 1234678-HpCDD 80OCDD ND 7.51 ES OCDD 762378-TCDF ND 2.36 ES 2378-TCDF 8712378-PeCDF ND 2.37 ES 12378-PeCDF 8523478-PeCDF ND 2.05 ES 23478-PeCDF 88123478-HxCDF ND 2.39 ES 123478-HxCDF 79123678-HxCDF ND 2.15 ES 123678-HxCDF 80234678-HxCDF ND 2.29 ES 234678-HxCDF 79123789-HxCDF ND 2.94 ES 123789-HxCDF 781234678-HpCDF 5.97 J ES 1234678-HpCDF 771234789-HpCDF ND 3.18 ES 1234789-HpCDF 76OCDF EMPC 7.79 J ES OCDF 72

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 9

Total TCDD 6.79 6.79 SS 12347-PeCDD 10Total PeCDD ND 4.12 ND SS 12346-PeCDF 10Total HxCDD ND 3.85 ND SS 123469-HxCDF 94Total HpCDD ND 3.8 ND SS 1234689-HpCDF 99

AS 1368-TCDD 86

Total TCDF ND 2.36 ND AS 1368-TCDF 84Total PeCDF ND 2.21 NDTotal HxCDF ND 2.42 NDTotal HpCDF 5.97 5.97

Total PCDD/Fs 12.8 20.5ITEF TEQsTEQ: ND=0 0.0597 0.0675 

TEQ: ND=DL/2 4.75 4.76 TEQ: ND=DL 9.45 9.45 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 072-909 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Oven-R1 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_007 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.05 ES 2378-TCDD 8212378-PeCDD ND 2.86 ES 12378-PeCDD 80123478-HxCDD ND 2.45 ES 123478-HxCDD 73123678-HxCDD EMPC 3.43 J ES 123678-HxCDD 77123789-HxCDD EMPC 4.47 J ES 123789-HxCDD 741234678-HpCDD 41.2 J ES 1234678-HpCDD 69OCDD 284 ES OCDD 4.62378-TCDF ND 2.3 ES 2378-TCDF 8512378-PeCDF ND 1.42 ES 12378-PeCDF 7823478-PeCDF ND 1.31 ES 23478-PeCDF 78123478-HxCDF ND 1.54 ES 123478-HxCDF 70123678-HxCDF ND 1.41 ES 123678-HxCDF 72234678-HxCDF ND 1.43 ES 234678-HxCDF 73123789-HxCDF ND 1.99 ES 123789-HxCDF 721234678-HpCDF 5.03 J ES 1234678-HpCDF 521234789-HpCDF ND 3.15 ES 1234789-HpCDF 6OCDF ND 22 ES OCDF 11

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 96

Total TCDD 7.69 41.1 SS 12347-PeCDD 94Total PeCDD 33 45.3 SS 12346-PeCDF 97Total HxCDD 44.3 72.7 SS 123469-HxCDF 9Total HpCDD 97.9 97.9 SS 1234689-HpCDF 12

AS 1368-TCDD 79

Total TCDF 22.5 26.4 AS 1368-TCDF 78Total PeCDF ND 1.36 NDTotal HxCDF ND 4.09Total HpCDF 5.03 5.03

Total PCDD/Fs 494 576ITEF TEQsTEQ: ND=0 0.746 1.54 

TEQ: ND=DL/2 4.18 4.72 TEQ: ND=DL 7.62 7.9 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 607-417 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Oven-R2 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_008 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 3.86 ES 2378-TCDD 8412378-PeCDD ND 4.57 ES 12378-PeCDD 87123478-HxCDD ND 2.92 ES 123478-HxCDD 85123678-HxCDD ND 3.12 ES 123678-HxCDD 83123789-HxCDD ND 3.14 ES 123789-HxCDD 851234678-HpCDD EMPC 13.9 J ES 1234678-HpCDD 83OCDD 77.2 J ES OCDD 772378-TCDF ND 2.29 ES 2378-TCDF 8312378-PeCDF ND 1.9 ES 12378-PeCDF 8123478-PeCDF ND 1.69 ES 23478-PeCDF 84123478-HxCDF ND 1.51 ES 123478-HxCDF 80123678-HxCDF ND 1.34 ES 123678-HxCDF 83234678-HxCDF ND 1.56 ES 234678-HxCDF 83123789-HxCDF ND 1.92 ES 123789-HxCDF 801234678-HpCDF ND 2.36 ES 1234678-HpCDF 811234789-HpCDF ND 3.12 ES 1234789-HpCDF 80OCDF ND 3.56 ES OCDF 74

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 95

Total TCDD 40.7 54.1 SS 12347-PeCDD 9Total PeCDD 68.9 82.4 SS 12346-PeCDF 99Total HxCDD 95.2 95.2 SS 123469-HxCDF 96Total HpCDD ND 57.3 SS 1234689-HpCDF 98

AS 1368-TCDD 84

Total TCDF 28.8 42.1 AS 1368-TCDF 81Total PeCDF ND 1.79 NDTotal HxCDF ND 1.57 NDTotal HpCDF ND 2.7 ND

Total PCDD/Fs 311 408ITEF TEQsTEQ: ND=0 0.0772 0.216 

TEQ: ND=DL/2 4.56 4.68 TEQ: ND=DL 9.03 9.14 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 315-975 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Plant 4 Oven-R13 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_009 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 4.82 ES 2378-TCDD 8212378-PeCDD ND 5.13 ES 12378-PeCDD 84123478-HxCDD ND 3.87 ES 123478-HxCDD 86123678-HxCDD ND 3.61 ES 123678-HxCDD 88123789-HxCDD ND 3.98 ES 123789-HxCDD 891234678-HpCDD 6.53 J ES 1234678-HpCDD 85OCDD EMPC 28.4 J ES OCDD 812378-TCDF ND 3.09 ES 2378-TCDF 8312378-PeCDF ND 2.6 ES 12378-PeCDF 8123478-PeCDF ND 2.32 ES 23478-PeCDF 83123478-HxCDF ND 2.37 ES 123478-HxCDF 84123678-HxCDF ND 2.39 ES 123678-HxCDF 86234678-HxCDF ND 2.46 ES 234678-HxCDF 85123789-HxCDF ND 3.23 ES 123789-HxCDF 81234678-HpCDF ND 2.38 ES 1234678-HpCDF 831234789-HpCDF ND 3.43 ES 1234789-HpCDF 82OCDF ND 5.9 ES OCDF 78

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 96

Total TCDD ND 7.1 SS 12347-PeCDD 10Total PeCDD ND 5.13 ND SS 12346-PeCDF 10Total HxCDD ND 7.97 SS 123469-HxCDF 99Total HpCDD 15.5 15.5 SS 1234689-HpCDF 99

AS 1368-TCDD 82

Total TCDF ND 4.59 AS 1368-TCDF 80Total PeCDF ND 2.45 NDTotal HxCDF ND 2.59 NDTotal HpCDF ND 2.84 ND

Total PCDD/Fs 15.5 63.6ITEF TEQsTEQ: ND=0 0.0653 0.0937 

TEQ: ND=DL/2 5.69 5.71 TEQ: ND=DL 11.3 11.3 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 781-663 AP D/F 2010 Rev. L Report Created: 14-
Sample ID: Blank 

Client Data Sample Data Laboratory Data Software 

Name: Analytical Testing Consultants, Inc. Matrix: Air Lab Project ID: P2694 Date Rec

Project ID: P-10124 Weight/Volume: 1 Lab Sample ID P2694_8209_010 Date ExtDate Collected: 16 Sep 2010 QC Batch No: 8209 Date Ana

Split: 2 Dilution: - Time Ana

Analyte Conc. (pg) DL (pg) EMPC (pg) Qualifiers Standard ES Rec

2378-TCDD ND 2.85 ES 2378-TCDD 8112378-PeCDD ND 2.53 ES 12378-PeCDD 86123478-HxCDD ND 2.56 ES 123478-HxCDD 84123678-HxCDD ND 2.42 ES 123678-HxCDD 88123789-HxCDD ND 2.81 ES 123789-HxCDD 851234678-HpCDD ND 2.64 ES 1234678-HpCDD 85OCDD ND 4.01 ES OCDD 802378-TCDF ND 1.54 ES 2378-TCDF 8112378-PeCDF ND 1.58 ES 12378-PeCDF 7823478-PeCDF ND 1.44 ES 23478-PeCDF 82123478-HxCDF ND 1.46 ES 123478-HxCDF 83123678-HxCDF ND 1.33 ES 123678-HxCDF 84234678-HxCDF ND 1.35 ES 234678-HxCDF 85123789-HxCDF ND 1.84 ES 123789-HxCDF 81234678-HpCDF ND 1.59 ES 1234678-HpCDF 821234789-HpCDF ND 2.21 ES 1234789-HpCDF 79OCDF ND 3.18 ES OCDF 79

Totals Standard SS/AS R

SS 37Cl-2378-TCDD 10

Total TCDD ND 2.85 ND SS 12347-PeCDD 10Total PeCDD ND 2.53 ND SS 12346-PeCDF 10Total HxCDD ND 2.59 ND SS 123469-HxCDF 10Total HpCDD ND 2.64 ND SS 1234689-HpCDF 10

AS 1368-TCDD 81

Total TCDF ND 1.54 ND AS 1368-TCDF 8Total PeCDF ND 1.51 NDTotal HxCDF ND 1.48 NDTotal HpCDF ND 1.87 ND

Total PCDD/Fs ND NDITEF TEQsTEQ: ND=0 0 0 

TEQ: ND=DL/2 3.26 3.26 TEQ: ND=DL 6.52 6.52 

 Tel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 

Checkcode: 624-408 AP D/F 2010 Rev. L Report Created: 14-