Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to 

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This 

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. 

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are 

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are automatically 

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Information 

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865-

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet.

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected 

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the units of 

measure.
EIA Facility Code Facility Name Boiler ID Fuel Type 1

8906 ASTORIA 40 No.6 Fuel Oil (residual or bunker C)
Fuel Type 2 Fuel Type 3 Other Fuel Description

 or bunker C)
EIA Facility Code Facility Name Boiler ID Basis Analyte

8906 ASTORIA 40 As Received Higher Heating Value

8906 ASTORIA 40 As Received % Moisture

8906 ASTORIA 40 As Received % Ash

8906 ASTORIA 40 As Received % Sulfur

8906 ASTORIA 40 Dry basis Higher Heating Value

8906 ASTORIA 40 Dry basis % Ash

8906 ASTORIA 40 Dry basis % Sulfur

8906 ASTORIA 40 Dry basis Antimony

8906 ASTORIA 40 Dry basis Arsenic

8906 ASTORIA 40 Dry basis Beryllium

8906 ASTORIA 40 Dry basis Cadmium

8906 ASTORIA 40 Dry basis Chlorine

8906 ASTORIA 40 Dry basis Chromium

8906 ASTORIA 40 Dry basis Cobalt

8906 ASTORIA 40 Dry basis Fluorine

8906 ASTORIA 40 Dry basis Lead

8906 ASTORIA 40 Dry basis Manganese

8906 ASTORIA 40 Dry basis Mercury

8906 ASTORIA 40 Dry basis Nickel

8906 ASTORIA 40 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D 240

ASTM D 482

ASTM D 1552

SW6010B

SW6010B

SW6010B

SW6010B

ASTM E776/9253

SW6010B

SW6010B

ASTM D 3761

SW6010B

SW6010B

ASTM D 3684/SW7471

SW6010B

SW6010B
EIA Facility Code Facility Name Boiler ID HAPs Test Group

8906 ASTORIA 40 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

4/27-55148 4/27/2010 4/28/2010 18770

4/28-55153 4/28/2010 4/29/2010 18790

4/29-55174 4/29/2010 4/30/2010 18790

 Fuel Testing Results



HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Btu/lb 0.06 0.3 0.01% <0.001 mg/Kg <3 mg/Kg <2

Btu/lb 0.07 0.3 0.01% <0.001 mg/Kg <3 mg/Kg <2

Btu/lb 0.12 0.31 0.02% <0.001 mg/Kg <3 mg/Kg <2



Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.52 mg/Kg 4.83 mg/Kg

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.21 mg/Kg 4.01 mg/Kg

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.35 mg/Kg 3.96 mg/Kg



Note the Proximate/Ultimate data below should be recorded on a dry ba

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

5.02 mg/Kg 18 mg/Kg 0.222 mg/Kg 0.06

4.48 mg/Kg 15 mg/Kg 0.162 mg/Kg 0.07

4.03 mg/Kg 24 mg/Kg 0.128 mg/Kg 0.12

Proximate Analyses, % by wt



e data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

87.1 11.8 0.41 0.3 0.33

87.0 11.6 0.42 0.3 0.57

87.6 11.3 0.4 0.31 0.24

Ultimate Analyses, % by wt



EIA Facility Code Facility Name Boiler ID HAPs Test Group

8906 ASTORIA 40 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

4/27-55148 4/27/2010 4/28/2010

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

18770 Btu/lb 0.06 0.3


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

0.01 % <0.001 mg/Kg <3 mg/Kg <2 mg/Kg <1


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.52 mg/Kg


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

4.83 mg/Kg 5.02 mg/Kg 18 mg/Kg 0.222 mg/Kg


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

0.06 87.1 11.8 0.41 0.3

Proximate Analyses, % by wt Ultimate Analyses, % by wt


 basis (including ash).

Oxygen

0.33


EIA Facility Code Facility Name Boiler ID HAPs Test Group

8906 ASTORIA 40 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

4/30-55177 4/30/2010 5/1/2010

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

18730 Btu/lb 0.07 0.29


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

0.01 % <0.001 mg/Kg <3 mg/Kg <2 mg/Kg <1


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.36 mg/Kg


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

4.26 mg/Kg 3.94 mg/Kg 16 mg/Kg 0.119 mg/Kg

Proximate Analyses, 


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.07 87.2 11.9 0.42 0.29 0.12

Proximate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

8906 ASTORIA 40 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

4/28-55153 4/28/2010 4/29/2010

4/29-55174 4/29/2010 4/30/2010

 Fuel Testing Results


y metalic HAPs

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

18790 Btu/lb 0.07 0.3

18790 Btu/lb 0.12 0.31


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

0.01 % <0.001 mg/Kg <3 mg/Kg <2 mg/Kg <1

0.02 % <0.001 mg/Kg <3 mg/Kg <2 mg/Kg <1


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.21 mg/Kg

mg/Kg <1 mg/Kg <1 mg/Kg <1 mg/Kg 1.35 mg/Kg


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

4.01 mg/Kg 4.48 mg/Kg 15 mg/Kg 0.162 mg/Kg

3.96 mg/Kg 4.03 mg/Kg 24 mg/Kg 0.128 mg/Kg

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.07 87.0 11.6 0.42 0.3 0.57

0.12 87.6 11.3 0.4 0.31 0.24

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm

mg/Kg