Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. 

to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific 

This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were 

tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted 

yellow are required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fi

automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865-04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If 

of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, ora

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results works

6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a m

3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you 

collected more.

7. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the uni

measure.
Information

nformation about chemical analyses of fuels 

, chlorine, fluorine, and metals, such as 

nd selenium. This spreadsheet is intended 

p to 4) fuel analyses at that specific boiler. 

esting for all 4 HAP surrogates were being 

Fields that are highlighted in 

down boxes, included. Gray fields are 

_Testing.xls).

ler on the Boiler Information worksheet.

fuel column of the Boiler Information 

 the Other Fuel Description column.

ethods worksheet. For example: "ASTM 

 Picklist worksheet (orange tab). If the units

le, please fill them in the blank, orange 

e in the Fuels Sample Results worksheet.

s worksheet. You must provide a minimum of 

re not limited to that number if you have 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Test Date

997 MichiganCityIN Unit 12 3/10/2010
Fuel Type 1 Fuel Type 2 Fuel Type 3

subbituminous subbituminous subbituminous
Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

997 MichiganCityIN Unit 12 As Received Higher Heating Value

997 MichiganCityIN Unit 12 As Received % Moisture

997 MichiganCityIN Unit 12 As Received % Ash

997 MichiganCityIN Unit 12 As Received % Sulfur

997 MichiganCityIN Unit 12 Dry basis Higher Heating Value

997 MichiganCityIN Unit 12 Dry basis % Moisture

997 MichiganCityIN Unit 12 Dry basis % Ash

997 MichiganCityIN Unit 12 Dry basis % Sulfur

997 MichiganCityIN Unit 12 Dry basis Antimony

997 MichiganCityIN Unit 12 Dry basis Arsenic

997 MichiganCityIN Unit 12 Dry basis Beryllium

997 MichiganCityIN Unit 12 Dry basis Cadmium

997 MichiganCityIN Unit 12 Dry basis Chlorine

997 MichiganCityIN Unit 12 Dry basis Chromium

997 MichiganCityIN Unit 12 Dry basis Cobalt

997 MichiganCityIN Unit 12 Dry basis Fluorine

997 MichiganCityIN Unit 12 Dry basis Lead

997 MichiganCityIN Unit 12 Dry basis Manganese

997 MichiganCityIN Unit 12 Dry basis Mercury

997 MichiganCityIN Unit 12 Dry basis Nickel

997 MichiganCityIN Unit 12 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865-00

ASTM D3173-03

ASTM D3174-07

ASTM D4239-08

ASTM D5865-00

ASTM D3173-03

ASTM D3174-07

ASTM D4239-08

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

SW846 6010B

CFR136A 1631E

SW846 6010B

SW846 6010B
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

997 MichiganCityIN Unit 12 M29

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Run 1 3/10/2010 9460.00 Btu/lb 24.05

Run 2 3/11/2010 9430.00 Btu/lb 23.98

Run 3 3/11/2010 9580.00 Btu/lb 23.64

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

5.46 0.46 12455.563 Btu/lb 7.19 0.60

5.16 0.49 12404.630 Btu/lb 6.79 0.64

4.92 0.45 12545.836 Btu/lb 6.44 0.59


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

218 ppm 0.0518 μg/g 1.9 mg/Kg 0.28 mg/Kg 0

298 ppm 0.0471 μg/g 2.3 mg/Kg 0.27 mg/Kg 0

243 ppm 0.0418 μg/g 2.1 mg/Kg 0.26 mg/Kg 0


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/Kg 5.4 mg/Kg 1.8 mg/Kg 10 mg/Kg 3.8 mg/Kg

mg/Kg 4.6 mg/Kg 1.6 mg/Kg 8.7 mg/Kg 4 mg/Kg

mg/Kg 4.3 mg/Kg 1.6 mg/Kg 9.2 mg/Kg 3.6 mg/Kg


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

0.42 mg/Kg 84.4 1.2 mg/Kg

0.58 mg/Kg 0 1 mg/Kg

0.53 mg/Kg 0 1.1 mg/Kg


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

997 MichiganCityIN Unit 12

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

997 MichiganCityIN Unit 12

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

997 MichiganCityIN Unit 12

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm