### , \ 

### f.i;\Wp(jO\SCOTT\RPTS\2333.RPT



## AMERICAN NICKELOID COMPANY CHROJ\.1IUM EMISSION COMPLIANCE TEST FROM PLATING OPERATIONS CONTROLLED BY SCRUBBER AND WST ELIMINATOR

Prepared for: American Nickeloid Company Walnutport, Pennsylvania Plan Approval No. 48-318-001A Submitted to: Pennsylvania Department of

Environmental Protection and United States Environmental Protection Agency
Prepared by: Davi Williamson Senior Field Techni ian Region III

February 1997 Reviewed by: Steve Dy k 

### Manager
- Field Servic


### ERD ENVIRONMENTAL INC. 

### A Division of ERD Waste Corporatioll Pipersville, Pennsylvania 18947 (215) 766-7230

### TABLE OF CONTENTS

1.0 INTRODUCTION .....................................................• , . 1 

### 2.0 PROCESS DESCRIPTION ................................................ 

### 2 3.0 

### SAMPLING AND 

### ANALYTICAL PROCEDURES ............................. 3 

### 3.1 INTRODUCTION ................................................. 

### 3 3.2 SAMPLING LOCATION ............................................ 

### 3 3.3 VOLUMETRIC FLOW ................' .."; ..**~** 

### ................... " .. 3 3.4 CHROMIUM TESTING ................... : .......................... 4 4.0 TEST RESULTS ........... , ........................... , ................ 5 

# I APPENDIX A CALCULATIONS APPENDIXB DATA SHEETS 

# I APPENDIXC LABORATORY DATA 

# I APPENDIXD CALIBRATIONS APPENDIXE PROCESS LOG DATAIEMISSION PRODUCTION DATA 

# I APPENDIXF BACKGROUND INFORMATION 

# \

# I I 

# I I 

# I I 

# I 

# I I I 

# I · 

### .... 1 

### F:\WP60\SCOTnRPTS\2333 .RPT 1.0 INTRODUCTION 

### ERD Environmental Inc. conducted an emission test program at the American 

## " Nickeloid facility in Walnutport, Pennsylvania. The date ofthe evaluation was January 21, 1997. 

### The purpose ofthe test program was to evaluate compliance with applicable Pennsylvania Department ofEnvironmental Protection (pADEP) and the Environmental Protection Agenc¥,.s regulations under NESHAP governing a chrome plating operation. The objectives ofthe evaluation were to determine emission levels oftotal chromium, Stack testing was performed for the following parameters at the mist eliminator exhaust: Total Chromium' •



### . Oxygen/Carbon Dioxide

Volumetric Flow Rate

Stack 

### Gas Moisture Presented in**thi~** 

### report are the complete results ofthe test program. Questions may be addressed to: Mr. David 1. 

### Williamson
- Senior Field Technician or Mr. Steven Dyck
- Manager
- Field Services ERD Environmental, Inc. 6205 

### Easton Road Pipersville, P A 18947 (215)766-7230 

### Phone (215)766-2051 Fax 

### The facility contact is: Mr. William Cline American Nickeloid Company 129 

### Cherry Street Walnuport, PA 18088 (610)767-3841 

### Phone

### , . 2 

### F:IWP60ISC OTTIRPTS I2333. RPT 2.0 PRO CESS D ESC RIPTIO N The emissien compli ance te st evaluated total chromium em issi o ns emanati ng from plating operatio ns. Fum es exhau sted from the soluti o n tanks are treated 

### by a Heii packed tower scrubber and a KCH chemical mi st eliminat or. Ap pend ix E co ntain s a sketch of the sy stem and 

### pre s ents the process obtained during the te sting. Additional information is pre sented in Appen3ix F .3 

### F:\ WP60\SCOTT\RPTS\2333.RPT 

### 3.0 

### SAMPLING AND ANALYTICAL PROCEDURES 3.1 INTRODUCTION The procedures employed for testing are as defined in detail in the following US EPA Reference Methods found in the Code ofFederal Regulations, Title 40, Part 60,**Appendi~** 

### A 

### (40 CFR60): Method 1 Method 2 "Sample and Velocity Traverses for Stationary Sources"; "Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S Pitot Tube)";



### . 

# . Method 3 "Gas Analysis for the Detennination QfDry Molecular Weight"; Method 4 "Determination ofMoisture Content in Stack Gases"; Method 306 "Determination ofChromium Emission from Decorative and Hard Chromium Electroplating and Anodizing Operations". 

### . 

# . The remainder ofthis section is presented to summarize the test procedures. 

### 3.2 SAMPLING LOCATION Sampling was conducted at the outlet ofthe mist eliminator. Flow measurement was also conducted at this location. ERD Environmental accomplished a characterization ofthe flow patterns for each stack port arrangement to ensure the absence ofcyclonic flow. This measurement took place prior to the conduct ofthe emission compliance test. 

### 3.3 

### VOLUMETRIC FLOW The procedures and apparatus employed for flow measurement are as defined in EPA Methods 1-4. Volumetric stack gas flow was measured using a type S pitot tube assembly. All pitot tubes were calibrated using the procedures in Method 2, Section 4.1.2 and meet the construction criteria ofSection 4.1. A type K thermocouple was used for measuring stack gas temperature. The barometric pressure measurement required during the test was obtained using an aneroid barometer which was brought into the field by the test crew. The aneroid barometer was calibrated using a mercury barometer before leaving the office.

### F:\**WP60\SCOTT\RPTS~333** 

### .RPT 

### 3.4 CHROMIUM TESTING 4


### EPA Methpd 306 "Determination ofChromium Emissions from Decorative and Hard Chromium Electroplating and Anodizing Operations" was employed in characterizing Cr concentration and emission rate from the plating operation. A gaseous sample was extracted from the exhaust gas stream using an unheated EPA method 5 sampling train. A glass nozzle and " . 

# .**~.** 

### probe liner were used. The filter was omitted. Chromium emission are collected in an alkaline solution of0.1 N sodium hydroxide (NaOH). Subsequent laboratory analysis was performed by inductively coupled plasma emission spectrometry (ICP). Sampling was conducting isokentically at 12 traverse points across the stack for a test duration of 130 minutes collecting a minimum sample ?f**S~** 

### dscf. Throughout the testing period, meter readings, temperatures and pressure readings were recorded at 5 minute intervals. Following each sample run, all 

### ofthe glassware including connection glassware, probe line, nozzle were rinsed three time with O.IN NaOH solution. The impinger solution volume was measured. Gas sampling for**~he** 

### determination ofdry gas molecular weight was performed by EPA Reference Method 3 procedures. An Orsat apparatus was used for the measurement ofO2 

### and CO2 

### concentrations. Gaseous samples were extracted from the exhaust at a constant rate. A three-point traverse was made at locations 16.7%,50.0% and 83.3% across the stack diameter. A stainless steel probe was used followed by a teflon sample line. Moisture removal took place in an ice-cooled coil condenser. After passing through a teflon-lined diaphragm pump, the sample was collected in a leak-free tedlar bag. Tedlar bags were leak-checked in accordance with Method lOA Section 4. A portion ofthe bag sample was analyzed for CO2 

### and O2 

### content. Orsat analysis provides for the selective absorption ofoxygen in alkaline pyrogallic and carbon dioxide in potassium hydroxide solutions. The difference in gas volume before and after the absorption represents the amount ofconstituent gas in the sample. Constant temperature and pressure was maintained during the analysis. Stack gas moisture content was determined using EPA Reference Method 4 procedures. The impinger sampling train incorporating sodium hydroxide and silica gel was used for moisture capture. The net increase in the weight ofthe two reagents were recorded as volume ofwater collected (1 gram 

## = 1 milliliter). 

### Dry gas meters used in the sampling train were calibrated in accordance with EPA Method 5 Section 7.2.5 

### F:\ WP60\SCOTnRPTS\2333 .RPT**:~** 

### 4.0 TEST RESULTS

." 

### Presented in this section are the test presents ofthe compliance evaluation performed on J rulUmy 

### 21, 1997 at 

### the American Nickeloid Company. Table 4-1 summarizes all 

### parameters tested.



# .. .

### ....... 

# ..:

# .. 6 F:IWP 60I SCOTT\RPTS I23 33 .RPT Tab l e -I-I

Ca!culatlon Summary Date 1 / 21/97 1121 /9 7 11 2 1 /9 7 Average Pcnlllt Limit


# - Run ID 1.00 2.00 3 .00 Start Time 7: 1 7 9 :4 7 12 : 10 F

lIlish Time 9 :30 \1 :55 14 :22 Stack Gas Temperature 

### F ' 109 1 10 II I 110 .00 Velocity fps 38 .40 37. 68 . 3S. 16 3S .0S Vo lume Flow aeon 5,027 - \.932 4 .9 94 -1 984 dscfrn 4.433 - U4 6 -1 .994 -15 91 Oxygen % 1 9.9 19 .8 20 .0 19 .90 Carbon Dioxide % 0.3 0.2 0.2 0 .2 Moisture % 4 .9 4.S 3. 7 4 .5 Multiple Metals Sample Vol ume dscf 6 1.8 9 6 1. 06 6 2 .36 61.77 Isokinctic Ratio % 96.9 9 7 . 5 9 7.4 973 Emission Rates Chromium (gr /dsc!) 1.52E · 06 2.27E- 06 4 . 7 IE- 06 2 . S3E · 06 l m gldscm) 0 .00 0.0 1 O.DI 0.01 0.0 1 ( Ib/hr l 5.78 E· 05 S.6 2E-05 1.79E
- 04 1.0SE · O -l

### J

..... 

# I**~** 

# I I . 

# . 

# I I I APPENDIX A CALCULATIONS 

# I I 

# I I I 

# I I 

# I 

# IProject#: 2333 PLANT: American Nickeloid DATE: 1121197 SAMP.LOCATION : Mister Outlet ... RUN: TEST ID : Method 306 • Total Chromium START TIME : 7:17 FINISH TIME : 9:30 SAMPLE TIME (Mi) 130.00 minutes NOZZLE DIA. (On) BAR. PRESSURE (Pb) = 29.80 in.Hg NOZZLE AREA (An) STK. PRESSURE (ps) 

### = -0.22 in. H20 METER ORIFICE (dH) = STACK AREA (As) 2.18 sq.ft. METER VOLUME (Vm) 

### = STACK TEMP. (Ts) 109 F Pilot Factor (Cp) 0.84 GAS ANALYSIS 0.3 % C02 19.9 %02 79.8 %N2 CHROMIUM 6.10 ug
=== Vm(std) = (Tstd+460)/29.92 x (pb + (dH 113.6)] I (Tm+460) x Yd x Vm V\\(std) = 0.04707 x Vic Bws = V\l\{std) 1 [Vm(std) + V\l\{std)] Md =(.44 x %C02)+(.32 x %02)+[.28 x (%N2 + o/oCO)] Ms = [Md x (1-Bws)] + (18.0 x Bws) METER TEMP. (Tm) SQRT.dP CONDo LIQ. (VIc) METER Y(Yd) STD. TEMP. (Tstd)

Vs = 85.49 x Cp x (SQRT[dP)) x [SQRT {(TS+460)IMsIPs)] Qs = Vs x As x 60 Qs(std)=Qs x (l-BM)X(T std+460)l(TS+460)x(Pb+Psi 13. 6)129.92 %1 = 0.0945 x (460+Ts) x Vmstd I (ps x Vs x An x M.i x (I-Bws»**~** 0.211 inches**.~** 2. 43E-04 sq.ft. 0.75 in. H2O 61.214 cu. ft. 57 F 0.651 in. H2O

67.2 ml 0.9884 70 F

61.888 dty std. cu. ft.

3.16 cu. ft. 0.049 28.84 Ib.llb.-mole (dty basis) 28.31 Ib.nb.-mole (stack) 38.40 ft. per second 5,027 eu.ft. per minute(actual) 4,433 eu.ft. per minute(dry,std.)

96.9 %



### ======== === === = ======== = 

### === METALS Chromium MASS COLLECTED ug 6.10 Cs 

### = 15.432 x grams I Vm(std) 11000000 Lblhr 

### =Cs x 60 x Qs(std) 17000 Cs gr/dsef 1.52E·06 mgldscm 0.00 mgldscm = (ugll OOO)l(Vm

### * 0.028317 (conversion from dsefto dsem}) Emission Rate Iblhr 5. 78E-05

# I



# I I 

# I I 

# I I 

# I I I**~:** ... Project#: 2333 PLANT: American Nickeloid DATE: 1121197 SAMP.LOCAnON: Mister Outlet .. RUN: 2 TEST ID : Method 306
- Total Chromium START TIME : 9:47 FINISHTIME: 11:55 SAMPLE TIME (Mi) 130.00 minutes BAR PRESSURE(Pb) ::: 29.80 in.Hg STK. PRESSURE (ps) -0.22 in. H2O STACK AREA (As) 2.18 sq.ft. STACK TEMP. (Ts) llOF Pitot Factor (Cp) 0.84 GAS ANALYSIS 0.2 % C02 19.8 %02 80.0 %N2 CHROMIUM 9.10 ug
======= === === = Vm(std) = (Tstd+460)l29.92 x [pb + (dH 113.6)] / (Tm+460) x Yd x Vm**V~std)** =0 0.04707 x Vic Bws :::**V~std)** I [Vm(std) +**V~std)]** Md =(.44 x %C02}+(.32 x %02)+[.28 x (%N2 + %CO)] NOZZLE DLA. (Dn) NOZZLE AREA (An) = METER ORIFICE (dH) ::: METER VOLUME (Vm) 

### = . METER TEMP. (Tm) SQRT. dP CONDo LIQ. (VIc) METER Y (Yd) ... STD. TEMP. (Tstd)



### = 

# I Ms::: [Md x (1-8ws)] + (18.0 x 8ws) Vs = 85.49 x Cp x (SQRT[dP)) x [SQRT{(Ts+460)IMsIPs}J =0 

# I Qs=VsxAsx60 

# I Qs(std)=Qs x (1-8ws)x(Tstd+460)l(TS+460)x(pb+PslI3.6)/29.92 %1 = 0.0945 x (460+Ts) x Vmstd I (ps x Vs x An x Mi x (1-8ws» =


### = 0.211 inches 2.43E-04 sq.ft. 0.74 in. H2O 60.74 cu. ft. 60 F 0.638 in. H20

66.0 m1 0.9884 70 F

= 61.0S7 dry std. cu.ft.

3.11 co. ft. 0.048 28.82 Ib.nb.-mole (dry basis) 28.30 Ib.nb.-mole (stack) 37.68 ft. per second 

### _0

4,932 cu.ft. per minute(ac:tual) 4,346 cu.ft. per minute(dJy,stcl)

97.S %

======= === = === = ======= = === = 

### ====== METALS Chromium MASS COLLECTED ug 9.10 Cs::: 15.432 x grams I Vm(std) 11000000 Lblhr = Cs x 60 x Qs(std) /7000 Cs gr/dscf 2. 27E-06 mgldscm 0.01 mgldscm = (ugll000)l(Vm* 0.028317 (conversion from dsefto dsem}) Emission Rate Iblhr 8. 62E-OSProject#: 2333 PLANT: Americaa Nickeloid DATE: 1/21197 SAMP.LOCAnON: Mister Outlet ... RUN: 3 TEST ID : Method 306
- Total Chromium STARTTIME: 12:10 FINISH TIME: 14:22 SAMPLE TIME (Mi) 

## = 130.00 minutes NOZZLE DlA. (On) BAR. PRESSURE (Pb) = 29.80 in.Hg NOZZLE AREA (An) STK. PRESSURE (ps) 

## = -0.2 in. H20 METER ORIFICE (d.H) STACK AREA (As) = 2.18 sq.ft. METER VOLUME (Vm) = STACK TEMP. (Ts) 11IF Pitot Factor (Cp) 0.84 GAS ANALYSIS 0.2 % C02 20.0 %02 79.8 %N2 CHROMIUM 18.90 ug
====== === === Vm(std) 

### =(Tstd+460)l29.92 x (pb + (dH 113.6)] 1 (Tm+460) x Yd x Vm Vw(std) 

### =0.04707 x Vic Bws =**V~std)** 1 (Vm(std) +**V~std)]** Md =(.44 x %C02)+(.32 x 0/002)+[.28 x (%N2 + %CO)] Ms = (Md x (l-Bws)] + (18.0 x Bws) METER TEMP. (Tm) SQRT. dP CONDo LIQ. (VIc) METER Y(Yd) 

## sm. TEMP. (Tstd)

Vs =- 85.49 x Cp x (SQRT[dP]) x [SQRT {(TS+460)/MsIPs}] Qsc Vs x As x 60 Qs(stdFQs x (I-Bws)x(Tstd+460)l(Ts+460)x(pb+PslI3. 6)129. 92 %1 = 0.0945 x (460+Ts) x Vmstd 1 (ps x Vs x An x Mi x (I-Bws»**~**

=- 0.211 inches 

## ...- 2.43&04 sq.ft. 0.76 in. H2O 62.993 eu. ft. 68 F 0.647 in. H2O

51.0 m1 0.9884 70 F

62.364 dry std. cu.ft. 2.40 cu. ft. 0.037 28.83 Ib.lIb.-moie (dry basis) 28.43 Ib.llb.-moie (stack) 38.16 ft. per second 4,994 cu.ft. per minute(actual) 4,444 cu.ft. per minute(dry,std.)

97.4 %



### ====== 

### == = === 

### ======= === ======= METALS Chromium MASS COLLECTED ug 18.90 Cs = 15.432 x grams 1Vm(std) I 1000000 Lblhr 

### =Cs x 60 x Qs(std) 17000 Cs gr/dscf 4.71&06 mgldscm 0.01 mgldscm = (uglIOOO)l(Vm* 0.028317 (conversion from dscfto dscm}) Emission Rate Iblhr 1. 79E-04

# ~



# I

. 

# I I



# I 

# I :t.

-. 

# ,
. .,



# ..

. 

# .

. .

APPENDIXB DATA SHEETS ....... ..;

### Particulate Sampling Data Sheet Project Number ,)... \ 

## ? ) Plant 

## A,i.Ij"", 

### '/N 

## Al: _**k~** 

## Iv: d Dale _--ll,--"/--l,..c:.l..ul/_'.L,.'j,.,!,."1 _____ _ 

### Sample LocationJ 

### 1''1 !!, 

# tee u!/d&t Run Number 

## tt I f.,t 

### 30(., 

### Operators ft-l 

## n)/ I) ;,y' 

### Ambienl Temperature jQo 

## f Barometer**_..,;,.~::....;~~i..:..l_** 

## 3"""--____ _ Sialic Pressure _-_'-..::.,1.==:).."--__ _ 

### Pilot Factor _.......,;,. •..J.ct.8:....;..L....{____ _ Inches tlg 

# 1<-' S II 

## D

, [,1 '-'1**l~akRak** _ L' Traverse Sampling Gas Healer RClidin.

Poinl Time Inil. 

### 1[2. )- 

## 2 9 

## At 10**"?tJ,~** 

### , () 

# if**~** 

# ).,:**3/~** 

### J 

### It"**~ ~L**  

### l' 7.1 

## 3'1 Lf**~/l ~7/**  

## 4 7 S <;C' 

### -';:Ji ... 

## J .• 71 \ .,.**~** 

### ll' 

### 3' /";**~-** 

### (, 

## c1 ,. 

## I; I 

### 10 -=] q/I. 

### Db .J. )..1) 

## { qt.f ,)7**.~** "JiJ 

### "]'IB.'1::A I.} 

### :./0**LIO>.1/~** t) 

### 50**t.lu~** 

### 7.) t;. t;;:::Ij, 7() 

## '1 (g. c; ,**~** 

### Total**~11V** 

### Average I 

### D.**~~**

# -~'ra 

# I C'I}:iJlVJt!£ /2\/1-" ·tP / Estimates for K-Faclor 

### Determination

p. 

## = - I 

### )J.. 

### t,Oz = 

## d-.a 0,-(' 

### "C02 

### = () 

# "1" T. = 

# I /J 

## 5- Tm = 

### hf" 

## Bws =

### _1~o_6,---- 

# __ _ Yd 

# = (1; 

### 9M35/ dH@ = 

# i, 741'39 Slack ID = 

## ;;..IJ I, K = 

## /.73 (I,

### 7~ HI

### A-~') (. , I 

# a It.ffr'1' 

### 6 -1)
Vel. Press. Orif. Press. 

### dP dH



## . "1

# t1 .71 •**,~;J..** 

## • ''il**.~J..** 

## 19"1 ,**~2** 

## Ib 

## 7

.**?~'** 

## , ,., I

')(, 

## • (.. L/ 

## ·31 J 

### I, 

## If**~:J** -(J 

# 1
I 

## 17 .197 1'-17 l**~y**



### ....**i~ ~**  

## '3L:


## , i.i../ 

# .7" Slack Temp. 

### T. 

## I{JE 10'1 

## 101 101 i 

## 10 jDh 

# 'iJ**~** ; 10 I 

## 10 I J() 

### II () lD9 Ih.·.• foe. 

### -'1/

..' •

';;J 

### C I.. 

### C \I**~** 

# r f. 

## o ., ,\ :I L;' 1-

MelCrTemp.



### .. T. In Oul**,,-~**

# . It,;o .t;';J.. 

## ,6 

## S 1 S'7 ') 1./**1~/1** f)'

### '1 

# fJ-Z 5**~ I,,~'** **.~)** 

### ,l. 

### fi"I
.. 

## c7 '56 C;x 

# <x /." 

# ,**i,~f)** 

### ';';1**~I** (jl I/J**~-** .f.-"n F.-ImNrtmIoI T«ItItt>It>('I .ct flMri",. til N".11111 AI, Nnwo,l. Inc 

## .'

. ;' 

### Page I 

### of ......fl.-_ 

### Test Number ...,,;q:=.:,... . .;../ __ _ 

### Meter Box 

### Number --,--,I**d-.~--­** 

### Port Upstream Duel

### _=3:..:b~- 

## ...... 

# --=-_ 10'(-;" Port Downstream Duct ___ _ Impinger Catch ml lj 0 

### Tolal ml H 2 

### 0

### _~...,..G,::......:.-t-_.**~2** 

## ______ Silica Gel grams _'**...:.)_-=r~·....:·2::....-** __ % O 2 

### i 

# 1: 

# t , % CO2 _!-I .,L)__ ....-___ _ 

### Nozzle 10 _'-,'

# j!!,.J~/~Jr-'----- Start lime**_7L-..J../~7:..._**

### ____ _ 

### Finish Time**......,!".;.~.~.3L~;**

## ____ _
Pump Impinger 

### Box 

### Filler Vacuum Temp. Temp_ Temp. ').. 1(,) f)-/./ 

### il**:~t** 

## .'l- 1',;// 

### )..,0 '\**.~** 

### )'\ l' 

## _S- .;2. 

## J.d:) 

# t)'u J..ti 

## 4", l,E. 

### ../7**.~** I)**,(~'"** 

### l,{j 

## 0./1**~,IJ** 

### Iff( .:1. 

### ,0,; 

### !JI 

# :175 

# 5",-**~,D** ':>Lf II j**~_.o**

### Particulate Samplioa Data Sheet ;J ., ., 

### Project Number 

## d-.**~** 

## 5 ) 

# 1f;+iLl £:.htc;M (..

## ~vtJ**1F~** Estimates for K-Factor Determination Pale 

## I 

# orL Test Number pS' , ;2.. 11 

### Plant

### 4M~€.'kdAI 

# !V:Leke/();,,) Dale 

### I / .)../ / 

# 9 7 Sample Location**(.,~** ''1 I 

### trW&. 

# au tle-f' 

## P 

# = --, ,-A,b Meter BOK 

### Number

# #~~ •**~Ol=** 

# lrt.**~** Port Upstream Duct 

## "COl = 

# 0,3. Port Downstream Duct 

## 10 

# J? Run Number 

# #"c**~** 

### 30(., T 

# = • 110 Implnlcr Catch ml 

# yo C?pcrators MfP

# lOw Ambient Temperature**~'?~[)** _iJ

__ _ 

### Barometer 

## J/J .$ 

### Sialic Pressure - : 

## fl.).. 

## T 

# = 

# tz?: Total ml "20 fc,b 

## • &wI 

# = .(25 Silica Oelarams**~** V.. 

# = Ot 

# 98 gJ5"1 %0

### 2 

## l2,8 • dH@ == 

## /,**7~"S~l** % CO

### 2 

# O,a1 ,. Pitot Factor , 

# g{ Stack ID 

## = ;)../) 1/ 

### Nozzle ID 

## ' L" 

## K= 

# l·<;(t Start TIme 

# 9 t 

# /+- • 

# i 0 Finish lime 

## il**S-~**

a Trivcrse ' Samplinl 015**H~'{{** 

### Radial Vel. 

# 'rca. Ortf. Plea. 

### Sladt Temp. Meter

### TClllp. Pump fmpiDJCr BOI 

### FIlter

Poinl 

### Time lnil. 

## y \**:r~** 

### i, dP 

### dH . 

### T. 

## T. Vacuum Temp. Temp. Temp. i 

### fa Oul 

## i**~** I() 

# YL;'; ·3i**.~~** (to 

### ' (j;fL, (':'V 

## J.. 

# " {, 

## ,ViA 

## .viA' 'L 

## IJ**cA~** 

## tJ**c3~** 

# . to**~** 

### \0'1 ' (pI**Co~** 

## 2-**~')** I '} 

### :;J 

### '13d-.. ,**,,~** 

### ,IA"Z**I~** 

### vi) 

### h? . 

## ::to 

## hL I <..\**~(J** 

### 'l.,,?A-·O

# ~"'''' 

# ":g InlJ 

# f'"4**IA~** 

## ;;;... 

## 1:,/**~** )1) 

### ;J 

## "'-1 q**,~** 

## t&'3 ' Ilo**~'~** 

# k1 2. 

### 6,2 

## G 

## to "'''

## ",71~ J 

## t./ IJ I 

### 7:.1 

### IDl$**~7** hI) ;).. 

### VlS 

## \ '3 '1'1) 

### L({1. 

## '3 JIIIIIf.q;). 

### ...-.iitt,7h 110 

# "to C;tj**~** 

## loO 2- '?f{J**i..f5~1** 

## 1**~** 

### 1./7**a~<** 

# ua**-,~** 

## 57 ;)... 

## bO '? "\t 

## (lill L{ 

## l5D I

### ~ 

## I 

## If:) bl**~1** LA J1 

### J**~** 

### \i1U 

# 4"" 0**l~q** I 

### 11 

### , '0 

## Sq ')9**~** 

### 61 

## c:, \\U 

## L/ 7/J '"**t~b** 

### ,fA) 

# '" {"O**~IJ** 

### d.. 

### foL 

## lu**,~** 

## pllfl/8**~11J** 

## .. 

## Lf<'1 l37 It, 7 

### 108**~1 ~J..**  

### ;t 

## b7 \ Total**i~**

# ~ " 

# \ Avcragc 

## \ $t:0II T«"""" A DItUoItof IAIr

# --.'ItC. DIIt .....

### Particulate Samplina Data Sheet 

### Project Number 

## 2= 3' 

## 1 3 Plant

### A,...~g'{dtJ 

## M, ke/;J;d Dale 

# I / ,j. 

## II 

# 9 -; Sample localion C. t. 

### M... 

### Ire tJvH& 

## fRun Number -J:I:' 

## 3**--~---- ~perators**  

## t1 

## (f,l 0 

## a,v Ambient Temperature 

## -----.:''-''0'-' __ _ Baromeler 

# 19 , g Static Pressure -.**)~** 

### Pitol Factor c 

# 4

# r

Inches liS Leak Rate



### Traverse

Poin. 

## AI 

# 4 

# 8' J
Average SCOff / 

### ...**~** 

### I) 

# 5 0 

## 0 t) 

### Samplinl Ou Healer Radin,



### Time Inll. 

## y.**Z~! (1.~**  

## tJ. If) 

# ;0 liD 

## c;o 

# bO
\00 

### Estimates for K-PlICtor Determination 

### P = -,;).;;)..



## • .OJ = 

## 19.a -COl = 

# t2. ;}.. T. = 

### 110 

## T. = 

### b)" 

## Bws= 

## tOS'**~= O.98&~~1**  dH@ = 

## I .. 

## 7 1119 Slack ID 

### = 

# a,.O " K = 

# 1.81

Vel. 

### Pras. dP 

# .36**I~n**
;1*. 

### Odl. Prca. dH
0



# 80**-~** 

### Sid

### Tcmp. 

# T. ( ( cJ 

# HI flO flD 

## Ut , I J 

### HI 

## lJl I I/) 

### Meier Tealp. 

## T. I. Out



## " 70 1l 

## 1"5 

# - Page , of 

### i -:::--r:- 

### Test Number 

### II":!
00 

### Meier 

### Box Number 

### I.;t 'l 

### Port Upstream 

### Ducl 

## <6jt-;.. Port Downstream Duct 

## I()**~;'** Imploler Catch ml 

### '1 

# & ... I Total ml 

### HIO 

## S- 

# i ,.. / Silica Oellrams 

## _L....:I**3~j~**

## __ % 

### 0 1 -:2-0.0 

### % COl 

## O/a-.·· Nozzle 

### ID , ;}../ / Start TIme ___'wd--I%:...!/.J,o:():-....-__ _ 

### Finish lime**---&.:£l/~2~.2-==----**

Pump Vacuum



## 2 2 Impinler 801 Filla 

### Temp. Temp. Temp. 

### vIA AI/II t .


## biTRAVERSE POINT LOCATION FORCIRCULAR**DU~**

INSIDE OF FAR WAU. TO II _"**~** ,.,0, OUTSIDE 01: NIPPLE (DiSrANCE A) __________ _ INSIJ)E OF NEAR WAI.I. TO 0;"

OUTSIDE OF NIPPI.E (1)ISrANCE 8)
___ -:--_____ _**"A~** HACK 1.0.• (DiSfANCE A·DlSTANCE B) __ ·vv;.:"",.-:: _____ _ NEARESr DOWNSfREAM DISTURBANCE

### ~_--L()i=--l-%L.D _____ _ NEAREST UPSTREAM' DISTURBANCE

### ~" STAC.K STATIC PRESSURE

### ~~=-....:I%:.=::I4lJ=-_]l~_.cz;:~

### ___ :-=:--_ SCHEMATIC OF SAMPLING LOCATION MEASURED BY

### ----'y.~.loo~"(--- VERIFIED BY

### _-"M~.ff:..,,-- 

## _____ _ TRAVERSE! ,RODUCTO' UAVI!IIIII POINT LOCAnO/f

rOINT tRACTION COW_2AHDl FROW ounlDE 0' NIPPU! STAat STAat HUMBI!R Of' STACIC LD. STACXLD. (I'D NeAREST IJIJNOI) DDTAMClla (SUM OP COLUMHI 4 AHD J) 'RI!SSURI! Tl!MPERATURI! 

### I 

## .o--l4 

## 20"**~~** / 

# -::rtf! 'L 

### ·/L1t 

### 3 

# /. 

# 'S 

# 3 ·tt1IJ**~** 

# /**~** , 

# . }1titI 

# 1'1 

# / 14 • 

### Y )"**.~** 

## 11- 

# I 

# ri. er; }iS1 

## V Iq**.y~** 

# / L'lYr

. 

# .

£RD£_,_.I ..... NOTE: stack diameter and calculations must be checked by another member of the test team 

### ,.



# ,.

r :

## Dry Molecular Weight Determination I' 

### Plant:

# /Ja..Q.iJ"h~ 

# NIC!tloid... ' Sampling Time (24-Hour Clock): _-:f.!.....:..-l

### :t-...:...--_'i.t...3~D 

# _________ -:--______________ _ I Concurrent with Run 

### #: _.-.:/ ____ --:-____________**~':~:**

### ________________ _ Sampling Location: 

## Illt

### .5k.r 

## tJ

# v-M.J Date:

# _t..;...~_2_,/_'_t_.,.:,-- __ -------"'.---**~rnple~e~In~rn~Coo~oo~:** _____________________________ _**~n~~lkaJ~ethod: _[_.~~5~~**  

### ___________**~perato~** 

### __**~~**

### _____________**~**

### __**~** 

### Comments:**----------------------------~~---------------------------** 

### Run 1 Run 2 Run 3 Average Molecular Weight of Actual Actual Actual Net Stack Gas (dry basis) Gas Reading Net Reading Net Reading Net Volume Multiplier Mdt Ib/lb-moJe CO2 

# ,.1**.~ ,~**  

# ·3 -1 r) 

### 44/100 

# -3 -?
... <) 

# --



# . 02 (net is actual 

# 1U-]**Jq,~**

### t~. 

# 'I 

# 11·1**l1~** 

# '1 C02 reading minus 

# tv,2**~-Z** 32/100 actual**~2 readin~)**  

### CO (net is actual 02 reading minus 

# - 28/100 actual CO reading) N2 (net is 100 minus actual 281100 CO reading) c,**~** F.RD F.llvironnrellla/a dMsion of ERD W_e CorporGl;on F:lqproscotl/orms\d'J'mo/e

## Dry Molecular Weight Determination Plant:

# .{b'\~·;Uvh**N,{;,kJ~<l** Date: ----.' 6:...- 2

_ 1



## ...;.../_1_"1 __________ ---.£ __ _ 

### Sampling Time (24-Hour Clock): __

# 4....;......-Ll_t-~-(;...:.I....=;S-5-----------_- __---------- Concurrent with Run #: __ 

# 2 ____ :--_-:--___________________________ _ Sampling

# LOC~: 

# Itt, skr- OV·Kl)**Sampk~pe~l~qrn~~Continuo~~------------------------------**

. (; (:.5

# p--r- 7> Analytical Method: ______________ Operator: __**~** 

### _______________**___=~**__ _ 

### Comments: ___________**~------------------------------** 

### Run 1 Rtin2 Run 3 Average Molecular Weight of Actual Actual Actual Net Stack Gas (dry basis) Gas ReadiI!& Net Reading Net Reading Net Volume Multiplier Md, Ib/lb-mole CO2 

# .Z •..-z. 'b ."L- 

## ,1."**.~** 

# .,z. 44/100



# . , 

### 02 (net is actual 

# .**11~~** C02 reading minus 

# W·D \'t. 

## b lA,(j \'{,**~** 

# Y,u 

# ,q**~** 

### 32/100 actual 02 readingl ; 

### CO (nel is actual 02 reading minus 28/100 actual CO reading) , ; 

### N2 (nel is 100 j : 

### minus actual 28/100 CO reading) r, : ERD Et.virollTMntoi 0 divUion ofERD Wasre Co'porDlion F:lqproscollfomultirymoie

### Dry 

## Molecular Weight Determination Plant: 

# KlhlJr I 

### (a,j(\

# AJrcJiJ~,-J Date: 

## _--40'"""-"2_'...;...../_77 ____________ _ Sampling Time (24-Hour Clock): 

### (2 {I!)
- 

### t**~** Z 

### L**~ ------------~--~~------------------------------------------------**  

### Concurrent with Run 

### #: -')



# ------------------------------------------------------------------------- Sumpling Location: __**(\t.;,;,11.:....!~** k..;;,;V"'L-.--=O...::.IJ..!.:.flvV:::.-__________________________________________ _

# ~nJ~~~(~,fuWgrn~,~~inoom~ ______________________________

# ~**~naJylkaJ~ethod:** __

## ~~~(~s~~~~~~~~~~~~~**~pe~to~** __

## ~~~~~~~~~~~~~~~~~~,~~~ Comments:



# ------------------------------------------------------------- Run 1 Run 2 Run') Average Molecular Weight of Actual Actual Actual Net Stack Gas (dry basis) Gas Reading Net Reading Net Reading Net Volume Multiplier Md, Ib/lb-mole 

### CO2

### ~ 

# .t, .1,.- 

### .1.-

## ~~ 

# .2·**.~** 44/100 ,


# . • 02 (net is actual 

# w-Z- to .() C02 reading minus 

# UJ·?. U·o**~O,z..-** 

### 'l(}o 

## 1.,0 

## aU 32/100 actual 02 reading) 

### CO (nel is actual 02 reading minus 

### 28/100 actual CO readil!&) 

### N2 (nel is JOO 

### minus actual 28/100 CO reading) i. ;**I~R[) F.'II';rolln1~/uol**  0 divisioll 01 ERD Wasre CorporlJliofl F:IqFOSCOllformsldrymole**~OIsn;RE** 

### IN STACK GAS 

### BY WET BULB-DRY BULB MEASUREMENT 

## (.,4.F{.a.r II;fo t-.y- 

## Ciw-k-

# J

Plant:

## A,,~)'(ao**tJ\~(Lt.\P-l6** Location: 

## -M 

## ,s

## ~- C 

# vI-ttlStack: 

### Run: 

## I



# ---- Date: 

## (IZl!'?:)..

# Ope~to~: _______

# ~~.~'~(4~k£~e---------------------------------------- 

# ___ Barometric Pressure (Hg) = Static 

### Pressure of Stack (P

### s) = 

### Absolute P bar 

## ±.**~** 

### (P,J 

# = - -2'7.- 

### Pressure 13.6 Wet Bulb 

### Temperature e'F) = Dry 

### Bulb 

### Temperature e'F) 

### = Temp 

### Difference (Td - 

### T",) = 

### Vapor Pressure of H2

### 0 

### at Tw 

### (from table) Panial Pressure of H 2 

### 0 = 

### pp. : PP 

# = ( VP) _ (PA - 

### VP) (.\T) 

### 2800 - (1.3) (T,,) PP =(\.33r)-

### (ZIf.-}(-/.~"J.s)(..s ) 

### 2800
- (1.3) ( 

# e6 ) % 

### Moisture by 

### vOlume 

# = M (PP) ( 

# -r '- '(f 

## 2. )**~** = 

### -(P- A --) 

### (100) 

# = ( '2'7.

### ~ ) 

## Tw 

## =
VP 

# =

=
(100) 

### Vapor Pressure 

### of Water

16**~I** 15 6 105 9 10:**~l** 3"':143 .41**6~** 18 O.O!**~z** 0.l67 6j 1..5 

### a 1.1 10: tz:!.Ii4Z 141 6. 

# 5

11 11**iDH~** 

### in 

## HI

;'

## ;~.~ 

# :**~=~=-'t-i~::-t-~=-+--:-::=+~ ~~~~;'+--~~~~~:~~Ha+~uiH-iirHr;n~n--~l:Z6J~** **~** 0,1: .&6,.3 

### a E**1.6j~:** SI 106 .16 4.1**~** 6 •**~** 1.7 O. n 0..;: E 11M 

### ,.,:n .... ,14 141 " •



## ..**~** 

## (**~ ~-~E·H~a~~~~~~I~~~=+~4~·~~~;H~H-~~irriifttiit1DH**  :9**~9** i9 0 1'1 •. iZI. ... 7. :!O**~l!O** '0 a 10**~** D 2.191 ... , 7. :1 (,t6:! '1 

### a**~l** 46' 1 1 :"a'1Z ".1 7. 1**)~** O.IB1D::' _ 0 "Z i.513 111 :.:,,' t J -, Z ".93J 

### z ._,

### MOISTURE IN STACK GAS BY WET BULB-DRY BULB MEASUREMENT
, 

### Plant:

# /~ M€£It;.}l\) 

# 1\1; L 

# ke**1~'1**

# J Location: Stack: 

## J.O·' Run: 

# P re·1f< 

# I Operators:**_~/'.f..;;;X.:..t1..;;.../""",(}..;...tJ** 

### ___________________ _

## ~ Barometric Pressure (Hg) = 

### Static Pressure of Stack (Ps) 

# = Absolute P bar 

## .±.**~** 

### (PA) 

### = 

### Pressure 13.6**W~t** 

### Bulb Temperature e'F) 

# = Dry 

### Bulb Temperature ("F) 

### = 

### Temp Difference (T d - 

### T'IV) 

### = 

### , Vapor Pressure of H2

### 0 at Tw (from table) Partial Pressure of H2

### 0 = pp pp 

### = ( VP). (PA
- 

### VP) (AT) 

### 2800 - (1.3) (T,,) 

### pp 

### = ( ,. Co£.:, ) _

## (~--1'-I~ ( 

### "3. S- ) 

## 2800 • (1.3) 

### ('1.C{-) ) % 

### Moisture by 

### volume 

# = M ) 

## ( 1**~'L~2)** (100) 

# = ( 2 

## 1.

# -::r1> ) (PP ) 

## P bar 

# = Ps 

# - PA 

# = Tw 

# = Td == .**~T** 

# = VP 

# =

=
(100) 

### Vapor Pressure of Water 

## 2Q. 

# 22 

# - I 

### -2C[

### ~+

# <g 

# 9'1. ')!**i~**

## ~l,t~E



# '3 I 

# t; r.. 

## I::: 

# " .G {,.,



# 5.Sl6 OJ**~I** 1m 6 1.54G7 8 1] 101 un**1~-** l41 i.i il 9.BiI

0.: !O I.3G6 o.l !r1 90 1 m. l14:.n 7. I0.1 H 0.37101 o.7IWI 91 1 467 II z.6l 4.66' 7.**~-** 

## inHa.

.... inHzQ

inHg Of Of 

## :E 

## in Hi

%

It

# fta_ft_, ve1aaL&r , Sua& 

# I cye!-.a.a JDlaC ... 

### (6..**~** 

### ;... 

# n_ 0_. 

# ,.....**~ 1a..~**  

# (,.. ). ·,.t.**~** IftIU 

## l 

# I**Ij~** 

# 1**.~~** 

# I**~** 

# S 'L 

# I .s-/ 

# I 1t, 

# I tot 

# I
L 

# ?' 

# I .**)~** 

# I 10 I 

# I 

# :r / u / 

# ,51 

# I**I~I** 

# 3

. 

# I .(0 ( , 

# If .S" 

# iD 5""

# ~ 

# I I)) 

# fl(, 

# V 

# I 

# , I 

# , I I I 

# I I 

# I 

# I / 

# I 

# I I 

# I I I . 

# I I I I I I 

# I 

# .' I 

# -**~**



# .. 

# , SCItIe_dI:**~ ~a_ft_**  "1&&**~.,..** 

# ftaW"·1- 1

... 

# cr , StMa 

# I cree • .as ... C6 .. 1 ,.... 

# n.-o.••**-~** 

# la.. (If. 

# I,. •**~"11**



# . f. ., / 

# L/1 'JtJ 

# q 

# I Ie 

# tiL Y**~** 

# ;10 

# I**~** 

# I :3

# I'L4~ ./110 

# I**~** 

# I

.

# ~ 

# I " fa L( 

# I flo 

# I 0 

# I
)" I 

# ,& I lto 

# I**rro~** '((0 

## I



# - I I I 

# I I I 

# I / / 

# / I 

# /. I I I 

# I I I I 

# I I I I**------------------~** 

# / I I / 

# I 

# I /'**---I----I--~I --~I**  

# I I I I 

# I I 

# I I 

# I 

# I I 

# I 

# I

L 

# I \-Aw-
....



# ---l**---I--I--~I-** 

# A ..... , I I ____**~**______________ _ 

# I 

# I 

# I I

# jj

# li**;~ ~~**  

# Iijii I 

# i 

# I f ( r .1 

# fit · r · I : t: • ., 

# I' -.'**~** Ii 

# i 

# I 

# : i 

# ! i

# ~ orif . · 

# ! "'-' · 

# f' , .. P J' 

# 111, ,I., J 

### l

# ~**~...** : 

# f ! : 

# T-r' f
.

- i

# ~**t·~ "/.~**  i

# I~ i I . 8 . 

# F ." H III 

### C:." 

# - .. 

# ... ·t 

# tEl .!' - -:;.

## ~**~** 

# ...**~** 

### ;**~** 

# ... 1- .,. :. • 

# .. 'I .. ..**~.:",** 

## ! 

# I i

.. D**~** 

# i**~~** 

# i· .. ·· i 

# f = 

# t i**l~** I _ ii 

# i : .. A 

### • 

# ... " 

### • 

# i 

# J •



# I 

# I. p

# j

:a I- 

# -

1- 

# - Jf

# a:- G
.. - ...

## ~ I- .. 

### Iw '" .... 1--1-- 

# .. il**~f**

- 

# - - - 

## ,- 

## - 

# - 

# -

..**f~** 

# . 

# .. t-**~**

## ~ '.

### ~ .J:. €' 

# ... IoN

### l~ 

### 1. A E=;'



# - - - 

# - - 

## - 

# - 

# - - - - 

# -
. (: 

# .....
- - 

# - -**~** 

# ... , i.e-

- <::. 

# a**~**

## ~ 

# - 1



## - - - 

# - 

# - 

# - - - 

# - 

# - 

# - 

# !iii.:

- - -**~_~I-** 

# = E.**~ ~.** **~** 

# ... 

# ..**~** 

## •**~ ~** **~** 

# - 

# -

, 

# . 

# .. , 

# :1 ; 

# ,"(

- 

# - - - - 

# - - 1- 

# - - - I



# .. 

# ... F '. • u \}.J

### ~ k**~** J 

### Vi 

## ..... 

# .. .. rJ

# I~ -4 

# "

- - - - 

## - - - 

## C\ 

# -**~**

# ~ 

# a ......**~** () 

# ..;;**i~'** II) -<" -(:. ,...



# - - - - 

# - 

# - - 

# - - 

# - - 

# - Ii ...... 

# iH'i:j
i_l-o· 

# . 

# ... .. 

# . Y I § ; I

I I

# !ii

# ,~~:r I c;. 

### r**~** 

### t"t i\' 

## • •**~** , <":: 

### • Q**~** 

# 1ft 

# U If

# I 

# r :1

u 

# g

# t~ 

# I**~** I I 1--0**~** 

### • 

# I N:: II 

# aI Y & DII":'iJ



### .. I I: 

### C,! • • 

# - ...**~** 

# .- • 

# ,. 

# e**~ ~**  , !;

### ,

I 

## l. " '."

## ..

APPENDIXC LABORATbRY DATA

# First Analytical Laboratories CASE NARRATIVE Project 

## #: 70107 Client: ERD Environmental Client Project ID: 2333 Samples: Report Date:**17-Feb-:~7**



### The samples submitted consisted ofthree impiuger solutions and a blank. All were received intact with no apparent leakage. The "target element was chromium only. Preparation: The samples were prepared and analyzed according to EPA Method 306, 

## Determination of Chromium Emissions from Decorative and Hard Chromium Electroplating and

## Anodizing Operations.. Analysis: Chromium was determined by Graphite Furnace Atomic Absorption Spectrophotometry (GFAA). Results: Chromium was measurable 

## in all of the samples. The levels of chromium in the samples ranged from about 6 p.g to 19 ",g. Quality Control: Chromium was not detected in the blank. The spike recovery (102 %) 

### was well within the normal range of 75 

## % to 125 

## %.

# First Analytical Laboratories g MOWlt 

### 'Bolus Road Chapel 

### Hill, NC 27514 (919) 942-8607 

# ANALYSIS REPORT Project 

### #: 70107 Client: ERD Environmental Report Dote: 1 7-Feb-97 :: Dote Received: 24-Jan-97 Client Project 10: 2333


### Sample 

### Run 1 Run 2 

### Run 3 Blank
Spike, %Recovery 

## Total Micrograms in Sample pg Cr 6.1 9.1 18.9 

### < 0.8 

### QUALITY CONTROL SUMMARY 102.2%

# .. 

# First Analytical Laboratories
ANALYSIS REPORT

. 

# . Total Chromium Method 306 Project 

# #: 2333

Prepared for: ERD Environmental 6205 Easton Road Pipersville, PA 18947 Reviewed and Approved by:

# LJ"L)~ William H. Wadlin, Ph. D. Laboratory Manager

February 17, 1997 -

# .. 

# -'CHROMIUM GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET


# .. Client: ERO IOL 

### = 5 pgfL Proj. #: 70107 Postdig'n spike cone. 50 pgfl Dote: 17-Feb-97 Sample 10 Test Dig'te DiI'n Init. Vol. Client FAL Sol'n Cone FV Fodor Vol. Oig'd pg/l pg/l ml ml ml Run 1 70107.1 37.5 37.5 100 1 485 300 Run 2 70107.2 44.2 44.2 100 1 616 300 Run 3 70107.3 102.1 102.1 100 • 1 555 300 Blank 70107.B 4.3 4.3 100 500 300 %REC 

### SPIKE 70107.1S 88.6 102.2% Calibration Data Abs. True cone.,pg/l Blank 0.000 0 Standard 1 0.114 10 Standard 2 0.201 20 Standard 3 0.473 50 Standard 4 0.901 100 Calibration Verifications ICV 

### = 50 50.8 CCVl 

## = 50 ICB 

## = 0 1.7 CCBl 

### = 

## a CCVl 

### = 50 52.4 CCBl 

## = 0 5.3 Thtal ug

6.1 9.1 18.9 < 0.8

# ~ CHAIN OF CUSTODY RECORD 

# PO, j}

# 1~~ Lf87**N~** 

# 002208 EawiroamentaI Services of America, lac. 

## E"'S4 client:;:: .,

## /I/II4Iyl/c.~1**Lei.JtJ/,lflk~/es.** Project Number: 

### ProJect Name: 

# LlL,

# i ..**~** 

# :A

# 33

# .i 

# ;ll'1Eie IL:. AU

## ~ '/ 

## £.;(;.. ,I'> Task Number. Task

# M.~fhtJJ JIJ6 - c..hrlJl"f

## ;'v"" £,..iU;IJJJS 

## I 

# III Sample,. SignaIwe:

# !P2L~**·~U~** Remarka

&b.**~** Dftc:dpIIon Number Dat. TIme Sample ldentlflcatlon 

## 1



# / 1/J.J;'7 ·1;'1 .... 

## :i:30 09300 1'1/ff" CI.II'fIUG /1, ,.£.I • ...L IF L 

## X

" 

# :A I

### 1J.lI'll**~** :-(1'· 

## JJ9KtJ!I fIlS" £J,iJ.flAl.l/lJt. )( ,I:» 

### J1vJkf: (tUAJlt). 

### .. 

# 2 IIJ.J197 I:J.!//)- f) (j 

## 31)/5**~ST** eJ"lMUJa >(**,!i:).~** 

### 11,,-&1-· 

### f",;*-? 

# L/ 1/}.l/97 

## /**lJ9J!/~** 

# 8iAAlk.. K

, •

# ~FL~')&/2~ Date: TIme:

## RectMd~~

# '~"l?Z ReIinquIthed by. (Sig.) Dale: Time: Received by: (SIg.) 

### i/tw91 

## I**itI~/.J IA~**  

### ..(. 

## I c.**~** Relinquished byl'{Sig.) 

# , Dale: Time: Received by: (Slo.) ReJlnquIahed by. (Slo.) Date: TIme: Received by: (SIg.) 

## I 

## I Relinquished by: (Sig.) Dale: Time: ReceHed for LaboralOfy by: (SIg.) Date: Thne: Remarks 

# I 

# 1**----~------------------------------------------------- -----------------------** **~lement** File: CR.GEL Element: Cr Waveleneth:**3S7.~** Date: 1)1/30/97 Time: 13:51 Slit: 0.7 L Data File: rO/Wt File: 70107.IOW Lamo Current: 14 Technieue: HGA Calib. Tyoe: Linear Enercy: 59



## ----------------------------------------------------------------------------- Cr 10: BLANK 

# .. Sea. No.: 00001 AIS Pos.: 0 Date: 01/30/9 uL disoensed: 10 from O. 5 frem 38. 10 from 0**~"?olic=te** !**Pea~** Area (A-s): 0.010 Sackeround Pk Area (A-5): 0.021 Blank Corrected Pk Area (A-s): -0.005 Concentration iue/L 1: -1.1 Time: 13: 53 Peak Heieht (A): 0.012 BacKeround Pk Heieht (A):**O~017**



### to: ELA"'''' Sea. No.: 00002 AIS Pos.: I) Date: 01/3()/9 uL disoensed: 10 from 

### O. 5 from 38. 10 from 0**~c>"'!i,==t5!** 1**Tim~:·13:5~ P"?a~**  Area lA-s): 0.010 BaGkeround Pk Area (A-s): 0.022 Blank Corrected Pk Area (A-s): -0.005 Concentration (ua/L 1: -1.1 '1L Ijisoensed: .!.O from O. 5 -From 39. 10**:;"!'=!lic~te** ., Peak Area (A-s): 0.009 8ackarcund Pk Area (A-51: 0.023 Blank Corrected**P~** Area (A-5): -0.006 Concentration Cue/L ): -1.2 Mean Cone Cua/L ) : -1.2 Auto-zero oerformed.**Pea~** Heioht (A): \).011 Backoround Pk Heioht CAl: 0.018
fr-om ('I Time: 14:02 Peak Heicht CAl: 0.010 Backor-ound Pk Heioht (Al: 0.018


## so: 0.05 RSOC7.): 4.03

i D: 10 PP8 Sea. No.: 00003 A/5 Pos.: 1 Date: 01/30/9 uL disoen5ed: 10**':<~~li,=ate** 1**~"?a"'.** Are Sackor-aun Blank Cor-r cted Pk Area (ua/L 5 from 38. 0.0270.057 39.**'::Qnl;,=?'t~** -; "L tjisoensed: _S;from 

## o.**;::;"!?~...** t:\rea i t:\-s '!: _.07'2 \\, 10 fr-om 1 Time: 14:1)5 Peak Heioht CAl: 0.035 8ackaround Pk Heicht (Al: 0.020
10 from 1 Tim"?:**!.4:1')~** Peak H5!ioht (A): 0.036 Backoround Pk Heiaht CAl: 0.018 BaGYoro\.lnd PI-: Area A-si: 0.027\ 81ank Corrected PI-:

### A'~ea (A-s i: 0\06'" Concentration (uoiL ).. 4 7 .,\- "'ean Cone iuo/L ),

# .",~ 4.; Standard number 1

## aoolied.~ rIO.Ol Correlation coe11icient: 1.00000 50: 0.34 R5DC'l.l: 7.47 S 1 ooe: ·).0060 lnt: 0),000**uL~~is** _nsed: 10**~Qolio:at** 2**~eak** Area O.44Q 8ackoround P. Area (A-s): Blank Correcte Pk Area (A-s): Concentration (u L'): 70.2 Mean Conc (ue/L 64.5 QC samole is out of ranee 39.51 from S Time: 15:18 Peak Heieht (A): 0.224 8ackoround Pk Heieht (A): 0.006
8.12 RSD ( 'l. ): 12.**S~**
10: 50 PPE Sec. No.: r)0009 A/S Pos.: 3 -gate: 01/301 uL disoensed: 10 from O. 5 from 38. 10 from 3**:::;~oli,=ate** 1**~eak** Area 

### (A-s): 0.495 8acKoround Pk Area (A-s): -0.033 Blank Corrected Pk Area (A-s): 0.486 Concentration (ue/L ): 77.7 Time: .! 5: 22 Peak Heioht (A): 0.222 8ackoround Pk Heieht CA): 0.013



### . 

# . I.!!.... disoensed: 10 from O. 5 from 38. 10 from·3 

### .., Peak Area (A-s): 0.469 Backeround. Pk Area (A-s): -0.133 Blank Corrected Pk Area (A-s): 0.460 Concentration (ue/L ): 73.5 Mean Conc iue/L ) : 75.6 Standard number 

### 3 aoolied. 

### rSO.Ol Correlation coefficient: 0.96338 Time: 15:25 Peak Heieht (A): 0.200 BacKoround Pk Heieht (A): 0.021


## so: 2.94 RSOC'l.): 3.89 Slooe: 0.0065 Int: 0.022 

## r:r !D: 100 PPB Seo. "'0.: 00010 A/S Pos.: 4 Da te: 01/30/( uL discensed: 10 from O. 5 from 38. 10 from 4**j;~!:!li,=e.te** ! Peak Area (A-s): 0.869 8ackeround Pk Area (A-s): -0.126 Blank Corrected Pk Area (A-s): 0.860 Concentration Cuo/L ): 129.5 Time: 15:29 Peak Heioht (A): 0.367 BacKeround Pk Heieht (A): 0.002

IlL disoensed: 10 from O. 5 from 38. 10 from 4**:::;~o!i,==.te** 

### :? Peak Area (A-s): 0.950 Backeround Pk Area (A-s): -0.112 Blank Corrected Pk Area (A-s): 0.941 Concentration (ue/L ): 142.0 Mean Conc iue/L ) : 135.7 Standard number 4 aoolied. rIOO.Ol Correlation coefficient: 0.99755 Time: 15:32 Peak Heioht (A): 0.415 Backoround Pk Heioht (A) :" 0.012
SD: 8.85 RSOCI.): 6.52 SloDe: 0.0093 Int: -0.022

f""
.. 

### r D: 10 PPE Sea. 1\10.: 00011 A/9 Pos.: 1 Date: 01/30/1: 0JI... disoensed: 10 from 38. 10 from 1**P~!:'lJcat'? P~alt:**  Area 3ackaround Pk AI'" (A-s): -O.OQ2 8lank Corrected Pk**A~ea** (A-s): 0.151 Concentration (uo/L ): 18.6 15:41 (A): 0.072 around Pk Heiaht (A): 0.012
'JL disoensed: 10 5 from 38. 10 from 1 Peak Area (A-s): 0.133 Backaround Pk Area (A-s): -0.109 Blank Corrected Pk Area (A-5): 0.124 Concentration (uo/L ): 15.7 Mean Conc Cua/L 1 : 17.2 'j i me: 1. 5: 45 Peak Heiaht A): 0.061 Backaround Pk Heiaht CAl: 0.003

so: 2.09 RSO ( !. ): 12. 15 Standard ab5. 

### & conc. values are not in the same order. 10: 20 PPB Sea. 

### No.: 00012 A/S Pas.: 2 Date: 01/30/9" uL di5censed: 10 fram O. 5 from 38. 10 from 2**~D.,li,=at'?** ! Peak Area (A-s): 0.214 8ackaround Pk Area (A-s): -0.050 Blank Corrected Pk Area (A-s): 0.205 Concentration (uo/L ): 24.0 'jime: "15:48**Pea~** Heiaht (Al: 0.096 Backoround Pk Heiaht (A): 0.009
'oiL discensed: 10 from O. 5 from 38. 10 from 2**~~!:'lio::ate** 

### 2 Peak Area (A-s): 0.206 8ackaround Pk Area (A-s): -0.140 Blank Corrected Pk Area (A-5): 0.197 Concentration (uo/L ): 23.1 Mean Conc (uo/L ) : 23.6 Standard number 2 aODlied. r20.01 Correlation coefficient: 0.99949 'jime: 15: 51 Peak Heioht (A): 0.106 Backoround Pk Heioht CAl: 0.016

so: 0.63" R50C'l.): 2.67 SloDe: 0.0089 Int: 0.013 Sea. "10.: (1)013 AI5 Pas.: 1 Oa te: 01/30/9" uL discensed: 10 from O. 5 from 38. 10**~Dnl;r:~.t'?** 1**P~ak** Area (A-s): 0.125 Backoround Pk Area (A-s): -0.049 Blank Corrected Pk Area (A-s): 0.116 Concentration (uo/L ): 11.5 from 1 Time: 16:0 4 Peak Heiaht CAl: 0.064 8ackoround Pk Heioht (A): 0.013

'JL disoensed: 11) from O. 5 from 38. 11) from 1**P~a~ ~r'?a**  IA-s): 0.121 8ackaround Pk Area (A-s): -0.089 Blank Corrected Pk Area (A-5l: 0.112 Concentration Cuo/L ): 11.0 Mean Conc (ua/L ) : 11.2 Standard number 1 acclied. f10.0l Correlation coefficient: 0.99947 Tim'?: 16:()8 Peak Heiont (A): 0.055 8ackoround Pk Heioht (A): 0.005

so: 0.33 RSO(!.): 2.95 Sloce: 0.0089 lnt: 0.017

# I 

# I I I I**I~DisDlay** 

# Calibration - 

# C:\AA USER\AA**FILE~\** 

# •

# I

...-

0.0

Cr 10: lCV Sec. No.: 00014 AIS Pos.: 

### 5 Date: 01/30/( uL disoensed: 10 from O. 5 from 38. 10 from 5 R5l'olicat5l' 1 Peak Area (A-s): 0.492 8ackeround Pk Area CA-s): -0.085 Blank Corrected Pk Area (A-s): 0.482 Concentration (ue/L ): 51.1

....**~** 

### .....**~-** . .,.--..... uL**disoens~d:** 10 from O. 5 from 38. 10 R5l'olicate 

### 2 Peak Area (A-s): 0.487 Backeround Pk Area CA-s): -0.063 Elank Corrected Pk Area CA-s): 0.477 Concentration (ue/L ): 50.5 Mean Cone: (ue/L ) : 50.8 Time: 16:12 Peak Heioht CAl: 0.241 Backeround Pk Heieht CAl: 0.004
from 5 Time: 16:15 Peak Heieht CAl: 0.217 Backeround Pk Heioht CAl: 0.009 

### SO: 0.41 

### RSOCY.): 0.80 QC samole is within ranee 39.51 60.49 10: I CB Seo. No.: 00015 AIS Pos.: 0 Da te: 01/30/c '. 'JL disoensed:**~~!:'li,=~i:e** 1 10 from 

## o. 5 from 38. 10 from 0**~ea~ ~r5l'a**  CA-s): 0.039**8ac~oround** Pk Area (A-s): -0.144 8lank Corrected Pk Area (A-s): 0.030 Concentration iuo/L ): 2.4 Tim5l': 16:19 P5l'ak Heieht CAl: 0.026 8ackoround Pk Heioht CAl: 0.017

'.Ii- oj i 5 Q5l'nsed :**=-eolic~t5l'** 2 10 from O. 5 from 38. 10 trom 0**cea~** Area (A-s): 0.022 8ackoround Pk Area (A-s): -0.145 Blank Corrected Pk Area (A-s): 0.013 Concentration (ue/L ): 1.0 Time: 16:22 Peak Heioht CAl: 0.023 Backeround Pk Heicht CAl: 0.019Meal}. Cone:: (ua/L ) : 1.7 

## so: 1.00 QC samele is within ranee -10.49 10.49 

# I ( (



# l I Reelie:ate Cone::entration**Q'?~lie=te** ...., Cone:entration (ua/l Mean Cone:: (ua/l

Reelie:ate Cone:entration ) :

Cone:entration iue/l Mean Cone:: (ue/l 

### r. .... 7(1107.1**wD~lie:ate** 

### 2 Cone:entration Mean Cone: (ue/L ) :

) : 

# l Ree::overY is 102.3% TO: 70107.2**Q"'~lie~te** 2 Concentration Mean Cone (ue/l
T !): Reolic::ate Cone:entration 2 Cone::entration ) : Sec. 1\10.: 00016 AIS Pos.: 6 Time: 16: 43 ): 4.2 Time: 16:46 4.3 

## so: 0.19

Sec. No.: 00017 A/S Pos.: 7 Time: 16:49 ): 37.3 

# .- Time:- 16:52 37.7 37.5 

## so: 0.30 Sea. No.: 00018 A/S Pos.: 7 Time: 16:55 ): 88.2 Time: 16: 59 89.1 88.6 

## so: 0.59

Sec. No.: 00019 AIS Pos.: 8 Time: 17: 02 ): 44.9 Time: 17: 05 43.6 44.2 SO: 0.89 Sec. No.: 0(021) A/S Pos.: 9 Time: 17:08 ): 103.1 T i**~e:** 17: l! 101.0 RSO ( %): 58. 19

Date: 01/30/C:

RSO(%): 4.42

Da_te:**01/30/~**

RSOC%): 0.81

Date: 01/30/9

RSDC%): 0.67

Date: 01/30/9

RSD(i'.): 2.02

Date: 01/30/9

# I 

# I I I 

# I
t

I' Mean Cone

# ~l' to: 70108.8 See. No.: 00021 A/S Pos.: 10 Reolicate 1 Time: 17:14 Concentration (ua/L ) : 90.2 

# ..**:;Clr'li'::!~9** 2 Time: 17:17 Concentration (ue/L ) : 85.8 Mean Conc (ue/L ) : 88.0 SO: 3.09 TO: 70108.1-1 Sea. No.: 00022 A/S Pos.: 11 Samole abs. is oreater than that of Reolicate 1 the lareest standard. Time: 17:22 Concentration (uo/L ): 280.5
r ... Tn: AS Position 000 See. No.: 00023 A/S Pos.: 0**~eoli.O::3te** 1 Concentratien (ua/L :; ...... 1i.o::at9 :2 Concentration (ua/L Mean Canc iue/L ) : Time: 17: 28 ): 18.4 Tim,:: 17:31 ): 8.4 13.3 

## so: 7.08 

### r,.. TD: 70108.1-1 X 10 See. No.: 00024 A/S Pos.: 11 Reolicat9 1 Concentration (ue/L :;",,...1**(,=~,t"?** 2 ':on ,=,,?n "=.ra tion (ua/L M93n Conc (ua/L ) : Corrected Conc (uo/L ) : ) :

) : 35.4 33.9 34.6 346. Time: 17:34 Corrected Cone (ue/L Tim,: : 17 : 37 Corrected Cone (ua/L SO: 1.02


### ro: 70108.1-1 X 10 See. No.: 00(125 A/SPos.: 11**R~olio::ate** 1 Concentration 

## =", ... 1;o::at9 2**;:onl:~,.,tration** (ue/L (ue/L Mean Conc (uoiL 1: Corr9cted Conc (ue/L Recoverv is 92.21. ): 80.7 ',: 80.7 80.7 l: 807. Time: 17: 41 Corrected Conc Tim"?: !.7:44 Corrected Conc SD: 0.00 (ue/L (ue/L , 

# ... . ". RSO ( Yo): 1. 51

Date: 01/30,

RSD ( Yo ): 3. 51



## .... Date: 01/301

Date: 01/301

RSO(;'): 52.77

Date: 01/30/ ): 354. ): 339. RSOCYo): 2.93

Date: 01/30fc ): 807. ): 807. RSDCI.): 0.00r,.. TO: 

### CCV Seo. No.: 00026 A/S Pos.: 5 Reelicate 1 Time: 17: 47 Concentration (ue/L 53.5**~** ... ,., I**i,=~** te 2 Time: 17:50 

# .. Concentration (ua/l ): 51. 4 Mean Conc (ua/l ) : 52.4 SO: 1.50 QC samele is within ranee 39.51 60.49
r,.. 

### TO: CCE Sea. No.: 00027 A/S Pos.: 0 1 Time: 17: 53 Concentration (ua/l ): 6.7 2 Time: 17:57**Con~ent~ation** luo/l l: 3. q Mean Conc (uo/l ) : 5.3 SO: !. 97 QC samele is within ranae -10.49 10.49 r,.. TO: 70108.1-2 X 10 Sec. 1\10.: 00028 A/S Pos.: 12 Reelie:ate 1 Cone:entration (uo/l**~** ... ,.,I ;-::ote 

### 2 Concentration (ua/l Mean Conc (ua/l ); Corrected Conc tuq/L ): 48.7 1: 51.2 50.0.1' ): 500. Time: 18:00 Corrected Conc Cua/l Time: 18:03 Corrected Conc (ua/l 

## so: 1.77
TO: 70108.1-3 X 10 Seo. No.: 00029 A/S Pos.: 13 Reelicate 1 Concentration ::; ... "Iicate 

### 2 Concentration (uo/L (uo/l Mean Cone (ua/l ) : Corrected Cone: (uo/l ): 39.7 ) : 35.3 37.5V ): 375. Time: 18 :06 Corree:ted Cone: (uo/L Time: 18 :09 Corree:ted Cone: (ua/l 50: 3.13

r".. r D : 70 t 08 . 3 - 1. X 10 Seo. No.: 00030 A/S Pos.: 14**~eolicate** 1 Time: 18:13 (oncentration (uo/l ): 36.6 Time: 18:16 Concentration (ue/l 39.3 Daten 01/30

RSOC'l.): 2.86**.~**

Oa te: 01/30,

RSO(I.): 37.06

Date: 01/301 ): 487. ): 512. RSDCI.): 3.53

Date: 01/30/c ): 397. ):**.~53.** R50CI.): 8.35

Date: 01/3(1/Q., "



## APPENDIXD CALIBRATIONS .... '" '

### .PITOT CALIBRATION PITOT#: 40 DATE: 

### 3/26/96 A-SIDE CALIBRATION 

### RUN# 

### 1 2 3
B-SIDE CALIBRATION 

### RUN # 1 

### 2 3

Dev. 

### = Cp(s) - Cp(s)(avg) 

### = Cp Difference 

### = Aavg - Bavg 

### = Cal 

### by:

dPstd 0.64 0.64 0.64

dPstd 0.64 0.64 0.64 

### " 

## , EW
dP(s) Cp(s) Dev. 

### 0.89 0.840 0.000 

### 0.89 0.840 0.000 

## ,. 0.89 0.840 0.000 Avg. 0.840
dP(s) Cp(s) Dev. 0.89 0.840 

### -0.003 0.88 0.844 0.002 0.88 0.844 0.002 Avg. 0.843 Cp Differ -0.003 (Must be 

### < or 

# = .01) (Must be 

### < or 

# = .01)METER BOX CALIBRATION BY REFERENCE STANDARD DRY GAS METER METERBOX # DATE 12 1/8/97 LEAK CHECKS' Front 1/2 @ 15" Hg= = 

## o Y= OeltaH@ 

### '.

- ,

0.988351

1.79339 Back 1/2 @ 10" H20= Meterbox values Standard Dry Gas Meter Values Delta H Tm Vf Vi Delta H (in. water) 

### (F) (cu. ft.) (cu.ft.) (in. water) 0.5 52 951.728 946.033 0.12 0.5 61 958.377 951.728 0.12

1 64 969.648 958.377 0.14 1 66 981.136 969.648 0.14 2.0 68 999.792 981.136 0.15 2.0 72 1005.504 999.792 0.15 3.0 73 1012.629 1005.504 0.16 3.0 75 1028.476 1012.629 0.16 NIST Traceable reference meter calibration date 2113/96. Yds 

## = NIST Temperature Standard Reading (Calibration Meter) OR (Ft46D) 1 461 109 569 246 706 500 960 751 1685 1004 1464 Each Yd must be +/- 2% of the overall average Yd. Tm Vf Vi 

### (F) (cu.ft.) (cu.ft.) 63 n4.356 768.314 64 781.154 774.356 64 792.613 781.154 64 804.228 : 192.613 64 823.036 804.228 64 828.762 823.036 64 835.936 828.762 64 851.828 835.936 Thermocouple Reader Display (Box) Of' OR (F+46D) -2 458 107 567 243 703 500 960 750 1686 1004 1464
Overall average Yd should be less-than 1.02 and greater than 0.98. Average error on the thermocouple reader must be less than 1 %. 

### o Time Tamb (min.) 

### (F) 15 65 17 65 20 65 20.5 65 24.5 65

7.5 65 7.5 65 16.5 65 0.971528

, Difference %

0.65 0.35 0.42 0.00 -0.06 0.00 Average 0.23 Calibrated By: MJP

Pbar Y Delta H@ Qn. Hg) 29.61 1.0081 1.763 29.61 0.9867 

# . 1.764 29.61 0.9856 1.709 29.61 0.9839 1.741 29.61 0.9824 1.889 29.61 0.9843 1.896 29.61 0.9880 1.808 29.61 0.9878 1.777

L.•

# .

# I**~-**


# - I. I I 

# I 

# i' I 

# I. I I'. 

# I 

# I: I. 

# t l.
'- 

# l ..... 

# . 

# -

. 

# .

APPENDIXE 

## PROCESS LOG DATA/EMISSION PRODUCTION DATA

# I l.
t 

# I AMERICAN NICKELOID COMPANY MANUFACTI...F1ERS OF PRE.FINISHED METALS

ADDRESS REPLY TO: EASTERN WORKS

Wl/nurpon. htIMY",."i. ISD88**T~'phOM:** (2161161-3114 t


### Mr. David I. 

### Williamson Field Technician ERD Environmental, Inc. 6205 Easton Road Pipersville PA 18947-1025 Dear 

### Mr. Williamson: February 13, 1997 PERU, ILLINOIS 81364 (815) 223-0373



### As per your request, I 

### am submitting to you 

### an enclosed process schematic, and 

### a description ofthe process, as follows: Hexavalent chromium is plated onto continuous coil product in a chrome plating tank, powered by five DC power supplies (rectifiers). Due to rinses, water 

### is accumulated in the bath and 

### is therefore pumped to an evaporator. This 

### will drain back to the plating tank. The plating tank 

### is hooded for ventilation, and this airstream passes through the evaporator. A new demister, downstream ofthe evaporator, 

### will reduce the chromium content within 

### this airstream. There are several pumps doing such things as circulating solution to the plating tank and transfering solution to a storage tank. These pumps have water-cooled mechanical seals, thus, a water coolant tank and water pump exist to handle this need. This tank is what collects the demister's wash-down. Some process data that PADEP requested is listed below. Pressure drop across demister 

## = 1. 6 - 1. 7 in. water column Water flow rate to demister = 

### 5 - 7 gallons per hour Typical plating voltages = 

### 6 - 9 volts on each of5 rectifiers Typical plating currents 

## = 2000
- 3000 amps on each of5 rectifiers Very truly yours,

MORE THAN A METAL IT'S A METHODJ H G F
6



### 5

4

3 

# ---!

2 ___ ..._AMIIe ..


# _ ......

# -

J H. GE D C 8

6



### 5

4

3

2

.... -'-

# ..........

# --

- 

# ---

lMI ...... D ...... a ... DQi ... KIU .....**~** 

# • ".... ... IIIlC "".. 

# ....**~** AIIOlIC:.<H KtCIICI.CID**CO~AHT a:rr~**  ......... lIICIIiIlCIQ. •• COftDAII, IfO • QIJpI lD 'KIU 

# -- ,.-- .... 

# _ .. 

# -**"'&lM!m~",.** ... 

# --**.~CN~'"** 

## I=.:r PRO
... CESS SCHEMATIC**'DtI~** ... 

### ItIIt'_", 

# -- 1I....**HIf.~~CQII·** CUNOaw.?IIXItG,.
... B.S.U'C'!'.:t ... CHROME PLATING

.... lilt IUllldO p;J OQCIII. to! ., "1IIIOCIAtItII • IMDI 

# .....**"",,"QQC'~.** 

### '"' 

# _ ... PL20-07-10 AIIDaID ,... ft. ___ ORP 1-.11-17 0**~a.Gill:IIBII~** 

# -- - E D C 8 A-;



## APPENDIXF BACKGROUND INFORMATION1!!!!!!:;:.._. __ .....__**~**____**~:...;,..0..<:1.~** ••'.; ............**....,-.-~.--.---...:.-** ....... _.0.--._____ •.. -- .


# AMERICAN

AODRESS REPLY TO: EASTERN WORKS

N.'n..,,,..,,. P.rrnIV"'U'" 1808B rll.",.,."., (2151161-3/141 

### EPA Region III Director 

# ..

Air, Radiation, and Toxics Division 841 Chestnut Street Philadelphia. PA 19107 Re: Notification Under Section 63.347 

# -. NICKELOID COMPANY MANUFACTU'lEFlS CF I='Fle.FINISHEO METAI.S


### July 

### 20, 1995 I=IERU, ILLINCIS B'l3B4 (815) 22:3.0:37:3



### The American Nickeloid Company, hereby submits initial notification to the Administrator in accordance with Subpart 

# N: National Emission Standards for Chromium Emissions from Hard and Decorative Chromium Electroplating and Chromium Anodizing Tanks. The American Nickeloid Company owns and operates a source which consists of a decorative chromium electroplating tank. This source is located at 129 Cherry Street. Walnutport, PA 18088. The applicable emission limitation for the source is 

### 0.01 mg/dscm and the compliance date is 

### January 29, 1996. The American Nickeloid Company is 

### considered a major source for hazardous air pollutant emissions because we have the potential to. emit greater than 10 tpy or more of any hazardous air pollutant or 25 tpy or more of any combination of hazardous air pollutants. The American Nickeloid Company has applied for a Synthetic Minor air permit which will limit emissions from the facility to levels below "Major" thresholds. Actual HAP emissions are well below the limmits speciiied above.

EPA (Return Receipt 2355 866 544) cc: PADER Northeast Regional Office 2 Public Square Sincerely.

Plant Manager

Wilkes-Barre. PA lS711·0790 (Return Receipt 2355 866 545) MORE THAN A METAL IT'S A METHOD

# I**~**



# I 

# I I 

# I I 

# I 

# I I 

# I 

# I I 

# I


# ,

- I 

# ·1 -. AMERICAN NICKELOID COMPANY

ADDRESS REPI.Y TO: EASTERN WORKS

We/ftutptJIr. 

### 1'.""...",,,,,. 180811 r.,.pllo".: 12'51161·384'



### Mr. Babu Patel PADER 

# ..

Northeast Regional Office 2 Public Square Wilkes-Barre, PA 18711-0790 

### Re: 40 CFR Parts 9 

### and 63 

### Chromium Emissions Dear Mr. Patel, MANWFACTL.FlEF!S OF PF'lE.FINISHEO METAI.S


### July 24. 

### 1995 PERU. ILLINCIS 81354 (615] 223-037:3



### . The National Emission Standards for Chromium Emissions from Hard and Decorative Chromium Elecn-oplating specifies emissions standards for existing decorative chromium sources of 0.01 

### mg/dscm or 45 

### dynesf.:m for operators using a fume suppressant containing wetting agent 

## as a control technique. Operators must demonstrate compliance no later than one year after January 25, 1995. The American Nickeloid Company currently operates a chromium emission 'source under PADER Permit number 48-318-001. 

### This emission source consists of a decorative chromium electroplating tank 

### and asso:iated pollution control equipment. On January 26, 1995 a series of stack tests was performed to determine chromium emissions from the scrubber system serving the chrome plating line. The test program consisted of duplicate two hour sampling sessions, conducted while the plant was running under normal operating conditions. Chromium emissions during run #1 were measured at 0.0604 mg/dscm. Run #2 produced**~n** 

### emission rate of 0.056 mg/dscm. 

### Test results indicate that the control system does not meet the emissions standards specified in the final rule. American Nickeloid Company is not interested in using a fume suppressant containing a wetting agent due to the proven inherent explosive nature of a foam blanket. We are investigating alternative or additional add-on control techniques, and we do not expect to have a system installed, operational, and tested by January 25, 1996. Therefore, we hereby request a one year extension of compliance in accordance with section 63.343(6) of the final rule. If you have any questions, or need further information, please call me at (610) 767-3841.
MORE THAN A METAL M**IT'~** 6 UC:Turon

# I 

# I I I 

# I 

# I. I 

# I I 

# , , , AMeRICAN NICKEl-otD CQJMPANY



# ..

Certified RR
- 2355 866 548 

# . \



## ..... SHEET NO.


### Sincerely, 

### AMERICAN NICKELOID COMPANY

# ~t!~ Plant Manager

. 

# .

..COMMONWEALnt OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL RESOURces 

### GENERAL SOURCE**~** BUREAU OF AIR aUAUTY CONT:ROL Application for Pfan Approval to Construct. Modify or Reactjvate an Air Contamination Source and/or Air Cleaning Device and fer a Permit to Operata 

### ,**-----------------------------------------------------------------~, ~**  

### Section A Identity and Location ofAir Contamination Source**~ ~**  IA. AopllauCft is beinq made for: OFF1CIAL USE ONLY 0 Consuvcdon 01 New SourcalOperatJng Pennit Application No. __ 

# - 

# - --- 

# --- 0 Relcdvadon at a Sautee/Operating Permit Plant Code Unit 10 Oatil Rllceived 

# . ,**~** Modification ot Exileng SOUIcII/Operating Permit Reviewed By 

### XI Instillation 01 AI, CIIII1iI19 OIvi",Operltlng Permit PocentiaJ Emissions ITPYl 

### 0 Amendment to a Previaus AillcatiOn PM S02 VOC Previou. Application No. j, -]. 

## J.. Jl.
- Q.. Q.. 

### l. NOX CO Other 

### 0 Olhllr Actual emissions ITPYl**~** 

### . Type at sourci PM S02 VOC lB. NOX .CO Other Chrome Plating System Change in Actual-Emiuions 1+ or -to 

### " IC. F1l1nt in which source i. located PM S02 VOC NOX CO Other 

### ::i NEW**~** EXISilNG 

# .. 10. If sourc. is new. does it repllce anoUler source DYES DNO IE. Excectlld date of completion 

### .' 

# . (dll.cnbe soures replecadl 

### 12/15/96



## - lA. Owner of .aures 2B. Employe, 1.0. No. IFederal IRS No.1 

# . , 

### Anerican Nickeloid Co. 

### .1..6..-0..1.2..8..8..1-0- : : 3A. Owner. da.lon-don 01 sourc. andlo, plant if any J8. Location of source Political Subdivision Count'( IStreet address 0' Aouta No.1 

### , ITownsnip. etc.1 129 ""'h@"'TV**~::-t.,..ppt- T~h;nh**  Nort' 

### n 

# II 3C. Mlillng addresl IStreet or P.O. Box. City. ZIp Code'**~ 3~.** **Tef~M** No. 

### 129 Olen:y st., Walnutp:::>rt , PA 

### 18088-1698 (610) 767-3841**~** 4A. Person to COI1UCI tlgaraimJ this Appllc:alio" 48. Mailing address IStree, or P,O. Box. City. State. Zip Code' 4C. Telephona No. Inama and 

## dtII. ' William A. 

### Cline Sane Same 

# II

. , 

# lII_ s._O_H1_cl_'l_S_'G_"_IncJ_'_P_IIl_Ica_d_cn_mus_t_b_e_'"_'V_II_n_'_0_'_th_lI_c_o_m_p_l_nv_h_a_Vi_ng_p_rim_arv_r_es_p_o_n_Si_b_iII_till_S_'O_'_O_PII_,_au_'o_"_o_,_tn_e_"_Cl_'II_ lV _IO_W_hl_ch_th_1_'_'_PP_II_ca-_, tlon ,ppll... Althaugh he may not h,v. plltticipatlld in the dllsiqn of thll 'acilllV he should ba responllible 'or approval of the design!', ;
• AFF1DAVIT**~** I 

## III I 

# Ric

# JIfIR J) 

# 8 · 

# /J Q

### N 

# e , being duly sworn according to law depose and say that I

## am~': the official having primary responsibility for the design and operation of the facilities to which this application applies!**~** .,. 

# II and that the information included in the foregoing application is true to

### th~ est t my knowl ormation and bellBf{

### ~ • Sworn to and subscribed before me this 

# L day '. ;

Notarial seal Walter A, Searlass. Notary Public Nonh Whitehall Twp.• Lehigh County My Commission Expires Dae. 17, 1998 Mentler. PemsyMIr1a Association 01 Notaries ,. , ,'.• " 

## ...**~:** 

### ..**~** / 

### ,,,':-.:

....

### :. , 

# . Tiel. Plant Manager

I,Pege**_~** __ 01**_~** __ 

## Section B



## - 

# --- I. SotmCE 2. NORMAL PROCESS OPERATING SCHEDULE



## - 

# --- D. A.led E.' Type 01 A. Amounl 8. C. D. % ThlupullOuelle, A. TyplI So,,"ca 8. Manuleclu,., C.Modet Clp.dl" M.I.,""**P'~I**••d/yr. A....·all Tol" Unil ,Delcrlbe' 01 SouIce No. 'Sped:" unllll ,'oc.... d ISped." unll., ""d.y hrI" hi 2nd 3.d 4th


# - -- -- --- -- 

# -- - 1 

### Mist Eliminator KOI

### ~tmOtra 5000 CFM

### I~~ii!/Brass 2500 'lbns 

### 12 3000 25 25 25 25


# -- 

# -- ._- 2



# -- --- __ a 

# -- _4 __ 3



# -- ----- --- 

# -- ----- 

# -- 4



# -- . 

# ----**~-** .-- 

### -- 

# -- 5



# -- -- .-- 

## ---



## . . 6



# -- -I- 

## --- 

# .- 7


# -- -- -- B



## -- .-- 

## -" 9


## - 

# -- -- .-' .0 

## --_. -- --- -_.. 3. ESTIMATED FUel USAGE ,Spec'" Un'll' , 4. ANNUAL FUEL USAGE A. C. A...'ege D. M••1rnum**~** B. C. D. % Th.upullOulI.te, lIed Hourly Hourly E. 'e'cenl F. Percenl G. Hlletlna A. Annual A ..... glI Tote' In B. Type Fuel 

# A.,. 

# n.,. Sulfur Ash Value Amounl. h,/d.y hlly, lsi 2nd 3.d 41h tlnlt 

## . .- 

# -- -- Extreme .oJA 

### Electric IDW Same 

# - - - - 

# - 25 25 25 25



# -- 

# --

-- 

# -- -- --



# - --

---

, 

## -**~"TAHT.** 

# 1.\, Attach now cI..,.m 01**~**..gMng .. I,a_. lIQuId. and .aIIef'lIow rat•• lettach "pet.. a ..... ,. ltJlO ... f
..... m.le,''', ch.. ged to ptOC1tI' equlpnMn' and tt.a _'I dlarVed ftonstt-. elc.' al , ..811**~y** ,give _lmum, mWmurn and .".,.,. dlargll. d•• c:rIbIno luIIy**.~c1.d** vatlallon, In ptOductfun fll•• I. IndIc.t. ,on dllgram' .11 poIntl where conllmlnmls ar. cont,onlld (Iocallon d ..... t., apt'Y'. hoodt Of other pickup pain" ••

lc.l.**.~.-. '-~--"."-'"**  ........ - .. .



# I

# -r-"",.: "w_ 3'.8 

### Section B Source Information Continued 

# I I 

# I I 

# I I I 

# I I 

# I I I 

# I a. Oescnbt fully tl1e faCIlities provided to monlCor and record all operating conditions tnat may attect tne emission of air**~anuminams.** Provide detailed information to show tnac: the facilities provided are adequate. . 

### Temperature controls, .manometer will l::::e 

### recorded. Fans and 

### pump speed and 

### VOlUlleS 

### are sized correctly.

7. O_crib. modlftcationl to praclss equipment in dltail. 

### We are installing 

### an additional mist eliminator to 

### the present 

### system.

S. Tvpe and method of dlspo.. ' of all waste materials gunlrlled by this prOCISS. 

### Process is closed loop and 

### no, waste is 

### generated.

Is. Solid Weste O'-PoNl Permit Neededl 

### Dves m:I No 9. Btfefly describe the method ot handling thl wate wlter from this proclss and Its associated air pollution a2ntrol equipmenc. ." .'



## , Process puts 

### diluted waste water back 

### into process and 

### .evaporation peJ:mits pmcess to 

### stay within process 

### limits.

Is t Wlter QUlnty Management Permit Neadedl aVes QD No 10. Attach any and .11 .ddftlonal information necessary to adequlltely describe the proce.. equipment and to perlorm I thorough lVatuaaan ot thl ut.nt Ind n.rur. of iu Imlulon.._.

# v~

# .., ".v. 

# "'B. Section C Control Equipment 1. POTeNTIAL PROCJ;SS EMISSIONS (OUTLET FROM PROCESS. BEFORE ANY CONTROL EQUIPMENn ' ____ s_ee __

## p_e_~ __ 

### ·_t

__

## #4_8_-~3-18---0-0-1-- __ --------------------------------__________________ __ A. OUe/11t paniculatl leading IIbSlhr or grlSCF Dryl 

# , .. 

# 1

_____ a_.__ S_pe

__

d_fl_C __**gr_a_~_·~** __**o_'_p_~** __

·cu_'_a_tl __

ln_o_t_b_U_'k __**de_n_s_I~** __

I ____________________________________________________**~**________ __ C. Anact1 outlat partJcte size distribution intormation 

# , ,
2.



## 3: O. SpecifY gas.oua ccntaminlnu and caneenuation Cone,nrration 11' SO. (2) NO. ppm IVol.1 ppm IVol.1 ___ Ibs/hr

___ lbSlhr (31 CO ppm IVaI.) Ibs/hr GAS CONDITIONER (IF APPUCABLEI 

### N/A A. Wlter quenching DYes DNa Water injection ratl ____________ GPM 

### a. Radiation and convection cooling 

# o YIS 

# a No C. Air dilution 

## a Yes 

# a No CFM O. Gas condldoner aue/ae ACFMfJ SETTUNG CHAM8ERS IIF APPlICABLE! 

### N/A A. ManufactUrer
B. Volume 01 g .. handled ACfM, QF O. Leng1h of e"p.".ion chamber 1ft) F. Height of explnsion chlmber (ttl H. Inlae concentration . I. Outler concena-ation IIbslhr or grlSCF Oryl tlblJhr or grlSCF Oryl voe 141 (51 (81

K. Water injactIon L Water injection rate IGPMl 

### Dves DNa CDntaminants Cane,nrratiQn

____ ppm IVol.1 ___ Ibslhr

__ --"'pm IVol.1 Ibslhr

ppm IVol.1 IbsIhr

C. Gas velocity E. Width ot expansion chamber Iftl 

### , G. Number ct crays J. Overall etticiency 1%1 

# I M. Anaeh panicle size Ernclenc:y cut\le

# 1~-I.' Rw. l/ •• 

## Section C 

## Control Equipment, Continued 7. PARTICULATE MAmA SCRUBBERS IIF.APPUCABLEI N/A A. Manufacturer B. Tyge 

# I C. Model No. D. Presaure drop Iweter gagel across scrubber only. 00 not inclUde duct or demlster loues. E. GGS temperarures IoF) at inlat outlet ___________ _ F. Volume of gasea handlad at inlat Ismgera""ra IACFMI G. Design inlat volume IACFM,
H. Water flow rata IGFMI I. Relative partiCUlatefgas velocity lejector scrubbersl

J. Inlet conc:antretionJRate UbI/hr. or ;r/SCr- Dry) K. Outlet concentration/Rate Ubs/hr. or grlSCF Dryl

N. .Describe equipmant provided to measure prassure drop and water /low fate to scrubber.L Overall efficiency 1%1

O. Oescribe ICNbber weter supgly system ramoUnt of maka-ug and recirculating water. capacity ot recirculeting watar sysum ••

tCo'
P. aascrib. milt eliminator or saparator (configuration. backtlush. capability. frequency).


### a. pH monitoring and adjustment 1 Desenbe it yes. DYes 

# a No

# ./ s. 

# , I I 

# I I 

# I I 

# I I I 

# I I I 

# , Section C 

## Control Equipment, Continued ELECTROSTATIC. ?RECIPITATOR IIF A?PUCASLEI 

### N/A A. Manu'8C1Urer 

# 'j B. MOdel No.

#> D. Preasure droQ Iwacer gagal Aero .. collector only F. Maximum oQ""ling temperature I oF) Actual oQer,tlnq tempereture I oF) H. Oust resistively lohm/ernl J. Tow collec:UncJ surilce area SQ. ft. 

# IC. 0 Wet 

## o 5ingl.Stage 

## o Dry 

# a Multi-Stage 

# I e. Oesign inlet VOlume (ACFMI Ac:rual volume handled IACJ=MI _________ _ G. Maximum Oust InIaC Concantrlcion Igr/DSCFl _____ _ Mum/mum Ouse Outlet Conceneralion Igr/DSCFl ___ _ I. Gas Distribution Grids 

# a Yes 

# a No Collector plat.. size lenQlh ft. lC width ____ ft. Numb., of field. number of collector placeS/field SPicing between collector plates ________ inches Maximum gas velocity ________ /Usee Minimum gas lIeaunent cime sec. K. Total discharge eleccrode length ________ ft Number of discharge electrodes _______ _ L Number and Size of Transformer Rectifier Sets By Electrical Field No. 411 E.dI Rtlctifitl' ITMI NG.**~** KV A""IPrttlk**~**

M. Cunwnt denlicy N. Coronl power

______ Micro ampereSlft. 1 _______ Wansl1000 ACFM O. Cotona power densicy

______ WlnSlft. J P. Number ccllllding .Iectrode rappers ________ _ MInImum accelemon rating 'or riPpers ______ g's



### a. Flue gas conditioning equipment usedl Describe Iff Yesl 

# o Ves 

## o NoPage 

## --1... of.-:2.:.. 

## Se,ction C Control Equipment, Continued 12. COSTS A. Cast ot all canuel eQuipment Including installation cesu lust individual controls seQaratelyl


# .. $20,000 for 

### equipment. $5,000 for controls. 9. E:slimated annual operating casu of control equipment only. Unkncwn - expected 

### to be 

### minimal. 1 J. Describe modlflcauans to concrol equipment in detail. Add 

### on of danister. 14. Oescnbe in datail rhe method at dust removal Irom the air cleaning and methods of controlling fugitive emIssions Iram dust removal. handling and disposal. 

### N/A

1S. Does air cleaning deYice emplov hopper heatersl hopper vibrators or hopper leyel detlctors1 If so desctlbe.

16. Anach manutaCNl1lr's performanea guarantees ancUor warranties tor each of thl major components of the control svstem lor complet. systeml. 

### 99.96% See 

### brochure attached.
I7. Anach the mainten.nc. schedule for the control equipment .1nd anv part of the process equipment that if in disrepair would Inere... "'. air contaminant emissions. PeriOdIc maintenanca repom ara to be submitted to the Department. 

### N/A

, B. Attach any and .11 .1dclluanal information necessary to thoroughly evaluate the control equipment.**P'ge-Lot~**

# r-I~'."'JJ

# .. Section D Flue and Air Contaminant Emission Information 1. STACK ANO exHAUSTER 

### See Permit**#48-318-00~** A. Exhauster laRach fan curves, _____ in w.g. ______ HP @ _____ RPM B. Stadt height above grade Iftl Gr.do elev.lion Iftl C. Slack diameter I ftl or Outlet duct area ISQ. ft.1 • O. We.",er Cap Ols«arlce from discharge to nearest CJrQCMn'V line Ift.1 

### Cl Yes 

# a No E. 'ndlClllce on an attached sheet the location of sampljng POrts with respoet (0 exnaust tans, creecning. etc. Give all n.c:auary dimensions.

F. Can the contral equipment be bypassed 1 lit Yas. allplainl 

## o Ves

2. A TM05PHERIC EMISSIONS A. Panicula'e !NIner emlss/ans IIbSlhr ar grlSCF Dryl 

### Expect to be 

### un:Ier 

### for Chranium of .000012 gr/S01 

### day S. Gaseous conamln.nc emissions Conctmrnlflon IU 50. ppm IVal.1 121 NO. ppm IVai. I 13' CO ppm IVal.1 C. 

### Owe' volum. of exhaust gases 

### 4100 CFM· 

# ,**lQQ-l~!l** OF 3 6**~** Maisture ___ Ibs/hr

___ lbSlhr

___ lbSlhr voe 141 151 161 

### IlD No

Concl1ntnrritm

__ --"Dam IVol.1 __ -,lbslhr

__ --"Clam IVai. I Ib8lhr

ClPf11 IVal.1 IlWhr**-~--** ..**~---** 

# --_._----------_._--_._._- - .•.

## - ........

### - 

## _ ..__._ -0_---------**~** 

## ----...**~-** 

# I

# ~;~, Rn.31•• Page 

## ..L 01 

## --1.. Miscellaneous Information 

# , t Section E 1. Oescnbe fUlly lacllities to monitor and record the emission of air contaminants. Provide detaded**informa~on** to snow that the facilities provided ani adeQuate. Include cost and maintenance informanon. Periodic maintenance repons are to be suCmltted to the.Oepartment. ' 

## o o Opacity monitor 

### so. monitor NONE 

## o Other _____ _ 'f checked provide mlll11.lfacwrer name. modal no. and penlnent technical sOllclficatlOns.

2. Attach Air Pollution Epgcde Stllnegy lif applicablel 

### pressure differential will l::e 

### :recorded. If too great a change of pressure differential 

### occurs, 

### we will shut the line down 

### and 

### detennine the cause. 3. The following raQVitemenca are applicable only to c:onsuuclion only to c:onsuuction of a new source. a. Briefly describe the nnure of melnta in whiCh the proposed source Is located. Attach a copy of the apPlOptiateponion of Ut. quadranvle map C7%' scalel published by the U.S. Geological Su,..,ey and identify the location 01 proposed source. 

### N/A

b. Oemonstrate that the estabnshment of the new source is justifiable as a result 01 necessary economic: or social developmenL

4. If the sourc. is subiect to Section' 27.63 Ispecial permit requirementsl a. Oemonstrate the availability at emission offset iii applicablel 

### N/A b. Provide an analysis at alternate sites. sizes. production processes and environmental control techniques demonsttatinv that ttle benefits of the proposed source outweigh the environmenral and social costs.

S. Actacl1 calculetions and any additional information necessary to thoroughly evaluata compliance with ail the applicable requiremenca 01 Arode III**~f** the Nles and,regulatlons of the ,Oepanment of Environmental Resources and those requirements promulgated by the Administrator 01 the United States EnVironmental Protection Agency DUlsuant to thlt provisions 01 the Clean Air Act. See attached brochure.
6. List ail attac:tlments made to this Application. 'I\-.u 

### pages on Spectra Series Mi ,0::1- "'1 im; ...**~** ..---ua,-- L a-ss 14.GB FROH. 

# " ID.SI07S?S070 PACE 2/3**~,.,** 

## ... ollur**It-~** mrclf' 

# SPECTRA SERIES
SIGt. 

# CHEMICJ\L MIST
tr lIME I
SIIICt I 

# ELIMINATOR

• fUIIIQ ...cr**~-** II p,P. SIIa' III2US _ID1IaIB 1111 'GL1t (TIP.) 

# .,....- II.**~IUICID** 

# L**'~~-------I-------~** L • CIII:IaJ am. ..SIll =,**==-~====I~!=::====:::::::::!:II!** 

### .....---:,r'------t FRONT VIEW I , F

P.O. BOX 1287 FOREST CITY, NO 28043 704-246-9836 FI\X NO. 704-245-1437 SIO£ VIEW I

P.O. BOX 67 HOWE. INDIANA "6746 219-Q62-3737 FAX NO. 219-562-3846 P.O. BOX 266 MART. TEXAS 76664 817-876-3060 FI\X NO. 81747&-3071 

# PVC 

# • POLY·PRO 

# • FRP 

# HOODS ---DUCT---SCRUBBERS---FANS

# ~**~** Approved

# .~DEC-lS-SS 15.00 FROM. 10·6107676070 PAGE :3/' 

# CHEMICAL MIST ELIMINATOR

..' SERIES

• eliminates discharge of 

### expensive chrome to your 

### waste treatment • complies with 

### state hexavalent chromium requirements todayand 

### the federal hexavalent chromium standards oftomorrow • ultra 

### high 

## efficiencies - up to 

### 99.96% 

## • solves the -Waterproblem· 

## so often 

## encounteredbychrome platers in using conventional control devices

The 

# IfJ<crr Spectra Series Chemical Mist ElIminators consist of units ranging in size and capacity including 

### the Spectra-I through the 

### Spectra-v and the ultra efflcfent Spectra-U which 

### is most useful on Chromic Acid Fumes. These units are designed for installation in 

### horizontal runs of duct. 

### Contaminant removal takes place when the fumes pass through the two cfdferent types of media.. The first stage 

### is used to entrap the heavier droplets. The second type of media Is carefully designed to 

### entrap the remaining 

### micron sil:e particles with 

### ultra high 

### efficiencies. 

### Each stage is also 

### equipped 

### With 

### a wash down 

### chamber for periodfc cleaning. The drain, in some cases, can be 

### run back to the source to reduce cost of adding chemicals. 

### -KCH" also offers control panels for static**pressu~** 

### monitOrir9 

### and/or completely automated wash 

### down 

### systems. 

# PVC eo 

# POLY·PRO • FRP CONSTRUCTION

## ,.

HElL



# . . Root

Floor

# M37458 WALNVTPORT . ·PLATING LINE·· ·'OBROJlE. DEKIST.ER PAD •. POLrPROPYLENB •

. ··CR HElL .', 

# 9 6 - 0 1 0 0 0 9 W·ITBH 01 GXC . WLT'078 00261 REQU·IS.ITIONERDR.P. . '.
46"' DI.l 

### X "**'''~**

### ' .. 09.1.30/1996CO......O_EA&.'I'W OF PIt"N.y.. V .... NI .. DC""RTNENT 010 IUfVINONMCHTAL rnrSOURC:W::;
, IUAJEAU 0" AIR QUAUTT a "0'115 I;O"TIlOI.


# .. APPLICATION FOR PLAN APPROVAL TO CONSTRUCT. MODIFY OR REACTIVATE AN AIR CONTAMINATioN SOURCe ANO/OA AIR CLEANING DEVICE OR FOR A PERMIT TO OPERATE**/lJwI'lh~** 'UatructilJftS etuefblJy**~o""** toltfP"dng rhb form. Submit dup/lcrue copiu. Section .A -'**Id~n/ilY** t1Jzd L<Jcation of Air Contamf1l4llon SoII1'f:e lA.. ApplicatiCIJI. ia lIc:ina lllade for: Cl COIISIt1ICIIaa ot Hew S«a1Cll 

### o RoacdYadoQ ot • $Ga_ O**,~doo** ot**~tblS** Source 

### m r..Datica of Air OooInmC De-rb 18. TyPO of scuzce 

# . \: 

### Chrome Pta.tiDg Tank. ·0 Hew 

### ... 

## o E...... oC P1m Approql A'**~** ,to • .Pzariaus ApplbdcD



## . a E:Il1m8cIa of 

### rw. Apprvral CJ Opaatiq**f~** [J XmaskIQ ot Opendug hmUt

ID.**~ed** date of agllqliedOll : . Scptc::mbe:r:, 197-4 IE. l(**~** is 1I.n'. docs 11**J~** anodlct**s~** (de:Iaibo lICIlJRC**~)** 

### Clirome pta ting 

### T8#k " American Nickeloid COm"PaJJY 

### :Ie. Name of COlDpaIS' oUlclal sfIDIAI applJc:adOD ($eo iuUucdaaa) . Ceorge, Maze 

# . . 

# . 2JL Emplr:lrcr LD. No. <FedaIQ 36.. 0728810 .' 

## .

I·" •• 

### . '. 

# .**~** ,**~** 

## .

. 

### ,



# ..
'. West Main Street Peru 

## nlinoia . 61354 .' 

## ... . ., 815--223-0373 .. 3A.. 0WDas**~II** 01 $CIIIlOO ud/or plaDt U ., ;' Chrome 'Tank
-- Wa.lnutport Plant 38. Loc:l1So1I o( soalal (Street 

### =cizas 01 RoaaD No.) Cher1'"1 & Oak· Street s 3C**~falUDS** ad1lml. it dlrra.c (rom 2G- (Stnec or 

### P.o. Box. aty, Zip Code) Cherry & Oak Streets Walnutoort a. 18088 4A. PeJ:101l IG __ I**I~** th1I AP9'kadoa.**(~me :m~**  dUo) OtT or Malli;ipal1ty



### . Walnutport

Colin MacCrindle
-- Assistant 

### Factory Manager 48. MailinI adtbas (Sblect or 

### r.o. JJQ. OC7, StIISc. Zip Coclo) if .unl:ICIU (ZVIft 2e. Cherry & Oak Streets
-- Walnutport, Pa. t8088 3D. ToJapll911G . , -:.' 

### .. ,

. 215--767-3841

. 4C.**To~pllcac**

215-7&7-3841' 5. NUIO
_**~** ot ,.. 'MIlo is to naUN !'Ia**A~ a1I~**  O,..mal Permit U cIiffcmIt (rom .20. Colin Mac:Crindle r.h4llrrv 1" Oak Streets WAtnnt-nn,." 'D_.......I ....**-~-** tonoo 

# .. -

, "

' 

# ..

" '.



## ., :. ".**~** s.ction B - JnJce:a [nf()nnJJ.tion

, 'co $ 1. PROCESS EQUInWrr' B. Model No •**.A~eriean** Nic:keloid CO. 

### N/A N/A F. Dc!:SCDbe the pt'OCIIS**~pmw** (tim**~** 11$1.. PtQd!Ict. eu:.**~ ~**  $beet)**Ch~CJme** Plating Tank for metal stl"i-p

'.

2. Ol'ERA'IJNG SCBEDUU variable' blJart/d!q 3. SEASONAL**~ODS** (K0N'l'BS)

, 'Opsatfas 

### . 

# .**------------~-----. --------------~­**  . 

# .

.N/A __**~S()** ...

• ___ .."..
" 

## .... '**~** 

### .**lf~**



# ------------------- 

# ----------------

7. llJtefly**~** tM medlod 01 1uaIdDn, tIIG**~** -.tcr trom this ptOCUI &ncl its &SaJCiatoll ail poUDdoa GQDaW**~'I** (Is • Watn Q\aalit)'**~t** PftIItit needed? 

### a, - Yes 0 No} .A 11 

### waste water,is ;**~ecycled**

. 01' 

### trellted by**a.pprove~ '~a'ij.ng:**  

### ,

c:b.etnical de,struction. :: 8. AltlCft 211)' aad aD UcIt1IOlIai intonDtioll na:essary to patonn a thDn::up**~D** or lbc**~** 

# all' mlUrO 

### Oi .'1 icea fiom N/A<Z\ 2 

## a:

Section B
- Procus III/ormation. Continued



## ... ..' 

### 9. FUEL AND PQWER 

### REQUIREMENTS 

## . . . 

## '. ., " .,

••• 0 

## . QUANTITY :ANNUALLY TYPE 'SULFUR I- . 

### HOURLY



## . 

# . . ·OPH· Oil No. 

### N/A @ 6O·P 

### N/.A 

### x 10'**~** 

## .. NJA % bY.Wl. , 

## .

. . . 

# . sr/100 Natural Gu SCPH 

### xiO'scp , 

### N/A 

# . SCF : .. I , 

### . 

# . .



## . 

# . .. 08& 

## scm**~lJo!** 

### SCF 

### .p/JPD**(O~r)** 

## N/A . :**~** 

### SCF . 

# - 

# .. . . 

# - "


# . .. 

## • 

# .. .. 

# . .' 

### CoaJ 

## N/A TPH toOl : 

## .. "**b~ ~I.**  

### . ,
. 

### . 

# .. CQke 

### TPH TOlU**~** by 

### wt. 

## N/A

,

, Other 

## .. .

# - .•' 

## . .' 

## .- lilootrtc: Pown 

### extromoly ICWA 

### oxtromoly 

### KWH 

# --- variable 

### variable &

" 

### .. .• ASH : 

### £WEIGHT) 

## N/A

.'



## .

. . . ,



# .

.



# - . ..

' 

### . . . BTU 

### CONTENT
'" 

### ,. . Bro/sal .. 

## N/A ."**Jb~8aJ.** @60 F



# . .., BTU/SCF
BTUJSCF

BTU/lb.
.BTU/lb.



# -- .. o 

## . OJ 

# .. &**~** OJ <oJ OJ &**~** 151

(J] 

# , 

# .. tl o**~:** n I II) "I,) I OJ III



# .. OJ '11 ;U o :r

# I

t t Section C
-**~nl1'Ol** Equipment I. rotEtmAL pR.()CDS**EM~IONS** (OUJ'LET FROM**PR~.** BERlRE ANY CONI1l0L EQUIPNENl) A.. Outlet p.2tliasbte loadins abflhr Of rtlSCF OIT),. obtain**da.~** 

### frOlXl control eq\lipment 

### mallufaeturer'a warranty B. Spociiu: &Drily of**~(O** 

### approximately 1. Z5

(1) ____ ...

PPtn {VOl.) 

### _lbatllr

____ ....sPPIQ (VoL) _11II/lJI _________________ NCf.M (1) (3) ____**~ptJDl** (VolJ 

### .--:,..lbJIbt

" 

## o 'Yes • C Ho

## ----------------~QPW 

## o. Y. '0 No 

## o Ya 

### C Ho

_________**A~'** 

## e ______------.-'**_~F** 

### " .



## . '

• 0". .". 

### AO'M @l ,**~F** 

# --------------- 

# ---------------- D. 

### a .......i.ions

G.**IMIt~D** (1btIla- or p/9CP Dry)
J.**W._~** 

## a Yet 0 No " 

### e**~F**


# -----------------**..~.:-** 

# . . ,



### , 

## . '

# .

, ' " " ,. ,

# \ Section 

### C - Control Equipment. Conrlnuf!d 7. SCRUBBERS (IF MPUCAaU)

£.. Gas zempeqt111'CS (.F ) at inlet ambient f. Vobmc of pICS hllldled at ioIet b:nrpc;raQn (AarJd) "
...



# . •

" Co Mo6e1 No. 

## N.A.
Zit

wllet**tmkno~** at present
4000 6000 '. 50 X. OcUli, CU••PI,AIml .,.., • I;fISC1t Dq) 

### .0000131 gr'SCi'

(tma.ranti!**e~ ~~~~nnal1~**  e) 

### not avaite.bte
I •• 0"

•! •


# . ' : ' 

# ...

. . '.



## '. . 

# . "

• I. ' 

## .

. . . ' 

## .. 

# ., ...• .'

'

## . ... 

## . ,

• ". "0 •



### . 

### .

# ... , : '



## .,
"
0° ,° 0 • '0° • " . " ' , 

## .**~,** ".

:-.



### .

# ,

# .. $t:'C'tion C - (Antrol Eqllipmmt, Ccnlinlleci 11. COSTS

.' 

### . '. ,

'.. -\ .' 

### . " 

### ..•. . 

# . " ,


# . . "

.' 

## . .'

, new"iusta.Uaticm

, 

# . " ;. :. .' 

## . .**~**

## .. • " " 13. DIs=sI**~r** UJo**~_** POhSJdal 01 !.he ,RKlIW ... alatal cntn:li**~** aM.**~ ~**  cbIYkea .... to ........ Giro COI:tI, .' .'. , , • • ", No deciDel figures' a.re' a.vailable a.t -pr'eaeIL'C t1.1ne, but we haTe be.. informed that the equltnnent:camtJl1es 

### 'with.**~e** Wa.lsh-Healy Act. 'We ccm.1.der hbise tJotentia.llnin;maL ': .. 

## :1': ' ' , " , . . , ,1 " , , , 

# ., " "**--~~------~--~--~--------------~--------~~~~~~~----------~~--~--------~----** 14. Anxll an:anurac:aam's**~CIIaDCO** puutMa 'UldJor 1PU1WdWS COl' tela of UN·,..r CIOIIftl'OlICIIU 01 • ccetroL qIlaD (01 _plete**~.** ' . ' , , , , , , 

# .. IS. AltKh tho tuiataaDce .choduk for lho caurol equi,.-l :aD4 any puc of tba**~ ~.**  lba, If In**~** ..w iDcte::ac tile air**~t** cniId.cnd. hdadic**~** IqIOrts am to be submitted CO Ul. DepaztIDtAt.' Periodic inspectioDs 

## win be made. Frequency will be

### de'PeAden~**uP~ezp.riec~e** but'; s est:i:mated to be r-equired no more often than yearly.



### , " "" Sedlo/l "D

### Flu~ 

### And Air Contaminant Emission 

### In/OrmtJ1iolt. 1. STACK AND £XJIAUSTEI\

A.**~cr** (allKb**(~** CUI\'CS)
___**l:.::O~_HP** 

## e "

I t, Stu:Jc heicht (nJ 

### 5' 

### L 6 It. C, Y. ' , CJ, He Eo ln4iclt. on an .ttKho4 shiel ._ 10000tkm of saElllnl portS with**~** to**~** 1Ua.**~** O\D. On..n DCCIfSIIJy dimensions. 

### N/A

:

" .,0° 1, ATMOSntD.IC DIISSIONS 

# ... ': 

# '.
a'Ya

'.. • - "0 •• 

### •.• ,'I " ' , 

# -

• ; • :.0 • I 

### ...**~**

, 

## .. I!l No

,.0000131 (r/SCr L Gaeaa:s .-al" ' ot tqdIIIoIII " , ' , 

# . " "

,**"~** 

## .. .. ...

__ -=:-_.. 

### ',p. (Val)**_~1bfIIIr** :: (I) (2) (3) _____ l'PPS, '(Vol) 

### 'DIIIiu**~** 

### , 

## .**.~**

____ ..... <VoLl**~!**



# ____.....-----------------------CFM**~-----------------** .p

_________________________ " Mol.lutl , 

# ..

. I •

, 

# '.
.: 

## ,. '"

., ,. , '



# ,.

, "

"0: .


### . 

## ."**~** . , , 

## .

"
, ' "

"

..' ':

, "

# I

" 

### ... Seerioll E -**JltI.1c~lIall(POllS** 

### 1n/rmnallon " 1. [)c:S.(ribo fuJI, (xilities to "!",,iI01' gqd teeGrd lho cmiItIIoq of**~Ir ~OI\Qminaa.,.** **P~dc'** c1C1Ui1cd Inrormadoll 10 

### mow &hat UIa .

r.:tc:iitics pRJTfttcd**.~re ~ualC.**  hu::!uclc COlt aDd**~tcn:ance** infonnztion. Periodic lD:lIiftteft:ll:lcv reports aN 10 be _1:ImJtt04 to the DepanlnCllc. . ...'

.. "::. 

# '.

. , '.' ",

.' , 2. Attach Air PoIbnIoa Episode Sasll!g (If _pplieallle)

, \. 

## . ".'**.····~IA** 

### , i lJdeJlY ck:Icrib: tbe 'pmraI**1Ia~1t** or the aa iD**~** the**~** Is**Ioc:a~** , , .':

### ~ '. "Edge of smalt xural

### c~UDity.

: r •



### .'.

" "

Flow diagram of "pJ.'ocess MazlufactuJ.'e+'**~** w,a.rranty , 

### .



# .. . ' to' .. '. "
• 0'. .'



### -p.9 :p.10 

## . 

# . ..**~,** 

## . " '.

\ 

## . .' " '.



# .



# ... . " 

## .' 

# ., :-, ," "

## .



# . :-'.

.'



### . ," . 

# . , 

## .

", .": 

### . 

# .. 

# .. Ii \

## •

, 

# . '0 _ •• I ..... 0', ...... ·0

"

## ~"£.TAl--iTR'P

## (~f4'J' 'Dept.J, 

## "f'"**~""'l'** 

### • ",,;JCiJ J 

## <te.) 

# - "**~** ,

;



# .; 

# . : , " : 

## ,



# . .

t



## .. " 0 

## .. '.

" # " 

## .**~** 

## . 

# . "



# . , : , 

### :.

"

1- "



# - , , '\

, 

# . .

'. "



# . , [
, 

# .

.

... c



# " )) n 111



# .. f.) 

# , .. u

# I 

# I I I
I 

## \

:- 11901 SMWOOD AYINUE • CUYIlAND. OHIO +4111 •**~** Aaa CoR 216 -**U2-&1~1'** AYON ORlCI 216427-6011**~2t'l'"** 

### .nane 3. 1974 

## .... a'ftlez:ic:an Nickeloid 

### eoinpany peru. Ill.1D.ois ,61.354 

### attention;**~.** 

### George Maze , " 

### ':1\efel:enoe:**~ur** 

### P.O. H 12419 

### Reil S.O. 11331 " \ • '. '0 •• 

## . ' 

### .'. , t.Dear 'Hr.**~ze#** 

# . ' 

### ..... " 

## . 

# . " 

# . ' "0' • "

o • • • .., • • , '.

## '?w:S~Dt to oux

## phone:"co.rrve.r~DtiC;;~s**,~n'** -t::be above subjec:t. 

### arid 

### • .AtmoSpber:i.Q**~aporatiye,** 

### coole; b.... d on, 

### perfoz:manc:.**test.iD~."**..



### . ·we guanutee 

### an ail:' 4iscbal:ge**p.~foD1ance** 

### :to 

### meat ,or ezcee4 -:t:.be :!011Ow!nQ1 .' -, • '. .,,' '. ,'.. "


### , ,**~ome** 

### as' C2 

### 1es8 than .02' 

### mg/C!ubia 

## me1:er '

, 

# . . - '



### .**~s** 

### level happens to bit 

### the O'.S.H.A. .T.L.V. 

### level. lOI: 

### plant: -.UJ: . :foz 

### 'oantin11OUS 9 bour exposure., ';,
•• • '0 • • 

### ,X 

## ,.t:rG.st t:be

### ~e iDformatiou.' praves

### :help~u1. ShoulCl 

# You lurIr;'**,~,questions. pl.a.~** **~e.l ~%ee**  

### t:o**~taC!e** 

### the 

### vri.taz. We J:'8!Da'\D,



## . ',,-:, 

### . 

# f

• 

# .- 

# - '.' 

# . . :', v.e£Y'**t:u~l"** YOm's. , " " 

## . ' 

## .. , , ' 

## ':',**~'JiaxL** 'PDCaBSS JiQOLPMD'Z**~RP,,"** ,

# <.~. 

# :; ..**~~ /cL~···:···**  '. - 'rOm' 

### Kol' •• ar. product, KeDIICJez
.**w.8te·~reatma.nt Depar~~**  

# ., , 

# . "

,

# . , 

# .

.... 

# , '

# .. , 

# . "

.' , .It j -s • ·4

t,**~** i ''f :; 

# ," 

# ..**~** \ 

# ,-

,

# . · 

# .. · "

# ·

, "

" 'j• .J 

# ...'.**~**

\ 

# .. " " Ii II \:l , OJ 

# · , :

. ': i

, .\ "**~**

" 

## .' .:,

.'



# . , 

### I:

,

# . ". 

# ·

, 

# . .'

" ,

,;

, "