Su -- Native Conc. Of analyte

Sample No Date Method Filename Hcl (ppm) SF6 (ppm)

1 3/17/2010 321 C:\CalcmetSample 0.00 0.63

2 3/17/2010 321 C:\CalcmetSample 0.00 0.593 3/17/2010 321 C:\CalcmetSample 0.19 04 3/17/2010 321 C:\CalcmetSample 2.45 0.475 3/17/2010 321 C:\CalcmetSample 2.51 0.496 3/17/2010 321 C:\CalcmetSample 2.36 0.477 3/17/2010 321 C:\CalcmetSample 2.45 0.478 3/17/2010 321 C:\CalcmetSample 2.51 0.499 3/17/2010 321 C:\CalcmetSample 2.36 0.47

10 3/17/2010 321 C:\CalcmetSample 2.49 0.4511 3/17/2010 321 C:\CalcmetSample 2.50 0.4612 3/17/2010 321 C:\CalcmetSample 2.53 0.45

Avg. Conc. (ppm) 0.453 1.86

Sm --Spiked Data

Sample No Date Method Filename Hcl (ppm) SF6 (ppm) Calculated d d2

1 3/17/2010 321 C:\CalcmetSample 10.78 0.63 7.85 2.93 8.59

2 3/17/2010 321 C:\CalcmetSample 14.33 0.59 7.85 6.48 42.003 3/17/2010 321 C:\CalcmetSample 11.72 0 8.03 3.69 13.624 3/17/2010 321 C:\CalcmetSample 13.09 1.34 10.18 2.91 8.495 3/17/2010 321 C:\CalcmetSample 12.87 1.37 10.23 2.64 6.956 3/17/2010 321 C:\CalcmetSample 14.14 1.47 10.09 4.05 16.407 3/17/2010 321 C:\CalcmetSample 7.90 0.88 10.18 (2.28) 5.18

8 3/17/2010 321 C:\CalcmetSample 6.49 0.87 10.23 (3.74) 14.019 3/17/2010 321 C:\CalcmetSample 8.09 0.85 10.09 (2.00) 4.00

10 3/17/2010 321 C:\CalcmetSample 10.27 0.5 10.21 0.06 0.00

11 3/17/2010 321 C:\CalcmetSample 10.98 1.47 10.22 0.76 0.5712 3/17/2010 321 C:\CalcmetSample 12.23 1.49 10.25 1.98 3.91

Avg. Conc. (ppm) 0.955 11.07 9.62 1.46 10.31

Sm ppm Mean concentration of spiked analyte 11.07

Su ppm Native concentration of analyte 1.86

DF 5.0% % Dilution Factor (Target < 10%)

Cs ppm Cylinder value of spiked gas 156.0

 ppm Cylinder value of tracer gas (SF6) 9.97

CS 9.62 ppm Expected concentration of analyte DF x Cs + Su(1-DF)

B Bias at spike level Sm -CS 1.46

SD EQ 301-2 Standard deviation of the calcualted spike values to actual spike values 0.97

SDM EQ 301-3 Standard deviation of the mean 0.2795

ts 5.21 EQ 301-4 Calculated t-statistic 

t 2.201 Critical value two-sided t-distribution at the 95% conf. level at 11 deg. of freedom

Bias is significant

CF 0.87 EQ 301-5 Correction Factor must be between 0.7 to 1.3

Data is acceptable

Recovery (%) 118.5% 70 - 130 %

Sm - Su(1-DF)

Recovery (%) = DF x Cs

VALIDATION RUN
Date Time SpectrumFile Water vapoUnit Compensa Residual Hydrogen c

3/17/2010 10:34:16 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0005 0 3/17/2010 10:34:22 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0006 0 3/17/2010 10:34:28 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0009 0 3/17/2010 10:34:34 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0007 0.1 

Averages 0 0.025 
Date Time SpectrumFile Water vapor H2O Unit Compensa Residual Hydrogen 

3/17/2010 13:41:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00005.SPE 2.59 vol-% wet 0.0028 3/17/2010 13:41:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00006.SPE 0.85 vol-% wet 0.0005 3/17/2010 13:41:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00007.SPE 0.39 vol-% wet 0.0003 3/17/2010 13:41:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00008.SPE 0.15 vol-% wet 0.0004 3/17/2010 13:41:49 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00009.SPE 0.03 vol-% wet 0.0005 3/17/2010 13:41:55 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00010.SPE 0 vol-% wet 0.0019 3/17/2010 13:42:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00011.SPE 0 vol-% wet 0.0037 3/17/2010 13:42:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00012.SPE 0 vol-% wet 0.0041 3/17/2010 13:42:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00013.SPE 0 vol-% wet 0.0044 3/17/2010 13:44:38 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00014.SPE 0 vol-% wet 0.0063 3/17/2010 13:44:44 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00015.SPE 0 vol-% wet 0.005 3/17/2010 13:44:50 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00016.SPE 0 vol-% wet 0.0058 3/17/2010 13:48:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00017.SPE 0 vol-% wet 0.0057 3/17/2010 13:51:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00018.SPE 0 vol-% wet 0.0051 3/17/2010 13:51:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00019.SPE 0 vol-% wet 0.0006 3/17/2010 13:51:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00020.SPE 0 vol-% wet 0.0025 3/17/2010 13:51:19 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00021.SPE 0 vol-% wet 0.0042 3/17/2010 13:51:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00022.SPE 0.05 vol-% wet 0.0003 3/17/2010 13:51:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00023.SPE 0 vol-% wet 0.0029 3/17/2010 13:51:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00024.SPE 0 vol-% wet 0.0021 3/17/2010 13:54:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00025.SPE 0 vol-% wet 0.0001 3/17/2010 13:56:53 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00026.SPE 0 vol-% wet 0.0012 3/17/2010 13:56:59 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00027.SPE 0 vol-% wet 0.0025 3/17/2010 13:57:05 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00028.SPE 0.06 vol-% wet 0.0003 3/17/2010 13:57:11 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00029.SPE 0 vol-% wet 0.0028 3/17/2010 13:57:17 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00030.SPE 0.01 vol-% wet 0.0003 3/17/2010 13:57:23 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00031.SPE 0 vol-% wet 0.0018 3/17/2010 13:57:29 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00032.SPE 0 vol-% wet 0.0025 3/17/2010 13:57:35 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00033.SPE 0 vol-% wet 0.0022 3/17/2010 13:57:41 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00034.SPE 0 vol-% wet 0.0005 3/17/2010 13:57:47 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00035.SPE 0 vol-% wet 0.0024 3/17/2010 13:57:53 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00036.SPE 0.02 vol-% wet 0.0004 3/17/2010 13:57:59 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00037.SPE 0 vol-% wet 0.002 3/17/2010 13:58:05 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00038.SPE 0.01 vol-% wet 0.0003 3/17/2010 13:58:11 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00039.SPE 0 vol-% wet 0.0038 3/17/2010 13:58:17 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00040.SPE 0 vol-% wet 0.0003 3/17/2010 13:58:23 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00041.SPE 0 vol-% wet 0.0012 3/17/2010 13:58:28 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00042.SPE 0.02 vol-% wet 0.0004 3/17/2010 13:58:34 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00043.SPE 0.04 vol-% wet 0.0005 3/17/2010 13:58:40 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00044.SPE 0.06 vol-% wet 0.0003 3/17/2010 13:58:46 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00045.SPE 0.01 vol-% wet 0.0002 3/17/2010 13:58:52 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00046.SPE 0 vol-% wet 0.0042 3/17/2010 13:58:58 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00047.SPE 0 vol-% wet 0.0005 3/17/2010 13:59:04 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00048.SPE 0 vol-% wet 0.001 3/17/2010 13:59:10 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00049.SPE 0 vol-% wet 0.0032 3/17/2010 13:59:16 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00050.SPE 0 vol-% wet 0.0036 

Averages 0.01 
Date Time SpectrumFile Water vapor H2O Unit Compensa Residual Hydrogen ch

3/17/2010 14:01:20 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00060.SPE 6.79 vol-% wet 0.0028 3/17/2010 14:01:26 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00061.SPE 6.79 vol-% wet 0.0027 3/17/2010 14:01:32 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00062.SPE 6.82 vol-% wet 0.0029 3/17/2010 14:01:38 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00063.SPE 6.91 vol-% wet 0.0028 3/17/2010 14:01:44 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00064.SPE 6.99 vol-% wet 0.0026 3/17/2010 14:01:50 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00065.SPE 7.1 vol-% wet 0.0028 3/17/2010 14:01:56 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00066.SPE 7.14 vol-% wet 0.0028 3/17/2010 14:02:02 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00067.SPE 7.14 vol-% wet 0.0029 3/17/2010 14:05:28 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00068.SPE 6.86 vol-% wet 0.0026 3/17/2010 14:06:48 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00069.SPE 6.79 vol-% wet 0.0028 3/17/2010 14:07:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00070.SPE 6.75 vol-% wet 0.0027 3/17/2010 14:07:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00071.SPE 6.6 vol-% wet 0.0023 3/17/2010 14:07:55 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00072.SPE 6.8 vol-% wet 0.0018 3/17/2010 14:08:01 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00073.SPE 6.68 vol-% wet 0.0017 3/17/2010 14:08:07 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00074.SPE 6.77 vol-% wet 0.0017 3/17/2010 14:08:13 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00075.SPE 6.76 vol-% wet 0.0018 3/17/2010 14:08:35 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00076.SPE 6.82 vol-% wet 0.0017 3/17/2010 14:09:03 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00077.SPE 6.84 vol-% wet 0.0019 3/17/2010 14:09:57 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00078.SPE 6.79 vol-% wet 0.0019 3/17/2010 14:10:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00079.SPE 6.89 vol-% wet 0.0019 3/17/2010 14:10:13 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00080.SPE 6.84 vol-% wet 0.0019 3/17/2010 14:10:20 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00081.SPE 6.93 vol-% wet 0.0019 3/17/2010 14:11:50 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00082.SPE 5.8 vol-% wet 0.0024 3/17/2010 14:11:57 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00083.SPE 5.83 vol-% wet 0.0024 3/17/2010 14:12:04 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00084.SPE 5.86 vol-% wet 0.0023 3/17/2010 14:13:33 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00085.SPE 6.36 vol-% wet 0.0024 3/17/2010 14:13:41 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00086.SPE 6.09 vol-% wet 0.0024 3/17/2010 14:13:47 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00087.SPE 5.97 vol-% wet 0.0024 3/17/2010 14:13:54 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00088.SPE 5.93 vol-% wet 0.0023 3/17/2010 14:14:09 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00089.SPE 5.82 vol-% wet 0.0025 3/17/2010 14:14:19 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00090.SPE 5.89 vol-% wet 0.0024 3/17/2010 14:14:25 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00091.SPE 5.79 vol-% wet 0.0024 3/17/2010 14:14:31 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00092.SPE 5.74 vol-% wet 0.0024 3/17/2010 14:14:37 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00093.SPE 5.69 vol-% wet 0.0025 3/17/2010 14:14:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00094.SPE 5.7 vol-% wet 0.0024 3/17/2010 14:14:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00095.SPE 5.75 vol-% wet 0.0025 
HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 10.78 C:\CalcmetSam 1.12

03/17/10 321 C:\CalcmetSamples\L 14.33 C:\CalcmetSam 1.17

03/17/10 321 C:\CalcmetSamples\L 11.72 C:\CalcmetSam 1.17

Avg. Conc. (ppm) 1.153 12.28 

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 0.00 C:\CalcmetSam 0.63

03/17/10 321 C:\CalcmetSamples\L 0.00 C:\CalcmetSam 0.59

03/17/10 321 C:\CalcmetSamples\L 0.19 C:\CalcmetSam 0

Avg. Conc. (ppm) 0.407 0.06 

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 12.28 ppm Mean concentration of spiked analyte

Su 0.06 ppm Native concentration of analyte

DF 7.5% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

 ppm Cylinder of tracer gas (SF6) 9.98

Ce 10.85 ppm Expected concentration of analyte

Recovery (%) 113.3% 70 - 130 %
Date Time SpectrumFile Water vapoUnit Compensa Residual Hydrogen cUnit Compensa Residual SF6 Unit C

3/17/2010 14:26:50 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00142.SPE 6.88 vol-% wet 0.0027 4.76 ppm wet 0.0054 0.41 ppm w3/17/2010 14:27:50 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00143.SPE 6.93 vol-% wet 0.0027 4.71 ppm wet 0.0054 0.42 ppm w3/17/2010 14:28:51 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00144.SPE 6.93 vol-% wet 0.0028 4.98 ppm wet 0.0057 0.42 ppm w3/17/2010 14:29:51 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00145.SPE 6.94 vol-% wet 0.0027 5.19 ppm wet 0.0056 0.43 ppm w3/17/2010 14:30:52 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00146.SPE 6.94 vol-% wet 0.0028 4.91 ppm wet 0.0056 0.43 ppm w3/17/2010 14:31:53 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00147.SPE 7.07 vol-% wet 0.0028 4.89 ppm wet 0.0054 0.42 ppm w3/17/2010 14:32:53 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00148.SPE 7.08 vol-% wet 0.0028 4.6 ppm wet 0.0054 0.42 ppm w3/17/2010 14:33:54 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00149.SPE 6.97 vol-% wet 0.0027 4.92 ppm wet 0.0053 0.41 ppm w3/17/2010 14:34:54 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00150.SPE 7.04 vol-% wet 0.0028 4.62 ppm wet 0.0052 0.42 ppm w3/17/2010 14:35:55 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00151.SPE 7.13 vol-% wet 0.0029 4.64 ppm wet 0.0053 0.41 ppm w3/17/2010 14:36:56 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00152.SPE 7.18 vol-% wet 0.0029 4.82 ppm wet 0.0053 0.42 ppm w3/17/2010 14:37:56 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00153.SPE 7.27 vol-% wet 0.003 5.03 ppm wet 0.0054 0.43 ppm w3/17/2010 14:38:57 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00154.SPE 7.32 vol-% wet 0.003 5.02 ppm wet 0.0054 0.44 ppm w3/17/2010 14:39:58 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00155.SPE 7.36 vol-% wet 0.0029 4.76 ppm wet 0.0052 0.44 ppm w3/17/2010 14:40:58 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00156.SPE 7.2 vol-% wet 0.0029 4.77 ppm wet 0.0053 0.44 ppm w3/17/2010 14:41:59 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00157.SPE 7.09 vol-% wet 0.0028 4.35 ppm wet 0.0052 0.43 ppm w3/17/2010 14:42:59 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00158.SPE 7.03 vol-% wet 0.0028 4.4 ppm wet 0.0052 0.43 ppm w3/17/2010 14:44:00 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00159.SPE 7.17 vol-% wet 0.0028 4.46 ppm wet 0.005 0.43 ppm w3/17/2010 14:45:01 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00160.SPE 7.21 vol-% wet 0.0029 4.68 ppm wet 0.0052 0.44 ppm w3/17/2010 14:46:01 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00161.SPE 7.27 vol-% wet 0.0029 4.73 ppm wet 0.0053 0.46 ppm w3/17/2010 14:47:02 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00162.SPE 7.36 vol-% wet 0.0029 4.44 ppm wet 0.0052 0.45 ppm w3/17/2010 14:48:02 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00163.SPE 7.24 vol-% wet 0.0029 4.6 ppm wet 0.0054 0.44 ppm w3/17/2010 14:49:03 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00164.SPE 7.18 vol-% wet 0.0029 4.5 ppm wet 0.0054 0.45 ppm w3/17/2010 14:50:03 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00165.SPE 7.38 vol-% wet 0.003 4.4 ppm wet 0.0054 0.48 ppm w3/17/2010 14:51:04 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00166.SPE 7.38 vol-% wet 0.003 4.33 ppm wet 0.0052 0.47 ppm w3/17/2010 14:52:05 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00167.SPE 7.46 vol-% wet 0.003 4.37 ppm wet 0.0052 0.48 ppm w3/17/2010 14:53:05 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00168.SPE 7.51 vol-% wet 0.0031 4.47 ppm wet 0.0052 0.48 ppm w3/17/2010 14:54:06 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00169.SPE 7.29 vol-% wet 0.003 4.37 ppm wet 0.0055 0.48 ppm w3/17/2010 14:55:06 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00170.SPE 7.04 vol-% wet 0.0028 4.76 ppm wet 0.0056 0.46 ppm w3/17/2010 14:56:07 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00171.SPE 6.95 vol-% wet 0.0028 4.61 ppm wet 0.0055 0.46 ppm w3/17/2010 14:57:08 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00172.SPE 7.02 vol-% wet 0.0028 4.17 ppm wet 0.0054 0.47 ppm w3/17/2010 14:58:08 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00173.SPE 7.13 vol-% wet 0.0028 4.33 ppm wet 0.0054 0.48 ppm w3/17/2010 14:59:09 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00174.SPE 7.05 vol-% wet 0.0028 4.49 ppm wet 0.0054 0.47 ppm w3/17/2010 15:00:09 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00175.SPE 6.99 vol-% wet 0.0028 4.51 ppm wet 0.0054 0.47 ppm w3/17/2010 15:01:10 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00176.SPE 7.04 vol-% wet 0.0028 4.43 ppm wet 0.0053 0.46 ppm w3/17/2010 15:02:11 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00177.SPE 7.12 vol-% wet 0.0029 4.19 ppm wet 0.0053 0.47 ppm w3/17/2010 15:03:11 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00178.SPE 7.07 vol-% wet 0.0028 4.16 ppm wet 0.0052 0.47 ppm w3/17/2010 15:04:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00179.SPE 7.01 vol-% wet 0.0028 4.53 ppm wet 0.0052 0.46 ppm w3/17/2010 15:05:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00180.SPE 7.01 vol-% wet 0.0028 4.08 ppm wet 0.0052 0.47 ppm w3/17/2010 15:06:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00181.SPE 6.9 vol-% wet 0.0028 4.09 ppm wet 0.0052 0.46 ppm w3/17/2010 15:07:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00182.SPE 6.84 vol-% wet 0.0028 3.99 ppm wet 0.0052 0.46 ppm w3/17/2010 15:08:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00183.SPE 6.84 vol-% wet 0.0028 4.31 ppm wet 0.0052 0.47 ppm w3/17/2010 15:09:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00184.SPE 6.83 vol-% wet 0.0028 4.15 ppm wet 0.0054 0.47 ppm w3/17/2010 15:10:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00185.SPE 6.77 vol-% wet 0.0027 4.15 ppm wet 0.0053 0.46 ppm w3/17/2010 15:11:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00186.SPE 6.72 vol-% wet 0.0027 4.11 ppm wet 0.0052 0.46 ppm w3/17/2010 15:12:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00187.SPE 6.8 vol-% wet 0.0028 5.53 ppm wet 0.008 0.48 ppm w3/17/2010 15:13:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00188.SPE 6.82 vol-% wet 0.0028 5.66 ppm wet 0.0077 0.5 ppm w3/17/2010 15:14:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00189.SPE 6.67 vol-% wet 0.0026 4.84 ppm wet 0.0063 0.47 ppm w3/17/2010 15:15:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00190.SPE 6.58 vol-% wet 0.0026 5.07 ppm wet 0.0064 0.46 ppm w3/17/2010 15:16:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00191.SPE 6.62 vol-% wet 0.0026 4.75 ppm wet 0.0065 0.46 ppm w3/17/2010 15:17:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00192.SPE 6.61 vol-% wet 0.0026 5.14 ppm wet 0.0065 0.46 ppm w3/17/2010 15:18:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00193.SPE 6.63 vol-% wet 0.0026 4.16 ppm wet 0.0055 0.43 ppm w3/17/2010 15:19:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00194.SPE 6.64 vol-% wet 0.0025 3.09 ppm wet 0.0049 0.42 ppm w3/17/2010 15:20:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00195.SPE 6.74 vol-% wet 0.0026 3.16 ppm wet 0.0049 0.43 ppm w3/17/2010 15:21:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00196.SPE 6.75 vol-% wet 0.0027 3.74 ppm wet 0.0049 0.43 ppm w3/17/2010 15:22:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00197.SPE 6.78 vol-% wet 0.0028 3.09 ppm wet 0.0047 0.43 ppm w3/17/2010 15:23:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00198.SPE 6.78 vol-% wet 0.0026 2.75 ppm wet 0.0047 0.43 ppm w3/17/2010 15:24:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00199.SPE 6.73 vol-% wet 0.0026 2.74 ppm wet 0.0047 0.42 ppm w3/17/2010 15:25:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00200.SPE 6.77 vol-% wet 0.0027 2.88 ppm wet 0.0047 0.43 ppm w3/17/2010 15:26:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00201.SPE 6.82 vol-% wet 0.0026 2.85 ppm wet 0.0047 0.45 ppm w3/17/2010 15:27:26 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00202.SPE 6.8 vol-% wet 0.0027 2.91 ppm wet 0.0047 0.43 ppm w

Averages 4.36
HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 13.09 C:\CalcmetSam 1.34

03/17/10 321 C:\CalcmetSamples\L 12.87 C:\CalcmetSam 1.37

03/17/10 321 C:\CalcmetSamples\L 14.14 C:\CalcmetSam 1.47

Avg. Conc. (ppm) 1.393 13.37 

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 2.88 C:\CalcmetSam 0.43

03/17/10 321 C:\CalcmetSamples\L 2.85 C:\CalcmetSam 0.45

03/17/10 321 C:\CalcmetSamples\L 2.91 C:\CalcmetSam 0.43

Avg. Conc. (ppm) 0.437 2.88 

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 13.37 ppm Mean concentration of spiked analyte

Su 2.88 ppm Native concentration of analyte

DF 9.6% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

 ppm Cylinder of tracer gas (SF6) 9.98

Ce 16.43 ppm Expected concentration of analyte

Recovery (%) 77.9% 70 - 130 %
Date Time SpectrumFile Water vapoUnit Compensa Residual Hydrog

3/17/2010 15:36:21 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00203.SPE 6.37 vol-% wet 0.0025 3/17/2010 15:36:30 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00204.SPE 6.36 vol-% wet 0.0025 3/17/2010 15:36:38 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00205.SPE 6.35 vol-% wet 0.0026 133/17/2010 15:37:14 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00206.SPE 6.3 vol-% wet 0.0025 123/17/2010 15:37:17 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00207.SPE 6.33 vol-% wet 0.0028 143/17/2010 15:37:19 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00208.SPE 6.24 vol-% wet 0.0023 113/17/2010 15:37:22 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00209.SPE 6.31 vol-% wet 0.0026 83/17/2010 15:37:24 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00210.SPE 6.32 vol-% wet 0.0027 33/17/2010 15:37:26 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00211.SPE 6.32 vol-% wet 0.0021 1
Date Time SpectrumFile Water vapor H2O Unit Compensa Residual Hydrogen cUnit Compensa Residual SF6 Unit 

3/17/2010 15:52:48 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00310.SPE 6.35 vol-% wet 0.0026 1.8 ppm wet 0.0051 0.95 ppm 3/17/2010 15:53:48 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00311.SPE 6.5 vol-% wet 0.0027 1.92 ppm wet 0.0053 0.51 ppm 3/17/2010 15:54:49 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00312.SPE 6.54 vol-% wet 0.0026 2.06 ppm wet 0.0054 0.5 ppm 3/17/2010 15:55:50 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00313.SPE 6.52 vol-% wet 0.0026 2.24 ppm wet 0.0055 0.5 ppm 3/17/2010 15:56:50 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00314.SPE 6.49 vol-% wet 0.0026 2.13 ppm wet 0.0057 0.51 ppm 3/17/2010 15:57:51 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00315.SPE 6.47 vol-% wet 0.0027 2.26 ppm wet 0.0058 0.51 ppm 3/17/2010 15:58:51 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00316.SPE 6.43 vol-% wet 0.0026 2.47 ppm wet 0.0057 0.5 ppm 3/17/2010 15:59:52 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00317.SPE 6.4 vol-% wet 0.0026 2.29 ppm wet 0.0057 0.5 ppm 3/17/2010 16:00:53 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00318.SPE 6.34 vol-% wet 0.0027 2.29 ppm wet 0.0057 0.5 ppm 3/17/2010 16:01:53 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00319.SPE 6.31 vol-% wet 0.0026 2.52 ppm wet 0.0059 0.5 ppm 3/17/2010 16:02:54 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00320.SPE 6.27 vol-% wet 0.0026 2.55 ppm wet 0.0059 0.51 ppm 3/17/2010 16:03:54 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00321.SPE 6.29 vol-% wet 0.0026 2.61 ppm wet 0.006 0.52 ppm 3/17/2010 16:04:55 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00322.SPE 6.38 vol-% wet 0.0026 2.57 ppm wet 0.0059 0.52 ppm 3/17/2010 16:05:56 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00323.SPE 6.4 vol-% wet 0.0026 2.42 ppm wet 0.0057 0.51 ppm 3/17/2010 16:06:56 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00324.SPE 6.44 vol-% wet 0.0026 2.31 ppm wet 0.0057 0.49 ppm 3/17/2010 16:07:57 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00325.SPE 6.49 vol-% wet 0.0026 2.48 ppm wet 0.0057 0.49 ppm 3/17/2010 16:08:57 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00326.SPE 6.51 vol-% wet 0.0026 2.39 ppm wet 0.0056 0.49 ppm 3/17/2010 16:09:58 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00327.SPE 6.57 vol-% wet 0.0027 2.05 ppm wet 0.0054 0.48 ppm 3/17/2010 16:10:59 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00328.SPE 6.63 vol-% wet 0.0028 2.32 ppm wet 0.0054 0.49 ppm 3/17/2010 16:11:59 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00329.SPE 6.76 vol-% wet 0.0028 2.31 ppm wet 0.0055 0.49 ppm 3/17/2010 16:13:00 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00330.SPE 6.87 vol-% wet 0.0028 2.39 ppm wet 0.0055 0.48 ppm 3/17/2010 16:14:00 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00331.SPE 6.9 vol-% wet 0.0028 2.21 ppm wet 0.0056 0.48 ppm 3/17/2010 16:15:01 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00332.SPE 7.01 vol-% wet 0.0029 2.21 ppm wet 0.0053 0.49 ppm 3/17/2010 16:16:01 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00333.SPE 7.1 vol-% wet 0.0029 2.08 ppm wet 0.0052 0.49 ppm 3/17/2010 16:17:02 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00334.SPE 7.17 vol-% wet 0.0029 1.95 ppm wet 0.0052 0.48 ppm 3/17/2010 16:18:03 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00335.SPE 7.25 vol-% wet 0.003 1.96 ppm wet 0.005 0.49 ppm 3/17/2010 16:19:03 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00336.SPE 7.32 vol-% wet 0.003 1.87 ppm wet 0.005 0.48 ppm 3/17/2010 16:20:04 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00337.SPE 7.42 vol-% wet 0.0031 1.74 ppm wet 0.005 0.48 ppm 3/17/2010 16:21:04 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00338.SPE 7.57 vol-% wet 0.0033 1.66 ppm wet 0.005 0.46 ppm 3/17/2010 16:22:05 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00339.SPE 11.18 vol-% wet 0.003 5.37 ppm wet 0.0043 0.29 ppm 3/17/2010 16:23:06 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00340.SPE 12.2 vol-% wet 0.0029 9.19 ppm wet 0.005 0.16 ppm 3/17/2010 16:24:06 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00341.SPE 7.67 vol-% wet 0.0028 3.56 ppm wet 0.0051 0.42 ppm 3/17/2010 16:25:07 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00342.SPE 7.55 vol-% wet 0.003 2.27 ppm wet 0.0051 0.45 ppm 3/17/2010 16:26:07 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00343.SPE 7.37 vol-% wet 0.0029 2 ppm wet 0.0052 0.46 ppm 3/17/2010 16:27:08 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00344.SPE 7.26 vol-% wet 0.0029 1.93 ppm wet 0.0053 0.48 ppm 3/17/2010 16:28:09 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00345.SPE 7.23 vol-% wet 0.0029 1.82 ppm wet 0.0051 0.47 ppm 3/17/2010 16:29:09 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00346.SPE 7.16 vol-% wet 0.0029 2.18 ppm wet 0.0053 0.48 ppm 3/17/2010 16:30:10 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00347.SPE 7.1 vol-% wet 0.0029 2.05 ppm wet 0.0055 0.48 ppm 3/17/2010 16:31:10 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00348.SPE 7.06 vol-% wet 0.0029 1.98 ppm wet 0.0053 0.48 ppm 3/17/2010 16:32:11 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00349.SPE 7.03 vol-% wet 0.0028 2.17 ppm wet 0.0057 0.48 ppm 3/17/2010 16:33:12 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00350.SPE 6.95 vol-% wet 0.0028 2.16 ppm wet 0.0057 0.47 ppm 3/17/2010 16:34:12 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00351.SPE 6.88 vol-% wet 0.0028 2.43 ppm wet 0.0057 0.47 ppm 3/17/2010 16:35:13 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00352.SPE 6.84 vol-% wet 0.0028 2.05 ppm wet 0.0057 0.47 ppm 3/17/2010 16:36:13 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00353.SPE 6.75 vol-% wet 0.0027 2.22 ppm wet 0.0058 0.47 ppm 3/17/2010 16:37:14 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00354.SPE 6.68 vol-% wet 0.0027 2.19 ppm wet 0.0057 0.47 ppm 3/17/2010 16:38:15 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00355.SPE 6.7 vol-% wet 0.0027 2 ppm wet 0.0056 0.47 ppm 3/17/2010 16:39:15 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00356.SPE 6.69 vol-% wet 0.0027 2.25 ppm wet 0.0058 0.46 ppm 3/17/2010 16:40:16 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00357.SPE 6.67 vol-% wet 0.0026 2.34 ppm wet 0.0059 0.48 ppm 3/17/2010 16:41:16 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00358.SPE 6.65 vol-% wet 0.0026 2.43 ppm wet 0.0059 0.46 ppm 3/17/2010 16:42:17 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00359.SPE 6.62 vol-% wet 0.0027 2.3 ppm wet 0.0058 0.46 ppm 3/17/2010 16:43:18 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00360.SPE 6.56 vol-% wet 0.0026 2.38 ppm wet 0.0059 0.45 ppm 3/17/2010 16:44:18 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00361.SPE 6.51 vol-% wet 0.0026 2.3 ppm wet 0.0058 0.46 ppm 3/17/2010 16:45:19 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00362.SPE 6.51 vol-% wet 0.0026 2.29 ppm wet 0.0057 0.47 ppm 3/17/2010 16:46:19 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00363.SPE 6.49 vol-% wet 0.0026 2.42 ppm wet 0.0059 0.47 ppm 3/17/2010 16:47:20 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00364.SPE 6.45 vol-% wet 0.0026 2.47 ppm wet 0.0059 0.48 ppm 3/17/2010 16:48:20 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00365.SPE 6.43 vol-% wet 0.0026 2.14 ppm wet 0.0057 0.47 ppm 3/17/2010 16:49:21 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00366.SPE 6.47 vol-% wet 0.0026 2.23 ppm wet 0.0057 0.46 ppm 3/17/2010 16:50:22 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00367.SPE 6.44 vol-% wet 0.0026 2.3 ppm wet 0.0058 0.47 ppm 3/17/2010 16:51:22 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00368.SPE 6.39 vol-% wet 0.0026 2.45 ppm wet 0.006 0.47 ppm 3/17/2010 16:52:23 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00369.SPE 6.37 vol-% wet 0.0026 2.51 ppm wet 0.0059 0.49 ppm 3/17/2010 16:53:23 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00370.SPE 6.37 vol-% wet 0.0026 2.36 ppm wet 0.0059 0.47 ppm 

Averages 2.41
HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 7.90 C:\CalcmetSam 0.88

03/17/10 321 C:\CalcmetSamples\L 6.49 C:\CalcmetSam 0.87

03/17/10 321 C:\CalcmetSamples\L 8.09 C:\CalcmetSam 0.85

Avg. Conc. (ppm) 0.867 7.49 

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 2.45 C:\CalcmetSam 0.47

03/17/10 321 C:\CalcmetSamples\L 2.51 C:\CalcmetSam 0.49

03/17/10 321 C:\CalcmetSamples\L 2.36 C:\CalcmetSam 0.47

Avg. Conc. (ppm) 0.477 2.44 

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 7.49 ppm Mean concentration of spiked analyte

Su 2.44 ppm Native concentration of analyte

DF 3.9% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

 ppm Cylinder of tracer gas (SF6) 9.98

Ce 7.98 ppm Expected concentration of analyte

Recovery (%) 91.4% 70 - 130 %
Date Time SpectrumFile Water vapoUnit Compensa Residual Hyd

3/17/2010 17:02:01 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00397.SPE 6.62 vol-% wet 0.0029 3/17/2010 17:02:04 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00398.SPE 6.56 vol-% wet 0.0028 3/17/2010 17:02:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00399.SPE 6.55 vol-% wet 0.0023 3/17/2010 17:02:09 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00400.SPE 6.55 vol-% wet 0.0025 3/17/2010 17:02:11 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00401.SPE 6.54 vol-% wet 0.0026 3/17/2010 17:02:14 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00402.SPE 6.53 vol-% wet 0.0024 3/17/2010 17:02:17 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00403.SPE 6.5 vol-% wet 0.0028 3/17/2010 17:02:19 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00404.SPE 6.54 vol-% wet 0.0027 3/17/2010 17:02:22 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00405.SPE 6.46 vol-% wet 0.0026 
Date Time SpectrumFile Water vapoUnit Compensa Residual Hydrogen cUnit Compensa Residual SF6 Unit 

3/17/2010 17:17:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00417.SPE 9.11 vol-% wet 0.0027 2.24 ppm wet 0.005 0.48 ppm w3/17/2010 17:18:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00418.SPE 9.1 vol-% wet 0.0027 2.24 ppm wet 0.005 0.48 ppm w3/17/2010 17:19:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00419.SPE 9.07 vol-% wet 0.0027 2.22 ppm wet 0.005 0.47 ppm w3/17/2010 17:20:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00420.SPE 9.06 vol-% wet 0.0027 2.32 ppm wet 0.005 0.47 ppm w3/17/2010 17:21:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00421.SPE 8.98 vol-% wet 0.0027 2.42 ppm wet 0.0052 0.47 ppm w3/17/2010 17:22:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00422.SPE 8.99 vol-% wet 0.0027 2.36 ppm wet 0.0052 0.47 ppm w3/17/2010 17:23:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00423.SPE 8.97 vol-% wet 0.0027 2.33 ppm wet 0.0051 0.46 ppm w3/17/2010 17:24:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00424.SPE 8.99 vol-% wet 0.0027 2.45 ppm wet 0.0052 0.47 ppm w3/17/2010 17:25:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00425.SPE 8.99 vol-% wet 0.0027 2.35 ppm wet 0.0052 0.47 ppm w3/17/2010 17:26:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00426.SPE 8.99 vol-% wet 0.0027 2.26 ppm wet 0.0051 0.48 ppm w3/17/2010 17:27:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00427.SPE 8.98 vol-% wet 0.0027 2.3 ppm wet 0.0051 0.47 ppm w3/17/2010 17:28:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00428.SPE 8.96 vol-% wet 0.0027 2.16 ppm wet 0.0051 0.46 ppm w3/17/2010 17:29:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00429.SPE 8.98 vol-% wet 0.0027 2.01 ppm wet 0.005 0.46 ppm w3/17/2010 17:30:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00430.SPE 8.96 vol-% wet 0.0026 2.03 ppm wet 0.005 0.46 ppm w3/17/2010 17:31:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00431.SPE 8.98 vol-% wet 0.0026 2.19 ppm wet 0.005 0.47 ppm w3/17/2010 17:32:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00432.SPE 9.02 vol-% wet 0.0026 1.93 ppm wet 0.0048 0.46 ppm w3/17/2010 17:33:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00433.SPE 9.07 vol-% wet 0.0026 1.87 ppm wet 0.0048 0.45 ppm w3/17/2010 17:34:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00434.SPE 9.06 vol-% wet 0.0027 1.87 ppm wet 0.005 0.46 ppm w3/17/2010 17:35:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00435.SPE 9.02 vol-% wet 0.0026 1.97 ppm wet 0.005 0.47 ppm w3/17/2010 17:36:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00436.SPE 9.03 vol-% wet 0.0026 2.11 ppm wet 0.0051 0.47 ppm w3/17/2010 17:37:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00437.SPE 9.01 vol-% wet 0.0026 2.13 ppm wet 0.0052 0.47 ppm w3/17/2010 17:38:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00438.SPE 9.98 vol-% wet 0.0027 2.16 ppm wet 0.005 0.47 ppm w3/17/2010 17:39:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00439.SPE 9.97 vol-% wet 0.0027 2.28 ppm wet 0.0052 0.48 ppm w3/17/2010 17:40:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00440.SPE 9.99 vol-% wet 0.0026 2.21 ppm wet 0.0051 0.48 ppm w3/17/2010 17:41:26 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00441.SPE 9.92 vol-% wet 0.0026 2.4 ppm wet 0.0053 0.47 ppm w3/17/2010 17:42:27 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00442.SPE 9.88 vol-% wet 0.0026 2.32 ppm wet 0.0051 0.46 ppm w3/17/2010 17:43:27 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00443.SPE 9.9 vol-% wet 0.0027 2.31 ppm wet 0.0051 0.46 ppm w3/17/2010 17:44:28 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00444.SPE 9.9 vol-% wet 0.0027 2.11 ppm wet 0.005 0.48 ppm w3/17/2010 17:45:28 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00445.SPE 9.9 vol-% wet 0.0026 2.1 ppm wet 0.005 0.48 ppm w3/17/2010 17:46:29 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00446.SPE 9.92 vol-% wet 0.0027 2.29 ppm wet 0.0051 0.48 ppm w3/17/2010 17:47:30 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00447.SPE 9.94 vol-% wet 0.0026 2.27 ppm wet 0.0054 0.5 ppm w3/17/2010 17:48:30 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00448.SPE 9.9 vol-% wet 0.0026 2.37 ppm wet 0.0054 0.47 ppm w3/17/2010 17:49:31 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00449.SPE 9.86 vol-% wet 0.0026 2.35 ppm wet 0.0053 0.47 ppm w3/17/2010 17:50:31 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00450.SPE 9.84 vol-% wet 0.0026 2.29 ppm wet 0.0052 0.47 ppm w3/17/2010 17:51:32 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00451.SPE 9.85 vol-% wet 0.0026 2.46 ppm wet 0.0052 0.48 ppm w3/17/2010 17:52:33 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00452.SPE 9.8 vol-% wet 0.0027 2.27 ppm wet 0.005 0.46 ppm w3/17/2010 17:53:33 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00453.SPE 9.79 vol-% wet 0.0026 2.08 ppm wet 0.0049 0.47 ppm w3/17/2010 17:54:34 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00454.SPE 9.75 vol-% wet 0.0026 2.05 ppm wet 0.0049 0.46 ppm w3/17/2010 17:55:34 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00455.SPE 9.75 vol-% wet 0.0026 2.24 ppm wet 0.005 0.47 ppm w3/17/2010 17:56:35 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00456.SPE 9.78 vol-% wet 0.0026 2.08 ppm wet 0.0049 0.48 ppm w3/17/2010 17:57:36 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00457.SPE 9.84 vol-% wet 0.0026 1.99 ppm wet 0.0049 0.47 ppm w3/17/2010 17:58:36 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00458.SPE 9.91 vol-% wet 0.0027 2.03 ppm wet 0.005 0.46 ppm w3/17/2010 17:59:37 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00459.SPE 9.88 vol-% wet 0.0027 2.03 ppm wet 0.0051 0.46 ppm w3/17/2010 18:00:37 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00460.SPE 9.88 vol-% wet 0.0026 2 ppm wet 0.0052 0.46 ppm w3/17/2010 18:01:38 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00461.SPE 9.9 vol-% wet 0.0026 1.84 ppm wet 0.0052 0.46 ppm w3/17/2010 18:02:39 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00462.SPE 9.86 vol-% wet 0.0027 2.11 ppm wet 0.0053 0.46 ppm w3/17/2010 18:03:39 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00463.SPE 9.87 vol-% wet 0.0026 2.06 ppm wet 0.005 0.47 ppm w3/17/2010 18:04:40 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00464.SPE 9.85 vol-% wet 0.0027 1.95 ppm wet 0.005 0.47 ppm w3/17/2010 18:05:41 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00465.SPE 9.86 vol-% wet 0.0027 2 ppm wet 0.0049 0.45 ppm w3/17/2010 18:06:41 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00466.SPE 9.8 vol-% wet 0.0027 2.04 ppm wet 0.005 0.46 ppm w3/17/2010 18:07:42 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00467.SPE 10.74 vol-% wet 0.0027 2.32 ppm wet 0.0049 0.47 ppm w3/17/2010 18:08:43 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00468.SPE 10.84 vol-% wet 0.0033 2.21 ppm wet 0.0047 0.45 ppm w3/17/2010 18:09:43 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00469.SPE 10.77 vol-% wet 0.0032 2.33 ppm wet 0.0048 0.44 ppm w3/17/2010 18:10:44 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00470.SPE 10.74 vol-% wet 0.0032 2.65 ppm wet 0.005 0.45 ppm w3/17/2010 18:11:44 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00471.SPE 10.75 vol-% wet 0.0031 2.21 ppm wet 0.0047 0.43 ppm w3/17/2010 18:12:45 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00472.SPE 10.72 vol-% wet 0.0032 2.51 ppm wet 0.0047 0.43 ppm w3/17/2010 18:13:46 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00473.SPE 10.68 vol-% wet 0.0031 2.54 ppm wet 0.0049 0.45 ppm w3/17/2010 18:14:46 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00474.SPE 10.68 vol-% wet 0.0031 2.61 ppm wet 0.0049 0.46 ppm w3/17/2010 18:15:47 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00475.SPE 10.69 vol-% wet 0.0031 2.49 ppm wet 0.0048 0.45 ppm w3/17/2010 18:16:47 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00476.SPE 10.71 vol-% wet 0.0031 2.5 ppm wet 0.0049 0.46 ppm w3/17/2010 18:17:48 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00477.SPE 10.71 vol-% wet 0.0032 2.53 ppm wet 0.0049 0.45 ppm w

Averages 2.22
Date Time SpectrumFile Water vapoUnit Compensa Residual Hydrog

3/17/2010 18:20:37 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00478.SPE 5.54 vol-% wet 0.0026 4

3/17/2010 18:20:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00479.SPE 6.52 vol-% wet 0.0023 63/17/2010 18:20:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00480.SPE 5.55 vol-% wet 0.0026 43/17/2010 18:21:29 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00481.SPE 6.2 vol-% wet 0.0021 6

3/17/2010 18:21:35 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00482.SPE 5.91 vol-% wet 0.0019 7

3/17/2010 18:21:41 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00483.SPE 5.78 vol-% wet 0.0021 103/17/2010 18:21:47 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00484.SPE 5.74 vol-% wet 0.0019 103/17/2010 18:21:53 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00485.SPE 5.72 vol-% wet 0.0019 103/17/2010 18:21:59 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00486.SPE 5.58 vol-% wet 0.0019 123/17/2010 18:22:05 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00487.SPE 5.62 vol-% wet 0.002 123/17/2010 18:22:11 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00488.SPE 5.57 vol-% wet 0.0019 123/17/2010 18:22:17 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00489.SPE 5.48 vol-% wet 0.002 113/17/2010 18:22:23 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00490.SPE 5.57 vol-% wet 0.0019 153/17/2010 18:22:55 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00491.SPE 6.17 vol-% wet 0.0021 13/17/2010 18:23:00 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00492.SPE 6.21 vol-% wet 0.002 23/17/2010 18:23:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00493.SPE 6.38 vol-% wet 0.0023 33/17/2010 18:23:12 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00494.SPE 6.42 vol-% wet 0.0022 1
HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 10.27 C:\CalcmetSam 0.5

03/17/10 321 C:\CalcmetSamples\L 10.98 C:\CalcmetSam 1.47

03/17/10 321 C:\CalcmetSamples\L 12.23 C:\CalcmetSam 1.49

Avg. Conc. (ppm) 1.153 11.16 

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\L 2.49 C:\CalcmetSam 0.45

03/17/10 321 C:\CalcmetSamples\L 2.50 C:\CalcmetSam 0.46

03/17/10 321 C:\CalcmetSamples\L 2.53 C:\CalcmetSam 0.45

Avg. Conc. (ppm) 0.453 2.51 

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 11.16 ppm Mean concentration of spiked analyte

Su 2.51 ppm Native concentration of analyte

DF 7.0% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

 ppm Cylinder of tracer gas (SF6) 9.98

Ce 12.45 ppm Expected concentration of analyte

Recovery (%) 87.3% 70 - 130 %
Date Time SpectrumFile Water vapoUnit Compensa Residu

3/17/2010 18:27:03 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00520.SPE 2.46 vol-% wet 0.003/17/2010 18:27:09 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00521.SPE 2.41 vol-% wet 0.003/17/2010 18:27:15 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00522.SPE 2.41 vol-% wet 0.003/17/2010 18:27:21 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00523.SPE 2.36 vol-% wet 0.003/17/2010 18:27:27 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00524.SPE 2.3 vol-% wet 0.003/17/2010 18:27:33 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00525.SPE 2.34 vol-% wet 0.003/17/2010 18:27:39 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00526.SPE 2.23 vol-% wet 0.003/17/2010 18:27:45 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00527.SPE 2.19 vol-% wet 0.003/17/2010 18:27:51 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00528.SPE 2.04 vol-% wet 0.003/17/2010 18:27:57 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00529.SPE 2.08 vol-% wet 0.003/17/2010 18:28:03 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00530.SPE 2.07 vol-% wet 0.003/17/2010 18:28:09 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00531.SPE 2.07 vol-% wet 0.003/17/2010 18:28:15 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00532.SPE 2.05 vol-% wet 0.003/17/2010 18:28:21 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00533.SPE 1.95 vol-% wet 0.003/17/2010 18:28:26 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00534.SPE 1.91 vol-% wet 0.003/17/2010 18:28:32 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00535.SPE 1.92 vol-% wet 0.003/17/2010 18:28:38 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00536.SPE 1.96 vol-% wet 0.003/17/2010 18:28:44 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00537.SPE 1.86 vol-% wet 0.003/17/2010 18:28:50 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00538.SPE 1.85 vol-% wet 0.003/17/2010 18:28:56 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00539.SPE 1.57 vol-% wet 0.003/17/2010 18:29:02 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00540.SPE 1.46 vol-% wet 0.003/17/2010 18:29:08 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00541.SPE 1.51 vol-% wet 0.003/17/2010 18:29:14 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00542.SPE 1.46 vol-% wet 0.00

Averages 
Date Time SpectrumFile Water vapoUnit Compensa Residual H

3/17/2010 18:39:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00578.SPE 0 vol-% wet 0.0236 3/17/2010 18:39:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00579.SPE 0 vol-% wet 0.0189 3/17/2010 18:39:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00580.SPE 0 vol-% wet 0.013 3/17/2010 18:39:19 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00581.SPE 0 vol-% wet 0.0236 3/17/2010 18:39:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00582.SPE 0 vol-% wet 0.0227 3/17/2010 18:39:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00583.SPE 0 vol-% wet 0.0254 3/17/2010 18:39:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00584.SPE 0 vol-% wet 0.017 3/17/2010 18:39:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00585.SPE 0 vol-% wet 0.011 3/17/2010 18:39:49 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00586.SPE 0 vol-% wet 0.0258 3/17/2010 18:39:54 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00587.SPE 0 vol-% wet 0.0192 3/17/2010 18:40:00 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00588.SPE 0 vol-% wet 0.0247 3/17/2010 18:40:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00589.SPE 0 vol-% wet 0.0232 3/17/2010 18:40:12 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00590.SPE 0 vol-% wet 0.0108 3/17/2010 18:40:18 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00591.SPE 0 vol-% wet 0.0235 3/17/2010 18:40:24 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00592.SPE 0 vol-% wet 0.021 3/17/2010 18:40:30 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00593.SPE 0 vol-% wet 0.0241 3/17/2010 18:40:36 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00594.SPE 0 vol-% wet 0.0153 3/17/2010 18:40:42 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00595.SPE 0 vol-% wet 0.0287 3/17/2010 18:40:48 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00596.SPE 0 vol-% wet 0.0214 3/17/2010 18:40:54 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00597.SPE 0 vol-% wet 0.026 3/17/2010 18:41:00 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00598.SPE 0 vol-% wet 0.0171 3/17/2010 18:41:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00599.SPE 0 vol-% wet 0.0281 3/17/2010 18:41:12 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00600.SPE 0 vol-% wet 0.0189 3/17/2010 18:41:18 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00601.SPE 0 vol-% wet 0.0141 3/17/2010 18:41:24 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00602.SPE 0 vol-% wet 0.0254 3/17/2010 18:41:30 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00603.SPE 0 vol-% wet 0.0158