Su -- Native Conc. Of analyteSample NoDate Method Filename Hcl (ppm) SF6 (ppm)1 3/17/2010 321 C:\CalcmetSample0.00 0.632 3/17/2010 321 C:\CalcmetSample0.00 0.593 3/17/2010 321 C:\CalcmetSample0.19 04 3/17/2010 321 C:\CalcmetSample2.45 0.475 3/17/2010 321 C:\CalcmetSample2.51 0.496 3/17/2010 321 C:\CalcmetSample2.36 0.477 3/17/2010 321 C:\CalcmetSample2.45 0.478 3/17/2010 321 C:\CalcmetSample2.51 0.499 3/17/2010 321 C:\CalcmetSample2.36 0.4710 3/17/2010 321 C:\CalcmetSample2.49 0.4511 3/17/2010 321 C:\CalcmetSample2.50 0.4612 3/17/2010 321 C:\CalcmetSample2.53 0.45Avg. Conc. (ppm)1.860.453Sm --Spiked DataSample NoDate Method Filename Hcl (ppm) SF6 (ppm) Calculated d d21 3/17/2010 321 C:\CalcmetSample10.78 0.63 7.852.938.592 3/17/2010 321 C:\CalcmetSample14.33 0.59 7.856.4842.003 3/17/2010 321 C:\CalcmetSample11.72 0 8.033.6913.624 3/17/2010 321 C:\CalcmetSample13.09 1.34 10.182.918.495 3/17/2010 321 C:\CalcmetSample12.87 1.37 10.232.646.956 3/17/2010 321 C:\CalcmetSample14.14 1.47 10.094.0516.407 3/17/2010 321 C:\CalcmetSample7.90 0.88 10.18(2.28)5.188 3/17/2010 321 C:\CalcmetSample6.49 0.87 10.23(3.74)14.019 3/17/2010 321 C:\CalcmetSample8.09 0.85 10.09(2.00)4.0010 3/17/2010 321 C:\CalcmetSample10.27 0.5 10.210.060.0011 3/17/2010 321 C:\CalcmetSample10.98 1.47 10.220.760.5712 3/17/2010 321 C:\CalcmetSample12.23 1.49 10.251.983.91Avg. Conc. (ppm)11.070.9559.621.4610.31Sm11.07ppm Mean concentration of spiked analyteSu1.86ppm Native concentration of analyteDF5.0% % Dilution Factor (Target < 10%)Cs156.0ppm Cylinder value of spiked gas9.97ppm Cylinder value of tracer gas (SF6)CS 9.62ppm Expected concentration of analyte DF x Cs + Su(1-DF)B1.46Bias at spike level Sm -CSSD0.97EQ 301-2 Standard deviation of the calcualted spike values to actual spike valuesSDM0.2795EQ 301-3 Standard deviation of the meants5.21EQ 301-4 Calculated t-statistict2.201 Critical value two-sided t-distribution at the 95% conf. level at 11 deg. of freedomBias issignificantCF 0.87EQ 301-5 Correction Factor must be between 0.7 to 1.3Data isacceptableRecovery (%) 118.5%70 - 130 %Sm - Su(1-DF)Recovery (%) = DF x CsVALIDATION RUNDate Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 10:34:16 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0005 0 ppm wet 0.0003 0 ppm wet 0.0063/17/2010 10:34:22 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0006 0 ppm wet 0.0003 0 ppm wet 0.00223/17/2010 10:34:28 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0009 0 ppm wet 0.0002 0.2 ppm wet 0.00273/17/2010 10:34:34 C:\CalcmetSamples\Lehigh\20100317\CTS Scan Zero 0 vol-% wet 0.0007 0.1 ppm wet 0.0002 0.2 ppm wet 0.0027Averages 0 0.025 0.1Date Time SpectrumFile Water vapor H2O Unit CompensaResidual Hydrogen chloride HCl Unit CompensaResidual SF6 Unit CompensaResidual3/17/2010 13:41:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00005.SPE 2.59 vol-% wet 0.0028 1.48 ppm wet 0.0012 0.19 ppm wet 0.00293/17/2010 13:41:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00006.SPE 0.85 vol-% wet 0.0005 18.7 ppm wet 0.0003 0.04 ppm wet 0.0023/17/2010 13:41:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00007.SPE 0.39 vol-% wet 0.0003 43.39 ppm wet 0.0004 0.08 ppm wet 0.00113/17/2010 13:41:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00008.SPE 0.15 vol-% wet 0.0004 121.27 ppm wet 0.0003 0 ppm wet 0.00063/17/2010 13:41:49 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00009.SPE 0.03 vol-% wet 0.0005 139.99 ppm wet 0.0002 0.03 ppm wet 0.00123/17/2010 13:41:55 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00010.SPE 0 vol-% wet 0.0019 146.87 ppm wet 0.0003 0.01 ppm wet 0.00133/17/2010 13:42:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00011.SPE 0 vol-% wet 0.0037 151.48 ppm wet 0.0003 0.02 ppm wet 0.00233/17/2010 13:42:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00012.SPE 0 vol-% wet 0.0041 153.8 ppm wet 0.0004 0.01 ppm wet 0.00133/17/2010 13:42:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00013.SPE 0 vol-% wet 0.0044 157.06 ppm wet 0.0004 0.02 ppm wet 0.00163/17/2010 13:44:38 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00014.SPE 0 vol-% wet 0.0063 153.27 ppm wet 0.0006 0.02 ppm wet 0.00073/17/2010 13:44:44 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00015.SPE 0 vol-% wet 0.005 153.35 ppm wet 0.0004 0.02 ppm wet 0.00183/17/2010 13:44:50 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00016.SPE 0 vol-% wet 0.0058 153.37 ppm wet 0.0004 0.02 ppm wet 0.0013/17/2010 13:48:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00017.SPE 0 vol-% wet 0.0057 167.38 ppm wet 0.0005 0.01 ppm wet 0.00063/17/2010 13:51:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00018.SPE 0 vol-% wet 0.0051 145.63 ppm wet 0.0002 0 ppm wet 0.00243/17/2010 13:51:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00019.SPE 0 vol-% wet 0.0006 147.19 ppm wet 0.0002 0.01 ppm wet 0.0023/17/2010 13:51:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00020.SPE 0 vol-% wet 0.0025 147.32 ppm wet 0.0003 0 ppm wet 0.00173/17/2010 13:51:19 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00021.SPE 0 vol-% wet 0.0042 146.75 ppm wet 0.0003 0.02 ppm wet 0.00083/17/2010 13:51:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00022.SPE 0.05 vol-% wet 0.0003 144.03 ppm wet 0.0002 0.01 ppm wet 0.00173/17/2010 13:51:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00023.SPE 0 vol-% wet 0.0029 146.32 ppm wet 0.0003 0 ppm wet 0.0053/17/2010 13:51:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00024.SPE 0 vol-% wet 0.0021 146.3 ppm wet 0.0002 0.02 ppm wet 0.00153/17/2010 13:54:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00025.SPE 0 vol-% wet 0.0001 144.67 ppm wet 0.0001 0 ppm wet 0.00113/17/2010 13:56:53 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00026.SPE 0 vol-% wet 0.0012 145.12 ppm wet 0.0002 0 ppm wet 0.00173/17/2010 13:56:59 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00027.SPE 0 vol-% wet 0.0025 145.71 ppm wet 0.0002 0 ppm wet 0.00123/17/2010 13:57:05 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00028.SPE 0.06 vol-% wet 0.0003 146.25 ppm wet 0.0002 0.06 ppm wet 0.00153/17/2010 13:57:11 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00029.SPE 0 vol-% wet 0.0028 145.99 ppm wet 0.0002 0 ppm wet 0.00143/17/2010 13:57:17 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00030.SPE 0.01 vol-% wet 0.0003 145.44 ppm wet 0.0002 0.03 ppm wet 0.00143/17/2010 13:57:23 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00031.SPE 0 vol-% wet 0.0018 145.89 ppm wet 0.0004 0 ppm wet 0.00183/17/2010 13:57:29 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00032.SPE 0 vol-% wet 0.0025 144.75 ppm wet 0.0003 0 ppm wet 0.00113/17/2010 13:57:35 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00033.SPE 0 vol-% wet 0.0022 144.18 ppm wet 0.0002 0 ppm wet 0.00143/17/2010 13:57:41 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00034.SPE 0 vol-% wet 0.0005 144.73 ppm wet 0.0002 0 ppm wet 0.00173/17/2010 13:57:47 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00035.SPE 0 vol-% wet 0.0024 144.03 ppm wet 0.0002 0.03 ppm wet 0.00233/17/2010 13:57:53 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00036.SPE 0.02 vol-% wet 0.0004 144.19 ppm wet 0.0002 0 ppm wet 0.00143/17/2010 13:57:59 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00037.SPE 0 vol-% wet 0.002 144.4 ppm wet 0.0002 0 ppm wet 0.0033/17/2010 13:58:05 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00038.SPE 0.01 vol-% wet 0.0003 144.23 ppm wet 0.0004 0.02 ppm wet 0.00133/17/2010 13:58:11 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00039.SPE 0 vol-% wet 0.0038 144.57 ppm wet 0.0002 0.02 ppm wet 0.00193/17/2010 13:58:17 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00040.SPE 0 vol-% wet 0.0003 144.83 ppm wet 0.0002 0 ppm wet 0.00243/17/2010 13:58:23 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00041.SPE 0 vol-% wet 0.0012 144.52 ppm wet 0.0002 0 ppm wet 0.00133/17/2010 13:58:28 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00042.SPE 0.02 vol-% wet 0.0004 144.17 ppm wet 0.0003 0.03 ppm wet 0.00173/17/2010 13:58:34 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00043.SPE 0.04 vol-% wet 0.0005 145.94 ppm wet 0.0002 0.01 ppm wet 0.00223/17/2010 13:58:40 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00044.SPE 0.06 vol-% wet 0.0003 144.33 ppm wet 0.0003 0.02 ppm wet 0.0023/17/2010 13:58:46 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00045.SPE 0.01 vol-% wet 0.0002 144.42 ppm wet 0.0002 0 ppm wet 0.00163/17/2010 13:58:52 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00046.SPE 0 vol-% wet 0.0042 144.92 ppm wet 0.0002 0.02 ppm wet 0.00163/17/2010 13:58:58 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00047.SPE 0 vol-% wet 0.0005 144.13 ppm wet 0.0002 0.02 ppm wet 0.00173/17/2010 13:59:04 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00048.SPE 0 vol-% wet 0.001 144.11 ppm wet 0.0002 0.02 ppm wet 0.00183/17/2010 13:59:10 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00049.SPE 0 vol-% wet 0.0032 144.47 ppm wet 0.0003 0 ppm wet 0.00223/17/2010 13:59:16 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL_00050.SPE 0 vol-% wet 0.0036 144.63 ppm wet 0.0003 0.03 ppm wet 0.0011Averages0.01 144.79 0.01Date Time SpectrumFileWater vapor H2O Unit CompensaResidual Hydrogen chloride HCl Unit CompensaResidual SF6 Unit CompensaResidual3/17/2010 14:01:20 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00060.SPE 6.79 vol-% wet 0.0028 3.46 ppm wet 0.0012 0.57 ppm wet 0.00533/17/2010 14:01:26 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00061.SPE 6.79 vol-% wet 0.0027 3.43 ppm wet 0.0012 0.58 ppm wet 0.00543/17/2010 14:01:32 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00062.SPE 6.82 vol-% wet 0.0029 1.95 ppm wet 0.0012 0.61 ppm wet 0.00543/17/2010 14:01:38 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00063.SPE 6.91 vol-% wet 0.0028 5.03 ppm wet 0.0013 0 ppm wet 0.00933/17/2010 14:01:44 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00064.SPE 6.99 vol-% wet 0.0026 3.49 ppm wet 0.0012 0.56 ppm wet 0.00593/17/2010 14:01:50 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00065.SPE 7.1 vol-% wet 0.0028 4.93 ppm wet 0.0011 0 ppm wet 0.01043/17/2010 14:01:56 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00066.SPE 7.14 vol-% wet 0.0028 3.03 ppm wet 0.0013 0.56 ppm wet 0.00533/17/2010 14:02:02 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00067.SPE 7.14 vol-% wet 0.0029 3.19 ppm wet 0.0011 0 ppm wet 0.01083/17/2010 14:05:28 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00068.SPE 6.86 vol-% wet 0.0026 0 ppm wet 0.0014 0.63 ppm wet 0.00513/17/2010 14:06:48 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00069.SPE 6.79 vol-% wet 0.0028 0 ppm wet 0.0012 0.59 ppm wet 0.00573/17/2010 14:07:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00070.SPE 6.75 vol-% wet 0.0027 0.19 ppm wet 0.0011 0 ppm wet 0.00883/17/2010 14:07:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00071.SPE 6.6 vol-% wet 0.0023 1 ppm wet 0.0011 0 ppm wet 0.00913/17/2010 14:07:55 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00072.SPE 6.8 vol-% wet 0.0018 10.35 ppm wet 0.001 0.58 ppm wet 0.00523/17/2010 14:08:01 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00073.SPE 6.68 vol-% wet 0.0017 15.34 ppm wet 0.001 0.52 ppm wet 0.00483/17/2010 14:08:07 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00074.SPE 6.77 vol-% wet 0.0017 18.56 ppm wet 0.001 0.53 ppm wet 0.00523/17/2010 14:08:13 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00075.SPE 6.76 vol-% wet 0.0018 24.04 ppm wet 0.001 0 ppm wet 0.00783/17/2010 14:08:35 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00076.SPE 6.82 vol-% wet 0.0017 23.41 ppm wet 0.001 0.55 ppm wet 0.0053/17/2010 14:09:03 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00077.SPE 6.84 vol-% wet 0.0019 11.85 ppm wet 0.001 0 ppm wet 0.00773/17/2010 14:09:57 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00078.SPE 6.79 vol-% wet 0.0019 10.62 ppm wet 0.001 0 ppm wet 0.00743/17/2010 14:10:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00079.SPE 6.89 vol-% wet 0.0019 10.78 ppm wet 0.0011 1.54 ppm wet 0.0053/17/2010 14:10:13 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00080.SPE 6.84 vol-% wet 0.0019 14.33 ppm wet 0.0009 1.1 ppm wet 0.00663/17/2010 14:10:20 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00081.SPE 6.93 vol-% wet 0.0019 11.72 ppm wet 0.001 1.55 ppm wet 0.00473/17/2010 14:11:50 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00082.SPE 5.8 vol-% wet 0.0024 0 ppm wet 0.0011 0 ppm wet 0.03213/17/2010 14:11:57 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00083.SPE 5.83 vol-% wet 0.0024 0.05 ppm wet 0.001 0 ppm wet 0.03243/17/2010 14:12:04 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00084.SPE 5.86 vol-% wet 0.0023 0 ppm wet 0.001 0 ppm wet 0.03313/17/2010 14:13:33 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00085.SPE 6.36 vol-% wet 0.0024 0 ppm wet 0.0015 1.22 ppm wet 0.0073/17/2010 14:13:41 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00086.SPE 6.09 vol-% wet 0.0024 0 ppm wet 0.0015 1.87 ppm wet 0.00673/17/2010 14:13:47 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00087.SPE 5.97 vol-% wet 0.0024 0 ppm wet 0.0012 1.12 ppm wet 0.00643/17/2010 14:13:54 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00088.SPE 5.93 vol-% wet 0.0023 0 ppm wet 0.0012 1.17 ppm wet 0.00643/17/2010 14:14:09 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00089.SPE 5.82 vol-% wet 0.0025 0 ppm wet 0.0011 1.17 ppm wet 0.00643/17/2010 14:14:19 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00090.SPE 5.89 vol-% wet 0.0024 0 ppm wet 0.0012 1.99 ppm wet 0.00633/17/2010 14:14:25 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00091.SPE 5.79 vol-% wet 0.0024 0 ppm wet 0.0014 0 ppm wet 0.00633/17/2010 14:14:31 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00092.SPE 5.74 vol-% wet 0.0024 0 ppm wet 0.0013 0 ppm wet 0.00623/17/2010 14:14:37 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00093.SPE 5.69 vol-% wet 0.0025 0 ppm wet 0.0012 0 ppm wet 0.00633/17/2010 14:14:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00094.SPE 5.7 vol-% wet 0.0024 0 ppm wet 0.0013 0 ppm wet 0.00673/17/2010 14:14:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike NB1_00095.SPE 5.75 vol-% wet 0.0025 0 ppm wet 0.0011 0 ppm wet 0.007

# HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 10.78 C:\CalcmetSa m 1.12

03/17/10 321 C:\CalcmetSamples\ L 14.33 C:\CalcmetSa m 1.17

03/17/10 321 C:\CalcmetSamples\ L 11.72 C:\CalcmetSa m 1.17

Avg. Conc. (ppm) 12.28 1.153

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 0.00 C:\CalcmetSa m 0.63

03/17/10 321 C:\CalcmetSamples\ L 0.00 C:\CalcmetSa m 0.59

03/17/10 321 C:\CalcmetSamples\ L 0.19 C:\CalcmetSa m 0

Avg. Conc. (ppm) 0.06 0.407

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 12.28 ppm Mean concentration of spiked analyte

Su 0.06 ppm Native concentration of analyte

DF 7.5% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

9.98 ppm Cylinder of tracer gas (SF6)

Ce 10.85 ppm Expected concentration of analyte

Recovery (%) 113.3 % 70 - 130 %Date Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 14:26:50 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00142.SPE 6.88 vol-% wet 0.0027 4.76 ppm wet 0.0054 0.41 ppm wet 0.00723/17/2010 14:27:50 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00143.SPE 6.93 vol-% wet 0.0027 4.71 ppm wet 0.0054 0.42 ppm wet 0.00723/17/2010 14:28:51 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00144.SPE 6.93 vol-% wet 0.0028 4.98 ppm wet 0.0057 0.42 ppm wet 0.00723/17/2010 14:29:51 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00145.SPE 6.94 vol-% wet 0.0027 5.19 ppm wet 0.0056 0.43 ppm wet 0.00723/17/2010 14:30:52 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00146.SPE 6.94 vol-% wet 0.0028 4.91 ppm wet 0.0056 0.43 ppm wet 0.00713/17/2010 14:31:53 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00147.SPE 7.07 vol-% wet 0.0028 4.89 ppm wet 0.0054 0.42 ppm wet 0.00723/17/2010 14:32:53 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00148.SPE 7.08 vol-% wet 0.0028 4.6 ppm wet 0.0054 0.42 ppm wet 0.00713/17/2010 14:33:54 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00149.SPE 6.97 vol-% wet 0.0027 4.92 ppm wet 0.0053 0.41 ppm wet 0.0073/17/2010 14:34:54 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00150.SPE 7.04 vol-% wet 0.0028 4.62 ppm wet 0.0052 0.42 ppm wet 0.00713/17/2010 14:35:55 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00151.SPE 7.13 vol-% wet 0.0029 4.64 ppm wet 0.0053 0.41 ppm wet 0.00713/17/2010 14:36:56 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00152.SPE 7.18 vol-% wet 0.0029 4.82 ppm wet 0.0053 0.42 ppm wet 0.00723/17/2010 14:37:56 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00153.SPE 7.27 vol-% wet 0.003 5.03 ppm wet 0.0054 0.43 ppm wet 0.00733/17/2010 14:38:57 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00154.SPE 7.32 vol-% wet 0.003 5.02 ppm wet 0.0054 0.44 ppm wet 0.00733/17/2010 14:39:58 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00155.SPE 7.36 vol-% wet 0.0029 4.76 ppm wet 0.0052 0.44 ppm wet 0.00743/17/2010 14:40:58 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00156.SPE 7.2 vol-% wet 0.0029 4.77 ppm wet 0.0053 0.44 ppm wet 0.00733/17/2010 14:41:59 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00157.SPE 7.09 vol-% wet 0.0028 4.35 ppm wet 0.0052 0.43 ppm wet 0.00723/17/2010 14:42:59 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00158.SPE 7.03 vol-% wet 0.0028 4.4 ppm wet 0.0052 0.43 ppm wet 0.00723/17/2010 14:44:00 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00159.SPE 7.17 vol-% wet 0.0028 4.46 ppm wet 0.005 0.43 ppm wet 0.00733/17/2010 14:45:01 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00160.SPE 7.21 vol-% wet 0.0029 4.68 ppm wet 0.0052 0.44 ppm wet 0.00743/17/2010 14:46:01 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00161.SPE 7.27 vol-% wet 0.0029 4.73 ppm wet 0.0053 0.46 ppm wet 0.00753/17/2010 14:47:02 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00162.SPE 7.36 vol-% wet 0.0029 4.44 ppm wet 0.0052 0.45 ppm wet 0.00753/17/2010 14:48:02 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00163.SPE 7.24 vol-% wet 0.0029 4.6 ppm wet 0.0054 0.44 ppm wet 0.00753/17/2010 14:49:03 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00164.SPE 7.18 vol-% wet 0.0029 4.5 ppm wet 0.0054 0.45 ppm wet 0.00763/17/2010 14:50:03 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00165.SPE 7.38 vol-% wet 0.003 4.4 ppm wet 0.0054 0.48 ppm wet 0.0083/17/2010 14:51:04 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00166.SPE 7.38 vol-% wet 0.003 4.33 ppm wet 0.0052 0.47 ppm wet 0.0083/17/2010 14:52:05 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00167.SPE 7.46 vol-% wet 0.003 4.37 ppm wet 0.0052 0.48 ppm wet 0.00813/17/2010 14:53:05 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00168.SPE 7.51 vol-% wet 0.0031 4.47 ppm wet 0.0052 0.48 ppm wet 0.00843/17/2010 14:54:06 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00169.SPE 7.29 vol-% wet 0.003 4.37 ppm wet 0.0055 0.48 ppm wet 0.00823/17/2010 14:55:06 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00170.SPE 7.04 vol-% wet 0.0028 4.76 ppm wet 0.0056 0.46 ppm wet 0.0083/17/2010 14:56:07 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00171.SPE 6.95 vol-% wet 0.0028 4.61 ppm wet 0.0055 0.46 ppm wet 0.00783/17/2010 14:57:08 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00172.SPE 7.02 vol-% wet 0.0028 4.17 ppm wet 0.0054 0.47 ppm wet 0.00793/17/2010 14:58:08 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00173.SPE 7.13 vol-% wet 0.0028 4.33 ppm wet 0.0054 0.48 ppm wet 0.00823/17/2010 14:59:09 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00174.SPE 7.05 vol-% wet 0.0028 4.49 ppm wet 0.0054 0.47 ppm wet 0.00793/17/2010 15:00:09 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00175.SPE 6.99 vol-% wet 0.0028 4.51 ppm wet 0.0054 0.47 ppm wet 0.00773/17/2010 15:01:10 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00176.SPE 7.04 vol-% wet 0.0028 4.43 ppm wet 0.0053 0.46 ppm wet 0.00793/17/2010 15:02:11 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00177.SPE 7.12 vol-% wet 0.0029 4.19 ppm wet 0.0053 0.47 ppm wet 0.0083/17/2010 15:03:11 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00178.SPE 7.07 vol-% wet 0.0028 4.16 ppm wet 0.0052 0.47 ppm wet 0.00793/17/2010 15:04:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00179.SPE 7.01 vol-% wet 0.0028 4.53 ppm wet 0.0052 0.46 ppm wet 0.00793/17/2010 15:05:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00180.SPE 7.01 vol-% wet 0.0028 4.08 ppm wet 0.0052 0.47 ppm wet 0.00783/17/2010 15:06:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00181.SPE 6.9 vol-% wet 0.0028 4.09 ppm wet 0.0052 0.46 ppm wet 0.00783/17/2010 15:07:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00182.SPE 6.84 vol-% wet 0.0028 3.99 ppm wet 0.0052 0.46 ppm wet 0.00773/17/2010 15:08:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00183.SPE 6.84 vol-% wet 0.0028 4.31 ppm wet 0.0052 0.47 ppm wet 0.00793/17/2010 15:09:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00184.SPE 6.83 vol-% wet 0.0028 4.15 ppm wet 0.0054 0.47 ppm wet 0.00793/17/2010 15:10:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00185.SPE 6.77 vol-% wet 0.0027 4.15 ppm wet 0.0053 0.46 ppm wet 0.00783/17/2010 15:11:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00186.SPE 6.72 vol-% wet 0.0027 4.11 ppm wet 0.0052 0.46 ppm wet 0.00783/17/2010 15:12:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00187.SPE 6.8 vol-% wet 0.0028 5.53 ppm wet 0.008 0.48 ppm wet 0.00823/17/2010 15:13:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00188.SPE 6.82 vol-% wet 0.0028 5.66 ppm wet 0.0077 0.5 ppm wet 0.00843/17/2010 15:14:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00189.SPE 6.67 vol-% wet 0.0026 4.84 ppm wet 0.0063 0.47 ppm wet 0.0083/17/2010 15:15:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00190.SPE 6.58 vol-% wet 0.0026 5.07 ppm wet 0.0064 0.46 ppm wet 0.00773/17/2010 15:16:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00191.SPE 6.62 vol-% wet 0.0026 4.75 ppm wet 0.0065 0.46 ppm wet 0.00783/17/2010 15:17:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00192.SPE 6.61 vol-% wet 0.0026 5.14 ppm wet 0.0065 0.46 ppm wet 0.00763/17/2010 15:18:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00193.SPE 6.63 vol-% wet 0.0026 4.16 ppm wet 0.0055 0.43 ppm wet 0.00723/17/2010 15:19:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00194.SPE 6.64 vol-% wet 0.0025 3.09 ppm wet 0.0049 0.42 ppm wet 0.00693/17/2010 15:20:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00195.SPE 6.74 vol-% wet 0.0026 3.16 ppm wet 0.0049 0.43 ppm wet 0.00723/17/2010 15:21:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00196.SPE 6.75 vol-% wet 0.0027 3.74 ppm wet 0.0049 0.43 ppm wet 0.00733/17/2010 15:22:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00197.SPE 6.78 vol-% wet 0.0028 3.09 ppm wet 0.0047 0.43 ppm wet 0.00733/17/2010 15:23:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00198.SPE 6.78 vol-% wet 0.0026 2.75 ppm wet 0.0047 0.43 ppm wet 0.00733/17/2010 15:24:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00199.SPE 6.73 vol-% wet 0.0026 2.74 ppm wet 0.0047 0.42 ppm wet 0.00733/17/2010 15:25:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00200.SPE 6.77 vol-% wet 0.0027 2.88 ppm wet 0.0047 0.43 ppm wet 0.00733/17/2010 15:26:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00201.SPE 6.82 vol-% wet 0.0026 2.85 ppm wet 0.0047 0.45 ppm wet 0.00753/17/2010 15:27:26 C:\CalcmetSamples\Lehigh 210158\20100317\Run 1_00202.SPE 6.8 vol-% wet 0.0027 2.91 ppm wet 0.0047 0.43 ppm wet 0.0075Averages4.36

# HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 13.09 C:\CalcmetSa m 1.34

03/17/10 321 C:\CalcmetSamples\ L 12.87 C:\CalcmetSa m 1.37

03/17/10 321 C:\CalcmetSamples\ L 14.14 C:\CalcmetSa m 1.47

Avg. Conc. (ppm) 13.37 1.393

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 2.88 C:\CalcmetSa m 0.43

03/17/10 321 C:\CalcmetSamples\ L 2.85 C:\CalcmetSa m 0.45

03/17/10 321 C:\CalcmetSamples\ L 2.91 C:\CalcmetSa m 0.43

Avg. Conc. (ppm) 2.88 0.437

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 13.37 ppm Mean concentration of spiked analyte

Su 2.88 ppm Native concentration of analyte

DF 9.6% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

9.98 ppm Cylinder of tracer gas (SF6)

Ce 16.43 ppm Expected concentration of analyte

Recovery (%) 77.9 % 70 - 130 %Date Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 15:36:21 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00203.SPE 6.37 vol-% wet 0.0025 2.3 ppm wet 0.0045 0.41 ppm wet 0.00713/17/2010 15:36:30 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00204.SPE 6.36 vol-% wet 0.0025 2.4 ppm wet 0.0043 0.42 ppm wet 0.00713/17/2010 15:36:38 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00205.SPE 6.35 vol-% wet 0.0026 13.09 ppm wet 0.0045 0.4 ppm wet 0.00723/17/2010 15:37:14 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00206.SPE 6.3 vol-% wet 0.0025 12.87 ppm wet 0.0043 0.43 ppm wet 0.00673/17/2010 15:37:17 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00207.SPE 6.33 vol-% wet 0.0028 14.14 ppm wet 0.0045 0.36 ppm wet 0.00723/17/2010 15:37:19 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00208.SPE 6.24 vol-% wet 0.0023 11.56 ppm wet 0.0044 1.34 ppm wet 0.00743/17/2010 15:37:22 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00209.SPE 6.31 vol-% wet 0.0026 8.03 ppm wet 0.0048 1.37 ppm wet 0.00773/17/2010 15:37:24 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00210.SPE 6.32 vol-% wet 0.0027 3.52 ppm wet 0.0044 1.47 ppm wet 0.00753/17/2010 15:37:26 C:\CalcmetSamples\Lehigh 210158\20100317\spike na1_00211.SPE 6.32 vol-% wet 0.0021 1.81 ppm wet 0.0045 0.47 ppm wet 0.0073Date Time SpectrumFile Water vapor H2O Unit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 15:52:48 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00310.SPE 6.35 vol-% wet 0.0026 1.8 ppm wet 0.0051 0.95 ppm wet 0.00773/17/2010 15:53:48 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00311.SPE 6.5 vol-% wet 0.0027 1.92 ppm wet 0.0053 0.51 ppm wet 0.00833/17/2010 15:54:49 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00312.SPE 6.54 vol-% wet 0.0026 2.06 ppm wet 0.0054 0.5 ppm wet 0.00833/17/2010 15:55:50 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00313.SPE 6.52 vol-% wet 0.0026 2.24 ppm wet 0.0055 0.5 ppm wet 0.00853/17/2010 15:56:50 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00314.SPE 6.49 vol-% wet 0.0026 2.13 ppm wet 0.0057 0.51 ppm wet 0.00853/17/2010 15:57:51 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00315.SPE 6.47 vol-% wet 0.0027 2.26 ppm wet 0.0058 0.51 ppm wet 0.00853/17/2010 15:58:51 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00316.SPE 6.43 vol-% wet 0.0026 2.47 ppm wet 0.0057 0.5 ppm wet 0.00843/17/2010 15:59:52 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00317.SPE 6.4 vol-% wet 0.0026 2.29 ppm wet 0.0057 0.5 ppm wet 0.00843/17/2010 16:00:53 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00318.SPE 6.34 vol-% wet 0.0027 2.29 ppm wet 0.0057 0.5 ppm wet 0.00833/17/2010 16:01:53 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00319.SPE 6.31 vol-% wet 0.0026 2.52 ppm wet 0.0059 0.5 ppm wet 0.00843/17/2010 16:02:54 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00320.SPE 6.27 vol-% wet 0.0026 2.55 ppm wet 0.0059 0.51 ppm wet 0.00853/17/2010 16:03:54 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00321.SPE 6.29 vol-% wet 0.0026 2.61 ppm wet 0.006 0.52 ppm wet 0.00863/17/2010 16:04:55 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00322.SPE 6.38 vol-% wet 0.0026 2.57 ppm wet 0.0059 0.52 ppm wet 0.00843/17/2010 16:05:56 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00323.SPE 6.4 vol-% wet 0.0026 2.42 ppm wet 0.0057 0.51 ppm wet 0.00843/17/2010 16:06:56 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00324.SPE 6.44 vol-% wet 0.0026 2.31 ppm wet 0.0057 0.49 ppm wet 0.00833/17/2010 16:07:57 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00325.SPE 6.49 vol-% wet 0.0026 2.48 ppm wet 0.0057 0.49 ppm wet 0.00813/17/2010 16:08:57 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00326.SPE 6.51 vol-% wet 0.0026 2.39 ppm wet 0.0056 0.49 ppm wet 0.00813/17/2010 16:09:58 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00327.SPE 6.57 vol-% wet 0.0027 2.05 ppm wet 0.0054 0.48 ppm wet 0.0083/17/2010 16:10:59 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00328.SPE 6.63 vol-% wet 0.0028 2.32 ppm wet 0.0054 0.49 ppm wet 0.00813/17/2010 16:11:59 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00329.SPE 6.76 vol-% wet 0.0028 2.31 ppm wet 0.0055 0.49 ppm wet 0.00813/17/2010 16:13:00 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00330.SPE 6.87 vol-% wet 0.0028 2.39 ppm wet 0.0055 0.48 ppm wet 0.0083/17/2010 16:14:00 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00331.SPE 6.9 vol-% wet 0.0028 2.21 ppm wet 0.0056 0.48 ppm wet 0.00813/17/2010 16:15:01 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00332.SPE 7.01 vol-% wet 0.0029 2.21 ppm wet 0.0053 0.49 ppm wet 0.00793/17/2010 16:16:01 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00333.SPE 7.1 vol-% wet 0.0029 2.08 ppm wet 0.0052 0.49 ppm wet 0.00793/17/2010 16:17:02 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00334.SPE 7.17 vol-% wet 0.0029 1.95 ppm wet 0.0052 0.48 ppm wet 0.00793/17/2010 16:18:03 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00335.SPE 7.25 vol-% wet 0.003 1.96 ppm wet 0.005 0.49 ppm wet 0.00793/17/2010 16:19:03 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00336.SPE 7.32 vol-% wet 0.003 1.87 ppm wet 0.005 0.48 ppm wet 0.00773/17/2010 16:20:04 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00337.SPE 7.42 vol-% wet 0.0031 1.74 ppm wet 0.005 0.48 ppm wet 0.00783/17/2010 16:21:04 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00338.SPE 7.57 vol-% wet 0.0033 1.66 ppm wet 0.005 0.46 ppm wet 0.00763/17/2010 16:22:05 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00339.SPE 11.18 vol-% wet 0.003 5.37 ppm wet 0.0043 0.29 ppm wet 0.00533/17/2010 16:23:06 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00340.SPE 12.2 vol-% wet 0.0029 9.19 ppm wet 0.005 0.16 ppm wet 0.00613/17/2010 16:24:06 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00341.SPE 7.67 vol-% wet 0.0028 3.56 ppm wet 0.0051 0.42 ppm wet 0.0073/17/2010 16:25:07 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00342.SPE 7.55 vol-% wet 0.003 2.27 ppm wet 0.0051 0.45 ppm wet 0.00733/17/2010 16:26:07 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00343.SPE 7.37 vol-% wet 0.0029 2 ppm wet 0.0052 0.46 ppm wet 0.00753/17/2010 16:27:08 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00344.SPE 7.26 vol-% wet 0.0029 1.93 ppm wet 0.0053 0.48 ppm wet 0.00763/17/2010 16:28:09 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00345.SPE 7.23 vol-% wet 0.0029 1.82 ppm wet 0.0051 0.47 ppm wet 0.00773/17/2010 16:29:09 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00346.SPE 7.16 vol-% wet 0.0029 2.18 ppm wet 0.0053 0.48 ppm wet 0.00793/17/2010 16:30:10 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00347.SPE 7.1 vol-% wet 0.0029 2.05 ppm wet 0.0055 0.48 ppm wet 0.00773/17/2010 16:31:10 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00348.SPE 7.06 vol-% wet 0.0029 1.98 ppm wet 0.0053 0.48 ppm wet 0.00793/17/2010 16:32:11 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00349.SPE 7.03 vol-% wet 0.0028 2.17 ppm wet 0.0057 0.48 ppm wet 0.00793/17/2010 16:33:12 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00350.SPE 6.95 vol-% wet 0.0028 2.16 ppm wet 0.0057 0.47 ppm wet 0.00793/17/2010 16:34:12 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00351.SPE 6.88 vol-% wet 0.0028 2.43 ppm wet 0.0057 0.47 ppm wet 0.00783/17/2010 16:35:13 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00352.SPE 6.84 vol-% wet 0.0028 2.05 ppm wet 0.0057 0.47 ppm wet 0.00773/17/2010 16:36:13 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00353.SPE 6.75 vol-% wet 0.0027 2.22 ppm wet 0.0058 0.47 ppm wet 0.00763/17/2010 16:37:14 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00354.SPE 6.68 vol-% wet 0.0027 2.19 ppm wet 0.0057 0.47 ppm wet 0.00773/17/2010 16:38:15 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00355.SPE 6.7 vol-% wet 0.0027 2 ppm wet 0.0056 0.47 ppm wet 0.00783/17/2010 16:39:15 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00356.SPE 6.69 vol-% wet 0.0027 2.25 ppm wet 0.0058 0.46 ppm wet 0.00783/17/2010 16:40:16 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00357.SPE 6.67 vol-% wet 0.0026 2.34 ppm wet 0.0059 0.48 ppm wet 0.00783/17/2010 16:41:16 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00358.SPE 6.65 vol-% wet 0.0026 2.43 ppm wet 0.0059 0.46 ppm wet 0.00793/17/2010 16:42:17 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00359.SPE 6.62 vol-% wet 0.0027 2.3 ppm wet 0.0058 0.46 ppm wet 0.00773/17/2010 16:43:18 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00360.SPE 6.56 vol-% wet 0.0026 2.38 ppm wet 0.0059 0.45 ppm wet 0.00773/17/2010 16:44:18 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00361.SPE 6.51 vol-% wet 0.0026 2.3 ppm wet 0.0058 0.46 ppm wet 0.00773/17/2010 16:45:19 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00362.SPE 6.51 vol-% wet 0.0026 2.29 ppm wet 0.0057 0.47 ppm wet 0.00783/17/2010 16:46:19 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00363.SPE 6.49 vol-% wet 0.0026 2.42 ppm wet 0.0059 0.47 ppm wet 0.00783/17/2010 16:47:20 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00364.SPE 6.45 vol-% wet 0.0026 2.47 ppm wet 0.0059 0.48 ppm wet 0.00793/17/2010 16:48:20 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00365.SPE 6.43 vol-% wet 0.0026 2.14 ppm wet 0.0057 0.47 ppm wet 0.00783/17/2010 16:49:21 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00366.SPE 6.47 vol-% wet 0.0026 2.23 ppm wet 0.0057 0.46 ppm wet 0.00793/17/2010 16:50:22 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00367.SPE 6.44 vol-% wet 0.0026 2.3 ppm wet 0.0058 0.47 ppm wet 0.00793/17/2010 16:51:22 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00368.SPE 6.39 vol-% wet 0.0026 2.45 ppm wet 0.006 0.47 ppm wet 0.00783/17/2010 16:52:23 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00369.SPE 6.37 vol-% wet 0.0026 2.51 ppm wet 0.0059 0.49 ppm wet 0.00813/17/2010 16:53:23 C:\CalcmetSamples\Lehigh 210158\20100317\run 2_00370.SPE 6.37 vol-% wet 0.0026 2.36 ppm wet 0.0059 0.47 ppm wet 0.008Averages2.41

# HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 7.90 C:\CalcmetSa m 0.88

03/17/10 321 C:\CalcmetSamples\ L 6.49 C:\CalcmetSa m 0.87

03/17/10 321 C:\CalcmetSamples\ L 8.09 C:\CalcmetSa m 0.85

Avg. Conc. (ppm) 7.49 0.867

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 2.45 C:\CalcmetSa m 0.47

03/17/10 321 C:\CalcmetSamples\ L 2.51 C:\CalcmetSa m 0.49

03/17/10 321 C:\CalcmetSamples\ L 2.36 C:\CalcmetSa m 0.47

Avg. Conc. (ppm) 2.44 0.477

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 7.49 ppm Mean concentration of spiked analyte

Su 2.44 ppm Native concentration of analyte

DF 3.9% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

9.98 ppm Cylinder of tracer gas (SF6)

Ce 7.98 ppm Expected concentration of analyte

Recovery (%) 91.4 % 70 - 130 %Date Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 17:02:01 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00397.SPE 6.62 vol-% wet 0.0029 1.74 ppm wet 0.005 0.88 ppm wet 0.00583/17/2010 17:02:04 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00398.SPE 6.56 vol-% wet 0.0028 1.1 ppm wet 0.0053 0.87 ppm wet 0.00633/17/2010 17:02:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00399.SPE 6.55 vol-% wet 0.0023 0.57 ppm wet 0.0052 0.85 ppm wet 0.00683/17/2010 17:02:09 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00400.SPE 6.55 vol-% wet 0.0025 1.74 ppm wet 0.0046 0.83 ppm wet 0.00613/17/2010 17:02:11 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00401.SPE 6.54 vol-% wet 0.0026 1.12 ppm wet 0.0048 1.83 ppm wet 0.00543/17/2010 17:02:14 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00402.SPE 6.53 vol-% wet 0.0024 2.41 ppm wet 0.0049 1.82 ppm wet 0.00663/17/2010 17:02:17 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00403.SPE 6.5 vol-% wet 0.0028 7.9 ppm wet 0.0051 1.89 ppm wet0.00633/17/2010 17:02:19 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00404.SPE 6.54 vol-% wet 0.0027 6.49 ppm wet 0.0045 1.85 ppm wet 0.00683/17/2010 17:02:22 C:\CalcmetSamples\Lehigh 210158\20100317\Spike After run 2_00405.SPE 6.46 vol-% wet 0.0026 8.09 ppm wet 0.005 1.85 ppm wet 0.0059Date Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 17:17:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00417.SPE 9.11 vol-% wet 0.0027 2.24 ppm wet 0.005 0.48 ppm wet 0.00493/17/2010 17:18:12 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00418.SPE 9.1 vol-% wet 0.0027 2.24 ppm wet 0.005 0.48 ppm wet 0.00473/17/2010 17:19:13 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00419.SPE 9.07 vol-% wet 0.0027 2.22 ppm wet 0.005 0.47 ppm wet 0.00473/17/2010 17:20:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00420.SPE 9.06 vol-% wet 0.0027 2.32 ppm wet 0.005 0.47 ppm wet 0.00473/17/2010 17:21:14 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00421.SPE 8.98 vol-% wet 0.0027 2.42 ppm wet 0.0052 0.47 ppm wet 0.00473/17/2010 17:22:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00422.SPE 8.99 vol-% wet 0.0027 2.36 ppm wet 0.0052 0.47 ppm wet 0.00473/17/2010 17:23:15 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00423.SPE 8.97 vol-% wet 0.0027 2.33 ppm wet 0.0051 0.46 ppm wet 0.00463/17/2010 17:24:16 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00424.SPE 8.99 vol-% wet 0.0027 2.45 ppm wet 0.0052 0.47 ppm wet 0.00473/17/2010 17:25:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00425.SPE 8.99 vol-% wet 0.0027 2.35 ppm wet 0.0052 0.47 ppm wet 0.00463/17/2010 17:26:17 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00426.SPE 8.99 vol-% wet 0.0027 2.26 ppm wet 0.0051 0.48 ppm wet 0.00463/17/2010 17:27:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00427.SPE 8.98 vol-% wet 0.0027 2.3 ppm wet 0.0051 0.47 ppm wet 0.00463/17/2010 17:28:18 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00428.SPE 8.96 vol-% wet 0.0027 2.16 ppm wet 0.0051 0.46 ppm wet 0.00453/17/2010 17:29:19 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00429.SPE 8.98 vol-% wet 0.0027 2.01 ppm wet 0.005 0.46 ppm wet 0.00463/17/2010 17:30:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00430.SPE 8.96 vol-% wet 0.0026 2.03 ppm wet 0.005 0.46 ppm wet 0.00443/17/2010 17:31:20 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00431.SPE 8.98 vol-% wet 0.0026 2.19 ppm wet 0.005 0.47 ppm wet 0.00463/17/2010 17:32:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00432.SPE 9.02 vol-% wet 0.0026 1.93 ppm wet 0.0048 0.46 ppm wet 0.00453/17/2010 17:33:21 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00433.SPE 9.07 vol-% wet 0.0026 1.87 ppm wet 0.0048 0.45 ppm wet 0.00463/17/2010 17:34:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00434.SPE 9.06 vol-% wet 0.0027 1.87 ppm wet 0.005 0.46 ppm wet 0.00473/17/2010 17:35:22 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00435.SPE 9.02 vol-% wet 0.0026 1.97 ppm wet 0.005 0.47 ppm wet 0.00463/17/2010 17:36:23 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00436.SPE 9.03 vol-% wet 0.0026 2.11 ppm wet 0.0051 0.47 ppm wet 0.00473/17/2010 17:37:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00437.SPE 9.01 vol-% wet 0.0026 2.13 ppm wet 0.0052 0.47 ppm wet 0.00483/17/2010 17:38:24 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00438.SPE 9.98 vol-% wet 0.0027 2.16 ppm wet 0.005 0.47 ppm wet 0.00463/17/2010 17:39:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00439.SPE 9.97 vol-% wet 0.0027 2.28 ppm wet 0.0052 0.48 ppm wet 0.00473/17/2010 17:40:25 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00440.SPE 9.99 vol-% wet 0.0026 2.21 ppm wet 0.0051 0.48 ppm wet 0.00473/17/2010 17:41:26 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00441.SPE 9.92 vol-% wet 0.0026 2.4 ppm wet 0.0053 0.47 ppm wet 0.00453/17/2010 17:42:27 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00442.SPE 9.88 vol-% wet 0.0026 2.32 ppm wet 0.0051 0.46 ppm wet 0.00443/17/2010 17:43:27 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00443.SPE 9.9 vol-% wet 0.0027 2.31 ppm wet 0.0051 0.46 ppm wet 0.00463/17/2010 17:44:28 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00444.SPE 9.9 vol-% wet 0.0027 2.11 ppm wet 0.005 0.48 ppm wet 0.00473/17/2010 17:45:28 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00445.SPE 9.9 vol-% wet 0.0026 2.1 ppm wet 0.005 0.48 ppm wet 0.00473/17/2010 17:46:29 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00446.SPE 9.92 vol-% wet 0.0027 2.29 ppm wet 0.0051 0.48 ppm wet 0.00473/17/2010 17:47:30 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00447.SPE 9.94 vol-% wet 0.0026 2.27 ppm wet 0.0054 0.5 ppm wet 0.00473/17/2010 17:48:30 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00448.SPE 9.9 vol-% wet 0.0026 2.37 ppm wet 0.0054 0.47 ppm wet 0.00483/17/2010 17:49:31 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00449.SPE 9.86 vol-% wet 0.0026 2.35 ppm wet 0.0053 0.47 ppm wet 0.00463/17/2010 17:50:31 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00450.SPE 9.84 vol-% wet 0.0026 2.29 ppm wet 0.0052 0.47 ppm wet 0.00453/17/2010 17:51:32 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00451.SPE 9.85 vol-% wet 0.0026 2.46 ppm wet 0.0052 0.48 ppm wet 0.00463/17/2010 17:52:33 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00452.SPE 9.8 vol-% wet 0.0027 2.27 ppm wet 0.005 0.46 ppm wet 0.00453/17/2010 17:53:33 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00453.SPE 9.79 vol-% wet 0.0026 2.08 ppm wet 0.0049 0.47 ppm wet 0.00453/17/2010 17:54:34 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00454.SPE 9.75 vol-% wet 0.0026 2.05 ppm wet 0.0049 0.46 ppm wet 0.00453/17/2010 17:55:34 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00455.SPE 9.75 vol-% wet 0.0026 2.24 ppm wet 0.005 0.47 ppm wet 0.00473/17/2010 17:56:35 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00456.SPE 9.78 vol-% wet 0.0026 2.08 ppm wet 0.0049 0.48 ppm wet 0.00463/17/2010 17:57:36 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00457.SPE 9.84 vol-% wet 0.0026 1.99 ppm wet 0.0049 0.47 ppm wet 0.00463/17/2010 17:58:36 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00458.SPE 9.91 vol-% wet 0.0027 2.03 ppm wet 0.005 0.46 ppm wet 0.00453/17/2010 17:59:37 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00459.SPE 9.88 vol-% wet 0.0027 2.03 ppm wet 0.0051 0.46 ppm wet 0.00463/17/2010 18:00:37 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00460.SPE 9.88 vol-% wet 0.0026 2 ppm wet 0.0052 0.46 ppm wet 0.00453/17/2010 18:01:38 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00461.SPE 9.9 vol-% wet 0.0026 1.84 ppm wet 0.0052 0.46 ppm wet 0.00453/17/2010 18:02:39 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00462.SPE 9.86 vol-% wet 0.0027 2.11 ppm wet 0.0053 0.46 ppm wet 0.00463/17/2010 18:03:39 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00463.SPE 9.87 vol-% wet 0.0026 2.06 ppm wet 0.005 0.47 ppm wet 0.00463/17/2010 18:04:40 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00464.SPE 9.85 vol-% wet 0.0027 1.95 ppm wet 0.005 0.47 ppm wet 0.00473/17/2010 18:05:41 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00465.SPE 9.86 vol-% wet 0.0027 2 ppm wet 0.0049 0.45 ppm wet 0.00463/17/2010 18:06:41 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00466.SPE 9.8 vol-% wet 0.0027 2.04 ppm wet 0.005 0.46 ppm wet 0.00453/17/2010 18:07:42 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00467.SPE 10.74 vol-% wet 0.0027 2.32 ppm wet 0.0049 0.47 ppm wet 0.00453/17/2010 18:08:43 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00468.SPE 10.84 vol-% wet 0.0033 2.21 ppm wet 0.0047 0.45 ppm wet 0.00453/17/2010 18:09:43 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00469.SPE 10.77 vol-% wet 0.0032 2.33 ppm wet 0.0048 0.44 ppm wet 0.00453/17/2010 18:10:44 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00470.SPE 10.74 vol-% wet 0.0032 2.65 ppm wet 0.005 0.45 ppm wet 0.00463/17/2010 18:11:44 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00471.SPE 10.75 vol-% wet 0.0031 2.21 ppm wet 0.0047 0.43 ppm wet 0.00463/17/2010 18:12:45 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00472.SPE 10.72 vol-% wet 0.0032 2.51 ppm wet 0.0047 0.43 ppm wet 0.00453/17/2010 18:13:46 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00473.SPE 10.68 vol-% wet 0.0031 2.54 ppm wet 0.0049 0.45 ppm wet 0.00463/17/2010 18:14:46 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00474.SPE 10.68 vol-% wet 0.0031 2.61 ppm wet 0.0049 0.46 ppm wet 0.00443/17/2010 18:15:47 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00475.SPE 10.69 vol-% wet 0.0031 2.49 ppm wet 0.0048 0.45 ppm wet 0.00453/17/2010 18:16:47 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00476.SPE 10.71 vol-% wet 0.0031 2.5 ppm wet 0.0049 0.46 ppm wet 0.00463/17/2010 18:17:48 C:\CalcmetSamples\Lehigh 210158\20100317\Run 3_00477.SPE 10.71 vol-% wet 0.0032 2.53 ppm wet 0.0049 0.45 ppm wet 0.0047Averages2.22Date Time SpectrumFile Water vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 18:20:37 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00478.SPE5.54 vol-% wet 0.0026 4.05 ppm wet 0.005 0.47 ppm wet 0.00453/17/2010 18:20:43 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00479.SPE6.52 vol-% wet 0.0023 6.75 ppm wet 0.0051 0.47 ppm wet 0.00463/17/2010 18:20:49 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00480.SPE5.55 vol-% wet 0.0026 4.19 ppm wet 0.005 0.47 ppm wet 0.00463/17/2010 18:21:29 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00481.SPE6.2 vol-% wet 0.0021 6.21 ppm wet 0.0046 0.39 ppm wet 0.00423/17/2010 18:21:35 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00482.SPE5.91 vol-% wet 0.0019 7.87 ppm wet 0.0037 0.31 ppm wet 0.00333/17/2010 18:21:41 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00483.SPE5.78 vol-% wet 0.0021 10.47 ppm wet 0.0035 0.29 ppm wet 0.00263/17/2010 18:21:47 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00484.SPE5.74 vol-% wet 0.0019 10.27 ppm wet 0.0034 0.45 ppm wet 0.00363/17/2010 18:21:53 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00485.SPE5.72 vol-% wet 0.0019 10.98 ppm wet 0.0034 0.31 ppm wet 0.00313/17/2010 18:21:59 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00486.SPE5.58 vol-% wet 0.0019 12.23 ppm wet 0.0037 0.28 ppm wet 0.00293/17/2010 18:22:05 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00487.SPE5.62 vol-% wet 0.002 12.93 ppm wet 0.0035 0.31 ppm wet 0.00323/17/2010 18:22:11 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00488.SPE5.57 vol-% wet 0.0019 12.39 ppm wet 0.0036 0.28 ppm wet 0.00283/17/2010 18:22:17 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00489.SPE5.48 vol-% wet 0.002 11.09 ppm wet 0.0036 0.3 ppm wet 0.00313/17/2010 18:22:23 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00490.SPE5.57 vol-% wet 0.0019 15.66 ppm wet 0.0034 0.3 ppm wet 0.0033/17/2010 18:22:55 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00491.SPE6.17 vol-% wet 0.0021 1.37 ppm wet 0.0055 0.47 ppm wet 0.00433/17/2010 18:23:00 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00492.SPE6.21 vol-% wet 0.002 2.23 ppm wet 0.0057 0.5 ppm wet 0.00513/17/2010 18:23:06 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00493.SPE6.38 vol-% wet 0.0023 3.89 ppm wet 0.0054 1.47 ppm wet 0.00523/17/2010 18:23:12 C:\CalcmetSamples\Lehigh 210158\20100317\Spike Run 3 spike after_00494.SPE6.42 vol-% wet 0.0022 1.27 ppm wet 0.0051 1.49 ppm wet 0.0044

# HCL Lehigh

Sm --Spiked Data

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 10.27 C:\CalcmetSa m 0.5

03/17/10 321 C:\CalcmetSamples\ L 10.98 C:\CalcmetSa m 1.47

03/17/10 321 C:\CalcmetSamples\ L 12.23 C:\CalcmetSa m 1.49

Avg. Conc. (ppm) 11.16 1.153

Su -- Native Conc. Of analyte

Date Method Filename HCl(ppm) SF6 (ppm)

03/17/10 321 C:\CalcmetSamples\ L 2.49 C:\CalcmetSa m 0.45

03/17/10 321 C:\CalcmetSamples\ L 2.50 C:\CalcmetSa m 0.46

03/17/10 321 C:\CalcmetSamples\ L 2.53 C:\CalcmetSa m 0.45

Avg. Conc. (ppm) 2.51 0.453

Sm - Su(1-DF)

Recovery (%) = DF x Cs

Ce = DF x Cs + Su(1-DF)

Sm 11.16 ppm Mean concentration of spiked analyte

Su 2.51 ppm Native concentration of analyte

DF 7.0% % Dilution Factor (Target < 10%)

Cs 144.2 ppm Cylinder of spiked gas

9.98 ppm Cylinder of tracer gas (SF6)

Ce 12.45 ppm Expected concentration of analyte

Recovery (%) 87.3 % 70 - 130 %Date Time SpectrumFileWater vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 18:27:03 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00520.SPE 2.46 vol-% wet 0.0007 99.83 ppm wet 0.00060.05 ppm wet 0.00263/17/2010 18:27:09 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00521.SPE 2.41 vol-% wet 0.0006 96.85 ppm wet 0.00060.02 ppm wet 0.00173/17/2010 18:27:15 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00522.SPE 2.41 vol-% wet 0.0005 95.01 ppm wet 0.00060 ppm wet 0.0023/17/2010 18:27:21 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00523.SPE 2.36 vol-% wet 0.0005 95.91 ppm wet 0.00040 ppm wet 0.00163/17/2010 18:27:27 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00524.SPE 2.3 vol-% wet 0.0005 98.38 ppm wet 0.0005 0.03 ppm wet 0.00113/17/2010 18:27:33 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00525.SPE 2.34 vol-% wet 0.0005 100.69 ppm wet 0.0005 0 ppm wet 0.00183/17/2010 18:27:39 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00526.SPE 2.23 vol-% wet 0.0004 105.21 ppm wet 0.0007 0 ppm wet 0.00443/17/2010 18:27:45 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00527.SPE 2.19 vol-% wet 0.0005 112.42 ppm wet 0.0006 0 ppm wet 0.0053/17/2010 18:27:51 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00528.SPE 2.04 vol-% wet 0.0004 117.84 ppm wet 0.0005 0 ppm wet 0.00173/17/2010 18:27:57 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00529.SPE 2.08 vol-% wet 0.0005 125.33 ppm wet 0.0006 0 ppm wet 0.00313/17/2010 18:28:03 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00530.SPE 2.07 vol-% wet 0.0006 130.76 ppm wet 0.0006 0 ppm wet 0.00153/17/2010 18:28:09 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00531.SPE 2.07 vol-% wet 0.0005 128.73 ppm wet 0.0006 0 ppm wet 0.00223/17/2010 18:28:15 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00532.SPE 2.05 vol-% wet 0.0004 125.91 ppm wet 0.0006 0 ppm wet 0.00183/17/2010 18:28:21 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00533.SPE 1.95 vol-% wet 0.0004 121.97 ppm wet 0.0008 0 ppm wet 0.00173/17/2010 18:28:26 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00534.SPE 1.91 vol-% wet 0.0003 122.56 ppm wet 0.0006 0 ppm wet 0.00223/17/2010 18:28:32 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00535.SPE 1.92 vol-% wet 0.0005 128.15 ppm wet 0.0005 0 ppm wet 0.00393/17/2010 18:28:38 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00536.SPE 1.96 vol-% wet 0.0004 144.06 ppm wet 0.0006 0 ppm wet 0.00153/17/2010 18:28:44 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00537.SPE 1.86 vol-% wet 0.0005 144.41 ppm wet 0.0005 0 ppm wet 0.00173/17/2010 18:28:50 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00538.SPE 1.85 vol-% wet 0.0004 142.54 ppm wet 0.0006 0 ppm wet 0.00333/17/2010 18:28:56 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00539.SPE 1.57 vol-% wet 0.0007 144.91 ppm wet 0.0008 0 ppm wet 0.00163/17/2010 18:29:02 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00540.SPE 1.46 vol-% wet 0.0007 144.72 ppm wet 0.0006 0 ppm wet 0.00813/17/2010 18:29:08 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00541.SPE 1.51 vol-% wet 0.0007 145.61 ppm wet 0.0007 0 ppm wet 0.00263/17/2010 18:29:14 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Scan HCL Run 3 after_00542.SPE 1.46 vol-% wet 0.0007 142.04 ppm wet 0.0006 0 ppm wet 0.002Averages144.04Date Time SpectrumFileWater vapoUnit CompensaResidual HydrogencUnit CompensaResidual SF6 Unit CompensaResidual3/17/2010 18:39:01 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00578.SPE 0 vol-% wet 0.0236 0 ppm wet 0.0013 0.07 ppm wet 0.00543/17/2010 18:39:07 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00579.SPE 0 vol-% wet 0.0189 0 ppm wet 0.0012 0.08 ppm wet 0.00413/17/2010 18:39:13 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00580.SPE 0 vol-% wet 0.013 0 ppm wet 0.0013 0.1 ppm wet 0.00863/17/2010 18:39:19 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00581.SPE 0 vol-% wet 0.0236 0 ppm wet 0.0014 0.08 ppm wet 0.00513/17/2010 18:39:25 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00582.SPE 0 vol-% wet 0.0227 0 ppm wet 0.0013 0.08 ppm wet 0.00533/17/2010 18:39:31 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00583.SPE 0 vol-% wet 0.0254 0 ppm wet 0.0014 0.09 ppm wet 0.00623/17/2010 18:39:37 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00584.SPE 0 vol-% wet 0.017 0 ppm wet 0.0015 0.08 ppm wet 0.00723/17/2010 18:39:43 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00585.SPE 0 vol-% wet 0.011 0 ppm wet 0.0015 0.06 ppm wet 0.00473/17/2010 18:39:49 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00586.SPE 0 vol-% wet 0.0258 0 ppm wet 0.0013 0.1 ppm wet 0.00813/17/2010 18:39:54 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00587.SPE 0 vol-% wet 0.0192 0 ppm wet 0.0014 0.07 ppm wet 0.00473/17/2010 18:40:00 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00588.SPE 0 vol-% wet 0.0247 0 ppm wet 0.0014 0.1 ppm wet 0.00683/17/2010 18:40:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00589.SPE 0 vol-% wet 0.0232 0 ppm wet 0.0016 0.1 ppm wet 0.0043/17/2010 18:40:12 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00590.SPE 0 vol-% wet 0.0108 0 ppm wet 0.0013 0.12 ppm wet 0.00573/17/2010 18:40:18 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00591.SPE 0 vol-% wet 0.0235 0 ppm wet 0.0014 0.09 ppm wet 0.00693/17/2010 18:40:24 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00592.SPE 0 vol-% wet 0.021 0 ppm wet 0.0015 0.09 ppm wet 0.00343/17/2010 18:40:30 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00593.SPE 0 vol-% wet 0.0241 0 ppm wet 0.0014 0.06 ppm wet 0.0043/17/2010 18:40:36 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00594.SPE 0 vol-% wet 0.0153 0 ppm wet 0.0013 0.1 ppm wet 0.0043/17/2010 18:40:42 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00595.SPE 0 vol-% wet 0.0287 0 ppm wet 0.0014 0.07 ppm wet 0.00583/17/2010 18:40:48 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00596.SPE 0 vol-% wet 0.0214 0 ppm wet 0.0015 0.11 ppm wet 0.00323/17/2010 18:40:54 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00597.SPE 0 vol-% wet 0.026 0 ppm wet 0.0015 0.07 ppm wet 0.00473/17/2010 18:41:00 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00598.SPE 0 vol-% wet 0.0171 0 ppm wet 0.0015 0.09 ppm wet 0.00543/17/2010 18:41:06 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00599.SPE 0 vol-% wet 0.0281 0 ppm wet 0.0015 0.06 ppm wet 0.00643/17/2010 18:41:12 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00600.SPE 0 vol-% wet 0.0189 0 ppm wet 0.0015 0.08 ppm wet 0.00553/17/2010 18:41:18 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00601.SPE 0 vol-% wet 0.0141 0 ppm wet 0.0013 0.1 ppm wet 0.00843/17/2010 18:41:24 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00602.SPE 0 vol-% wet 0.0254 0 ppm wet 0.0015 0.11 ppm wet 0.0053/17/2010 18:41:30 C:\CalcmetSamples\Lehigh 210158\20100317\CTS Zero Run 3 after_00603.SPE 0 vol-% wet 0.0158 0 ppm wet 0.0004 0.07 ppm wet 0.0033