Dry Scrubber Blue Goose Combustion Data Septem ber 2011 Fyrite

Location : Dry

Scrubber Date 9/25/12 Time:

run O2 CO2

1 18 3 2 18 3 3 18 3
Avg 18 3

Molecular wt

1 29.2 2 29.2 3 29.2

AVG 29.2

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien &Gere

Page 1Test ID: 9-25-12-POM-ABF Run#2 

### Value 0.0003 0 0.0003

150.00 220.00 0.0017 0.0001 0.0000 200.00 200.00 0.001625

200.00 275.00 0.0021 0.002

1305.00 1000.00 0.0002 0 0.00020



### Value 2.2000 1.9250 4.1250 Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #2** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/25/2012

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml) Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)Test ID: 9-25-12-POM-ABF Run#2



### Value 0.6722 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 3.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.2 28.7193372 0.042916321 550.1 642.4 29.9 58 1.55 1.044 29.9 128 1.26 84.575 80.9 29.92 0.25 0.00034088462



### Value 84.9548134 41.73276 62.5 2.94188 18.4 0.86756 0.042916 0.040836 98.8482 Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #2**  **9/25/2012**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficient

Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute av erage temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg)

I = % Isokinetic variation



### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moistureTest ID: 9-25-12-POM-ABF Run#2 LIMS ID#: 2012010669



### Value 2.2000 0.0022 1.925 0.001925 84.95481343 29.9 38.48 8.23 Green Carbon Baked tons/hr 0.042916321 75795.19717 4547711.8302 96352.58853 Acfm 79193.90838 Scfm 0.0007 Emission Rate of Total MCEM gr/dscf 0.26 6.23 0.2270 5.45 **0.49**

**0.032 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.028 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.059 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 17:16 End time: 19:34

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #2**  **9/25/2012**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

## Value 2.9

0.0029 84.95481343 29.9 38.48 8.23 Green Carbon produced tons/hr 0.042916321 75744.5319 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 4544671.916 0.0005 Particulate gr/dscf **0.34 Particulate lb/hr** 

**0.041 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Emission Calculations Test #2 9/25/2012** 

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions