Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-001Date Collected:09/11/2013Date Received:9/12/2013 

### Field Blank

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg < 0.20 0.50 TLT EPA 1631E 0.20 09/18/2013 U



### Sample Number:133724-002Date Collected:09/11/2013Date Received:9/12/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 7.43 0.050DPC EPA 200.8 0.010 09/18/2013 13:35 ug/L Arsenic, As 63.3 0.10 DPC EPA 200.8 0.030 09/18/2013 13:35 ug/L Barium, Ba 763 0.10 DPC EPA 200.8 0.020 09/18/2013 13:35 ug/L Beryllium, Be < 15 50 DAM EPA 200.7 15 09/18/2013 15:04 U ug/L Cadmium, Cd 246 0.050DPC EPA 200.8 0.010 09/18/2013 13:35 ug/L Chromium, Cr 204 0.20 DPC EPA 200.8 0.040 09/18/2013 13:35 ug/L Cobalt, Co 282 0.020DPC EPA 200.8 0.0040 09/18/2013 13:35 ug/L Copper, Cu 220 0.050DPC EPA 200.8 0.010 09/18/2013 13:35 ug/L Lead, Pb 104 0.010DPC EPA 200.8 0.0020 09/18/2013 13:35 ng/L Mercury, Hg 181000 5000 TLT EPA 1631E 2000 09/18/2013 ug/L Molybdenum, Mo 171 0.050DPC EPA 200.8 0.010 09/18/2013 13:35 ug/L Nickel, Ni 1740 0.20 DPC EPA 200.8 0.050 09/18/2013 13:35 ug/L Selenium, Se 649 0.50 DPC EPA 200.8 0.20 09/18/2013 13:35 ug/L Silver, Ag 0.174 0.010DPC EPA 200.8 0.0020 09/18/2013 13:35 ug/L Thallium, Tl 15.1 0.050DPC EPA 200.8 0.0020 09/18/2013 13:35 ug/L Tin, Sn < 150 500 DAM EPA 200.7 150 09/18/2013 15:04 U ug/L Titanium, Ti 106 100 DAM EPA 200.7 15 09/18/2013 15:04 ug/L Zinc, Zn 2630 0.50 DPC EPA 200.8 0.10 09/18/2013 13:35 mg/L Aluminum, Al 8.14 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:35 mg/L Boron, B 461 1.0 DAM EPA 200.7 0.20 09/18/2013 15:04 mg/L Calcium, Ca 6960 1.0 DAM EPA 200.7 0.20 09/18/2013 15:04 mg/L Iron, Fe 78.4 2.5 DAM EPA 200.7 0.50 09/18/2013 15:04 mg/L Magnesium, Mg 4160 0.50 DAM EPA 200.7 0.10 09/18/2013 15:04 mg/L Manganese, Mn 94.3 0.025DAM EPA 200.7 0.0050 09/18/2013 15:04 mg/L Potassium, K 74.6 2.5 DAM EPA 200.7 0.35 09/18/2013 15:03 mg/L Sodium, Na 374 1.5 DAM EPA 200.7 0.40 09/18/2013 15:03 mg/L Strontium, Sr 25.6 0.050DAM EPA 200.7 0.015 09/18/2013 15:03 mg/L Ammonia, NH3, as N < 0.020 0.050DMM EPA 350.1 0.020 09/17/2013 U mg/L Total Kjeldahl Nitrogen, TKN as N0.56 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N39.9 0.10 DMM SM20 4500NO3 H 0.020 09/21/2013

Mountaineer Plant, 133724 Page 1 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-002ADate Collected:09/11/2013Date Received:9/12/2013 

### CPS Influent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.21 0.050DPC EPA 200.8 0.010 09/18/2013 13:40 ug/L Arsenic, As 2.17 0.10 DPC EPA 200.8 0.030 09/18/2013 13:40 ug/L Barium, Ba 57.9 0.10 DPC EPA 200.8 0.020 09/18/2013 13:40 ug/L Beryllium, Be < 15 50 DAM EPA 200.7 15 09/18/2013 15:08 U ug/L Cadmium, Cd 159 0.050DPC EPA 200.8 0.010 09/18/2013 13:40 ug/L Chromium, Cr 0.6 0.20 DPC EPA 200.8 0.040 09/18/2013 13:40 ug/L Cobalt, Co 209 0.020DPC EPA 200.8 0.0040 09/18/2013 13:40 ug/L Copper, Cu 4.72 0.050DPC EPA 200.8 0.010 09/18/2013 13:40 ug/L Lead, Pb 0.134 0.010DPC EPA 200.8 0.0020 09/18/2013 13:40 ng/L Mercury, Hg 57.1 10 TLT EPA 1631E 4.0 09/18/2013 ug/L Molybdenum, Mo 97.0 0.050DPC EPA 200.8 0.010 09/18/2013 13:40 ug/L Nickel, Ni 1300 0.20 DPC EPA 200.8 0.050 09/18/2013 13:40 ug/L Selenium, Se 251 0.50 DPC EPA 200.8 0.20 09/18/2013 13:40 ug/L Selenite, Se+4 (Hydride) 176 20 TLT AEP Method 4.0 09/24/2013 ug/L Silver, Ag 0.014 0.010DPC EPA 200.8 0.0020 09/18/2013 13:40 ug/L Thallium, Tl 7.82 0.050DPC EPA 200.8 0.0020 09/18/2013 13:40 ug/L Tin, Sn < 150 500 DAM EPA 200.7 150 09/18/2013 15:08 U ug/L Titanium, Ti < 15 100 DAM EPA 200.7 15 09/18/2013 15:08 U ug/L Zinc, Zn 731 0.50 DPC EPA 200.8 0.10 09/18/2013 13:40 mg/L Aluminum, Al 0.0644 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:40 mg/L Boron, B 475 1.0 DAM EPA 200.7 0.20 09/18/2013 15:08 mg/L Calcium, Ca 732 1.0 DAM EPA 200.7 0.20 09/18/2013 15:08 mg/L Iron, Fe < 0.50 2.5 DAM EPA 200.7 0.50 09/18/2013 15:08 U mg/L Magnesium, Mg 3940 0.50 DAM EPA 200.7 0.10 09/18/2013 15:08 mg/L Manganese, Mn 94.2 0.025DAM EPA 200.7 0.0050 09/18/2013 15:08 mg/L Potassium, K 73.8 2.5 DAM EPA 200.7 0.35 09/18/2013 15:07 mg/L Sodium, Na 377 1.5 DAM EPA 200.7 0.40 09/18/2013 15:07 mg/L Strontium, Sr 9.41 0.050DAM EPA 200.7 0.015 09/18/2013 15:07

Mountaineer Plant, 133724 Page 2 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-003Date Collected:09/11/2013Date Received:9/12/2013 

### Primary Clarifier Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.69 0.050DPC EPA 200.8 0.010 09/18/2013 13:45 ug/L Arsenic, As 3.36 0.10 DPC EPA 200.8 0.030 09/18/2013 13:45 ug/L Barium, Ba 78.3 0.10 DPC EPA 200.8 0.020 09/18/2013 13:45 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 15:12 U ug/L Cadmium, Cd 129 0.050DPC EPA 200.8 0.010 09/18/2013 13:45 ug/L Chromium, Cr 4.4 0.20 DPC EPA 200.8 0.040 09/18/2013 13:45 ug/L Cobalt, Co 177 0.020DPC EPA 200.8 0.0040 09/18/2013 13:45 ug/L Copper, Cu 7.42 0.050DPC EPA 200.8 0.010 09/18/2013 13:45 ug/L Lead, Pb 0.850 0.010DPC EPA 200.8 0.0020 09/18/2013 13:45 ng/L Mercury, Hg 599 50 TLT EPA 1631E 20 09/18/2013 ug/L Molybdenum, Mo 166 0.050DPC EPA 200.8 0.010 09/18/2013 13:45 ug/L Nickel, Ni 1130 0.20 DPC EPA 200.8 0.050 09/18/2013 13:45 ug/L Selenium, Se 367 0.50 DPC EPA 200.8 0.20 09/18/2013 13:45 ug/L Silver, Ag 0.030 0.010DPC EPA 200.8 0.0020 09/18/2013 13:45 ug/L Thallium, Tl 9.88 0.050DPC EPA 200.8 0.0020 09/18/2013 13:45 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 15:12 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 15:12 U ug/L Zinc, Zn 142 0.50 DPC EPA 200.8 0.10 09/18/2013 13:45 mg/L Aluminum, Al 0.267 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:45 mg/L Boron, B 419 0.20 DAM EPA 200.7 0.040 09/18/2013 15:12 mg/L Calcium, Ca 755 0.20 DAM EPA 200.7 0.040 09/18/2013 15:12 mg/L Iron, Fe 0.701 0.50 DAM EPA 200.7 0.10 09/18/2013 15:12 mg/L Magnesium, Mg 3550 0.10 DAM EPA 200.7 0.020 09/18/2013 15:12 mg/L Manganese, Mn 75.0 0.0050DAM EPA 200.7 0.0010 09/18/2013 15:12 mg/L Potassium, K 63.3 0.50 DAM EPA 200.7 0.070 09/18/2013 15:11 mg/L Sodium, Na 342 0.30 DAM EPA 200.7 0.080 09/18/2013 15:11 mg/L Strontium, Sr 8.53 0.010DAM EPA 200.7 0.0030 09/18/2013 15:11 mg/L Ammonia, NH3, as N 1.55 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N1.31 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N41.8 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 3 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-003ADate Collected:09/11/2013Date Received:9/12/2013 

### Primary Clarifier Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.43 0.050DPC EPA 200.8 0.010 09/18/2013 13:50 ug/L Arsenic, As 2.48 0.10 DPC EPA 200.8 0.030 09/18/2013 13:50 ug/L Barium, Ba 73.3 0.10 DPC EPA 200.8 0.020 09/18/2013 13:50 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 15:21 U ug/L Cadmium, Cd 109 0.050DPC EPA 200.8 0.010 09/18/2013 13:50 ug/L Chromium, Cr 1.6 0.20 DPC EPA 200.8 0.040 09/18/2013 13:50 ug/L Cobalt, Co 154 0.020DPC EPA 200.8 0.0040 09/18/2013 13:50 ug/L Copper, Cu 2.67 0.050DPC EPA 200.8 0.010 09/18/2013 13:50 ug/L Lead, Pb 0.059 0.010DPC EPA 200.8 0.0020 09/18/2013 13:50 ng/L Mercury, Hg 32.4 5.0 TLT EPA 1631E 2.0 09/18/2013 ug/L Molybdenum, Mo 157 0.050DPC EPA 200.8 0.010 09/18/2013 13:50 ug/L Nickel, Ni 927 0.20 DPC EPA 200.8 0.050 09/18/2013 13:50 ug/L Selenium, Se 320 0.50 DPC EPA 200.8 0.20 09/18/2013 13:50 ug/L Selenite, Se+4 (Hydride) 261 20 TLT AEP Method 4.0 09/24/2013 ug/L Silver, Ag 0.0090 0.010DPC EPA 200.8 0.0020 09/18/2013 13:50 J ug/L Thallium, Tl 9.81 0.050DPC EPA 200.8 0.0020 09/18/2013 13:50 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 15:22 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 15:21 U ug/L Zinc, Zn 104 0.50 DPC EPA 200.8 0.10 09/18/2013 13:50 mg/L Aluminum, Al 0.0356 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:50 mg/L Boron, B 413 0.20 DAM EPA 200.7 0.040 09/18/2013 15:21 mg/L Calcium, Ca 739 0.20 DAM EPA 200.7 0.040 09/18/2013 15:21 mg/L Iron, Fe < 0.10 0.50 DAM EPA 200.7 0.10 09/18/2013 15:22 U mg/L Magnesium, Mg 3490 0.10 DAM EPA 200.7 0.020 09/18/2013 15:21 mg/L Manganese, Mn 73.6 0.0050DAM EPA 200.7 0.0010 09/18/2013 15:21 mg/L Potassium, K 62.6 0.50 DAM EPA 200.7 0.070 09/18/2013 15:20 mg/L Sodium, Na 335 0.30 DAM EPA 200.7 0.080 09/18/2013 15:20 mg/L Strontium, Sr 8.33 0.010DAM EPA 200.7 0.0030 09/18/2013 15:20

Mountaineer Plant, 133724 Page 4 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-004Date Collected:09/11/2013Date Received:9/12/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.59 0.050DPC EPA 200.8 0.010 09/18/2013 13:55 ug/L Arsenic, As 2.73 0.10 DPC EPA 200.8 0.030 09/18/2013 13:55 ug/L Barium, Ba 81.6 0.10 DPC EPA 200.8 0.020 09/18/2013 13:55 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 15:30 U ug/L Cadmium, Cd 20.3 0.050DPC EPA 200.8 0.010 09/18/2013 13:55 ug/L Chromium, Cr 2.7 0.20 DPC EPA 200.8 0.040 09/18/2013 13:55 ug/L Cobalt, Co 59.6 0.020DPC EPA 200.8 0.0040 09/18/2013 13:55 ug/L Copper, Cu 0.92 0.050DPC EPA 200.8 0.010 09/18/2013 13:55 ug/L Lead, Pb 0.890 0.010DPC EPA 200.8 0.0020 09/18/2013 13:55 ng/L Mercury, Hg 159 20 TLT EPA 1631E 8.0 09/18/2013 ug/L Molybdenum, Mo 196 0.050DPC EPA 200.8 0.010 09/18/2013 13:55 ug/L Nickel, Ni 602 0.20 DPC EPA 200.8 0.050 09/18/2013 13:55 ug/L Selenium, Se 330 0.50 DPC EPA 200.8 0.20 09/18/2013 13:55 ug/L Silver, Ag 0.0070 0.010DPC EPA 200.8 0.0020 09/18/2013 13:55 J ug/L Thallium, Tl 6.72 0.050DPC EPA 200.8 0.0020 09/18/2013 13:55 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 15:31 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 15:30 U ug/L Zinc, Zn 32.3 0.50 DPC EPA 200.8 0.10 09/18/2013 13:55 mg/L Aluminum, Al 0.189 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:55 mg/L Boron, B 401 0.20 DAM EPA 200.7 0.040 09/18/2013 15:30 mg/L Calcium, Ca 756 0.20 DAM EPA 200.7 0.040 09/18/2013 15:30 mg/L Iron, Fe 0.20 0.50 DAM EPA 200.7 0.10 09/18/2013 15:31 J mg/L Magnesium, Mg 3360 0.10 DAM EPA 200.7 0.020 09/18/2013 15:30 mg/L Manganese, Mn 68.3 0.0050DAM EPA 200.7 0.0010 09/18/2013 15:30 mg/L Potassium, K 60.6 0.50 DAM EPA 200.7 0.070 09/18/2013 15:29 mg/L Sodium, Na 329 0.30 DAM EPA 200.7 0.080 09/18/2013 15:29 mg/L Strontium, Sr 8.37 0.010DAM EPA 200.7 0.0030 09/18/2013 15:29 mg/L Ammonia, NH3, as N 2.62 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N1.89 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N35.3 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 5 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-004ADate Collected:09/11/2013Date Received:9/12/2013 

### CPS Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.46 0.050DPC EPA 200.8 0.010 09/18/2013 13:59 ug/L Arsenic, As 2.35 0.10 DPC EPA 200.8 0.030 09/18/2013 13:59 ug/L Barium, Ba 71.2 0.10 DPC EPA 200.8 0.020 09/18/2013 13:59 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 15:48 U ug/L Cadmium, Cd 1.05 0.050DPC EPA 200.8 0.010 09/18/2013 13:59 ug/L Chromium, Cr 1.6 0.20 DPC EPA 200.8 0.040 09/18/2013 13:59 ug/L Cobalt, Co 43.1 0.020DPC EPA 200.8 0.0040 09/18/2013 13:59 ug/L Copper, Cu 0.39 0.050DPC EPA 200.8 0.010 09/18/2013 13:59 ug/L Lead, Pb 0.066 0.010DPC EPA 200.8 0.0020 09/18/2013 13:59 ng/L Mercury, Hg 3.5 2.0 TLT EPA 1631E 0.80 09/18/2013 ug/L Molybdenum, Mo 173 0.050DPC EPA 200.8 0.010 09/18/2013 13:59 ug/L Nickel, Ni 503 0.20 DPC EPA 200.8 0.050 09/18/2013 13:59 ug/L Selenium, Se 298 0.50 DPC EPA 200.8 0.20 09/18/2013 13:59 ug/L Selenite, Se+4 (Hydride) 261 20 TLT AEP Method 4.0 09/24/2013 ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 13:59 U ug/L Thallium, Tl 5.39 0.050DPC EPA 200.8 0.0020 09/18/2013 13:59 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 15:48 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 15:48 U ug/L Zinc, Zn 22.5 0.50 DPC EPA 200.8 0.10 09/18/2013 13:59 mg/L Aluminum, Al 0.0332 0.0010DPC EPA 200.8 0.0003 09/18/2013 13:59 mg/L Boron, B 397 0.20 DAM EPA 200.7 0.040 09/18/2013 15:48 mg/L Calcium, Ca 736 0.20 DAM EPA 200.7 0.040 09/18/2013 15:48 mg/L Iron, Fe < 0.10 0.50 DAM EPA 200.7 0.10 09/18/2013 15:48 U mg/L Magnesium, Mg 3320 0.10 DAM EPA 200.7 0.020 09/18/2013 15:48 mg/L Manganese, Mn 67.1 0.0050DAM EPA 200.7 0.0010 09/18/2013 15:48 mg/L Potassium, K 60.3 0.50 DAM EPA 200.7 0.070 09/18/2013 15:46 mg/L Sodium, Na 330 0.30 DAM EPA 200.7 0.080 09/18/2013 15:46 mg/L Strontium, Sr 8.35 0.010DAM EPA 200.7 0.0030 09/18/2013 15:46

Mountaineer Plant, 133724 Page 6 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-005Date Collected:09/11/2013Date Received:9/12/2013 

### Landfill Leachate

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 11.2 0.050DPC EPA 200.8 0.010 09/18/2013 14:33 ug/L Arsenic, As 38.9 0.10 DPC EPA 200.8 0.030 09/18/2013 14:33 ug/L Barium, Ba 31.1 0.10 DPC EPA 200.8 0.020 09/18/2013 14:33 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 15:57 U ug/L Cadmium, Cd 1.33 0.050DPC EPA 200.8 0.010 09/18/2013 14:33 ug/L Chromium, Cr 0.2 0.20 DPC EPA 200.8 0.040 09/18/2013 14:33 ug/L Cobalt, Co 2.33 0.020DPC EPA 200.8 0.0040 09/18/2013 14:33 ug/L Copper, Cu 0.44 0.050DPC EPA 200.8 0.010 09/18/2013 14:33 ug/L Lead, Pb 0.122 0.010DPC EPA 200.8 0.0020 09/18/2013 14:33 ng/L Mercury, Hg 42.6 10 TLT EPA 1631E 4.0 09/18/2013 ug/L Molybdenum, Mo 7200 0.050DPC EPA 200.8 0.010 09/18/2013 14:33 ug/L Nickel, Ni 8.17 0.20 DPC EPA 200.8 0.050 09/18/2013 14:33 ug/L Selenium, Se 235 0.50 DPC EPA 200.8 0.20 09/18/2013 14:33 ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 14:33 U ug/L Thallium, Tl 3.05 0.050DPC EPA 200.8 0.0020 09/18/2013 14:33 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 15:57 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 15:57 U ug/L Zinc, Zn 3.3 0.50 DPC EPA 200.8 0.10 09/18/2013 14:33 mg/L Aluminum, Al 0.0166 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:33 mg/L Boron, B 58.0 0.20 DAM EPA 200.7 0.040 09/18/2013 15:57 mg/L Calcium, Ca 454 0.20 DAM EPA 200.7 0.040 09/18/2013 15:57 mg/L Iron, Fe < 0.10 0.50 DAM EPA 200.7 0.10 09/18/2013 15:57 U mg/L Magnesium, Mg 432 0.10 DAM EPA 200.7 0.020 09/18/2013 15:57 mg/L Manganese, Mn 1.64 0.0050DAM EPA 200.7 0.0010 09/18/2013 15:57 mg/L Potassium, K 120 0.50 DAM EPA 200.7 0.070 09/18/2013 15:55 mg/L Sodium, Na 1990 0.30 DAM EPA 200.7 0.080 09/18/2013 15:55 mg/L Strontium, Sr 6.08 0.010DAM EPA 200.7 0.0030 09/18/2013 15:55 mg/L Ammonia, NH3, as N 1.39 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N0.83 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N5.25 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 7 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-005ADate Collected:09/11/2013Date Received:9/12/2013 

### Landfill Leachate Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 10.4 0.050DPC EPA 200.8 0.010 09/18/2013 14:38 ug/L Arsenic, As 34.8 0.10 DPC EPA 200.8 0.030 09/18/2013 14:38 ug/L Barium, Ba 26.2 0.10 DPC EPA 200.8 0.020 09/18/2013 14:38 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:01 U ug/L Cadmium, Cd 1.15 0.050DPC EPA 200.8 0.010 09/18/2013 14:38 ug/L Chromium, Cr 0.16 0.20 DPC EPA 200.8 0.040 09/18/2013 14:38 J ug/L Cobalt, Co 1.54 0.020DPC EPA 200.8 0.0040 09/18/2013 14:38 ug/L Copper, Cu 1.00 0.050DPC EPA 200.8 0.010 09/18/2013 14:38 ug/L Lead, Pb 0.191 0.010DPC EPA 200.8 0.0020 09/18/2013 14:38 ng/L Mercury, Hg 7.6 2.0 TLT EPA 1631E 0.80 09/18/2013 ug/L Molybdenum, Mo 6710 0.050DPC EPA 200.8 0.010 09/18/2013 14:38 ug/L Nickel, Ni 9.95 0.20 DPC EPA 200.8 0.050 09/18/2013 14:38 ug/L Selenium, Se 217 0.50 DPC EPA 200.8 0.20 09/18/2013 14:38 ug/L Selenite, Se+4 (Hydride) 160 20 TLT AEP Method 4.0 09/24/2013 ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 14:38 U ug/L Thallium, Tl 2.78 0.050DPC EPA 200.8 0.0020 09/18/2013 14:38 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:01 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:01 U ug/L Zinc, Zn 3.0 0.50 DPC EPA 200.8 0.10 09/18/2013 14:38 mg/L Aluminum, Al 0.0109 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:38 mg/L Boron, B 58.3 0.20 DAM EPA 200.7 0.040 09/18/2013 16:01 mg/L Calcium, Ca 456 0.20 DAM EPA 200.7 0.040 09/18/2013 16:01 mg/L Iron, Fe < 0.10 0.50 DAM EPA 200.7 0.10 09/18/2013 16:01 U mg/L Magnesium, Mg 440 0.10 DAM EPA 200.7 0.020 09/18/2013 16:01 mg/L Manganese, Mn 1.36 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:01 mg/L Potassium, K 120 0.50 DAM EPA 200.7 0.070 09/18/2013 15:59 mg/L Sodium, Na 1990 0.30 DAM EPA 200.7 0.080 09/18/2013 15:59 mg/L Strontium, Sr 6.06 0.010DAM EPA 200.7 0.0030 09/18/2013 15:59

Mountaineer Plant, 133724 Page 8 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-006Date Collected:09/11/2013Date Received:9/12/2013 

### 1st Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 5.65 0.050DPC EPA 200.8 0.010 09/18/2013 14:42 ug/L Arsenic, As 16.5 0.10 DPC EPA 200.8 0.030 09/18/2013 14:42 ug/L Barium, Ba 59.1 0.10 DPC EPA 200.8 0.020 09/18/2013 14:42 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:05 U ug/L Cadmium, Cd 13.6 0.050DPC EPA 200.8 0.010 09/18/2013 14:42 ug/L Chromium, Cr 2.1 0.20 DPC EPA 200.8 0.040 09/18/2013 14:42 ug/L Cobalt, Co 38.6 0.020DPC EPA 200.8 0.0040 09/18/2013 14:42 ug/L Copper, Cu 1.12 0.050DPC EPA 200.8 0.010 09/18/2013 14:42 ug/L Lead, Pb 0.212 0.010DPC EPA 200.8 0.0020 09/18/2013 14:42 ng/L Mercury, Hg 104 10 TLT EPA 1631E 4.0 09/18/2013 ug/L Molybdenum, Mo 3290 0.050DPC EPA 200.8 0.010 09/18/2013 14:42 ug/L Nickel, Ni 352 0.20 DPC EPA 200.8 0.050 09/18/2013 14:42 ug/L Selenium, Se 286 0.50 DPC EPA 200.8 0.20 09/18/2013 14:42 ug/L Silver, Ag 0.010 0.010DPC EPA 200.8 0.0020 09/18/2013 14:42 ug/L Thallium, Tl 5.15 0.050DPC EPA 200.8 0.0020 09/18/2013 14:42 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:05 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:05 U ug/L Zinc, Zn 20.3 0.50 DPC EPA 200.8 0.10 09/18/2013 14:42 mg/L Aluminum, Al 0.141 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:42 mg/L Boron, B 254 0.20 DAM EPA 200.7 0.040 09/18/2013 16:05 mg/L Calcium, Ca 605 0.20 DAM EPA 200.7 0.040 09/18/2013 16:05 mg/L Iron, Fe 0.34 0.50 DAM EPA 200.7 0.10 09/18/2013 16:05 J mg/L Magnesium, Mg 2050 0.10 DAM EPA 200.7 0.020 09/18/2013 16:05 mg/L Manganese, Mn 39.1 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:05 mg/L Potassium, K 85.8 0.50 DAM EPA 200.7 0.070 09/18/2013 16:03 mg/L Sodium, Na 1020 0.30 DAM EPA 200.7 0.080 09/18/2013 16:03 mg/L Strontium, Sr 7.25 0.010DAM EPA 200.7 0.0030 09/18/2013 16:03 mg/L Ammonia, NH3, as N 1.53 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N1.98 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N20.6 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 9 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-006ADate Collected:09/11/2013Date Received:9/12/2013 

### 1st Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 5.49 0.050DPC EPA 200.8 0.010 09/18/2013 14:47 ug/L Arsenic, As 14.3 0.10 DPC EPA 200.8 0.030 09/18/2013 14:47 ug/L Barium, Ba 54.0 0.10 DPC EPA 200.8 0.020 09/18/2013 14:47 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:14 U ug/L Cadmium, Cd 1.25 0.050DPC EPA 200.8 0.010 09/18/2013 14:47 ug/L Chromium, Cr 1.1 0.20 DPC EPA 200.8 0.040 09/18/2013 14:47 ug/L Cobalt, Co 26.7 0.020DPC EPA 200.8 0.0040 09/18/2013 14:47 ug/L Copper, Cu 0.70 0.050DPC EPA 200.8 0.010 09/18/2013 14:47 ug/L Lead, Pb 0.065 0.010DPC EPA 200.8 0.0020 09/18/2013 14:47 ng/L Mercury, Hg 3.7 2.0 TLT EPA 1631E 0.80 09/18/2013 ug/L Molybdenum, Mo 3180 0.050DPC EPA 200.8 0.010 09/18/2013 14:47 ug/L Nickel, Ni 308 0.20 DPC EPA 200.8 0.050 09/18/2013 14:47 ug/L Selenium, Se 276 0.50 DPC EPA 200.8 0.20 09/18/2013 14:47 ug/L Selenite, Se+4 (Hydride) 225 20 TLT AEP Method 4.0 09/24/2013 ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 14:47 U ug/L Thallium, Tl 4.55 0.050DPC EPA 200.8 0.0020 09/18/2013 14:47 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:14 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:14 U ug/L Zinc, Zn 14.3 0.50 DPC EPA 200.8 0.10 09/18/2013 14:47 mg/L Aluminum, Al 0.0212 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:47 mg/L Boron, B 257 0.20 DAM EPA 200.7 0.040 09/18/2013 16:14 mg/L Calcium, Ca 630 0.20 DAM EPA 200.7 0.040 09/18/2013 16:14 mg/L Iron, Fe < 0.10 0.50 DAM EPA 200.7 0.10 09/18/2013 16:14 U mg/L Magnesium, Mg 2100 0.10 DAM EPA 200.7 0.020 09/18/2013 16:14 mg/L Manganese, Mn 40.3 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:14 mg/L Potassium, K 87.2 0.50 DAM EPA 200.7 0.070 09/18/2013 16:13 mg/L Sodium, Na 1040 0.30 DAM EPA 200.7 0.080 09/18/2013 16:13 mg/L Strontium, Sr 7.42 0.010DAM EPA 200.7 0.0030 09/18/2013 16:13

Mountaineer Plant, 133724 Page 10 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-007Date Collected:09/11/2013Date Received:9/12/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.07 0.050DPC EPA 200.8 0.010 09/18/2013 14:52 ug/L Arsenic, As 0.68 0.10 DPC EPA 200.8 0.030 09/18/2013 14:52 ug/L Barium, Ba 62.7 0.10 DPC EPA 200.8 0.020 09/18/2013 14:52 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:23 U ug/L Cadmium, Cd 0.018 0.050DPC EPA 200.8 0.010 09/18/2013 14:52 J ug/L Chromium, Cr 0.8 0.20 DPC EPA 200.8 0.040 09/18/2013 14:52 ug/L Cobalt, Co 0.067 0.020DPC EPA 200.8 0.0040 09/18/2013 14:52 ug/L Copper, Cu 0.07 0.050DPC EPA 200.8 0.010 09/18/2013 14:52 ug/L Lead, Pb 0.047 0.010DPC EPA 200.8 0.0020 09/18/2013 14:52 ng/L Mercury, Hg 2.8 1.0 TLT EPA 1631E 0.40 09/18/2013 ug/L Molybdenum, Mo 66.2 0.050DPC EPA 200.8 0.010 09/18/2013 14:52 ug/L Nickel, Ni 2.70 0.20 DPC EPA 200.8 0.050 09/18/2013 14:52 ug/L Selenium, Se 1.2 0.50 DPC EPA 200.8 0.20 09/18/2013 14:52 ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 14:52 U ug/L Thallium, Tl 0.035 0.050DPC EPA 200.8 0.0020 09/18/2013 14:52 J ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:23 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:23 U ug/L Zinc, Zn 1.5 0.50 DPC EPA 200.8 0.10 09/18/2013 14:52 mg/L Aluminum, Al 2.28 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:52 mg/L Boron, B 228 0.20 DAM EPA 200.7 0.040 09/18/2013 16:23 mg/L Calcium, Ca 602 0.20 DAM EPA 200.7 0.040 09/18/2013 16:23 mg/L Iron, Fe 1.19 0.50 DAM EPA 200.7 0.10 09/18/2013 16:23 mg/L Magnesium, Mg 1830 0.10 DAM EPA 200.7 0.020 09/18/2013 16:23 mg/L Manganese, Mn 33.9 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:23 mg/L Potassium, K 86.3 0.50 DAM EPA 200.7 0.070 09/18/2013 16:22 mg/L Sodium, Na 1010 0.30 DAM EPA 200.7 0.080 09/18/2013 16:22 mg/L Strontium, Sr 7.14 0.010DAM EPA 200.7 0.0030 09/18/2013 16:22 mg/L Ammonia, NH3, as N 2.35 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.26 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.72 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 11 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-007ADate Collected:09/11/2013Date Received:9/12/2013 

### Bioreactor Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.06 0.050DPC EPA 200.8 0.010 09/18/2013 14:57 ug/L Arsenic, As 0.62 0.10 DPC EPA 200.8 0.030 09/18/2013 14:57 ug/L Barium, Ba 60.1 0.10 DPC EPA 200.8 0.020 09/18/2013 14:57 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:32 U ug/L Cadmium, Cd 0.023 0.050DPC EPA 200.8 0.010 09/18/2013 14:57 J ug/L Chromium, Cr 0.7 0.20 DPC EPA 200.8 0.040 09/18/2013 14:57 ug/L Cobalt, Co 0.069 0.020DPC EPA 200.8 0.0040 09/18/2013 14:57 ug/L Copper, Cu 0.045 0.050DPC EPA 200.8 0.010 09/18/2013 14:57 J ug/L Lead, Pb 0.059 0.010DPC EPA 200.8 0.0020 09/18/2013 14:57 ng/L Mercury, Hg 1.0 0.50 TLT EPA 1631E 0.20 09/18/2013 ug/L Molybdenum, Mo 60.6 0.050DPC EPA 200.8 0.010 09/18/2013 14:57 ug/L Nickel, Ni 2.45 0.20 DPC EPA 200.8 0.050 09/18/2013 14:57 ug/L Selenium, Se 1.0 0.50 DPC EPA 200.8 0.20 09/18/2013 14:57 ug/L Selenite, Se+4 (Hydride)< 0.080 0.40 TLT AEP Method 0.080 09/24/2013 U ug/L Silver, Ag 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 14:57 J ug/L Thallium, Tl 0.024 0.050DPC EPA 200.8 0.0020 09/18/2013 14:57 J ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:32 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:32 U ug/L Zinc, Zn 2.6 0.50 DPC EPA 200.8 0.10 09/18/2013 14:57 mg/L Aluminum, Al 2.15 0.0010DPC EPA 200.8 0.0003 09/18/2013 14:57 mg/L Boron, B 237 0.20 DAM EPA 200.7 0.040 09/18/2013 16:32 mg/L Calcium, Ca 635 0.20 DAM EPA 200.7 0.040 09/18/2013 16:32 mg/L Iron, Fe 1.23 0.50 DAM EPA 200.7 0.10 09/18/2013 16:32 mg/L Magnesium, Mg 1930 0.10 DAM EPA 200.7 0.020 09/18/2013 16:32 mg/L Manganese, Mn 35.7 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:32 mg/L Potassium, K 90.2 0.50 DAM EPA 200.7 0.070 09/18/2013 16:31 mg/L Sodium, Na 1060 0.30 DAM EPA 200.7 0.080 09/18/2013 16:31 mg/L Strontium, Sr 7.52 0.010DAM EPA 200.7 0.0030 09/18/2013 16:31

Mountaineer Plant, 133724 Page 12 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-008Date Collected:09/11/2013Date Received:9/12/2013 

### 2nd Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.73 0.050DPC EPA 200.8 0.010 09/18/2013 15:02 ug/L Arsenic, As 8.95 0.10 DPC EPA 200.8 0.030 09/18/2013 15:02 ug/L Barium, Ba 58.9 0.10 DPC EPA 200.8 0.020 09/18/2013 15:02 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:41 U ug/L Cadmium, Cd 0.43 0.050DPC EPA 200.8 0.010 09/18/2013 15:02 ug/L Chromium, Cr 1.2 0.20 DPC EPA 200.8 0.040 09/18/2013 15:02 ug/L Cobalt, Co 6.04 0.020DPC EPA 200.8 0.0040 09/18/2013 15:02 ug/L Copper, Cu 0.34 0.050DPC EPA 200.8 0.010 09/18/2013 15:02 ug/L Lead, Pb 0.062 0.010DPC EPA 200.8 0.0020 09/18/2013 15:02 ng/L Mercury, Hg 3.2 2.0 TLT EPA 1631E 0.80 The analysis result for dissolved Hg was higher than the total Hg. It is suspected that the bottles were labelled incorrectly in the field. 09/18/2013

ug/L Molybdenum, Mo 2190 0.050DPC EPA 200.8 0.010 09/18/2013 15:02 ug/L Nickel, Ni 41.7 0.20 DPC EPA 200.8 0.050 09/18/2013 15:02 ug/L Selenium, Se 14.7 0.50 DPC EPA 200.8 0.20 09/18/2013 15:02 ug/L Silver, Ag 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 15:02 J ug/L Thallium, Tl 0.72 0.050DPC EPA 200.8 0.0020 09/18/2013 15:02 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:42 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:41 U ug/L Zinc, Zn 1.5 0.50 DPC EPA 200.8 0.10 09/18/2013 15:02 mg/L Aluminum, Al 0.399 0.0010DPC EPA 200.8 0.0003 09/18/2013 15:02 mg/L Boron, B 242 0.20 DAM EPA 200.7 0.040 09/18/2013 16:41 mg/L Calcium, Ca 649 0.20 DAM EPA 200.7 0.040 09/18/2013 16:41 mg/L Iron, Fe 0.582 0.50 DAM EPA 200.7 0.10 09/18/2013 16:42 mg/L Magnesium, Mg 1990 0.10 DAM EPA 200.7 0.020 09/18/2013 16:41 mg/L Manganese, Mn 40.4 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:41 mg/L Potassium, K 96.6 0.50 DAM EPA 200.7 0.070 09/18/2013 16:40 mg/L Sodium, Na 1040 0.30 DAM EPA 200.7 0.080 09/18/2013 16:40 mg/L Strontium, Sr 7.50 0.010DAM EPA 200.7 0.0030 09/18/2013 16:40 mg/L Ammonia, NH3, as N 0.82 0.050DMM EPA 350.1 0.020 09/17/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.44 0.50 DMM EPA 351.2 0.10 09/26/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.64 0.10 DMM SM20 4500NO3 H 0.020 09/13/2013

Mountaineer Plant, 133724 Page 13 of 14

### Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number:133724-008ADate Collected:09/11/2013Date Received:9/12/2013 

### 2nd Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.57 0.050DPC EPA 200.8 0.010 09/18/2013 15:06 ug/L Arsenic, As 8.27 0.10 DPC EPA 200.8 0.030 09/18/2013 15:06 ug/L Barium, Ba 54.3 0.10 DPC EPA 200.8 0.020 09/18/2013 15:06 ug/L Beryllium, Be < 3.0 10 DAM EPA 200.7 3.0 09/18/2013 16:50 U ug/L Cadmium, Cd 0.36 0.050DPC EPA 200.8 0.010 09/18/2013 15:06 ug/L Chromium, Cr 1.3 0.20 DPC EPA 200.8 0.040 09/18/2013 15:06 ug/L Cobalt, Co 5.72 0.020DPC EPA 200.8 0.0040 09/18/2013 15:06 ug/L Copper, Cu 0.35 0.050DPC EPA 200.8 0.010 09/18/2013 15:06 ug/L Lead, Pb 0.115 0.010DPC EPA 200.8 0.0020 09/18/2013 15:06 ng/L Mercury, Hg 16.2 1.0 TLT EPA 1631E 0.40 The analysis result for dissolved Hg was higher than the total Hg. It is suspected that the bottles were labelled incorrectly in the field. 09/18/2013

ug/L Molybdenum, Mo 2000 0.050DPC EPA 200.8 0.010 09/18/2013 15:06 ug/L Nickel, Ni 38.2 0.20 DPC EPA 200.8 0.050 09/18/2013 15:06 ug/L Selenium, Se 5.0 0.50 DPC EPA 200.8 0.20 09/18/2013 15:06 ug/L Selenite, Se+4 (Hydride) 1.5 5.0 TLT AEP Method 1.0 09/24/2013 J ug/L Silver, Ag < 0.0020 0.010DPC EPA 200.8 0.0020 09/18/2013 15:06 U ug/L Thallium, Tl 0.62 0.050DPC EPA 200.8 0.0020 09/18/2013 15:06 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 09/18/2013 16:51 U ug/L Titanium, Ti < 3.0 20 DAM EPA 200.7 3.0 09/18/2013 16:50 U ug/L Zinc, Zn 2.7 0.50 DPC EPA 200.8 0.10 09/18/2013 15:06 mg/L Aluminum, Al 0.378 0.0010DPC EPA 200.8 0.0003 09/18/2013 15:06 mg/L Boron, B 245 0.20 DAM EPA 200.7 0.040 09/18/2013 16:50 mg/L Calcium, Ca 667 0.20 DAM EPA 200.7 0.040 09/18/2013 16:50 mg/L Iron, Fe 0.534 0.50 DAM EPA 200.7 0.10 09/18/2013 16:51 mg/L Magnesium, Mg 2030 0.10 DAM EPA 200.7 0.020 09/18/2013 16:50 mg/L Manganese, Mn 41.3 0.0050DAM EPA 200.7 0.0010 09/18/2013 16:50 mg/L Potassium, K 97.8 0.50 DAM EPA 200.7 0.070 09/18/2013 16:49 mg/L Sodium, Na 1050 0.30 DAM EPA 200.7 0.080 09/18/2013 16:49 mg/L Strontium, Sr 7.59 0.010DAM EPA 200.7 0.0030 09/18/2013 16:49

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

Mountaineer Plant, 133724 Page 14 of 14