EMISSION TEST REPORT 

for the 


Cargill Incorporated Plant 


located in 


Sioux City, Iowa 


on 


October 19 tbru 22, 1999 


Conducted by 

Comprehensive Emission Services 


1112 Maple Street 


West Des Moines, Iowa 50265 


(515) 225-7372 ~ 

Project No. 8799 


. ! 
TABLE OF CONTENTS 

CONTENTS 

Preface .2 


IntroduG.tion.......................,,,.....,.,,.,"''',,....................,.....,..............,., ................................................,,,,.,...,..,...,,.,,,,...........................,,.,",,..... ,3 


Summary of Results.. .. ..... ..... ......... .... .................. ....... ........... ...................... ............... 4 


Sampling and Analytical Procedures ................................................................... ; ..... 7 


M5 Sampling Apparatus ............................................................................................... 8 


M 17 Sampling Apparatus..................................................................... 9 


Appendix A - Example Calculations 


Appendix B - Laboratory Data Fonns 


Appendj·x C - Field Data Forms 


Appendix D - Pretest Calibrations 


Appendix E - Posttest Calibrations 


Appendix F - Process Data 


Appendix G - Opacity Certification 


Appendix H - Cern Data 


Appendix I - Gas Protocols 


TABLES 

~ 

Table 1, Summary of Test Results Flaker Aspiration (EP # 13) ................................ 4 


Table 2, Summary of Test Results Grain Receiving Two (EP #26) .......................... ~ 

Table 3, Summary of Test Results Grain Cleaner (EP #1) ......................................... ) 


Table 4, Swnmary of Test Results Facility Boiler #3 (EP #23) ................................ 6 


FIGURES 

Figure 1, M5 Sampling Apparatus ...................................................... ....................... 8 


Figure 2, Ml 7 Sampling Apparatus.. ............................ ............................... .............. 9 

PREFACE 


This report summarizes the results of the data collected for compliance testing performed 

at the Cargill, Inc. in Sioux City, Iowa. To the best ofour knowledge, the data in this 

report are accurate and complete. Any questions concerning this report should be 

directed to Mr. Tim Titus or Mr. Jay Titus. They may be reached by phone at (5 15) 225­

7372. • 

Doug Ostrander 

Test Leader 

Tim Titus 

Reviewed by 

October 29, 1999 
INTRODUCTION 


Emission testing was conducted by Comprehensive Emission Services on the following 

sources using the corresponding methods. Testing was conducted at the Cargill Plant, in 

Sioux City: 

Flaker Aspiration (EP #13) - Method 5/202, TSP 

Grain Receiving Two (EP #26) - Method 5/202, TSP 

Grain Cleaner (EP #1) - Method 5/202, TSP 

Facility Boiler (EP #3)- Method 51202, TSP, and Method 7E NOx 

The testing was performed on October 19 thru 22, 1999. 

Coordinating the field tests: 

Tim Titus w Comprehensive Emission Services 

Lisa Schmidt - Thompson Environmental Consultants 

Conducting the field tests: 

Jay Titus - Comprehensive Emission Services 

Chad Siems - Comprehensive Emission Services 

Brad Bucldy - Comprehensive Emission Services 

Doug Ostrander - Comprehensive Emission Services 

Mike Ankerstjeme - Comprehensive E,:nission Services 

Witnessing the field tests: 

Kerry Riley- University of Iowa Hygienic Laboratory 

The appendices to this report contain the following information and data: 

Appendix A: Example Calculations 


AppendixB: Laboratory Data Forms 


Appendix C: Field Data Forms 


Appendix D: Pretest Calibrations 


Appendix E: Posttest Calibrations 


Appendix F: Process Data 


Appendix G: Opacity Certification 


Appendix H: Cem Data 


Appendix I: Gas Protocols 

SUMMARY OF RESULTS 

In accordance with current IDNR protocol, when less than 10 mg of sample is collected, 

10 mg ofsample catch is used for calculations. Sources with sample collections less than 

10 mg are shown with a '<' symbol in the following tables to indicate that actual samples 

were less tban the assumed 10 mg catch. Both the actual and the assumed emission rates 

can be found in Appendix C. 

!­
Table 2 summarizes the test results for testing performed on Grain Receiving Two (EP 

#26). Method 5, TSP, with 202 backhalf was used for testing. PM10 emissions will have 

to be assumed from the TSP samples for this sources. Testing fulfills requirements fOlmd 

in IDNR Permit #96-A-1253-S2. Testing was perfomled on October 19, and 20, 1999. 

The allowable limit for TSP is O.006gr/dscf, and 1.81blhr, and PM10 is 0.87 Iblhr, and 

0_0 0 3 gr/dscf .. 

NQ blank corrections were perfonned. 

Table 2 

Summary of Test Results 

Grain Receivinl!; Two (EP #26) 

units Run 1 Run 2 Run 3 

Particulate Net Weight g 0.Q188 0.0184 <0.0100 

Particulate Emissions gr/dscf 0.0016 0.0016 <0.0008 

Particulate Emission Rate lblhr 0.44 0.43 <0.23 

Flow Rate dscfm 31,747 31,047 31.791 

Flow Rate acfm 31.912 30,946 32,342 

Isokinetics % 98.2 98.5 99.2 

Start Time HH:MM 7:40 12:36 7:20 
SAMPLING AND ANALYTICAL PROCEDURES 


SampJing Procedures 

Particulate emissions were determined by U.S. Environmental Protection Agency (EPA) 

Methods 1,2,3,4,5, 201A, and 202. These Methods are titled; 

Method 1 - "Sample and Velocity Traverse for Stationary Sources" 

Method 2 - "Determination of Stack Gas Velocity and Volumetric Flow Rate" 

Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air and Dry 

Molecular Weight" 

Method 4 - "Determination for Moisture Content in Stack Gases" 

Method 5 - "Determination of Particulate Emissions from Stationary 

Sources" 

Method 7E - "Determination ofNiteregino xi de (NOx) Emissions from Stationary 

sour Sources" 

Method 20lA - "Determination of PM10 Emissions (Constant Sampling Rate 

Procedure)" 

Method 202 - "Condensible Particulate Emissions" 

These methods appear in detail in Title 40, Code of Federal Regulations (CFR), Part 60, 

Appendix A, and Part 5 1, Appendix M. 

The Sampling Apparatus is shown in Figure 1 on Page 8, and Figure 2 on Page 9. All 

equipment was calibrated at Comprehensive Emission Services' office prior to shipment 

to the test site. 

Sampling Locations 

The stack sampling point locations can be found along with the field data sheets in 

Appendix C. 

Analytical Procedures 

The particulate emission rate was determined following procedures detailed in EPA 

Methods 5, 201A and 202. Particulate samples collected on Whatman glass fiber filters 

were analyzed gravimetrically. The probe and nozzles were rinsed with acetone. The 

rinse was transferred to talTed beakers and evaporated to dryness. The back-half water 

was collected and separated into organic and in-organic parts. The samples were then 

transferred to tarred beakers and evaporated to dryness. 
Probe 

Nozzle 

Slack Exit Temp ~ Thermocouple Sample Probe 

~ 

I 

1;7 

Sample Line 

Heel ted 

S Type Pilot Tube Filter 

Ice Bath 

Tl1cnnocouples Fine Vacuum Adjust Gauge

Orif ice I~ l~ 1: __ )., 

/ t;;; 

(] 

Ory 

Gas 

Meter 

Leak Free 

Pump 

Schematic of Method 5 Sampling Train 

Figure 1 

\. 

Stack In-slile\: ~ Exit Temp 

-~-- " rhermocouplc ~~r Fi~lt~er~~~~~~S~(J.m~p~le~p~r~O:b:e=::=::~~~~}~ U --t!l~ )' " 


PI'obe 

Nozzle S Pilot Tube 

Ice 8ath 

Sample line 

Thermocouples Fine Vacuum Adjust Gauge

Orifice ~ ~[ ~ 

i.: ", r0 

Leak Free 


Pump 


Schematic or Method 17 Sampling Train 
Appendix A 


Example Calculations 

Symbol 

acfm 

As 

Bws' 

C; 

~ 

Dil 

dscfm 

gr/dscfin 

ID 

Md 


Ms 


~ 

Pb 


Ps 


SP 


Tm 


Ts 


Vi 

Vf 


Vm 


Vmstd 

Vs 

We 

WI gain 

y 

e 

% H20 

% CO, 

%02 

%1 

AH 

AP 

NOMENCLATURE 

Description 

Actual cubic feet per minute 

Area of stack 

Percent water 

Pitot tube calibration coefficient 

Concentration of palticulate dry basis, standard conditions 

Diameter of nozzle 

Dry standard cubic feet per minute 

Grains per dry standard cubic feet per minute 


Inside diameter of stack 


Molecular weight, dry stack gas 


Molecular weight, stack gas 


Stack flow rate, dry standard conditions 


Barometric pressure 


Stack pressure 


Static pressure 


Average meter temperature 


Temperature of stack gas 


Initial meter reading 


Fii meter reading 


Volume meter, actual 


Volume meter, standard conditions 


Average stack gas velocity 


Total moisture collected 


Total particulate matter collected 


Meter correction factor 


Sampling time 


Percent moisture by volume 


Percent carbon dioxide by volume, dry 


Percent oxygen by volume, dry 


Percent isokinetic 


Pressure drop across orifice meter 


Gas velocity pressure 
PARTICULATE CACULATION EQUATIONS 

Run 1 

1. Volume of meter 

Vm = (641.169 -497.100)x 0.998 

v,,, = 143.781 ft3 

2. Volume ofmeter, standard conditions (68' ,29.92 in. Hg) 

17.65xVm x Ph '1.~) ( 13.6 

V1II(SId) :=: T.. + 460 

17.65 x 143.7&1 x (29.75 _I _1.1_9) 

V 13.6 

m(,td} = ----50-.7-+-"-4-60---...:.. 

148.232 ft3 

3. Percent moisture by volume 

B = 100 x 0.4707 x We 

W$ 0.04707 X We + Vm(Sld} 

B = 100 X 0.4707x 134.0 

lI'5 0.04707 X 134.0 + 148.232 

B".. =4.1 % 

4. Molecular weight, dry stack gas 

Md 0.16 x %CO~ + %0.2 + 28.0 

Md O.l6xO.OO+21.00+28.0 

Md = 28.84 
5. Molecular weight, stack gas 

M.== MdXO-B"'S)+18X(I-Bw.) s 100 100 

Ms:: 28.84X(I- 4.1)+ 18x (l_il) 100 100 

Ms = 28.40 . 

6. Stack Presure 

SP P =p<+­

S u 13.6 

P. == 29.75 + 0.05 s 13.6 

Ps = 29.75 inch. Hg 

7. 	 Velocity of stack gas 

V: T +460 (r=) 60 x 85.349 x C p x 	 s X v/!.p p. +Ms 	 (]I'g 

Vs = 60 x 85.349 x 0.84 x -110 + 460- x 0.6290 

29.75 + 28.40 

v,,;:: 2,227 ftlmin 

8. 	 Percent isokinetic 

100 x (Ts + 460)x %1 

17.65xBxV. xP X(l- B''''')X1l'x(DII) , s 100 	 24 

%1 = _____10_0_x..:.-(1_1_0_+4_6_0..:-)x_l_4_8_.2_32_____ 

17.65 x 240 x 2,227 x 29.75X(1- 4.1)x 1CX (.252) 100 24 

%1 == 90.4% 
9 • Area of stack 

A = 7r X(ID)2 s 24 

A = 7r X (36.00)2 $ 24 

A, = 7.07 ftl 

10. Stack volummetric flow rate actual conditions 

Qa =2,227x7.07 

Qa ~ 15,742 acfin 

11. Stack volummetric flowrate, standard conditions (68· , 29.92 in .Hg) 

17.65XV XA XP X(1- BlI'S) s s s 100 


QstrJ = Ts + 460 

4.1 ) 17.65 x 2,227x7.07 x 29.75x (1 100 

Q5ld = 110 + 460 

Q"d = 13,897 dscfm 

12. Grains per dry standard cubic feet 

15.43 xWt g(Jin 


C,,,d 
 "" 

15.43xO.0645 


Cl1d = --14-8-.2-3-2­

e,td 0.0067 gr/dscf 
13. Emission rate 

Ib 60x WtgaillX QS1tl ! . 

- = ill 453.5924 X 

Vlll(!ld) 

lb 60 x 0.0645 x - :=: 

hI 453.5924x 148.232 

Ib = 0 80 Iblhr 

hr 
Appendix B 

Laboratory Data Forms , 

, . 

! 

; 
Project Number: :::--"g~7:.....,:7r,-:i______ :::. C = CoMPREHENS[VE Plant Name: C~rl1lll Date: EMISSION If) -2 >:1 1 = ES~ Analysis Type:,--J.,s;;;...iL..)________ = '; SERVICES 


Run { 'Irvd< Rpc, flVI h Y 

Type Identification F j il Tare Net 

Number Weight Weight Weight 

Filter f~lJr 3~OO/j ),OO(q. O.o0c;;>C> 

Probe Rinse ( rol) PItt-I} bt, '1GG 5 b6.. II b;) £' "OO)r 

Organic ( ml) C f{J~p I o~ /ir 1- 'TO Ioq "'if "1-/ 6 _,00 }I{ 

Inorganic b {Or:; r:} CJA '1b1-'1 i?O., 1bo;A .. Qo-:;'-1­

Total Net Weight , of {ff{ 

Run ] 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filter F~(i)~ 1'- ooo7:J­ ,,(,013 O.IO()OO 

Probe Rinse ( ml) )3 IG l./l.f -:;. b, 11r-32. 7-6~ l=t 99 ,. 0 0 '3 3 

Organic ( ml) C 1(/&1 /o;),j'J.?.S fOd,1-JO~ ",,0/2.0 

Inorganic D /(ll~ / -:t-6,fr '1£-6 i*.. ~~SS ,. 0011 

Total Net Weight , 0/>it! 

Run') 

Type Identification Final- Tare Net 

Number Weight Weight Weight 

Filter F<6-£J] 2. tJ>~ 0 :;2.. ),9¥ t;A r;;J. 0'000 :;:;. 

Probe Rinse ( ml) I; "Lf) "1-1, 3'2::;'6 -:;.60 3J 51 .. 0025 

Organic ( ml) L fO~2 /00, f:1t{;;. foo~ ~1-1 ;:l ,0°30 

Ioorganic j) (0-7'1­ /""".., T7• L/'<;;zQ . J ) I""Fi-, 43cJ. ;. oo;:x rTotal Net Weight , oo<ir;)... 

Blanks 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Water Blank ( rnl) 

ketone Blank ( ml) 

MeCI, Blank ( mJ) 

Identification 

F'" 3 inch filter P A 47mm filter B =150ml Beaker C = 250ml Beaker D '" 400ml Beaker 

.0037­

... 0053 
--- -

FINAL WEIGHT 


WEIGHING SHEET 


Time . ;(JJ;J 1t =OV 

Date 

Analyst 

JDNo. Run 

ot-l b I 

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F ~(J~ 

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-.!fI rfj rfr-:Zo 

Check Weight 

10 / t :rti1 j(,'/7.'"(111 

-j/' tr 

Weighing (grams) 

;2 ,1?60 / 2 3 4 

~~tl'7 :;.~~QO 

2,&-';J..2.1 2. 75,22'J 

2 , f; /'1( Cj 2. <!j t({ b 

'3. 001"3 ,),ooIG 

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:1.'1'1' 719' 2.9990 t 

3,o3C?O 3,CJ3G--~ 

,), pl..t Ie; J.o(..fl9 

7· CJ'1I-/tG 2.1150 

7.99fr5 2.9'7''8'6 

2, ?7'97 :1.000(} 

;;:.9972 ;1, QCf1ti 

),otJ§:z. 5.-;;."7c5 J. 

5 

-

Average 

Final 

Weight 

.:t-'d'501 

~.~.:<)~ 

2, tfl{/~ 

5.DO I~ 

3.dJOO 7­

.:1_ 9?o.z 

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~. 99'5-5 

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2~ "191-3 

C 

Tllre Net 

Wcigllt . Weight 

Cn MPR RHRNSIVR 

I 

, 

Check Weight _E EMISSION 

Check Weight ==- S-= SERvrCES 

Check Weight 
FINAL WEIGHT 


WEIGHING SHEET 


Time 

Dnle 

Analyst 

ID No. Run 

() ,o9€f 

D 1£790, 

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Weighing (grams) 

2 3 4 

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Average 

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/:;0" '1'6 7L</ 

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;=:17'_'11:< 9 

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It:? tffol 

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J6tJ_6/3 '5 

166_ ff3:< 

=-C -­ - -

Tare Net 

Weight Weigh 

. 

COMPREHENSIVE 

I 

1 

, 

EMISSION 

Check Weight I SERVICES 

I c:heck Weicht I 
---

FINAL WEIGHT 


WEIGHING SHEET 


Time 

Date 

Analyst 

In No. RUII 

/0 :J-O 

CO {O ::;'1 

Check Weight 

aleck Weight 

Check Weight 

i 

100. oo11lko, ()O-q. 

Weighing (grams) 

:,\ ;1 5 

COMPREHENSIVE 

EMISSION 

SERVICES 

Check Wciehl 
FINAL WEIGHT 


WEIGHING SHEET 


Time I /f:.:/7 C1 ;; ;/to 

An:llyst 

ID No. Run 

Check Weight 

Check Weight 

Check WeiJ?ht 

':;. 0,03/119-0.03 '2 

Weighing (~r:lJlls) 

J 4 = 

Date 

EMISSION 

SERVICES 
"-.--­

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TARE WEIGHT 

WEIGHING SHEET 

Analvst q 

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Average 

:),9720 

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3, ()O I ~ 

:J. r 'f 1-[ ~ 

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3, (jOS6 

3, 00 17 

7,001; 

COMPREHENSIVE 

EMISSION 

SERVICES 
---

---

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u cr­ ::;­ t:.O I::f:::>. ).. 

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TARE WEIGHT 


WEIGHING SHEET 


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DULl.. :i.,<dl '5 

Notes: 

/0,: 15 ~ / '(to 

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VVcighillg (grams) 

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COMPREHENSIVE 

E~ISSION ~ERVICES 
- ---

"'.,­

" , '.',:',1 

TARE WEIGHT 

WEIGHING SHEET 

Time 

Date 

Amllyst 

mNu, 

rh",," W..;"hl 

Weighing (g.'lUlIS) 

3 

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4 5 

!.·c - ---­ - E 

S~ 

COMPREHENSIVE 

EMISSION 

SERVICES 
IW 

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.)-" 

I~ -::::::. 

;:;­ ~ ~ ~ r:-I­

~~- .::::,. -::::::. -.::0, 

~ j

r-I.­ fV\ r{­ ri-­ ~ ~ ....:s t-I­ ~ 

~ ~ = :r' r<'\ 1....1', lr:; 

~ '""< ~ ~ "i. ~ "~ ~ 

--.. --... "~ = "­

~ - ~ if-.

t+­ r+ N­

~ ~ .~ 

--.. --.> M<

~ 

'::J. T"" 

I~t~ 1-;+ 

0 ~ 

I~ ~ I~ I~

\,Q ~ 

.J--­ ~ 

N-

.:::::,. I~::;­

~5i" "=> 

s-­

~ !.n 

s: rta 

~ ~ ~ -­ ......s;, 

,{- t ~ .;:::::.

-

H-' 

J'{... 

= Q 

~ 

<::::,

-

I~ 

It­

~ 

I~I~ 

:70 

"0 

~ .,., 

tl 

e 

til 

2: V'l V'l l!.l 

Z Z U L:l 0 ...... =: ..... > 

,,' V'l c:: ,.r., V'l t.:l 

g: ~U) 

~~ 

U 

IIIIII~I~ 

S?1"11111111111 
1II111~'~ 

~'1I1111111111 

Appendix C 


Field Data Forms 

Run No. 

Location: Cargill Truck Receiving 

Date: Oct19,99 

Project # 8799 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected( 


Percent Water= 


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 


Wet Molecular Weight= 


Sampling Time' (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Diameter (lnches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate loading - Total Catch Including Impingers 


Particulate Weight Net (g)= 


Particulate loading, Dry Std, 68 Deg (grlscf)= 


Emission Rate (lb/hr)= 


Percent Impinger Catch= 


98.2 

390.400 

566.906 

0.995 

0.001 

175.623 

178.852 

29.75 

-10.00 

29.01 

21 .00 

0.00 

17.0 

0.5 

57.6 

1.67 

1.4500 

47 

28.84 

28.79 

240.0 

0.185 

38.00 

7.88 

0.84 

·1.2008 

4,031 

31,747 

31,912 

0.0037 

0.0003 

0.09 

0.0188 

0.0016 

0.44 

80.32 
Run No. 2 

Location: Cargill Truck Receiving 

Date: Oct19,99 

Project # 8799 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu FUmin)'" 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 De9)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected( 


Percent Water-


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 


Wet Molecular Weight= 


Sampling Time (Minutes):::: 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches)= 


Stack Area (Square Feet) :::: 


Pitot Coefficient:::: 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, fUmin)= 


Flow Rate (Actual. Cubic fUmin)= 


Flow Rate (Std, Dry, Cubic fUmin 68 De9)= 


Particulate Loading - Front Half 


ParticUlate Weight Net (9)= 


Patlculate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


Particulate Weight Net (g)= 


Particulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Percent Impinger Catch:::: 


98.5 

567.300 

739.792 

0.995 

0.001 

171.630 

173.946 

29.75 

-10.00 

29.01 

21 .00 

0.00 

24.2 

0.7 

60.0 

1.57 

1.3708 

50 

28.84 

28.77 

240.0 

0.185 

38.00 

7.88 

0.84 

1.1701 

3,942 

31,047 

30.946 

0.0033 

0.0003 

0.08 

0.0184 

0.0016 

0.43 

82.07 
Run No. 3 Assumed 1 Omg 

Location: Cargill Truck Receiving 

Date: Oct 20,99 

Project # 8799 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen :::; 


Percent Carbon Dioxide= 


Moisture Collected( 


Percent Water-


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 


Wet Molecular Weight= 


Sampling Time'{Minutes)= 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches): 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading • Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (lb/hr)= 


Particulate Loading ~ Total Catch Including Impingers 

Particulate Weight Net (g)= 


Particulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (lblhr)= 


Percent Impinger Catch= 


99.2 

740.000 

921.630 

0.995 

0.001 

180.722 

183.014 

29.75 

10.00 

29.01 

21 .00 

0.00 

2.0 

0.1 

60.6 

1.72 

1.4667 

43 

28.84 

28.83 

240.0 

0.185 

38.00 

7.88 

0.84 

1.2082 

4,037 

31,791 

32,342 

0.0025 

0.0002 

0.06 

0.0100 

0.0008 

0.23 

75.00 
Run No. 3 

Location: Cargill Truck Receiving 

Date: Oct 20,99 

Project # 8799 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Rnal Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)"" 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected{ml)= 


Percent Water-


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 


Wet Molecular Weight= 


Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)== 


Particulate Loading ~ Front Half 

Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (lb/hr);::: 


ParticUlate Loading - Total Catch Including Impingers 


Particulate Weight Net (g)= 


Particulate Loading, Dry Std. 68 Deg (grlscn;::: 


Emission Rate (Ib/hr)= 


Percent Impinger Catch:::: 


99.2 

740.000 

921.630 

0.995 

0.001 

180.722 

183.014 

29.75 

-10.00 

29.01 

21 .00 

0.00 

2.0 

0.1 

60.6 

1.72 

1.4667 

43 

28.84 

28.83 

240.0 

0.185 

38.00 

7.88 

0.84 

1.2082 

4,037 

31,791 

32,342 

0.0025 

0.0002 

0.06 

0.0082 

0,Q007 

0.19 

69.51 
COMPREHENSIVE 

EMISSION 

SERVICES 

Project Number--"K"""'--"71 ___Cf_______ Project Leader ~(J,~·'='"'-;!9~O~'....t... :;;;,o... -..,,~c=>(f~'=.-__

Run Number_.......I'____________ 
 Meter Operator --Q;=tS-:""'r)---~='-- Date /Q-IC, .:. qq Lab Person __.::t't1=!ZJ"""'_____=--_ 

Sample Type _TS~I?E:;.·________ Support Personnel ______===--_ 

Plant C,c.vi)" l t 

l<:lcatiOD I Vw Ie' Oh"""J9 

Assumed Moisture % Q Meter NumberJ:i-+__ 


Minutes Per Point (min.) Oven Number :rr: 


Sampling Time (min.) 440 Umbilical Numr.er s:d..bl....e 


Meter Factor Y .5'95' PilOt Number 313 


Meter AH@ _,-..J.o1..... l"....K'-"'--_ Probe Number 31? 


3' Pitot Coefficient Cp--,-'~-=-'1__ Probe Length ___ 

Stack Axis 1 (inch.) -,3..L~""--__ Noz.zle Type -...,S.~2,,-_ Schematic of Testing Location 

Stack Axis 2 (inch.) -'3.....~.>o.L-__ 

Barometric Pressure (in. Kg) g'\)5 

Static Pressure (in. HP) < -10 

Nozzle Diameter (inch.) ,l~ 5" 

Initial Meter Volume (tr) :'.:1. Go. LlOV 

Final Meter VQ)uroe (ft') 5&-(p. 7(,)0 

Leak Rate Before 005 CFM@ Ita" 15 in. Hg 

Leak Rate After ."Ot Cf}.1@ { in.Hg 

PilOt Leak Check ~ Before 

---­ After 

RECOVERY DATA 

Orsat Impingers 

Trial 

1 () V'-' 

Avg 

Final Initial Differe.nce 

Impinger 1 '-1'5 IUO -is 

Impinger 2 /9-0 100 ;(0 

Impinger 3 lIn IUO jO 

Impinger 4 0;;r-~ (bY/ 4?.. 

Condirion/Color Total 11 

Notes: Filler Number: ---'-F.....;:~=~:..-..c...._·---"~_O_/~__ ~){) 
Field Data Sheet 

Run NO._-I-/____ 

Project No. ~/9:z 

( Location /"''-tc !c V).'::l<-I.;« 

Date la-IS -ct2 

Operator C. ~"'~ K"'\.-~...-~ 4 

Start TIme ,:LI[2 

Stop TIme U.· L/cl, t 

v 

NC:es: 
COMPREHENSIVE 

EMISSION 

SERVICES 

Project Number--"-(\L,J-L.-G...L(_S.L·_______ Project Leader -/:<:..4J..L_________ 

Run rJ Num~be~r~'~~__________________ Meter Operator. ..J-......~------"""""'­

Date 19 - ,C1":Q Ct Lab Person -----"'..;:.:;..::=;..-------­

Sample Type __T.!...>,~ .....J!:;.....)________ Support Personnel ---------__ 

Pl~t ____~~~-~~~~;l~________________ _ J 1(\ 

~tion __~I~v~~~c~k~l.)~"~~~~~--~--_____ 

Assumed Moisture % 3 Meter Number _4~__ 


Minutes Per Point (min.) Oven Number .----:::.=--_ 


Sampling Time (min.) 8-Lf() Umbilical Number 50'e1~ 

Meter Factor Y /1'15 Pilot Number 36 


Meter AH@ __1'_~_~=--<7.l.....-_ Probe Number -=J~B,,--_ 

Pitot Coefficient Cp I ~tj Probe Length ..;:3=<--1____ 


Slack Axis 1 (inch.) _3"",'J...l~r-- }l'ozzIe Type __'--__ Schematic of Testing Location 

Stack Axis 2 (inchj 3~ 

Barometric Pressure (in. Hg) c?3 J 5 

Static Pressure (in. H20) __<--=--·....:l...:::O=--_ 

Nozzle Diameter (inch.) . \5<5 

Initial Meter Volume (fil) 5fo7 :gO(J 

Final Meter Volume Cfr) 731.2~ Leak Rate Before .00 CFM@ !D:, ~ 15 in. Hg 

Leak Rate After ,DOL CFM@ ?? in. Hg 

PilOt Leak Check / Before ..­ After 

RECOVERY DATA 

Orsat Impingers 

Trial %C02 %CO!.;.7c°2 5Wl 

1 \... 

2 (\ " 

1\ r r~\ 

3 ~ WI 

Avg 

Final . Initial Difference 

Impinge! 1 .~:5: IUd M-.1Y 

lmpinger 2 ttl:\. IOD ,'1 

Impinger 3 /1 "') i()O ,g 

Impinger 4 """JOY /... '7~.X" <r.::l 

ConrlitioD/Colo[ Total ;1#, l.­

Filler Number: ...I-..!tL.:.:::....:..!......___________ 

Notes: C./~\\'()\ Q~ 
Field Uata ;::,nem 

/':-:' 

Run No. ;J. 

Project No, .LR/-.7L-q~9_____ 

Location-C:.c"''''j'' (.,/ 


Date ---10 19 -Cj9 


Operator --"-C~<2,,,-5.1.--______ 


Start TIme -..!.\fJ;.st::.':?J..o~~_____ 


Stop Time ~&z::"'·..L11l~:L../3--=--____ J3 

, 
- -- - -- - - - -

-- -

---!...L..l.l..=:­___ 

:"C­ - -- COMPREHENSIVE 

= 

-

- E=--­ - - EMISSION 

----

==- S-:::.:: ­

- SERVICES 

Run 

Sample Type -\.~f-________ 

Meter Operator ~=,-....a-________ 

Lab Person _~I:)...!.!.•..!:::O~ ________ 

Support Personnel ---------­

pla:nt l hV'Q~! ! 

Location TV' ....",k Ol6W! 0 

Assumed Moisture % Meter Number _4__ 

Minutes Per Point (min.) ll-- Oven Number jJ: 

Sampling Time (min.) &lYO Umbilical Number 5.t:ibIl...'f' 

Meter Factor Y ---l..-Q~__ Pilot Number ?t2 

Meter AH@ Probe Number ....:.Jl.....tii::__ 

Pilot Coefficient LI1.~"-'--- Probe Length ..,;3::...-'__ 

Nozzle Type .....,~5'54-__ Schemalic of Testing Location 

Barometric Pressure (in. Hg) g.'1:J0 

Static Pressure (in. HlO) --'--""":";=::-_ 

Nozzle Diameter (inch.) 

_..J,J..:...............__ 

...-L~__ 

Stack Axis 2 (inch.) ~!,.I...-­

Initial Meter Volume{ft') I'-/() ,-"l (I 

Final Meter VoJume (fr) q;)/.ta.?Q 

Leak Rate Before ri:~""'-i... CFM@ Ie. ~ 15 in. Hg 

i Leak Rate A fler • (XJ/ Cfl.1@ 7 in. Hg 

Pitot Leak Check v Before v After 

RECOVERY DATA 


Orsat Impingers 


Trial %C01 %C01~ %02 

1 \ 

2 f\ ,1\'hI- fV\"\ 

3 j'<J yl \ 

Avg 

Final Initial Difference 

lmpinger 1 35 /00 -faS 

Impinger2 1f t.\ iW 14 

3 ;lq flY) I~ 

Impinger4 Id.'J t (0;)1,0 34 

Condition/Color Total Z 

Notes: Filter Number: ---I.f:l~Ri<l.oQ,-5.L-_______
rtelu Udla ull~~l 

(7 Run NO'==---::-l.:J___== 

Project No. ====-9""'""?7I.....C~I(1=--·__-=== 

Location _"--+-,IV,--,,"-'-"-' t ~k--,,~-' \ .......",,=..'11-'-)-­

Date __----.1.11(,..LI~-+..!-()~'\-_S1..-q.:.,...'__ 

e<'-{, Operator =~-~-'-9-9 "--~== 

Start lime ===1=7...... ' d ...(,,--)__--== 

Stop lime ==--___-=== 

NC:es: "lI>" 
Preliminary Velocity <­

!3 

Plant Project No.--.;::~,-7..... 5-L-'34---___

Date [)-iZ-c,9 

locatio~ ~~C";j.ilI5"~H5<C''I7 Stack 1.0. Ir...c ~ au'YJ 

Pitot Cp ,<6) , /) 

Static Pressure in H 0 <. -IQ /-;j 2

Barometer Pressure in. Hg ;;0,.9 

Start Time '1-.3 -.312 "'" Stop Time---:;;;:--________ 

Operators C~Cd{S,'r('- ~.., 

td./JC'-t.'O Oskri .. Etc ".. 

SCHEMATIC OFTPAVEHSEPOINTLAYOUT 

Final Pitot Le,ak Check at ?!:S· H.o PI F 

Traverse Velocity Stack Cyclonic Row Traverse Velocity Stack Cyclonic Row 

Point Head Temp. 

Number aP OF 

in. H~O 

AI I.v 150 

:1 

:z 

; 

J 

(p 

/ 

8' 

c; 

/0 

/I 

[J 

.L<~ J' , -..J 

/'5 

1/, 'L 

I 

I (/) 

I, Lf 

It:;" 

~ 

5t-. 

I 

S?, I 

S~ 

Sfo 

..7fn 

Determination 

t:? at O· Angle \\'hich 

Reference Yields 

a Null l!.P 

I 

I 

Point 

Number 

l1J 

g 

? 

~ 

e;­

~ 

7 

~ 

C; 

10 

I / 

''d. 

Head Temp Determination 

aP OF 

in.Hp boP at 0° Angle Which 

Reference Yields 

aNuJl AP 

/.~ s,,! 

1:2 S?-., I 

I 

'I. ) 5b I 

I 

/.5 sb.1 

I 

'1,1,5 S(,.., 

I I 

I. 0 !i51 

I 

Notes: 

"".0 ... ~c COM1'REHENSIVE 

3.0 - ­ ~1i -E- EMISSION l·a 

5.7 -- ­ S -- SERVICES 

I;). i~ 11 < 

-v~ 
- --

-- - - - -

:...c­ - -- COMPREHEN"SIVE 

=- E-:::::::= - - EMISSION 

s-:: SERVICES 

1112 Maple 

West Des Moines, Iowa 50265 

'-~--.-.--r---~-r--.--r-. 

o 15 30 45 XX 0 15 30 45 

0-- 0 

o 

2 

3 

7 0 0 

8 0 0 

9 0 0 

STACK 

~ LOCATE: SUN ON ARC 

() 

0 

0 () 

cJ /\

,­

(? 
=.c COMPREIIENSIVE E­ EMISSION

=- S-: SERVICP.s 

1112 Maple 


West Des Moines, Iowa 50265 


$la~AnmE OF OBS'£RVD\ 

o 

2 

29 

45 
- -- - -

=-c - --­ -

- ---- COMPREHENSIVE - ----E ---- EMISSION 

S~ SERVICES 

1112 Maple 

West Des Moines, Iowa 50265 


') P~""Tl':A.'.!i 

ADOR£SS 

C:;;'7~ 

STACK!!£JGIl1 

S~Y CiX'1:lmOS 

0 

f~ 

:rACK ;1!/ 

7 


8 


9 

Appendix D 


Pretest Calibrations 

METER CALIBRATION 

Operator BB K Factor 

~ate Oct 11, 1999 Meter Number ·t.· revious Y Factor 1.000 Orifice Number 

RUN 1 

Meter Volume 

Final Cubic Feet 480.705 

initial Cubic Feet 475.600 

Net Cubic Feet 5.105 

Meter Temperature 

Inlet 

Initial Oeg. F 76.0 

Final Deg. F 77.0 

Outlet 

Initial Oeg. F 76.0 

Final Oeg. F 76.0 

Avg. Meter Temp Deg. F 76.3 

Time sec 480.0 

Meter Delta H inches H2O 1.20 

;" ,·~8arometric ..", 

Pressure inches Hg 29.90 ; . ... ~.:. .' 

Room Temperature 

Initial Oeg. F 75.0 

Final Oeg. F 74.0 

Avg.Room Temperature Deg. F 74.5 

Pump Vacuum inches Hg 21 

Vcr (std) dscf 5.015 

Vm (std) dscf 5.036 

Y Factor 0.996 

Delta H@ 1.665 

Average Y 0.998 

Average Delta H@ 1.672 

+/- 2% Criteria 

Percent of Avg Y 0.23 

PASS 

+1· 5% Criteria 

Percent of Final Y 0.19 ..../ PASS 

0.4847 

1 

6 

RUN 2 

485.884 

480.800 

5.084 

77.0 

78.0 

76.0 

76.0 

76.8 

480.0 

1.20 

29.90 

75.0 

75.0 

75.0 

21 

5.013 

5.011 

1 .000 

1.680 

1 
CON~OLE WORK SHE I I ' . ,­

C!=sratcr. .....;b~B.=-___= :< ~r. • 4'$"-{7 


Date: b -II ... ("rCz Mei:ErLD.. =:::!::'==-____ 


Frcvicus Y rill Crifics Nl.!mcer. ==~=---___ 


.~~'i ;\tL!:';'!:s.r 

ME: ::..... '/C\...:..Me. 

I i':~2.1 

;:::~ 

IMelar i"am!=l!fl!!:.:."a 

c;::ts 

.....

., 

..... 

" 

I 

I '-lID. ]0<)" 

I Lf7S-;WO 

z. 

'-Its-. J{~ £j , ; 

1 'fCJD .iJOD I 

I INt..:: \ 

:rJ;;a/ .~ 7~7 214 ·1 

.:::r:id .c:-. I 77 73' i 

1 

CUI!....':; I ........ 
 :,-.r..ai I -;: I 7& I 7b I 

2'.r.a. 'F I I 71h I 7G I 

Tir:-:e sac I I I LlSO I 4150 Me!Ef"~:': I 1~4 :-;'0 I Ird I .\. ?-- I 

c..!t:c:rr.etric ?~~'Ja ~;r. ~;- ~1·10 I I ~1·9D I I ~ccm L~;&.-c:.::..:..~ I ,e:: ;~;:a I I 75 1 i5 I 

,==.,":aj ':=- I 'I.) I I . I I 7Lf 

?...:rr.p VE.C"...:t::7l in. r:; &-1 ! .:AI I II I 

CCMPR..E-....::.:.\is:i.""YE 

1-.:?>{iSSlON 

SSV!(;3 

....../.: 'J' ~'::"'" 

..--..... _­
ORIFICE BRACKETING 

Operator BB BRACKET ORIFICES: 


Date Oct 11,1999 Orifice No.1 6
 I'd 

~::~;;. K Factor 0.4847 

Meter Number 1 Orifice No. 2 4 

Meter Y Factor 0.998 K Factor 0.2533 

ORIFICE #1 ORIFICE #2 

Meter Volume 


Final Cubic Feet 491.265 496.951 


Initial Cubic Feet 486.200 491.600 


Net Cubic Feet 5.065 5.351 

Meter Temperature 

Inlet 

Initial Oeg.F 78.0 78.0 , 

Final Oe9. F 78.0 79.0 

Outlet 

Initial Oeg. F 76.0 77.0 

Final Oeg. F 77.0 78.0 

Avg. Meter Temp Oeg. F 77.3 78.0 

Time sec 480.0 960.0 

Meter Delta H inches H2O 1.20 0.31 

r ~&arometric Pressure inches Hg 29.90 29.90 

\~~ ''''). 

Room Temperature 


Initial Oeg. F 76.0 76.0 


Final Oeg. F 75.0 76.0 


Avg.Room Temperature Oeg. F 75.5 76.0 

Pump Vacuum inches Hg 20 25 

Vcr (std) dscf 5.010 5.234 


Vm (std) dscf 4.987 5.250 


Y Factor (brackets) 1.005 0.997 


+/- 2% Criteria 


Percent of Y 0.66 0.10 


PASS PASS 

-- -- - - - -

SHACKSl !NG WORK SHEl= I 

C!=erater: _O_b___--= 

Date: \0 ~ \ l-91 

Freviews Y F..:.c:cr .9915" 

MetEr LD. ========= 


K F..:.c:cr No. 1 ==:=~tj~1S=q=I======l=G:,~) 

K Facer No. 2 =1'=~=5:=3=?'==(==~~j ,

i . 


~I.er~ ~/Cl!.:!t~E I 2 J
 I I 


?::;cj I I 
 :oj ;;;;rlaJ ., , L{7f~ 'dOD I q9! jj§o i
 I ! 

I INL.:: 

'F I ?if 715 


I F.mti I 711 


evn..:::.: 

k:!rlaJ I .~ 

r:r,a I eft 

Ilr..a I S'cC 

I Meter :1..t..; I ~n. ~~O 

7& 

77 

C-f?fo - J. 'J.-. 

I 

/ I I 

I 

7?f I 

./G() . i t~ \ I 

, .:or.... . 

1 


I ~arcmetric F'rass~:'S I :0:. ::g I ~1,90 ! ~q·20 I 


F.ccm 7ar..~:.!at:.:;a I 


I ,"C- it; 


75 


I J.O 


=-c - -- CCMXR.E:-;.:::..:.~S:':: =-

~L-1:-== E~;{!s5:;:ON 

-

--

=- s=-- - -. S-c"">v-:C-:;'" - ....::.... ... -­

.,-/) ...... 
METER CALIBRATION 

Operator BB K Factor 

r' Cate Oct 10, 1999 Meter Number 

)revious Y Factor 1.004 Orifice Number 

Meter Volume 

Final 

Initial 

Net 

Cubic Feet 

Cubic Feet 

Cubic Feet 

RUN 1 

838.495 

833.300 

5.195 

Meter Temperature 

Inlet 

Outlet 

Avg. Meter Temp 

Initial 

Final 

Initial 

Final 

Ceg. F 

Oeg. F 

Oeg. F 

Deg. F 

Oeg. F 

56.0 

60.0 

52.0 

59.0 

56.8 

Time 

Meter Celta H 

Barometric Pressure 

sec 

inches H2O 

inches Hg 

960.0 

0.32 

29.90 

"~., 

Room Temperature 

Avg. Room Temperature 

Initial 

Final 

Oeg. F 

Ceg. F 

Ceg. F 

63.0 

66.0 

64.5 

Pump Vacuum inches Hg 24 

Vcr (std) 

Vm (std) 

Y Factor 

Celta H@ 

dscf 

dscf 

5.291 

5.307 

0.997 

1.713 

Average Y 

Average Delta H@ 

1.001 

1.713 

+/- 2% Criteria 

Percent of Avg Y 

PASS 

0.41 

+/~ 5% Criteria 

Percent of Final Y 0.28 

... PASS 

0.2533 

2 

4 

RUN 2 

843.793 

838.600 

5.193 

61.0 

65.0 

59.0 

63.0 

62.0 

960.0 

0.32 

29.90 

66.0 

68.0 

67.0 

25 

5.279 

5.251 

1.005 

1.714 
- -

- - - -

- -

CONSOLE WORK SHEET 

t-­

CCer.l.lcr: a: -k~J.:: . - U 

Data: IO~I(·9 9. 

Previous Y 1-0 0::1 C.;;7cs NI2fi1ber. __J-....I___..........
 ;-c.c:r:i. 

ME: :.~ '/Ct.:..:ME 

;t> 

:t 

!1)38 .. l-~'iSI 633 ~300 I?iLl 6~ 

I r -_HI .. 

1'13 l_ 

7;­

Meter Temperan.::a 

lNt...E:: 

I 


I 


Initial ,~ s Co I G ( ~I 

Clil!...::: i 

!llitiai I Of I :;'-d-.. ~1

Fnal of I ~1 b -5 J 

lime $2C" r I J b;n.-v-. 1t,Dy_ 

Meter!1.l-i ~'l. 1-;0 I ,,)~ .#3~ r 

2arcmetric:-F~ in'" H;"" l I a.Cf-'1D :A0, <tV

Rccm Tampe-ta.iura 

IniiiaL "F (,3 be::, I I I 
 . .c::" , F.I'lai I I b& I b~ 

?t.U7ip Vac+~t.:m I in.;"':; I ~'-t rJ5 I 

:..c­ - - COMl'R E:--:::NSI"'v'E 

-

=- E~­ -

- -- EiYfISSlON 

=-

- S-=- -- ­

- SERT

"1CES 
ORIFICE BRACKETING 

Operator BB BRACKET ORIFICES: 


..Date Oct 11,1999 Orifice No. 1 1 


K Factor 0.5055 


Meter Number 2 Orifice No.2 4 


Meter Y Factor 1.001 K Factor 0.2533 


ORIFICE #1 ORIFICE #2 

Meter Volume 


Final Cubic Feet 860.070 854.729 


Initial Cubic Feet 854.800 849.500 


Net Cubic Feet 5.270 5.229 

Meter Temperature 

inlet 

Initial Oeg. F 69.0 68.0 

Final Oeg. F 69.0 69.0 

Outlet 

Initial Oeg. F 68.0 67.0 

Final Oe9. F 69.0 68.0 

Avg. Meter Temp Oeg. F 68.8 68.0 

Time sec 480.0 960.0 


Meter Delta H inches H2O 1.40 0.32 


.' Barometric Pressure inches Hg 29.90 29.90 
 :: ~ ~. 

:: "..~. ~. 

(';" 

"Room Temperature 


Initial Oeg. F 74.0 68.0 


Final Oeg. F 70.0 69.0 


Avg.Room Temperature Oeg. F 72.0 68.5 

f. Pump Vacuum inches Hg 21 25 

Vcr (std) dscf 5.242 5.271 


Vm (std) dscf 5.275 5228 


Y Factor (brackets) 0.994 1.008 


+/- 2% Criteria 


Percent of Y 0.72 0.73 


PASS PASS 

- - - - -- --

BRACKEIING WORK SHEF 1 


,"IET=-~ '/CL!...'ME I L:..i!s 

iniial ! 

iljjtiai I 'f 5cr (,')" I ~Z5 I 

F.naJ I 'P b'1 "70 I. bi 

cun...:: I 

Initial I ..r:

, b~ 05 b I I c::: ' ••tH!J I 0<::

. b9! b '/ b~ 

I Jro.a I s~c I :i'CO I .Cj&D .I Meter~ I in.}-J.p I i i-f ' 'j'(j) 

i:arcrnetric Prcssura 1 in. Hg ~'1'1 ~Cj, '10 

Fccm Tem;:sran:re 

. Inilial 

frr.al 

I 

i 

.c=, 

'p 

7'-/ 

7V1 

7D 

&0 

b'd 

b, 

Furr:p '/.ec~t.:t7l .1 :n. r:g l.ft ~ ! C).':J 

" . 

:..c­

-.c,­ =- T:-==
 ~ 

-----

--

= s=-

---­

COMl'RE:~\jSIV; 

EMISSlON' 

SE?V!C3 

',":"- . -,.;;.~ _..r: 

-.----..- p- .......... . 

CON~OLEWOF.KSHEEI 

. " ~ 

C~efC.l"Cr: ~:n~\3",,--____ KP~r:==·=2=J~==~========= 

Date: IV - "S"' q1 	 Mets'" 1.0. ==-=Jj~========== 

Previcus Y P:ic:r:r. ,297 Crffic;; Nt.:llice:r. _-11-/""--___

ME:::.."": '/CLLME I I 	 2 

I 67'1 . ]·n S 1_ 

,~.'_I "'I~ I I 3(.,2(.'100

1 

INt..=: 1 

!r.itla! I 'f ·1 

.=r.aI I I t?-	 ] CUT~; I 

!.'iitaJ. 'F I ~-:;t I I 	 I ~ 

fr.il 'F I ,)'c( 1 (,3 I ! 	 . I :rt:9 r *= I 7bO T 7bU I Mell1:("~--: ...,," r-:;;Q I . .3U -I ..,., I I I 

- -- - ~. 

I 'f 

2srcmeiir: F:a!'5t!....a. 1'1:. ;-:;- I d'1· J..3 I '<AI."J- j I I 

:r.;hl I G9 	 11 

'f ;0 ?,O ~ii~ :-:; .9.3 	 "3 

II f:.aI I 

E.M15SiON 

SBV!c=.s 

.- _... _-- - ... 

, 

I 
I 

METER CALIBRATION 

Operator BB K Factor 

,--: Date Oct 15, 1999 Meter Number 

:: 'revious Y Factor 0.997 Orifice Number 

RUN 1 

Meter Volume 

Final Cubic Feet 374.098 

Initial Cubic Feet 368.900 

Net Cubic Feet 5.198 

Meter Temperature 

Inlet 

Initial Oeg. F 54.0 

Final Oeg. F 62.0 

Outlet 

Initial Deg. F 52.0 

Final Deg. F 58.0 

Avg. Meter Temp Deg. F 56.5 

Time sec 960.0 


Meter Delta H inches H2O 0.30 


. Barometric Pressure inches Hg 29.23 


Room Temperature 

Initial Deg. F 69.0 

Final Deg. F ~70.0 

Avg.Room Temperature Deg. F 69.5 

Pump Vacuum inches Hg 23 

Vcr (std) dscf 5.148 

Vm (std) dscf 5.193 

Y Factor 0.991 

Delta H@ 1.673 

Average Y 0.995 

Average Delta H@ 1.689 

+/~ 2% Criteria 

Percent of Avg Y 0.37 

PASS 

+/- 5% Criteria 

Percent of Final Y 0.20 

PASS 

0.2533 

4 

4 

RUN 2 

379.415 

374.200 

5.215 

62.0 

66.0 

59.0 

63.0 

62.5 

960.0 

0.31 

29.23 

71.0 

70.0 

70.5 

23 

5.143 

5.150 

0.999 

1.705 
ORIFICE BRACKETING 


Operator SS BRACKET ORIFICES: 


_Date 

Meter Number 

Meter Y Factor 

Oct 15,1999 

4 

0.997 

Orifice No. 1 

K Factor 

Orifice No.2 

K Factor 

4 

0.2533 

1 

0.5055 

Meter Volume 

Final 

Initial 

Net 

Cubic Feet 

Cubic Feet 

Cubic Feet 

ORIFICE #1 

384.726 

379.500 

5.226 

ORIFICE #2 

390.145 

384.800 

5.345 

Meter Temperature 

inlet 

Initial 

Final 

Outlet 

Initial 

Final 

Avg. Meter Temp 

Oeg.F 

Oeg. F 

Deg. F 

Oeg. F 

Oeg. F 

66.0 

69.0 

64.0 

67.0 

66.5 

68.0 

70.0 

67.0 

69.0 

68.5 

L 

Time 

Meter Delta H 

Barometric Pressure 

sec 

inches H2O 

inches Hg 

960.0 

0.31 

29.23 

480.0 

1.40 

29.23 

Room Temperature 

initial 

Final 

Avg.Room Temperature 

Oeg. F 

Oeg. F 

Oeg. F 

70.0 

71.0 

70.5 

72.0 

71.0 

71.5 

Pump Vacuum inches Hg 24 21 

Vcr (std) 

Vm (std) 

Y Factor (brackets) 

dscf 

dscf 

5.143 

5.122 

1.004 

5.127 

5.233 

0.980 

+/- 2% Criteria 

Percent of Y 

PASS 

0.72 

PASS 

1.73 
, " 

--..-~. : -. 

I ClfTl _: i 

I r.CC:':1 IE,r;:;: ate'''':; a I 

I :=:::aJ 7}' I 

BRf\CKETiNG WORK SHEI= J 

CFcra.tcr. ~B"-.!D-,--____ MetEr I.D. ==l-.l:=J============== 


Date: to -15' n :< F::c:cr No. 1 =.~Q=53=3========C=/..I=) 

I 

j !Nt.=: l 

I ::::: I tW i g 1 

I .~ ! 

I F'..!r.;p \hC"~'.;... . I ;~. F; I J< II 911 j 

'C' 

--

- ­--- - - CCM:?~=""="':'\!s:L';=: 

,1 

r: -c­ - - -

==­ - S-=- - - - -

-

E~&SS~ON 

.:~ ........., ~J-:C-=' - --­ J 

i 

".~:...." 

. -~. 
Appendix E 


Posttest Calibrations 

METER CALIBRATION 

Operator DO K Factor 

Date Oct 25, 1999 Meter Number 

Previous Y Factor 0.998 Orifice Number 

RUN 1 

Meter Volume 

Final Cubic Feet 147.279 

Initial Cubic Feet 142.200 

Net Cubic Feet 5.079 

Meter Temperature 

Inlet 

Initial Oeg. F 61.0 

Final Oeg. F 66.0 

Outlet 

Initial Oeg. F 60.0 

Final Oeg. F 65.0 

Avg. Meter Temp Oeg. F 63.0 

Time sec 780.0 

Meter Delta H inches H2O 0.43 

Barometric Pressure inches Hg 29.60 

Room Temperature 

Initial Oeg. F 69.0 

Final Oeg. F 69.0 

Avg.Room Temperature Oeg. F 69.0 

Pump Vacuum inches Hg 24 

Vcr (std) dscf 5.074 

Vm (std) dscf 5.076 

Y Factor 1 .000 

Delta H@ 1.614 

Average Y 0.997 

Average Delta H@ 1.588 

+/- 2% Criteria 

Percent of Avg Y 0.29 

PASS 

+/- 5% Criteria 

Percent of Final Y 0.12 

PASS 

0.3033 

1 

5 

RUN 2 

152.445 

147.300 

5.145 

66.0 

68.0 

65.0 

68.0 

66.8 

780.0 

0.43 

29.60 

69.0 

69.0 

69.0 

23 

5.074 

5.105 

0.994 

1.562 
-- -- - --

---- - --

-- --

-

CONSOLE WORK SHEET 


Operator: _:!J_1_V..;..1______ K Factor: ___/w3;.L.>o<;Q_3:-3L---~. _____ 

Date: IOfo/<i.q Meter I.D. _-,,<-1_________ 

Previous Y Factor:· t f1t, Orifice Number: _""£_______ 

METER VOLUME Units 

Final if 

Inital tf 

Meter Temperature 

INLET 

Initial of 

Fina! of

• 

OUTLET 

Initial of 

Final of 

Time sec 

Meter ~H in. H~O 

Barometric Pressure in. Hg 

i Room Temperature 

! Initial of 

Final OF 

Pump Vacuum in. Hg 

Run Number 

1 

147 .'J.~1_ 

l",'1~O 

G/ 

hC:. 

'0eli: 

7'16 

. t..f3 

;(er.t:.,v 

0!!{ 

~!L 

d'i 

2 

is-J... t.{'i~ 

i'17.30 

c,_, 

'1 

&~ 

c. ~ 

'7~O 

' J13 

::<1, Ct 0 

(;q 

£9 

13 

··C­ - -- COMJ?REHENSIVE

=- E-­~ 

-

- -- EMISSION 

= 

--

-- s=- SERVICES 
ORIFICE BRACKETING 

Operator DO BRACKET ORIFICES: 

Date Oct. 25, 1999 Orifice No. 1 5 

K Factor 0.3033 

Meter Number I Orifice No. 2 2 

Meter Y Factor 0.997 K Factor 0.6426 

ORIFICE #1 ORIFICE #2 

Meter Volume 

Final Cubic Feet 157.820 164.169 

Initial Cubic Feet 152.600 158.200 

Net Cubic Feet 5.220 5.969 

Meter Temperature 

Inlet 

Initial De9. F 71.0 72.0 

Final Deg. F 72.0 72.0 

Outlet 

Initial Deg. F 71.0 72.0 

Final De9. F 72.0 72.0 

Avg. Meter Temp De9. F 71.fi 72.0 

Time sec 780.0 420.0 

Meter Delta H inches H2O 0.44 2.10 

Barometric Pressure inches Hg 29.60 29.60 

Room Temperature 

Initial Deg. F 69.0 69.0 

Final De9. F 69.0 69.0 

Avg.Room Temperature De9. F 69.0 69.0 

Pump Vacuum inches Hg 24 19 

Vcr (std) dscf 5.074 5.789 

Vm (std) dscf 5.134 5.889 

Y Factor (brackets) 0.988 0.983 

+/- 2% Criteria 

Percent of Y 0.86 1.40 

PASS PASS 
EHACK!::IING \NORK SHE~ i 

CPSf2.tcr. --D...I "",,».:...;\ ____ MetEr 1.0. .. I 


Cate: ----'/...;:;..o+Z'I:t~s--{-I'1._'_<'{~__ K F~Ccr No. 1 --',....3...0""""'3,.;;;3;;....____ I I 


.­

~1ET~ ~lCL~:!,~2 ....:~"':!3 :2 

..... ;::::u 2­ ....:; :;:ttll .. ,5";2... (,0 l5~.;J 0 

I I 11;" ~~e[!:r T-rr:--r--"~ 1; h:-= ea..... :; 
 I 


;NL.::: I I 


,.: :nicai I


1 


i


---...... 

'=:.ti . ~ ~~ \ ~ GlJ II..:: 1:-' --).. ~,: -.' . ..~,., 

I ..~ 

I . 

;r;;i:ai . I
 I I -a 7:a, I 
 , ;-:::aJ .:= I i ~ I
 72 1 


i ;r::2 S;:C ) i 4J..~ i
 :1fH.2 M.m;r~ ;;-:.. ..O I I I 
 '-/4 I 2.[ I


I 
 earcmetric ?:~:..:;= .~ -J, ._: -~ I 2Cf. (. :(q., I 


Rccm 1ar;!;S!ah..::'s I 
 .e- I .i.!'Cel I c.q I 
 I
 '1 

F=::al <C= I 

I 
 C;9 I (.,q I


F'..:mp \/ac!.:~~ .j'i~ :-".; I ~c..j 1 I '1 1 


. \ s . 

J 
METER CALIBRATION 

Operator BB K Factor 

Date Oct 25, 1999 Meter Number 

Previous Y Factor 1.001 Orifice Number 

Meter Volume 

Final 

Initial 

Net 

Cubic Feet 

Cubic Feet 

Cubic Feet 

RUN 1 

104.566 

99.500 

5.066 

Meter Temperature 

Inlet 

Outlet 

Avg. Meter Temp 

Initial 

Final 

Initial 

Final 

Deg. F 

Deg. F 

Deg. F 

Deg. F 

Deg. F 

49.0 

58.0 

44.0 

56.0 

51.8 

Time 

Meter Delta H 

Barometric Pressure 

sec 

inches H2O 

inches Hg 

960.0 

0.31 

29.60 

Room Temperature 

Avg.Room Temperature 

Initial 

Final 

Deg. F 

Deg. F 

Deg. F 

6B.O 

66.0 

67.0 

Pump Vacuum inches Hg 24 

Vcr (std) 

Vm (std) 

Y Factor 

Delta H@ 

dscf 

dscf 

5.226 

5.173 

1.010 

1.797 

Average Y 

Average Delta H@ 

0.995 

1.707 

+/- 2% Criteria 

Percent of Avg Y 

PASS 

i.48 

+/- 5% Criteria 

Percent of Final Y 

PASS 

0.56 

0.2533 

2 

4 

RUN2 , 

109.905 

104.600 

5.305 

59.0 

64.0 

57.0 

63.0 

60.8 

960.0 

0.31 

29.60 

67.0 

69.0 

68.0 

24 

5.221 

5.323 

0.981 

1.617 
- - -- -- - - - - - -

. I 

CONSOLE WORK SHEEr 

C{:er.:.tcr. ...,;\3;;;;....;b:......4.____ ~~r. ___._)_5=33~_______ 

Q Date: t?c."\ ! 2-s: J Sq MetErI.D. _===-_____ 

Frevicus Y .:".ac:r:r. /.$ 1 Cones ·- I N' t!mcer. =====<-- tf ____ 

ME; ::::.~ '/Ct.:..'ME L::-Jts 2. I ..... 0' f 0 t..( S'f,G. I ioA . DJoS- I ;;,J 

" '1'1.S"O I 

_ 

1 


INL=: 

Set ·1 

::T.al .c;-

. J ! I S<;( I (~1 I 

CUT!....:: 

!r.ilia1 OF I 5"'7 , tftf , ..... .. .. \ ',....: 

~ ." ·e r.r.ai .. :,.:;", I I 5"'b b~

lIme sac I I '1&0 qc.t> I Meter~:": in.. r-:O ,:':)1 I I ,3i • 0' Carcmemc- F~ I lrT.. 1~;- j J.q.(~ ! ;;Cf.C,O 

Room l.amJ:erall:ta 

lniiiaL I ~ I & 't/' I 
 C7 . i=:la! <0::' hy I . I (.;J/ 

rump Vac:.:t.:.-;t i m.E; I ~t.-f :J'f

'C- -- ­- COMPRE-:;:..:.~srVE =. E~ 

-

=- .-=- EMISSiON 

--

= s=-- SS'fnczs 

\ )} ....~ 

..----­
ORIFICE BRACKETING 

Operator DD BRACKET ORIFICES: 

Date Oct. 25, 1999 Orifice No. 1 4 

K Factor 0.2533 

Meter Number 2 Orifice No.2 I 

Meter Y Factor 0.995 K Factor 0.5055 

ORIFICE #1 ORIFICE #2 

Meter Volume 

Final Cubic Feet 115.215 120.752 

Initial Cubic Feet 110.000 115.500 

Net Cubic Feet 5.215 5.252 

Meter Temperature 

Inlet 

Initial Deg. F 66.0 68.0 

Final Deg. F 67.0 68.0 

Outlet 

Initial Deg. F 64.0 67.0 

Final Deg. F 67.0 68.0 

Avg. Meter Temp Deg. F 66.0 67.8 

Time sec 960.0 480.0 

Meter Delta H inches H2O 0.32 1.40 

Barometric Pressure inches Hg 29.60 29.60 

Room Temperature 

Initial Deg. F 67.0 68.0 

Final De9. F 68.0 68.0 

Avg.Room Temperature De9. F 67.5 68.0 

Pump Vacuum inches Hg 24 20 

Vcr (std) dscf 5.223 5.209 

Vm (std) dscf 5.181 5.214 

Y Factor (brackets) 1.008 0.999 

+/- 2% Criteria 

Percent of Y 1,32 0.41 

PASS PASS 
ERACKETiNG WORK SHEET ".. 

~! 

G

\:i·':· Operatc!: ----:'1)=-v_____ Meter 1.0. __2_---___ 

Data: lvJlS'/11

I I 

K F'3.c:cr NO.1 _ ..... ' d"'""'5"3-.l..:::::.3o.L-___ 

FrsvicL's Y F'3.c:cr ! q'if' :< Fac:crNo. 2 _.L...'-...:::.>O:::;.f).~~~ ____ 

'.. 

initial 110,00 

I !NLE 

I initial 

"C:::ai I 'F I &7 !. G~ 

OUit..:::: 

Initial j 0<: . I (1 I G7 

F:m>I I OF I (07 I (;'3 

, 


I 


I 


I 
 . ~: r.:e,. SeC q> (, f.) ·'i.ljD . Maler t:H in, P..p ! I , 31­ /. 'i I

Earcmettic rt2ssura in~ Eg I I lq. t ::<4[" 

Rccm Terrq:efail.:re 

. Initial .c;- , I r C:.7 I Gg 

F:nal .'" I I r:~ I ~.g I F~mp '/sc!1L.!r;1 . , :n. ;-;g ;}.o I ~t.J .1 .. 

COM?RE...~'i.$l1.-S 

E:vrrSSiON 

S-"Jv-;C=t::: t:"" __

": .~ ..". ...-.. -___, A.-' 
METER CALIBRATION 

Operator BB K Factor 

. .Date Nov. 1, 1999 Meter Number 

}revious Y Factor 0.995 Orifice Number 

RUN 1 

Meter Volume 

Final Cubic Feet 79.673 

Initial Cubic Feet 74.500 

Net Cubic Feet 5.173 

Meter T emperatlJre 

Inlet 

Initial Oeg. F 70.0 

Final Oeg. F 72.0 

Outlet 

Initial Deg. F 69.0 

Final Deg.F 72.0 

Avg. Meter Temp Deg.F 70.8 

Time sec 780.0 


Meter Delta H inches H2O 0.45 


" t;:larometrfc Pressure inches Hg 29.65 


Room Temperature 

Initial Oeg. F 73.0 

Final Oeg. F -71 .0 

Avg. Room Temperature Deg. F 72.0 

Pump Vacuum inches Hg 23 

Vcr (std) dscf 5.069 

Vm (std) dscf 5.103 

Y Factor 0.993 

Delta H@ 1.620 

Average Y 0.993 

Average Delta H@ 1.637 

+/- 2% Criteria 

Percent of Avg Y 0.01 

PASS 

+/- 5% Criteria 

Percent of Final Y 0.20 

PASS 

0.3033 

4 

5 

RUN 2 

84.884 

79.700 

5.184 

72.0 

73.0 

72.0 

73.0 

72.5 

780.0 

0.46 

29.65 

73.0 

74.0 

73.5 

23 

5.061 

5.098 

0.993 

1.653 
CONSOLE WORK SHEET 


t , 

.~ Cr:eratcr. _B..=...oB~____ Kr~r.~·3~·~o=3~~========== 

Oae: rP: ( -9'1 Met=r 1.0. =='-1=========== 

Frevicus Y ?=.ccr. ' 91~ 

At.tn Nur.::er 

ME: '::.:-:' '/Ct.:.:ME L'::iis I I 2­

o::-:;u .,.,\

., I 

! rib7?:" , I '%7·38-'-/ 1_ 

...
 !r.:t:.i I 7'-1.50 0 r " /::t 7f!..U I i

IMete;; r;;.;r.:!=,!r~<! I 

I 
 INL.::: 
 I 

I .c:: ~i~aI 7V 7 ''J.,. .j 

;-.r.ai ";:- iJ-. 73 I I 

CLiit.Z:" I 

I :rjtjal ''1;." I 

:=.r:~ •,= 

f.::> 1 

I 

Tir.:e I sa-::-

Mer&.r~~ I 1-", ;':,,:0 

7).. 

7gD 

I ~ ~/f5 

I .. "'.'~ 

·'1 

~ : .. ',' 

?:cem 1:"C!7":;:E;-~-a 

, ..... 7:;; ,r.;:.a ';::: 7;:; I I ! 
 , '/~ J F::u 'F I 7} I 
 ;:~p v~C"-'~~ L~ .. :...:~ I ~3 ~3 I ! I 

&!:riC' F:;;='ra :-r. :-.:;- )f.b.S- J/1h'J I 

..eMISSION 

SD."'i!GS 

j ,: 'J' "-''-­

,-- ~----
Meter 1.0. _....:..-- 4 ______ 

FreViCl:S Y f:c:cr ;~Cfi3 

l·:AE!='~ \:Cl~:~E c::!ts 2­ I I '/ 

I 

., I I=:.ai """ I ero·lo 7 'qe:,.::< 7':1, J 

I 

...;; !1i~tieJ .\ '10 . ')00 1 I 15~.~o 0 I IMarer t",r;:;:..,an.::e I 

iNLE I I 


:r.ijcj 'F 13 i

I J 7;'- i

, r.~a.i 7J I. 7S- i

. ' . ""'\""\ CUTLE: I I I " " ," '. .c: 1 -: !;;:t:«ti j I I 73 I 7'1 ! ... ;-' -. 

c;: r:;-:a I I I 11 I 7,-/ I TI~a s~c I I I '78'0 I .'1:).0 ! 

I MetE, ;;l.~ I :n. ;.:~O I " 

. '-1'7 I ). ~ J I carcme:trfc .=:ass:.::a I :::. Eg ?,cr&5"'"
 / I 2/:"&:;- I 


I ~ccm TEJ'i':;:S!'2r;.::'a -. I 

ini;5E1 '=p 7,-/ I I I I 


[ I I '7Q I 

I ;~I I
 :=:::<1 'F 

1 

FfJ~p ~/:=C-":L"'7i I .1 :n.. E; I d-,) I fJJQ I 
ORIFICE BRACKETING 

Operator BB BRACKET ORIFICES: 

::Eate Nov 1,1999 Orifice No. 1 5 

K Factor 0.3033 

Meter Number 4 Orifice No. 2 2 

Meter Y Factor 0.993 K Factor 0.6462 

ORIFICE #1 ORIFICE #2 

Meter Volume 

Final Cubic Feet 90.107 96.272 

Initial Cubic Feet 84.900 90.300 

Net Cubic Feet 5.207 5.972 

Meter Temperature 

Inlet 

Initial Oeg. F 73.0 75.0 

Final Oeg. F 74.0 75.0 

Outlet 

Initial Oeg. F 73.0 74.0 

Final Oeg. F 74.0 74.0 

Avg. Meter Temp Deg. F 73.5 74.5 

Time sec 780.0 420.0 

Meter Delta H inches H2O 0.47 2.20 

:- Barometric Pressure inches Hg 29.65 29.65 

Room Temperature 

Initial Oeg. F 74.0 74.0 

Final Oeg. F 74.0 74.0 

Avg. Room Temperature Oeg. F 74.0 74.0 

Pump Vacuum inches Hg 23 20 

Vcr (std) dscf 5.059 5.804 

Vm (std) dscf 5.111 5.876 

Y Factor (brackets) 0.990 0.988 

+/- 2% Criteria 

Percent of Y 0.31 0.53 

PASS PASS 
Appendix F 


Process Data 

----------------------------

Compliance Emission Test 

Operating Data 

Owner: Car&!ll, Sioux City Date: October 19-22 

Source:EP #26 - Grain Rec~iving 11 Permit #: 96-A-1253-S2 

Maximum Continuous Process Rate (Manufacturer's Rating) 1500 Tonslhr.soybeans 

Hislorical Average Process Rate'----_______________________ 


Historical Maximum Process Rate 


Types and Sources (ifany) of Fuels normally 8umed,_N_T_IA_______________ 


Type of Fuel Bumed During this ._...._____________________ 

If Fuel is used Approximate Quantities of each listed above burned Annually_N;;..;./:.;.A~______ 

Recycling Capability Yes___ No X 

Recycling in Progress Yes___ No X 

Erocass Data O\~ jog Ryns 

Process Rate . 


(gallhr, Iblhr. tonslhr, etc ... ) 


Process Rate Wet 


Percent Moisture ('Yo) 

Process Rate Dry 

How Process Rate was 

Determined 

Run 1 Run 2­ Run 3 

515.2 tonslhr 466.4 tonslbr 419.6 tonslhr 

process scales 

Person Responsible for Data,__________-'B'-o....,;b-:-S'-u_nd_li....;·e___________ 

~;-:; < /-" 

Signature____________---',-\~l..;.X;;;;. __ ·-_--..::.J~.'.!;.:-..::.)_.~_-\._1...,:\!.",,"'..;_":..­ ••'-_':..=-=--_______

Tlt1e/Position,____________F:..:a:.:c.:.;il;.:,ity~S.;;..u;;,ip:..:.e.:.:rin=te=nd=e;;;;;nt'----___________ 

d Please indicate in the same units 8S your historical information 
AIR POLLUTION CONTROL EQUIPMENT OPERATING DATA 

Plant Cargill,Inc. LOC3rionSioux City 


Source Type ;.part! __·cul .......... ate-----__
*____ 
 Rated. Produc:rion -. Date ____ T.une ____ Actu:al Production--------------------- Air RuaNo. ---------­ Flaw Data __~~_----_ 

Mechanical Collector: 


'Tube Dia. in.. Number of!ubes Design 6p ______in. HiO Gas Temp ___ 


Observed ap in H~ Design cfm/tube @ Olmrnd t.\p @ ____ 


Fan Rated H.P. Openlting Volts Operating Amps _____ 


Electrostatic Precinitator 

Field No. Primary Primary Secondary Sect)nd:uy SparkRa:te 

Voltage (volts) Current (amps) Voltage (KV) Current (ma) (per min) 

Scrubber: 


Type ___________ Ap(aaoss scrubber} _________ in H~O. 

Fan Rated HP Operating Volts ______ Operating Amps ______ - Liquid Cin:uIation Rate gal/min. % Make-up ________ Blowdown ______ gpm 

Scrubbing Water Change Interval ___________-------_------___ 

Settling Tank Cleaning Interval 

Baghouse: 

p~..positive Nega~ No. Compa:mnents 

Type Cle::m.ing Cleon Cycle' :min 

Avg. BaghouseAp 2.6 inH:P ilpRange 

Fan: Rated H.P. Ope:ating Volts Operating Amps 

Cvclon;: 

Type 6p inH.<J Diameter 

FanRatedEP OpeIating Volts Operating Amps 

Penion Resp.lnsible for Data -=Bo=b.;;;;S.;;;un;;;;d;.;.;li;.:;.e~-------- ~') t, ~' :.' 

SignatUre ,~:t'-\J \. \. /, ~. ;!r \.';4. _' 

TItle/Position Facility Superintendent 

10 
Appendix G 


Opacity Certification 

DEPARTMENT OF NATURAL RESOURCES 

PAUL W. JOHNSON, DIRECTOR THOMAS J. VILSACK. GOVERNOR 

SALLY J. PEDERSON, LT. GOVERNOR 

May 12, 1999 

Doug Ostrander 

C.E.S 


1112 Maple 


West Des Moines IA 50265 


Dear Mr. Ostrander: 

We wish to acknowledge your attendance at the Spring 1999 session 

of the visible emissions recertification program conducted by the 

University of Iowa Hygienic Laboratory on April 20-21, 1999. 

The records show that you have suC 


making visual determination of ~ 

specifiedin subrule 567--29.1 of L 


Transmitted with this letter a I 

are qualified to make visible emi 

Chapter 567--29 of the Iowa Adminis 

Sincerely, 

~a~ddP' !/ DOUGLAS A. CAMPBELL 

AIR QUALITY BUREAU 

Enclosure 

cc: Pamela Kastle, U.H.L. 

7900 HICKMAN ROAD, SUITE 1/ URBANDALE, IOWA 50322/515-242·5100 I FAX 515-242·5094 
DEPARTMENTOFNATURALRESOURCES 

ST...TEOF I --.l 

PAUL W. JOHNSON. DIRECTOR THOMAS J, VILSACK. GOVERNOR 

SALLY J. PEDERSON. LT. GOVERNOR 

May 12, 1999 

Jay Titus 

CES 

1112 Maple St 

West Des Moines IA 50265 

Dear Mr. 

We wish to acknowledae your attendance at the Spring 1999 session 

of the emissions recertification program conducted by the 

University of Iowa Hygienic Laboratory on April 20-21, 1999. 

The records show that you have successfully met the criteria 

making sual determination of the opacity of emissions, as 

specified in subrule 567--29.1 of the Iowa Administrative Code. 

Transmitted with this letter is a certificate indicating that you 

are quali to make visible emissions evaluations pursuant to 

Chapter 567--29 of the Iowa Administrative Code. 

Notice of 1 1999 session will be issued around the end of 

September and you will be informed of the exact date and location 

of the next session. 

@elY, O~~p

DOUG~CAMPBELL AIR BUREAU 

Enclosure 

cc: Pamela Kastle, U.H.L. \'IDillg~I~~",;QILWrr~milt}fe.&1t: 

l1!1S IS TO Cl:Rl1Fl1 1'HA1' 

~~g~~b~~~%~~~~~1l~~::;O{ 

viNc:\t:\dl:ft!lcMt.4sorwI.(:j>~o! 

l'_~.....p.,.M......on!llt 

7900 HICKMAN ROAD. SUITE 1/ URBANDALE, IOWA 50322/515-242-5100 I FAX 515-242-5094