### EMISSION TEST REPORT 

### for the Cargill Incorporated Plant located in Sioux City, 

### Iowa on October 19 tbru 22, 1999

Conducted by 

### Comprehensive Emission Services 1112 Maple Street West Des Moines, Iowa 50265 (515) 225-7372**~** 

### Project No. 8799

. !

### TABLE OF CONTENTS

CONTENTS
Preface .2 IntroduG.tion
....................... ,,, ..... ,.,,.,"''',,
.................... , ..... ,

.............. ,., ................................................ ,,,,., ... , .. ,

... ,,.,,,, ........................... ,,.,",,..... ,3 Summary of Results..
.. ..... ..... .... ..... .... .................. ....... ........... ...................... ............... 4 Sampling and Analytical Procedures
................................................................... ; ..... 7 M5 Sampling Apparatus
............................................................................................... 8 M 17 Sampling Apparatus..................................................................... 9 Appendix A - Example Calculations Appendix B - Laboratory Data Fonns Appendj·x C - Field Data Forms Appendix D - Pretest Calibrations Appendix E

- Posttest Calibrations Appendix F - Process Data Appendix G

- Opacity Certification Appendix H - Cern Data Appendix I - Gas Protocols TABLES**~** 

### Table 1, Summary of Test Results Flaker Aspiration (EP # 

### 13)
................................ 4 Table 2, Summary of Test Results Grain Receiving Two (EP #26)
..........................**~** 

### Table 3, Summary of Test Results Grain Cleaner (EP #1)
......................................... ) Table 4, Swnmary of Test Results Facility Boiler #3 (EP #23)
................................ 6

FIGURES
Figure 1, M5 Sampling Apparatus
...................................................... ....................... 8 Figure 2, Ml 7 Sampling Apparatus..
............................ ............................... .............. 9

### PREFACE
This report summarizes the results of the data collected for compliance testing performed at the Cargill, Inc. in Sioux City, Iowa. To the best of our knowledge, the data 

### in this report are accurate and complete. Any questions concerning this report should be directed to 

### Mr. Tim Titus or Mr. Jay Titus. They may be reached by phone at 

### (5 15) 225­ 

### 7372. •

Doug Ostrander Test Leader

Tim Titus Reviewed by

October 29, 1999

### INTRODUCTION

Emission testing was conducted by Comprehensive Emission Services on the following sources using the corresponding methods. Testing was conducted at the Cargill Plant, in Sioux City: Flaker Aspiration (EP #13)

- Method 

### 5/202, TSP Grain Receiving Two (EP #26)

- Method 

### 5/202, TSP Grain Cleaner (EP #1)

- Method 

### 5/202, TSP Facility Boiler (EP #3)- Method 

### 51202, TSP, and Method 7E NOx The testing was performed on October 19 

### thru 22, 1999. Coordinating the field tests: Tim Titus w 

### Comprehensive Emission Services Lisa Schmidt

- Thompson Environmental Consultants Conducting the field tests: Jay Titus

- Comprehensive Emission Services Chad Siems

- Comprehensive Emission Services Brad Bucldy

- Comprehensive Emission Services Doug Ostrander

- Comprehensive Emission Services Mike Ankerstjeme

- Comprehensive E,:nission Services Witnessing the field tests: Kerry Riley- University of Iowa Hygienic Laboratory
The appendices to this report contain the following information and data: Appendix A: Example Calculations AppendixB: Laboratory Data Forms Appendix C: Field Data Forms Appendix D: Pretest Calibrations Appendix E: Posttest Calibrations Appendix F: Process Data Appendix G: Opacity Certification Appendix H: Cem Data Appendix I: Gas ProtocolsSUMMARY OF RESULTS
In accordance with current IDNR protocol, when less than 10 mg of sample is collected, 

### 10 mg of 

### sample catch 

### is used for calculations. 

### Sources with sample collections 

### less 

### than 10 mg are shown with a 

### '<' symbol in the following tables to indicate that actual samples were less tban the assumed 10 mg catch. Both the actual and the assumed emission rates can be found in Appendix C.

!­

### Table 2 summarizes the test results for testing performed on Grain Receiving Two (EP #26). Method 5, TSP, with 202 backhalf was used for testing. PM10 emissions will have to be assumed from the TSP samples for this sources. Testing fulfills requirements 

### fOlmd in IDNR Permit #96-A-1253-S2. Testing was perfomled 

### on October 19, and 20, 1999. The allowable limit 

### for TSP is O.006gr/dscf, and 1.81blhr, and PM10 is 0.87 Iblhr, and 0_0 0 3 gr/dscf
.. NQ blank corrections were perfonned. Table 2 Summary of Test Results 

### Grain Receivinl!; Two (EP #26) units Run 1 

### Run 2 

### Run 3 Particulate Net Weight g 

### 0.Q188 0.0184 <0.0100 Particulate Emissions gr/dscf 0.0016 0.0016 <0.0008 Particulate Emission Rate lblhr 0.44 0.43 

### <0.23 Flow Rate dscfm 

### 31,747 31,047 

### 31.791 Flow Rate 

### acfm 31.912 30,946 32,342 Isokinetics % 98.2 

### 98.5 

### 99.2 Start 

### Time HH:MM 7:40 12:36 

### 7:20

### SAMPLING AND ANALYTICAL PROCEDURES SampJing Procedures Particulate emissions were determined by U.S. Environmental Protection Agency (EPA) Methods 

### 1,2,3,4,5, 201A, and 202. These Methods are titled; Method 1 - "Sample and Velocity Traverse for Stationary Sources" Method 2 - "Determination of Stack Gas Velocity and Volumetric Flow Rate" Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air and Dry Molecular Weight" Method 

### 4 - "Determination for Moisture Content in Stack Gases" Method 

### 5 - "Determination of Particulate Emissions from Stationary 

### Sources" Method 7E

- "Determination of Nitere gino xi

de (NOx) Emissions from Stationary sour Sources" Method 20lA

- "Determination of PM 10 Emissions (Constant Sampling Rate Procedure)" Method 202

- "Condensible Particulate Emissions" These methods appear in detail in Title 40, Code of Federal Regulations (CFR), Part 60, Appendix A, and Part 

### 5 

### 1, Appendix M. The Sampling Apparatus is shown in Figure 

### 1 on Page 

### 8, and Figure 

### 2 on Page 

### 9. All equipment was calibrated at Comprehensive Emission Services' office prior to shipment to the test site. 

### Sampling Locations The stack sampling point locations can be found along with the field data sheets in Appendix C. 

### Analytical Procedures The particulate emission rate was determined following procedures detailed in EPA Methods 5, 201A and 202. Particulate samples collected on Whatman glass fiber filters were analyzed gravimetrically. The probe and nozzles were rinsed with acetone. The rinse was transferred to talTed beakers and evaporated to dryness. The back-half water was collected and separated into organic and in-organic parts. The samples were then transferred to tarred beakers and evaporated to dryness.Probe Nozzle Slack Exit Temp

## ~ Thermocouple Sample Probe**~**
I 

## 1;7

Sample Line Heel ted S Type Pilot Tube Filter



### Ice Bath Tl1cnnocouples Fine Vacuum Adjust Gauge

## I~ l~ Orif ice 1:

__ ).,

/ t;;; 

# (] Ory Gas Meter Leak Free Pump 

## Schematic of Method 5 Sampling Train Figure 1 

## \.

### Stack In-slile\:

### ~ 

### Exit Temp**-~--** " 

### rhermocouplc

# Fi~lt~er~~~~~~S~(J.m~p~le~p~r~O:b:e=::=::~~~~}~**~~r** 

### U

### --t!l~ )' " 

### PI'obe Nozzle 

### S Pilot Tube



### Ice 8ath Sample line Thermocouples Fine 

### Vacuum Adjust 

### Gauge

## ~**~** Orifice**~[** 

## i.: ", 

# r 

# 0

Leak Free Pump 

## Schematic or Method 

## 17 Sampling Train

# Appendix A Example Calculations

### Symbol 

### acfm As 

## Bws' C;**~** Dil 

### dscfm 

### gr/dscfin ID 

### Md Ms**~** 

## P

b 

## P

s 

### SP 

## Tm Ts Vi 

## V

f 

## Vm Vmstd 

### Vs 

### We WI gain 

### y 

## e % H 2 

### 0 % CO, 

### %0 2 

### %1 

### AH 

## AP NOMENCLATURE Description Actual cubic feet per minute Area of stack Percent water 

### Pitot tube calibration coefficient Concentration of palticulate dry basis, standard conditions Diameter of nozzle Dry standard cubic feet per minute Grains per dry 

### standard cubic feet per minute Inside diameter of stack Molecular weight, dry 

### stack gas Molecular weight, stack gas Stack flow rate, dry 

### standard conditions Barometric pressure Stack pressure Static pressure Average meter temperature Temperature of stack gas Initial meter reading Fii meter reading Volume meter, actual Volume meter, standard conditions Average stack gas velocity Total moisture collected Total particulate matter collected Meter correction factor Sampling time Percent moisture by volume Percent carbon dioxide by volume, dry 

### Percent oxygen by volume, 

### dry Percent isokinetic Pressure drop across orifice meter Gas velocity pressure

### PARTICULATE CACULATION EQUATIONS Run 1 1. 

### Volume of meter



### Vm = 

### (641.169 

### -497.100)x 0.998 

# v,,, = 

### 143.781 

### ft3
2. Volume of meter, standard conditions (68' ,29.92 in. Hg)


### 17.65xV m x 

### Ph

# '1.~) ( 13.6 

### V

1II (SId) :=: 

### T
.. + 460


### 17.65 

### x 143.7&1 

### x (29.75 _I 

### _1.1_9) V 13.6 m(,td} 

### = ----50-.7-+-"-4-60---...:..
148.232 

### ft3
3. Percent moisture 

### by volume 

### B 

# = 100 x 0.4707 x 

### We

W$ 

### 0.04707 X 

### We 

### + Vm(Sld} 

### B 

# = 100 X 

### 0.4707x 134.0

lI'5 

### 0.04707 X 

### 134.0 

## + 148.232
B"
.. =4.1 

### % 

### 4. Molecular weight, dry stack gas 

### Md 0.16 

### x**%CO~** 

### + %0. 2 

### + 28.0 

### Md O.l6xO.OO+21.00+28.0 

### Md = 

### 28.84

### 5. Molecular weight, stack gas 

## M.== MdXO-B"'S)+18X(I-Bw.)
s 

### 100 100


### Ms:: 28.84X(I- 4.1)+ 18x (l_il) 100 100 

### Ms 

### = 28.40
. 6. Stack Presure 

## SP P =p<+­

S u 

### 13.6
P. == 

### 29.75 

### + 0.05

s 

### 13.6 

### P

s = 

### 29.75 inch. Hg


### 7. Velocity of stack gas


### T 

### + 460 

# (r=) 

# V: 60 x 

### 85.349 x C p 

### x s X 

# v /!.p 

### p. 

### +Ms (]I'g


### Vs = 

### 60 

### x 85.349 

### x 0.84 

### x -110 

### + 460- 

### x 0.6290 

### 29.75 

### + 28.40 

# v,,;:: 2,227 

### ftlmin


### 8. Percent isokinetic 

### 100 x 

## (Ts + 

### 460)x %1 

### 17.65xBxV. 

# xP 

# X(l- B''''')X1l'x(DII) , s 

### 100 24
%1 =

_____ 

### 10_0_x..:.-(1_1_0_+4_6_0..:-)x_l_4_8_.2_32

____ _ 

### 17.65 x 240 

### x 2,227 x 29.75X(1- 

### 4.1)x 1CX 

# (.252) 100 24 %1 == 

### 90.4%

### 9 • Area of stack 

### A = 7r 

# X(ID)2

s 

### 24



### A 

# = 7r X 

# (36.00)2

$ 

### 24 

### A, 

## = 7.07 

# ftl
10. Stack volummetric flow rate actual conditions



### Qa 

### = 2,227x7.07 Qa**~** 

### 15,742 

### acfin
11. Stack volummetric flowrate, standard conditions (68· , 29.92 in .Hg)


### 17.65XV XA XP X(1- 

# BlI'S) s s s 

# 100 QstrJ 

# = Ts 

## + 460
4.1 ) 17.65 x 2,227x7.07 x 29.75x (1 100 

### Q5ld 

# = 110 

### + 460 

### Q"d = 

### 13,897 dscfm
12. Grains per dry standard cubic feet 

### 15.43 

### x 

### Wt g(Jin 

### C,,,d 

### ""

15.43xO.0645 

### C l1d = 

### --14-8-.2-3-2­


# e ,td 

### 0.0067 gr/dscf

### 13. Emission rate 

### Ib 60x WtgaillX QS1tl 

### ! . 

## - = ill 453.5924 X 

### V lll (!ld) 

### lb 60 

### x 0.0645 

### x

- :=: 

### hI 453.5924x 148.232 

### Ib = 

### 0 80 Iblhr hr

# Appendix B Laboratory Data 

# Forms

, , 

### . ! ;

### Project Number:

## :::--"g~7:.....,:7r,-:i _____ _ 

## :::. C = CoMPREHENS[VE 

### Plant Name:

## C~rl1lll EMISSION 

### Date: If) 

### -2 

# >:1 1 =

# ES~ Analysis 

### Type:,--J.,s;;;...iL..)

________ 

# = '; SERVICES
Run 

# { 'I 

# rvd< R pc, flVI h 

### Y Type Identification F j il Tare Net Number Weight Weight Weight Filter

## f~lJr**3~OO/j** 

## ),OO(q. O.o0c;;>C> Probe Rinse ( rol) 

# PItt-I} bt, 

# '1GG 5 b6

.. II b;) 

# £' "OO)r Organic ( ml) 

# C**f{J~p** I**o~** 

## /ir 

# 1- 

# 'TO I 

## oq " 

## 'if 

# "1-/ 

# 6 _,00 

### }I{ Inorganic 

# b {Or:; r:} CJA 

# '1 b 

## 1- 

# '1 i?O., 

## 1bo;A
.. Qo-:;'-1­ Total Net Weight 

## , of {ff{ Run ] Type Identification Final Tare Net Number Weight Weight Weight Filter 

# F**~(i)~** 

## 1'- ooo7:J­ 

## ,,(,013 O.IO()OO Probe Rinse ( ml) 

# )3 IG l./l.f -:;. b, 11r- 

## 3 2.

## 7-6~ 

## l=t 

# 99

,. 0 0 

## '3 

## 3 Organic ( ml) 

# C 

# 1(/&1 /o;),j'J.?.S**fOd,1-JO~** 

## ",,0/2.0 Inorganic 

# D**/(ll~** / -:t-6,fr 

## '1£-6 

# i*
..**~~SS** ,. 0011 Total Net Weight 

## , 0/ 

# >it! Run') Type Identification Final- Tare Net Number Weight Weight Weight Filter 

# F <6-£J] 2.**tJ>~** 0 

### :;2.. 

## ),9¥ t;A r;;J. 0'000 :;:;. Probe Rinse ( ml) 

# I; "Lf) 

## "1-1, 3'2::;'6 -:;.6 0 

## 3J 

# 51

.. 0025 Organic ( ml) 

# L**fO~2** /00, 

## f:1t{;;.**foo~ ~1-1**  

### ;:l ,0°30 Ioorganic 

# j) 

# (0-7'1­ /""".., L/'<;;zQ T7 • . J ) 

## I""Fi-, 

# 43cJ. ;. oo;:x 

# rTotal Net Weight 

### , oo<ir;)... Blanks Type Identification Final Tare Net Number Weight Weight Weight Water Blank ( rnl) ketone Blank ( ml)
MeCI, Blank ( mJ) Identification F'" 3 inch filter P A 47mm filter B 

### = 150ml Beaker C 

### = 250ml Beaker D '" 400ml Beaker 

## .0037­



# ... 0053

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Time

. ;(JJ;J 

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## =OV Date Analyst
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# ?7'97 :1.000(} 

## ;;:.9972 ;1, 

# QCf1ti ),otJ§:z. 

### 5.-;;."7c5 

## J. 5 

# - Average

Final Weight 

## .:t-'d'501**~.~.:<)~** 

## 2,**tfl{/~** 

## 5.DO**I~** 3.dJOO 

# 7­ .:1_ 9?o.z 

## .<, 7'?<f 

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## "191-3 

# C Tllre Net Wcigllt
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# Cn MPR RHRNSIVR I

,

Check Weight 

# _E EMISSION Check Weight 

# ==- S-= SERvrCES Check Weight

## FINAL 

# WEIGHT WEIGHING SHEET
Time Dnle Analyst
ID No. Run 

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# 1£790, 

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# < n 70.0'
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## '12.;).. It:? 

# tffol 

# Itt:;., 65tl J6tJ_6/3 

## '5 166_ ff3:<

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# .

COMPREHENSIVE 

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# I SERVICES I c:heck Weicht I

## --- 

## FINAL WEIGHT WEIGHING SHEET
Time Date Analyst
In No. RUII



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# Appendix C Field Data FormsRun No. Location: Cargill Truck Receiving Date: Oct19,99 Project 

### # 8799 % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected( Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= Wet Molecular Weight= Sampling Time' (Minutes)= Nozzle Diameter(lnches)= Stack Diameter (lnches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate loading - Total Catch Including Impingers Particulate Weight Net (g)= Particulate loading, Dry Std, 68 Deg (grlscf)= Emission Rate (lb/hr)= Percent Impinger Catch= 98.2 390.400 566.906 

### 0.995 0.001 175.623 178.852



### 29.75 

### -10.00 29.01 21 .00

0.00 17.0 0.5 57.6 1.67 1.4500 47 28.84 28.79 240.0 0.185 38.00

7.88 0.84 ·1.2008

4,031 31,747 31,912

0.0037 0.0003 0.09

0.0188 0.0016 0.44 80.32Run No. 

### 2 Location: Cargill Truck Receiving Date: Oct19,99 Project 

### # 8799 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu FUmin)'" Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 De9)= Barometric Pressure 

### (in Hg) 

# = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected( Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= Wet Molecular Weight= Sampling Time (Minutes):::: Nozzle Diameter(lnches)= Stack Diameter (Inches)= Stack Area (Square Feet) :::: Pitot Coefficient:::: Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, fUmin)= Flow Rate (Actual. Cubic fUmin)= Flow Rate (Std, Dry, Cubic fUmin 68 De9)= Particulate Loading - Front Half ParticUlate Weight Net (9)= Patlculate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers Particulate Weight Net (g)= Particulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Percent Impinger Catch:::: 98.5 567.300 739.792 0.995 0.001 171.630 173.946

29.75 -10.00 

### 29.01 

### 21 .00

0.00 

### 24.2

0.7 60.0 1.57 1.3708 50 28.84 28.77 240.0 0.185 38.00

7.88 0.84 1.1701

3,942 31,047 30.946

0.0033 0.0003 0.08

0.0184 0.0016 0.43 82.07Run No. 3 Assumed 1 Omg Location: Cargill Truck Receiving Date: Oct 20,99 Project 

### # 8799 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen :::; Percent Carbon Dioxide= Moisture Collected( Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= Wet Molecular Weight= Sampling Time'{Minutes)= Nozzle Diameter(lnches)= Stack Diameter (Inches): Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= Particulate Loading • Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lb/hr)= Particulate Loading**~** Total Catch Including Impingers Particulate Weight Net (g)= Particulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lblhr)= Percent Impinger Catch= 99.2 740.000 921.630 0.995 0.001 180.722 183.014



### 29.75 

### 10.00 29.01 21 .00

0.00

2.0 

### 0.1 60.6 

### 1.72 1.4667 43 28.84 28.83 240.0 0.185 38.00

7.88 0.84 

### 1.2082

4,037 31,791 32,342

0.0025 0.0002 0.06



### 0.0100 0.0008 0.23 75.00Run No. 

### 3 Location: Cargill Truck Receiving Date: Oct 20,99 Project 

### # 8799 % Isokinetic= Initial Meter Volume (Cubic Feet)= Rnal Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)"" Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected{ml)= Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= Wet Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Diameter (Inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)== Particulate Loading**~** Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lb/hr);::: ParticUlate Loading - Total Catch Including Impingers Particulate Weight Net (g)= Particulate Loading, Dry Std. 68 Deg (grlscn;::: Emission Rate (Ib/hr)= Percent Impinger Catch:::: 

### 99.2 740.000 921.630 0.995 0.001 180.722 183.014



### 29.75 -10.00 29.01 21 .00

0.00

2.0 0.1 60.6 1.72 1.4667 43 28.84 28.83 240.0 0.185 38.00

7.88 0.84 1.2082 4,037 31,791 32,342

0.0025 0.0002 0.06

0.0082 0,Q007 0.19 69.51

### COMPREHENSIVE EMISSION SERVICES

Project Number--"K"""'--"71

___ 

## Cf

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# ')**P~""Tl':A.'.!i** ADOR£SS

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# ;1!/ 7 8 9

# Appendix D Pretest CalibrationsMETER CALIBRATION Operator BB K Factor

### ~ate 

### Oct 11, 1999 Meter Number 

# ·t.· revious Y Factor 1.000 Orifice Number

RUN 1 Meter Volume Final Cubic Feet 480.705 initial Cubic Feet 475.600

Net Cubic Feet 5.105 Meter Temperature Inlet Initial Oeg. F 76.0 Final Deg. F 77.0 Outlet Initial Oeg. F 76.0 Final Oeg. F 76.0 Avg. Meter Temp Deg. F 76.3 Time 

### sec 480.0 Meter Delta H inches H2O 1.20**,·~8arometric** Pressure inches Hg 29.90 ;" 

### .. ",

; 

# .

...**~.:.** .' Room Temperature Initial Oeg. F 75.0 Final Oeg. F 

### 74.0 Avg.Room Temperature Deg. F 74.5 Pump Vacuum inches Hg 21 Vcr (std) dscf 5.015 Vm (std) dscf 5.036 Y Factor 0.996 Delta 

### H@ 1.665 Average Y 0.998 Average Delta 

### H@ 1.672 

### +/- 2% Criteria Percent of Avg Y 0.23 PASS 

### +1· 5% Criteria Percent of Final Y 

### 0.19



### ... ./ PASS 0.4847 

### 1 

### 6

RUN 2

485.884 480.800 5.084



### 77.0 78.0 76.0 76.0 76.8 480.0

1.20 29.90

75.0 75.0 75.0

21 5.013 5.011 1 .000 1.680

1

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## BB BRACKET ORIFICES: Date 

### Oct 11,1999 Orifice No.1 

### 6 

# I'd**~::~;;.** K Factor 

### 0.4847 Meter Number 

### 1 Orifice No. 2 

### 4 Meter Y Factor 

### 0.998 K Factor 

### 0.2533 ORIFICE 

### #1 ORIFICE #2 Meter Volume Final Cubic Feet 491.265 

### 496.951 Initial Cubic Feet 

### 486.200 491.600

Net Cubic Feet 

### 5.065 5.351 Meter Temperature Inlet Initial Oeg.F 

### 78.0 78.0 

## , Final Oe9. F 

### 78.0 79.0 Outlet Initial Oeg. F 

### 76.0 77.0 Final Oeg. F 

### 77.0 78.0 Avg. Meter Temp Oeg. F 

### 77.3 78.0 Time 

## sec 480.0 960.0 Meter Delta H inches 

### H2O 1.20 

### 0.31

r**~&arometric** Pressure inches Hg 

### 29.90 29.90 

### '''')**\~~** . Room Temperature Initial Oeg. F 

### 76.0 76.0 Final Oeg. F 

### 75.0 76.0 Avg.Room Temperature Oeg. F 

### 75.5 76.0 Pump Vacuum inches Hg 

### 20 25 Vcr (std) dscf 

### 5.010 5.234 Vm (std) dscf 

### 4.987 5.250 Y Factor (brackets) 

### 1.005 0.997 +/- 2% Criteria Percent of Y 

### 0.66 0.10 PASS PASS

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### Cate Oct 10, 1999 Meter Number 

### )revious Y Factor 1.004 Orifice Number

Meter Volume Final Initial

Net Cubic Feet Cubic Feet Cubic Feet RUN 1 838.495 833.300 5.195 Meter Temperature Inlet
Outlet Avg. Meter Temp Initial Final Initial Final Ceg. F Oeg. F Oeg. F Deg. F Oeg. F 56.0 60.0 52.0 59.0 56.8 Time Meter Celta H Barometric Pressure 

## sec inches H2O inches Hg 960.0 

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### dscf dscf 5.291 5.307 0.997 1.713 Average Y Average Delta H@ 1.001 1.713 +/- 

### 2% Criteria Percent of Avg Y PASS 0.41**+/~** 

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... 

### PASS 0.2533 

### 2 4

RUN 2

843.793 838.600 5.193

61.0 65.0 59.0 63.0 62.0 960.0

0.32 29.90

66.0 68.0 67.0



### 25 5.279 5.251 1.005 1.714

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## BB BRACKET ORIFICES:

.. Date Oct 11,1999 Orifice No. 1 

### 1 K Factor 

### 0.5055 Meter Number 

### 2 Orifice No.2 

### 4 Meter Y Factor 

### 1.001 K Factor 

### 0.2533 ORIFICE 

### #1 ORIFICE 

### #2 Meter Volume Final Cubic Feet 

### 860.070 854.729 Initial Cubic Feet 

### 854.800 849.500

Net Cubic Feet 

### 5.270 5.229 Meter Temperature inlet Initial Oeg. F 

### 69.0 

### 68.0 Final Oeg. F 

### 69.0 

### 69.0 Outlet Initial Oeg. F 

### 68.0 67.0 Final Oe9. F 

### 69.0 68.0 Avg. Meter Temp Oeg. F 

### 68.8 68.0 Time sec 

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### 29.90 29.90 ::**~ ~.**  :: "



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### 72.0 

### 68.5 f. Pump Vacuum inches Hg 21 

### 25 Vcr (std) dscf 

### 5.242 5.271 Vm (std) dscf 

### 5.275 5228 Y Factor (brackets) 

### 0.994 1.008 

### +/- 2% Criteria Percent of Y 

### 0.72 0.73 PASS PASS

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# I METER CALIBRATION Operator BB K Factor ,--: Date Oct 15, 1999 Meter Number :: 'revious Y Factor 0.997 Orifice Number

RUN 1 Meter Volume Final 

### Cubic Feet 374.098 Initial Cubic Feet 368.900

Net Cubic Feet 5.198 Meter Temperature Inlet Initial Oeg. F 54.0 Final Oeg. F 62.0 Outlet Initial Deg. F 52.0 Final Deg. F 58.0 Avg. Meter Temp Deg. F 56.5 Time sec 960.0 

### Meter Delta H inches H2O 0.30

. Barometric Pressure inches Hg 29.23

Room Temperature Initial Deg. F 69.0 Final Deg. F**~70.0** 

### Avg.Room Temperature Deg. F 69.5 Pump Vacuum inches Hg 23 Vcr (std) dscf 5.148 Vm (std) dscf 5.193 Y Factor 0.991 Delta H@ 1.673 Average Y 0.995 Average Delta H@ 1.689**+/~** 

### 2% Criteria Percent of Avg Y 0.37 PASS +/- 

### 5% Criteria Percent of Final Y 0.20 PASS 0.2533 

### 4 4



### RUN 2

379.415 374.200 5.215

62.0 66.0 59.0 63.0 62.5 960.0

0.31 29.23

71.0 70.0 70.5

23 5.143 5.150 0.999 1.705ORIFICE BRACKETING Operator 

## SS BRACKET ORIFICES: 

## _Date

Meter Number Meter Y Factor 

### Oct 15,1999 

### 4 0.997 Orifice No. 1 K Factor Orifice No.2 K Factor 4 0.2533 

### 1 0.5055
Meter Volume Final Initial

Net Cubic Feet Cubic Feet Cubic Feet ORIFICE #1 384.726 379.500 5.226 ORIFICE #2 390.145 384.800 5.345 Meter Temperature inlet Initial Final Outlet Initial Final Avg. Meter Temp Oeg.F Oeg. F Deg. F Oeg. F Oeg. F 66.0 69.0 64.0 67.0 66.5 68.0 70.0 67.0 69.0 68.5 

### L

Time Meter Delta H Barometric Pressure 

### sec inches H2O

inches Hg 960.0 0.31 29.23 480.0 1.40 29.23 Room Temperature initial Final Avg.Room Temperature Oeg. F Oeg. F Oeg. F 70.0 71.0 70.5 72.0 71.0 71.5 Pump Vacuum inches Hg 24 

### 21 Vcr (std) Vm (std) Y Factor (brackets) dscf dscf 5.143 5.122 1.004 5.127 5.233 0.980 

### +/- 2% Criteria Percent of Y PASS 0.72 PASS 1.73, "**--..-~.** : -. 

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# Appendix E Posttest CalibrationsMETER CALIBRATION Operator DO K Factor Date 

### Oct 25, 1999 Meter Number Previous Y Factor 0.998 Orifice Number

RUN 1 Meter Volume Final Cubic Feet 147.279 Initial Cubic Feet 142.200

Net Cubic Feet 5.079 Meter Temperature Inlet Initial Oeg. F 61.0 Final Oeg. F 66.0 Outlet Initial Oeg. F 60.0 Final Oeg. F 65.0 Avg. Meter Temp Oeg. F 63.0 Time 

## sec 780.0 Meter Delta H inches H2O 0.43 Barometric Pressure inches Hg 29.60 Room Temperature Initial Oeg. F 69.0 Final Oeg. F 69.0 Avg.Room Temperature Oeg. F 69.0 Pump Vacuum inches Hg 24 Vcr (std) dscf 5.074 Vm (std) dscf 5.076 Y Factor 1 .000 Delta 

### H@ 1.614 Average Y 0.997 Average Delta 

### H@ 1.588 

### +/- 2% Criteria Percent of Avg Y 0.29 PASS 

### +/- 5% Criteria Percent of Final Y 0.12 PASS 0.3033 

### 1 

### 5

RUN 2 152.445 147.300 5.145

66.0 68.0 65.0 68.0 66.8 780.0

0.43 29.60

69.0 69.0 69.0

23 5.074 5.105 0.994 1.562

# - 

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_____ _ 

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# _""£

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### 25, 1999 Orifice No. 

### 1 5 K Factor 

### 0.3033 Meter Number 

### I Orifice No. 

### 2 2 Meter Y Factor 

### 0.997 K Factor 

### 0.6426 ORIFICE #1 ORIFICE #2 Meter Volume Final Cubic Feet 

### 157.820 164.169 Initial Cubic Feet 

### 152.600 158.200

Net Cubic Feet 

### 5.220 5.969 Meter Temperature Inlet Initial De9. F 

### 71.0 72.0 Final Deg. F 

### 72.0 72.0 Outlet Initial Deg. F 

### 71.0 72.0 Final De9. F 

### 72.0 72.0 Avg. Meter Temp De9. F 

### 71.fi 72.0 Time 

## sec 780.0 420.0 Meter Delta 

### H inches 

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### 29.60 29.60 Room Temperature Initial Deg. F 

### 69.0 69.0 Final De9. F 

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### 69.0 69.0 Pump Vacuum inches Hg 

### 24 19 Vcr (std) dscf 

### 5.074 5.789 Vm (std) dscf 

### 5.134 5.889 Y Factor (brackets) 

### 0.988 

### 0.983 +/- 2% Criteria Percent of Y 

### 0.86 1.40 PASS PASS

## EHACK!::IING 

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## BB K Factor Date 

### Oct 25, 1999 Meter Number Previous Y Factor 1.001 Orifice Number

Meter Volume Final Initial

Net Cubic Feet Cubic Feet Cubic Feet RUN 1 104.566

99.500

5.066 Meter Temperature Inlet
Outlet Avg. Meter Temp Initial Final Initial Final Deg. F Deg. F Deg. F Deg. F Deg. F 

### 49.0 

### 58.0 44.0 56.0 

### 51.8 Time Meter Delta H Barometric Pressure 

## sec inches H2O inches Hg 

### 960.0 0.31 29.60 Room Temperature Avg.Room Temperature Initial Final Deg. F Deg. F Deg. F 6B.O 66.0 67.0 Pump Vacuum inches Hg 24 Vcr (std) Vm (std) Y Factor Delta 

### H@ dscf dscf 5.226 5.173 1.010 1.797 Average Y Average Delta 

### H@ 0.995 1.707 

### +/- 2% Criteria Percent of Avg Y PASS 

### i.48
+/- 5% Criteria Percent of Final Y PASS 0.56 0.2533 

### 2 4

RUN2 

## ,

109.905 104.600 5.305

59.0 64.0 57.0 63.0 60.8 960.0

0.31 29.60

67.0 69.0 68.0

24 5.221 5.323 0.981 1.617

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# ----­ORIFICE BRACKETING Operator DD BRACKET ORIFICES: Date Oct. 25, 1999 Orifice No. 1 

### 4 K Factor 0.2533 Meter Number 

### 2 Orifice No.2 

### I Meter Y Factor 0.995 K Factor 0.5055 ORIFICE #1 ORIFICE #2 Meter Volume Final Cubic Feet 115.215 120.752 Initial Cubic Feet 110.000 115.500

Net Cubic Feet 5.215 5.252 Meter Temperature Inlet Initial Deg. F 66.0 68.0 Final Deg. F 67.0 68.0 Outlet Initial Deg. F 64.0 67.0 Final Deg. F 67.0 68.0 Avg. Meter Temp Deg. F 66.0 67.8 Time sec 960.0 480.0 Meter Delta H inches H2O 0.32 1.40 Barometric Pressure inches Hg 29.60 29.60 Room Temperature Initial Deg. F 67.0 68.0 Final De9. F 68.0 68.0 Avg.Room Temperature De9. F 67.5 68.0 Pump Vacuum inches Hg 24 20 Vcr (std) dscf 5.223 5.209 Vm (std) dscf 5.181 5.214 Y Factor (brackets) 1.008 0.999 +/- 2% Criteria Percent of Y 1,32 0.41 PASS PASS

## ERACKETiNG 

# WORK SHEET
"..**~!** 

### G \:i·':· 

### Operatc!: ----:'1)=-v

_____ Meter 

### 1.0.

__ 

## 2_---

___ Data: 

# lvJlS'/11 I 

### I K F'3.c:cr 

### NO.1
_ ..... ' d"'""'5"3-.l..:::::.3o.L-

__ _ 

### FrsvicL's Y F'3.c:cr ! 

## q'if' :< Fac:crNo. 2 _.L...'

### -...:::.>O:::;.f).~~~ ____

' 

## ..

initial 

## 110,00 

# I !NLE 

## I initial "C:::ai 

# I 'F 

# I &7 

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### j 0<: 

# . I (1 

# I G7 F:m>I 

# I OF 

# I (07 

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# q
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### ·'i.ljD



# . Maler t:H in, P

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## p /. 'i 

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# I , 

## 31­ Earcmettic rt2ssura**in~** Eg 

# I I lq. t 

## ::<4[" Rccm Terrq:efail.:re



# . Initial .c;- 

### , 

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## C:.7 

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__ 

# S

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":**.~** .. ". ...- .. -

___ , A.-'METER CALIBRATION Operator BB K Factor

. .Date Nov. 

### 1, 1999 Meter Number }revious Y Factor 

### 0.995 Orifice Number

RUN 

### 1 Meter Volume 

### Final Cubic Feet 

### 79.673 

### Initial Cubic Feet 

### 74.500

Net Cubic Feet 

### 5.173 Meter T emperatlJre Inlet Initial Oeg. F 

### 70.0 Final Oeg. F 

### 72.0 Outlet Initial Deg. F 

### 69.0 Final Deg.F 

### 72.0 Avg. Meter Temp Deg.F 

### 70.8 Time 

## sec 780.0 Meter Delta 

### H inches 

### H2O 0.45 " t;:larometrfc Pressure inches 

### Hg 

### 29.65

Room Temperature Initial Oeg. F 

### 73.0 Final Oeg. F 

### -71 .0 Avg. Room Temperature Deg. F 

### 72.0 Pump Vacuum inches Hg 

### 23 Vcr (std) dscf 

### 5.069 Vm (std) dscf 

### 5.103 Y Factor 

### 0.993 Delta H@ 

### 1.620 Average Y 

### 0.993 Average Delta H@ 

### 1.637 +/- 2% Criteria Percent of Avg Y 

### 0.01 PASS 

### +/- 5% Criteria Percent of Final Y 

### 0.20 PASS 

### 0.3033 4 

### 5

RUN 

### 2 84.884 79.700 5.184

72.0 73.0 72.0 73.0 72.5 780.0

0.46 29.65

73.0 74.0 73.5

23 5.061 5.098 0.993 1.653

## CONSOLE WORK SHEET

t ,**.~** 

### Cr:eratcr.

### _B..=...oB~ 

# ____**Kr~r.~·3~·~o=3~~==========** Oae: 

# rP: ( - 

# 9'1 Met=r 1.0. 

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### SD."'i!GS

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## 'J'

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# ,--**~----**

# 4 Meter 1.0. _....:..--

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# I I '/ I



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## 7 

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# I 

# I I " " ," '. .c: 

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# I I 73 

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# I 

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## - . 

# I ini;5E1 '=p 

# 7,-/ 

# I I I I 

# [ I I 

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# I .1 :n .. E; 

# I d-,) I 

# fJJQ 

# IORIFICE BRACKETING Operator 

## BB BRACKET ORIFICES: 

# ::Eate Nov 1,1999 Orifice No. 1 

### 5 K Factor 0.3033 Meter Number 

### 4 Orifice No. 2 

### 2 Meter Y Factor 0.993 K Factor 0.6462 ORIFICE 

### #1 ORIFICE #2 Meter Volume Final Cubic Feet 90.107 96.272 Initial Cubic Feet 

### 84.900 90.300

Net Cubic Feet 5.207 5.972 Meter Temperature Inlet Initial Oeg. F 73.0 75.0 Final Oeg. F 74.0 75.0 Outlet Initial Oeg. F 73.0 74.0 Final Oeg. F 74.0 74.0 Avg. Meter Temp 

### Deg. F 73.5 74.5 Time sec 780.0 420.0 Meter Delta H inches H2O 0.47 2.20 :- Barometric Pressure inches Hg 29.65 29.65

Room Temperature Initial Oeg. F 74.0 74.0 Final Oeg. F 74.0 74.0 Avg. Room Temperature Oeg. F 74.0 74.0 Pump Vacuum inches Hg 23 

### 20 Vcr (std) dscf 5.059 5.804 Vm (std) dscf 

### 5.111 5.876 Y Factor (brackets) 0.990 0.988 

### +/- 2% Criteria Percent of Y 0.31 

### 0.53 PASS PASS

# Appendix F Process Data

# ---------------------------- Compliance Emission Test 

### Operating Data
Owner: Car&!ll, Sioux City Date: October 19-22 Source:EP #26 - Grain**Rec~iving** 11 Permit 

### #: 96-A-1253-S2

Maximum Continuous Process Rate (Manufacturer's Rating) 1500 Tonslhr.soybeans Hislorical Average Process Rate'----

______________________ _ Historical Maximum Process Rate Types and Sources (if any) of Fuels normally 8umed,_N_T_IA

______________ _ Type of Fuel Bumed During this ._ .... ____________________ _ If Fuel is used Approximate Quantities of each listed above burned**Annually_N;;..;./:.;.A~** _____ _ Recycling Capability Yes

__ _ No 

# X Recycling in Progress Yes

__ _ No 

## X Erocass Data**O\~** jog Ryns

Process Rate . (gallhr, Iblhr. tonslhr, etc ... ) Process Rate Wet Percent Moisture ('Yo) Process Rate Dry How Process Rate was Determined Run 1 Run 2­ Run 3 515.2 tonslhr 466.4 tonslbr 419.6 tonslhr

process scales

Person Responsible for Data,

__________ -'B'-o....,;b-:-S'-u_nd_li....;·e

___________**~;-:;** < /-" Signature

____________

### ---',-\~l ..;.X;;;;.

__ •• '-_':..=-=--

______ _

·-_-

### -..::.J~.'.!;.:-..::.)_.**~_-** \._1. ..,:\!.",,"' ..;_":..­ Tlt1e/Position,

____________**F:..:a:.:c.:.;il;.:,ity~S.;;..u;;,ip:..:.e.:.:rin=te=nd=e;;;;;nt'----** ___________

d Please indicate 

### in the same units 8S your historical information

### AIR POLLUTION CONTROL EQUIPMENT OPERATING DATA
Plant Cargill,Inc. LOC3rionSioux City 

### Source Type ;.part!

__

·cul 

### ate-----
__ .......... *

___ _ 

### Rated. 

### Produc:rion 

### Date

____ 

# -. T.une

____ 

### Actu:al Production 

# --------------------- RuaNo.

---------­ Air Flaw Data

__**~~_----_** 

### Mechanical Collector: 'Tube 

### Dia. in.. 

### Number of!ubes Design 6p

______ in. 

### HiO Gas Temp

__ _ Observed ap 

### in**H~** Design cfm/tube @ Olmrnd t.\p @

___ _ Fan Rated H.P. Openlting Volts Operating Amps

____ _ Electrostatic Precinitator Sect)nd:uy 

### Field No. Secondary Primary 

### Primary SparkRa:te Voltage (volts) 

### Current (amps) Voltage (KV) 

### Current (ma) (per min)

Scrubber: 

### Type
___________ Ap(aaoss scrubber}

_________ in**H~O.** Fan Rated HP Operating Volts
______ Operating Amps

_____ _ 

# - Liquid Cin:uIation Rate gal/min. 

### % Make-up
________ Blowdown
______ gpm Scrubbing 

### Water Change Interval

___________ -------_------

__ _ Settling Tank Cleaning Interval Baghouse:**p~..positive Nega~**  No. Compa:mnents 

### Type Cle::m.ing 

### Cleon Cy cle' :min Avg. BaghouseAp 2.6 inH:P ilpRange 

### Fan: Rated H.P. Ope:ating Volts Operating Amps Cvclon;: 

### Type 6p inH.<J Diameter 

### FanRatedEP Ope Iating Volts Operating Amps
Penion Resp.lnsible for Data**-=Bo=b.;;;;S.;;;un;;;;d;.;.;li;.:;.e~-------- ~')**  t,**~'** :.' 

### SignatUre

## ,~:t'-\J 

# \. \. /,**~.** ;!r \.';4. _' TItle/Position Facility Superintendent

10

# Appendix G Opacity CertificationDEPARTMENT OF NATURAL RESOURCES PAUL W. JOHNSON, DIRECTOR THOMAS J. VILSACK. GOVERNOR SALLY J. PEDERSON, L T. GOVERNOR May 

### 12, 1999 Doug Ostrander C.E.S 1112 Maple West Des Moines IA 50265 Dear Mr. Ostrander: We wish to acknowledge your attendance at the Spring 1999 session of the visible emissions recertification program conducted by the University of Iowa Hygienic Laboratory on April 20-21, 1999. The records show that you have suC making visual determination of**~** 

### specifiedin subrule 567--29.1 of L 

### Transmitted with this letter a I 

### are qualified to make visible emi Chapter 567--29 of the Iowa Adminis

Sincerely,

# ~a~ddP' !/ 

### DOUGLAS A. CAMPBELL AIR QUALITY BUREAU Enclosure cc: Pamela Kastle, U.H.L.

7900 HICKMAN ROAD, SUITE 1/ URBANDALE, IOWA 50322/515-242·5100 I FAX 515-242·5094DEPARTMENTOFNATURALRESOURCES ST

...

TEOF 

# I --.l
PAUL W. JOHNSON. DIRECTOR THOMAS J, VILSACK. GOVERNOR SALLY J. PEDERSON. LT. GOVERNOR 

### May 12, 1999 Jay 

### Titus CES 1112 Maple St West Des Moines IA 50265 Dear Mr. We wish to acknowledae your attendance at the Spring 1999 session of the emissions recertification program conducted by the University of Iowa Hygienic Laboratory on April 20-21, 1999. The records show that you have successfully met the criteria making sual determination of the opacity of emissions, as specified in subrule 567--29.1 of the Iowa Administrative Code. Transmitted with this letter is a certificate indicating that you 

### are quali to make visible emissions evaluations pursuant to Chapter 567--29 of the Iowa Administrative Code. Notice of 1 1999 session will be issued around the end of September and you will be informed of the exact date and location of the next session. 

# @el Y ,**O~~p**

# DOUG~CAMPBELL AIR BUREAU Enclosure
cc: 

### Pamela Kastle, U.H.L.**\'IDillg~I~~",;QILWrr~milt}fe.&1t:** l1!1S IS TO Cl:Rl1Fl1 1'HA1'**~~g~~b~~~%~~~~~1l~~::;O{ viNc:\t:\dl:ft!lcMt.4sorwI.(:j>~o!** **l'_~** ..... p.,.M

...... on!llt

7900 HICKMAN ROAD. SUITE 1/ URBANDALE, IOWA 50322/515-242-5100 I FAX 515-242-5094