Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-001 Date Collected: 09/11/2013 Date Received: 9/12/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg < 0.20 ng/L U 0.50 0.20 TLT 09/18/2013 EPA 1631E

Sample Number: 133724-002 Date Collected: 09/11/2013 Date Received: 9/12/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 7.43 ug/L 0.050 0.010 DPC 09/18/2013 13:35 EPA 200.8

Arsenic, As 63.3 ug/L 0.10 0.030 DPC 09/18/2013 13:35 EPA 200.8

Barium, Ba 763 ug/L 0.10 0.020 DPC 09/18/2013 13:35 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 09/18/2013 15:04 EPA 200.7

Cadmium, Cd 246 ug/L 0.050 0.010 DPC 09/18/2013 13:35 EPA 200.8

Chromium, Cr 204 ug/L 0.20 0.040 DPC 09/18/2013 13:35 EPA 200.8

Cobalt, Co 282 ug/L 0.020 0.0040 DPC 09/18/2013 13:35 EPA 200.8

Copper, Cu 220 ug/L 0.050 0.010 DPC 09/18/2013 13:35 EPA 200.8

Lead, Pb 104 ug/L 0.010 0.0020 DPC 09/18/2013 13:35 EPA 200.8

Mercury, Hg 181000 ng/L 5000 2000 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 171 ug/L 0.050 0.010 DPC 09/18/2013 13:35 EPA 200.8

Nickel, Ni 1740 ug/L 0.20 0.050 DPC 09/18/2013 13:35 EPA 200.8

Selenium, Se 649 ug/L 0.50 0.20 DPC 09/18/2013 13:35 EPA 200.8

Silver, Ag 0.174 ug/L 0.010 0.0020 DPC 09/18/2013 13:35 EPA 200.8

Thallium, Tl 15.1 ug/L 0.050 0.0020 DPC 09/18/2013 13:35 EPA 200.8

Tin, Sn < 150 ug/L U 500 150 DAM 09/18/2013 15:04 EPA 200.7

Titanium, Ti 106 ug/L 100 15 DAM 09/18/2013 15:04 EPA 200.7

Zinc, Zn 2630 ug/L 0.50 0.10 DPC 09/18/2013 13:35 EPA 200.8

Aluminum, Al 8.14 mg/L 0.0010 0.0003 DPC 09/18/2013 13:35 EPA 200.8

Boron, B 461 mg/L 1.0 0.20 DAM 09/18/2013 15:04 EPA 200.7

Calcium, Ca 6960 mg/L 1.0 0.20 DAM 09/18/2013 15:04 EPA 200.7

Iron, Fe 78.4 mg/L 2.5 0.50 DAM 09/18/2013 15:04 EPA 200.7

Magnesium, Mg 4160 mg/L 0.50 0.10 DAM 09/18/2013 15:04 EPA 200.7

Manganese, Mn 94.3 mg/L 0.025 0.0050 DAM 09/18/2013 15:04 EPA 200.7

Potassium, K 74.6 mg/L 2.5 0.35 DAM 09/18/2013 15:03 EPA 200.7

Sodium, Na 374 mg/L 1.5 0.40 DAM 09/18/2013 15:03 EPA 200.7

Strontium, Sr 25.6 mg/L 0.050 0.015 DAM 09/18/2013 15:03 EPA 200.7

Ammonia, NH3, as N < 0.020 mg/L U 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 0.56 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 39.9 mg/L 0.10 0.020 DMM 09/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 1 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-002A Date Collected: 09/11/2013 Date Received: 9/12/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.21 ug/L 0.050 0.010 DPC 09/18/2013 13:40 EPA 200.8

Arsenic, As 2.17 ug/L 0.10 0.030 DPC 09/18/2013 13:40 EPA 200.8

Barium, Ba 57.9 ug/L 0.10 0.020 DPC 09/18/2013 13:40 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 09/18/2013 15:08 EPA 200.7

Cadmium, Cd 159 ug/L 0.050 0.010 DPC 09/18/2013 13:40 EPA 200.8

Chromium, Cr 0.6 ug/L 0.20 0.040 DPC 09/18/2013 13:40 EPA 200.8

Cobalt, Co 209 ug/L 0.020 0.0040 DPC 09/18/2013 13:40 EPA 200.8

Copper, Cu 4.72 ug/L 0.050 0.010 DPC 09/18/2013 13:40 EPA 200.8

Lead, Pb 0.134 ug/L 0.010 0.0020 DPC 09/18/2013 13:40 EPA 200.8

Mercury, Hg 57.1 ng/L 10 4.0 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 97.0 ug/L 0.050 0.010 DPC 09/18/2013 13:40 EPA 200.8

Nickel, Ni 1300 ug/L 0.20 0.050 DPC 09/18/2013 13:40 EPA 200.8

Selenium, Se 251 ug/L 0.50 0.20 DPC 09/18/2013 13:40 EPA 200.8

Selenite, Se+4 (Hydride) 176 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.014 ug/L 0.010 0.0020 DPC 09/18/2013 13:40 EPA 200.8

Thallium, Tl 7.82 ug/L 0.050 0.0020 DPC 09/18/2013 13:40 EPA 200.8

Tin, Sn < 150 ug/L U 500 150 DAM 09/18/2013 15:08 EPA 200.7

Titanium, Ti < 15 ug/L U 100 15 DAM 09/18/2013 15:08 EPA 200.7

Zinc, Zn 731 ug/L 0.50 0.10 DPC 09/18/2013 13:40 EPA 200.8

Aluminum, Al 0.0644 mg/L 0.0010 0.0003 DPC 09/18/2013 13:40 EPA 200.8

Boron, B 475 mg/L 1.0 0.20 DAM 09/18/2013 15:08 EPA 200.7

Calcium, Ca 732 mg/L 1.0 0.20 DAM 09/18/2013 15:08 EPA 200.7

Iron, Fe < 0.50 mg/L U 2.5 0.50 DAM 09/18/2013 15:08 EPA 200.7

Magnesium, Mg 3940 mg/L 0.50 0.10 DAM 09/18/2013 15:08 EPA 200.7

Manganese, Mn 94.2 mg/L 0.025 0.0050 DAM 09/18/2013 15:08 EPA 200.7

Potassium, K 73.8 mg/L 2.5 0.35 DAM 09/18/2013 15:07 EPA 200.7

Sodium, Na 377 mg/L 1.5 0.40 DAM 09/18/2013 15:07 EPA 200.7

Strontium, Sr 9.41 mg/L 0.050 0.015 DAM 09/18/2013 15:07 EPA 200.7

Mountaineer Plant, 133724 Page 2 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-003 Date Collected: 09/11/2013 Date Received: 9/12/2013

Primary Clarifier Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.69 ug/L 0.050 0.010 DPC 09/18/2013 13:45 EPA 200.8

Arsenic, As 3.36 ug/L 0.10 0.030 DPC 09/18/2013 13:45 EPA 200.8

Barium, Ba 78.3 ug/L 0.10 0.020 DPC 09/18/2013 13:45 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 15:12 EPA 200.7

Cadmium, Cd 129 ug/L 0.050 0.010 DPC 09/18/2013 13:45 EPA 200.8

Chromium, Cr 4.4 ug/L 0.20 0.040 DPC 09/18/2013 13:45 EPA 200.8

Cobalt, Co 177 ug/L 0.020 0.0040 DPC 09/18/2013 13:45 EPA 200.8

Copper, Cu 7.42 ug/L 0.050 0.010 DPC 09/18/2013 13:45 EPA 200.8

Lead, Pb 0.850 ug/L 0.010 0.0020 DPC 09/18/2013 13:45 EPA 200.8

Mercury, Hg 599 ng/L 50 20 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 166 ug/L 0.050 0.010 DPC 09/18/2013 13:45 EPA 200.8

Nickel, Ni 1130 ug/L 0.20 0.050 DPC 09/18/2013 13:45 EPA 200.8

Selenium, Se 367 ug/L 0.50 0.20 DPC 09/18/2013 13:45 EPA 200.8

Silver, Ag 0.030 ug/L 0.010 0.0020 DPC 09/18/2013 13:45 EPA 200.8

Thallium, Tl 9.88 ug/L 0.050 0.0020 DPC 09/18/2013 13:45 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 15:12 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 15:12 EPA 200.7

Zinc, Zn 142 ug/L 0.50 0.10 DPC 09/18/2013 13:45 EPA 200.8

Aluminum, Al 0.267 mg/L 0.0010 0.0003 DPC 09/18/2013 13:45 EPA 200.8

Boron, B 419 mg/L 0.20 0.040 DAM 09/18/2013 15:12 EPA 200.7

Calcium, Ca 755 mg/L 0.20 0.040 DAM 09/18/2013 15:12 EPA 200.7

Iron, Fe 0.701 mg/L 0.50 0.10 DAM 09/18/2013 15:12 EPA 200.7

Magnesium, Mg 3550 mg/L 0.10 0.020 DAM 09/18/2013 15:12 EPA 200.7

Manganese, Mn 75.0 mg/L 0.0050 0.0010 DAM 09/18/2013 15:12 EPA 200.7

Potassium, K 63.3 mg/L 0.50 0.070 DAM 09/18/2013 15:11 EPA 200.7

Sodium, Na 342 mg/L 0.30 0.080 DAM 09/18/2013 15:11 EPA 200.7

Strontium, Sr 8.53 mg/L 0.010 0.0030 DAM 09/18/2013 15:11 EPA 200.7

Ammonia, NH3, as N 1.55 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.31 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 41.8 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 3 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-003A Date Collected: 09/11/2013 Date Received: 9/12/2013

Primary Clarifier Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.43 ug/L 0.050 0.010 DPC 09/18/2013 13:50 EPA 200.8

Arsenic, As 2.48 ug/L 0.10 0.030 DPC 09/18/2013 13:50 EPA 200.8

Barium, Ba 73.3 ug/L 0.10 0.020 DPC 09/18/2013 13:50 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 15:21 EPA 200.7

Cadmium, Cd 109 ug/L 0.050 0.010 DPC 09/18/2013 13:50 EPA 200.8

Chromium, Cr 1.6 ug/L 0.20 0.040 DPC 09/18/2013 13:50 EPA 200.8

Cobalt, Co 154 ug/L 0.020 0.0040 DPC 09/18/2013 13:50 EPA 200.8

Copper, Cu 2.67 ug/L 0.050 0.010 DPC 09/18/2013 13:50 EPA 200.8

Lead, Pb 0.059 ug/L 0.010 0.0020 DPC 09/18/2013 13:50 EPA 200.8

Mercury, Hg 32.4 ng/L 5.0 2.0 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 157 ug/L 0.050 0.010 DPC 09/18/2013 13:50 EPA 200.8

Nickel, Ni 927 ug/L 0.20 0.050 DPC 09/18/2013 13:50 EPA 200.8

Selenium, Se 320 ug/L 0.50 0.20 DPC 09/18/2013 13:50 EPA 200.8

Selenite, Se+4 (Hydride) 261 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.0090 ug/L J 0.010 0.0020 DPC 09/18/2013 13:50 EPA 200.8

Thallium, Tl 9.81 ug/L 0.050 0.0020 DPC 09/18/2013 13:50 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 15:22 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 15:21 EPA 200.7

Zinc, Zn 104 ug/L 0.50 0.10 DPC 09/18/2013 13:50 EPA 200.8

Aluminum, Al 0.0356 mg/L 0.0010 0.0003 DPC 09/18/2013 13:50 EPA 200.8

Boron, B 413 mg/L 0.20 0.040 DAM 09/18/2013 15:21 EPA 200.7

Calcium, Ca 739 mg/L 0.20 0.040 DAM 09/18/2013 15:21 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/18/2013 15:22 EPA 200.7

Magnesium, Mg 3490 mg/L 0.10 0.020 DAM 09/18/2013 15:21 EPA 200.7

Manganese, Mn 73.6 mg/L 0.0050 0.0010 DAM 09/18/2013 15:21 EPA 200.7

Potassium, K 62.6 mg/L 0.50 0.070 DAM 09/18/2013 15:20 EPA 200.7

Sodium, Na 335 mg/L 0.30 0.080 DAM 09/18/2013 15:20 EPA 200.7

Strontium, Sr 8.33 mg/L 0.010 0.0030 DAM 09/18/2013 15:20 EPA 200.7

Mountaineer Plant, 133724 Page 4 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-004 Date Collected: 09/11/2013 Date Received: 9/12/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.59 ug/L 0.050 0.010 DPC 09/18/2013 13:55 EPA 200.8

Arsenic, As 2.73 ug/L 0.10 0.030 DPC 09/18/2013 13:55 EPA 200.8

Barium, Ba 81.6 ug/L 0.10 0.020 DPC 09/18/2013 13:55 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 15:30 EPA 200.7

Cadmium, Cd 20.3 ug/L 0.050 0.010 DPC 09/18/2013 13:55 EPA 200.8

Chromium, Cr 2.7 ug/L 0.20 0.040 DPC 09/18/2013 13:55 EPA 200.8

Cobalt, Co 59.6 ug/L 0.020 0.0040 DPC 09/18/2013 13:55 EPA 200.8

Copper, Cu 0.92 ug/L 0.050 0.010 DPC 09/18/2013 13:55 EPA 200.8

Lead, Pb 0.890 ug/L 0.010 0.0020 DPC 09/18/2013 13:55 EPA 200.8

Mercury, Hg 159 ng/L 20 8.0 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 196 ug/L 0.050 0.010 DPC 09/18/2013 13:55 EPA 200.8

Nickel, Ni 602 ug/L 0.20 0.050 DPC 09/18/2013 13:55 EPA 200.8

Selenium, Se 330 ug/L 0.50 0.20 DPC 09/18/2013 13:55 EPA 200.8

Silver, Ag 0.0070 ug/L J 0.010 0.0020 DPC 09/18/2013 13:55 EPA 200.8

Thallium, Tl 6.72 ug/L 0.050 0.0020 DPC 09/18/2013 13:55 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 15:31 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 15:30 EPA 200.7

Zinc, Zn 32.3 ug/L 0.50 0.10 DPC 09/18/2013 13:55 EPA 200.8

Aluminum, Al 0.189 mg/L 0.0010 0.0003 DPC 09/18/2013 13:55 EPA 200.8

Boron, B 401 mg/L 0.20 0.040 DAM 09/18/2013 15:30 EPA 200.7

Calcium, Ca 756 mg/L 0.20 0.040 DAM 09/18/2013 15:30 EPA 200.7

Iron, Fe 0.20 mg/L J 0.50 0.10 DAM 09/18/2013 15:31 EPA 200.7

Magnesium, Mg 3360 mg/L 0.10 0.020 DAM 09/18/2013 15:30 EPA 200.7

Manganese, Mn 68.3 mg/L 0.0050 0.0010 DAM 09/18/2013 15:30 EPA 200.7

Potassium, K 60.6 mg/L 0.50 0.070 DAM 09/18/2013 15:29 EPA 200.7

Sodium, Na 329 mg/L 0.30 0.080 DAM 09/18/2013 15:29 EPA 200.7

Strontium, Sr 8.37 mg/L 0.010 0.0030 DAM 09/18/2013 15:29 EPA 200.7

Ammonia, NH3, as N 2.62 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.89 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 35.3 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 5 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-004A Date Collected: 09/11/2013 Date Received: 9/12/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.46 ug/L 0.050 0.010 DPC 09/18/2013 13:59 EPA 200.8

Arsenic, As 2.35 ug/L 0.10 0.030 DPC 09/18/2013 13:59 EPA 200.8

Barium, Ba 71.2 ug/L 0.10 0.020 DPC 09/18/2013 13:59 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 15:48 EPA 200.7

Cadmium, Cd 1.05 ug/L 0.050 0.010 DPC 09/18/2013 13:59 EPA 200.8

Chromium, Cr 1.6 ug/L 0.20 0.040 DPC 09/18/2013 13:59 EPA 200.8

Cobalt, Co 43.1 ug/L 0.020 0.0040 DPC 09/18/2013 13:59 EPA 200.8

Copper, Cu 0.39 ug/L 0.050 0.010 DPC 09/18/2013 13:59 EPA 200.8

Lead, Pb 0.066 ug/L 0.010 0.0020 DPC 09/18/2013 13:59 EPA 200.8

Mercury, Hg 3.5 ng/L 2.0 0.80 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 173 ug/L 0.050 0.010 DPC 09/18/2013 13:59 EPA 200.8

Nickel, Ni 503 ug/L 0.20 0.050 DPC 09/18/2013 13:59 EPA 200.8

Selenium, Se 298 ug/L 0.50 0.20 DPC 09/18/2013 13:59 EPA 200.8

Selenite, Se+4 (Hydride) 261 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 13:59 EPA 200.8

Thallium, Tl 5.39 ug/L 0.050 0.0020 DPC 09/18/2013 13:59 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 15:48 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 15:48 EPA 200.7

Zinc, Zn 22.5 ug/L 0.50 0.10 DPC 09/18/2013 13:59 EPA 200.8

Aluminum, Al 0.0332 mg/L 0.0010 0.0003 DPC 09/18/2013 13:59 EPA 200.8

Boron, B 397 mg/L 0.20 0.040 DAM 09/18/2013 15:48 EPA 200.7

Calcium, Ca 736 mg/L 0.20 0.040 DAM 09/18/2013 15:48 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/18/2013 15:48 EPA 200.7

Magnesium, Mg 3320 mg/L 0.10 0.020 DAM 09/18/2013 15:48 EPA 200.7

Manganese, Mn 67.1 mg/L 0.0050 0.0010 DAM 09/18/2013 15:48 EPA 200.7

Potassium, K 60.3 mg/L 0.50 0.070 DAM 09/18/2013 15:46 EPA 200.7

Sodium, Na 330 mg/L 0.30 0.080 DAM 09/18/2013 15:46 EPA 200.7

Strontium, Sr 8.35 mg/L 0.010 0.0030 DAM 09/18/2013 15:46 EPA 200.7

Mountaineer Plant, 133724 Page 6 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-005 Date Collected: 09/11/2013 Date Received: 9/12/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.2 ug/L 0.050 0.010 DPC 09/18/2013 14:33 EPA 200.8

Arsenic, As 38.9 ug/L 0.10 0.030 DPC 09/18/2013 14:33 EPA 200.8

Barium, Ba 31.1 ug/L 0.10 0.020 DPC 09/18/2013 14:33 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 15:57 EPA 200.7

Cadmium, Cd 1.33 ug/L 0.050 0.010 DPC 09/18/2013 14:33 EPA 200.8

Chromium, Cr 0.2 ug/L 0.20 0.040 DPC 09/18/2013 14:33 EPA 200.8

Cobalt, Co 2.33 ug/L 0.020 0.0040 DPC 09/18/2013 14:33 EPA 200.8

Copper, Cu 0.44 ug/L 0.050 0.010 DPC 09/18/2013 14:33 EPA 200.8

Lead, Pb 0.122 ug/L 0.010 0.0020 DPC 09/18/2013 14:33 EPA 200.8

Mercury, Hg 42.6 ng/L 10 4.0 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 7200 ug/L 0.050 0.010 DPC 09/18/2013 14:33 EPA 200.8

Nickel, Ni 8.17 ug/L 0.20 0.050 DPC 09/18/2013 14:33 EPA 200.8

Selenium, Se 235 ug/L 0.50 0.20 DPC 09/18/2013 14:33 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 14:33 EPA 200.8

Thallium, Tl 3.05 ug/L 0.050 0.0020 DPC 09/18/2013 14:33 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 15:57 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 15:57 EPA 200.7

Zinc, Zn 3.3 ug/L 0.50 0.10 DPC 09/18/2013 14:33 EPA 200.8

Aluminum, Al 0.0166 mg/L 0.0010 0.0003 DPC 09/18/2013 14:33 EPA 200.8

Boron, B 58.0 mg/L 0.20 0.040 DAM 09/18/2013 15:57 EPA 200.7

Calcium, Ca 454 mg/L 0.20 0.040 DAM 09/18/2013 15:57 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/18/2013 15:57 EPA 200.7

Magnesium, Mg 432 mg/L 0.10 0.020 DAM 09/18/2013 15:57 EPA 200.7

Manganese, Mn 1.64 mg/L 0.0050 0.0010 DAM 09/18/2013 15:57 EPA 200.7

Potassium, K 120 mg/L 0.50 0.070 DAM 09/18/2013 15:55 EPA 200.7

Sodium, Na 1990 mg/L 0.30 0.080 DAM 09/18/2013 15:55 EPA 200.7

Strontium, Sr 6.08 mg/L 0.010 0.0030 DAM 09/18/2013 15:55 EPA 200.7

Ammonia, NH3, as N 1.39 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 0.83 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 5.25 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 7 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-005A Date Collected: 09/11/2013 Date Received: 9/12/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.4 ug/L 0.050 0.010 DPC 09/18/2013 14:38 EPA 200.8

Arsenic, As 34.8 ug/L 0.10 0.030 DPC 09/18/2013 14:38 EPA 200.8

Barium, Ba 26.2 ug/L 0.10 0.020 DPC 09/18/2013 14:38 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:01 EPA 200.7

Cadmium, Cd 1.15 ug/L 0.050 0.010 DPC 09/18/2013 14:38 EPA 200.8

Chromium, Cr 0.16 ug/L J 0.20 0.040 DPC 09/18/2013 14:38 EPA 200.8

Cobalt, Co 1.54 ug/L 0.020 0.0040 DPC 09/18/2013 14:38 EPA 200.8

Copper, Cu 1.00 ug/L 0.050 0.010 DPC 09/18/2013 14:38 EPA 200.8

Lead, Pb 0.191 ug/L 0.010 0.0020 DPC 09/18/2013 14:38 EPA 200.8

Mercury, Hg 7.6 ng/L 2.0 0.80 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 6710 ug/L 0.050 0.010 DPC 09/18/2013 14:38 EPA 200.8

Nickel, Ni 9.95 ug/L 0.20 0.050 DPC 09/18/2013 14:38 EPA 200.8

Selenium, Se 217 ug/L 0.50 0.20 DPC 09/18/2013 14:38 EPA 200.8

Selenite, Se+4 (Hydride) 160 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 14:38 EPA 200.8

Thallium, Tl 2.78 ug/L 0.050 0.0020 DPC 09/18/2013 14:38 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:01 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:01 EPA 200.7

Zinc, Zn 3.0 ug/L 0.50 0.10 DPC 09/18/2013 14:38 EPA 200.8

Aluminum, Al 0.0109 mg/L 0.0010 0.0003 DPC 09/18/2013 14:38 EPA 200.8

Boron, B 58.3 mg/L 0.20 0.040 DAM 09/18/2013 16:01 EPA 200.7

Calcium, Ca 456 mg/L 0.20 0.040 DAM 09/18/2013 16:01 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/18/2013 16:01 EPA 200.7

Magnesium, Mg 440 mg/L 0.10 0.020 DAM 09/18/2013 16:01 EPA 200.7

Manganese, Mn 1.36 mg/L 0.0050 0.0010 DAM 09/18/2013 16:01 EPA 200.7

Potassium, K 120 mg/L 0.50 0.070 DAM 09/18/2013 15:59 EPA 200.7

Sodium, Na 1990 mg/L 0.30 0.080 DAM 09/18/2013 15:59 EPA 200.7

Strontium, Sr 6.06 mg/L 0.010 0.0030 DAM 09/18/2013 15:59 EPA 200.7

Mountaineer Plant, 133724 Page 8 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-006 Date Collected: 09/11/2013 Date Received: 9/12/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.65 ug/L 0.050 0.010 DPC 09/18/2013 14:42 EPA 200.8

Arsenic, As 16.5 ug/L 0.10 0.030 DPC 09/18/2013 14:42 EPA 200.8

Barium, Ba 59.1 ug/L 0.10 0.020 DPC 09/18/2013 14:42 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:05 EPA 200.7

Cadmium, Cd 13.6 ug/L 0.050 0.010 DPC 09/18/2013 14:42 EPA 200.8

Chromium, Cr 2.1 ug/L 0.20 0.040 DPC 09/18/2013 14:42 EPA 200.8

Cobalt, Co 38.6 ug/L 0.020 0.0040 DPC 09/18/2013 14:42 EPA 200.8

Copper, Cu 1.12 ug/L 0.050 0.010 DPC 09/18/2013 14:42 EPA 200.8

Lead, Pb 0.212 ug/L 0.010 0.0020 DPC 09/18/2013 14:42 EPA 200.8

Mercury, Hg 104 ng/L 10 4.0 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 3290 ug/L 0.050 0.010 DPC 09/18/2013 14:42 EPA 200.8

Nickel, Ni 352 ug/L 0.20 0.050 DPC 09/18/2013 14:42 EPA 200.8

Selenium, Se 286 ug/L 0.50 0.20 DPC 09/18/2013 14:42 EPA 200.8

Silver, Ag 0.010 ug/L 0.010 0.0020 DPC 09/18/2013 14:42 EPA 200.8

Thallium, Tl 5.15 ug/L 0.050 0.0020 DPC 09/18/2013 14:42 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:05 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:05 EPA 200.7

Zinc, Zn 20.3 ug/L 0.50 0.10 DPC 09/18/2013 14:42 EPA 200.8

Aluminum, Al 0.141 mg/L 0.0010 0.0003 DPC 09/18/2013 14:42 EPA 200.8

Boron, B 254 mg/L 0.20 0.040 DAM 09/18/2013 16:05 EPA 200.7

Calcium, Ca 605 mg/L 0.20 0.040 DAM 09/18/2013 16:05 EPA 200.7

Iron, Fe 0.34 mg/L J 0.50 0.10 DAM 09/18/2013 16:05 EPA 200.7

Magnesium, Mg 2050 mg/L 0.10 0.020 DAM 09/18/2013 16:05 EPA 200.7

Manganese, Mn 39.1 mg/L 0.0050 0.0010 DAM 09/18/2013 16:05 EPA 200.7

Potassium, K 85.8 mg/L 0.50 0.070 DAM 09/18/2013 16:03 EPA 200.7

Sodium, Na 1020 mg/L 0.30 0.080 DAM 09/18/2013 16:03 EPA 200.7

Strontium, Sr 7.25 mg/L 0.010 0.0030 DAM 09/18/2013 16:03 EPA 200.7

Ammonia, NH3, as N 1.53 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.98 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 20.6 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 9 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-006A Date Collected: 09/11/2013 Date Received: 9/12/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.49 ug/L 0.050 0.010 DPC 09/18/2013 14:47 EPA 200.8

Arsenic, As 14.3 ug/L 0.10 0.030 DPC 09/18/2013 14:47 EPA 200.8

Barium, Ba 54.0 ug/L 0.10 0.020 DPC 09/18/2013 14:47 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:14 EPA 200.7

Cadmium, Cd 1.25 ug/L 0.050 0.010 DPC 09/18/2013 14:47 EPA 200.8

Chromium, Cr 1.1 ug/L 0.20 0.040 DPC 09/18/2013 14:47 EPA 200.8

Cobalt, Co 26.7 ug/L 0.020 0.0040 DPC 09/18/2013 14:47 EPA 200.8

Copper, Cu 0.70 ug/L 0.050 0.010 DPC 09/18/2013 14:47 EPA 200.8

Lead, Pb 0.065 ug/L 0.010 0.0020 DPC 09/18/2013 14:47 EPA 200.8

Mercury, Hg 3.7 ng/L 2.0 0.80 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 3180 ug/L 0.050 0.010 DPC 09/18/2013 14:47 EPA 200.8

Nickel, Ni 308 ug/L 0.20 0.050 DPC 09/18/2013 14:47 EPA 200.8

Selenium, Se 276 ug/L 0.50 0.20 DPC 09/18/2013 14:47 EPA 200.8

Selenite, Se+4 (Hydride) 225 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 14:47 EPA 200.8

Thallium, Tl 4.55 ug/L 0.050 0.0020 DPC 09/18/2013 14:47 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:14 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:14 EPA 200.7

Zinc, Zn 14.3 ug/L 0.50 0.10 DPC 09/18/2013 14:47 EPA 200.8

Aluminum, Al 0.0212 mg/L 0.0010 0.0003 DPC 09/18/2013 14:47 EPA 200.8

Boron, B 257 mg/L 0.20 0.040 DAM 09/18/2013 16:14 EPA 200.7

Calcium, Ca 630 mg/L 0.20 0.040 DAM 09/18/2013 16:14 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/18/2013 16:14 EPA 200.7

Magnesium, Mg 2100 mg/L 0.10 0.020 DAM 09/18/2013 16:14 EPA 200.7

Manganese, Mn 40.3 mg/L 0.0050 0.0010 DAM 09/18/2013 16:14 EPA 200.7

Potassium, K 87.2 mg/L 0.50 0.070 DAM 09/18/2013 16:13 EPA 200.7

Sodium, Na 1040 mg/L 0.30 0.080 DAM 09/18/2013 16:13 EPA 200.7

Strontium, Sr 7.42 mg/L 0.010 0.0030 DAM 09/18/2013 16:13 EPA 200.7

Mountaineer Plant, 133724 Page 10 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-007 Date Collected: 09/11/2013 Date Received: 9/12/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.07 ug/L 0.050 0.010 DPC 09/18/2013 14:52 EPA 200.8

Arsenic, As 0.68 ug/L 0.10 0.030 DPC 09/18/2013 14:52 EPA 200.8

Barium, Ba 62.7 ug/L 0.10 0.020 DPC 09/18/2013 14:52 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:23 EPA 200.7

Cadmium, Cd 0.018 ug/L J 0.050 0.010 DPC 09/18/2013 14:52 EPA 200.8

Chromium, Cr 0.8 ug/L 0.20 0.040 DPC 09/18/2013 14:52 EPA 200.8

Cobalt, Co 0.067 ug/L 0.020 0.0040 DPC 09/18/2013 14:52 EPA 200.8

Copper, Cu 0.07 ug/L 0.050 0.010 DPC 09/18/2013 14:52 EPA 200.8

Lead, Pb 0.047 ug/L 0.010 0.0020 DPC 09/18/2013 14:52 EPA 200.8

Mercury, Hg 2.8 ng/L 1.0 0.40 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 66.2 ug/L 0.050 0.010 DPC 09/18/2013 14:52 EPA 200.8

Nickel, Ni 2.70 ug/L 0.20 0.050 DPC 09/18/2013 14:52 EPA 200.8

Selenium, Se 1.2 ug/L 0.50 0.20 DPC 09/18/2013 14:52 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 14:52 EPA 200.8

Thallium, Tl 0.035 ug/L J 0.050 0.0020 DPC 09/18/2013 14:52 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:23 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:23 EPA 200.7

Zinc, Zn 1.5 ug/L 0.50 0.10 DPC 09/18/2013 14:52 EPA 200.8

Aluminum, Al 2.28 mg/L 0.0010 0.0003 DPC 09/18/2013 14:52 EPA 200.8

Boron, B 228 mg/L 0.20 0.040 DAM 09/18/2013 16:23 EPA 200.7

Calcium, Ca 602 mg/L 0.20 0.040 DAM 09/18/2013 16:23 EPA 200.7

Iron, Fe 1.19 mg/L 0.50 0.10 DAM 09/18/2013 16:23 EPA 200.7

Magnesium, Mg 1830 mg/L 0.10 0.020 DAM 09/18/2013 16:23 EPA 200.7

Manganese, Mn 33.9 mg/L 0.0050 0.0010 DAM 09/18/2013 16:23 EPA 200.7

Potassium, K 86.3 mg/L 0.50 0.070 DAM 09/18/2013 16:22 EPA 200.7

Sodium, Na 1010 mg/L 0.30 0.080 DAM 09/18/2013 16:22 EPA 200.7

Strontium, Sr 7.14 mg/L 0.010 0.0030 DAM 09/18/2013 16:22 EPA 200.7

Ammonia, NH3, as N 2.35 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.26 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.72 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 11 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-007A Date Collected: 09/11/2013 Date Received: 9/12/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.06 ug/L 0.050 0.010 DPC 09/18/2013 14:57 EPA 200.8

Arsenic, As 0.62 ug/L 0.10 0.030 DPC 09/18/2013 14:57 EPA 200.8

Barium, Ba 60.1 ug/L 0.10 0.020 DPC 09/18/2013 14:57 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:32 EPA 200.7

Cadmium, Cd 0.023 ug/L J 0.050 0.010 DPC 09/18/2013 14:57 EPA 200.8

Chromium, Cr 0.7 ug/L 0.20 0.040 DPC 09/18/2013 14:57 EPA 200.8

Cobalt, Co 0.069 ug/L 0.020 0.0040 DPC 09/18/2013 14:57 EPA 200.8

Copper, Cu 0.045 ug/L J 0.050 0.010 DPC 09/18/2013 14:57 EPA 200.8

Lead, Pb 0.059 ug/L 0.010 0.0020 DPC 09/18/2013 14:57 EPA 200.8

Mercury, Hg 1.0 ng/L 0.50 0.20 TLT 09/18/2013 EPA 1631E

Molybdenum, Mo 60.6 ug/L 0.050 0.010 DPC 09/18/2013 14:57 EPA 200.8

Nickel, Ni 2.45 ug/L 0.20 0.050 DPC 09/18/2013 14:57 EPA 200.8

Selenium, Se 1.0 ug/L 0.50 0.20 DPC 09/18/2013 14:57 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 09/24/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/18/2013 14:57 EPA 200.8

Thallium, Tl 0.024 ug/L J 0.050 0.0020 DPC 09/18/2013 14:57 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:32 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:32 EPA 200.7

Zinc, Zn 2.6 ug/L 0.50 0.10 DPC 09/18/2013 14:57 EPA 200.8

Aluminum, Al 2.15 mg/L 0.0010 0.0003 DPC 09/18/2013 14:57 EPA 200.8

Boron, B 237 mg/L 0.20 0.040 DAM 09/18/2013 16:32 EPA 200.7

Calcium, Ca 635 mg/L 0.20 0.040 DAM 09/18/2013 16:32 EPA 200.7

Iron, Fe 1.23 mg/L 0.50 0.10 DAM 09/18/2013 16:32 EPA 200.7

Magnesium, Mg 1930 mg/L 0.10 0.020 DAM 09/18/2013 16:32 EPA 200.7

Manganese, Mn 35.7 mg/L 0.0050 0.0010 DAM 09/18/2013 16:32 EPA 200.7

Potassium, K 90.2 mg/L 0.50 0.070 DAM 09/18/2013 16:31 EPA 200.7

Sodium, Na 1060 mg/L 0.30 0.080 DAM 09/18/2013 16:31 EPA 200.7

Strontium, Sr 7.52 mg/L 0.010 0.0030 DAM 09/18/2013 16:31 EPA 200.7

Mountaineer Plant, 133724 Page 12 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-008 Date Collected: 09/11/2013 Date Received: 9/12/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.73 ug/L 0.050 0.010 DPC 09/18/2013 15:02 EPA 200.8

Arsenic, As 8.95 ug/L 0.10 0.030 DPC 09/18/2013 15:02 EPA 200.8

Barium, Ba 58.9 ug/L 0.10 0.020 DPC 09/18/2013 15:02 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:41 EPA 200.7

Cadmium, Cd 0.43 ug/L 0.050 0.010 DPC 09/18/2013 15:02 EPA 200.8

Chromium, Cr 1.2 ug/L 0.20 0.040 DPC 09/18/2013 15:02 EPA 200.8

Cobalt, Co 6.04 ug/L 0.020 0.0040 DPC 09/18/2013 15:02 EPA 200.8

Copper, Cu 0.34 ug/L 0.050 0.010 DPC 09/18/2013 15:02 EPA 200.8

Lead, Pb 0.062 ug/L 0.010 0.0020 DPC 09/18/2013 15:02 EPA 200.8

Mercury, Hg 3.2 ng/L 2.0 0.80 TLT EPA 1631E

The analysis result for dissolved Hg was higher than the total Hg. It is suspected that the bottles were labelled incorrectly in the field.

09/18/2013

Molybdenum, Mo 2190 ug/L 0.050 0.010 DPC 09/18/2013 15:02 EPA 200.8

Nickel, Ni 41.7 ug/L 0.20 0.050 DPC 09/18/2013 15:02 EPA 200.8

Selenium, Se 14.7 ug/L 0.50 0.20 DPC 09/18/2013 15:02 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/18/2013 15:02 EPA 200.8

Thallium, Tl 0.72 ug/L 0.050 0.0020 DPC 09/18/2013 15:02 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:42 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:41 EPA 200.7

Zinc, Zn 1.5 ug/L 0.50 0.10 DPC 09/18/2013 15:02 EPA 200.8

Aluminum, Al 0.399 mg/L 0.0010 0.0003 DPC 09/18/2013 15:02 EPA 200.8

Boron, B 242 mg/L 0.20 0.040 DAM 09/18/2013 16:41 EPA 200.7

Calcium, Ca 649 mg/L 0.20 0.040 DAM 09/18/2013 16:41 EPA 200.7

Iron, Fe 0.582 mg/L 0.50 0.10 DAM 09/18/2013 16:42 EPA 200.7

Magnesium, Mg 1990 mg/L 0.10 0.020 DAM 09/18/2013 16:41 EPA 200.7

Manganese, Mn 40.4 mg/L 0.0050 0.0010 DAM 09/18/2013 16:41 EPA 200.7

Potassium, K 96.6 mg/L 0.50 0.070 DAM 09/18/2013 16:40 EPA 200.7

Sodium, Na 1040 mg/L 0.30 0.080 DAM 09/18/2013 16:40 EPA 200.7

Strontium, Sr 7.50 mg/L 0.010 0.0030 DAM 09/18/2013 16:40 EPA 200.7

Ammonia, NH3, as N 0.82 mg/L 0.050 0.020 DMM 09/17/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.44 mg/L 0.50 0.10 DMM 09/26/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.64 mg/L 0.10 0.020 DMM 09/13/2013 SM20 4500NO3 H

Mountaineer Plant, 133724 Page 13 of 14
Location: Mountaineer Plant Report Date: 10/4/2013

Sample Number: 133724-008A Date Collected: 09/11/2013 Date Received: 9/12/2013

2nd Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.57 ug/L 0.050 0.010 DPC 09/18/2013 15:06 EPA 200.8

Arsenic, As 8.27 ug/L 0.10 0.030 DPC 09/18/2013 15:06 EPA 200.8

Barium, Ba 54.3 ug/L 0.10 0.020 DPC 09/18/2013 15:06 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/18/2013 16:50 EPA 200.7

Cadmium, Cd 0.36 ug/L 0.050 0.010 DPC 09/18/2013 15:06 EPA 200.8

Chromium, Cr 1.3 ug/L 0.20 0.040 DPC 09/18/2013 15:06 EPA 200.8

Cobalt, Co 5.72 ug/L 0.020 0.0040 DPC 09/18/2013 15:06 EPA 200.8

Copper, Cu 0.35 ug/L 0.050 0.010 DPC 09/18/2013 15:06 EPA 200.8

Lead, Pb 0.115 ug/L 0.010 0.0020 DPC 09/18/2013 15:06 EPA 200.8

Mercury, Hg 16.2 ng/L 1.0 0.40 TLT EPA 1631E

The analysis result for dissolved Hg was higher than the total Hg. It is suspected that the bottles were labelled incorrectly in the field.

09/18/2013

Molybdenum, Mo 2000 ug/L 0.050 0.010 DPC 09/18/2013 15:06 EPA 200.8

Nickel, Ni 38.2 ug/L 0.20 0.050 DPC 09/18/2013 15:06 EPA 200.8

Selenium, Se 5.0 ug/L 0.50 0.20 DPC 09/18/2013 15:06 EPA 200.8

Selenite, Se+4 (Hydride) 1.5 ug/L J 5.0 1.0 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/18/2013 15:06 EPA 200.8

Thallium, Tl 0.62 ug/L 0.050 0.0020 DPC 09/18/2013 15:06 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 09/18/2013 16:51 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/18/2013 16:50 EPA 200.7

Zinc, Zn 2.7 ug/L 0.50 0.10 DPC 09/18/2013 15:06 EPA 200.8

Aluminum, Al 0.378 mg/L 0.0010 0.0003 DPC 09/18/2013 15:06 EPA 200.8

Boron, B 245 mg/L 0.20 0.040 DAM 09/18/2013 16:50 EPA 200.7

Calcium, Ca 667 mg/L 0.20 0.040 DAM 09/18/2013 16:50 EPA 200.7

Iron, Fe 0.534 mg/L 0.50 0.10 DAM 09/18/2013 16:51 EPA 200.7

Magnesium, Mg 2030 mg/L 0.10 0.020 DAM 09/18/2013 16:50 EPA 200.7

Manganese, Mn 41.3 mg/L 0.0050 0.0010 DAM 09/18/2013 16:50 EPA 200.7

Potassium, K 97.8 mg/L 0.50 0.070 DAM 09/18/2013 16:49 EPA 200.7

Sodium, Na 1050 mg/L 0.30 0.080 DAM 09/18/2013 16:49 EPA 200.7

Strontium, Sr 7.59 mg/L 0.010 0.0030 DAM 09/18/2013 16:49 EPA 200.7

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133724 Page 14 of 14