Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as an

beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to b

boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This numbe

would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for mu

should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Gre

cells should be filled using the drop-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuel

(example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information workshe

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Information 

you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If th

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet.

6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you hav

more.

7. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the units 
ormation about chemical analyses of fuels used 

ne, fluorine, and metals, such as antimony, 

This spreadsheet is intended to be used for one 

at that specific boiler. This number of analyses 

tes were being tested. Data for multiple boilers 

d in yellow are required fields. Green highlighted 

omatically filled from other fields.

: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls

r on the Boiler Information worksheet.

el column of the Boiler Information worksheet. If

Description column.

hods worksheet. For example: "ASTM D5865-

icklist worksheet (orange tab). If the units of

lease fill them in the blank, orange highlighted, 

Sample Results worksheet.

worksheet. You must provide a minimum of 3 

ot limited to that number if you have collected 

down boxes to fill in the units of measure.
EIA Facility Code Facility Name Boiler ID Test Date

470 COMANCHE2 3/16/2010
Fuel Type 1 Fuel Type 2 Fuel Type 3

subbituminous
Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

470 COMANCHE 2 As Received Higher Heating Value

470 COMANCHE 2 As Received % Moisture

470 COMANCHE 2 As Received % Ash

470 COMANCHE 2 As Received % Sulfur

470 COMANCHE 2 Dry basis Higher Heating Value

470 COMANCHE 2 Dry basis % Moisture

470 COMANCHE 2 Dry basis % Ash

470 COMANCHE 2 Dry basis % Sulfur

470 COMANCHE 2 Dry basis Antimony

470 COMANCHE 2 Dry basis Arsenic

470 COMANCHE 2 Dry basis Beryllium

470 COMANCHE 2 Dry basis Cadmium

470 COMANCHE 2 Dry basis Chlorine

470 COMANCHE 2 Dry basis Chromium

470 COMANCHE 2 Dry basis Cobalt

470 COMANCHE 2 Dry basis Fluorine

470 COMANCHE 2 Dry basis Lead

470 COMANCHE 2 Dry basis Manganese

470 COMANCHE 2 Dry basis Mercury

470 COMANCHE 2 Dry basis Nickel

470 COMANCHE 2 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865-04

ASTM D3302

ASTM D5142

ASTM D4239

ASTM D5865

ASTM D3302

ASTM D5142

ASTM D4239

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6721

ASTM D6357

ASTM D6357

ASTM D3761

ASTM D6357

ASTM D6357

ASTM D6722

ASTM D6357

SW-846-7740
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

470 COMANCHE 2 M29, OTM 27/28, M30B

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Hg & Non-Hg Run 1 3/16/2010 8601.00 Btu/lb 28.78

Hg & Non-Hg Run 2 3/17/2010 8539.00 Btu/lb 29.72

Hg & Non-Hg Run 3 3/19/2010 8641.00 Btu/lb 27.32

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

4.75 0.23 12077 Btu/lb 0 6.67 0.32

4.76 0.29 12150 Btu/lb 0 6.77 0.42

6.02 0.2 11888 Btu/lb 0 8.28 0.27


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.07 μg/g <1 μg/g 0.2 μg/g <0.2

0.12 μg/g <1 μg/g <0.2 μg/g <0.2

0.07 μg/g <1 μg/g 0.4 μg/g <0.2


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

μg/g 5 μg/g 2 μg/g 29 μg/g 4 μg/g

μg/g 4 μg/g <2 μg/g 20 μg/g 3 μg/g

μg/g 6 μg/g 4 μg/g 8 μg/g 6 μg/g


Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

<1 μg/g 1 μg/g

<1 μg/g <1 μg/g

<1 μg/g 2 μg/g


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

470 COMANCHE 2

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

470 COMANCHE 2

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

470 COMANCHE 2

Sample Number 

(minimum of 3 

composite samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results


% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm

μg/g