## Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

## Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units of

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

PPL Montour Station

032 - Unit 2 bitum inous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte

0 PPL Montour Station

032 - Unit 2

As Received Higher Heating Value 0 PPL Montour Station

032 - Unit 2

As Received % Moisture 0 PPL Montour Station

032 - Unit 2

As Received % Ash 0 PPL Montour Station

032 - Unit 2

As Received % Sulfur 0 PPL Montour Station

032 - Unit 2

Dry basis Higher Heating Value 0 PPL Montour Station

032 - Unit 2

Dry basis % Ash 0 PPL Montour Station

032 - Unit 2

Dry basis % Sulfur 0 PPL Montour Station

032 - Unit 2

Dry basis Antim ony 0 PPL Montour Station

032 - Unit 2

Dry basis Arsenic 0 PPL Montour Station

032 - Unit 2

Dry basis Beryllium 0 PPL Montour Station

032 - Unit 2

Dry basis Cadmium 0 PPL Montour Station

032 - Unit 2

Dry basis Chlorine 0 PPL Montour Station

032 - Unit 2

Dry basis Chromium 0 PPL Montour Station

032 - Unit 2

Dry basis Cobalt 0 PPL Montour Station

032 - Unit 2

Dry basis Fluorine 0 PPL Montour Station

032 - Unit 2

Dry basis Lead 0 PPL Montour Station

032 - Unit 2

Dry basis Manganese 0 PPL Montour Station

032 - Unit 2

Dry basis Mercury 0 PPL Montour Station

032 - Unit 2

Dry basis Nickel 0 PPL Montour Station

032 - Unit 2

Dry basis Selenium

### An alysis M ethod for each Analyte

(example: ASTM D5865-04)EIA Facility Code Facility

Name Boiler ID HAPs Test Group 0 PPL Montour Station 032 - Unit 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Test 1 1.2D 3/17/2010 3/17/2010 15151.20 Btu/lb 1.18 8.02 2.661 Test 2 1.2D 3/18/2010 3/18/2010 15267.70 Btu/lb 1.35 8.06 1.892 Test 3 1.2D 3/18/2010 3/18/2010 15242.60 Btu/lb 1.23 8.57 1.813 Fuel Testing Results% Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 8.11 2.693 0.12 % 0.07449 ppm <4.99 ppm 2.53 ppm <0.04 ppm <0.05 8.17 1.918 0.12 % 0.07151 ppm <4.91 ppm 2.21 ppm <0.04 ppm <0.05 8.68 1.835 0.12 % 0.13436 ppm <4.93 ppm 3.59 ppm <0.04 ppm <0.05Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ppm 14.6 ppm 3.66 ppm 14.6 ppm 5.89 ppm 0.67 ppm <0.25 ppm ppm 15.8 ppm 4.11 ppm 12.5 ppm 6.16 ppm 0.83 ppm <0.25 ppm ppm 16.8 ppm 5.14 ppm 12.7 ppm 6.93 ppm 0.37 ppm <0.25 ppmEIA Facility Code Facility

Name Boiler ID HAPs Test Group 0 PPL Montour Station 032 - Unit 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Test 3 1.2C 3/17/2010 3/17/2010 15147.80 Btu/lb 1.45 8.17 2.545 Test 4 1.2C 3/17/2010 3/17/2010 15139.60 Btu/lb 1.41 8.03 2.485 Test 5 1.2C 3/17/2010 3/17/2010 15164.50 Btu/lb 1.39 8.18 2.437 Fuel Testing Results% Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 8.29 2.582 0.11 % 8.14 2.521 0.12 % 8.29 2.471 0.14 %Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### HAPs Test Group 0 PPL Montour Station 032 - Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### HAPs Test Group 0 PPL Montour Station 032 - Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm