ATC PROJECT No. P-10142 

BORAL BRICKS 

EPAEi&f~~ f'i~!WPR8!J~/R AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Results 

APPENOIX PAGE No. 334 
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Analyst EO 

Parameters EPA Method 26A (H2S04) 

#Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job# 0910-96 

PO# P-10124 

Report Date 1016/2010 

MDL 0.0100 (ug/mL) 

LOQ 0.200 (ug/mL) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Compound Hydrogen Fluoride as Fluolide 

Sample LabiD Lab ID Analysis Ret Ret % Qjff Cone Cone % Diff 

ID # 1 #2 Method Time Time Ret Itt #2 Cone (min) (min) (ug/mL) (ug/mL) 

Salisbury Run 1 In A 009-tOOt.D 009-1002.0 HPLC53PGS8.M 3.13 3.13 0.0 7.99 7.99 0.0 

Avg Ac

Cone Conve

(uglmL) Fac

7.99 1.0

OaiiiibUrY Run 21n A I 012-1301.0 I 012-1302.0 [ HPLC53PG98.M I 3.13 I 3.13 I o.o I 7.99 I 7.97 I 0.1 I 7.98 I 1.0

OafiiibiiiYRun31nA--TOt3-140t.D[013=t402-:DTRI'Lc53PG98.'1vfi3.T3]}}3] (fO I 8.07- I 8.-65-[DJ r-8.06 I i.o5

[§alisbury RuntOutA r (ij<(:jso-f:o I o14:tsoz-:ol HPLCS3PG§S;M I NA I NA-1 NA I o-:QTtj(j(j I 0.010DQTM I d.01b-02J:::t.

I SalisburyRun20utA I 015-1601.0 I 015-1602.0 I HPLC53PG98.M I NA I NA IJIIA] o.otoooTo.01050TQJ?TO.OT~~05

C§iilisiJuryRUri30utA 1 ot6:1fforD 1 016-t9d2~b-l HPLC53P<l98:M 1 NA p~il-1 NA 1 o.blooo 1 o.otooorn 1 o.otoorr=t.o5

c P4RuntlnA m ]o2il=330Toro26:J352])1 HPI..C53i'<l9&rv\T3.1213.t2l 6.6J----s:84 r 3.86 I 0.3 I 3.85 I 1.05

I P4Run21nA I 029-3601.D I 029-3602.D I HPLC53PG98.M 13.1413.141 0.0 I 11.7 I 11.7 I 0.1 I 11.7 I 1.05

I P4 Run 31nA I 030-3701.D I 030-3702.D I HPLC53PG98.M 13.1413.141 0.0 I 11.0 I 10.9 I 0.1 I 10.9 I 1.05

I P4 Run 1 Out A- T031-380Ul]'03t-3602.D [Ri'l.C53f>G98.M I :3:121 3.121 o.ifT 0:4921 6.487-("0.S I ().4!'l6Lt.d5

I P4 Run 2 Out A I 032-3901.0 I 032-3902.0 I HPLC53PG98.M I 3.12 I 3.12 I 0.0 I 0.608 I 0.606 I 0.1 I 0.607 I 1.05

I P4 Run 3 Out A I 033-4001.D I 033-4002.D I HPLC53PG98.M I 3.12 I 3.12 I 0.1 I 0.685 I 0.684 I 0.1 I 0.684 I 1.05

0910-96 res 

EA# 091 0-96 Page 8 of 202 
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Analyst EO 

Parameters EPA Method 26A (H2S04) 

#Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job# 0910-96 

PO# P-10124 

Report Date 10/6/2010 

MDL 0.0100 (ug/mL) 

LOQ 0.200 (ug/mL) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Compound Hydrogen Fluoride as Fluoride 

Sample LabiD Lab ID Analysis Ret Ret % Diff Cone Cone 0/n Diff Time Time #1 #2 ID # 1 #2 Method (min) (min) Ret (ug/mL) (ug/mL) Cone 

P5 Run 1 In A 040-4901.0 040-4902.0 HPLC53PG98.M 3.13 3.13 0.0 6.19 6.24 OA 

Avg Ac

Cone Conve

(ug/mL) Fac

6.21 1.0

I P5 Run 21nA I 009-1001.0 I 009-1002.0 I HPLC53PG100.M I 3.141 3.14F6.ifT-8.7:fT 8.68 n I' 0.3 I' ll.?o -, - 1:6I P5Run31nA I010-1101.0I010-1102.DIHPLC53PG100.MI3.14I3.17I1.0 I 11.0 I 11.1 I 0.51 11.0 I 1.0

I P5 Run 1 Out A I 043-5201.0 I 043-5202.0 I HPLC53PG98.M I 3.12 I 3.12 I 0.0 I 0.750 I 0.702 I 3.3 I o.i28-[-T5

I P5 Run 2 Out A I 044-5701.0 I 044-5702.0 I HPLC53PG98.M I 3.1313.131 0.0 I 0.622 I 0.839 I 1.0 I 0.830 I 1.0

I P5 Run 3 Out A I 045-5801.0 I 045-5802.0 I HPLC53PG96.M I 3.12 13.121 0.0 I 0.776 I 0.766 I 0.5 I 0.772 I 1.0

I Acid Blank I 052-6701.0 I 052-6702.0 I HPLC53PG98.MT3.17 I NA I 0.0119 I n1:b

I 01 H20 blank I 054-6901.0 I 054-6902,0 I HPLC53PG96.M I NA I NA I NA I 0.0100 I 0.0100 I 0.0 I 0.0100 I 1.0

I 0.01N H2S04/NaOH RB I 008-0901.0 I 006-0902.0 HPLC53PG96.M I NA I NA NA o.I5100TM10l[Tll.i5nl 0.0100 1.1J

I 0.01N H2S04/Na0H RBI 008-3201.0 I 008-3202.0 HPLC53PG98.M I NA I NA NA 0.0100 I 0.0100 I 0.0 I 0.0100 1.0

I O.OtN H2S04/Na0H RBI 103-5601.0 1103-5602.0 HPLC53PG98.M I NA I NA NA 0.0100 I 0.0100 I 0.0 I 0.0100 1.0

I 0.01N H2S04/NaOH RBI 008-0901.0 I 008-0902.0 HPLC53PG100.M I NA I NA NA 0.0100 I 0.0100 I 0.0 I 0.0100 1.0

0910-96 res 

EA# 0910-96 Page 9 of 202 
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0910-96 res 

EA#0910-96 Page 10of202 

Avg Acid 

Cone Conversio

(ug/mL) Factor 

11.3 1.053 

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Spi

10.1 I 1.053 

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Spi

6.94 1 1.053 

Sp

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Spi

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Parameters EPA Method 26A (H2S04) 

# Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job # 0910-96 

PO# P-10124 

Report Date 10/612010 

MDL 0.0100 (ug/mL) 

LOQ 0.200 (ug/mL) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Compound Hydrogen Fluoride as Fluoride 

Sample LabiD Lab ID Analysis Ret Ret % Diff Cone Cone % Diff 

ID # 1 #2 Method Time Time Ret #1 #2 Cone (min) (min) (ug/ml) (ug/mL) 

HPLC53oo98 #LCS 102-5501.0 102.0502.0 HPLC53PG98.M 3.12 3.12 0.0 5.22 5.22 0.0 

HPLC53oo1 00 #LCS 007-0801.0 I 007-DB02.D HPLC53PG100.M I 3.12 I 3.13 0.0 5.27 I 5.29 I 0.1 

0910-96 res 

EA# 0910-96 Page 11 of 202 

Avg Aci

Cone Conve

(ug/mL) Fact

5.22 1.05

S

5.28 1.05

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Analyst EO 

Parameters EPA Method 26A (H2S04) 

#Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job# 0910-96 

PO# P-10124 

Report Date 10/6/2010 

MDL 0.00695 (ug/ml) 

LOQ 0.200 (ug/ml) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Compound Hydrogen Chloride as Chloride 

Sample LabiD Lab ID Analysis Ret Ret % Oiff Cone Cone % Diff Time nme #1 #2 

ID # 1 #2 Method (min) (min) Ret (ug/mL) (ug/ml) Cone 

Salisbury Run 1 In A 009-1001.0 009-1002.0 HPLC53PG98.M 4.26 4.26 0.0 0.533 0.532 0.0 

Avg Acid 

Cone Convers

(ug/ml) Facto

0.533 1.028 

I SalisburyRun21nA I 012-1301.0 I 012-13020 I HPLC53PG98.M 14.2614.261 0.0 I 0.650 I 0.644 I 0.5 I 0.647 r 1.028 

I Salisbllii-RUii31;;-;o;-jJji3-1461b I 013-1402~oTRPLC:53PG§S:MT4.26T4:26T 0.0 I 0742 r Oi4iJTifT 0.741 I 1.~

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I Salisbury Run 2 DutA I 015-1601.0 I 015-1602.0 I HPLC53PG98.M I 4.25 I 4.25 I 0.0 I 0.0648 I 0.0869 I 1.2 I 0.0859 I 1.028 

I Salisbury Run 3 Out A I 016-1901.0 I 016-1902.0 I HPLC53PG98.M I 4.251 4.251 0.0 I 0.0825 I 0.0764 I 3.8 I 0.079T r. 1.028 

I P4Run11nA I026-3301.Dio26-3302.DIHPLCS3PG98.MI4.26pi:261ool 0.218 ]-if21d I1.7T0.214\ 1.0

I P4Run21nA I 029-3601.0 I 029-3602.0 I HPLC53PG98.M 14.2614.261 0.0 I 1.01 I 1.01 I 0.3 I 1.01 I 1.028 

I P4 Run 31n A I 030-3701.0 I 030-3702.0 I HPLC53PG98.M I 4.261 4.261 0.0 I 0.815 I 0.823 I 0.5 I 0.819 I 1.028 

I P4 Run 1 Out A I 031-36010 I 031-3802.0 I HPLC53PG98.M I 4.26 I 4.26[ 0.0 I 0.325 [Jl.327 I 0.3 I -0~32_6_1_1.028 

I P4 Run 2 Out A I 032-3901.0 I 032-3902.0 I HPLC53PG98.M I 4.26 I 4.26 I 0.0 I 0.378 I 0.378 I 0.1 I 0.378 I 1.028 

I P4 Run 3 Out A I 033-4001 0 I 033-4002.0 I HPLC53PG98.M I 4.26 I 4.26 I 0.0 I 0.386 I 0.385 I 0.2 I 0.385 I 1.028 

0910-96 res 

EA# 0910-96 Page 12 of 202 
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Parameters EPA Method 26A (H2S04) 

#Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job # 0910-96 

PO# P-10124 

Report Date 10/6/2010 

MDL 0.00695 (uglmL) 

LOQ 0.200 (uglmL) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (uglmL) 

Compound Hydrogen Chloride as Chloride 

Semple LabiO Lab 10 Analysis Ret Ret % Oiff Cone Cone % Diff 

ID #1 #2 Method Time Time Ret # 1 #2 Cone (min) (min) (ug/mL) (ugimL) 

P5 Run tin A 040-4901.0 040-4902.D HPLC53PG98.M 4.26 4.26 0.0 0.206 0.203 0.6 

Avg Ac

Cone Conve

(uglmL) Fac

0.205 1.0

~--P5Run2-rtiil 

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I P5Run30utA I 045-580-1.D I 045-5802.0 I HPLC53PG98.M P26}T26-I o.o I 0.114 I 0.118 [2]]--5:1fs-r 1.0

I Acid Blank I o5z-6701.o I 052-6702.0 I HPLC53PG98.M 11'11\TNJ\ I NA I o.00695 I o.oo695 I-O:oloJl6695]- 1.o

I Dl H20 blank I 054-6901.0 I 054-6902.0 I HPLC53PG98.M I 4.29 I 4.29 I 0.0 I 0.113 I 0.0436 I 44.3 I 0.0783 I 1.0

I o.01N H2S041NaOH RBI oQ8:'o901.0 I 008-0902.D I HPLC53PG98.M 1-NATNA I NA I 0.00695 I o.00695 I o.o I o.oo695_1_ 1.0

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0910-96 res 

EA# 0910-96 Page 14 of 202 

Avg Acid 

Cone Convers

(ug/mL) Facto

3.65 1.028 

S

N

Sp

3.45 I 1.028 

S

N

Sp

3.06 1 1.028 

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3.07 I 1.028 

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Parameters EPA Method 26A (H2S04) 

#Samples 18 Runs, 2 Blanks 

Client# P-10124 

Job# 0910-96 

PO# P-10124 

Report Date 10/6/2010 

MDL 0.00695 (ug/ml) 

LOQ 0.200 (ugiml) 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) Compound Hydrogen Chloride as Chloride 

Sample Lab ID Lab ID Analysis Ret Ret % Diff Cone Cone % Diff 

10 # 1 #2 Method Tlme Time Ret # 1 #2 Cone (min) (min) (ug/ml) (ug/ml) 

HPLC53pq98 #LCS 102-5501.D 102-5502.0 HPLC53PG98.M 4.26 4.27 0.0 4.88 4.87 0.1 

HPLC53pg100 #LCS I 007-0801.0 J 007-0802.0 I HPLC53PG100.M I 4.25 L 4.25 I 0.0 I 4.92 L 4.92 J 0.1 1 

0910-96 res 

EA# 0910-96 Page 15 of 202 

Avg Acid 

Cone Convers

(ug/ml) Facto

4.87 1.028 

S

Sp

4.92 I 1.028 

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Parameters EPA Method 26A (NaDH) 

# Samples 18 Runs, 1 Blank 

MDL 0.00695 (uglmL) 

LDQ 0.200 (uglmL) 

Compound Chloride 

Sample LabiO Lab 10 Analysis 

10 # 1 #2 Method 

Client# P-10124 

Job# 0910-96 

PD # P-10124 

Report Date 101612010 

Lower Curve Umit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Ret Ret % Diff Cone Cone % Diff Time Time #1 #2 

(min) (min) Ret (uglmL) (ug/mL) Cone 

Avg 

Cone 

(ug/mL) 

Salisburv Run 1 In B 017-2001.0 017-2002.0 HPLC53PG98CL.M 4.23 4.23 0.0 

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I Salisbury Run 31n B I 019-2201.0 I 019-2202.0 I HPLC53PG98CLM I NA I NA I NA I 0.008951 0.006951 0.0 I 0.00695 I 1 

I Salisbury Run 1 Out ifi223~2601.oTo23-26o2:5JHPCC53PG98CL:wq 4.15 I 4.15 [Jf[T7.48--!"""?:39-CO:Iq=y4 I 1 

I Salisbury Run 2 Out 8 I 021-2401.0 I 021-2402.0 I HPLC53PG98CL.M I NA I NA I NA I 0.00695 I 0.00695 I 0.0 I 0.00695 I 1 

I Salisbury Run 3 Out B I 022-2501.0 I 022-2502f5THP[C53PG98CL.Ml424 14.241 o.lfT 2A2-- I -2.36 -TT2 I 

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I P4 Run 21n 8 I 035-4401.0 I 035-4402.0 I HPLC53PG98CLM I NA I NA I NA I 0.006951 0.006951 0.0 I 0.006951 1 

I P4 Run 31n B I 036-4501.0 I 036-4502.0 I HPLC53PG98CLM I NA I NA I NA I 0.00695 I 0.006951 0.0 I 0.00695 l 1 

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j; 

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0910-96 res 

EA# 091 0-96 Page 16 of 202 
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Company Analytical Testing Consul 

Analyst EO 

Parameters EPA Method 26A (NaOH) 

# Samples 18 Runs, 1 Blank 

MDL 0.00695 (u9/mL) 

LOQ 0.200 (ugtmL) 

Compound Chloride 

Sample Lab ID Lab ID Analysis 

ID # t #2 Method 

Client# P-10124 

Job# 0910-96 

PO# P-10124 

Report Date 10/6/2010 

Lower Curve Limit 0.200 (ug/mL) 

Upper Curve Limit 15.0 (ug/mL) 

Ret Ret % Diff Cone Cone % Diff Time Time #1 #2 

(min) (min) Ret (ug/mL) (ug/mL) Cone: 

P5 Runt In B ---- _046-590t ,D_ 046-5902.0 H_pLC53PG98CLf>1 NA NA ----··- - NA 0.00695 0.00695 0.0 

Avg Aliquo

Cone 

(ug/mL) Facto

0.00695 1 

~-- P5 Run 21n-B I 

047-aooi~b I 047-60b2]j] HPLC53PG98cLMT 1'1/Cr-NA" [ NAT0:00695] o.00695 1 o.o 1 o.00695 1 1 

I P5 Run 31n B I 048-6101.0 I 048-6102.0 I HPLC53PG98CL.M I NA I NA I NA I 0.00695 I 0.00695 I 0.0 I 0.006951 1 

~-- P5 Ru/11-oUIB I 649:e'201:"o I o49.:a?OWJ HPLC53PG98CLMI. NA [ NA !NIITif00695 r-o.oo6¥["f6Jo.oo695) 1 

I P5 Run 2 Out B I 050-6301.0 I 050-6302.0 I HPLC53PG98CL.M I NA I NA I NA I 0.006951 0.006951 0.0 I 0.006951 1 

I P5 Run 3 Out B I 051-6401.0 I 051-6402.0 I HPLC53PG98CL.M I NA I NA I NA I 0.00695 I 0.00695 I 0.0 I 0.00695 I 1 

c saseBiank- ro53-680T"o 1 o53-68o2.bJ HPLC53PG98CL.M 1 4~2IT4J:H-o.o 1 o.oz35-fa-:tlz31 1 oe-r o.o233 1 ,-

I DIH20blank I 054-6901.0 I 054-6902.0 I HPLC53PG98.M 14.2914.291 0.0 I 0.113 I 0.0436 144.31 0.0783 I 1 

@]! N H2S04TNaoH R\31 008-090Ui I oo8-(j96i5] HPLC53PG98.M [ NA l NA I NA 0.06695 I 0.00695 ra.o I 0.00695T- 1 

~ I 0.01N H2S04/NaOH RBI 008-3201.0 I 008-3202.0 I HPLC53PG98.M I NA I NA I NA 0.00695 I 0.006951 0.0 I 0.006951 1 

z ~ I O.OtN H2S04/NaOH RBl103-5601.D 1103-5602.0 I HPLC53PG98.M I NA I NA I NA 0.00695[ 0.006951 0.0 I 0.006951 1 

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0910-96 res 

EA# 0910-96 Page 17 of 202 
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Analyst EO 

Parameters EPA Method 26A (NaOH) 

#Samples 16 Runs, 1 Blank 

Client# P-10124 

Job # 091 0-96 

PO# P-10124 

Report Date 101612010 

MDL 0.00695 (uglmL) 

LOQ 0.200 (uglml) 

Compound Chloride 

Lower Curve Limit 0.200 (uglmL) 

Upper Curve Limit 15.0 (uglml) 

Sample LabiO LabiD Analysis Ret Ret % Diff Cone Cone % Diff 

10 Time Time # 1 #2 # 1 #2 Method (min) (min) Ret (uglmL) (uglml) Cone 

HPLC53pg98 #LCS 007-0801.D 007-0802.0 HPLC53PG98.M 4.26 4.26 0.1 5.00 5.01 0.1 

HPLC53pg98 #LCS I 007-3101.0 I 007.;)102.0 I HPLC53PG98.M I 4.26 4.26 0.0 5.01 5.01 I 0.0 I 

Avg 

Cone 

(uglmL) 

5.01 

5.01 

HPLC53pg98#LCS I_ 102-5501.0 I 102-5502.0 I HPLC53PG98.M I 4.26 4.27 0.0 4.86 I 4.67 I 0.1 I 4.87 I 

0910-96 res 

EA# 0910-96 Page 18 of 202 

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ATC PROJECT No. P-10142 

BORAL BRICKS 

Narrative Summary 

EA# 0910-96 Paae 19 of 202 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 346 
BORAL BRICKS 

Enthalpy Analytical Narrative Summary 

.. !:!}.; Sll.sJtg~ly•••·•· David Eckard received the samples on 9/24/10 after being relinquished 

by Analytical Testing Consultants fnc. The samples were received at 

15.9°C and in good condition. Samples Plant 5 Inlet and Outlet Runs 

Li .. } :.>• : . 2 and 3 were received in glass. Prior to, during, and after analysis, the 

samples were kept under lock with access only to authorized personnel 

by Enthalpy Analytical, Inc. 

;ijj~\~HX•R The samples were analyzed for hydrogen chloride (HCI), hydrogen 

fluoride (HF), and chloride using the analytical procedures in EPA 

Method 26A, Determination of Hydrogen Halide and Halogen 

Emissions 11-om Stationary Sources !so kinetic Method (40 CFR Part 60, 

Appendix A). 

With the exceptions noted above, all samples and standards were 

prepared, stored, and analyzed using high-density polyethylene 

containers. 

The Metrohm 861, High Perfom1ance Liquid Chromatograph "Mr 

Burns" (SIN 1861004003180) was equipped with a Metrohm 861 ;;;F ,.•}/;') .••••••.•. ·.·:· .. ::···· c· i Conductivity Detector and a Metrosep A Supp 5 - ll 0/4.0mm column 

(SIN # 7908297), for these analyses. 

·y • •·(~alll:iiril'tioli • .. (. The calibration curves are included in the Calibration Curve 

C!hr()~!ll?g~!!Phic C!!I!Iditiops 

ATC PROJECT No. P-10142 

Chromatograms section of this report and referenced in the Analysis 

Method column on the Detailed Results page. 

For each calibration curve used, the first page of the curve contains all 

method specific parameters (i.e., curve type, origin, weight, etc.) used to 

quantity the samples. The calibration curve section also includes a table 

with the Retention Time (RetTime ), Level (Lvl), Amount 

(corresponding units), Area, Response Factor (Amt/Area) and the 

analyte Name. The calibration table is used to identify (by retention 

time) and quantity each target compound. 

The acquisition method Metrohm.M is included in the Calibration 

Curve Chromatograms section of this report. 

EP~/5-§li!Jtfffillf~IJ~r?Sf AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 347 
BORAL BRICKS 

Enthalpy Analytical Narrative Summary 

(continued) 

Fluoride was not identified above the MDL in the analyses of the lab . 

reagent blanks and client 01 H20 blank. Fluoride was detected below 

;;l"t,,;;;\.(0',/,~t;i,;:'; the LOQ in the acid blank. 

~'~1·;~'i[.!~in!''(f;c,' Chloride was not identified above the MDL in the analyses of the lab (:, reagent blanks and client acid blank. Chloride was detected below the 

LOQ in the client base blank and Dl H20 blank. 

Matrix spike and matrix spike duplicates (MS and MSD) were prepared 

using aliquots of the samples Salihury Rl-In A and P4 Rl InA. The 

recovery values were 111%, 91 .3%, 103%, and I 05% for HF. The 

recovery values were 104%,97.3%, 94.7%, and 95.4% for HCJ. 

Laboratory Control Samples (LCS) were prepared and analyzed with 

the samples. TI1e recovery values ranged from 104% to 107 for HF and 

97.5% to 100% for HCL. 

The samples were analyzed within the four-week holding time specified 

by the method. 

The results presented in this report are representative of the samples as 

provided to the laboratory. 

The H2S04 matrix samples were analyzed for Cl- and F- but are 

reported as HCI and HF. The results were converted using an acid 

conversion factor of 1.028 for HCI and 1.053 for HF. 

Enthalpy Analytical, Inc. is accredited to perform EPA Method 26A for 

compliance purposes by the National Environmental Laboratory 

Accreditation Conference (NELAC) through the Louisiana 

Environmental Laboratory Accreditation Program (LELAP), certificate 

number 04010. 

EA# 0910-96 Page 21 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 348 
BORAL BRICKS 

General Reporting Notes 

The following are general reporting notes that are applicable to all Enthalpy Analytical, Inc. data 

reports, unless specifically noted otherwise. 

• The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot 

determine the presence of the analyte of interest reliably. 

• The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot 

quantitate the analyle of interest within the criteria of the method. 

• The acronym ND following a value indicates a non-detect or analytical result below the MDL. 

• The Jetter J following a value indicates an analytical result between the MDL and the LOQ. A J flag 

indicates that the laboratory can positively identify the analyte of interest as present, but the value 

should be considered an estimate. 

• The Jetter E following a value indicates an analytical result exceeding I 00% of the highest calibration 

point. The associated value should be considered as an estimate. 

• The acronym DF represents Dilution Factor. This number represents dilution of the sample during the 

preparation and/or analysis process. The analytical result taken from a laboratory instrument is 

multiplied by the DF to determine the final undiluted sample results. 

• The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual sample is 

spiked with a known amount of analyte so that a percent recovery value can be determined. This shows 

what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample 

matrix interferes with the analysis ofthe analyte(s). 

• The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same 

manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality 

by showing the consistency of results gained by performing the same steps multiple times. 

• The addition of LD to the Sample lD represents a Laboratory Duplicate. The analyst prepares an 

additional aliquot of sample for testing and the results of the duplicate analysis are compared to the 

initial result. The result should have a difference value of within 10% of the initial result (if the results 

of the original analysis are greater than the LOQ). 

• The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an 

additional aliquot at a different dilution factor (usually double the initial factor). This analysis helps 

confirm that no additional compound is present and coeluting or sharing absorbance with the analyte of 

interest, as they would have a different response/absorbance than the analyte of interest. 

• The Sample lD LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample 

matdx, prepared and analyzed by the laboratory using the same reagents, spiking standards and 

procedures used for the client samples. The LCS is used to assess the control of the laboratory's 

analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. 

The extras (randomly chosen) are labeled with the associated project number and kept in-house at the 

appropriate temperature conditions. When the project samples are received for analysis, the LCSs are 

analyzed to confirm that the analyte could be recovered from the media, separate from the samples 

which were used on the project and which may have been affected by source matrix, sample collection 

and/or sample transport. 

ATC PROJECT No. P-10142 EP~Mf&fl.,ll!lS/GN!ff!g'f ~fl<i'JEil:!¥2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 349 
BORAL BRICKS 

General Reporting Notes 

(continued) 

• Significant Figures: Where the reported value is much greater than unity (1.00) in the units expressed, 

the number is rounded to a whole number of units, rather than to 3 signiticant figures. For example, a 

value of 10,456.45 ug catch is rounded to I 0,456 ug. There are five significant digits displayed, but no 

confidence should be placed on more than two significant digits. 

• Manual Integration: The data systems used for processing will flag manually integrated peaks with 

an "M". There are several reasons a peak may be manually integrated. These reasons will be identified 

by the following two letter designations. The peak was not integrated by the software "NI", the peak 

was integrated incorrectly by the software "II" or the wrong peak was integrated by the software 

"WP". These codes will accompany the analyst's manual integration stamp placed next to the 

com pound name. 

ATC PROJECT No. P-10142 EP~ft~8ll.ll~'§l8l'f~ ~Ml~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 350 
ATC PROJECT No. P-10142 

BORAL BRICKS 

Sample Custody 

EPI'EM ~~fi38R!N ~PM:i.lta112 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 351 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)·733·3193 

CHAIN OF CUSTODY RECORD Project No. P-10124 

REQ\JESTEC PARAMETERS 

CLIENT: BoraJ Bricks 11El1100 !l'LEA61i CIHCI.£) 5 6 8 

PLANT LOCATION: Augu~ta, 11 18 23 2S 26 

SAMPUNQ LOCAllON: Plant 4 In et VOST MULTIPLE-METALS OTHER 

SAMPLE 10: 

Run #1-HCI-Container 3 

Run #2~HC1-Contalner 3 

Run #3-HCf..Contalner 3 

Container #6-HCI 

Run #1-HCt-Container 4 

Run #2-HC!--Container 4 

Run #3·HCJ..Confainer 4 

container #7 -HCI 

Container #8-HCI 

REl.INOU4SHEO BY 

wt~~ RE\.INQUISHEt> BY 

AELO REMARKS: 

NOTE: 

FORI.! No. A T'C 1 

DATE TIME 1.0CAT10N VOI.l.JM£ IML) OR fll,;fl.l\ I CONTAINER: CONTENTS 

9.15.10 I \,t CFA 

Acid lmpingera Catch & 

-250 mL 01 Rinse 

I'.• , •··••· 

CFA -250mL 

Acid lmpingers Catch & 

01 Rinse 

1/. Acid lmpingers Catch & 

CFA -250 mL Dl Rinse 

•· ... Acid Blank-Dilute to 

·. ··.·•· .· . CFA -100 mL approx. volume of field 

....... samples with 01 water . 

I : Alkaline lmptngers 

CFA -200 mL Catch & 01 Rinse 

1

?:. Alkaline lmplngers 

CFA -200 mL Catch & 01 Rinse 

' ' Alkaline lmpingers 

CFA -200 ml Catch & 01 Rinse 

· ............ Alkaline Blank-Dilute to 

CFA -100 mL approx. volume of field 

/. samples with 01 water. 

'.'_2 CFA -100 mL Dl Water Blank 

OATE n•• RECE!VIW8Y DATE TIME 

cr/t 'f I {,tl.ii:>' • J', 'l."' cd 1 ~ .:k:lll\ 10. 

DATE TIME RECEIVED BY OAT!! To.IE 

I 

CFA: CLEAN FIELO AREA 

AnalyZe for HCI. HF and Cl2 per USEPA Method 26A procedures 

PLEASE MAAK LIQUID LEVEL ON ALL SAMPLE BOTTLES WITH GREASE PENCIL. 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL. 

Csn\:.A\f'R.r ~::: '":t-~. \ ~'d ~ \\(,.~ ~ \\~ ~ ·,,. 

~<'Rr 4-:::. -:I:~ ~L\ \&- ~ 

10 

202 

26A 

UilTJALS 

BK 

\~~-:::. \5,1\t:IC.. ~~l, 9P'~dC:\SOrl\1 ICR\COC'IIIJ\II26A COC)P!ant 4 Inlet• HCI HF Cll 

ATC PROJECT No. P-10142 

EA# 0910-96 Page 25 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Ver 1.0 29 August 2003 

APPENDIX PAGE No. 352 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)·733·3193 

CHAIN OF CUSTODY RECORD Project No P-10124 

REQUESTeD PARAMETER$-

CUENT~ Boral Bricka 1116TI4GD ji'L£o\Slil Cll'tC'I."£1 5 6 8 

PlANT LOCATIOn: AUgusta, bA 11 18 23 2!; 26 

SAAIPUNClOCATIOU: Pant 4 utlet YOST MULTIPLE-METALS OTHER 

SAMPLEJD: CATE TIME LOCATION 11'0\.t/lolll! fM!,.JO.IU'II.TEll• CONTAINER CO~TeNTS 

9.15.10 > CFA -250 ml 

Acid lmpingers Catch & 

Run #1-HCI~Container 3 Dl Rinse 

Run #2-HCJ-Container 3 .> CFA -250 mL 

Acid lmpingers Catch & 

Dl Rinse 

Run #3-HCI-Gonlainer 3 .·· .• \ ' CFA -250 ml 

Acid lmpingers Catch & 

Dl Rinse 

·.· ...... -. 

·---···-.· 

Run #1·HCI·Container 4 I < CFA -200ml 

Alkaline lmpingers 

Catch & Dl Rinse 

Run #2-HCl-Container 4 

.·-··.···· .. ··· CFA 

Alkaline lmpingers 

-200mL Catch & 01 Rinse 

1•:>:· Alkaline lmpingers 

Run #3-HCI-Contalner 4 CFA -200 mL Catch & Dl Rinse 

1)/\i 

' 

REUNQU/SHED BY DATE TIME ReGEIVEDBY DATE TlME 

lvtl?_.l-- 't/4-i '":If .S'ru,.J)JJ:S>I ·

1 .j.'XltU {b l~ REUNOUlSHEO BY OATE TlME RECEJVEDBY DATE TlME 

I 

FiELD REMARKS: ICFA: CLEAN FIELD AREA 

Analyze for HCt HF and C!2 per USEPA Method 26A procedures 

NOTE: 

FORM flo.ATC 1 

PlEASE MARK LIQUID LEVEL ON ALL SAMPLE BOTTLES WlTH GREASE PENCrL 

SEAL TfGHTL Y AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL. 

\.\\Jt ~ ~'~ ~= 3".~ \ ~? ~c \\c9-.. ~ \W 

G/'1-1."'1\&- ~~ \.\., "!..crqs ~\.\ ~ ~ 

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6A 

INITIALS 

BK 

C:\Bol'ai!CR\COC's\M23 COC\Piant 4 Otfllet• HCIHf C12 Ver 1.0 29 Allgust 2003 

ATC PROJECT No. P-10142 EA# 0910-96 Paqe 26 of 202 

EPA ICR E'MISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 353 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)·733-3193 

CHAIN OF CUSTODY RECORD Project No P-10124 

CUENT' Bo"'l Blici<S 

PLANT LOCATION: 

DATI TIME 

~~ f'(J\:.- I Run #1-HCI-Contalner 3 9.17.10 :·. • 

~~ I Run #2-HC~Container 3 

CFA 

CFA ~\..~ 

OJ:ii\J\b't """ ~· .• CFA I :• -250 rnL I Acid ""~i'Ri~~ecatch & .·. 

I Run #1-HCI-Contalner 4 

Run #2-HCI-Container 4 

Run #3-HCI-Coo!ainer 4 

>BY 

vlf:P~ 

'"' 

'FIElD 

NOTE: 

FORM N<1. ATC 1 

CFA -200 mL 

CFA -200 ml Catch & 01 Rins~~ 

CFA -200 mL 

LY 

DATE TIME >BY OA; TIME 

'i./l'f ltu:,.fl.t>\. ~\~~n.l 1 'i::<:t<t\ ID]'S" TIME >BY DATE TIME 

JvrA: CLEAN FIElD AREA 

Analyze for HCI. HF and Ct2 per USEPA Method 26A procedures 

PlEASE MARK UQWO LEVEL ON All SAMPLE BOTTLES WITH GREASE PENCIL. 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL. 

. 

\\\.i\c~~ ~~ --x:.i"'\~ '~ '}. ~r V\c.r.. \-'rtf; 

0.1?-\J'OL~'~u.--::~c-r.~ '1\'-\ ~ CJL-q. 

\~~-:::.. \5, C... ~\s..'l-. 'C:Oun ~~ 

BK 

C:\BOtaiiCR\COC's\M26A COC\Plllnt 51n~t ~ HCI HF Cl2 Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EPA'~~gslf.§NI'ffi\!r ~MJ?d¥ AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 354 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)-733-3193 

CHAIN OF CUSTODY RECORD Project No. P-10124 

REQUESTED PAR.AMIHERS 

cueHT: Boral Bltelcs 

PLANT 

lolll:THOD /l"t.~Sf CIR<:lfi!) 5 6 8 

lOCATION: i\~Sta~_~_!. 

SAMPUNQ LOCATIOU; 

11 18 23 25 2$ 

Plant ~Outlet VOST MULTIPLE-METALS OTHER 

SAMPLe 10: DATE TU<! LOCATION Yot.Wi.E (IilLI OR Flt. TE:R II CONTAINER CONTENTS 

Run #1-HCI-Container 3 9.17.10 !,\:') CFA 

Acid lmpingers CatCh & -250 mL OJ Rinse 

Run #2-HCJ~Container 3 ··g. CFA 

Acid lmpingers Catch & 

-250 mL Of Rinse 

·:' Run #3--HCI-Contafner 3 

Acid lmpingers Catch & 

CFA -250mL 01 Rinse 

~:/ Run #1-HCI-Conlalner ;.·· Alkaline lmpingers 

4 CFA -200 mL Catch & Dt Rinse 

Run #2-HCI-Container 4 n•: CFA 

Alkaline lmpingers 

-200 ml catch & Of Rinse 

Run #3--HCI-Ccntainer 4 IS .. ) CFA 

Alkaline lmpingers 

-200 mL catch & 01 Rinse 

1> 

I'·-:· . 

1\")!.\-' REUNOUJSHED BY DATE TIME RECEIVED BY DATE TIME 

0lll..s- t/rt.'lt.~ 1/<1;,{ .-E:;;. .. ~,Q"'-AJ~ •Ina cu ,J,s REUNQUISHEO BY 

FIELD REMARKS: 

NOTE: 

FORA! N.,. AlC 1 

DATE TlME RECEIVED BY DATE TIME 

I I CFA: CLEAN FJELD AREA 

Analyze for HC!, HF and Cl2 per USEPA Melhod 26A procedures 

PlEASE MARK liQUID lEVEl ON All SAMPLE BOTTLES WITH GREASE PENCIL. 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL 

10 

202 

26A 

INfTlALS 

BK 

C~OI'lll ICR\COC's\M26A GQC\Plan15 outset~ HCi HF C!2. Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EA# 0910-96 Paqe 28 of 202 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 355 
I 

\ 

BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)·733·3193 

CHAIN OF CUSTODY RECORD Project No. P-10124 

REQUESTED PARAMETERS 

CliENT: Bora! Brfcks U£Tii00(PIL<I81! C.JIICU!) 5 a 8 

PLANT lOCATION: Sa 1SbUty, NG 11 18 23 25 26 

SAMPWHOl0CA1'lOH! lola~ VOST MULTIPLE-METALS OTHER 

SA.MPI..E 10: DATe TIME LOCATION VOlOlot!' ftollJOR""-f!RJ CONTAINER CONTENTS 

Run #1-HCI-Conlainer 

'' :: Acid Jmpingers Catch & 

3 9.21.10 CFA -250 mL Dl Rinse 

: Run #2-HCI-Conlainer 

Acid lmpingers Catch & 

3 CFA -250 mL Dl Rinse 

Run #3-HCI-Container 3 \ CFA -250 mL 

Acid lmpingers Catch & 

Dl Rinse 

.. 

. < 

Run #1-HCI-Contalner-1 

.....•....•.. 

CFA -200 ml 

Alkaline lmpingers 

Catch & Dl Rinse '·.· 

Run Alkaline lmpingers 

#2-HCI-Container 4 CFA -200 mL Catch & 01 Rinse 

·····.·. Alkaline I mpingers 

Run #3-HCI-Contalner 4 .... CFA -200ml Catch & Dl Rinse 

! (,\ 

·: 

c 

RELINOUlSHEO BY OATe TIME AECEIVF..OBV DATE TIME 

l.vj( ,P, ..! 1/z"-lt •• it.· ~ L~C ,iJ ~_!{}_ -d 9XJrO rb '"') Ra.INO ISHED BY OATe TIME RECEIVeD 9V OATE TIME 

I FIELD REMARKS: CFA: CLEAN FIELD AREA 

Analyze for HCI, HF and Cl2 per USEPA Method 26A procedures 

NOTE: 

fORM No.ATG t 

. 

PLEASE MARK UOUlD LEVEL ON A•L SAMPLE BOTTLES WITH GREASE PENCIL 

SEAL TIGHTI. Y AND RE·CHECK UPON DELIVERY TO lAB PERSONNEL 

~'~ ~::. 3:.~~· ~~a. ~ \\tt ~ ~\­

~~(\~ \\ -~ ~~ ~ Ci<t-

\~-p?\5.6,0(...~~~~· 

to 

202 

26A 

INITIALS 

BK 

C:IBoraiiCR\COC's\M2SA COC\Sallsbury lnkn- HCI HF Cl2 Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EP.i:!Mlca-MGEOONitB§!I! M<:Jillml2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 356 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)-733-3193 

CHAIN OF CUSTODY RECORD Project No. P-10124 

REQUESTED PARAMETER& CLIENT: Boral Bricks MrnlOO (l't.O.::Je ctllct.El 5 6 8 

PLANT LOCATION: Sal Sb~ry, NC 11 18 23 25 26 SA.MPUNQ. LOCAT.ON: Utl~t YOST MULTIPLE-METALS OTHER 

SAMPLe: 10; DATE TIME LOCATION \IOI,.VtU (lofl.) OR A\.TER I CONTAINER CONTENT$ 

Run #1-HCI-Container 3 9.21.10 i·)i···· CFA -250 ml 

Acid lmpingers Catch & 

Di Rinse 

i•. ? CFA -250 ml Run 

Acid lmpingers Catch & 

#2-HCI-Container 3 

Di Rinse 

Run #3-HCI-Container 3 I> "< CFA -250 mL 

Acid lmplngers Catch & 

Dl Rinse 

. \ 

. \/ . ' 

_{/ £2 Alkaline lmpingers 

Run #1~HCI-Container 4 CFA -200 ml Catch & Dl Rinse 

Run #2-HCl-Container 4 ? .. CFA 

Alkafine I mpingers 

-200 ml Catch & Dl Rinse 

................ Alkaline lmpingers 

Run #3-HCI-Contalner 4 CFA -zoo ml Catch & Dl Rinse 

[\;}i . 

i······ 

RELINQUISHED BY DATE TIME RECENEOEI'Y DAlE TIME 

t.v;L.o '( /z.<t'k,) Vo: • ..--l-£l.u,;_ AXN'll o sl4N tol<k RaJHOU!SHt:;OBY DATE TIME RECCIVED BY DATE TIME 

J FE REMARKS: CFA: CLEAN FIELD AREA 

Analyze for HCI, HF and Cl2 par USEPA MethOd 26A procedures 

NOTE: PLEASE MARK LIQUID LEVEL ON At.L SAMPLE BOTTLES WITH GREASE PENCIL 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL 

~'~ ~ :::. Tt""'\~"- \ ~ d- w- \\CJ_ ~ 'n~ 

~ ... ~ ~ -=-~ '1\ '-\ ~ (!L";}-

\~{>=- \5,<\oG ~ ~Ul~ 

10 

202 

26A 

tNITW.S 

8K 

C:\SOf'aiiCR\COC'3\M26A COC\Sa!M:x!ry Outlet · HCI HF Cl2 Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EA# 0910-96 Page 30 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 357 
ATC PROJECT No. P-10142 

BORAL BRICKS 

Sample 

Chromatograms 

EPA~& ~rt1111lii~~ fEil,9fp~1:B~t~ 2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 358 
Sample Name: Salisbury Rl In A *20 0910-96 

BORAL BRICKS 

~=====================================::::============================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/l/2010 9:27:01 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HnC20lOQ3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

{modified after loading) 

10 

1 

ADC1 A, ADC1 c·HANNECi\iu·.IHPLC2010Q4\KlRBURNS\DATAIOCT\HPLC53PG981009·1001.D) 

uS/em j 180] 

160 . 

140 

120-

100-

80 

60 

40 

~ ,.; 

I

f\ ' ("') : l ('? r-:. { 

L.~~~~~2 :t-~~ ___________ 

,-~de~,~~"--.---~ ... ,.c::::::;:::::;:::;::::=;:=::;::=:::;:::::;::::'..j~-.~~~~~ ) ±___ __________ --- .--'".6 __ "_-_·~--~~-"~~--~--'1.9 ______ ··----------~·?;_==_~i~ 

===================================================================== External Standard Report 

======~====-===================~===================================== 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 Multiplier 

9:29:44 AM 

Dilution 

Ose Multiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.125 BV 467.71011 1.70755e-2 7.98639 Fluoride 

4.257 BB 17.94451 2.96828e-2 5.32643e-l Chloride 

'rotals : 8.51904 

==========:.:.:=========""'~"'====:;;:======='=======================""-'=""====:==== 

*** End of Report *** 

Ins trumen tAlC I?Q&.llt<2"0~6. P.l1dlil42 25 AM IGG EPf(2;U~1£sY8N ~~~f ~~6'JE~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGi!'~~59 1 of 1 
Data File 0:\HPLC2010Q4\MR B0RNS\DATA\OCT\HPLC53PG98\009-1002.D 

Sample Name: Salisbury Rl In A *20 0910-96 BORAL BRICKS 

===========<==========================,=============================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO 

Mr Burns 

Seq. Line 

Location 

10/1/2010 9:39:20 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

0: \HPLC2010Q3 \MR BURNS\METHODS\HPl.C53PG98. M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading} 

10 

2 

r----A"o'-'cTA.71oC1 CHANNECii (U:\HPLC2010041MR BURNSIDATAiOcT\HPLC53PG98\009--1Dil2".o"r _______ ] 

uS/em-~ 

180 J 

j 

160 ~ 

j 

140 •J 

120 -~ 

1oo--i 

80-

=============~,=====e==================================================· 

External Standard Report 

-=·=============================""====================================«::= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier &: D.ilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime 'fype Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/ll'.L] 

-------l------l----------l----------l----------l--1------------------

3.125 BV 467.69397 1.70755e-2 7.98612 Fluoride 

4.257 BB 17.93629 2.96844e-2 5.32427e-l Chloride 

Totals : 8.51854 

=============================="-~=""·=============='======================£, 

*** End of Report *~* 

InstrumentAllC ~B0d6C?IOrlOI P91:0H2 33 AM IGG EPA~~ ~mJlsfbSN ~~~;.?o~~~~z AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

I 

I 

APPENDIX PAGI?POGI'll60 1 of 1 
Sample Name: Salisbury R2 In A *20 0910-96 

BORAL BRICKS 

============================~=====~================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 10:40:59 PM Inj 

C:\llPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METBODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

{modified after loading) 

13 

1 

-·-i\oc1A: ADCTCHANNE[A (U:IHPTC2cffod4\MR!iiJRNS\i5AfAii5c'i\HPLC53PG98\012·1301 D) 

uS/em 

180 

160 

140-

120 

100 

80 

E 

" 

0 

~ 

u: 

I 

) 

===========~========================================================= 

External Standard Report 

===================================================================== 

Sorted By 

Calib- Data Nodified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor •·.dth ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/ll~rea Amount Grp Name 

[min] [uS/cm*s] lug/mL] 

-------i------l----------l----------l----------l--1------------------

3.126 BV 467.74438 J.70755e-2 7.98698 Fluoride 

4.257 BB 22.41548 2.90028e-2 6.50llle-l Chloride 

Totals : 8.63709 

========'"""=~"""=·============================================c=====·"''""==;.>::=-"" 

*** End of Report *** 

Instrument AtC~~giJIJ9. EA# 0910-96 Page 34 of 202 ill-l@ll<22 5 AN IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJ!'!'I6~61 1 of 1 
Sample Name: Salisbury R2 In A *20 0910-96 BORAL BRICKS 

===================,:.::=========,========,.,============================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis ·Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 10:53:19 PM Inj 

C:\HPLC2010Q3\t1R BURNS\t1ETHODS\METROHt1.t1 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\t1R BURNS\t1ETHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG . 

(modified after loading) 

13 

2 

,---~·ADC.1 A, ADC1 CHANNEL A (U:\HPLC201004\MR BURNS\DATAiOCT\HPLC53PG98\012-1302.D) 

============================================================,·==''"===== 

External Standard Report 

========================·================================'"-~============ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

(min] [uS/cm*s] [ug/mL] 

-------!------l----------l----------l----------1--l------------------

3.126 BV 466.99976 1.70755e-2 7.97425 Fluoride 

4.257 BB 22.18078 2.90316e-2 6.43944e-1 Chloride 

Totals : 8.61819 

===========================================================""<='======== 

*** End of Report *** 

InstrumentAIC~gClJI:Je. f!>1C!l11!l'33 AM !GG EPfm'l,~~~sli~N~l ~~aJm AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE'i!Nge362 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG98\013-140l.D 

Sample Name: Salisbury R3 In A *20 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 11:05:39 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4;15:36 PM 

U:\HPLC201DQ3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

14 

1 

AOC1 A, ADC1 CHANNEL A (U:\HPLC201004\MR BURNS\DATA\OCT\HPLC53PG98\013-1401.D) 

uS/em 

180 

160 

140 

120 . 

100 

80 

50 . 

40 

~ 

~ 

A 

! i t-

---l 

20- ~ I\ ~ ~ :g 

0 _j:::--=--=-~. 'C.:.~:.:.::~=-~,j-=-~1~:;;~::- =--~,.'~::-... ::" ;c:··=--=-=· =,;;:C;.==r=~:::;:=::;==;;=::;::=:;:=::...,._-r_~~-~-,-~~ L.. ______ 2__________ _L _________ 8,__ _____ ...:8,___ _____ _.1~0 _____ __,12<-_'-"m""l 

====,.=========<=<.e:====,=============""=='""=========================:====== 

External Standard Report 

"":<-'=====================================================.,====""======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

l. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------1--l------------------

3.126 BV 472.81418 1.70757e-2 8.07365 Fluoride 

4.257 BB 25.90080 2.86355e-2 7.41682e-1 Chloride 

Totals : 8.81534 

=========,========""·====="''="""==-==-:-~==""==""=-======='-""=""====""==========""===== 

*** End of Report *** 

Instrument AfCfrjlp<j!~i:>li.tJe- RJ-!fl¥?41 AM IGG EP~~~IQs'I.§Nflm ~~&Jiiffi2 AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e363 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1402.D 

Sample Name: Salisbury R3 In A *20 0910-96 

BORAL BRICKS 

================================~==================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 11:17:58 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC201 OQ3 \MR BURNS\~lETHODS \HPLC53PG98 .11 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

2 

j-------··--A5C1_A, .. A0c1 CHANNEL A (U:\HPLC2010Q4\MR BURNS:iJ5AfA\0Cl\HPCC53PG98\013~140'2.D) -· 

===================================================================== External Standard Report 

=========================================================="'--=""'======== 

Sorted By 

Calib. Data Modified 

Mul tipl.ier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s] [ug/mL] 

-------l------l----------r----------r----------r--r------------------ 3.125 BV 471.29227 l.70757e-2 8.04764 Fluoride 

4.257 BB 25.83895 2.86411e-2 7.40057e-1 Chloride 

Totals : 8. 78769 

*** End of Report *** 

1. 1.11.1 L2 1 n g .1 4 9 Instrument ATC"PRO"!JEC~Nb. P-i~l'll Al EA# 0910-96 Page 37 of 202 M IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~iJ.R.e364 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG96\014-1501.D 

Sample Name: Salisbury R1 Out A *10 0910-96 BORALBRICKS 

=======~===========~================================================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns JJocation 

10/l/2010 11:30:18 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

15 

1 

---····ADC1A."l\DC1 CHANNEL A (U:\HPLC2010Q4\MR BURNSIDAT/\\OCf\HPLcSJPG98\0{4:Tsof:iS-) -···----·--·· 

I 

l 

uS/em i 

1801 

160---i 

~ 

140 -3 

120~ 

100 ~ 

80~ j 

60..., ~ 

==============================~====================================== 

External Standard Report 

==,,==================""================================================ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] (uS/cm*s] [ug/rnlJ] 

-------r------r----------r----------r----------J--r------------------ 3.147 Fluoride 

4,254 BV 3.17554 3.7B526e-2 1.20202e-1 Chloride 

Totals ; 

1 \"larnings or Errors 

Warning : Calibrated cornpound(s) not found 

=============""====================""="''""='-"'=""=""'===:===================== 

*** End of Report *** 

Instrumen tAIC !'89'49'\loiJlg. P31QIIJ!;? 57 AM IGG EPR~~ g~1gs\l§N!f~!lr ~~c5'JEHf AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI!>IlJge'l65 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\0l4-l502.D 

Sample Name: Salisbury Rl Out A *10 0910-96 BORALBRICKS 

=~=~==================~~=====~======================================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/l/2010 11:42:38 PM Inj 

C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. ~1 

4/l/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\IIPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

15 

2 

-----ADC1 A ADC1 CHANNEL A (U \HPLC201004\MR !ilTRNS\iSI\fA\6CN·iPLCS3PG98\014-15026)-------~-~ 

uS/em~ j 

1801 

' 

' 

J 

' 

160 -~ 

140 j 

120~ 

·:l I 

40-1 

' 

20

0 1------.---r·--~-·:..,...-r j _______ j ~-r----~-~--·-~-',-'--',-----',:_·'-.I··:..,..._::··.::·,..· '-~1 s .. _ ~ : J 

___________ _,2~-----'4~---------~.§______ 

_:··c:..• ,=---=-,-----,---~-:-~~---=.d-.~~-~ ---,----r--~-~--1 _a ___ ~-·- 1'o. 12 

=======================================================~============= 

External Standard Report 

======~===~==========~=============================~====~============ 

Sorted By Signal 

Multiplier 

Calib. Data Modified 10/4/2010 9:29:44 AM 

1.0000 

Dilution 1.0000 

Use MuJ. tiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEJ, A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/em* s] [ug/mL] 

-------r------l----------r----------r----------r--r------------------ 3.147 

Fluoride 

4.255 BV 3.03742 3.78526e-2 l.l4974e-l Chloride 

Totals : l.l4974e-1 

1 Warnings or Errors 

Warning : Calibrated cornpound(s) not found 

=============~""=================="''=========-=========================="" 

*** End of Report *** 

IGG EPiE~!Iilrt~li'a!lll!~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

mi 

APPENDIX PAGij_,~~e366 l 0 f l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-160l.D 

Sample Name: Salisbury R2 Out A *10 0910-96 BORALBRICKS 

====================================~================================ 

Acq. Operator 

Acq. Instrurnen t 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/l/2010 11:54:58 PM Inj 

C: \HPLC2010Q3\MR B.URNS\METHODS\METROHM. M 

4/1/2010 4:15:36 PM 

O:\HPLC2010Q3\MR BURNS\METHODS\HFLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

16 

1 

~--··---- ADC1 A, ADCn:i'lANNEL A (U:\HPLC2010Q4\MR BURNSIDATAIOCnHPLCSJPG08\015C1fj(j'j~i))-···--·------f 

'· uS/em J f i 

I 1 j 

I 180-:j I . ' 160 ·1 

::: ~ I i 100 .. , 

j 

so j 

60 ~ 

.2 

.c 

I 40 ·· u I 

' 

2o ~ 

~ ~ ~ re Ol m 1 I C')M c:J.:S ~ ~ / J l ___ J -.,__.---J-~--.-=--,--J~---- t -- -~-- ------~ L 0 -----,-----~-~--, -1------,----,--~-~-r-,-~---~,----1---.----.,----.-- ~-........-----

, _________ 2 ________ £._ ___ ------~------~-L______ 10 12 --~ 

External Standard Report 

=:::.·.::-..;=-=======.:.:====================-==m=====~============================= 

Sorted By 

Calib. Data Modified 

I"'ul tiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1. 0000 

9:29:44 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm•s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.147 Fluoride 

4.250 BV 2.24146 3.78526e-2 8.4845le-2 Chloride 

Totals : 8.48451e-2 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

===============================================~====================~ 

*** End of Report *** 

Instrument AlfClR:R<Jli,EM:NJ>.II}!Q1>1i113 AM IGG EP~~<jilll\f~BJ'~1>~85~ AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!'il'll'e387 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1602.D 

Sample Name: Salisbury R2 Out A *10 0910-96 BORAL BRICKS 

==============<====================""'=========::::=============~:=<========= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 12:07:18 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

{modified after loading) 

16 

2 

~-------ADC1 A, ADC1 CHANNEL A (U:\HPLC201 004\MFf8[iRNSIDATAIOCnHPLC53PG98\015-1602.D) 

i uSicmlJ i 180 

i 

! 

160-

140 

I I 

10 ,. ________ ' i2 ' 

__ ._ml J 

====================================·===============================-== External Standard Report 

======:=================================-============================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

l. 0000 

9:29:44 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------1------l----------l----------l----------!--l------------------

3.147 

4.250 BV 

Totals ; 

2.29672 3.78S26e-2 8.69365e-2 

8.69365e-2 

1 Warnings or Errors 

Warning ; Calibrated compound ( s) not found 

Fluoride 

Chloride 

========,=========================================""<========·==="'-=·"··==== 

*** End of Report *** 

Instrument ATC:fi!\O!I~I<WN9-®-Hl121j122 AM IGG EPJI'~'l!IJI9ll/I:JJ'rl%'1-~MJ~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~368 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1901.D 

Sample Name: Salisbury R3 Out A *10 0910-96 BORAL BRICKS 

============================================================~======== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

J,ast changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 1:08:57 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10(4/2010 9:26:06 AM by IGG 

19 

1 

(modified after loading) 

r······--······ ADC1 A. ADCTCHANNELA (U:IHPLC2ioo-i-1o"'o"•'"\Miii<R·'>sii'ufi,RO;N;cS"'ID"A"T"A'"IO"'C""n=H'"'P"LC"'5"'3"'P"'G"'9 .. 81"o1"6'·1"9"'0.1.D) 

I us~:: I• 

160. 

140 

120 

100 

80 

60 

40. 

20 

" 

~ 

·~ 

0 

"' 

<..) 

I 

I 

' I ~ ~ ~~ § ~ I 

L--__ o__~...2 ... ~ 

·."'.-_· ... ~.---=---~4 ___ _c.. 

~~-+- _____ 

::::·:;;· c:T''=;.:::..:;::···.::c· 

__,6._ rc:::;::::·~:=,-:_:'""::· _____ :;:c::::;:;=:::;::::;::;:=:'_j~"""lr - -~,.--··--.----T· .. ·---,----·~ _,8c.. _______ ._.1_0 _________ g __ _!l]i<j 

===================~================================================= 

External Standard Report 

===========~============================~===================~======== 

Sorted By 

Calib. Data Hodified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1. 0000 

9:29:44 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTiroe Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------l------l----------l----------l----------l--1------------------

3.147 Fluoride 

4.250 BV 2.17866 3.78526e-2 8.24680e-2 Chloride 

Totals : 8.24680e-2 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

============================'"-"===:=======================">.'=-==::=·======= 

*** End of Report *** 

Instrument AID P!11P<I~GllH16. F!l1C!ll:!230 AM IGG EP~ ~\t,Ws?BN~~~f ~~c\'JJ:<fl AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIP11kje369 1 of 1 
( 

Sample Name: Salisbury R3 Out A *10 0910-96 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/2/2010 1:21:17 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

O:\HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

19 

2 

ADC1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNSIDATAIDCTIHPLC53PG9B\016-1902.D) 

uS/em 

180 -

160 

l40 

100 

80 

60. 

40 

20 :g ~ g~ ~ ;:: 

~ ~ ~~ :, 0 ·----~'------,-----J~---.-'-··· 1----------1----- ;:; I · r--~-'··-------r----·-J 

2 ___ _±_ s ________ L ______ 1Q__ ______ _ 

=========""-====~"="":=-=.--~======================-===""==="===========--======>=·""= 

External Standard Report 

===================================================================== 

sorted By Signal 

Calib. Data Modified 10/4/2010 9:29:44 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

3.147 Fluoride 

4. 250 BV 2.01728 3.78526e-2 7.63593e-2 Chloride 

Totals : 7.63593e-2 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

*** End of" Report *** 

Instrument l 10/4/2010 9:32:38 Al1 IGG EA#0910-96 Page43of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

12 mi~ 

Page 1 of 1 

APPENDIX PAGE No. 370 
Data File U: \HPLC2010Q4 \MR BURNS\DATA \OCT\HPLC53PG98\017-2001. D 

Sample Name: Salisbury Rl In B *10 0910-96 BORAL BRICKS 

=====================~=============================================== 

Acq. Operator EO Seq. Line 20 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 1:33:04 AM Inj 1 

Acq. 11ethod C:\HPLC2010Q3\11R BURNS\11ETHODS\METROHI1.M 

Last changed 4/1/2010 4:15:36 PH 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL. M 

Last changed 10/4/2010 9:33:01 AM by IGG 

. . ADC1 A, ADC1 CHAN'NEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCi\HPLCSJPG98\ciiT2o01.Df-·----

uS!cm J 

1801 

160 -~ 

1 

140 _j 

l 

120 -·1 

100 1 

1 aol ru 

____ 

~L-~---·r··-.J---~-·. 2'-. _______ __ _1_______________ J ! -~---,~·tr· 6 8 -----' 

--·-·····--··-_1_(J_·----··--·--

_) .--~'?:::;-~---=,_~-J 12 ml 

===============================================================o====== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 

1.0000 

1. 0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADC1 CHANNEL A 

RetTirne Type Area Amt/Area fu-nount Grp Name 

(min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------1--l------------------

4.233 VB 6.20973 3.61257e-2 2.2433le-l Chloride 

Total_s : 2.2433le-l 

================:o==========================""========oo~o:::================ 

*** End of Report *** 

InstrumentA1[q~9~9Q'I)Ij~ FIJ1:0j14 09 AM IGG EPiJ~~ ~~)£~ ~~Mo~~tH2 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEP~'lJ~71 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2002.D 

Sample Name: Salisbury Rl In B *10 0910-96 

BORAL BRICKS 

Acq. Operator EO Seq. Line 20 

Acq. Instrument Mr Burns Location 

Injection Date 1072/2010 1:50:22 AM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\t~ETHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG ~----·-··-·ADCTJ>.-;-!ibciCHANNELA(U:IHPL-;;Cc';2-;i01,;0;,;QC;4;'iiMT.R'c-iBUCfR"'N;iS'"\:;,Dc,A""TA"'I"'O"C"'T'"IH"P"L"c"'s"'3P"G"9"8"'10"1'7·""'2"'00"-2".o")c--~~~~-, 

I

. uS/em ·j I \1 

:::J II 1 

j ~ l i 140 --~ : 

I ::: l I 1 

BO~ ~ i 

-~--·····-.-·-·--· 

~L) .. ·-- ... ?.·-------~~---£__-----·----·---~--

T !o.,--1~-~-~---~,-_,_! _ _: __ ~---~-----.,.-_--_-_-_ ... ~_ .. _!_--'--------~.-~~----_-/_! 8 

_______ 10 

lr . .,~-----~-·=--:::-_-~- • --r=~l 12 mi 

====================================~=~============================== 

External Standard Report 

=============================================================~======~ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------J-~----I--~~~~~-~-)-~--------I-~~~------I~-J~----~-~-------~--

4.233 VB 6.02410 3.64293e-2 2.19454e-l Chloride 

Totals : 2.19454e-1 

==~o:=====::o=:==============::;==o:==::"====""""'"'~·-"""'============================== 

*** End of Report *** 

Instrument AlfclfJR'clJE{;(f:wl, ~~1ili4219 AM IGG EP~!R O~J~~1,g:r'l&~ ~~g~tg? AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~372 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2101.D 

Sample Name: Salisbury R2 In B *10 0910-96 BORAL BRICKS 

==========~=========~================================================ 

Acq. Operator EO Seq. Line 21 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:07:41 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC201 0Q3\MR BURNS\METHODS\HPLC53PG98CL. e1 

Last changed 10/4/2010 9:33:01 lll'l by IGG 

r-=~- ADC1A. ADC1 CHANNEL A(U :\HPLC201 OQ4\A1R··~B;:,U~R"'N;:_S;;\D;.A~T~A~\O"c'"T'"\H""P"'L""C53~G9~o18-21 iWi5j--

l u~~:o I ~ 

i ! I 1so.. 1 

! 140 -i i 

I 12o ~ 

100 ·l i 

I ao~ i 

20~ ~ ~ ~ ~ g c.:t ~ i \ i 

I 

I 

I

I :: ~ ~ - N ~ - 0 ~ i \ 

-i ______,.!:'_~-.--'__,....-~----,------'-~-- { _"!,_ 1-tri- --,-----------I-···<O ___ ..... :c;::=:;=::;::=:··'·::;:·.--'·-··· -~-"'---~----- ·r- ___ ______} 0 :f-.-~~--.-- ....,...--~-.~~-r·· --,.. - ·,.----..,---,...----.-· -;_-,,------1 _______ 2__ ~L________ _.,6'-------""- . 1 o 12 _!!!! 

=====~=============================================================== 

External Standard Report 

===============================·=========================:::.:============ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4(2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnLJ 

-------[------[----------[----------[----------l--1------------------

4. 225 BV 2.10500 3 _ 78526e-2 7. 96796e-2 Chloride 

Totals : 7.96796e-2 

===,==========o."o==========·================~"=========:-:o=..:==========""~·"==== 

**~ End of Report *** 

Ins t rumen tA llC ~ll~JqC21DI'I<il P91flH2 2 7 AM I GG EPA~~~ ~Bissro N f~~ pj~b~k~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'373 1 of 1 
Data File U;\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG98\0l8-2102.D 

Sample Name; Salisbury R2 In B *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 21 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:24:59 AM Inj 2 

Acq. Method C; \HPLC2 01 OQ3 \MR BURNS\METHODS \METROHM, M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U; \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL .M 

Last changed 10/4/2010 9:33:01 AM by IGG 

~- AI5cf A, ADC1 CHANNEL"i\(ii\HFLC2010Q4\MR BURNSib'~A"T"'A"IO'-C"nH""P"'LCS·J-PG98\018-2102.D) 

I u~:l· ~ 160 

140 _j 

j 

120 -! 

J 

100~ 

I 

' ;:13 I 

40 

·! r-.. Nco ~ g CO N _,lj 

20 -=j ~ q ~ N m ; g; 

\1 I 

I 

i N ("') . -i ...,; 10 ((:) I 

0 '.------~~·:.···+-, 'T--1

'·=. ~-~-,f~·'-.:<;== ----,·-==;===· . .J 

\__ i I ' , -- -...,.--------,------- ,. ... I .c.:::...r::C::;:::=;:=:;o::=;,.=~~ 

_______ ...... L........ 4 6 8 10 ___ 1£.______1!1!!] 

===================================================================== 

External Standard Report 

=================~============================~====================== 

Sorted By 

Calib. Data tvtodified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADCl CHANNEJ ... A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

4.225 BV 2.00891 3.78526e-2 7.60425e-2 Chloride 

Totals : 7.60425e-2 

=="'"·====.-:o·::::======o:.==============="====c:::"o======""======""=============:===== 

*** End of Report *** 

ATC PROJECT No. P-10142 EP'~~,.,.....,~.~. ~""""'""2 Instrument 1 10/4/2010 9:33:37 AM I~~ ~~~~~~ ·~VONUUtt~v 

IWGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE~<qij74 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2201.D 

Sample Name: Salisbury R3 In B *10 0910-96 BORAL BRICKS 

==============================================================~====== 

Acq. Operator EO Seq. Line 22 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:42:16 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG ~-------ADC1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATAiOCT\HPLC53PG"9'"8"'I0"'1"9~-2'"2"'0 1."D")- -----------.1 

j uS/em] [ ~ 

I

' :::J ;_, ! 

l . i : 140 -J ! i 

1 120 j ~ r I 1 

1 I ·!; I' 100-i 1 

1 I I . 

80~ I I 

j I i 

:: Ll ~,t_. __ ,_; .J. __ ! ; __ ) . -- _\;:-_____ T __ ___,__~L .. Q -T· --~-...,....- c:~::;:=:::::;,=:::;.:=~cc;:==r=-- -.-----,...---···-r··----·1 1 --~ _____ 2 __ 1._____ s ... __ a____ 10 _______ 1_? ___ r!J.llj 

=================================================================:=~~ 

External Standard Report 

======~==========================================~=================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1. 0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------i----------1--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

warnir:g : Calibrated compound(s) not found 

=============~~~-~""=========~·o::========="'"-"'============""=""=""=========·'~===== 

================="'·=======,=:c=======,========"-~========~=======c<'======= 

Area Percent Report 

======,=======-====""··~======""""""'""============::.:::'00======~==0'-';;;;============:oo:".=: 

Sorted By 

CaJ.ib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

InstrumentAli_q\1\)-lljQTOI'I'!i PWJ:l14 45 AM IGG EPR~ Q~J£;~ ~~YfPWo'3\otCf2 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEP~g<875 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2202.D 

Sample Name: Salisbury R3 In B *10 0910-96 BORALBRICKS 

===~===========~==============================;====================== 

Acq. Operator EO Seq. Line 22 

Acq. Instrument Mr_Burns Location 

Injection Date 10/2/2010 2:59:34 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

~-----·ADCi"I\:ADG1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATAIOCT\HPLCS3PG98\01g:2zo2:5)·------ ------~ 

I uS/em ··J ~ 1_: ; 

I - ~ 

I :::~ ~ II 140~ 

1 120i 

I 

100i I 80--\ II 

l 

l .. - ~L~~J~::t:~t-. ~1~;-= =Lh -=_,Lj =============================""===:::.::~======~============================ 

External Standard Report 

==================""'==•"'======o:======================================== 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 

9:32:52 At1 

Multiplier 

Dilution 

Use t1ultiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area A."''lt/Area Amount Grp Name 

[min) [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound ( s) no·t found 

=====================-======"""-'"''-~="'~~"'";=o:o===o:o==:::c·=========o:o=====""=""========o:o 

Area Percent Report 

a=::-::·=============== o:o= =="" == ==~="""::..c= '"==""' ==== ::.============================= 

sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

IGG EP!i'Mft~§Si\§NfT@S~ Pll<l'.f@f2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJF!I§e376 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG98\023-2601.D 

Sample Name: Salisbury Rl Out B *100 0910-96 BORALBRICKS 

=~==========================================~===============~=~====== 

Acq. Operator EO Seq. Line 26 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 5:00:41 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by I~G~G~~ 

~---:~,:~-l ADC1 A. ADtTCHANNELA(TJ:\HPLC2010Q4\MR BURNSIDATA\OCT(HPCC53PG98\023-2601 D)·--···--·----·---·-· 

1801 

160 1 

140 i 

120-.:j 

100 _j "' n 

·c 

_g 

'-' "' 

~ 

\ 

I 

' 

'• 

0 - -.--~--~---;-~c. ---, ,1\._1, ! ~ ~----~--_) ·-~~---'1cQ_·_\"_'-- ____ ·_~----. -~=-~--1··r·2 _____ _::_dm-=.; i '- t ·.,---""'·-- ·--,--,----,----··c·•••--, . 

2 .1. 6 ________ 8 -

=====~======~===================================================~==== 

External Standard Report 

========================================================~============ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1. 0000 

9:32:52 1\M 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: I\DC1 A, ADCl CHI\NNEI, A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s} [ug/mL) 

-------l------l----------l----------l----------l--1------------------

4.152 BV 282.51471 2.64899e-2 7.48380 Chloride 

Totals : 7.48380 

=======·'""'=======""============""'""=======================-"'""'============== 

*** End of Report *** 

Instrument:ATP '1\W.Jfifr.!ct!<u P91PW: 28 1\M IGG EPAEit/H\~i1;ll;~ f~p'iiM&c?2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGElli.<ij<l\77 1 of 1 
Sample Name: Salisbury Rl Out B *100 0910-96 

BORAL BRICKS 

Acq. Operator EO Seq. Line 26 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 5:17:59 AM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

J,ast changed 10/4/2010 9:33:01 AM by IGG 

~- .ADC1 A, AOC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\QCT\HPLC53PG98\Q23:2$Q2~0) 

I uS/em -J I l j ! ' 180 -I . I 1 

I 160 ~ 

' 140~ 

120 -1 

100 -~ 

80j 

-1l 

·c 

0 

"' (_) 

so ! ;}, : i 

A as ~ _,,/ \\ ;_: 

40 

20 ! \ t- :; ·....,....___ __ 

0 -+-~- ·--.-----..·~-·r··- ,--~L '--1~- .. · I ------- -~-------------· -..---~~----,-----..,.~--.,- .. ---~----~--~=-:=::;::=:;::::::::11 1 · 

'------------·£_ ____________________ __± __________ __,6,_ ______ 8 . _______ _1_Q________ 12 mid 

=========""=""===========================================::o==========--=== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 

9:32:52 AM 

Multiplier 

Dilution 

Use Multiplier & 

1. 0000 

Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------1--l------------------

4.154 BV 278.87683 2.64928e-2 7.38822 Chloride 

Totals : 7.38822 

=====·=======================================,.,=====================·=:;:;= 

*** End of Report *** 

Instrument 1 10/4/2010 9:35:37 AM IGG EA#0910-96 Page51of202 Page 1 of 1 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT APPENDIX PAGE No. 378 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-240l.D 

Sample Name~ Salisbury R2 Out B *10 0910-96 BORALBRlCKS 

===================================================================== 

Acq. Operator EO Seq. Line 24 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 3:51:29 AM Inj 1 

Acq. Method C:\HPLC2010Q3\M~ BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed : 10/4/2010 9:33:01 AM by IGG ,---·····----·- ADC1A."Ai5CTC-~lAFiNEL A (U:"IH.;P_;.L_:;C.;c20i.1C:O,:;Q-..4~1Mi,R~B~UC,1R"N_;S;_:I;,:D:;,A"'TA"'I"O"'C"n"H"'P"L"'C"53"'P"'G"'9"'8"10"'2 1·"'24""0"'1".D"')---

uS/em 

180 

160 . 

140· 

120 

100-

80. 

60. 

40 

20- ~ ~ a; 

N . f"5 ..,; 

I 

/ i -'-~~ ~=~ -~ ~-

L ------~---- L-==~-·-·_· _-_---.....:4c.·· _____ __,_6,_ _____ _,s ____ _ 

=.,.~·==~==============,====================================,============== 

External Standard Report 

================================================================~==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area F~t/Area Amount Grp Name 

(min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calib.rated compound(s} not found 

= := =~ :::.= . .,.- .== ======= === = = = ======:::o:==-::'oo~.::.== "~""===·'"-=========================== 

====================="'-'=======""~==============================="-'======= 

Area Percent Report 

===="="-''=>0:>================================================""'==--'===""'====== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier ~ Dilution Factor with ISTDs 

Instrument AfC:fWAJj'~j5 :1'\9 '9-! !\'IJI?32 AM I GG EP~ft!R~I§llJ@Nf1m ~~<'/J~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e379 1 of 2 
1../d.l.ct l'..L..Le u; \.tH'Lt....LU.l.UI.,J':I\lvl.K ~UKNCI\Uf\Tf\\UCT\HC'.LC!Jjt'G;l!j\U~l-L40L.0 

Sample Name: Salisbury R2 Out B *10 0910-96 

BORAL BRICKS 

=======================================================""'-============= 

Acq. Operator EO Seq. Line 24 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 4:08:47 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method t): \HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98CL.M 

Last changed : 10/4/2010 9:33:01 AM by IGG 

---------,.-DC1 7( ADC-1 CHANNEL A (U \HPLC201004\MRBURNSi'eoi=.A""TA00I"'O"'c"n"H"P"L"C'"'5:iPG98\621-2402D)--

uS/em l 

180 "1 

160 ·-j 

140---1 

120J 

100j 

~ 80-

60 

40-

20· 

0 

~ ~ N (f) _______. __ r·---' 

-----,-

C!> 

~ I 

I 

N o; "' ~ J -.:= a:) 

. ···---~-~-----:...~=:::::..: __ ·~-'-="-'-;::·:::-::::;:=::;:::~:;: - ' I ' -- -··.---,-------,-----·r-------'<"" 

__ ;c__ -- --- -- 4 6 . 8 ___ 1Q__ ____________ :!_? _____ mi 

=~=~==========================================~====================== 

External Standard Report 

====='""""-'==============================,=========================""=""-"== 

Sorted By 

Calib. Data Modified 

Multiplier 

DiluU.on 

Signal 

10/4/2010 9:32:52 AM 

l. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] (uS/cm*s] (ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning ; Calibrated compound(s) not found 

======================================================~=========~~=== 

================~.,=========="==~==============::.~""-======================== 

Area Percent Report 

::.~====================o-.;:::::=============""'"""========'='===:=:.===========::::======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

'-_,_ot.AL?_a,o ~ , •. _, 4 EA#0910-96 Page53of202 Instrument Al C""PRO"JECl "NO. P-iU1"4'z- AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!':'N"l#380 1 of 2 
Data File U:\HPLC2010Q4\MR BORNS\DATA\OCT\HPLC53PG98\022-2501.D 

Sample Name: Salisbury R3 Out B *10 0910-96 BORALBRICKS 

========================================.,'""=========================== 

Acq. Operator EO Seq. Line 25 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 4:26:05 AM Inj 1 

Acq. Method C: \HPLC20l0Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed : 10/4/2010 9:33:01 AM by IGG 

uS/em lADC1 A. ADC1-CHANt:fEL A (U:\HPLC201DQ4\MR BURNS\DATA\OCT\HPLC53~ .. G9~t2·2SOiJlf·--···-···---··---·--~ 

180. ' q i 

; I ; 

160 . ' i 

I 

140. l 

120 

100 

===================================================================== 

External Standard Report 

====================================<================================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 Al4 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[mic.J [uS/crn*s) [ug/mL] 

-------j------!----------l----------l----------1--l------------------

4.236 BB 89.76620 2.69549e-2 2.41964 Chloride 

Totals : 2.41964 

*** End of Report 

InstrumentAllC II'El04!l®lli1J F'l10J§2 06 AM IGG EPifC~ ~~1Bs?8N~g~jl ~~oJ&Cf AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!PilJgeJ81 1 of 1 
,--------- .. - , .... ------ ,~ ..... , ......... ~ , ............ .._ ..... __ .. .._._...._, ,,_,._" 

Sample Name: Salisbury R3 Out B *10 0910-96 

BORAL BRICKS 

================================~===============~================~=== 

Acq. Operator EO Seq. Line 25 

Acq, Instrument Mr Burns Location 

Injection Date 10/2/2010 4:43:22 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/l/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:IHPLC201 004\MR BURNSIDATAIOCnHPLC53PG981022·2502.D) 

' "' ~ ~ ~ tO 

~ F.!: 'V o;: N (") i\ ..j. --- ,.......-.-J--~..,.U..--'---+--

4 6 

1 

8! 

<ci --.----------- ..... ':::-=-

8 10 

================;'::;=======o:::=="-•======================::====,======"~"'·======c 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/em's] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.238 BB 87.67069 2.69712e-2 2.36459 Chloride 

Totals : 2.36459 

==================="'o'==="-"=~~=======:=::-==========o::==========;o;;;::o=::-::========= 

*** End of Report ->·*->-· 

Instrument 1 10/4/2010 9:35:19 AM IGG EA#0910-96 Page55of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Page 1 of 1 

APPENDIX PAGE No. 362 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-330l.D 

Sample Name: P4 R1 In A *10 0910-96 

BORAL BRICKS 

===========~=======================================~================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 8:23:39 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2010Q3\MR BURNS\METHODS\HPI,C53PG98 .M 

10/4/2010 9:36:41 AM by IGG 

33 

1 

(modified after loading) 

~---_""A"o"c"1"A'.'A"DC""'1'C"H'i:A<'iNi,NJiE~L::.,A<-;(U:iH'PLC2010Q4\MR BURNSiOATA\OCTIHPLC53PG98\026·3301.D) ---·- ·-·---, 

j uS/em j I l 180 _J 

! -! I 

1 1601 i 

i -i ! i 140 -~ 

i 120 i 

I 1:: J ~ 1 ~ I 

J N 0 I 

0 ;:;t; '\ ~ ~ ~ f 

1

40 o-; f 

--2 o ~r=>-_-~-__g,.--~-· .;.•-_-_·""~·-l'-~ __ ,._-:,, _.:!....:,. ,---~·-__ .:_--=·=6 =~;~~-~=_£_~ ----~._c.-:-_:..-~_f_··.---~--~-~-~~-~-~~---,'·o-~~---;'2 . J 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:36:41 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] {ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.121 BB 225.06882 l.70529e-2 3.83808 Fluoride 

4.261 BV 5.95215 3.6552le-2 2.17564e-l Chloride 

Totals : 4.05564 

*** End of Report *** 

Instrument A'tC~Ee~M>. i£.1Mil245 AB IGG EP~~ ~!j}lg;;IIBN~1l§~ ~~c?M¥l AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PAG1i'lllqe383 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D 

Sample Name: P4 Rl In A *10 0910-96 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Ana_J.ysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 8:35:58 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

33 

2 

ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D) 

uS/em 

180-

160 

140 

120-

100 

80- I 

~ 

"' /\ ~ ~ ~ N j '· ..j. ~ ···----~---· --- l_j/ __ \....__~ ---.--_j- 10 .---------' ~ 

0 ' ' 

60-

40 

~ 

20 <0 

N 

I 

I r----------· 

L ___________________ __ g____ __ _ _ ____________ _± __________________ _§__ ___________ ..§ _________ _._1 o'-------"12.,___'"m"'i 

External Standard Report 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1. 0000 

9:36:48 AM 

Multiplier 

Dilution 

Use t-1ultiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal l: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.121 BB 226.27061 1.70532e-2 3.85863 Fluoride 

4.261 BV 5.67176 3.70602e-2 2.10197e-1 Chloride 

Totals : 4.06882 

*** End of Report *** 

'Wl.'--1.~,, g -"' "·" 5 8 EA# 0910-96 Page 57 of 202 InstrumentATcfl<ill~tYN . t"-ltn'4~ AH IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~ 'l-/i!!'384 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-360l.D 

Sample Name: P4 R2 In A *10 0910-96 

BORAL BRICKS 

=================================~=================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 9:37:38 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

36 

1 

·------.A5c1A,.AocTCHANNEL A (U:IHPLCiO-fOQ4\MR BURNSiDATA\OCT\HPLC53PG981029-3601.0) 

============================~=======~===================~============ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

ExLernal Standard Report 

Signal 

10/4/2010 

1. 0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area P~t/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------[----------l----------l--!------------------

3.137 BB 685.05603 1.70822e-2 11.70224 Fluoride 

4.263 BB 36.18887 2.79640e-2 1.01198 Chloride 

Totals : 12.71423 

========='-""'==·-~==''"~~==============================================;:;:===== 

*** End of Report *** 

'-"-'·""" 111 ~' 7 EA# 0910-96 Page 58 of 202 Instrument MC.....VJt:b1JNO. j9.jtf17423 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & s. SALISBURY PLANT 6 

SEPTEMBER 2010 

------1 

I 

APPENDIX PAG~'Ni\!'385 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3602.D 

Sample Name: P4 R2 In A *10 0910-96 BORALBRICKS 

==============""==================,=======,===""======================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 9:49:58 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

0:\HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AH by IGG 

36 

2 

{modified after loading) r ·····--···-AocTJCAbc1TH-ANNEL A (U:IHPLC20;i=1"0,_;Q~4Ci1MiR~BUC'RiiNrcs"'I"DA""TA"'I"O"C'"T\"H"P"L""c"'s'"3P"'G"'9"'8"'10"2"'9-'3"'60"2'.~o)c--------, 

' uS/em 1 

180 -] 

j 

160 

140 

120 

100 . 

80 . 

60-

40 

20 

====================================================================:::; 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[mi.n] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.137 BB 686.89960 1.70822e-2 11.73376 Fluoride 

4.261 BB 35.98354 2.79736e-2 1.00659 Chloride 

Totals : 12.74035 

=================o=:·=================,.============""'="'-================== 

*** End of Report *** 

Instrument A-[Cflf)J-1~\il.i J'&· f9-~~1f? 4 5 AM IGG EP,i;'MF1~§11/6Nftl!S~ P~O>JE(W AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG\>~Ije386 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3701.D 

Sample Name: P4 R3 In A *10 0910-96 BORAL BRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Me~hod 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 10:02:17 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

37 

1 

~-····-···-·······Ao{TI\:"I\5c1·CHANNEL A (U:iRPLC20ib041MRBURNS\DAT AIOCTIHPlC53PG98\o:lo-370TD-J - -·· ·-·· 

I us::~ I 

1 160~ 1 

I 140 ~ I 

I 120 ~ 1 I 

I 100 ~ u:: I 

I 1 ~ I ao-i ·-· 1 

~ M Q) I ~ i\ "g I 

::l~ N n ~ ~ ~~ 1 

1 20 ~ I \ ~ ~ j l N I \ '<t U'l I 1 L_ o - --- ~-- ,----:-~~=~.-----~~ __ -~;~---- __ r __ ~ -~~ _ T----,-=--~-~--,-~~J 

=======~========================~================~~==~===========~~== 

External Standard Report 

===================·""'=~.,===='-"=='""================"''==,=-="'"""================ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[mln] [uS/em's] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.135 BB 641.72162 1.70812e-2 10.96138 Fluoride 

4.261 BB 28.69785 2.84053e-2 8.15170e-l Chloride 

Totals : 11.77655 

*** End of Report *** 

Instrument AJC]ft!'fll!J"fili'IJ> §·:1§1r':254 AM IGG EP~/S5l\IJ'im<r~IJ~J?8f AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGji~387 1 of 1 
Sample Name: P4 R3 In A *10 0910-96 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Metho.d 

Last chailgect 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/2/2010 10:14:37 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

37 

2 

~---· ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MRBURNS\DATA\0CT\HPLC53PG9-8\030~3fo~i0)~----·~----

uS/em l 

180-

160. 

140 

120 

===========~==============================================~====~===== 

External Standard Report 

="'"·========,.,=========~-~=,==""==,======================================== 

Sorted By 

Calib. Data Hodified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

1.0000 

9:36:48 AM 

Use l..IJultiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTi.me Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------i----------i----------l----------1--l------------------

3.135 BB 640.17627 1.70812e-2 10.93496 Fluoride 

4.261 BB 28.99791 2.83832e-2 8.23054e-1 Chloride 

Totals : 11.75801 

""""""''"'====-==:::=====""===::o·=::e:=============================;"===========o.-:.:=:o--=== 

*** End of Report *** 

lnstrument 1 10/4/2010 9:38:02 AM IGG EA#0910-96 Page61 of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Page 1 of 1 

APPENDIX PAGE No. 388 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3801.D 

Sample Name: P4 R1 Out A *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 10:26:57 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

38 

1 

(modified after loading) ~---~A~o~c~1~A-. ""'A"'o"c"1 "c;.H;;A:;:N.;N;;E:;L:.;A:.:;(u:IHPLc2oToa4\M"R suRNSIDA tlllocnHPCcs3PG9slo31-3ao1.DJ ________ ---------- --

uSJcm l 

180 j 

-1 

1 160 ·j 

.1 

140--! 

120 l_1 

100 J 

80 

60 __ -

40- I 

I 

__ j ~-,---r·---~-r-··--.··---~------,--

8 ___________ _!_0 ____________ ________11. ____ mi 

=======================""===========================================-=== 

External Standard Report 

====:;;:==:===========~,==,============,==============""'========='"'"·=""'======= 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 

9:36:48 AM 

Multiplier 

Dilution 

Use Multiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------l------l----------l----------l----------l--1------------------

3.118 BB 29.37646 1.67627e-2 4.92430e-1 Fluoride 

4.259 BB 10.03031 3.23729e-2 3.24710e-1 Chloride 

Totals ; 8.17140e-l 

========""'='""'·--==,=================================================:====="" 

*** End of Report *** 

IGG EP,Ii;II!IM.!Mi!lSl6Nfl1i§<f ~i!<llUE200 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~£18e389 1 of 1 
Sample Name: P4 Rl Out A *10 0910-96 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Hethod 

Last changed 

}:\nalysis Method 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/2/2010 10:39:16 AH Inj 

C:\HPLC2010Q3\HR BURNS\HETHODS\HETROHH.H 

4/1/2010 4:15:36 PH 

U:\HPLC2010Q3\MR BURNS\l-iETHODS\HPLC53PG98.!-i 

10/4/2010 9:36:41 Al-i by IGG 

(modified after loading} 

38 

2 

I

S::: j ADC1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCf\HPLC53PijG98\031-3802.D) 

160 l . < I 

j 140 -i \ . 1 : 

::: l I 

l

i ::j ~ ~ I N ~ ~ 

L 

2

: .k:: ~. •-::"3 3- 0 -~ ,;'; T • -~ --T - I - -c =:--'-'-

1 

~-,-~--~-r-----.------~ _ ____ ___1. _________________________ 4 6 ___________ B _____________ 10 12 mi 

============================..,==========,============================= 

External Standard Report 

==========================~==============~=========================== 

Sorted By 

Calib. Data Modified 

t-1ultiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s) [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.117 BB 29.06601 1.67592e-2 4.87122e-1 Fluoride 

4.258 BB 10.10172 3.23298e-2 3.26587e-1 Chloride 

Totals : 8.13709e-1 

*** End of Report *** 

1 1 o /4/2 01 o g 3 s EA# 0910-96 Page 63 of 202 Instrument ATCPROJECTNo. P-ioP4~ 1 AH IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE'm8 390 1 of 1 
Sample Name: P4 R2 Out A *10 0910-96 

BORAL BRICKS 

============~=============~=~====================================~=== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 10:51:37 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

{modified after loading) 

39 

1 

,--------iili"cf :;;:·A-15cTcHANNEL A (U:\HPLC201004\MR BURNSIDAT AiOCTIHPLCS3PG981532~39DT6) ____ _ 

I 

L 

u~::l 160-

140 _j 

' 

120.:! 

; 

., 

100 j 

80 ·j 

60~ 

6 8 

======,.=========================:::==""'""=================""============== 

External Standard Report 

==================================~================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] fuS/cm*s] [ug/mL] -------r------r----------l----------r----------r--r------------------

3.119 BB 36.11133 l.682SOe-2 6.07572e-1 Fluoride 

4.260 BB 12.06006 3.13464e-2 3.78039e-1 Chloride 

Totals : 9.8561le-l 

===""====='"-'""''-~~:.;:c,__-=,======::::==========:.=:~==::::.oo'~"'======================:::o=,;:::..~=:coo 

*** End of Report *** 

'- 1"'-'d .~.,. .. ,.,.o " -,.o _? 6 EA# 091 0·96 Page 64 of 202 Instrument A"C 1"1<' Jtet-'1'Ntl. ~-1,r.fz- AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIXPA~391 1 of 1 
Data File U:\HPLC2010Q4\MR BORNS\DATA\OCT\HPLC53PG98\032-3902.D 

Sample Name: P4 R2 Out A *10 0910-96 BORALBRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 11:03:56 AM Inj 

C:\HPLC2010Q3\MR 8URNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR 8URNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

39 

2 

~--:~:: --AocOC ADCi CHANNEL A (U:\HPLC2010Q4\MR BURNSIDATAIOCiiHPLC53~G98\o3·z:3-9b2.o)-----------~ 

i - l 

1 160- 1 

::: l I ~ I 

1oo -:1 I j ' 

oo, I 

60~ ~ ~ ! 

4

oi ~ (0 ~ ~ tl 

0 0) ! ! di 

2Ql K! '; ~ ~ 1 

I ___ 0 .t··;<:'c:;=. c5?.: ---:.,. ,. ~-~------------~- i----~c_--:; =-' c-;'Q~-:__-_=-··-1y~-;;;;-

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADC1 CHANNEL A 

RetTime Ty~e Area kmt/Area Amount Grp Name 

[min) [uS/cm*s) [ug/mL) 

-------:------~----------l----------r----------l--l------------------

3.120 88 36.00581 1.68242e-2 6.0576Be-l Fluoride 

4.260 BB 12.07534 3.13399e-2 3.78440e-l Chloride 

Totals : 9. 84209e-l 

*** End of Report *** 

Instrument A}Cf~,P,f~~lii'tl f9-!(\1gl?34 AM IGG EP~ifllA\!lffii§Nlffi!'f Pr'i6'J~ AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e392 1 of l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4001.D 

Sample Name: P4 R3 Out A *10 0910-96 BORALBRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 11:16:16 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

40 

1 

~---- ADC1 A ADC1 CHANNEL A (U IHPLC2010Q41MR BURNSIDATAIOCT\HPLC53PG98\033·4001Ti) -----· -----

1 "'::j 

I :::-1 

! 120~ ! 100 -j 

! 1 

80 "i 

60 i 1 

40 -i 1 :0 m o 

l 20l ___ J_~.---.J~~,~ ~ ~ ~ " _ _. ___ • ____ ) ! 

0 +- · --,-----1-~~---,----.-- - r .......,. -. - -.------~~-,--- ...----.---~--.,--~ 

------ - ______ 1 ____________ ..,1 _________ 8 ______ --- -~----·---· -- __ !.Q__ ___ ~- - ___ _1?..__/!!L 

External Standard Report 

'='=-=-===================================================;:::.==""=========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1, ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.117 BB 40.65833 1.68553e-2 6.85310e-1 Fluoride 

4.259 BB 12.36708 3.12204e-2 3.86105e-1 Chloride 

Totals : 1.07142 

==,==========================e========================================= 

*** End of Report *** 

InstrumentAICf'{Rp!I~Qlll-JO.i!)1QlliJ<'42 AN IGG EP~~l~ii/BN~\l'f ~~8J~ AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI!>!II<je393 1 of 1 
Sample Name: P4 R3 Out A *10 0910-96 

BORAL BRICKS 

===~================================================================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 11:28:36 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\HETHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

40 

2 

~--····· ... ADCTA. ADC1CHANNEL A(U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\o334002.D) 

I uS/em ·i 

180~ 1 

160 ~ 

' 

140 ~ i 

120 _j i 

100. 

80 

60 

40 _-

~ "' "' , 

0 ~ E a: () 

If) ~ .: j' 

200 J.=--='.-~-='--1'==.:.-t=:...··:' . ' • ' I ' -.::~:.· ·:..· 2';=:::;:::=::;=::::;====·---- •·•, ..... T·-,--~--,-----~--r---1 

'------'2'-- _________ _j _____________ 6 8 ___ 1_9 __________ ~1?.- mi 

====================~=================="""·==============""'========o======= 

External Standard Report 

=~=======================================================~=========== 

Sorted By 

Cnlib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, .~DCl CHANNEL A 

Ret'rirne Type Area Arnt/Area Amcunt Grp Name 

[min] {uS/cm*s] {ug/rnL] 

-------l------:----------l----------l·---------1--l------------------

3.119 BB 40.55775 1.68547e-2 6.83590e-1 Fluoride 

4.261 EB 12.31650 3.12407e-2 3.84776e-l Chloride 

Totals : 1.06837 

===========o=============='='·===============•:o======================~==== 

*** End of Report *** 

Instrument 1 10/4/2010 9:38:52 AM 1GG EA#0910-96 Page67of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Paqe 1 of 1 

APPENDIX PAGE N"o. 394 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-430l.D 

Sample Name: P4 Rl In B '10 0910-96 BORALBRICKS 

Acq. Operator EO Seq. Line 43 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 12:29:43 PM Inj 1 

Acq. Method C:\HPLCZ010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METH0DS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG r-·-····--·~----- ADC1 A, ADC1 CHA-NNEL".A:'(tJ:\HPLC20f0Q4\MffBuf.R'»N:«S;;,\D"A"T"-A"ID"c"n""H"'P;cLC"'s"'3"P"'G"'9'"8\"'0"'347-4301.D) 

I

I uS/em 1 i!; 

' 180-j 'f 

160 1 I 

140 ~ I 

External Standard Report 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/em's] [ug/mLJ 

-------j------l----------j----------l----------l--l------------------

4.234 BV 4.51100 3.78526e-2 1.70753e-l Chloride 

Totals : 1.70753e-l 

================·""""==~=-================="'"==================,=~-""""'""========= 

*** End of Report *** 

ATC PROJECT No. P-10142 

Instrument 1 10/4/2010 9:39:49 fu~ I EP!B(t!'l8GI1$1l!Nil'l!l!)ll~ 

X8GUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 395 Page 1 of 1 
ua1:a t~.Le u: \I11:'LCLU.iUU.q\MK tsU.KN::,\Uf\TA\UCT\H.r'LC~.:ll:'l:i!:lti\U.:Sll-ll.:lUL.U 

Sample Name: P4 Rl In B *10 0910-96 

BORAL BRICKS 

============================<==============-===============;::=========== 

Acq. Operator EO Seq. Line 43 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 12:47:01 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

.Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 l\1-1 by IGG 

r

.. ADC1 A. ADCi CHANNEL A (U:IHPLC2010Q4\Mil"8URNSIDATA\6cYiHPLC53P. G981034-4302.D) 

em -1 j 13 

MJ . ' "' i ~ 

~ i ! 60~ ! i -j i i 1 I ! I 140 :j I i 

1 ~ I 1 1 120 J 1 : I i , , 

I 

100i ' ! 

80-:j 

i 

I .. _..:_ \"' 

10 

========================================='-"==============::":============ 

External Standard Report 

='=============================================~~==============~====== 

Sorted By 

Calib. Data Modified 

Multiplier 

Si.gnal 

10/4/2010 9:32:52 AM 

1. 0000 

Dilution 1.0000 

Use Hultiplier & Dilution Factor with !STDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------i----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or E.rrors 

Warning : Calibrated compound(s) not found 

========================;==""'=-=,::==========-,=========================""== 

============""=:=:=================="-""'============;=:======·-"==============~· 

Area Percent Report 

========================================~=====================~====== 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument 1 10/4/2010 9:39:57 AM EA# 0910-96 Page 69 of 202 IGG 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

T 

12 

i 

'I II 

! i 

i i . ! 
Data File U: \HPI.,C2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4401.D 

Sample Name: P4 R2 In B *10 0910-96 

BORAL BRICKS 

================================================~==================== 

Acq. Operator EO Seq. Line 44 

Acq. Instrument lVJr Burns Location 

Injection Date 10/2/2010 1:04:23 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\MET'ROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

uS/em l AOC1 A, ADC1 CHANNECiiW~RPLc2010Q4\iofR""'B'"u"R"N"s\D~A"TCA\"O"c"'T'"IH"P"'L"'c"'s=apl <39~35-4401 .D)·--··· .. ······-··-·1 

1801 ~ 

1601 I I_ I' 140--1 \ 1 1 ! ! 

120 ~ I 1 , 

1:: l_ I I ' 

w~ 1 201 ~ ~ ~ ~ J \ j 

a-t=-·-'· N~-=.:' · ~:-==r:_~_:_.c=;:: .. _ ! ~-=;---==-r~~_:::_,-__-=;= __ r==;=d L_ ____ -<.2 ________ 4___ .. _______ 6 ______ ,__ a 10 ......... _11.._...!!l!tl 

=========================================''"========================"="""'"" 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4//010 9:32,52 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------j------j----------l----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

lr'Jarning : Calibrated compound(s) not found 

=·======.o::=::"="""'"~"'"-:::=============='-"'======================,================="":~::: 

=================::.~""'"""'====================================='"'=====.;======= 

Area Percent Report 

============================,...==·~..;=============:..::o.·===============,.,==""==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

Dilution 1.0000 

Use Mul tipl:Ler & Dilution Factor with ISTDs 

EA# 0910-96 Page 70 of 202 

IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~il-@397 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4402.D 

Sample Name: P4 R2 In B *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 44 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 1:21:41 P~J Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\IIFLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A. ADC1 CHANNEL A(U:IHPLC2010Q4\MR BURNSiDATA\i5ci'IHPLC53PG.S8\035'-4'4"0"2"D'-)-------, 

===================================================================== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

===-:-=~=:=o~===-================e:==~-,;:;;:===c""=========""="'===================== 

=============""'"========================================"'"-=~-"""'==========""" 

Area Percent Report 

================================,.,===============================::==.=== 

Sorted By 

Cal~b. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AIC:f\W)!JJ'l<WN91l}l~1Jig14 AM IGG EPm~9s'I8N%\li- P~8J~ AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~ill!le398 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D 

Sample Name: P4 R3 In B *10 0910-96 BORAL BRICKS 

==========~================================~=========~=============== 

Acq. Operator EO Seq. Line 45 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 1:38:59 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis t1ethod U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:\HPLC201004\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D) 

uS/em 

180-

160 

120· 

100 

80. 

60-

40 

N 

"' N 

N -'-

' 2 

~ I 

I 

i 

! 

I 

4 6 8 10 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with lSTDs 

Signal 1: ADCl A, ADCJ. CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[minJ [uS/cm"'"sJ fug/mL] 

-------l------l----------1----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(sj not found 

===~==~=============================================~======~========= 

Area Percent Report 

============,.~=="~'-"====""·=============="""'"===========~.,=================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AlfC:iAAOUJ'1jiNJ> 9-j Glll22 3 !\_M IGG EP~~t'R O~J&-~B~f~"r ~~8~~8f AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

fl 

'I I' ,! 

I' 

11 ------~--L_ 

12 mi 

APPENDIX PAGE~399 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4502.D 

Sample Name: P4 R3 In B *10 0910-96 BORAL BRICKS 

==~======================================================-=========== 

Acq. Operator EO Seq. Line 45 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 1:56:17 PM Inj 2 

Acq. Method C: \HPLC2010Q3\!~R BURNS\METHODS\~1ETROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed : 10/4/2010 9:33:01 AM by IGG ---------- A6C1"A;·;..oc1ci=fiiNNEL A (U:\HPLczo1oa4\MR BURNs\oATAiocni-IPLcs3PG9aio36-4so2.1:l)- ---- -----

uS/cm~- 180 

160 

140 -j 

120 -~ 

100-1 

I 80~ 

I ::1 M 

l ____ ;~~~~-~~~-~--i- 6 

===================================================================== 

External Standard Report 

=========================================,.,.==:;:"~,:,:,""'====================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1_0000 

1.0000 

9:32:52 1\!1 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEl, A 

RetTime Type Area Amt/Area Amount Grp Name 

[min J [us I em* s] [ ug /mL J 

-------l------l----------1----------[----------l--l------------------

4.156 Chlor.ide 

Totals : 0.00000 

1 Warnings or Errors 

Warning ; Calibrated compound(s) not found 

======================================""="·"""""""===================""~==== 

="'~·="'"""""'=""~==="-""=·~~=::.o::o-::=====================-,:==='-==='""""';;:,===================== 

Area Percent Report 

==================c-.,::.o======:..--o======================================:oo=== 

Sorted By 

Calib. Data Modified 

Ivlultiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

l. 0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AjTC1flRO!J,EM:Nl'-IJ"1q1J4i132 AM IGG EP~~Clrul$-§j\l,J'-fm't~85i?Bf AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJ.i«<l'e400 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-460l.D 

Sample Name: P4 Rl Out B *10 0910-96 BORALBRICKS 

Acq. Operator EO Seq. Line 46 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:13:36 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Ana1ysis.Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG ~----··-··-·;o;;oc1A;-ii:o(:"TCHANNEL A (U.:IHPLC2CllOQ41MR iillRlJs\bilfl\locnHPLt:"i5":ii'G981037:46oi·~o)··----·- ·--·1 

i uS/cm·l I g I J • I 180·i Cl l 

160 ~ I I 

140cj i 1 

J I I 1201 i I 

1001 i . 

80-1 

J 

60 -l 

~ 

I 40~ 

I 1 :'$ ~ ~ ~ 1 I 20 -~ N 00 "<t 0 I I 

I N ....j t,6 t- \ 

, a r~-~::-_....;-.::.;: =.=--~-=;:..-:.~=-==.---~-:::_:;._~-r---=.-=-~ .. =-------.---=--r--.--- - ~~-1=-=~- ---1 

L ______________ ____1. ___ ~-----------•---~--------------§ _______ -~--------~------------- ____ !Q_________ 12 mini 

External Standard Report 

==================--===·'-"===·==="'=======================================;,;;,; 

Sorted By 

Calib. Data Modified 

Mult.iplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Sjgnal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area A..'tlount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------i----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

============:=:==========="-'>==="--=""'""'~'·~="'================================= 

========""·"'"====================================================""====== 

Area Per:·cent Report 

==============-==================="-"'~""=====..,======"-"===================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AICfi\'P<fl'l'(itie· '9-!\1\1?41 At1 IGG EP~~fls'lt§Nifi!\19' ibft6'Jiil}12 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIP~e401 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4602.D 

Sample Name: P4 Rl Out B '10 0910-96 BORALBRICKS 

================~==~================================================= 

Acq. Operator EO Seq. Line 46 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:30:53 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BORNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

r

--·-·-·· ·:i\bci·A~ADC1 CHANNEL i\(iTiRPLC201 o·~oC.•i:,Mi;Ri-EisuifRi;-N;:is,;,,:;;D:;;A,.T A"l"'o"'c"'n"H"P"'L"c"s'3P'"G'"9'"a"'lo"3"'7-4602.l5j""'' ----· 

uSJcm :l ~ . "' 

! 180- 1 ~-~ 

I I I. 16o I 

140 

120 

100-

External Standard Report 

=========================================================~=========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

LOOOO 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

frnin) [uS/cm*sj [ug/mL] 

-------l------l----------!----------1----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s} not found 

=========""=============::;:;:========================"'~""'"-'======-============ 

==~.,=========================:::=::-~=""==================="'--"'-'=="-===:::o::==,===:oo== 

Area Percent Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

InstrumentAICPil!M~rJlii-IO.I'}Hii1Si'49 AM IGG EP~~Qs'/tJNfW\!'f ~~8J~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

i i 

I I 

I I 

APPENDIX PAG!f~e402 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-470l.D 

Sample Name: P4 R2 Out B *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 47 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 2:48:12 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC20J.OQ3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed : 10/4/2010 9o33:01 AM by IGG 

r·····:~;~:-~ADCi··;.,:·ABcrcHANNELA(U:\HPLC201iio4\MRBURNSIDAfA\ocniif'[c53~G9;63847oHi)"····--··········--~--~ 

1801 I 1 I 

160 ·l i I 

1401 1 

120 ~ j 

' i 

100 -~ i oo~ I oo~ \ 

~LJ~~L . !)."'-~~) .l~~~c_. . --·--·--·-··----------~-- 4 6 8 ___________ ,1.9~--------- 12 mi 

===================================================================== 

External Standard Report 

=====================================================================· 

Sorted By 

Calib. Data Modified 

l-lul tiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

1. 0000 

9:32;52 AM 

Use !'-1ultj.plier & Dilution Factor with ISTDs 

Signal 1 o ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound ( s l not found 

"-'""""''================================================================== 

==============::::::===-:o:.'=-=:::,===~-========================-================"===== 

Area Percent Report 

=-·=:o"·""'================================================================= 

Sorted By Signal 

Calib. Data Modified 10/4/2010 9:32:52 AN 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AJ.TCl~fi§O:NJ>. ~~1~WQO AM IGG EP~Ij\~,ClflJ~·~e;f,m- ~8~~ AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~403 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4702.D 

Sample Name: P4 R2 Out B *10 0910-96 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 47 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 3:05:30 PM Inj 2 

Acq. Method C: \!!PLC201 OQ3 \MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPI~C2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG f ADC1 A, ADC1 CHANNEL A (U:\HPLC2010041MR-BURNSIDATAiOCT\HPLC53PG98\038-4702.D) -----------

1 uS/em l ~ 

I 1801 i 

I 160 -~ 

' J 

140 -:l 

120 -J 

100 ~ 

1 i 

BOi I ' i f 

::o

0

1i eel•"-- ' ' c:=~-~:··~,-~. -~-.J~------- _j --~:;:~~~:-:~:=;:-==;==;==;== J ' ' --r-------r-------..-·---.---·--r---,-----.,---;- - I ...,......----

L_ ____ ~2,__ _____ _c4"------~6'-. ____________ ...!!________________________ 10 ·-··· ------------~_2 _ ______m.i 

External Standard Report 

=========="''"'""==""=======-======================================-======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1; ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/em's] [ug/mL] 

-------r------:----------r----------r----------r--r------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated co:mpound(s) not found 

===============""================================================"'""'=== 

========~:===:-.:co::c==:c.:;==================================================== 

Area Percent Report 

============================================================·======='=-~= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1- 0000 

1.0000 

Use Multipli.er & Dilution Factor with ISTDs 

_1n/_40.010 q jjJ 6 EA#0910-96 Page77of202 lnstrumen t A;-C"PRaJECTWo. P-i 1421 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'!Sbe404 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4801.D 

Sample Name: PI R3 Out B *10 0910-96 BORAL BRICKS 

~==================================================================== 

Acq. Operator EO Seq. Line 48 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 3:22:48 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

.ADC1 ,;;:·ADC1 CHANNEL A (U:\HPLC20 1 004\MR BURNSID;:;A"'T7

A"IO"c"n'"H"P'"L'C'"S"'3"'PG=sa"l. 0"'3"9.-·4"B"'07

1."D"l ------; 

. I ~ 

l ~ j i 

160 I i ii 

140 ) j li 

' li 

I! 120 

100 

;I 

,, 

80 II 

I 

60 / II 

40 - J 

! 20- ~ ~ C» ~ I \ i 

l . -"'-

c---"··.52_ ~-~ .; ~---~ ,_.: r-::::::;:;:::;::::C:;·.~/ -- -- - 'c~--~---·-····-·-·"J o- -·-1------,------.-----T-· 1 -· .,.. -····'T" ,... ------r ••. .,. , -· c.,.. ---,--..........,---

------- --~-------···----'•'-------"6'------"e _____ __,1"o'------'1"'2 _ __!!m""'i 

External Standard Report 

============================-====================-·=======~-:.==,=======-==::.== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------j------l----------j----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

======================~..:o==-====~=======""'0:'""'""'""==""=-""========-==:--==-:""'"'"====--===~o:.==-

Area Percent Report 

====""'"'"'"o============================================================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

InstrumentAICf~P~~\HitJe- '9-Hi"IJI?26 AM IGG EPR~<i!IJ1g!l//3N~ P~BJ~ AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!'~e405 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4802.D 

Sample Name: P4 R3 Out B *10 0910-96 BORAL BRICKS 

===================~===========================~===================== 

Acq. Operator EO Seq. Line 48 

Acq. Instrument Mr_Burns Location 

Injection Date 10/2/2010 3:40:05 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

uS/em J 

180 J 

160 ..J ' 

140~ 

120~ 

100~ 

80 ~ 

60 1 

ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q41MR BURNSIDATA\OCTIHPLC53PG98\039-4802.D) -----·-· 

1 

I 

,, 

il 

II 

II 

II 

!I 

i il 

::~ ~ ! 5 ~ I \ ___ j 0 i"-.. --~-·-- r···--' -- -~------__]------,----·-·· ~---;--....l-- . ...-·---~----- __ .....-.J __ ../. .... • -~ _'-.,_...,~--- ., I 

'------~2___ _ ____ i_ ________________________ § _________________ .§_ _________________ ... .1.9 ________ , ____ ~ _ _1!11_ 

=================================-,==================================== 

External Standard Report 

===============================~=============:======================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9;32:52 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[ruin} [uS/cm*s] [ug/mL] 

-------;------l----------;----------[----------1--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

\'Jarning : Calibrated cornpound{s) not found 

===='"'='·::..-============================================================== 

=·======================='"'==~-:o·=='-""'"'=================~=:::===='""==:.=::-.::======= 

Area Percent Report 

====;:::=====""==="'<;::':==='"'""-=====""'=============================:::==:========:::= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

l. 0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

InstrumencAICfflfW~Qjjtlg. l>tl'!!'til?37 AM IGG EPRit!l&'t/,gs'l§N~'f P~O'J~ AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGj;~e406 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-490l.D 

Sample Name: P5 R1 In A *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Ana~ysis Method 

Last changed 

EO Seq. Line 49 

Mr Burns Location 

10/2/2010 3:57:55 PM Inj 1 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

(modified after loading) 

r

·------------AoCfA.ADC 1-CHANNEl-A (U:\H-P"LC201 o0~4;;.\M~R"'siiuf!R;';;N"S"'ID"'A"T"A'"IO"c"'T"I"H"'P.cLc"'5"3"'P"'G"'9'"al"'o"'•o'."'•9"0"1-co"') ____ _ 

~ I 1 uS/em -1 

' " I ! 180-j ' ! 1 ' 

I :J j r 1so --! · 

I 140~ I 1203 ' j . 1 

100 ~ ~ J "0 

. ~ 80 ~ u. 

' ~ sol ~ ~ 

•ol '" '"' I 

2: ktd\\'=·l"-~-r':::_:::,:":~i.: ... ,:c:.:::;:.:C:::;~---·._c.-,--r'-=-r-1~~-~-~~-~---1 L _____________ 2 __ ------------------4 6 _________ __@___ _____ _,___________ 10 

External Standard Report 

=============="""===::=:======================""'=============.,==========""== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:58:17 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--!------------------

3.126 BB 362.59586 1.70694e-2 6.18931 Fluoride 

4.262 BB 5.50164 3.7393Be-2 2.05727e-l Chloride 

Totals : 6.39504 

*** End of Report **~ 

Instrument: AfC:MOJIJ1'§~.N!I-19-J!\tJI?22 AM IGG EPJ\'~'MIJ,g§/@Nflm ~R6'Jiil9f AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

12 ml 

APPENDIX PAG['~e407 1 of 1 
Data File U:\HPLC<UlUQ4\MR BURNS\DATA\OCT\HPLCoJPG~e\U40-49U<.D 

Sample Name: P5 Rl In A *10 0910-96 

BORAL BRICKS 

=================c-.:=======================================--========-""=== 

Acq. Operator EO Seq. Line 49 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 4:10:15 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4!1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by lGG ------------ ADC1-A-:-ADC1 Cl-IANNETA(U:\HPLC201 oo-4\MR BURNS\DATA,6Cl\HPLC53PG9Bm40:4902.D) ----- ------··-·--------

uS/em 1 

180 -~ 

160 j 

140J 1 

120 i 

100~ ~ 

80~ ~ 

60j ~ J ~ ~ 40~ M u r::,":J l (·· ' ~.'2 . N ;\ ~ -~- CO ~ 20-:1 M I\ N 0<'b' ~ , . ..! N I\... # It) r-.: 

o .:~~--~~:-~:_t;__:~~~~--,---:=-~: ... , .. _:_::~r----,-__-::. __ ~=.-.=;:_~ - --=-.=-~-,----,----~-~----..-----.,----~----.,--

---~2 ------------4 ________ _§_ ____________ ~-----------------·--_1Q ___________________ j1 _______ rpj_ 

===================================================================== 

Sorted By 

calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area Amount Gr.p Name 

[min] [uS/cm*s} [ug/rnLJ 

-------l------l----------l----------l----------l--l------------------

3.127 VB 365.51782 1.70697e-2 6.23926 Fluoride 

4.262 ~"~ 5.41333 3.75752e-2 2.03407e-l Chloride 

Totals : 6.44267 

*** End of Report *** 

IGG EA# 0910-96 Page 81 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGif\i!\!e408 l of l 
Data File U;\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-500l.D 

Sample Name: PS R2 In A *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

J ... ast changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 4:22:35 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\HETHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

(modified after loading} 

50 

1 

r-· --ADC1 A~Ai5C1CHANNEL A(U:IHPLC201D64iM.RiiTJR.NSIDATA\OCTIHPLC53f'698\041~55o1.D) -------, 

! uS/em-~ 

180..:) 

:::11 

120 .,..... 

"' 100-3 ;;; 

j I 

ao -1 I, 

l ,, ~ 

60 . ,! \

1 

:g l 1· ~ 

l I I () I 40. I : ' ill I 

·1 l(J \~ ;z (<) q r 

2: br&~k~~~~.:!~j~::~?: --,_~·- -~·~:~~) ~;~~----=·-·:~- ~;j=~ m;~ =======================================================~~============ 

External Standard Report 

===========================================,.,~.,.======================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:58:25 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Sj.gnal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area ~nt/Area Amount Grp Name 

(min] [uS/cm*s] [ug/mL] 

-------l------!----------r----------l----------1--!------------------

3.151 BV 937.34271 1.70860e-2 16.01546 Fluoride 

4.265 VB 28.33126 2.84328e-2 8.05538e-l Chloride 

Totals : 16.82100 

==================================================-'===o:·================-

*** End of Report *** 

Instrument AfC:WP!JJll!~:tJ9- f9-l~\ll?4 5 AM IGG EPJi'~i¥tlr§s'/BN~ ~~6'jli\9f AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e409 1 of 1 
Oa ta Hle U: \H>' l,CLU lU\14 \MR BURNS\DATA \OCT\HPLC53PG98 \041-5002. D 

Sample Name: P5 R2 In A *10 0910-96 

BORAL BRICKS 

================================================:==================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Metl;od 

Last changed 

Ana_lysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 4:34:54 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

O:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

{modified after loading) 

50 

2 

j:::~---ADCfA, AOCfCHANNEL A(D \HPLC201004\MR BURNS\DAl'A\OCf\HPLCs3P~9a\o41-s062 D} 

I 180 , 

I 160 • I j ~ 

! 140-l g , u: 

External Standard Report 

=====================-=-======================""'============="'-·-========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:58:25 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s} [ug/rnL} 

-------i------l----------l----------i----------1--l------------------

3.150 VV 935.54138 1.70860e-2 15.98466 Fluoride 

4.265 VB 28.56014 2.84155e-2 8.11552e-1 Chloride 

Totals : 16.79621 

===========================""""·=""=""-=======:c..-=o=:==:c"================"""-""~"== 

*** End of Report *** 

JO/ i/?010 q .SA 5 EA#0910-96 Page83of202 Instrument Atc"PRcfJECTNo. P-'10f42 4 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAc£'tlh"410 1 of 1 
Data File O:\HPLC2010Q4\MR BORNS\DATA\OCT\HPLC53PG98\042-510l.D 

Sample Name: P5 R3 In A *10 0910-96 BORALBRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 51 

Acq. Instrument Mr_Burns Location 

Injecti.on Date 10/2/2010 4:47:14 PI~ Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by IGG 

--------ADcT.(-AOCTCHANNEL A {LiiHPtJ:2o10Q4\MRBURNS\DAT A\OCT\HPL-C53PG98\042-s1 01.0) 

uS/em ·1 

' 

====================================================''""-"'=="==========""== 

External Standard Report 

============================================================~===~==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl Ar ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount G~p Name 

[min] [uS/cm*sj [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.158 MM 1155.25562 1.70880e-2 19.74100 Fluoride 

4.265 MM 41.25723 2.77563e-2 1.14515 Chloride 

Totals : 20.88615 

=-======================================================o======:.,c:;;:.·,.-..-,~,,...:oo-.""'=-o"" 

*** End of Report *** 

InstrumentAICflj!_P~~£ol"l9 FJ:~q1,fg: 25 AM IGGEPA=MR~§~NPrw'f ~1\&JEi!W AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

···-··-·------------~ 

i 

APPENDIX PAGip~e411 1 of 1 
Data Fi~e U:\HPLC201UQ4\MR BURNS\DATA\OCT\HPLC~oPG9e\U4Z-~l02.D 

Sample Name: PS R3 In A *10 0910-96 

BORAL BRICKS 

=:=.======:;===================================::o==:= ===================== 

Acq. Operator EO Seq. Line 51 

Acq. Instrument Mr Burns J_,ocation 

Injection Date 10/2/2010 4:59:35 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Ana 1ysi s Method 0: \HPLC20 1 0Q3 \MR BURNS\METHODS \HPJ"C53PG98. M 

Last changed 10/4/2010 9:39:38 AM by IGG 

----ADC1 ;;;;·ADC1 CHANNEL A {U:\HPLC2010Q4\MR BORNS\DATA\OCT\HPLCS3Pi398\o4·2:sio2:-D)-·· 

uS/em j 

180 ~ 

160 ~ 1 

::ll !\ 

'· :[ so~ ! I ~ 

6oJ I i ·g j !! t5 a,.'b 

40 -~ \ '*'ep<b 

J \ ID "<tO 1.0 

20 j re 1

· .. ~ ,e;'l> !;;t;::: t---

~ N ' \ ..... , ~ u:il.ci ,...: j I 

---~-~-·~--~~-. ----~-~- --:~-~~--t-=-1~:~~ --~~-----~=~~~~~~----·~r~·-=·=~~~=--,-----·~r;---~~~~~ 

====================~=====~~~======================================== 

External Standard Report 

===========o============================"''-==~===============""·=========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/em's) [ug/mL] 

-------l------l----------l----------l----------1--l------------------

3. 121 

4.265 MM 40.98282 2.77662e-2 1.13794 

Fluoride 

Chloride 

Totals ; 1.13794 

1 Warnings or Errors 

Warning : Calibrated compound ( s) not found 

==================================================================~== 

*** End of Report *** 

IGG EA# 0910-96 Page 85 of202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~~ge412 l of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1001.D 

Sample Name: P5 R2 In A *20 0910-96 BORALBRICKS 

====~==========================================================~~==== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 5:39:47 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \ HPLC20 1 OQ3 \MR BURNS\METHODS \HPLC53PG10 0. f1 

10/5/2010 9:18:49 AM by IGG 

10 

1 

(modified after loading) ~-----;tiliC1A.A1fCTCHANNECA-(O:\HPLC2o10d4\MR-BURNs\DAfA\ocnHPLC53PG1-60\(Y6s-1oD1.Dr ------··------------~ 

uS/em l 

i 

180 ~ ~ 

160 ~ 

J 

140 -4 

1 

120-1 ~ ~ 1001 ~ 

80 CJ ~ 

,1·! ~ ~ ,~ 60- ('<') ~ 

40~ f\\ 0 B 8 I 

2: 1.:_::::_:; '-~-.==:.-"L;"rL =-:-J . ·-·~::;:·: __ ~ __ :_:;-- . .Y~=::::_, -'-=--;---==;:==::;:.:! ___ ----- L ____ ····-··--·--·- 2 _____________ :!_------------··--·---~- ·--~---·--- __ !I!i 

==================,.,=====:::====""==-=''"""''='"'"'~====""==========="-"===""'===:o-.•'"'"''=="" 

External Standard Report 

=================================~=========================:========= 

Sorted By 

Calib. Data l"iodified 

Multiplier 

Dilution 

Signal 

10/5/2010 9:21:11 AH 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------!------1---------- l----------l----------j--j------------------

3.138 BV 508.88586 1.71526e-2 8.72872 Fluoride 

4.252 BB 14.43764 3.07776e-2 4.44356e-1 Chloride 

Totals : 9.17308 

==============-..---====:======O".o==~~-==-~==-~=:=="'-'==:·""~-~=====.,===c~::o":=;..-:""===::-;======:::-o= 

*** End of Report *** 

Instrument AJ:Cfljlp,lfl>lit\9· l/r!~;p?l4 AM IGG EP~fu'kllJI.lt\hJ/IiNfim ~~&!E\91< AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e413 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1002.D 

Sample Name: P5 R2 In A *20 0910-96 

BORAL BRICKS 

=========~=========================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 5:52:07 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:19 AM by IGG 

10 

2 

(modified after loading) .--... -Al)cT.("/(5-cTCHANNEL A (lEHP[C201 oo4\;:,M;;,R:;,B;cU~R!.,N"SI'"D"'A"'T A"'l"o"cn"'HPlcs3PGf60\009-1 00-i.D) ----- . ~--------~ 

uS/em l 

180 

160-

140 

100 ---i 

80~ ~ 

<0 

i 

___ ) .• , ·- __ "_J .. --~~-~· -,-----·-·-·-

---,-----~--------,---..,.------ -.------

6'----------"-8.. mi 

External Standard Report 

======"===========================================c:c-===e=============="'-" 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/5/2010 

1. 0000 

1.0000 

9:21:11 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/mL] 

-------;------l----------l----------l----------l--l------------------

3.137 BV 506.10544 1.71527e-2 8.68108 Fluoride 

4.251 BB 15.11480 3.059l7e-2 4.63306e-1 Chloride 

Totals : 9.14439 

====================================~==============~~~================ 

*** End of Report *** 

EA# 0910-96 Page 87 of 202 Instrument ATc~&f"ejl~Q. P'-liff4222 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~<Nile414 1 of 1 
Data File U;\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-110l.D 

Sample Name; PS R3 In A *20 0910-96 

BORAL BRICKS 

======~==========================~========~========================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 6:04:27 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/l/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

11 

1 

r

-·-·····-···----ADCTA,A6c1 CHANNEL A (U\HPLC2010Q4\MR 8URNS\DATA\OCT\HPLC-53P(fi50\0TO:,-,-iffl5f- -- -- ---------_.!1 

uS/em ~ 

I 1soi 1 

' 160-1 I ~ I 1 I 140 -~ 

120 -=i 

j 100. 

====================""'============:======,==================="=========.:::= 

External Standard Report 

==================o:===·================================================ 

Sorted By 

Calib. Data Modified 

Signal 

10/5/2010 

1. 0000 

9:21:11 AM 

Multiplier 

Dilution 

Use Multiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal l; ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s) [ug/mLJ 

-------l------l----------l----------l----------l--l------------------

3.142 BB 639.42731 1.71486e-2 10.96531 Fluoride 

4.251 BB 23.24886 2.9269le-2 6.80473e-1 Chloride 

Totals : 11.64579 

========:o::==============""-"'~=='·"==============-"''"-'=====,================== 

*** End of Report *** 

Instrument Alrclffi'oJEl:JT:!r% il'm4229 AM IGG EP~~~Ro~~g;~~J'-i'Jlir p~g~m AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~415 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1102.D 

Sample Name: P5 R3 In A *20 0910-96 BORAL BRICKS 

===========================::======================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 6:16:46 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

. 10/5/2010 9:18:49 AM by IGG 

{modified after loading) 

11 

2 

f------------------A6C1 A, ADC1 CHANNEL A (U:\HPLC201004\MR BURNS\5AfA\6Ct\HPlC53-PG100\010-1162.5} _______ ---------------

1 

I 

I 

' 

I '

i 

uS/em] 

1801 

160 cj 

1 

140 l 

1201 

100 -=l 

~ 80 ~ 

60~ ' 

i 

~~-

=================="'-'====·===========================.,.-.-~=::.~=============== 

External Standard Report 

~z==============·==~~======:==============================:.-,:==:::t'========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/5/2010 9:21:11 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.]74 BB 645.62323 1.71485e-2 11.07147 Fluoride 

4.287 BB 23.89014 2.92027e-2 6.97657e-l Chloride 

Totals : 11.76913 

=:=========""' ====.,-..::"' ""="""-~''-"=:;.:, = == ==o:o==== = = =--===-==== "-"C-~"" === =====-============= 

~~* End of Report *** 

I GG EP~~~IIlSIIlN~ ~~~<9jil\l)i1 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!'~e416 l of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5201.D 

Sample Name: P5 R1 Out A '10 0910-96 BORAL BRICKS 

============================================~====~=====~============= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 5:11:54 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

{modified after loading) 

52 

1 

--~A'-D'-C'-1-A: ADCiCl·lANNELI\(U:\HPLC2010Q4\MRBURNSID''A"T"'A'-IO"C"TI'"H"-P50L7c"s"3"'PG"9"'a>c\0"-4"3co·S'"2"o'1."D') -----~~---· 

uS/em] 

180 j 

160 ~ 

140 .j 

~ 

120 ~ 

j 

100 "i 

80-l ~ !D 

eaj· ~ ~ 40- ' 0 

(!) ;_jl.l') ~ a) ,... Ol J 

20 ~ ~~ ~ ~ ~ ~ ! I 1--A-..! ~~,..--~~ ~ "!' --- I~ ----- _, -.-!:'"~-,.- --- --~- __ / 

! ____________ ~------=r=~--=~==r-~-==-=--:·----r -=-~-~~~=i·-~~~--~ ... · __ ~ __ ~_~_-_-,'o--~-~-,,2-~m_,i 

=======,============<==;;===·=""·==,·==============================0'='=.,===== 

External Standard Report 

""""===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:58:25 AM 

l. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s) [ug/mL] 

-------!------l----------l----------l----------l--1------------------

3-121 BV 44.45597 1.68759e-2 7.50236e-1 Fluoride 

4.260 BV 3.20621 3.78526e-2 1.21364e-1 Chloride 

Totals : 8. 71600e-l 

==============================~"'=·""'===''""""'===:.======================.~=~"==•>'= 

*** End of Report *** 

Instrument ATCRRO!J)"Illli:NO. 8.-(leOO: 05 AM IGGEp)\'~fl!/J;g?lj1j~ft%'1-~~8)~ 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~~e417 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5202.D 

Sample Name: P5 Rl Out A *10 0910-96 BORAL BRICKS 

============================~======================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 5:24:14 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2 01 OQ3 \MR BURNS\METHODS \HPI,C53PG98. M 

10/4/2010 9:58:17 AM by IGG 

52 

2 

(modi~ i ed __ af t:_~~-~~.9}39 ) ____________________ _ :----ccA~D~C~1 7

A-. A,-DnC"1""CT;He;:A-c,N~N;;;EL A (U•IHPLC201 OQ4\MR BURNS\DA TA\OCT\HPLC53PG98\043""'-5~2"'02'.nD)~-· 

' 

I uS/cml 

180. 

160 

140 

120 .. 

100 

80 

==============================="""'-'==>=-==,.~============================== 

External Standard Report 

================================================='="·'-"'"-.,================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

10/4/2010 9:58:25 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

Ret?irne Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------i------l----------l----------l----------l--l------------------

3.122 BV 41.62362 1.68609e-2 7.01813e-l Fluoride 

4.258 BV 2.51682 3.78526e-2 9.52680e-2 Chloride 

Totals : 7.9708le-l 

=""="""'=============-="''==-===--"====""""=""=====<><=,============================ 

*** End of Report 

rnstrumentAic~eClll>J6 F!-aJU1~g: 14 AM IGGEp.ff?ik~~1£sW3NY~§'f~~d'M:o/ 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIPillqB418 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG98\044-5701.D 

Sample Name: P5 R2 Out A *10 0910-96 

BORAL BRICKS 

===========================-=====:o=c=========""==========""======""===""'==== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:15:12 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC20lOQ3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

(modified after loading) 

57 

1 

r·· ------··7ii:5cfA:-A·oc1cHANNEL A (U:\HPLC2010Q4\MR BURNSiDATAIOCT\l'iPLCSSPG98\644-5701.D) 

uSIGm] 

I 180~ 

' 160 -~ 

1 

140~ 

120 j 

100. 

80· 

" 60 " " ·co 

0 " 

"" " 0 

u:: ,., 40-- 0 

==========""'====;-:,-·=========""=========================""'===·~"============= 

External Standard Report 

=·""'"=""======================""==========='""-=============,================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:58:25 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s) [ug/mL) 

-------I------!----------J----------J----------J--I------------------

3.125 BV 48.65992 1.68950e-2 8.22109e-l Fluoride 

4.262 BV 3.04968 3.78526e-2 1.15438e-l Chloride 

Totals : 9.37547e-l 

<::= ======="'='""' =<==·="'~--,o=.= = ""'====== ========== ===================:: =:::= =; = === ==== =~~ 

~'* End of Report *** 

Instrument AlrclRlmlWI":Nl>. ~11 oOO: 25 AM I GG EPfi"!RO~J~~-JlBJ'fl!l;'t ~~8\~8f AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE"""'419 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5702.D 

Sample Name: P5 R2 Out A * 10 0910-96 BORAL BRICKS 

============""===============================-'='================::::==~===== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:27:32 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHOD.S\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

{modified after loading) 

57 

2 

~-------ADCTA. ADC1 CHANNEL A (U:IHPLC2oi0041MR BUR-NSIDATA\OCnHPLC53PG98\044-5702.D) --·--·-·------l 

! uS/em~ • i i 180 i 

I 160 · ~ 

Il

l ::: 

100-

80 

I i ~ 60~ ~ 

40.:.! I ., 

-f o ~~ Nf'-. (Xi m 201 ~ ~~:":! ~ ~ '<1: r-. 

j__ __ .J ~- r __ _____tL_.;g____--,.......l • .::!:.f '!. ·! 10 -~ ~- I 0 --l--- T-·····---,--..,..-------,---·-.------"r-

/ 

:;=c:::;:=:;::::::;-=::::..,.._, __ --. _____ -,----------,-----l----·-r··------ L __ _ 2 _____ ±___ ______ _ §. 8 __ J_Q _______________ _!? _____ .mL_ 

~=====================================================~~============= 

External Standard Report 

=================================================~=================== 

Sorted By 

Cal.ib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:58:25 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with !STDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s) [ug/mL) 

-------!------l----------l----------l----------l--i------------------

3.125 BV 49.63752 1.68990e-2 8.38823e-l Fluoride 

4.262 BV 3.03725 3.78526e-2 l.l4967e-1 Chloride 

Totals : 9.53790e-l 

=""============""-="·~===========~"'-======================~""-"''""'===========co=:/.~-oooo= 

*** End of Report *** 

ATC PROJECT No. P-10142 

Instrument 1 10/4/2010 10:00:35 AM EP£1\I,!Il~%S!WJ fl'§ge 00CO\E:ID2 AB~USTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 420 

Page 1 of 1 
( 

........... ~ .............. v. \.U-'...<.1'--.C.V.S.V\i":t 

Sample Name: 

\l"ll'\ DUI'\i~.:> \Ui'iJ.h\VO......! \tlt'.LO.......:::l.Jt'G~ti \V':I~-:.~U1. D 

PS R3 Out A '10 0910-96 

BORAL BRICKS 

============;==============================================~========= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:39:51 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:58:17 AM by IGG 

(modified after: loading) 

58 

1 

r----·---~--ADC1 A. ADC1 CHANNEL A (U:\HPCC201004\MR -BO"RNS\DAT A\OCT\HPLC53P~98\b45-5801~0) ____ ----~ 

I ~~ 

· 1ao 

I 

I 

160 

140 

120 .j 

100~ 1 

sol ~ 60-:J ·g I ff. 

1

1,1 401 1 <D ~co o N 

20-=! 10 a> --:;;; <D :,; eo "¢" i 

• 

I 

'" - V.~ r·'-..:!.1----::--f--"'.?....._-···.----'···~ ---..- _________ j 

I 0 J_I_-----·--r-'_-~.:::_,- , .. ---_ ·'"': ____ ., ___ ·_ - "! ~ ~ -.--T-~~----.......----

L-. _____________ 2___________ 

' ---··,-----.---...--~--.,.....--j 

4 6 __________ _____!! ________ _,1'-'0'------------------E-_miri 

======================"'"================~"=====================o::::======= 

External Standard Report 

~=======================================~=============~============== 

Sor:ted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4(2010 

1.0000 

1.0000 

9:58:25 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Ar:ea Amt/Area &~ount Grp Name 

[min] [uS/cm*sJ [ug/rnLJ 

-------l------l----------l----------l----------1--l------------------

3.123 BV 

4.260 BV 

Totals : 

45.96114 l.68832e-2 7.75969e-1 

3.00710 3.78526e-2 l.13826e-1 

8.89795e-l 

Fluoride 

Chlor:ide 

"'o-"'==•==~o:=~:--'==============""-=~-==============""'""'"'=========-='~'==========-==== 

*** End of Repor:t *** 

Instrument A;-cWJ.ktHWo ~-go~.iJ1' 48 AM IGG EA# 0910-96 Page 94 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA<Jfo'tlli' 421 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5802.D 

Sample Name: PS R3 Out A *10 0910-96 BORALBRICKS 

===============·-====================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:52:11 PM Inj 

C: \HPLC2010Q3\MR BURNS\Mt:THODS\,JETROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98. M 

10/4/2010 9;58:17 AM by IGG 

(modified after loading} 

58 

2 

=========================""-=::...-=.,:.~====================================== 

External Standard Report 

=========================================-,=-=========================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:58:25 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------\----------l----------l--1------------------

3.123 BV 45.52016 1.688lle-2 7.68430e-1 Fluoride 

4.260 BV 3.13018 3.78526e-2 1.18485e-1 Chloride 

Tot~als : 8.86915e-l 

""================================""'"·=:.=,=·=~:=""====""======================= 

*** End of ~eport *** 

Instrument AjfClftR4J,EM:NJl.IJ'1JQW: 57 AM IGG EP!i:fd/l!lJi9;-~5J'~~8~~ AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~ 422 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-590l.D 

Sample Name; P5 Rl In B *10 0910-96 BORALBRICKS 

==========~================~===~==~=======================~========== 

Acq. Operator EO Seq. Line 59 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 8:03:59 PM Inj 1 

Acq. Method C:\HPLC201DQ3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Ana 1 ysi s Method U: \HPLC2 0 10Q3\MR BURNS \METHODS\HPLC53PG98CL. M 

Last changed 10/4/2010 9:33:01 AM by IGG · 

. ·---ADC 1 A, ADC1CHANNE.CA (U:\HPCC201004\MR BURNS\DAT"~A~\O~C~n~H~P~L~C~5~3~PG=98~\.0~4~6~-5~9 0~1.~D-) ----'---~ 

uS/em J i ~ 

1801 I 1 

160 ~ I 

140 ~ i 

120~ I 

' 

1:: l 

60~ ~ 

~1 j I V 0:0 1'- t-- I 

1 2o i ~ ~ ~ ~ 0 \ 

I_----~~--~~~->"~~: ~--:---'=~-=~ i~~-~J ,C_ -=-~:~~~-~-L 1~~----·-· ---,--~;·-·--·~m: 

===============,:;=,===,==============================""===.,·==,.=====""===""'= 

External Standard Report 

================"""============="-'===,=====================:::::::============ 

Sorted By 

Calib. Data t1odified 

Multiplier 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [,ug/rnLJ 

-------l------j----------l----------l----------l--l------------------

4.156 Chloride 

Totals ; 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=======·==·===~'-'::======="'='"""=""============================================ 

========================================~"===·"=""=:==·"""================== 

Area Percent Report 

-""======""'·==:c~-=:==,.,===~-::=,,_,.=~===========================""======""="'""'-======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument AJ.TC11(j}(!Jf;M1ttP- ~(!9~2: 40 AM IGG E~~fM\~tffml'r~8~?8i! AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp'~ 423 1 0 f 2 
UdLct rl~e U:\tl~L~'U1UU4\MH HURNS\OATA\OCT\HPLC53PG98\046-5902.D 

Sample Name: P5 Rl In B '10 0910-96 

BORAL BRICKS 

=======~============================================================= 

Acq. Operator EO Seq. Line 59 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 8:21:17 PM Inj 2 

Acq. Met hod C: \HPLC2 01 OQ3 \MR BURNS \METHODS \METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

r-· ADC1 A, ADC1 CHAN'NELA(li,IHPLC201004\MR BURNSIDATJ\16cnHP[CS3PG981046-5902.D) 

I uS/em~ 180 

160 

~ 

====================================================~================ 

External Standard Report 

=================::o-==========o::-·======================================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1. oooo 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount G=p Name 

[min) [uS/em's) [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=================c""=========~'::.~============o..~o;o:;:o:===========.::::::============"" 

"""-"'-=================,.:=e~=============:o.o=""=======:=<:================·"'======~ 

Area Percent Report 

=====o:==,--"=~================,.-:.='='========"'-·================""========,====== 

Sorted By 

CaJ. .ib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

- EA# 0910-96 Page 97 of 202 lGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~~424 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6001.D 

Sample Name: P5 R2 In B *10 0910-96 BORALBRICKS 

==========:==================================================<=<=~·==·=== 

Acq. Operator EO Seq. Line 60 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 8:38:36 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3 \MR BURNS\METHODS\HPLC53PG98Cl •. M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A, ADC1 CHAffNELA (U\HPLc2o1iii:l41MR.BURNS\DATAIOCnHPLC53i'G981647~6il6H5j- ----. - --, 

uS/em 1 

180 

160 

140-

120 

100 

40 

20- ~ ~ ~ ~ ~ i 

~ ~ ~ ~ ~ I N ~ ~ ~ ~ j 

i 

i 

\ 

' 

\ ... _ 

0 JI----·-··T·----1-'--"--T~_c•~-.-----Tr_·_-_-_~_-_-T·_·.'-rCC'CC'CC'_-,=---___J -.--·------·-·-" ....-/ -1 ----,--.--.-,.--r----r-·--r·-------,----,---·-·r ········- . . ----,- -.---- 2 -- _1_ ___________ ,,,., ______ ____§_ _________________ IL_ ______________ l~-------·-_____:!l ______ ITI.t. 

==========;:,===~===================================================:=.== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCI A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/crn*s) [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 t-Jarnings or Errors 

Warning : Calibrated compound(s) not found 

================================================================='""==== 

===::::========================~~""=""~-,·===,;;=;;=======.,.=========:====:========= 

Area Percent Report 

==============:=:=="-'=~.,====c==~=============================~============= 

Sorted By Signal 

Calib. Data Modified 10/4/2010 9:32:52 At1 

Multiplier 1.0000 

Dilution 1.0000 

Use r-:Jultiplier & Dilution Factor with ISTDs 

ATC PROJECT No. P-1 0142 EPl'tl\lJl<f9>116l96Nff;!i@J 98<01120l2 Instrument 1 10/ 4 /Z010 lO:OZ:0 1 AM t-'i!f;usTAPLANTS4&5,SALISBURYPLANT6 

APPENDIX PAGE No. 425 

Page 1 of 2 

SEPTEMBER 2010 
Data File U:\HPLC20IOQ4\MR BURNS\DATA\OCT\HPLC53PG98\047-6002.D 

Sample Name: PS R2 In B *10 0910-96 BORALBRICKS 

=======""===•:;:;========================================================= 

Acq. Operator EO Seq. Line 60 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 8:55:53 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q41MRBURNSIDATMOCT\HPCCS3PG98\047·6002D) 

======================================·""=====================,==.::====== External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Moditied 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A1 ADCl CHANNEl, A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s) [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

._,,,_~====='~""==,==»·==~~'''"====~==-=~=============<=o========================= 

=::oo.-.,========""~==""==~"'-"""""-""'"'-'==========""====================-=::::::o:::o==-======== 

Area Percent Report 

======================================'-"'==="'"·'~===========::.:===""·'"''·""======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument ATCffi0!1)'2!n"~. llOGW: 10 AM IGGEPJI'~<¥J.li\~~f3rJ'ft!I/T~~8J~ 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PAGp<l'\j>e426 1 of 2 
Data File U:\HPLC201DQ4\MR BURNS\DATA\OCT\HPLC53PG98\048-6101.D 

Sample Name: PS R3 In B *10 0910-96 BORAL BRICKS 

================~========~=========================================== 

Acq. Operator EO Seq. Line 61 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 9:13:11 PM Inj 1 

Acq. Method C: \HPLC2010Q3 \MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/~/2010 9:33:01 AM by IGG ----···-·-~--A5C1A,A6c1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DA"fA\bCT\HPLCtr3PG98\Ci48~10fj)f -------------

;! 

~ 

External Standard Report 

=============~===============================================·======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/mLJ 

-------l------l----------l----------j----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=====================================,::=================="""'''""·'=~======= 

Area Percent Report 

======================o·~==-::=:==:o~==============================·"-'==.--======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument Atc~J<'~qJ J,J0. IL~o~: 21 AM I GG EPI¥itR 11~Ps~ib.ff'~gT WRo5~~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE~e427 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG98\048-6102.D 

Sample Name: PS R3 In B '10 0910-96 BORAL BRICKS 

Acq. Operator EO Seq. Line 61 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 9;30:29 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U;\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

~--~~:::·i ADC1 A, ADCi CHANNEL A (U:IHPLC2010Q4\MR BURNS\bl\f/i\()CTIHPLCSJ.PG9~,!648.:5i"ii2'.D") _________ l 

! 160 -~ 

140 ·~ 

120 ~ ., 100 ~ 

j M~ I 

.

i,. ,,1 

I 60 ..:1 

' 

I

' •o~ I 

---~;:t~=;~~=-:l~~ _ ~ :. : __ -_,::t<e ~--~ _::_ -· ~-'=~~~-:r··-··=~=~-=~~~=::-:·~=--=-';,_:_~: J 

=============:::,========-======,::::======================================== 

External Standard Report 

"-"''"'='"'"'·===c·.o========""==""'="'~=:::~,;:===,..,======================================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

l. 0000 

1.0000 

9:32:52 AM 

Use I'-1ultiplier & Dilution F'actor with IS'I'Ds 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------1------1----------l----------l----------1--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated cornpound(s) not found 

======""==="=''-"'"-"===~''""0::"""-'-'==,=~~="'-'"'-~~-""''~""-====::::=""=======""==""=================::=o== 

==============================================~===""===~~============= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Area Percent Report 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

InstrumentAICRWl!Jg~lJW. fh'lQtl!2: 32 At-1 IGGEM(!~@~\k~jbtfi'E~§'r1~o9bEH2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~<Nge428 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6201,D 

Sample Name: P5 R1 out 8 *10 0910-96 BORALBRICKS 

=~=================================================================== 

Acq. Operator EO Seq. Line 62 

Acq. Instrument Mr Burns Locat.ion 

Injection Date 10(2(2010 9:47:47 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q4\MR BURNSIDATAIOCTIHPLC53PG981049·6201.D) 

uS/em l 

180 -~ 

160 .j 

;::_1 

1001 

80·~ . 

l I w~ . 

~~ I 

2: l-• } T--:L §_ ~-·-" ~ -,----, ---~ § -~-;--·-,-··--~ .J . ~----~2,_ ___ , _________ i. ...... ,_ .. __ , ____ _§ __________ , 8 

~ 

i 

I 

I 

\ ' 

\ ! ~---------,---' 

I ! 

10 12 

============~,==,~==========:-.::c=:::'""======,======"""'=""='""·~==============="'-~==== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 

9:32:52 AM 

Multiplier 

Dilution 

Use Multiplier & 

l. 0000 

Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/crn*s] [ug(rn.L] 

-------l------l----------j----------l----------l .... i---------.. -------- 4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

-='==:=·=""=============================================""""==,============= 

=""'=============="'-"=~=============·======= ..,============================= 

Area Percent Report 

=========,=::.-o~·-"':.e:.=c"'============"-~=========""=~"'""~="''=====o::·~=~~-"'="'-===~==~'·""-===~~:-..:=c-.:: 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10(4/2010 9:32:52 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

mid 

Instrument AfCffiO!J)"§(!':NJ>.f!'()g'IJIJ: 42 AM IGGE~J{i~i!li\:;~fb,ij'fEJST ~\ot</2 AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~429 1 of 2 
Data File U:\HPLC2010Q4\MR BORNS\DATA\OCT\HPLC53PG98\049-6202.D 

Sample Name: P5 R1 out B *10 0910-96 

BORAL BRICKS 

=================================================================""=== 

Acq. Operator EO Seq. Line 62 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 10:05:05 PH Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/l/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

uS/em ~ a 

1

--- ---··- -~7\6¢1 A. ADC1CHANNEL -A-([}\Hf''Lc'201 DQ4\MR BURNS\DATA\OCTIHP[C53PG9B\049:fi2o2:t5) . -----· .. -·----

. 1801 i"' 

! 160 ~ 

t 140 -ll 1 

I 

120~ 

100 _:l 

80 

==============================================================~=~~=== 

External Standard Report 

=============================================~=~===================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multipli.er & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area AmL/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

VJarning : Calibrated compound ( s) not .found 

===;;o==============c===::;:.-c.:::======================""~=:::;:'-"'================"'-='==== 

====:==============================o=:=================:~:::=============== 

Area Percent Report 

==================~"=c.,-;===============·""'="'-"=""'========================-~=== 

Sorted By Signal 

Calib. Data Modified l0/4/2010 9:32:52 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

EA# 091 0·96 Page 103 of 202 

IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEiffil! 430 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6301.D 

Sample Name: PS R2 Out B *10 0910-96 BORALBRICKS 

====:o=============================================;:====================== 

Acq. Operator EO Seq. Line 63 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 10:22:23 PM Inj 1 

Acq. Method C: \HPLC2 010Q3 \MR BURNS\METHODS \METROHM. M 

Last changed 4/1/2010 4:15:.36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

uS/em l ADC1 A. ADC1 cHANNECA {U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PIG98:S0-6361 D) -- - -- -1 

180~ 1 

I ! 

160 

140 

.. I 

~ L=-=-.. ~-,..=: t-'T- ~-!:.:c.::;=:::;:==:'..:,~::.-e.::;=::;==;=~-=~='-}~~ ::.; .. ~~~------~--~~ 

120 

100 

....... _____ 2__ -···-······----1. 6 8 ..•...•.... --hl __________ ___J_;'~_mirt 

===================================================================== 

External Standard Report 

==========~=====================~==================================== 

Sorted By 

Calib. Data Modified 

Signal 

10/4/2010 

1.0000 

9:32:52 AM 

Multiplier 

Dilution 

Use Multiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/rc.L] 

-------j------j----------l----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warrtings or Errors 

Warning ~ Calibrated compound(.s) not found 

===""=====""""~~~=·~===============:oo:=-:=:.""=~·~c..oo"''""""='""=========================== 

Area Percent Report 

=============,"'=--'='==============================""====··"""""-'================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:32:52 AM 

Use Multiplier & Dilution Factor with ISTDs 

ATC PROJECT No. P-10142 E~fl>!>@~"f{lll)d£1all2 

Instrument 1 10/4/2° 10 10:03:0G 1\M j,_'6\jiuSTAPlANTS4&5,SAUSBURYPlANT6 

SEPTEMBER 2010 

APPENDIX PAGE No. 431 

Page 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6302.D 

sample Name: P5 R2 Out B *10 0910-96 BORAL BRICKS 

=======================================================~~============ 

Acq. Operator EO Seq. Line 63 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 10:39:41 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\"1ETROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG 

------------·---···AciC-rA-:-A5c1-CHANNEL A (U:\HPLC2010Q4\MR BURNS-.i\D'CA"T"A"Io"c"n"'HPLC53PG98\6S0-6302.b)---------------

uS/cm -~ I ~ 

1MJ I , 

;:: Ji IIi I 

120 ~ 

3 100--1 

j ,1 

80 ~ 

I 

M1 I 

40 ~ ' i , I 

2

: h=_ 2~_= __ :,. __ c::_= __ :::; __ ::. __ = ___ ~ __ =_"_c;:L=_=;=:;:::c::;:::.....,=6;::::::::;::::'::·! :.·~-~e~:= · ~;c ·· 1~\';-=- · · -~l~ ~d "' "' "' 

I 

"' 0 N 

N ci "'r 

L ___ _ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

.. 

"' .. r··- ~~ 

-External Standard Report 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Atllount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=========================="='=====~c:c:·.o-~=================::o:==·;.:o============= 

=""' ~ "-'"-=·"" .0::"-~e::- --- ="-"~=,-~=============-=~='-"'============================""=""= 

Area Pe:rcent Report 

====================,..-"==·""========================~===,..~=.:.============== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument ATC:MO!Jtt()'Wl. 11-ll OOO!: 15 AM I GG EM~,.O~~?s~?o~f~~TW~o~\&:if AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE<Npe432 1 of 2 
\ 

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6401.D 

Sample Name: P5 R3 ol.lt B *10 0910-96 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 64 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 10:56:59 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2 01 OQ3 \MR BURNS\METHODS \ HPLC5 3PG98CI,. M 

Last changed : 10/4/2010 9:33:01 AM by IGG 

r -- ---l- AocrA:-ADCTCHANNEL A (U:\HPLC2010041MR BURNSIDATAIOCT\HPLCS3PG98\051-6401.D) 

! uS/em ;;5 

! 1W ~1-

160 ' 

140 i 

120 _:j 

·I 

100~ 

-----~ 

i 

l 

80-1 

M~ I 11,1 

4o~ I 

2oj ~ § &1 ~ \. I 

o .:1'==;2-:c=N=,...~=:;:'C:_-=, __ ::. __"'~~=i;.: __ = __ =·-~---=-~ ... ~-~~~~~56~~~~~-~-~:_.-::._~_~r-::.~==- __ :::~ti==~~~~ -~~~~-~=:j 

=======================~============================================= 

External Standard Repcrt 

====================================~===~~=========================== 

Sorted By 

Culib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

Use Multi.plier & Dilution Factor with ISTDs 

Signal l: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[m.in I [uS/em* s] [ug/mL] 

-------]------]----------]----------]----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

VJarning : Calibrated compound ( s) not found 

==========:=======================.,.,=== .. ,=================-·""'""'="'-'====~======== 

=====::..~==''"'===-===,=====~==:::================·====:=-:;:.:"'-'=====:==================== 

Area Percent Report 

========================""-""""==============================="'-'=""·'""'======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

IGG EA# 0910-96 Page 106 of202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI?iifile433 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6402.D 

Sample Name: P5 R3 out B *10 0910-96 BORALBRICKS 

=============================~======================================= 

Acq. Operator EO Seq. Line 64 

Acq. Instrument Mr Burns Locatton 

Injection Date 10/2/2010 11:14:17 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \!JPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last chanaed 10/4/2010 9:33:01 AH by IGG 

--~---~ .. A£)C1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR 8URNS\OATA\OCT\HPLC53PG98\051-6402.D) 

uS/em l 

180 l 

160 "1 

140 ~ 

120 ·j 

100 ~ 

80~ 

60:1 

40 1 

I 

I 

I 

I 

I 

0 

gj 

of 

! 

\ 1 v "'*" 

2: L_;_~~~~;:-_c· ~~-=~::::::;=~:;·=:::;:l=r==~::;:::c:;==r==::::;:::!.:_:;::.::.,.::C::::;:==::;:=::;::=;~::j 2 4 

' ;:; I 

0 I \ 

,.: . _ _; ' ~ ---r--- -

-----------"'--------"-------"'------"---------' 6 8 10 

====================================================~=~========~===== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:32:52 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTOs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area ./\mount Grp Name 

[min] [uS/cm*s) [ug/rnL) 

-------l------l----------1----------l----------l--l------------------

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=,;:=o:=c===========-~~o-=:c..c=~"'="'o=,.==="'-"'"'======================================== 

Area Percent Report 

=::================================================:::"====='"-~======""====== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. oooo 

l. 0000 

Use Multiplier & Dilution Fact_or with ISTDs 

IGGEFW-\d!FOi111!0,91iJ~'iWOJE?;if2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

1~---- mi. 

APPENDIX PAGp~<J'e434 l of z 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6701.D 

Sample Name: Acid Blank * 10 0910-96 BORAL BRICKS 

~==================================================================== 

Acq. Operator EO Seq. Line 67 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 12:21:26 AM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METIIODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by IGG 

·- ~~-"1\D-ci A, AtliT c HANNELA(u:IHPLC2o1 oa41MR siJRN-siDAl'i\iocTIHPLc53PG9alo52-6701.DI 

"~:]_ 160~ 

140~ 

120 j 

1 

100-1 

80~ 

aoJ 

1 

40 _:j 

j I 

20 i ~ ~ ~ ~ ~ ,1 l C\i (") '<ttrl co Q -+~~~~---:-~___:_;::=-· 1 -=~,;_: __ :_:___,__i__~,:_-· ~, -· . .:.::;_:.-:.=-::::;::.- ...-__;_---;:·-:_::··:_:'·:;:-:::_:+' ·='"~~T, ~~~~~~,.-~_J 

L------···------l_ _______ , ___ ~ ________ 1_____________ 6 ·····---··?.· ....... ~-----------lQ__ 12 mid 

===================================================================~= 

External Standard Report 

==============================~===·~======~=========================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] (uS/cm*s] [ug/rnL] 

-------!------!----------!----------l----------1--l------------------

3.168 BB 8.45559e-l 1.62975e-2 1.37805e-2 Fluoride 

4.156 Chloride 

Totals : l.37805e-2 

1 Warnings or Errors 

Warning : Calibrated co~pound(s) not found 

==============================================~;-~''""-"===:.o:~~====--====:o:===== 

*** End of Report *** 

InstrurnentAIC:f'~P4~Ql)!l!g. fHQ1~~: 59 AM IGGEp/j(~fl;~~~~ 1JilbS&t?2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGiplll<je-435 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6702.D 

Sample Name: Acid Blank *10 0910-96 BORAL BRICKS 

Acq. Operator EO Seq. Line 67 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 12:33:46 AM Inj 2 

Acq. Method C:\HPLC201DQ3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC20 1 OQ3\MR BURNS\METHODS \HP!,C53 PG 98. M 

Last changed 10/4/2010 9:39:38 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q4iMR .. iiUR"NSIDATA\0CT\HPLC5:lPG.iiii\o"'s"2"-6"7"'D"z.ro") ------, 

uS/em l 

180 -1 

i 

160-1 

' :j 

140 "1 

120 1 

100~ 

I 

I 

~-- I soc' 

l ..

40 T""" I() 0) .- II 

20- ~ ~ ~ ~ 

0 -11-···_·_···,;·'-_·~--'r-~, --~,-------~r··_···_·"~-.i- · :L:~-tl() ---.-------.-----,- T.. ---,,-~-~~-~~---l' 2 c.4 ______ 6,_' --------·----~-------~------JQ_____ 12 mid 

=~"'=======,=================================="""""'"-~~===============:::"""==== 

External Standard Report 

Sorted By Signal 

Calib. Data t1odified 10/4/2010 9:36:48 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/JI..rea Arnount Grp Name 

[min) [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.121 Fluoride 

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

========""'-'-=======================::.""""'==""'========:=:o=====::::===::::===::c-"""""'·-::=== 

=======================::::c~==~========================="'-''"'=:,~:::.,~-=========::::= 

Area Percent Report 

==========================================="-~========== "-'===-~-=========== 

Sorted By 

Calib. Data Modified 

Mul tipl.i.er 

Dilut_ion 

Signal 

10/4/2010 9:36:48 ~~ 

1.0000 

l.. 0000 

Use rvlul tiplier & Dilution Factor with ISTDs 

Instrument N"'rcl>m'<rt:Citlrib. I>Qo~4l2: 30 AM IGG E$i'~S~Lqs~~o~'f~~T B~6'JE1;~2 

AUGUSTA PlANTS 4 & 5, SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PA~ 436 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6601.D 

Sample Name: Base Blank *10 0910-96 

BORAL BRICKS 

==============================~=========~==~========================= 

Acq. Operator EO Seq. Line 68 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 12:45:35 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG96CL.M 

Last changed 10/4/2010 9:33:01 AM by IGG ~-·--·-·---AbcrA·, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\bCT\HPLC53'PG98\053:6861X5f ·------------~ 

uS/em ·j 

1801 

160~ j 

1401 

120 j 

·I 100 -; 

! " 

~ 

I 

===================================================================== 

External Standard Report 

======================================="="""~=======,====::"""============== 

Sorted By Signal 

Calib. Data Modified 10/4/2010 9:32:52 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------1--l------------------

4.2.37 BB 6.20201e-1 3.78526e-2 2.34762e-2 Chloride 

Totals : 2.34762e-2 

====="" ===o:= ;o: =="" ===== ===""""' = = = = == == === = = ===-=- """"' ,_,= = == = =="'==,·= === ==-=-=======""' 

*** End of Report *** 

IGG EA# 0910-96 Page 110 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~4lbe437 1 of l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6802.D 

Sample Name: Base Blank *10 0910-96 BORALBRICKS 

Acq. Operator EO Seq. Line 68 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 1:02:52 AM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M 

Last changed 10/1/2010 9:33:01 AM by IGG ,. ···-----i\I5cTA. ADC1CHANNE'L"A (U:IHPiX:2oToa4iMR BURNS\"D;,A""T A"I"D:rc"'T"IH"P"L"C"'5'"3P'-G'-'9"B"'Io"s"'3-"B"B0'"2'.o"").-------, 

~ 

' 

i 

External Standard Report 

============~===========~=================================~========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:32:52 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/ml,] 

-------l------1··--------l----------l----------l--l-------·---------· 

4.238 BB 6.09262e-l 3.78526e-2 2.30621e-2 Chloride 

Totals : 2.30621e-2 

*** End of Report *** 

InstrumentAICf!JlP4~'2ol:Je IHQ1t14: 58 AM IGGE~~~tf~PRb9&e92 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJP!i'~e438 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6901.D 

Sample Name: DI H20 blank 0910-96 

BORAL BRICKS 

===================~===============~==============~================== 

Acq. Operator EO Seq. Line 69 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 1:20:42 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by IGG 

.. --- ADC1 A, ADC1 CHANNEL A (U:IHPLC2010Q4\MR -BURN'T,S~I;<D';;-AT"'A'-I"'O"'C"TI""H"'P"L"C~53"P"G"'9"'8"'1054-6901.D)"·------------

uSicm l 

180 ··1 

i ' 

160 _j 

140 ~ 120--3 

j 

100-1 

::j ~ ·c 

0 

:c 

(.) 

8l 

I 20l 

j l .... --~~- j ____ _ 

~ i 

--,-- :::..,:=:;=:::;:::==~----, ·r---,-----! __ .c4.___ _________ s _____________ a. --------'1"'o __________ 1_~-----·_rnL". 

=================;:..:.=================:;:::-=-==============:-================== 

External Standard Report 

==========================~===========-=====================""========= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area ~~t/Area Amount Grp Name 

[min] [uS/crn*s] [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

3.121 Fluoride 

4.286 VB 2.98664 3.78526e-2 1.13052e-l Chloride 

TotaJ.s : 1.l3052e-1 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

==="'-'=======:==============·"-""==::===================='============::::.·>======= 

*** End of Report *** 

EA# 0910-96 Page 112 of 202 Instrument MCWdJ!o:CEf:t-Jb. ~-qa1J.ii!: 32 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI!<t00439 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6902.D 

Sample Name: DI H20 blank 0910-96 

BORAL BRICKS 

==============================================-======================= 

Acq. Operator EO Seq. Line 69 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 1:33:02 AM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changea 10/4/2010 9:39:38 AM by IGG r----·--·--------ADC-1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR.ff(j';;R;:-;NS"-\i'>D';;-AT"'A'-\O"crcnnc;HP""L"C'5'3PG98\0-54-_-6902-.0)-~----

I us::: i_l 

1601 

140l 

1201 

100 l 

80-1 

60J 

1 

40 -J 

1 ~ 20 -~ ~ €i :;; a:l ~ r J NN ~ ~ ci ', 0-±-=-' -i- ___ ,_j _____ -+- r----·--- -------, +---- t t ......... ------,-----..,.-----·-r·- -.,..-----r---,----.-----~-,--~---1 

[_ _________________ ?______ 4 _______ !;_ __________ ------"'8 _______ 10 ---------- ___ 1~--- m1J 

Sorted By 

Calib. Data Modified 

External Standard Report 

Signal 

10/4/2010 

1. 0000 

9:36:48 AM 

Multiplier 

Dilution 

Use Multiplier & 

1.0000 

Dilution Factor with !STDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

Ret'I'ime Type Area Amt/Area Amount Grp Name 

(min] [uS/crn*s} [ug/rnL] 

-------l------l----------l----------l----------l--l------------------

3.121 Fluoride 

4.288 VB 1.15224 3.78526e-2 4.36153e-2 Chloride 

Totals : 4.36153e-2 

1 warnings or Errors 

Warnj.ng : Calibrated compound(s) not found 

=========·====================o:::o:::===========;..:============co;;,=:============= 

*** End of Report *** 

EA#0910-96 Page 113of202 Instrument NTciliJRdJAAlJ4b. pO,uq.f;.: 41 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAQ!;;jgo: 440 l of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0901.D 

Sample Name: 0. 01N H2S04/NaOH RB BORAL BRICKS 

=====:================================================================ 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 9:02:21 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

9 

1 

r-----,A:ro"'c"'1'A'. "A"'o;c1 cRANNETA(u:\HPCc251 oo4iMRiiliRiJS\5P:t A\o·cnRPl.i5":iPG9Biooa.osoC6)- - -----

uS/em ~ 

180 ~ 

160 

140-

120-

100 

External Standard Report 

==========""'========================================,==========="'-====""' 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area F~ount Grp Name 

[minj [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.147 Fluoride 

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

InstrumentAICfflfl!l~\llitl9· f?rlil1~?28 AM IGG E~~rJil$-~fb~~t>"\fu9~t92 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp'*J6 441 1 of 2 
Oa ta .t''lle U: \ti.t' LCLV 1 U\J!! \MK .!:5UKN::i \IJATA \UCT \til:'Lt..,.:=;.jl:'J,;,~tl \UUtl-U ~UL. IJ 

Sample Name: O.OlN H2S04/Na0H RB 

BORAL BRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analys.is Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 9:14:41 PM Inj 

C: \HPLC2010Q3 \MR BURNS\METHODS \~lETROHr1. M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

9 

2 

--------AoCfA-;--ADC1 CHANNEL A (U:\HPLC2Cdoo4iJJFfBDRNS\DATA\OCT\HPLC53PG98\008~(j962~!5}---··-----·--··j 

uS/em-~ j ~ : 

;:: ~ ! q 

140-1 

1201 

1:: -j 

601 

40] 

201 ~ ! 

···-----------...1 __ _/_ o -1==·-:_r~-~=-~-=.c.-.-:::_-~·:::.::-:.:::;:==;:=:;::::=;:::'.::;:":.=o::,;::.::: .. :::::;:= . -----r·-·-- ...,-·---·,-------,---,--------,-----· 

---·-------~1c.__________ 4 6 _________ 8 _________ _ 10 

==~=====:~~===============~=========================================== 

External Standard Report 

:=:-=::::·=======================""'==""============--"=========================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area P~ount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------i----------l----------l--l------------------

3.147 Fluoride 

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

====================="'·""'==============="""============""="""==============o.c;c.:. 

IGG EA# 091 0-96 Page 115 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

g _____ mi 

APPENDIX PA~e442 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-320l.D 

Sample Name: O.OlN H2S04/NaOH RB BORAL BRICKS 

===========================================~===~===================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last ehanged 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:58:59 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2010Q3\MR BURNS\METHODS \HPl.C53PG98. M 

10/4/2010 9:26:06 AM by IGG 

(modif.ied after loading) 

32 

1 

····~·~;c~-lADCTAJii)i'TCHANNEL A (U:IHPLC2010Q4\MR BURNSIDATAIOCT\HPLC53PGii~668-3ioi:of·-·-------··----·-----~ 

'oo1 • & I 

160 -~ i l 

;:: J : i 

' 

100-j 

., 80 J 

60 -i 

" 40 .j 

20~ ~ ~ 0 ---1-~--~------,~ ~N ;::========~===;==~--~~~~~============= ----··,--·---r ·r··-----· ' 

L_ __________ ?.____ 4 6 __________ ____§ ___ _ 

Sorted By 

Calib. Data Modified 

I-1ul tiplier 

External Standard Report 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------!----------j----------!----------l--l------------------

3.147 Fluoride 

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrat_ed compound(::>) not. found 

InstrumentAICPIJlP:)gGrD~6 F'f10'1'JZ54 AM IGG EP~~RO~J&~~~JfR~ j,'),~9~t9 2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIP11Jge443 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3202.D 

Sample Name: O.OlN H2S04/NaOH RB BORALBRICKS 

===============================;==================~================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Anal.ysis Method 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/2/2010 8:11:19 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC20l0Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

32 

2 

r-----------ADC1A~Ai5CT CHANNELA(U:IHPLC26Too4\MRBURNSIDATAIOCTIHPLC53PG981008-3202.D) 

I ~~m1 ~, - 180 l -

160 --i 

140 J I 

120~ Ill 

100 i 

80 -j \ 

60~ 

::~ -1 ~ N __ J 

~ .n 

o -~=::;=:=.;=:::;:=::;=:::: r -----.--..!.:r-----,--=~::,~.::~~.:.:~-----~--,-----'-cc_:__c;... __ ~--~-~-----1 

···-·-----···-··__1 _________________ ___1_ __________________ ~----------------8 _________ , ________ __2_Q _____________ _1L_Jl!L 

==""='""~=========""======oc:==:e-..:o~=~'='"-"='-"==="==============================e:===== 

External Standard Report 

============"-'===·================================================,.==== 

Sorted By 

Calib. Data Hodified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1; ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL} 

-------l------l----------l----------l----------l--!------------------

3.147 Fluoride 

4.156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound{s) not found 

==========================================::::================'-'""'""=~··==:o-..:=== 

InstrurnentAICf/1P<I~©ljljJg.Rj1QII6<o3 AM IGG Ef'ii.~f$-~Jf~lo"\?o9&e)l2 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp)lJ~e444 1 of 2 
Data File U: \HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5601. D 

Sample Name: 0.01N H2S04/NaOH RB 

BORAL BRICKS 

================================~==================================== 

Acq. Operator EO Seq. Line 56 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 6:50:32 PM Inj 1 

Acq. Method C: \HPLC2010Q3\~IR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis ~1ethod U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98 .M 

J"ast changed : 10/4/2010 9:39:38 AM by IGG 

Ai5c1A:-!iocTd=iANNEL ii(U:\FfPLc2o1o641MlHiV"R"'N"s''"o"A"T"A'"o"c"n"H"'P'"L"c"'s"3""P<i9-Bii-oa:setTb) -- ------------~ 

uS:::j 

140-J 

I 

120 ] 

" 100 -j 

801 

60 Cl 

~~ I 

20~ § ~ i I 0 -t~--- T~- ~~~~~- ..... 1.' :;=::::::;=:;::=;=::;::=c::=.""-·------J I 

2 -~-r~=~~-----:~----------~ -~----- .. ------ ____ "'8 _____ ~_-'1"'';;''-------~-===-=-~----~-s-~_::~~d 

==========================~========================================== 

External Standard Report 

====-==::==============================""======================-··==::======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1,0000 

9:36:48 Al'1 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

Ret'!'ime Type Area Amt/Area Amount Grp Name 

[minJ [uS/cm*sJ (ug/mL] 

-------l------l----------l----------l----------l--i------------------

3.121 Fluoride 

4. 156 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

="""=====,=======~=:'Oc·:,::o"=·~""==============""=====""''"'==oc=======:.=====c===,-;;======""== 

=================================""===oO'oo===============.==~============= 

Area Percent Report 

====================·.::.<::c-====""=============oo:=.""''-"'=================""====""""= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Instrument kc¥\16.@!1-Wo. M\o94i 32 AM . EA# 0910-96 Page 118 of 202 

IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PA~ 445 1 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5602.D 

Sample Name: O.OlN H2S04/NaOH RB 

BORAL BRICKS 

========~=======================~~=================================== 

Acq. Operator EO Seq. Line 56 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 7:02:52 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\MET!!ODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method 0; \HPLC2010Q3\MR BURNS\METHODS\HPI,C53PG98 .M 

Last changed 10/4/2010.9:39:38 AM by IGG 

- -------AOC-1 A, ADC1 CHANNEL-A(0:\HPLC201004\MR BURNS\DATA\i5CTiHPlC-53PG98\103-5602.D) 

uS/em l 

180 j 

; 

160 3 

j 

140jl 

120~ 

100 J 

80 -~ 

~ 

1 

::LI ~................ . .! . o -~ ··-··;·----·1-------.---.. ---- -==::;c.=;:::::~..'-";=:=;:;:::::;::::= ·r··----.,..... .. ·----~. ~---,.-~-~-~~-~· ,------

__ 2 __ -~-------j __ _ 6 ___ ___IL ____________ .... JQ. 12 mi 

=====·===""=""=~'"-'"'"===============::"===================="''===========,;::=:::=== 

External Standard Report 

====~===========~====================~=============================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area A.t-uount Grp Name 

[min] [uS/cm*s) [ug/mLJ 

-------l------l----------j----------j----------1--l------------------

3.121 Fluoride 

4.10>6 Chloride 

Totals : 0.00000 

1 Warnjngs or Errors 

Warning : Calibrated compound(s) not found 

=======================~~=="''·'""-"-"============="-'""===============o-.:oo:•=::--.c,===== 

====================·==~""=========="'=""~"==================o.~'"'"~=========== 

Area Percent Report 

='""====================""="-'""'="-'=================""""""-''"'===""=====oo-"~==='"'===== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Mtlltiplier & Dilution Factor with ISTDs 

Instrument AlfcWo.ft'tl!% ibf\o94J2: 41 AM rGG E~~~~~~~s~~o~mT1 ~~J'JE~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE'-.446 1 of 2 
Data File U: \HPLC2010Q4\MR BURNS\DATA\0CT\HP!,C53PG100\008-0901. D 

Sample Name: O.OlN H2S04/Na0H RB BORAL BRICKS 

================================,=========""=======================""== 

Acq. Operator 

Acq. Inst.rument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last. changed 

EO Seq. Line 

Mi Burns Location 

10/4/2010 5:15:07 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/I/2010 4:15:36 PM 

U: \HPLC2 01 OQ3 \t1R BURNS \METHODS\HPLC53PG1 00. M 

10/5/2010 9:18:49 AM by IGG 

(modified after .loading) 

9 

1 

~--- ------A5C1 "A-. A""D"c"1"C"'HP:NNE'C A (U:IHPLC201 004 IMR BURNSIDATAiOCTIHP'C<;53PG 1'"o"ol"'o"'o8"·"o9"'0"1".D'-)--------------- .. 

uS/em j 

180 j 

1 

160 -] 

140 .. 

120 

100 . 

80 

eoJ 1 

40 ·jl 1.() 

20 -~ ~ ~ 

,, 

f( 

\I 

li ,, 

\I 

" i' 

I_ 0 -l=-·;-'-~--- r·---=--~:::_:_·:-=::;::::.=. =;:, ==;:::::::=:;::::'.·'::'"'~- -. ':.·.:;::_.. -.---·· ·--~------,--~~~:1 

__ 2,_ _____________________ -"--4 --------------~---------- -----"8'-- _________________ J!'!!j 

:::::::::::c..cc""==========="-~=============================='""==============~-"'''======= 

External Standard Report 

============>====================================="===========·""'======== 

Sorted By 

Calib. Data Modified 

Signal 

10/5/2010 

1.0000 

9:21:11 AM 

Multiplier 

Dilution 

Use Hultiplier & 

1.0000 

Dilution Factor with ISTDs 

Signal l; ADCl A, ADCl CHANNEL A 

RetTime Type Area k~t/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------[----------[------------l--)---------------------

3.149 Fluoride 

4.153 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

Warning : Calibrated compound(s) not found 

=======•"'=->=====o.o·=====================================·o-o":O;=========="-~"'-=== 

InstrumentAl:C !'BP61i'Qll~O- F'.J1<lll!2 57 AM IGG EP~~ROJlJ/I;ilBlf!&'t ~~'b~U?2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!!'IHJ."147 1 of 2 
ua1:a n1e u: \li±' LCLU 1 U\.H \Ml< BURNS\DATA \OCT\HPLC53PG1 00\008-0902. D 

Sample Name: 0.01N H2S04/Na0H RB 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/4/2010 5:27:28 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

9 

2 

ADC1 A. ADCTCHANNEL-·A[O~iHPLC2010041MR BURNS\b7\TAI6cnRPLC53PG100I008-o9ci'2:-oj'·----- ----··· 

uS/em l 180~ 

160 j 

' 140~ 1

1 

12oj 1, 

1 :1 

100-j \i 

1 ll 

eo J ,

1 

i 60i ,, 

I ~ -1:1-=-=:;c, =-" :::-~':::--:.· =---=--=--=-=:::~=c;=--~- ~ ~ cc~ ~~,=~ "c J ~ ; 

L___ _ 2 __________ 4_ ___ ----"-6 ---------·--------- __ e

00' ____________ ;] 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/5/2010 

1.0000 

1.0000 

9:21:11 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area ~~t/Area Amount Grp Name 

[min] [uS/cm*s) [ug/mL] 

-------l------!----------!----------f----------t--l------------------

3.149 Fluoride 

4.153 Chloride 

Totals : 0.00000 

1 Warnings or Errors 

~\'arning : Calibrated compound (s) not found 

===:o=~-o:==o===:.o======================'"'"''""'"========·:::.;.-"::::===========,.·========~" 

01"/?0lO g n 0 EA#0910-96 Page 121 of202 

Instrument AT2PR8JECTNo. P:nn4z 5 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~I-/8. 4481 of 2 
Data File U:\HPLC2010Q4\MR BURNS\DATA\0CT\HPLC53PG9B\010-110l.D 

Sample Name: MS Salisbury Rl In A *20 0910-9EiJORALBRICKS 

====================================================="'"-'""'"'==========.::o==:.·= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/1/2010 9:51:40 PM Inj 

C:\HPLC20lOQ3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2 01 OQ3 \MR BURNS \f1ETHODS \HPLC53PG98. M 

10/4/2010 9:26:06 AM by IGG . 

11 

1 

(modified after loading) ----·-"""'c=-.-..=o-='i:~~:.;:;:.~~~;.;:.;~~"""~="'"===""""~~~~----, ADC1 A, ADC1 CHANNEL A (U:IHPLC201004\MR BURNS\DAT A\OCT\HPLC53PG98\01 0-1101 D) 

uS/em l 

180 -~ 

160 cl 

140 ~ 

120 J 

1::1·, 

40--. 

20-

====================~==~=======~=======~============================== 

External Standard Report 

=========='=·=="""='""=====""===========>"'=================================== 

sor.ted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor wj_th lSTDs 

Signal 1: ADCl A, ADCl CHANNEI~ A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------l------l----------l----------l----------l--l------------------

3.132 BV 663.60602 1.70817e-2 11.33552 Fluoride 

4.254 VB 136.56146 2.67214e-2 3.64911 Chloride 

Totals : 14.98464 

============""~="~"'==,~="""~"============================================== 

*** End of Report *** 

InstrumentAJ:Cfi19l41'~1i~e-19-1f!l16~40 AM IGG E~llr~~tl!l3'r1*b9~~92 AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGipll«je449 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\0l0-ll02.D 

Sample Name: MS Salisbury Rl In A *20 0910-96 

BORAL BRICKS 

===========================================~========================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

La.s t changed 

EO Seq. Line 

M;t' Burns Location 

10/1/201010:04:00 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

1l 

2 

j ·---··· .. ·----··-Aocr-A~A-OC"f CHAN-NEl-A (U:\HPLC201 004\MR BURNS\DA T A\0Cf\HPLC53PG9i~\0i0~-1102.())-~~----·---

J uS/em 

I 180-

160 

140 . 

External Standard Report 

==========""="=~================,==================================""===== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Siqna1 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min} [uS/cm*sJ [ug/mLJ 

-------l------l----------j----------l----------l--l------------------

3.131 BV 661.14001 1.70817e-2 11.29336 Fluoride 

4.253 VB 136.65158 2.67211e-2 3.65148 Chloride 

Totals : 14.94484 

*** End of Report *** 

I GG EA# 0910-96 Page 123 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGif~IJ.'l,so 1 of 1 
Data File U:\HPLC2010Q4\HR BURNS\DATA\0CT\HPLC53PG98\0ll-120l.D 

Sample Name: MSD Salisbury Rl In A *20 0910-9EfoRAL BRICKS 

======================================================~============== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 10:16:20 PM Inj 

C:\HPLC2010Q3\HR BURNS\METHODS\METROHM.H 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\HR BURNS\fffiTH0DS\HPLC53PG98.H 

10/4/2010 9:26:06 AM by IGG . 

12 

1 

(modified after loading) i --:~=~ i ADC1 A-, A"D"'c=1 'c,CHT;AC<NT.N;E;,:L7\ (Li.\HPLC201004\MR BURNS\DATA\OCT\HPLC53PG98\0n -120Tt5f------ - --l 

' 180 

' i 1sol I 

140 •j : 

1201 ~ 1 

J &: I 

::L:J r ) ~~f'~" _3 ~-~~-+1-... ~.L L--,-------~~ ;·---

l .... _____________ 2 _____ _1: _____________________ 6 8 --~------_1_0_______ 12 mir! 

External Standard Report 

===,.-,:=:::o===============;======="'="'=""=""'==========~o=-.o===o::r==""'============<'~==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area ~~t/Area Amount Grp Name 

[min) [uS/cm·-"s] [ug/mL] 

-------l------l----------j----------!----------l--1------------------

3.131 BV 626.82330 1.70808e-2 10.70667 Fluoride 

4.255 VB 129.13361 2.67472e-2 3.45396 Chloride 

Totals : 14.16063 

"''o::===========:oc~-==========""-~'================:::================::o========= 

*** End of Report *** 

InstrumentAllC ~B(I)JI;il7llfl0l Pl1:am 01 AM IGG EP~1l;#RQEgJI~s~8N~'lil;t ~~MJ.?P2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~~O!OI51 1 of 1 
( 

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1202.D 

Sample Name: MSD Salisbury R1 In A *20 0910-'~JfbRALBRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

ED Seq. Line 

Mr Burns Location 

10/1/2010 10:28:39 PM Inj 

C:\HPLC20l0Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

12 

2 

r·------- -ADC1A;7\DCTCHANNECA (U:IHPLC201 OQ41MR BURNSil5AtAi6cnHPLC53PG98ioTi~i2oi:"5j···-·· 

======-=======~~====================,,================================== 

External Standard Report 

,..=========""'""'==========================::.:o=~:c=============""·==>'c=:=========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:29:44 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area ~mt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.132 BV 629.07855 1.70809e-2 10.74523 Fluoride 

4.256 VB 128.93863 2.67479e-2 3.44883 Chloride 

Totals : 14.19406 

===:::===============~·================o•=============================,==·~ 

**~ End of Report *** 

Instrument Alrc~M>. ~-1iltl216 AM IGG EPIJ,~~rP~~?s~~o~~~~T ~~oM:If AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEiNle452 l of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3401.D 

Sample Name: MS P4 R1 In A *10 0910-96 BORAL BRICKS 

===~==============~===~=============~================~=============== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysi.s Method 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/2/2010 8:48:18 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METRO~M.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

{modified after loading) 

34 

1 

~----------------:o:DC1 .. A~AocTC}-IANNEL A. (U:YHPLC201004\MR8URNS\0ATA\OC-f\HPLC53PG~f8\027 -3401Df~ -·-·-··---··· .. ·-·-

uS/em 

180 

160 

140-

120 

100- " :g 

~ 

80 u: " "' "' 0 

60 N :2 ~ 0 

"' 

===================================================================== 

External Standard Report 

=====~====================================================~========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multip.lier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------!----------j----------l----------l--!------------------

3.125 BB 406.57947 1.70724e-2 6.94127 Fluoride 

4.259 BB 113.87910 2.68106e-2 3.05317 Chloride 

Totals : 9.99444 

=~=~====================================~============================ 

*** End of Report *** 

Instrument AfC:flWlll)i'§~:t\9 19-!~1Jii1o6 AM IGG E~/Ml~i!,\l;§lbifi'@S'r1AAB~e't2 AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~e453 1 of 1 
( 

Data File U:\HPLC2010Q4\V~ BURNS\DATA\OCT\HPLC53PG98\027-3402.D 

Sample Name: MS P4 Rl In A *10 0910-96 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/2/2010 9:00:38 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

lJ:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

34 

2 

ADC1 A. Aocrc"HA"NNE'U\(i:i'\iiPLC2o100-4iMRBUR-NS\DATA\OCTIHPLC-53i'G98\627=34o2.D} ___ _ 

uS/em l 

180 ~ 

' 

160 J 

j 

140 :i 

' 120J 

3 

100--1 

J 

80 ~ 

" 60~ ~ 

40J A 

i II Ng i j'\ ...: ;;f);! ~o m 20-~1 ~ i (.. ~ ~ ~ r..: : ~------J..-~ ,., ____ ,) __ _ \_ ____ , .. ,.,_..;_ .''"-,--.J ~! -~-~- 1-""--...-- r--'·-"""'"~-- ,- 0 ...... ----,-------.----, -----,-----~~--.---,-----,---..,...---.,.--~-.-~-~-~-,----1 

______ __g--------------~-------·····--.. -------·-··-~------------- __ .'?.8 ______ 1'.Co,_ ____ __,1_,2_-"m'"'; · 

=-==========================~-o=::::======================================= 

External Standard Report 

===========================,========""'""============================="""= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.125 BB 406.89011 1.70724e-2 6.94659 Fluoride 

4.260 BB 114.10727 2.68095e-2 3.05916 Chloride 

Totals : 10.00575 

=·"=·~===========""·""''"""'""'=="==============================================o:o=<".::= 

**i End of Report *~* 

~ 1.ru• L2m.n _9 7 1 EA# 091 0·96 Page 127 of 202 

InstrumentAtC"PRU:!Et:rNO.I'-i01<Z 4 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGfWi8454 1 of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3501.D 

Sample Name: MSD P4 Rl In A *10 0910-96 BORAL BRICKS 

===========~========================================================= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 9:12:58 At1 Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

(modified after loading) 

35 

1 

f ----------- _ ADC-fA--;-Ar5C1cHAN NEI1\(U:\-HPLCi6"1'"664\MR-8URNS\i)Al-:.A\ocT\HPLC53P,G98\028=35{Ff.b')··-···---

! uS/em ~ j 

il 180~ i 

·I , . 160 ~ 

1 

I 

i 

·····--..,.-·--·-~--·.-·· 

=====·.:::c"'"=============================================:o================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTj_me Type Area l~mt/Area Amount Grp Na.-ne 

[min] [uS/cm·lrs] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.126 BB 408.43451 1.70725e-2 6.97299 Fluoride 

4.260 BB 114.63012 2.68071e-2 3.07290 Chloride 

Totals : 10.04589 

="''==="''=""==========================""========="'-================.:===""=== 

*** End of Report *** 

Instrument AtCW<bl!Et~Ml.l<-~il1"74222 AM 'rGG EP'¥)~RO~~?s~itJ'f'~gT ~o~k~~z AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

12 mi 

APPENDIX PAGE<me455 1 Of 1 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3502.D 

Sample Na/(le: MSD P4 R1 In A *10 0910-96 BORALBRICKS 

=================================================~=================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/2/2010 9:25:18 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:36:41 AM by IGG 

35 

2 

{modified after loading) 

r----------ADC17\.-ADC1CHANNEL A (UTHPLC20io64iivfR BU_R,NS"'I"'D"A"T'AI"'o"c"'n"'H"P"L'C"s'3"PG"9"'B'"I0"'2"'8'·3"5"'D2"."'D') --------. 

uS/em l 

180 ~ 1 

160 

140 

======"-"===========»-.:=====~""'""=================================o=.=======""""' 

External Standard Report 

==========,.,========o:o:=========,.,.======================================= 

Sorted By 

Calib. Data Nodified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1; ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.124 88 406.71420 1.70724e-2 6.94358 Fluoride 

4.259 8B 114.74656 2.68066e-2 3.07596 Chloride 

Totals ; 10.01954 

::::=.":;;==========================::-~======o:~:==-co=:;::=::=:=:=:=-=====================-==--~ 

*** End of Report *** 

InstrumentA.fCfflOIJ~il'ill:N!>- ~J!)1/Ii!30 AM IGG EM~rP~i!1\§~jb~j'gTV!l\:J'3kt92 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGp~456 1 of 1 
Data FUe U: \HPLCLUlUQ4 \MR EURNS\DATA\OCT\HPLC~3PG98 \007-USUl. D 

Sample Name: HPLC53pg98 #LCS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last change-d 

Analysis Met_hod 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/1/2010 8:37:42 PM Inj 

C: \HPLC2010Q3\MR BURNS\ME.THODS\~lE'rROHM. M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

8 

1 

1

----------p:o·crA:-ADCfCHANNELA {U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0801.D) 

u~ml g 

I 1~j ~ 1 I 

. 160 -'1 i 

! ' I j ) 1 

; 140 ·· 1 

I 120- I 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

1. 0 00 0 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

I 

-------l------1----------l----------l----------l --1------------------

3.118 BB 314.60535 1.70653e-2 5.36884 Fluoride 

4.258 BB 188.15720 2.65985e-2 5.00471 Chloride 

Totals : 10.37355 

*** End of Report *** 

1.1lL L2n1n .o ,~ 5 EA#0910-96 Page 130of202 

Instrument AfCWcf.JE<OTNO.I"-ioN2 4 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'N"i\e457 1 of l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0802.D 

Sample Name: HPLC53pg98 *LCS 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 8 

Mr Burns Location 

10/1/2010 8:50;01 PM Inj 2 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(rnodi.tied after loading) 

r--~~::: I"'AD'C1~ ADC1 CHAN NET"iqU:\HPLC2610Q4\MRBURNS\5AfA\CR;n·HPLC53PG~i8\0D7~0802~6)''''-----·-···-·-------~ 

160-

140 -j 

1 

120 ·j 

100 -J 

~ 

80 ~ 

l 

60 -j ~ j • ' 

40 j c-j l2 

20 j ~ [\ :; ~ 0 g5 ~ 

j t'\! f\ /\ ~ <ci ~ ~ / i -l------------1-:::' -~--- _\..._.,_~J- .. >-. --------'-~+-'"'"-~ -+ ...... --~~, ----J..._/~----1-.../ I 

0 -+---~ -·r---·--...------.. ------~--- ··-··1-------,-----.,_,.-----·--r-·--r---.----,.-------,-~----r-- -,----~---···;··-.----: 

2 4 __ 6~--~--JI; _________________________ . .!Q ___ , _____________________ .11.._~_mir] 

Sorted By 

Calib. Data Modified 

I-:lultiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:26:06 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.115 BB 313.83789 1.70652e-2 5.35572 Fluoride 

4.255 BB 188.36598 2.65982e-2 5.01019 Chloride 

Totals : 10.36591 

========================================================""""""''""'""'"'='.=o".'""==="'" 

*** End of Report *** 

Instrument Nn;J.Pltc;.JEOj-JNb ~'1:()~#)3 AM IGG E~A~~~~~qs~?o~~~~T t~o"JE~~2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI'o'Nl>l458 l of l 
( 

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3101.D 

Sample Name: HPLC53pg98 *LCS BORAL BRICKS 

===::o====================-~~============================================ 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Bu.rns Location 

10/2/2010 7:34:20 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

31 

1 

(modified after loading) 

-------ADC1 A'-.'A"D"'C"'17C-i:H"A"NNECA.(U:\HPLC201004\MRB0RNS\OAtA\OCT\HPTC53PG98\oo7::3101J5)·--

uS/em l _, 

180 -~ 

• ' 160 -~ 

·I 

140j ., 

., 120 ··] 

j 

100 ··J 

80 . 

===================================================================== 

External Standard Report 

============""==~o:======:o-oo:::=============================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------!----------l----------l----------l--l------------------

3.116 BB 313.15643 1.70652e-2 5.34407 Fluoride 

4.256 BB 188.40083 2.65981e-2 5.01111 Chloride 

Totals : 10.35518 

======~:::::o====>==~"'"".='"'"-~================================================== 

*** End of Report *** 

r~strument AlfCJRJlQJ.ffil:Nl>. B-mllnl AM IGG EM~~~~?s~\br\'\"@5T\¥d?J~IJ2 AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

--

APPENDIX PAG!><Nj>e459 1 of 1 
UdLd ~..l..te u: \t1l:'1A.-LU.LUI,J<:i\l"l.K ~UK.N:J\UATi\\UCT\Hl:'LC:Jjp(.;i;it!\UU/-jlUL.U 

Sample Name: HPLC53pg98 #LCS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

.Analysis Method 

Last changed 

BORAL BRICKS 

EO Seq. Line 

Mr Burns Location 

10/2/2010 7:46:39 AM Inj 

C: \HPLC2 01 OQ3 \MR BURNS \METHODS\l~ETROHM. M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

31 

2 

~---------.A"D'-'C'-'1. A ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3102.D) 

! uS/em j ~ 180--=l o? ~ ! 

i 

I 

l 

::: ~j:.i 120-

100 

80--

=======================================================~====~====~=== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

t-1ultipl.ier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area l-lmount Grp Name 

[min] [•.1S/cm*s] [ug/mL] 

-------l------l----------l----------!----------!--l------------------

3.117 BB 313.53778 1.70652e-2 5.35059 Fluoride 

4.257 BB 188.47112 2.65980e-2 5.01295 Chloride 

Totals : 10.36354 

===:===='0--":0"" -"'::"-::.- ;co,-_,._=-~.o:.-- :.._ "'--"'=-=- -::=---= ====== _=. ====================="'" :::.=-==--======--

*** End of Report *** 

1 10/4/2010 q 29 o t I EA#0910-96 Page133of202 Instrument ATC PROJECT No. P-\014~2 A 4 

GG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'N/,e 460 1 of 1 
( 

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5501.D 

Sample Name: HPLC53pg98 iLCS BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 55 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 6:25:53 PM Inj 1 

Acq. Method C: \HPLC201 OQ3 \MR BURNS \METHODS \METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Joast changed : 10/4/2010 9:39:38 AM by IGG 

---···---"·--ADC1 A, ADC1 cHANNEL A (U:\HPLC201004\MR BURNS\DATA\OCnHPLC53PG98\102:5501.0}-. --~ 

""::J , . 140l I 1 

120- ! 

100 - ~ 

u 

80~ ~ i 

60· <5 

::ot J L_ ..,.--- · --J~_ ---T~--..-----..---- .. ~1~~--J"---~.-JJ ---r-- ....,..---·-r··----, _ .... -· . . -----,---------, . . L-d! 

2 ______ ________ L_____ _ __ 6 8 __________ ____ j_.9 _____ ________ ···------~ 2 mi 

==============================>=:==================="-"===========;;;o====== 

External Standard Report 

======;;;o;;;o===============~,~=====;;;o===~=================~=========~====== 

Sorted By Signal 

Calib. Data Modified 10/4(2010 9:36:48 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with IS1'Ds 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min} [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.121 BB 305.91211 1.70644e-2 5.22022 Fluoride 

4.263 BB 183,26718 2.66072e-2 4.87623 Chloride 

Totals : 10,09645 

~c~::.-;=========::::.===========-~=~,,==,~===================·=============='==::..~:=== 

*** End of Report *** 

InstrumentA)C \'~9~7Slo~'IJ Pi1f:W7: 13 AM IGcJ=Pl<MRillMitlSli'lN~ !PR4J.llf&fl2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEjo~<ge461 l of l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5502.D 

Sample Name: HPLC53pg98 #LCS BORAL BRICKS 

="'"·=================::=========================""'==:=====================-·== 

Acq. Operator EO Seq. Line 55 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 6:38:13 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by IGG 

Aoc1 A. Aoc1 cHANNEL ATo:w:iPLc2of004\MR suRNS\iYATA\OCT\HPTC53PG98\1o2-s5oz_o> 

us~::J j 

160 -~ 

-! 

140 l 

., 120-1 

100 . 

80 

0 

0 

~ 

I 

======================================:=-:==================="'-•==·""'"~====== 

External Standard Report 

=========~-:::;:;o==·======~"='-"'==================='=''""=="!:'~======================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AH 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADCl CHANNEl" A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mLJ 

-------j------j----------l----------l----------l--l------------------

3.122 BB 305.85730 1.70644e-2 5.21928 Fluoride 

4.265 BB 183.06128 2.66076e-2 4.87082 Chloride 

Totals : 10.09010 

========================================·~"===··=======================''"''~-

*** End of Report *** 

Instrument AlfCJRROllttiJ:Nm R.Oero: 23 AM IGGEp7fl~~~~?s~fo~~~~TW~o~\ot<f2 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEil!!>e462 l of 1 
Sample Name: HPLC53pg100 #LCS 

BORAL BRICKS 

~==================================================================== 

Acq. Operator EO Seq. Line 8 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 4:50:29 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\ME.THODS\HPLC53PG100.M 

Last changed 10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

r·· .. ··-·--7\i5c1"ii;"i\6cTc"HiiNNEL A (V:IHPLC20 iOCi4iMRT3DRNS\6.i\i'.i\\OcnHPLC53PG 100\007-080 1.of·--··---- ··--, 

uSfcm 3 

180 l 

~ ·:-------' _ .... ,-:::-.~.--- --rI 

!I 

, ···-,-----------,------

_ __,8'--. ______ . ..mlrl 

============o:o·=""-============""·==================~============,.::;=::======== 

External Standard Report 

===="""-"=~~=·-""======================="'=========================="""'o======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/5/2010 9:21:11 AM 

1. 0000 

] . 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A1 ADCl CHANNEL A 

RetTime Type .i'\rea Amt/Area AJrl.ount Grp Name 

[min] [uS/cm~<s) [ug/mL) 

-------l------l----------l----------l----------1--l------------------

3.124 BB 307.02579 1.71654e-2 5.2.7021 Fluoride 

4.249 BB 181.57738 2.71138e-2 4.92325 Chloride 

Totals : 10.19346 

*** End of Report *** 

EA# 091 0-96 Page 136 of 202 Instrument 1 10/5/2010 9:21:31 AM IGG 

ATC PROJECT No. P·10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'me463 l of l 
Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0802.D 

Sample Name: HPLC53pgl00 iLCS BORAL BRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysi~ Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 5:02:47 PM Inj 

C: \HPLC2010Q3\MR BURNS\METHODS \t<ETROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

{modified after loading} 

8 

2 

~---~~:~:-~A!5c1 A~ADCi CHANNEL A (U:IHPLC20iOQ4\MRBURNS\DAYAiOC·nm>t:cif:lf>(;160\6o7 :oao2:0)--

j 160~ 

140 ~ 

120 ~ 100-1 

80 

60. 

40 

20-

======================================================~============== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/5/2010 9:21:11 AM 

l. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCI CHANNEL A 

RetTime ·rype Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.125 BB 307.89706 1.71653e-2 5.28514 Fluoride 

4.249 BB 181.32318 2.71142e-2 4.91644 Chloride 

Totals : 1.0.20157 

*** End of Report *** 

Instrument Atc:f(Rd;jEt<na. P-l-1~114238 AM IGG EP):'IgRo~~?s~?orf.f~~W~o~t~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

"' "' 1 

APPENDIX PAGf<Ni!~464 1 of 1 
I 

'· 

BORAL BRICKS 

Calibration 

Curve Chromatograms 

ATC PROJECT No. P-10142 EA# 0910-96 Paqe 138 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 465 
Method U:\HPLC2010Q3\MR BURNS\~£THODS\HPLC53PG98.M 

BORAL BRICKS ===================================================================== 

Calibration Table 

==========================,========================================== 

Calib. Data Modified 

Calculate 

Based on 

Rel. Reference Window 

Abs. Reference Window 

Rel. Non-ref. Window 

Abs. Non-ref. Window 

10/4/2010 9o26:06 AM 

External Standard 

Peak Area 

10.000% 

0.000 min 

10.000 % 

0.000 min 

Use Multiplier & Dilution Factor with ISTDs 

Uncalibrated Peaks not reported 

Partial Calibration Yes, identified peaks are recalibrated 

Correct All Ret. Times: No, only for identified peaks 

Curve Type 

Origin 

Weight 

Linear 

Connected 

Linear (Amnt) 

Recalibration Settings: 

Average Response 

Average Retention Time: 

Calibration Report Options 

Average all calibrations 

Floating Average New 75% 

Printout of recalibrations within a sequence: 

Calibration Table after Recalibration 

Normal Report after Recalibration 

If the sequence is done with bracketing: 

Results of first cycle (ending previous bracket) 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime I~v.1. Amount Area Amt/Area Ref Grp Name 

[min] Sig [ug/mL] 

-------l--!--l----------l----------l----------l---l--1---------------

3.147 1 1 2.00000e-l 11.23373 1.78035e-2 Fluoride 

2 1.00000 61.93819 1.61451e-2 

3 5.00000 309.42168 1.61592e-2 

4 10.00000 593.11342 1.68602e-2 

5 15.00000 852.09720 1.76036e-2 

4.156 1 1 2.00000e-l 5.55649 3.59939e-2 Chloride 

2 1.00000 34.57356 2.89238e-2 

3 5.00000 185.83790 2.69052e-2 

4 10.00000 378.92274 2.63906e-2 

5 15.00000 570.98003 2.62706e-2 

======"-"'=="·================''='====="""'-"=:=======""""~~~:-o===c.:==:"'=·====='="'=""·==oo:-"O"=~~= 

Peak Sum Table 

:.~:~=;;;;:::======================================================.:=~'===-====== 

***No Entries in table*** 

==:=~=================================""=========::========:::::=====:==='"'""""':-==:0: 

Instrument Alrclf100!J.Ee1HJ<>. Gl-lfii/425 3 AM IGG EPE)\')@~~~9s~fo~~~~T ~~o~~t~2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PAGEa-q,e466 1 of 2 
.l"Je-cnoo U; \lit' l.A .. .:::: U l U!,!..i \l"lK .I:WKN::J \l'l.I!:THUU::i \HPLC:JjP(:i~tl. M 

==============================~~==========~~~A~=~~~~§================= 

Calibration Curves 

====:::o==============================-,========================='"'======== 

Area / 

/I 

~ n 1 

800. '5' _,./ i 

700 -~ / 

soo-j /r/ 

5001 ./ 

400-j 3// 

300l /_,.7" 

200 -~ l / 

100 ~1 2 __ /-

-j,/ Q -r-----,-·--·--,-·-·--~-------,----~-"f'-----, .. - - ·T---···-,-· 

0 10 

Amountrug/mll_ 

Fluoride at exp. RT: 3.147 

ADC1 A, ADC1 CHANNEL A 

Correlation: 

Residual Std. Dev.: 

0.99937 

18.29678 

Formula: y 

m: 

b: 

mx + b 

58.49156 

5.73482e-1 

x: Amount 

y: Area 

Calibration Level Weights: 

Level 1 1 

Level 2 0.2 

Level 3 

Level 4 

Level 5 

0.04 

0.02 

0.013333 

Chloride at exp. RT: 4.156 

ADC1 A, ADC1 CHANNEL A 

Correlation: 

Residual Std. Dev.: 

Formula: y = mx + b 

m: 38.06134 

b: -2.32861 

x: Amount 

y: Area 

0.99996 

2.00920 

Calibration Level Weights: 

Level 1 1 

Level 2 0.2 

Level 3 0.04 

Level 4 

Level 5 

0.02 

0.013333 

r n s truman t ATclfoR'd.!EOTJNb. 1>;1;]14:!5 3 A~; IGG E:;;t~~~L~s~?o~~~§T1 ~~cfM~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~467 2 of 2 
-~·'""'"" ~..,,, .. ,. \V'-.l.- \·" .. .L.J'-"'.J..JC'J..JU \UUJ--U4U.l. • LJ 

Sample Name: HPLC53pg98 #1 

BORAL BRICKS 

=================:::o=======================:============================ 

Acq. Operator EO Seq. Line 2 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 6:10:43 PM Inj 1 

Acq. Method C: \HPLC2 0 10Q3 \MR BURNS\METHODS\I~ETROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:21:17 AM by IGG f ---Aoc1~1ii5c1 CHANNEL A cu:IHPLt2o1oo4\MRBU-Fi"NSii5AT"A"'o""'cn=H"'PccLc"s"3"P"'G""98ioOr62-6i:i5) 

I 

' us:~: -. 

160 c 

140 

120 ~ J 

100 ·~ 

l 

80 ~ 1 (!) (ll 

60_j ~ :g 

-·-···---~ 

! 

j :J ~ 

:: ___ l_.' __ c_.c- ___ ?; ___ ~_-_j ~4ir-·c~J .,·6·'-_'--~_:_:.._~-._- ____ -_~-',_-_-_-_a'_-_·--~-- i . .... . . . -·· _ ... ----·-T_-_--"i1l0_ ~-... ~-==~---~li:=~.-~i.J 

===,..._,================""================="~==========~·=================== 

External Standard Report 

=========================================================~==========~ 

Sorted By Signal 

Calib. Data Modified Monday, October 04, 2010 9:21:13 AM 

Multiplier 1.0000 

Dilution L 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min} [uS/cm*s} [ug/mL} 

-------l------l----------l----------l----------l--1------------------

2.984 VB 11.43427 1.62975e-2 l.86350e-1 Fluoride 

4.161 EB 5.52259 3.73516e-2 2.06278e-1 Chloride 

Totals : 3. 92628e-l 

..... -~ .. == ---- - ·-======= ====:~·=""=================c::=.=::.-.= =====:=:·=====:::o======t+o===== 

*** End of Report '** 

Instrument 1 10/4/2010 9:21:47 A~1 IGG EA#0910-96 Page 141 of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAc!EfWo~ 468 1 0 f 1 
udLd ru.e u: \J1l:'L\...LU.lUIJ-'l\I"..K eUHN0\UA'l'A\OCT\HPLC:.3PG98\00l-0202.D 

sample Name: HPLC53pg98 #l 

BORAL BRICKS 

=================="'-'=============================:<==============,===== 

Acq. Operator EO Seq. Line 2 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 6:23:04 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

I.ast changed 4/l/2010 4:15:36 PH 

Analysis Method U:\HPLC2010Q3\MR BURNS\l1ETHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:21:17 AM by IGG 

~----- -. )\Dei -A"7--6cfCHANNE:L"i\(o:\HPLC2:00i.1 o'-o'-4;CIM:'iR~Bi.U~R""N:;,SI"D"A""T""A"IO'-'C"T\'"H"'P"'L'c"s"3"PG"'9"'s"ID"'D"1-;-0=2o2~r5)- ··-·· . - ---- 1 I uS/em J i 

, 

180 "j 

160 J j 

140-! 

j 

:::1 

80 "j 

60 ~ _-g g 1 § .2 

:., u:: ..._105 ...... 'lr'l- 40 -~ QI(:J ·'-' 

-1 0 ..,_c:,· <-:;"' Ol 2o-i ~ 0ttr· ~ r!ffo- ~ l ~- ~ # m • 

L_------~·-=~~~---1·=-~=-~~=~-;:::r~--~ ~--=-=-~-~=--=--· _-_-_-~_-_--,_~--J ____ ~_-.. -_._,·;r"~---_-~_-·_·--~--~~-~--_-- ~~;-~~--fl)-jJ 

=================================="-'·==="-'"=="======:====================== 

External Standard Report 

=========:=:==============================================""="'-="-"========= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

t>'londay, October 04, 2010 9:21:13 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

2. 980 Ml1 10.90178 1. 62975e-2 J. 776"12e-1 F'luoride 

4.156 Ml1 5.51022 3.73765e-2 2.05952e-l Chloride 

Totals : 3.83625e-1 

*** End of Report •** 

""" .o o.? 6 G EA#0910-96 Page 142of202 Instrument A'fcWcJ!Jte;~J.R,. ,-.;ol"-4~ 0 AM I ·G EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGg<Nl>e469 1 of 1 
Sample Name: HPLC53pg98 *1 

BORAL BRICKS 

Acq. Operator EO Seq. Line 70 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 1:45:22 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:21:17 AM by IGG 7\ocfA: ADClCHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\Hi'Cc53PG98\o61-700D5) 

=============================~=========================~=~==========~ 

External Standard Report 

=""'"'=========================================="""-~============~-=======""= 

Sorted By Signal 

Calib. Data Modif.ied Monday, October 04, 2010 9:21:13 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

2.990 VB 11.61392 1.62975e-2 1.89278e-1 Fluoride 

4.158 88 5.54815 3.73006e-2 2.06949e-l Chloride 

Totals : 3.96227e-l 

===============""======o:o""="'--========-"'='"'""""'==============""=======-======== 

*** End of Report *** 

101 0010 5 EA#0910-96 Page 143of202 Instrument A~Cl'RdfrrrNo. ~-'1bt4'} AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'W>e470 1 of 1 
uaLd i'l.ie u: \.tit'LLLU_iUl,J'f\l"iK _tjU.KN0\UA.TA\UCT\HI:'LC:J .. H'ti':H:S\UUl-/UUL.O 

Sample Name: HPLC53pg98 #1 BORAL BRICKS 

Acq. Operator EO Seq. Line 70 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 1:57:42 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed : 10/4/2010 9:21:17 AM by IGG 

ADC1 A ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCnHPLC53PG98\00T760~------~

uSfcm l j , 1 180 · , 1 

160 ! 

140--

120 

100 

80 

·····~---··-r. -·-·····-·-··-··! 

12 mi 1 

=:=:;·===========""'·"'"-'=:,==""'=""'===="''====================""======,============= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

Monday, October 04, 2010 9:21:13 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL .1\ 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/em's] [ug/mL] 

-------l------l----------l----------l----------1--l------------------

2.990 MM 10.98494 1.62975e-2 1.79028e-l Fluoride 

4.155 MM 5.64502 3.71113e-2 2.09494e-1 Chloride 

Totals : 3.88522e-l 

===='-"''"""·""'===,·~:::.::.::.;;::=:=;;=======~-=·=·"'-'=='-""==~===:===::::============================== 

*** End of Report *** 

InstrumentAICPR£xl~<21liiJ6. f'l1il'GI229 AM IGG EP~I}gRO~Jfli"~tbffllll'Tj,iM&tF AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE.Nge471 1 of 1 
Sample Name: HPLC53pg98 *2 

BORAL BRICKS 

=~=================================================================== 

Acq. Operator EO Seq. Line 3 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 6:35:23 PM Inj l 

Acq. Method C:\HPLC2010Q3\MR BURNS\HETHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed : 10/4/2010 9:21:17 AM by IGG 

[" .. ··- ·-·ADCfA. :A5c1CHANNEL A (Uc1HPLC2615541MR BURNS\DAT AIOCnHPLC53PG981002-03o1:b)"···----- -·----· 

uS/em ·1 ~ 

180 ~ :'! j ! 

160 ··~ 

J 

::1 

80 ~ 

i 

60 '! 1 

40] 

j Ng 20·-J M 

J___ N --·i-/\.. __ 

0-i-- r---~-....-----,.-

________ .. ___________ --~.£ __________ _ 

ru 

:g 

0 

E 

u 

======-============================================================== 

External Standard Report 

========""·========================================,=================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

Monday, October 04, 2010 9:21:13 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTiwE Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s) (ug/mL) 

-------l------l----------l----------l----------1--l------------------

3 .106 VB 62.57794 l. 69398e-2 1. 06006 Fluoride 

4.265 BB 34.83099 2.80299e-2 9.76308e-l Chloride 

Totals : 2.03637 

=====""=~.>.=="-'=================""=========:;::=""""~==========:=:================· 

*** End of Report *** 

Instrument 1 10/4/2010 9:22:59 AM IGG EA#0910-96 Page 145 of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~~ 472 1 of l 
oarnp~e Name: HPLC53pg98 #2 

BORAL BRICKS 

==================================================·=================== 

Acq. Operator EO Seq. Line 3 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 6:47:44 PM Inj 2 

Acq. Method C: \HPLC2010Q3\M!; BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC20lOQ3\MR BURNS\METHODS\HPLC53PG9B.M 

Last changed 10/4/2010 9:21:17 AM by IGG ~-- --~ADCTA~ADC1 CHANNEL A (U:\HPLC201004\MR BURNSIDATA\OCT\HPLC53PG98ioii2-0302 D)~-. ·-··---~ 

I US/em .j 0 ~ 

1ao~ !

1 ] 

::j : 

100 j II 

============-===========================<--'========================e:==== 

External Standard Report 

================~==================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, October 04, 2010 9:21:13 AM 

1.0000 

1.0000 

use MuJ.tiplier & Dilution Factor wit.h IS1'Ds 

Signal 1: ADCl A1 ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------l------l--·--·----l----------l-------·--l--l-----·------------

3.105 BB 60.57874 1.69346e-2 1.02588 Fluoride 

4.262 BB 33.81343 2.80827e-2 9.49573e-l Chloride 

Totals : 1. 97545 

==========""'==:~:=: ·""'=====c==·-'=';:::::::=======================o;::=============:.=~>:.::== 

*** Er1d of Report *** 

lnstrurnent 1 10/4/2010 9:23:48 AM IGG EA#0910-96 Page146of202 ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'IJ'/,e473 1 of l 
Sample Name: HPLC53pg98 #2 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 71 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 2:10:01 AM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Ana lysis Method U: \HPLC20 1003 \MR BURNS \METHODS\HPI"CS3PG98. M 

Last changed 10/4/2010 9:21:17 AM by IGG 

r···· ··---·)i:tic'1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCTIHPLC53PG98\002-7101.D) 

uS/em l ~ 

180l :il 

160 'l I :::j 'I 

i I 

100 ·l 

80 1 

1 f ~ 60-~ u: ~ 

i 

' ! 

l_ 

::1 

o -..----,----.~. ,---·--,--,--r--..----., ,1 ,i .~~...:~c.·_, -.~---·r---......,...------.,---....----r· 

L+i _____ ,.-'- .. --,---,---..,...---y---·-~----,...----~-,-~--1 

-~----~-....: ··--------~ 4 6 8 10 

===================================================================== 

External Standard Report 

=================='"""'"""'""'==:.==="'~""''--o·===""''"""'=====""·""'~"=="'~""==~"'""'-""==,=====-'""===:::===~ 

Sorted By 

Ca.lib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, 

1.0000 

1.0000 

October 04, 2010 9:21:13 AM 

Use Multiplier & Dilution Factor Hith ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTirne Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.116 VB 63.31603 1.69416e-2 1.07268 Fluoride 

4.267 BB 35.34018 2.80046e-2 9.89686e-l Chloride 

Totals : 2.06236 

===========~========================================================= 

**~ End of Report *** 

Ins t rumen tAlC l'lw.l~<:!1l ~6. f!l1 t2\42 56 AM I GG EP~~c!RO~JPs§ibJ'fE'Jl'T ~1lo3~t~2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

12 mi 

APPENDIX PAGi£'~1'474 1 of 1 
BORAL BRICKS 

===========,.=====::::===================,==============:================= 

Acq. Operator EO Seq. Line 71 

Acq. Instrument Mr Burns Location 

Injection Date 10l3/2010 2:22:21 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U; \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98 -~1 

Last changed 10/4/2010 9:21:17 AM by IGG ~-------ADCTA,ADCfCHANNEL A (U:\HPLi';-ioiOQ4\MR BURNS\D:;cAeoT"A-c\O~c~n=H~PL~C=s3PG9ii\iiiii=71o2:b) 

i uS/em l <? 

180~ ~ 

I 

! 

_, 

·! 

160 j 

140 l 

:::Jj.< 

80 

60 

3 

"' '0 

·c 

0 

:c 

(J 

40 l 10 t-- N 0 I 

20J ~ ~ i:!il ~ N 10 f?l I J N ·),__ "f ~ (0 ~ ~ .••• /_. 

0 J,=-=;_~_-;::__-:_~-::!::_: ·· r-----', ., __ :,..__~.:_-_··,-+~f------=-----,--.· ... .:=---,--'---- -l- ' . ' ' ---r-··----,---,--,-

-----~- 4 _ _ __ 2___________________ ____ 8 _ _1Q _______________________ _1~,___,m,i,..~ I L_ ____ _ 

========~==~=========================~=========~============~========= 

External Standard Report 

=========~====================================================~=~==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

Monday, October 04, 2010 9:21:13 AM 

L 0000 

Dilution 1.0000 

Use ~4ultiplier & Dilution Factor wittl ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/m.L] 

-------l------l----------l----------l----------l--l------------------

3.115 BB 61.28004 1.69365e-2 1.03787 Fluoride 

4.267 BB 34.30963 2.80566e-2 9.62610e-1 Chloride 

Totals : 2.00048 

==========~~-"'~=======-"-'""=""'=======================~===========""~"'-======== 

*** End of Report *** 

Instrument 1 10/4/2010 9:24:05 P.M IGG EA#0910-96 Page148of202 ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEW,0475 1 of 1 
Sample Name: HPLC53pg98 #3 BORAL BRICKS 

=======================~============================================= 

Acq. Operator EO Seq. Line 4 

Acq. Instrument Mr Burns Location 

Injection Date 10/l/2010 6:59:03 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.H 

Last changed 4/1/2010 4:15:36 PH 

Analysis Method. U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:21:17 AH by IGG r---- ADC1 A, ADC1 CHANNEL A (U:\HPLC201004\MR 8URN$\0AtA\0cnHPLC53PG98\oo3-6401~D) -------------·-·--, 

! uS/em l ~ 

1 180- ~ 

I 

I 

160 

140 

120 

100 

80. 

j 

60 ' 1 

40---l 

j <n 

20--J ~ 

1--·---' ~ 0 . ' 

2 

======~==~============================================~============== 

External Standard Report 

=========================================================::=~.,==,======= 

Sorted By Signal 

Calib. Data Modified Nonday 1 October 04, 2010 9:21:13 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor l-dt.h ISTDs 

Si.gnal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnLJ 

-------l------l----------l----------l----------l--!------------------

3.112 BB 308.75937 1.70647e-2 5.26889 Fluoride 

4.257 BB 185.12665 2.66039e-2 4.92508 Chloride 

Totals : 10.19398 

,.~==~"'""""===~-'""'~·"==~-~~==.-:c"-""'""'"'"'======""'==::::=::::===================''"~"-"""===·.-:t'"·=·======== 

*** End of Report *** 

Instrument ArC:Rll()ii,EZ~Nl>. B-1Q1!1215 AM IGG EM~~~~?s~lbr\"fEJS'r1p\~bq!ofN2 AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~~476 1 of 1 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 4 

P.cq. Instrument Mr Burns Location 

Injection Dat.e 10/1/2010 7:11:22 PM Inj 2 

Acq. Method C: \HPLC20l 0Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed : 10/4/2010 9:21:17 AM by IGG 

Aoc1 A. AoCTcH"ANNEL ii(u\HPLc2o1oa.,MR BuRNsioATA\ocnHPtcs3PG98\oo3-o4oz:or··-- ---

;g 

i 

' 

1~----~"--1Z~j -·~·----------

=-====,================:;,========::::============,:=========o:o=============== 

External Standard Report 

=============='-"======'-"===:o.~=============,-========"-'====================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, October 04, 2010 9:21:13 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s] [ug/mL) 

-------j------:----------l----------l----------l--l------------------

3.113 BB 308.33966 1.70647e-2 5.26172 Fluoride 

4.257 BB 185.05852 2.66040e-2 4.92329 Chloride 

Totals : 10.18501 

'"'======""============:o:==o=========·o•<>:<=============,.,====================:::: 

*** End of Report *** 

,nstrument 1 10/4/2010 9:24:23 AM IGG EA#0910-96 Page150of202 ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJE'ffi,e 477 l 0 f l 
Sample Name: HPLC53pg98 *3 BORAL BRICKS 

=-================================:================================""=>== 

Acq. Operator EO Seq. Line 72 

Acq. Instnlment Mr Burns Location 

Injection Date l.0/3/2010 2:34:41 AM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed : 10/4/2010 9:21:17 AM by IGG 

~-------~-;;;:ocrr. AoCTc"HANNEL-A tu:IHPLc2o 1 oa4\MR BuRNs\oA T AlocTIHPCcs3?898\oo3-no1 .o)~----~~-----

usrcm --~ ~ 

180 "J i ~ '1 

J 

160 -1 

140j 

~ 

120-1 

100 

so~ 

===================================================================== 

External Standard Report 

==============================================~====================== 

Sorted By Signal 

Calib. Data Modified Monday, October 04, 2010 9:21:13 AM 

Multiplier 1. 0000 

Dilution 1.0000 

Ose Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/em's] [ug/mL] 

-------;------l----------l----------l----------l--l------------------

3.124 BB 309.26727 1.70648e-2 5.27758 Fluoride 

4.263 BB 186~31842 2.66017e-2 4.95640 Chloride 

Totals : 10.23397 

==:oo========================-=---~o="'-~==:=o=="-"===============================·-= 

*** End of Report *** 

rnstrumentAtc~~enl<l. ~~~111236 AM IGG EP'l(;-U~~?silibtf-¥~~T ~~o~kt~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI?<Wge478 1 of 1 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

===========================~========================================= 

Acq. Operator EO Seq. Line 72 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 2:47:01 1\M Inj 2 

1\cq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METRDHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3 \MR BURNS\METHODS\HPLC53PG.98 .M 

J"ast changed 10/4/2010 9:21:17 ~_M by IGG ~---- ADC1 A, ADC1 CHANNEL A {U:\HPLC2010Q4\MR BURNS\DATA\6t"f\l.:(p['t53PG98\003--7202~-------~----·-··1 

I ' 

j uS/cmj I <!i!~ · ' I 

1 1so 1 

1eo 1 

140 

120. 

100 

===================================================================== 

Sorted By 

Calib. Data 1-lodified 

Multiplier 

Dilution 

External Standard Report 

Signal 

Monday 1 

1.0000 

1.0000 

October 04, 2010 9:21:13 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area J\rnount Grp Name 

[min] [uS/crn*s] (ug/mLJ 

-------l------l----------i----------i----------l--l------------------

3.125 BB 311.32043 1.70650e-2 5.31268 Fluoride 

4.266 BB 186.84802 2.66008e-2 4.97031 Chloride 

Totals : 10.28299 

========================================================~============ 

*** End of Report *** 

1 nt 1201n q 2 EA#0910-96 Page152of202 "nst rumen t AtCl>RO~ECT No. P· i u1'l.2 4 4 AM I GG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'l/ile479 l of l 
BORAL BRICKS 

=============================================================~======= 

Acq. Operator EO Seq. Line 5 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 7:23:42 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:21:17 AM by IGG ,..---- ~ Aoc1-A-;-iiocTcfiliFiFiEL A <u:\HPLc2o1o6<1"fR BURNs\oArA \OCT\HPLc53PG9aloo4-oso1.D> ·----

us/em ··i l8 

1Mj ~ i 

160 _:j 

140~ 

120 -1 

1 

100 . 

80 

60- ,-·, "' ~ 

I ::J,~l~)L~'·~{'~ ;~LJ ===========:>:·=======================================================::== 

External Standard Report 

===============================~~==========,====""============-=========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, 

1. 0000 

1.0000 

October 04, 2010 9:21:13 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

(min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.125 BB 592.99884 1.70799e-2 10.12839 Fluoride 

4.256 BB 377.41034 2.64355e-2 9.97703 Chloride 

Totals : 20.10542 

=============-==========="'·=-~=<========,============:"'===============::;.-:::.== 

*** End of Report 

...• strument 1 10/4/2010 9:24:57 A11 IGG EA#0910-96 Page 153of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Paae l of 1 APPENDIX PAGE N"o. 480 
Sample Name: HPLC53pg98 #4 

BORAL BRICKS 

=============:======================================================== 

Acq. Operator EO Seq. Line 5 

Acq. Instrument Mr Burns Location 

Injection Date 10/1/2010 7:36:02 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U; \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98. M 

Last changed 10/4/2010 9:21:17 Ar1 by IGG 

- ADC1 A, ADC1 CHANNEL A (U:\HPLC201004\MiHfURNS\DATA\OCTiHPLC53PG9S\004-050i:D)·-· ---------l 

uS/em l N 

180cj J -

~-

160 1 

1 

140~ ~-

120 ··J 

100-~ i 

ao.-.:1 ~ j ,.; 

60~ {\ ~ 

40 J IJ \__ i\ ·1 i\ N 0) N 

2: l:,).:;:;:=J.-L -~_\::-::,:;::-'J,__,-h",:~\--~-_c~},_~L---.--. ----,-----..... -- -i 

2 4 __ ...§_ _____________________ __!___ _________ ___ _!Q__ ________ g _____ mffi 

============='=============================================--""======o;o=o==:=: 

External Standard Report 

==,==~==="-'====·~~=========-=======================================""'===== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday 1 October 04, 2010 9:21:13 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTOs 

Signa1 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.123 BB 591.84839 1.70799e-2 10.10872 Fluoride 

4.254 BB 377.41174 2.64355e-2 9.97706 Chloride 

Totals : 20.08578 

=========================================================="-'""'·""''""=""===="" 

*** End of Report *** 

EA# 0910-96 PaQe 154 of 202 InstrumentAtcrndJ~§jlji.Jg_ Jl'-18'f120 5 AM IGG EPA ICR EMISSION T!OST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJ!'l\18•481 1 of 1 
Sample Name: HPLC53pg98 ~4 BORAL BRICKS 

====~========================================~====~================== 

Acq. Operator EO Seq. Line 73 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 2:59:21 AM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98. M 

J"ast changed 10/4/2010 9:21:17 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:iHPLC20fOQ4\MR BURNSIDATA\OCT\HPLC53PG981iio4~'i36cr-of·-------, 

uS/em~ 

======================================~========~===================== 

External Standard Report 

""'=========.:::~~O:OO'O::::~,====::o"::=::::::::-.=-o============================================ 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, 

1.0000 

1.0000 

October 04, 2010 9:21:13 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area &~ount Grp Name 

[min] [uS/cm*s) [ug/mL) 

-------t------l----------l----------l----------l--1------------------

3.135 BB 594.09766 l.70800e-2 10.14718 Fluoride 

4.263 BB 380.40378 2.64342e-2 10.05567 Chlo<ide 

Totals : 20.20285 

============================~=======~==========~=~=================~'~ 

*** End of Report *** 

Instrument Al"CJRRb!JEtiHJ0. ~-~ OP\221 AN I GG EP):'fgRo~~?s~i'ot\'f~TWRo5~~~2 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~<Wge482 1 of 1 
Sample Name: HPLC53pg9B #4 

BORAL BRICKS 

=========~========~=========~==============================~========= 

Acq. Operator EO Seq. Line 73 

Acq. Instrument Mr Burns Location 

Injection Date 10/3/2010 3:11:41 AM Inj 2 

Acq. Method C : \HPLC2 0 1 OQ3 \MR BURNS \METHODS \METROHM. M 

Last changed 4/1/2010 1:15:36 PM 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG9B .M 

Last changed. 10/4/2010 9:21:17 AM by IGG 

·-····----~Abc1A-.-ADC1 CHANNELA (U:\HPCC2'0"T604\MR BURNS\DATA\6CnHPLCsJPG98\004-7302.Df -----··--·---- -~ 

uS/em l ~ 

180 "1 1 ~ 

160j 

~ I 

:::~ ~ 1 

1

1

1

. 

100 i ~ ! I 

80 -~ M ~ I I 

eo -1 1i ~ 1 l !\ ...t 

•oJ i I f1 .- i 

I 

L 

200 -.1.-~-----.~ .f· t.~J \,T-;.:.__:r::-Ti~~c, ~-~~l, ::=::::.-'.::,c·./~->:-_···c_+_"_J~ ..... -- . ' ' • . ;---,.-----~----" 

_ 2_ _ • 6 L .. _______ .. __ 1,oc_ __ 

External Standard Report 

;=================================================,==========""·======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Monday, October 04, 2010 9:21:13 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min) [uS/cm*s) [ug/mL] 

-------r------r----------r----------r----------r--r------------------

3.135 BB 593.50879 1.70800e·2 10.13711 Fluoride 

4.264 BB 390.46509 2.64342e-2 10.05728 Chloride 

Totals ; 20.19439 

:..:""'=""========o.::==,._,======================:::~==::o::===,==:=-="===::;:,=;:o.=,_-=========== 

*** End of Report ~** 

.,,strument 1 10/4/2010 9:25:29 At1 IGG EA#0910-96 Page156of202 ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

12 
Sample Name: HPLC53pg98 ~5 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis t1ethod 

Last changed 

EO Seq. Line 

Mr Burns Location 

10l1/2010 7:48:22 PM Inj 

C:\HPLC2010Q3\MR BORNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U: \HPLC2010Q3\~1R BORNS\METHODS\HPLC53PG98 .M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

6 

1 

ADC1 A. ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG9B\005·0601.D) --- -··--·---··----------. 

uS/em g 

180 ~ 

160. 

140 

120 . 

===>=====,==================c:=:==""""""===,================================ 

External St.andard Report 

"'~'""==~o::=====""==================:=:;;:========================::::======:c.:======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Facto:r:- with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL} 

-------l------l----------l----------l----------l--l------------------

3.134 BB 847.65564 1.70849e-2 14.48213 Fluoride 

4.255 BB 568.12811 2.6381le-2 14.98783 Chloride 

Totals : 29.46995 

*** End of Report *** 

-w:..LA ""'"" .a ~"- 2 9 GG EA# 0910-96 Page 157 of 202 Instrument ATc+'«v.lc<:>YNn. e--~ ~1"1~ AM I • EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

I 

I 

' 

APPENDIX PAG~'iiae484 1 of 1 
Sample Name: HPLC53pg98 *5 

BORAL BRICKS 

=================================~=================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 8:00:42 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BORNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

6 

2 

(modified after loading) 1 -.-.. A"o"c"'1 'A-. A"o"c"1"'ci:iHiA"NiliNEL .. A(LTiRF'Cc2ofoa41MRi'isuC1REs'N"'s"''"o"'A"'TA"'"o"cnfirLcssPc9~-oo5-"06"o"'2'.o"J"---·----~ 

1 uS/em ~ ~ 

i 1801 q i J 

160 l 

140-

120 .. 

=================~===============~======================~============ 

External Standard Report 

===================,~====================================~============ 

Sorted By Signal 

Calib. Data Modified 10/4/2010 9:26:06 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l; ADCl A, ADCl CHANNEL A 

Ret'Time Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------r------l----------l----------l----------l--1------------------

3.134 BB 850.78156 1.70850e-2 14.53557 Fluoride 

4.254 BB 567.44427 2.63812e-2 14.96986 Chloride 

Totals : 29.50543 

============~ -=-,:c--,~~============-~~~-======""'="~==============='========""=== 

*** End of Report *** 

'nstrument 1 10/4/2010 9:26:37 AM IGG EA#0910-96 Page158of202 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

12 ' 

Paae 1 of 1 APPENDIX PAGE NO. 485 
Sarr~le Name: HPLC53pg98 #5 

BORAL BRICKS 

============~,======================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/3/2010 3:24:00 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\HETHODS\HPLC53P(.;98.M 

10/4/2010 9:26:06 AM by IGG 

74 

1 

(modified after loading) 

I . .,A"D'-'C"1'A'."A"OC""1'c-'H"'A.,:N.,;,N;;eEL i\(lJiHPLC2016o41MKBii'U;isR:.0NocSI"D"A""'TA"'I""O"'c"'TiHi5Cc53l'G98\oos:f4-6iD"f------, 

I 

; 

~ 

:g 

a 

:c 

CJ 

~ 

I 

===============================~=~=================================== 

External Standard Report 

==============================~=================================~==== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1. 0000 

l. 0000 

9:26:06 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL ~ 

RetTirne Type A.rea Amt/Area Amount Grp Name 

[min] [uS/cm*s) [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.147 BB 856.55316 1.70850e-2 14.63424 Fluoride 

4.266 BB 574.05273 2.63800e-2 15.14349 Chloride 

Totals : 29.77773 

:=::o;=:=.===========·=o:o.·.~-:C""-""'=============-"'."."O:=========o:::.:c.;=================~o='-" .. === 

*** End cf Report *** 

IGG EA# 0910-96 Page 159 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGj'o'NlJB486 1 of 1 
( 

Sample Name: HPLC53pg98 #5 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

An~lysis Method 

Last changed 

EO Seq. Line 

Hr Burns Location 

10/3/2010 3:36:20 AM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/l/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\MET!!ODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

74 

2 

·--·-··---·· ADC1A-:-.A.-t5C1CHANNEL A (U:\HPLC201004\MR BURNS\DATA\6CT\HPl.C53PG98\005-7402--:-D)---- -------------- ---·j 

External Standard Report 

==============~=~==========================~========================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/P..rea Amount Grp Name 

[min} [uS/crn*s] [ug/mL] 

-------l------l----------:----------l----------l--l------------------

3.148 BB 853.39844 1.70850e-2 14.58031 Fluoride 

4.268 BB 574.29498 2.63799e-2 15.14985 Chloride 

Totals : 29.73016 

••• End of Report *** 

Ins t rumen tAlc jb~611iefl~Q. plj(j'J~2 54 AM I GG EP~~[R O~J~~-~gNPT'i&"r ~~~~~~$2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGi!'fl!i.6187 1 of 1 
Sample Name: f!PLC53pg98 #SS 

BORAL BRICKS 

====~=====~=~=~====================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last chang.ed 

EO Seq. Line 

Mr Burns Location 

10/1/2010 8:13:01 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

10/4/2010 9:26:06 AM by IGG 

(modified after loading) 

7 

1 

r--- - . A-DC fA-: "AD-c·f-C'HAf\iNEL- X"{U:WfPCC20T6-Q4\MR BORNS\bA t-A\OC'RHPLC53PG98\006-0701 .D) 

· uS/em l 

I 

180 -=1 

1 

:::~ 120-

100-

80 

60 

" "' '§ 

~ 

u: 

N 

21 

"' . 

:g " 

0 

:c 

(.) 

External Standard Report 

============================'=""===============================""=====,,= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AM 

1. 0000 

1. 0000 

Use Multiplier & Dilution Factor \oJith ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

3.105 BB 75.83907 1.69672e-2 1.28678 Fluoride 

4.255 BB 89.04053 2.69605e-2 2.40058 Chloride 

'Totals : 3.68735 

*** End of Report *•* 

Instrument AircWctJ.E£<HJl> ll-1ilf.!.212 AM IGG E~~~~~~9s~~o~~~~T ?~ °}E~~2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE~488 1 of 1 
Sample Name: HPLC53pg98 #SS 

BORAL BRICKS 

====~================================================================ 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis t1ethod 

Last changed 

EO Seq. Line 7 

2 

==========================================·-=====,===-·======--=========== 

External Standard Report 

==============•-"====================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:26:06 AI~ 

1.0000 

1.0000 

use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL} 

-------l------l----------l----------l----------l--l------------------

3.109 BB 75.80476 1.69671e-2 1.28619 Fluoride 

4.259 BB 89.01553 2.69607e-2 2.39992 Chloride 

Totals : 3. 68611 

====:============::o~===;.co"-'==""""================="-"=<==~·"·"'"'-'~==-c=======""======== 

*~* End of Report *** 

10b41 o g 28 EA#0910-96 Page 162of202 

InstrumentAtC PR JEi:f~o. P-ioH:i 20 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Paqe 1 of 1 

APPENDIX PAGE NO. 489 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

======================~=======================~====================== 

Acq. Operator EO Seq. Line 17 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 12:19:37 AM Inj 1 

Acq. Hethod C: \HPLC2 010Q3 \HR BURNS\HETHODS \t-!ETROHH .H 

Last changed 4/l/2010 4:15:36 PH 

Analysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98 .M 

Last changed 10/4/2010 9:39:38 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U:\HPLC2010041MR BURNS\OATAiOC'f\HPCC53PGSBi1DD--:fio1:0)-··-····- ·-----1 

uS/em l i ;::! :::j 1 ,I 

140 

120 

===================================================================== 

External Standard Report 

===•====::::-"":<"C;:::~-,..=~-::==::...--:,-:::..""O~"======"'"•================================::::::::::::::::::::=::::=:::::::: 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNE'.L A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/crn*s] [ug/mLJ 

-------l------l----------l----------l----------l--l------------------

3.115 BB 305.79456 1.70644e-2 5.21821 Fluoride 

4.253 BB 183.50085 2.66068e-2 4.88237 Chloride 

Totals : 10.10057 

===================================================================== 

*** End of Report *** 

"nstrument l 10/4/2010 10:05:55 AM IGG EA#0910-96 Page 163of202 

I 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT Page 1 of 1 

APPENDIX PAGE No. 490 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 
Sample Name: HPLC53pg98 i3 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 17 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 12:31:57 1\M Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

.~nalysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98. M 

Last changed 10/4/2010 9:39:38 AM by IGG 

··-·A.ocTA;"i\6C1 cRA."ffNECA"(ul"H?Itzo·'=,::Coa;c4"1"M~R"BC'uf.oR"N;;S;:o\D~A"T'"'A'"Io"'c"'T"'I"H"PL"c"s'"3"'P""G~9~8\ 1D"'o~-1~7'"o~z•.o~)---

uSfcm l ::l 

"l 

'i 

i 

I 

! 

================================~=::::o.:o=""""'============================== 

External Standard Report 

========================================================="""""'"="'~======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

Ret.Time Type Area Amt/Area Amount Grp Name 

[min] [uS/crn*sJ [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

3.115 BB 305.05637 1.70643e-2 5.20559 Fluoride 

4.254 BB 182.77678 2.6608le-2 4.86334 Chloride 

Totals : 10.06893 

*** End of Report *** 

IGG EA#0910·96 Page 164 of202 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~~\1°491 1 of 1 
Sample Name: HPLC53pg98 i3 

BORAL BRICKS 

==========================''"==:<:·===""=====""""=========""================== 

Acq. Operator EO Seq. Line 29 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 6:45:00 ~I Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/l/2010 4:15:36 PM 

Analysis Method U: \HPI,C2010Q3 \MR BURNS\METHODS\HPLC53PG98 .M 

Last changed 10/4/2010 9:39:38 AM by IGG 1 Aoc1 A. Aoc' cHANNEDqrr>H-rcc2oToo4\MifiiFRfJs,oiltAiocnfii'l."cs:lPG9s\1oo.29o1 01 

' uS/em j 

180-j 

160 j 

j 

140 ~ 120 j 

~ 100~ i 80~ 

1 

60 -l 

4 

40~ i ~ 20i ~ ~ N 

0 t:--~J ... _ ,r 

2 

========,:=====:'='====================='"·===~.,============================== 

External Standard Report 

===============-==================:========================:====.o..,====== 

Sorted By 

Calib. Data t1odified 

Multiplier 

Dilution 

Signa 1 

10/4/2010 

1.0000 

1.0000 

9:36:48 A~1 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/crn'*s] [ug/mL] 

-------l------!----------!----------!----------!--l------------------

3.117 BB 305.44266 l.70644e-2 5.21219 Fluoride 

4.257 BB 183.08054 2.66076e-2 4.87132 Chloride 

Totals : 10.08352 

*** End of Report *** 

InstrumentAk ~~6.1!f&flil.9 plilJ~~p: 14 AM IG~p;~C~ g~~gN~~~~ !~~J~~~z AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEfN>9'492 l 0 f l 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

Acq. Operator EO Seq. Line 29 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 6:57:20 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/l/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3 \MR BURNS\METHODS\HPLC53PG98. M 

Last changed 10/4/2010 9:39:38 AM by IGG ;-··--··-----Ai5C1--Ii~ADCTCHANNELA(UIHPLi"czi.o,:;1;;0"0""41C:Mi;'R;,B,;;U7,R"Ni.s'i\D;iA~T"A"'I"O"c"'n""H"'P""LC"s'"3"P"G'-'9"'81'"'1"00""·""29"o'"zc-,.D""J~~~~~..., 

i uS/em-~ ~ 1 

180-1 

160~ " 

" "0 

-~ 

0 

~ 

u: 

" "' 0 

E 

{.) 

---~-6-----··-----~-8 ___________ 10 

External Standard Report 

====:========================================================~======= 

Sorted By 

Calib. Data Modified 

Nultiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] fuS/cm*s) (ug/mJJ] 

-------l------l----------!----------l----------!--l------------------

3.116 BB 304.76215 1.70643e-2 5.20056 Fluoride 

4.257 BB 182.93237 2.66078e-2 4.86743 Chloride 

Totals : 10.06799 

===============================================""'====;;-'"""='-"'""•'='"====::-..:=====-

*** End of Report *** 

IGG EA# 0910-96 Page 166 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'me 493 1 of l 
Sample Name: HPLC53pg9B #3 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 41 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 11:40:56 AM Inj l 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHH.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed 10/4/2010 9:39:38 AM by IGG 

1··· .. _ .......... ADC 11\:-Aoc f CHANNELA (U:IHP"'L"'c"2o"-1;;;o:r;a""41ii-Mi'cR;,Boiu"iiR'"N"'s"''"o"AT"'A;;;\"o"'c"'T"'IH"'P"L"c""s3"P"G"9"a"' 1"1"o.'471 o"-1".o"'),.-

us/cm l I 11; 

1ao ~ I ~ 

160 

140-

120 

100 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1. 0000 

I , 

I 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEI, A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.129 BB 305.45007 1.70644e-2 5.21232 Fluoride 

4.268 BB 183.04117 2.66076e-2 4.87029 Chloride 

Totals : 10.08261 

*** End of Report *** 

Instrument ArcWo'!if:e9W.. f1_q 0Jl4!2' so AM IGG EA# 0910-96 Page 167 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 
( 

Sample Name: HPLC53pg98 i3 

80RAL BRICKS 

Acq. Operator EO Seq. Line 41 

Acq. Instrument Mr_Burns Location 

Injection Date 10/2/2010 11:53:15 AM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\HETHODS\HPLC53PG98.!-l 

Last changed 10/4/2010 9:39:38 Al-l by IGG 

ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q41MR BURNSIDAfAIOCTIHPLCS3PG98\1\64i02~D)·-···- ······-··--, 

uSicm l 

180 j 

160 

140 

120 

100 

I 

i 

i 

==========,=============""'""""======""""-"=================================== 

External Standard Report 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution :~:~actor wi·th ISTDs 

Signal 1: ADCl A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

{min] {uS/cm*s] {ug/mL] 

-------l------l----------l----------l----------l--!------------------

3.119 BB 304.57260 1.70643e-2 5.19732 Fluoride 

4.259 BB 182.35q86 2.66089e-2 4.85226 Chloride 

Totals : 10.04957 

===:==========================="'-'""'=,..,==-=========::=c:==""==================== *~* End of Report *** 

InstrumentA-fcf>\ll6Uil-Jl/.J9. p.9o,C4~: 00 AM IGGEP~gRo~J:;;~I~:T~SeT~~~~g~2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGf¥~ij.'l\gs 1 of 1 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

Acq. Operator EO Seq. Line 53 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 5:36:34 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

Last changed : 10/4/2010 9:39:38 AM by IGG 

ADC1 A,- AoC1c8Ai~fNET-A(iJ:\HPLC201 OQ4H~Ff BURNS\DAT A\OCT\HPLC53PG98\11 0·5301.0) -------------- --~-1 

us:::~ ;1. ] 

1601 ! 

140 ·j '

120 -l 

100 --=1

1

.: en - :g J g ~ 80-J u: g 1 ~ 

soj ;; o 

40~ M ~ ~ /'', .:f 'It 0 CD 

20-:t ~ l \ f'; c; O 0? ~ I 

.., ~ j\ /1 ";!:_ c0 CD cci j ! 

1

-! ______ ;c:! J ' I \ ll> ...--~, /....,____ • ; 

o , ·-j --- -..:~·--;.::.~~.:,::::.c:;...=.:~-~-t:~.-r:.: ---~~-=·:,:._-:-____:;::::.c~=::::::.:_t::~ . .:--~-,-----,---.----.------, ---,----! 

'-------··£ ___________________ :1______ 6 ______________ § ________ 1_0 ----------·-········--l?. ... _____ ~ 

==================================================:==.,=======::-:o======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 

1.0000 

1.0000 

9:36:48 AM 

Use Multiplier & Dilution !?actor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.121 BB 306.69925 1.70645e-2 5.23367 Fluoride 

4.260 BB 183_57710 2.66066e-2 4.88437 Chloride 

Totals : 10.11805 

*** End of Report *** 

IGG EA# 0910-96 Page 169 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~"M\e 496 l of l 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

Acq. Operator EO Seq. Line 53 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 5:48:53 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BORNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

1\nal ys is Method U: \HPLC20 10Q3\MR BURNS\METHODS \HPLC53PG98. M 

Last changed 10/4/2010 9:39:38 1\M by IGG 

ADC1 A. ADC1 .CHANNELA"(U'IfiPTC20filQ.i\MRBURNS\DATAIOCT\HPLC53PG981 110-5302D) 

uS/em --1 

1801 

160 -i 

i 

140 -j 

120 ~ 

100 ~ ~ 

0 

~ I 

I 

External Standard Report 

--==·==========::::=-============:o===:::-·======================================= 

Sorted By 

Calib. Data Modified 

Multiplier 

Signal 

10/4/2010 9:36:48 1\M 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: 1\DCl A, 1\DC1 CHANNEL 1\ 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] (ug/mL] 

-------l------[----------l----------l----------[--l------------------

3.120 BB 305.72400 1.70644e-2 5.21700 Fluoride 

4.261 BB 182.98579 2.66077e-2 4.86884 Chloride 

Totals : 10.08584 

=================,=================""============::::=.:========='='====="'=""== 

*** End of Report "'** 

~ 1.Cl64.12.m.n.:JCl.·.no 18 1\M IGG EA#0910-96 Page170of202 Instrument AtC l"r< J~CrNo. t"'M~Z: EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGe'iil\1"497 l of 1 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

===============================================~=================~=== 

Acq. Operator EO Seq. Line 65 

Acq. Instrument Mr Burns Location 

Injecti.on Date 10/21201011:32:07 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method O:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M 

La_s_t_ .. changed 10/4/2010 9:39:38 ~.M by IGG 

ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6501.D) 

us:::i ~ 

160.1 .I 

140--! 

~ ! 

120 '~. ' 

~ \ 

100--i 

J ! 

80 -i 

' 

===================================================================== External Standard Report 

==========o~=""==""==-~==.,,..,========"-"=================::o::==================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1; ADCl A, ADCl CHANNEL A 

RetTLme Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--1------------------

3.123 BB 310.41275 1.70649e-2 5.29716 Fluoride 

4.263 BB 185.78922 2.66027e-2 4.94249 Chloride 

Totals : 10.23965 

===================================================================== *~* End of Report *** 

EA#0910-96 Page 171 of202 

IGGEPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~'I-£e498 1 of 1 
Sample Name: HPLC53pg98 #3 

BORAL BRICKS 

Acq. Operator EO Seq. Line 65 

Acq. Instrument Mr Burns Location 

Injection Date 10/2/2010 11:44:27 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis l~ethod U: \HPLC2 010Q3\MR BURNS\METHODS\HPLC53PG98. M 

Last changed 10/4/2010 9:39:38 AM by IGG 

~-----~------AoCTA.-A.bc 1 CHANNEL A {U:\HPLC2o f064\Mi3R'sii'uilR"Ni.s3i,iio:i;A"T"A"Io"c~n=H"P'Lc""s3"P"'G"9"'a"'"'2"o"-6"'s"o'"2'.o"l--------·-~ I t 

I us::l ~ I 

:::·l II I 

120..:] 

~ 

100-~ ~ ll -~ ru 

M~ ~ ~ ~ G: ~ 

sol ~ u 

40--_-l 0") Ng_ I 

1

l ,.... ;'\ v- v- I 

20 ~ f i r\ g '"": ~ ~ I i 

0 J.:=-,=~--~-__: __ ~-~-~~:: .. _:_.:_-,~L:::.-.=-~_-··--_·_' ~~_,,_-~_--,-~---"_-.,.'-.1 /_"_ .._·-_._·-~~ .. "---/-~~----:~--'_1__._._-·T· i ___ I ~- · · ··--·-r----..,..--·-i 

---------------------2 __________ 4 ______________ 6__________________ 8 -----~----~~~ 10 12 mi' 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/4/2010 9:36:48 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal l: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area f~t/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------l------)----------)----------!----------1--l------------------

3.122 VB 310.73752 1.70649e-2 5.30271 Fluoride 

4.263 BB 186.29073 2.66018e-2 4.95567 Chloride 

Totals ; 10.25838 

*** End of Report *** 

IGG EA# 0910-96 Page 172 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGEN\!e499 1 of 1 
~~=~~=""=====~=~~=~~~~~================~==!lQm!l~==~============== 

Calibration Table 

============~============~===================~======================= 

Calib. Data Modified 

Calculate 

Based on 

Rel. Reference Window 

Abs. Reference Window 

Rel. Non-ref. Window 

Abs. Non-ref. Window 

Use Multiplier & Dilution 

Uncalibrated Peaks 

Partial Calibration 

Correct All Ret. Times: 

Curve Type 

Origin 

Weight 

Recalibration Settings: 

Average Response 

Average Retention Time: 

Calibration Report Options 

10/5/2010 9:18:49 AM 

External Standard 

Peak Area 

10.000 % 

0.000 min 

10.000 % 

0.000 min 

Factor with ISTDs 

not reported 

Yes, identified peaks are recalibrated 

No, only for identified peaks 

Linear 

Connected 

l,inear ( Arnnt) 

Average all calibrations 

Floating Average New 75% 

Printout of recalibrations within a se~uence: 

Calibration Table after Recalibration 

Normal Report after Recalibration 

If the sequence is done with bracketing: 

Results of first cycle (ending previous bracket) 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Lvl Amount Area Amt/Area Ref GLp Name 

[min] Sig [ug/mL] 

-------l--1--l----------l----------l----------l---l--1---------------

3.149 1 1 2.00000e-1 9.95712 2.00861e-2 Fluoride 

4.153 1 

2 1.00000 61.11817 l.63617e-2 

3 5.00000 308.63791 l.62002e-2 

4 10.00000 589.09669 1.6975le-2 

5 15.00000 849.33438 1.76609e-2 

1 2.00000e-1 5.66901 3.52795e-2 Chloride 

2 1. 00000 33.68365 2. 96880e-2 

3 5.00000 182.2.7121 2.74317e-2 

4 10.00000 369.59518 2.70566e-2 

5 15.00000 562.35474 2.66736e-2 

='-~"'---"o===,·==o:'=='""==""====='''"""''="''================~====='""-'=:;o;=;;;;::::============== 

Peak Sum Table 

***No Entries in table*** 

==============================:o---'-"'"=""=.·.oo===============,-===:oo=:=:=====-=~===== 

, EA# 0910-96 Page 173 of 202 

IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGJ!'!'lS.E$00 1 of 2 
~~~~~~~~~~~~~~~~~~~~~-~~~~~~~~~~~~~~~~~~~~-~~l~~~~~g======~~~====~--~ 

Calibration Curves 

'ft:ffiaT----------------------~r/l 

500~ / 

400- // 

k 

300 ////

4 

200-- _y/ 

/ 

100' / 

2/ 

,,;.f- 0 -------,----~------.--·---,---.------,---·,-·i 

0 10 i 

______ _i_A\[m!)!OQ!Uill]nl[yg/miJ__ _________ _______ ! 

Fluoride at exp. RT: 3.149 

ADCl A, ADCl CHANNEL A 

Correlation: 

Residual Std. Dev.: 

Formula: y = mx + b 

m: 58.36617 

0.99933 

18.30415 

~: -5.76052e-1 

x: Amount 

y: Area 

Calibration 

Level 1 

Level 2 

Level 3 

Level 4 

Level 5 

Level Weights: 

1 

0.2 

0.04 

0.02 

0.013333 

Chloride at exp. RT: 4.153 

ADC1 A, ADCl CHANNEL A 

Correlation: 0.99993 

Residual Std. Dev.: 3.24460 

Formula; y = mx + b 

m: 37.31718 

b: -2.14447 

x: Am.ount 

y: A.rea 

Calibration Level Weights~ 

Level l 1 

Level 2 0.2 

Level 3 0.04 

Level 4 0.02 

Level 5 0.013333 

-:==::.::=======""-<".::=•:============================================""========== 

Instrument A'rCJMt:JiJE{;i;:t.Jl, Fl-~oil\24 9 AM I GG EP~g,n~?s~?or.\'~~MJ~o~~~~z AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGieii{J>e501 2 of 2 
Sample Name: HPLC53pgl00 #1 

BORAL BRICKS 

Acq. Operator EO Seq. Line 2 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 2:22:30 PM Inj 1 

Acq. Method C: \HPI.C2 010Q3\MR BURNS\METHODS \METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed 10/5./2010 9:16:05 AM by. IGG 

uS/em J ADC1 A. ADC.1CHANNETA(iJWPLC2010Q4\~1RBURNS\DATAiOcnHPLCS3PG1DO\ooT:o2oT~---· --·1 

180. ! 

160 

140-

120-

100 . 

80 

60. 

40 

20 

0 

External Standard Report 

==:;::======================================·=========::===::.:========="'"·""==== 

Sorted By Signal 

Calib. Data Modified Tuesday, October 05, 2010 9:15:59 AM 

Multiplier 1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTirne Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------!----------l----------l--l------------------

2.990 MM 9.55972 1.80226e-2 l.72291e-1 Fluoride 

4.157 BB 5.61364 3.70342e-2 2.07896e-1 Chloride 

Totals : 3.80187e-l 

===============================================:·===-,========""=======::::== 

*** End of Report *** 

~ 1.JlL~L2!l n .r; J.<' EA# 0910-96 Page 175 of 202 

Instrument AtCt'I<U;ltot: r No. l'"-iiJ1"2 41 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI!'fi0e502 1 of 1 
Sample Name: HPLC53pgl00 #l 

BORAL BRICKS 

================================-=====,==============================·'= 

Acq. Operator EO Seq. Line 2 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 2:34:50 PH Inj 2 

Acq. Hethod C: \HPLC2010Q3\MR BURNS\HETHODS\METROHM.M 

I.ast changed 4/1/2010 4:15:36 PM 

Analysis Method U: \HPLC2010Q3 \MR BURNS\METHODS\HPLC53PG100 .l'l 

Last ~hanged : 10/5/2blO 9:16:05 AM by IGG 

~-------·----p,ocTA,-Ai5cTcRii"NNEL A (U:IHPLC201 004\MR BURNS\DAT AIOCTIHPLC53PGfOD\D0-1 -02ifi:i5j-- . -- ··- ---- ·1 

"::j 

:::, 

100-

80 

60~ ~ ~ ~ g ..c 

40 -~ fL (_) ~.~' I 

i N "'C!:f ~ C'\1 ~ ES· i ; ! 20-j N 0) i ..- ,§> V 1 l ____ -0 j =-·=--c~~=~::-~:=~-=~;.:!t' -~ ~-- ~----~=:·----~ . ""[~~_::'"-~-~~-=-~· ·,;;;_ 

===========:::::============-=:.===::-~=-=============================·===~-"="=""==:= 

External Standard Report 

=================================================================== ... == 

Sorted By Signal 

Calib. Data Modified 

Multiplier 

Tuesday, October 05, 2010 9:15:59 AM 

1.0000 

Dilution 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area &~t/Area Amount Grp Name 

[min] !uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--!------------------

2.985 VB 10.01584 1.80226e-2 1.805lle-l Fluoride 

4.150 MM 5.87644 3.65764e-2 2.14939e-1 Chloride 

Totals : 3.95450e-l 

=====================-==-e==-===~~"'c~==============================''""""-'='-""'=="' 

*** End of Report *** 

Instrument A:tc:W~dill~~na 1'-lil-fll255 AM IGG EP7,~grf~~?s~forf-i'~~N~o5~~~2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~<Ni>e503 1 of 1 
Sample Name: HPLC53pgl00 #1 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 14 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 7:38:19 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/203.0 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed 10/5/2010 9:16:05 P~J by IGG r --· --·-ADCTA-;-Abci"·CHANNEL A (Uc\HPLC201004\MR BURNS\DATAicicTiHPLC53PG100\001·1401.D) 

uS/em l 

180 1 

l 

; 

160 __:~ 

140.1 

l 120....! 1 

100 -~ ·i 

< 

80 ·: 

=======================-~===================~.,========================== 

External Standard Report 

========~.=o~===,===================:=:::============''"============='========== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, 

1. 0000 

1. 0000 

October 05, 2010 9:15:59 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Arnt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------j----------l----------l----------l--l------------------

2.991 MM 10.05413 1.80226e-2 1.8120le-l Fluoride 

4.154 BB 5.65120 3.6966le-2 2.08903e-l Chloride 

ToT:als ; 3.90104e-l 

===~'~-,=="""='==--==-==========""·:oo-.======================-c=======,===o.:o""========== 

*** End of Report *** 

EA# 0910-96 PaQe 177 of 202 Instrument Alrclffidi.JE?;lf+Jl,. ~-1ef4~l O AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIXPA~504 1 of 1 
Sample Name: HPLC53pg100 #1 BORAL BRICKS 

================================:=================~================== 

Acq. Operator EO Seq. Line 14 

Acq. Instrument Mr_Burns Location 

Injection Date 10/4/2010 7:50:38 PM Inj 2 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis .Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100 .M 

Last changed 10/5/2010 9:16:05 AM by IGG 

ADC1 A. ADC1 CHANNEL A (U;\HPLC2010Q4\MR BURNS\DATA\0CTIHPLC53PG1001001·1402.D) 

uS! em 

180 

160 

140 

120 ~ 

===========================================================~========= 

External Standard Report 

=====;=============================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, 

1.0000 

1. 0000 

October 05, 2010 9:15:59 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/ em's] [ug/rnL] 

-------l------l----------j----------l----------1--l------------------

2.989 VB 10.19880 1.80226e-2 1.83809e-1 Fluoride 

4.153 MM 5.53477 3.71800e-2 2.05783e-l Chloride 

Totals : 3.89592e-l 

====,=========""'=·"-'======o-.===::-..o======~===========:======================== 

~** End of Report *** 

Ins trumentAtC )?~O'li!~ili116. Pl-101'422 5 AM IGG EP~~!R ~Jif~1~J'i'E'!fT VR~~~~~z AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIF~0~05 1 of 1 
Sample Name: HPLC53pgl00 #2 

BORAL BRICKS 

========================================================~============ 

Acq. Operator EO Seq. Line 3 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 2:47:11 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\~lETROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis t<lethod U; \HPLC2010Q3 \MR BURNS\METHODS\HPLC53PG1 00. M 

Last changed 10/5/2010 9:16:05 AM by IGG 

- --~-Aoc1A.ADC1CHANNELA (U \HPLC2010Q4\MR BURNS\OATA\OCT\HPLC53PG100\002-0301 Dll 

uS/em ~ I g 

18o, l I I 1 

160] I 1 

140 .: I II 

j i i 1201 I I: 

1oo.J 1 II 

1 l i 

80. 

60 

-1l 

~ 

' il 

I] 

I' 

I ~ 

(J i 40-_ v ~ ! 

\i 

i 

l

l 20 R ;:: ~ ~ ~ ~ ~ ! 

-~ ~ ~ '<t ll) <ci 10 . ;------·--~-- ·- _) 

---

o ~--_--___ -__ -_,.,·_-_'_= ____-_-__ -_~_--___ -_~-.:~ .. -~- -----'-'--,-_-'-_-0--_ __ ~-'-----~----. --------1:::::-1~~ ----i-~-r.=-.-....-- -.:------r-· "-...:.:---''-'--··',c__~-~, 

-"·---------'6'---- -·-----·-··----------------------~--------------.-------.l!!!.D: 

External Standard Report 

=====""·""'=":::::::=;==~======-===================='='===================~======== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area &~ount Grp Name 

[min] [uS/em's] [ug/mLJ 

-------l------j----------l----------]----------l--l------------------

3.114 VB 62.22894 l."l2918e-2 1.07605 Fluoride 

4.258 BB 34.35212 2.84702e-2 9.78010e-l Chloride 

Totals : 2.05406 

=<"-'·~-"'~'·"'"·=='-""'~~====~..,==============""~"'="'-~====:=================;o==>"~"'-·=========== 

*** End of Report *** 

Instrument M-clfiRf<yJ&tW,_ t9-~il¥4219 AM IGG EP~g~~~?s~?o~¥~~TV~o~fE~~2 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGI!iffiJe506 1 of 1 
UdLd J:: .l-.J.!:c! u; \flrL1...-£.U.J.UI,('i \lvlr\ DU.t'\LV;:l \Ul"\..1-l"\.\VI...-.1- \Dr.Lti...-:..I..Jr>.:~.J.UV \UVo<:.-U.JVo<:, ,,u 

Sample Name: HPLC53pg100 *2 BORAL BRICKS 

Acq. Operator EO Seq. Line 3 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 2:59:30 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed : 10/5/2010 9;16:05 AM by IGG 

I

.------·--·-ADC1 A. ADC1 CHANNEL A (U:IHPLC2010Q4\MRElURNSIDATAiOCTif·iP-LC53PG100\002·D302.D) . -·-·;::~·. 

uS/em "J :::= .1 

i 180 l 

1 1601 ! 1 

! 140 ~ 

1

. i 

I

I 1201 :I 

100 ··1 1 i -~ ! I w~ .. 

60 l ~ !, .... _,· \1' 

40 ···, 

' "' 

2

: 1_-=_:_.:_-£~·-· -~--__ -_-___ J'_.~_··~_- ,-~}:·_~·~~-~":.~~~~~1~~~-:::~--_ _ _-~_r_J, ~~~-~!.:::d 

External Standard Report 

============""========================================-·=~============== 

Sorted By 

Calib. Data Modified 

Multiplj_er 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTOs 

Signal l: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min} [uS/cm*s] [ug/n:L] 

-------l------l----------l----------l----------l--1------------------

3.115 BB 59.91656 l.72979e-2 1.03643 Fluoride 

4.257 BB 32.97707 2.85399e-2 9.4ll63e-l Chloride 

Totals : 1. 97760 

==""""============''""-"'-"''""==.:=.::====""""'""'""='==========o:========~""=""·""'~==="-"'-""======== 

~** End of Report *** 

InstrurnentAICPRPgllClJIIJB. Plt01fU28 l\11 IGG EP~gRO~Jfl;§~~N£eT ~SR~~te~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGIFNO.e507 l of 1 
.... - ~--- -- -. ·---. ------- '-· --.. '--- , ... ~~ ~ ~. ~~ ~ ... '.......... .... _, ....... ...., 

Sample Name: HPLC53pg100 #2 

BORAL BRICKS 

===================================================================== 

Acq. Operator EO Seq. Line 15 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 8:02:58 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed 10/5/2010 9:16:05 AM by lGG 

ADCTA. ADCf"CHANNel A (U:\HPLC201004\MR BURNS\DATA\ocnHPLC53PGT60\0o2-151)f"6) __ _ 

uS~:l ~ 160- i 

I! 

l! 

140 j l \ 

120] 1 i 

100 ' " -=1 !i 

80~ ij 

:g "'

g 

u: 

' 

20 ~- ~ ~ f6 ~ ~ ~ j ..f ~ :ri :=6 : / _,N_.. J_::c:,_ __ ... _l ___ L/':'-..__ __ ,------------,j_ --··+---···--+------- ,----'---- r.J ..... / ............ . 

0 ~-~----------.....-- --.------r-----------, ..---------,---------~--------

L_ ___ , ·----.. L_________ 4 .... _ .. ____ .§_....... • .. § ___ ·---..... - .• ml 

========================~=============~============================== 

External Standard Report 

===============================~=======================~=========~=== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with IS'l'Ds 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTirne Type -~rea Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/rnL] 

-------J------J----------1····--·-··I·········-J--I-·----------------

3.118 VB 62.23907 1.72918e-2 1.07622 Fluoride 

4.267 BB 34.30110 2.84726e-2 9.76643e-l Chloride 

Totals : 2.05287 

=============~='""''"'==o-o====o:..·=""=======================""'==============-:.::::o'"'""= 

*** End of Report *** 

!nstrument JilrcW~.ill-JNh. fi; 1J7,;~7 AM IGG El~\~g~L~s~~o~~~~T ~~c\'Mc~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~ 508 1 of 1 
lJdLd EJ.-1-t:::: u; \C"l.L.UV£..UJ.U\,.o!"t\1.U'\ UVnL'fU\LI.l>.J.r'>.\VVJ. \U.I.J..J'-'JJJ.U.I-VV\UVL. .t.JU<...,._., 

Sample Name: HPLC53pgl00 #2 BORAL BRICKS 

Acq. Operator EO Seq. Line 15 

Acq. Instrument Mr_Burns Location 

Injection Date 10/4/2010 8:15:17 PM Inj 2 

}\cq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed 10/5/2010 9:16:05 AM by IGG ----------AoC1-;\.ADCTi5'flAi{~iEL A (U \H',:,.P;i-L;iC;i;20oi;1;i;Oi;Qc;c4\;'.M;,R;-B,;iUC;iR~N,O:S\~DC.A"TA"I"'O"'C"'n"H"P"L"C 53;;Po;Goc:1"0"'0ID=o2"'· 15"0"2"'.D) 

External Standard Report 

=====================""===================================,.~===<======== 

Sorted By 

Calib. Data Modified 

Hultiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

l. 0 000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type P..rea Amt/A:r·ea Amount Grp Name 

[min] [uS/ern's] [ug/rnL] 

-------l------l----------l----------l----------l--1------------------

3.119 BB 60.08810 1.72975e-2 1.03937 Fluoride 

4.268 BB 33.10430 2.85332e-2 9.44572e-1 Chloride 

Totals : 1.98394 

*** End of Report *** 

Instrument A!C ~II'C1l1>16 l!l-Hlfll24 6 AM I GG EP't'}~RO~~Ps~tbJ-fl!\;'\ \>!!fo9tt~2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGH'akje509 1 of 1 
( 

Sample Name: HPLC53pgl00 #3 

BORAL BRICKS 

Acq. Operator EO Seq. Line 4 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 3:11:49 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROH~l. M 

Last changed 4/1/2010 4:15:36 PM 

Ana1ysi.s Method O:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG10D.M 

Last changed 10/5/2010 9:16:05 AM by IGG 

r

em l ADC1 A, ADC1 CHANNELA(tT\HPLC2tH004iMR BURNS\DATA\6cfiHPiC53PG1iio\Oo:i:o4oij:i)----

1

- ~.· l 

80~ l ql 1 I I I 

1so 1 : ; I 

I 140i 1 ! 1 

· 120 • I , ; ,OJ ~ i II 

1 ·g <1l J I 

80 J :;, "C !_' d 

u:: § I 'I 

60- ' :c \! ~ (,) j 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

E.xternal Standard Report 

Signal 

Tuesday, 

1. 0000 

1. 0000 

October 05, 2010 9:15:59 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

Ret'Iime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------:----------l--l------------------

3.123 BB 308.96735 1.71652e-2 5.30347 Fluoride 

4.252 BB 182.23886 2.71126e-2 4.94098 Chloride 

Totals : 10.24445 

*** End of Report *** 

InstrumentAtC~Ei:~N~. ~11Hl!253 AM IGG EP~RO~~?s~rb~f~gT~ Jo3~~~z AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE<Nll~510 1 of 1 
Sample Name: HPLC53pg100 #3 

BORAL BRICKS 

=============~=================================~===================== 

Acq. Operator EO Seq. Line 4 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 3:24:10 PM Inj 2 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM. M 

Last changed 4/1/2010 4:15:36 PM 

P.nalysis Method U: \HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100 .M 

~ 

Last changed 10/5/2010 9:16:05 AM by 1GG 

ADC1 A, ADC1 CHANNEL A (U:\HPLC.2(ff0Q4\MR BURNS\bATA\OCT\H?lC·5-iPG100\0(f:f-0462.D)-----.-~ 

' uS/cml / ;t/ 

1aoJ i ~I 

160j J . 'I / I -1 I I I 1 I I I 

140~ ' :II .l i 

120 1 1 

r 

100~ :g 4) \1' 

so-j g :g ~- u:: 0 \i j I E !j 

60---l ~ 0 \i :j IJ 

40 -~ (') ;n I i' ~ ,1\ ~ ~ I I, '\ tO ;'6 ::1, C'; 20 ..:j t-- ; , i' tn o ~ v 1

> I j C\! !·. 1\ ~ lci tO cci i 

0 t::.-=~=~::;=:'~:~C.-:;:=_-1 __ ==~~T '_c":~ I ~~=~~-=' ~ --·. ~~ -~?:.==- ~-~----J 

=====================================,=============================== 

External Standard Report 

=======o:·==::-===""'==============================~'-"'====================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1. 0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADC1 CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------j------l----------l----------!----------j--j------------------

3.123 BB 308.16321 1.71652e-2 5.28970 Fluoride 

4.251 BB 182.15358 2.71128e-2 4.93869 Chloride 

Totals : 10.22839 

==========================,.=============""'""'""·~'"'=""'"""-====================== 

*** End of Report *** 

'-""-'- L ~ EA# 0910-96 Page 184 of 202 Instrument AtC~CliJtC~W..I'l.~~-fli~Ol AM hG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PA~'Nl#511 1 of 1 
UCl'-Cl 1: ..L..l.O:::: v ~ \nr-.wv.:. V..lU\,!~ \t"J!"\ DUl"'-l>t.;:> \LIM..J.J-1. \U"-.l. \ttt'LI....:J.;)t'b.LUU \UU.;)-1.\::IUJ_. U 

Sample Name: HPLC53pg100 #3 

BORAL BRICKS 

===================================================================::= 

Acq. Operator EO Seq. Line 16 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 8:27:38 PM Inj 1 

Acq. Method C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

Last changed 10/5/2010 9:16:05 lili by IGG ----·~--·--ADC1A.-A1S'C1CHANNEL A (U:\HPLC201 004\MR BURNS\DAT A\ocT\HFi[C-s3P-G10moo3-1G01. ~------·-··-·--~., 

uS/em -j :55 I 

-i cq I 180-j OJ! I -1 i· i 160 ..:j if 

! 1 ~ : ~ 140----j il !, 

1 . ' 

120--1 fi 

100j " \I 

aoiJ. ~ i \1.: 

60 ~ 8 ~ ;::; v 

::J ...... J _)\'--,-}\ __ ~"~+-~lj __ .. , .... J .... 1 ... I 

0 ' ---·-1--·----;--------. -- -----------·- ··..,-----~·---·"··-1 

----·- _______ ;L _____ , ___ ,,_, ____ ,_ .....:4'!.' ________ ,_6 ___________ j ·-·-------_!!11~ 

=========================::::===============================,,===~'""·"'"""=== 

External Standard Report 

========================================~~========================~== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 N1 

1.0000 

1.0000 

Use f"lu.lt::i.plier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/crn*s] [ug/mL] 

-------j------l----------l----------l----------l--:------------------

3.127 BB 309.30249 1.71651e-2 5.30921 Fluoride 

4.264 BB 182.42313 2.71123e-2 4.94591 Chloride 

Totals : 10.25513 

=============·======-===~,.-=:===·'====,===========================""'="'0"-~-~,.--=o~~==--=-

*** End of Report *** 

EA# 0910-96 Paqe 185 of 202 InstrumentAtc~ESlJMl. Pl1~-fll20 9 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGli'M!e512 1 of 1 
Sample Name: HPLC53pgl00 #3 BORAL BRICKS 

Acq. Operator EO Seq. Line 16 

Acq. Instrument Mr_Burns Location 

Injection Date 10/4/2010 8:39:57 PM Inj 2 

Acq. ~lethod C: \HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHDDS\HPLC53PG100.M 

Last changed 10/5/2010 9:16:05 AM by IGG 

ADC1 A." ADC1 CHANNELA(iJ:IHPLC2010041MRBUR"NSIDATAiOcnHPi:c53PGforiliio3:16oTBj-·--·-----~ 

oi 

180 j ~~ j 

160-=i 

1 

140 -~ 

j 

120 --i 

i 

100-.:l 

1 

-1 80 -_:! 

60 _.:) ' Ln 

j ~ M ~ 401 (D (\ ':}. U) g ~- "' 

20 -i ~ i \ t\ ~ (D ~ ~ 

0 ..jL __ ---.,.~_-__ £'J_ .._. ·,cr_-_-_ ..u __ / -_-_·'--~---..:•-::::::-.,.~_/ ___ \_.__ ____ ·..:•~_ .. -__ "_-_..:f_-_·~,---r-·=-_-._·-~--'-1 .. _-r---.._ ___ ···-·· _-_---"--'· ~ ___.....~,_,_ __ _ 

' ' i _ _..! ' __ 

I! 

II II II 

i!l 

' 

2 --·-··1··---~----------······---·-··!5-----~-----------.. ------------S!:-------~----------- mi 

===~=========~======================================================= 

External Standard Repoxt 

=========================================~=================~========= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sj [ug/mL] 

-------l------l----------j----------j----------l--l------------------

3.125 BB 308.11859 l.71652e-2 5.28893 Fluoride 

4.262 BB 182.26926 2.71126e-2 4.94179 Chloride 

Totals : 10.23072 

*** End of Report *** 

lnstrumentAtCl?~ffli!Ci:lli\Jo i>J.1d1fil216 AM IGG EP~gRO~J&-~~~J'fJ!,"T ~~ ~~~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGi!'M!e513 1 of l 
Sample Name: HPLC53pgl00 #4 

BORAL BRICKS 

==========~==~======================================================= 

Acq. Operator EO Seq. Line 5 

Acq. Instrument Mr Burns Location 

Injection Date 10/4/2010 3:36:29 PM Inj 1 

Acq. Method C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

Last changed 4/1/2010 4:15:36 PM 

Analysis Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PGlOO.M 

Last changed : 10/5/2010 9:16:05 A."l by IGG · 

---- Aoc-fA~i\i5CfcH'i.>JNECA(O'Iiii'l.c2oToa41tlRB0RNsloAT AIO"c"'T"'I"H"P"Lc"'s"'3'"P"G"1"'oo"IO"'o"4"·o"s"'o"1."'o") -----, 

uS/em 

180-

160 

140 

120 "' u "§ 

~ 

100 u:: 

=======o"'-==<=,-~=====================;;o=================================== 

External Standard Report 

====·""'====::==========================================""-'=""-'=============== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

Tuesday, October 05, 2010 9:15:59 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Fact.or Y.1 ith ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/mLJ 

-------l------l----------l----------l----------l--1------------------

3.135 BB 587.12793 1.7l500e-2 10.06926 Fluoride 

4.251 BB 369.45987 2.69528e-2 9.95800 Chloride 

Totals : 20.02725 

=e:======="'~'-"'=="'-'"======================================================= 

*** End of Report *** 

'ell."-'"~'" n -" '"- 2 4 G EA# 0910-96 Page 187 of 202 Instrument AtCffilXlttr NO. t'-1u1'12 AM IG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

~ I 

I 

I 

I' II 

\I 

1 

i 

mlf1 

APPENDIX PAG§'me514 1 of 1 
Sample Name: HPLC53pg100 *4 

BORAL BRICKS 

===================""'''"==""'=====-======================================== 

I 

I 

I 

i 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

180..: 

160 

140 -

120-. 

I

. 100c 

80 

I

I : 'N 

20' 

I 

0 ...... ~ <'oi 

~-----··----?.... 

EO Seq. Line 

Mr Burns Location 

10/4/2010 3:48:49 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPJ.C2010Q3\NR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

5 

2 

===========-======================~-"==,====""''"'===-:======-·====,.,=====-======= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/5/2010 9:18:49 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug(mL] 

-------l------l----------j----------l----------l--l------------------

3.149 BB 590.64954 1.71499e-2 10.12959 Fluoride 

4.265 BB 369.45181 2.69529e-2 9.95778 Chloride 

Totals ; 20.08737 

-----·--;·,.==-"'-=====-=================~~·="'"'=~-'-'-'''"'='"'"·"'"'0""'"'·== -'''""""·=='""'======""'=""===""= 

*** End of R~port *** 

Instrument AlrcJffi'cYJE£1ff.!6.!l.;efl4252 AM IGG EP~g~~~?s~fo~~~ZT ~~o~~E~~2 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

... 

i I 

l 

I 

\ 

APPENDIX PAG~Wies15 1 of 1 
Sample Name: HPLC53pg100 *4 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 8:52:17 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

17 

1 

ADC1 A. ADCTCFfi\NNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1701.D) 

uS/em ·j 

180 -1 

' 

:::1 

120 ·~ 

100 

80 

60 

40 

20 

External Standard Report 

===============================================""-====·"""=='--=="·:=:=====-====~·= 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

Signal 

10/5/2010 9:18:49 AM 

1. 0000 

1. ooco 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/A:rea Amount Grp Name 

[min) [uS/cm*s) [ug/mL) 

-------l------l----------l----------l----------1--l------------------

3.154 BB 587.89532 1.71500e-2 10.08241 Fluoride 

4.280 BB 369.70758 2.69527e-2 9.96463 Chloride 

Tot.als : 20.04704 

=================""====;o==========""==========='--o=•"·'-"'="''""=:;c;"'-'~======"'======== 

*** End of Report ** "k 

· · 'u<:.l.:>"' '·9 -" ~.q 1 7 EA# 0910-96 Page 189 of 202 Instrumen tAtC PKU;J~t n< . >"'ft!14:1 AM IGG EPA iCR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE'Ml"s16 1 of 1 
Sample Name: HPLC53pgl00 *4 

BORAL BRICKS 

===================-=======""=~-=====:::.:=================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

P.na 1 ys is ~1e thod 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/4/2010 9:04:37 PM Inj 

C:\HPLC2010Q3\MR BURNS\M£THODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PGlOO.M 

10/5/2010 9:18:49 AM by IGG 

{modified- after loading) 

17 

2 

~~-----AOCTA,-ADCl.cHANNELA{U:IHPLC2010041M-RBURNS\DATAii5CnHPLC53PGlo6ioo4:f7o2.15) _________ ·1 

I uS/em·: I g 

180 

160-

140 

<D 

120 '0 

15 

~ 

100 u: 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/5/2010 9:18:49 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1~ ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------t--l------------------

3.138 BB 590.71399 1.71499e-2 10.13070 Fluoride 

4.265 BB 369.76144 2.69527e-2 9.96608 Chloride 

Totals : 20. 096TI 

~=~================================================~====~============ 

+** End of Report *** 

L Ul.LS.L2m n " 1 o 2 8 EA# 0910-96 Page 190 of 202 

Instrument A1 C'PRUJ!ct;T NO. l"·lo-t'42 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

"' oi 

APPENDIX PAG~'N!>e517 l of l 
Sample Name: HPLC53pg100 #5 

BORAL BRICKS 

===================================================================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Jl..nalysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 4:01:09 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHN.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

6 

1 

(modified after loading) 

· · AocTil. ·Aoc T cFii\NNEi:A: (u:\HPLc2o1 oil•IM;~R;:;B;;;U:;:Rc,.;N'"S"I"DA'T'A"'I"ocrc"'T"'IH"'P"L"c"s3"'P"'G"1"oo""'lo"os"-a"6o.o"1'.o")------,, 

uS/em ·3 

180-j 

160 ~ ,'l 

140 _:J ·g 

120 ~ u:: J ,. 

100·-l :! 1 ,.; 

80 -i (\ 

:g "

0 

"' '-' 

J I' . /I 

60 ,• ', '\ 

j I l i\ M 

40 -~ ' 1 \ o\C ~ 0<-

~I 

1! 

II 

,, 

li 

i! 

'·I 

!i 

!I 

I• 

~ v I L I ..-U) !'.{) 

I 

2

: ~b~-;:: ] .. ;:-::-') \':-:;::= ) .~-;=_. . .c;-:::::.3 . }~_,_/\ __ .. , ..... ~A'-, ____ ). 

I 2 4 6 

I 

L _______________________ ------------------------------------···--··------------ 8 

===·==-~======="'"'===u=====""'==============================c;;.=============== 

External Standard Report 

~===========~========================~===================~=========== 

Sorted By Signal 

Calib. Data ModHied 10/5/2010 9:18:49 AM 

Multiplier 1.0000 

Dilutj.on 1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1' ADCl A, ADC1 CHANNEL A 

RetT.ime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.144 BB 849.68134 1.11448e-2 14.56764 Fluoride 

4.250 BB 562.55444 2.68995e-2 15.13241 Chloride 

Totals : 29.'70005 

*** End of Report *** 

1n.J.S.L?.IlHl 9 10 . __ 1 EA#0910-96 Page 191 of202 

Instrument AlrC'PRGJECT'Nl>. P-ior4'z- S AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

mi · 

APPENDIX PAG~'!-jl,e518 1 of 1 
( 

Sample Name: HPLC53pgl00 #5 

BORAL BRICKS 

=================================;==~==========================~===~= 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 4:13:29 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

6 

2 

(modified after loading) 

r---·---·--ADC1i\-:l\t5c1cHI\NNEL A (U:IHPLC20;1"0Q;<-4;;\;;M"'R"BC,:UfiR<.N"S"'ID'"A'"'T"A"'IO"C~T"I"H"P"LC""5'"'3"'P"'G"1"0o=\ooS:o6l5Hij-·· . ···--·-·- ··1 

~I .::qi 

~] 

~ 

"0 

·co 

0 

~ ~ u: "0 

._, ' 0 

"' :c ;!: () 

..; 

======="'"-""======~,==,-~=~.eo===============""================================ 

External Standard Report 

====================================================~==~~============ 

Sorted By 

Calib. Data t1odified 

Multiplier 

Dilution 

Signal 

10/5/2010 9;18;49 AM 

1.0000 

1.0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/em's] (ug/mL] 

-------l------l----------l----------l----------l--l------------------

3.145 BB 847.86249 1.71449e-2 14.53648 Fluoride 

4.250 BB 562.09290 2.68995e-2 15.12004 Chloride 

Totals : 29.65652 

9 ** End of Report *** 

l.iV-'L"'-'"'n " '"··-" 6 EA# 0910-96 Page 192 of202 Instrument JiirC"Pt<t:r.!tl.'i""NO. ~-1vY-iL· AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PlANTS 4 & 5. SALISBURY PlANT 6 

SEPTEMBER 2010 

! I 

:1 !l 

II ll 

\! 

\! 

tl !i 

!I 

1 

! '·--·-4 --,---------1. 

mi 

APPENDIX PA~'\W' 519 1 of 1 
Sample Name: HPLC53pg100 #5 

BORAL BRICKS 

===============================================================~====~ 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 9:16:57 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

18 

1 

(modified after loading} 

,--u-S-Ic-m1

-.A""D"'C"1"Ac-.-.A"D"'C"1'C_;H,:;Ac;N:7N;;E;=L A (ii\flPic2o1oi54iMRBURNSiliATAIOCTIHPIC53PGl.OOIDOS:181ll~15f·-·····-~---~ 

180- 11 

~ It ·g 1l 

160 

140 

120 u: ~ II (>:) ·g ll 

100 ~ t5 11 

M !i 

80~- r: ~ II 

0 I \ .\ \i 

6 -. 1 ; " ' 

40 ,!' : n to 1 ro · i ' 1 ~ ftig ~~ «! ~ g ~ ,II 20 -4 t:; 1 j \ ~ tt}q:j ,r'-_ cd 

0 l-·--··-·J' ~ -:-·---::.::.~.:.. .. ::._''::::=.~~/~-~':-::: . ._.:;:::~::'-_:~l--~~~----:--~.:-~:-.-._-__ -___ 2_=~2:-- ._.-"~---~---! '---- ____ L .... _____________ 1_··-·····- -·-------- ....... § .... ·-·-··--·------'8'--------"m""l 

========,-=·========c:=:==============:-::===="-~============================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/5/2010 

1.0000 

1.0000 

9:18:49 AM 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------l----------l----------j----------l--1------------------

3.148 BB 851.27545 1.71448e-2 14.59495 Fluoride 

4.265 BB 562.78735 2.68994e-2 15.13865 Chloride 

Tot-als : 29. "73360 

=====o"'='"'"'· ·''"'==""============'""=======~-'-=~"'""""======-======================== 

*** End of Report *** 

l.ll.t.c .L~o1 n .o a. 54 AM EA# 0910-96 Page 193 of 202 Instrument AkT'ffviil=tHW. t-'-1oM~ IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGg%\e520 1 of 1 
Sample Name: HPLC53pgl00 #5 

BORAL BRICKS 

=========================================~=========================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

Last changed 

EO Seq. Line 

Mr_Burns Location 

10/4/2010 9:29:17 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\ME:rROHM.M 

4/1/2010 4:15:36 PM 

lJ:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading} 

18 

2 

~--······-·--AoCi·A;"Aot"T'CHANNEL A (U:\HPLC201 004\MR BURNS\DAT AIOCDHPLC53PG1 00\005·1802.0) 

1 us~: J 

:::1 

120-1 

1:: l 

60. 

40 . 

20. 

=========================================================,=•:=========== 

External Standard Report 

==============================================================,,...,.,.,.,.....,=== 

Sorted By 

Calib. Data Modified 

t.!Jul tipli_er. 

Dilution 

Signal 

10/5/2010 9:18:49 AM 

1.0000 

l. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] {uS/cm*s] [ug/rnL] 

-------l------:----------l----------l----------l--!------------------

3.146 BB 848.51825 1.71448e-2 14.54771 Fluoride 

4.263 BB 561.98425 2.68996e-2 15.11713 Chloride 

Totals : 29.66484 

~================~=,=========================='""""'===""=~"="-"·"""""'======""====== 

*~* End of Report *** 

L11.l nmn-" 7 n 0 EA#0910-96 Page 194 of202 

Instrument AtcffibjtCT NO. l"'-iu1'12 2 AM IGG EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

~ 

I 

! 

i 

( 

APPENDIX PAGgw,e521 1 of 1 
Sample Name: HPLC53pg100 iSS 

BORAL BRICKS 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis .Method 

Last changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 4:38:08 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHH.M 

4/1/2010 4:15:36 PH 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

{modified after loading) 

7 

2 

~------·---Aoc1-A;-J\o·c·rcHANNEL il(u:IHF>n;-2o1ocf41MR sDRNs\5AtAiocnHPLcs3PG1oo\oo6-o7o2.o1 

uS/em l 

' 180 j 

160 -i 

1401 

120 

100 

80 

60 . 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

:g "

0 

~ 

;:;: 

, 

,._ 

:g " 

0 

:c 

() 

:;; 

N 

External Standard Report 

Signal 

10/5/2010 9:21:11 AM 

1.0000 

1. 0000 

Use Multiplier & Dilution Factor with ISTDs 

Signal 1: ADCl A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*sJ [ug/mLJ 

~ 

I 

; 

I 

i 

i 

I 

I 

I 

--r'-j_ 

ml 

-------l------l----------l----------l----------l--l------------------

3.117 BB 76.75529 1.72618e-2 1.32493 Fluoride 

4.251 BB 90.33049 2.74335e-2 2.47808 Chloride 

Totals : 3.80301 

*** End of Report *** 

-r EA# 0910-96 Page 195 of 202 InstrurnentAfcPil18i~§ill.J9. PJ-1Jl'1"1!223 AI~ .l~G EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG!'<AA!e522 1 of 1. 
Sample Name: HPLC53pg100 ffSS 

BORAL BRICKS 

=="'"=================,================:,===""========::;:================== 

Acq. Operator 

Acq. Instrument 

Injection Date 

Acq. Method 

Last changed 

Analysis Method 

J_,ast changed 

EO Seq. Line 

Mr Burns Location 

10/4/2010 4:25:48 PM Inj 

C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M 

4/1/2010 4:15:36 PM 

U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M 

10/5/2010 9:18:49 AM by IGG 

(modified after loading) 

7 

1 

··-·~-Abcf/i; ADCTCHANNEL A (U:\HPLC201-if64\Mi'r80RNS\DATAIOCT\HPLC53PG1001006·070f0)--·---

L 

===================================================================== 

Sorted By 

Calib. Data Modified 

Multiplier 

Dilution 

External Standard Report 

Signal 

10/5/2010 9:18:49 AM 

l. 0000 

l. 0000 

Use Multiplier & Dilution Factor Hith ISTDs 

Signal 1: ADC1 A, ADCl CHANNEL A 

RetTime Type Area Amt/Area Amount Grp Name 

[min] [uS/cm*s] [ug/mL] 

-------l------j----------!----------l----------l--[------------------ 3.119 BE 76.93913 1.72615e-2 1.32808 Fluoride 

4.253 BE 90.24962 2.7434le-2 2.47591 Chloride 

Totals : 3.80400 

=~~~================================================================= 

*** End of Report *** 

U\.t..c,.<~a1n .a ~.1. OS AM IGG EA# 0910-96 Page 196 of 202 Instrument Alc...-r<v.J~bY M>. t--1~1"1~ EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAG~%1~523 l of l 
Modified on: l/13/2010 at 7:06:26 AM 

BORAL BRICKS 

Method Information 

Method: U: \HPLC201 OQ1 \SM ITHERS\METHODS\METROHM. ~~ 

Modified: 1/13/2010 at 7:06:26 AM 

ANALOG DIGITAL CONVERTER 

=======::=o=============================================::o:=====:::="-'""'""--""""''"""-===·~== 

Description: 

Source: 

Unit: 

Units/Volt: 

Peakwidth (Data Rate): 

Stop Time: 

Data Stora9e: 

Signal 1 

ADCl A, Metrohm 

Signal 

mAU 

100.000 

0.027 Min (10.00 Hz) 

No Limit 

All 

Start Signal Source: External Device Will Start 35900 

Timed Event Table: 

<no events> 

EA# 091 0-96 Page 197 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE Ni\"511'4 1 of 1 
( 

BORAL BRICKS 

Sequence Table: 

Method and Injection Info Part: 

Line Location SampleName 

Data File 

Method 

AutoBalance 

1 Vial 127 DI Rinse METROHM 

2 Vial 1 HPLC53pg98 #1 METROHM 

3 Vial 2 HPLC53pg98 12 METROHM 

4 Vi a.l 3 HPLC53pg98 #3 i1ETROHM 

5 Vial 4 HPLC53pg98 #4 METROHM 

6 Vial 5 HPLC53pg98 #5 METROHM 

7 Vial 6 HPLC53pg98 #SS METROHM 

8 Vial 7 HPLC53pg98 #LCS METROf~ 

9 Vial 8 O.OlN H2S04/Na0H RB METROHM 

10 Vial 9 Salisbury Rl In A *20 0910-96 METROHM 

11 Vial 10 MS Salisbury R1 In A *20 0910-96 METROHM 

12 Vial 11 MSD Salisbury Rl In A *20 0910-96 METROHM 

13 Vial 12 Salisbury R2 In A *20 0910-96 METROHM 

14 Vial 13 Salisbury R3 In A *20 0910-96 METROHM 

15 Vial 14 Salisbury Rl Out A *10 0910-96 METROHM 

16 Vial 15 Salisbury R2 Out A *10 0910-96 METROHM 

17 Vial 100 HPLC53pg98 #3 METROHM 

18 Vial 101 HPLC53pg98 #4 METROHM 

19 Vial 16 Salisbury R3 Out. A *10 0910-96 METROHM 

20 Vial 17 Salisbury Rl In B *10 0910-96 METROHM 

21 Vial 18 Salisbury R2 In B *10 0910-96 METROHM 

22 Vial 19 Salisbury R3 In B *10 0910-96 METROHM 

23 Vial 20 Salisbury Rl B Out *10 0910-96 METROHM 

24 Vial 21 Salisbury R2 Out B *10 0910-96 METROHM 

25 Vial 22 Salisbury R3 Out B *10 0910-96 METROHM 

26 Vial 23 Salisbury Rl Out B *100 0910-96 METROHM 

27 Vial 24 Salisbury R2 out B *100 0910-96 METROHM 

Inj 

LimsiD 

4 

2 

2 

2 

2 

2 

2 

2 

2 

2 

2 

EA# 0910-96 PaQe 198 ol202 

Instrument A'fcrn61JEs~W,. M0142: 32 PM IGGEPA ICR EMISSION TloST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

SampleType InjVolume 

Sample 

Sample 

Sart',ple 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

Sample 

Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

2 Sample 

APPENDIX PAGE rJOaSJU 1 of 3 
( 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S 

Line Location SampleName 

DataFile 

Me th~8RAL BRICKS 

AutoBalance 

Inj 

LimsiD 

28 Vial 25 Salisbury R3 Out 8 *100 0910-96 METROHM 

29 Vial 100 HPLC53pg98 *3 METRO HI~ 2 

30 Vial 101 HPLC53pg98 #4 METROHM 2 

31 Vial 7 HPLC53pg98 #LCS METROHM 2 

32 Vial B 0.01N H2S04/Na0H RB METROHM 2 

33 Vial 26 P4 R1 In A *10 0910-96 METROHM 2 

34 Vial 27 MS P4 Rl In A * 10 0910-96 METROHM 

35 Vial n MSD P4 Rl In A *10 0910-96 METROHM 

36 Vial 29 P4 R2 In A *10 0910-96 METROHM 2 

37 Vial 30 P4 R3 In A *10 0910-96 METROHM 2 

38 Vial 31 P4 Rl Out A *10 0910-96 METROHM 

39 Vial 32 P4 R2 Out A *10 0910-96 METROHM 

40 Vial 33 P4 R3 Out A *10 0910-96 METROHM 

41 Vial 110 HPLC53pg98 #3 METROHM 2 

42 Vial 111 HPLC53pg98 #4 METROHM 2 

43 Vial 34 P4 Rl In B *10 0910-96 METROHM 2 

44 Vial 35 P4 R2 In B *10 0910-96 METROHM 2 

45 Vial 36 P4 R3 In B *10 0910-96 METROHM 2 

46 Vial 37 P4 Rl Out B *10 0910-96 METROHM 

47 Vial 38 P4 R2 Out B *10 0910-96 METROHM 

48 Vial 39 P4 R3 Out B *10 0910-96 METROHM 

49 Via] 40 PS Rl In A *10 0910-96 METROHM 2 

50 Vial 41 P5 R2 In A *10 0910-96 METROHM 2 

51 Vial 42 P5 R3 In A *10 0910-96 METROHM 2 

52 Vj.a.l 43 PS P.l Out A *10 0910-96 t'-1ETROHM 

53 Vial 110 HPLC53pg98 #3 METROHM 2 

54 Vial 111 HPLC53pg98 #4 METROHM 2 

55 Vial 102 HPLC53pg98 #LCS METROHM 2 

56 Vial 103 O.OlN H2S04/NaOH RB METROHM 2 

57 Vial 44 P5 R2 Out A *10 0910-96 METROHM 

Instrument AkP~~~gjl j\J~ f"i.:f01l!i?: 32 PM I GGEP~1M~~fl;~~J'f~T 1Jlr?o~~~~z AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

2 

2 

2 

2 

2 

2 

2 

2 

2 

SampleType InjVolume 

2 Sample 

Sample 

Sample 

Sample 

Sample 

SaiTI.ple 

Sample 

2 Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

APPENDIX PAGE Nll- 2 of 3 
( 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S 

Line Location SampleName Me ttJlcflRAL BRICKS Inj 

DataFile AutoBalance LimsiD 

====""""'""= ====~~===~=====~==== ===~================ ======== 

58 Vial 45 P5 R3 Out A *10 0910-96 METROHM 2 

59 Vial 46 PS Rl In B *10 0910-96 METROHM 2 

60 Vial 47 PS R2 In B *10 0910-96 METROHH 2 

61 Vial 48 PS R3 In B *10 0910-96 METROHM 2 

62 Vial 49 P5 R1 out B *10 0910-96 METROHM 2 

63 Vial 50 PS R2 Out B *10 0910-96 METROHM 2 

64 Vial 51 P5 R3 out 8 *10 0910-96 METROHM 2 

65 V:iaJ. 120 HPLC53pg98 #3 METROHM 2 

66 Vial 121 HPLC53pg98 #4 METROHM 2 

67 Vial 52 Acid Blank *10 0910-96 METROHM 2 

68 Vial 53 Base Blank *10 0910-96 METROHM 2 

69 Vial 54 Dl H20 blank 0910-96 METROHM 2 

70 Vial 1 HPLC53pg98 #1 METROHM 2 

71 Vial 2 HPLC53pg98 #2 METROHM 2 

72 Vial 3 HPLC53pg98 #3 METROHM 2 

73 Vial 4 HPLC53pg98 #4 METROHM 2 

74 Vial 5 HPLC53pg98 #5 I~ETROHM 2 

Instrument A'tC~EGiVM\. !L'loil<l!: 32 PM IGGEP~gRo~~?s~lttf~:/p 3~~~2 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

sampleType InjVolurne 

""========= ========= 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

sample 

Sample 

sample 

APPENDIX PAGE Nlli>SI!'l' 3 of 3 
Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG100.S 

BORAL BRICKS 

Sequence Table: 

Method and Injection Info Part: 

Line Location Sample Name Method Inj 

DataFile AutoBalance LimsiD 

======== ==================== ==================::::;.=. o=:===o==== 

1 Vial 127 DI Rinse METROHM 4 

2 Vial 1 HPLC53pg100 #1 METROHM 2 

3 Vial 2 HPLC53pglOO #2 METROHM 2 

4 Vial 3 HPLC53pgl00 #3 METROHM 2 

5 Vial 4 HPLC53pgl00 #4 METROHM 2 

6 Vial 5 HPLC53pg100 #5 METROHM 2 

7 Vial 6 HPJ"C53pg100 itSS METROHM 2 

8 Vial 7 HPLC53pgl00 #LCS METROHM 2 

9 Vial 8 O.OlN H2S04/Na0H RB METROHM 2 

10 Vial 9 PS R2 In A *20 0910-96 METROHM 2 

11 Vial IO P5 R3 In A *20 0910-96 METROHM 2 

12 Vial 11 R1 C4 *10 1010-10 METROHM 2 

13 Vial 12 R2 C4 "10 1010-10 METROHM 2 

14 Vial 1 HPLC53pg100 #l METROHM 2 

15 Vj.a 1 2 HPLC53pg100 #2 METROHM 2 

16 Vial 3 HPLC53pg100 #3 METROHM 2 

17 Vial 4 HPLC53pglOO #4 METROHM 2 

18 Vial 5 HPLCS 3pg 100 #5 METROHM 2 

'- '-~'~'-~"2Q1fl-"' ~-"- o3 GG EA#0910-96 Page201 of202 

Instrument AtC-pffi.)jiot;f NO. 1-'-lrn-42 AM I EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

SampleType InjVolume 

=====""==== ========= 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sarnple 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

Sample 

APPENDIX PAGE J&a5![8 1 of l 
( 

BORAL BRICKS 

This Is The Last Page 

Of This Report. 

ATC PROJECT No. P-10142 

EA# 0910-96 Page 202 of 202 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 529 
( 

BORAL BRICKS 

METALS 

LABORATORY RESULTS 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 530 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Fr<><>-(800)·733-3193 

CHAIN OF CUSTODY RECORD Project No p -10124 

~OU6!lfEO PAIUold~ 

C.l~£-"11: 8Ciral Blic).S tlf.l-f'l,.l;>.-CfltU) 

~L<;IcATlOI<: 

i>LANJ'C.Ot:'ATION; ""'. """" .. " " ;, " ' 2~ ~ "' YOST OTHER 

~LEW; 

Run #1-M-1 

Run #2-M-1 

Run #3-M-1 

Run #1-M-3 

Run#2-M-3 

Run#3-M·3 

Run #1-M-4 

Run#2-M-4 

Run #3-M-4 

Run#1-M-5A 

Run#2-M-5A 

Run#3-M-5A 

Run #1-M-SB 

Run#2-M-5B 

Run#3-M-5B 

Run#1-M-5C 

Run#2-M-5C 

Run #3-M-5C 

~B.II«l;;..ISHEOI!Y 

L> f.JP-.1'---

"'""""""" ~ 

fl LO REMARKS: 

NOTE: 

OA"fe ""' "'"'- va.IIMI fi&JOfl,.,;rno CONTIJNEI't t:ONT£Nn 

9.17.18 CFA FILTER Exposed Quartz Filter 

' ' CFA FILTER Exposed Quartz Riter 

i CFA .FilTER Exposed Quartz Filter 

i CFA -100 ml 0.1 HN03 FH R\n!.la 

; CFA -100 ml 0.1 HNO. FH Rln~e • 

\ CFA -100ml 0.1 HN01 FH Rinse 

I ·,· ·. Catch+ 100 ml 

CFA Riflse Imp. 1&2 C&R 5"/o/10% 

i · .. _·_· CFA 

Catch+ 100 mL 

Rinse- Imp. 1&2 C&R !i%.'1 0% 

i Catch+ 100 ml 

I , .. ,· CFA Rinse Imp. 1&2: C&R s•..w1 0% 

.·_. CFA 100ml Imp. 3 C&R W/100ml HN~ 

i CFA 100ml imp. 3 e&R wr 100mt HN~ 

L CFA 100ml Imp. 3 C&R WI 100m1 HNO, 

: Catch+ 100 n'll 

i Rinsa KMN0-4 + 

I 100mLOI H20 

' CFA Rinse Imp, 4&5 C&R ~'loOo~. Rkl&e 

l Ca!ch + 100 ml ' ! Rinse KMN04 + 

f 

100ml Of H20 

CFA Rinse Imp. 4&5 C&R KMn04 Rln&eI 

CatCh+ 100 ml 

Rinse KMN04 + 

tOOml Dl H20 I CFA Rins;e tmp. 4&5 C&R KMnO, Rinse 

! 2oOmL rn H20 '~" 25 

I CFA ml8NHO BN HCl rinse of imp, 4&5 

' l 200ml. 01 H20 + 25 

CFA ml3N HCJ 8N HCI rtnse of Imp. 4&5 

1 200mL 01 H20 t- 25 

CFA ml8N HCJ SN HCI rins~ of Imp. 4&5 

. 

"'" ,.. """" ' TIME. 

~/Z'/ ~~-,.<1 ~-~ 9/R..i¥/0 I e;, I) 

"'" - ""'"'"' ''" '~ 

w~ ll~'lll I '!/R'-111~ I CFA:CLEAN FIEl-D AArt(J 

Please analyze for standard metal& list {Brlck MACT !GR Emissions Testing) and HG. 

My quMtlcns contact B\11 Kissel (704) 241-Q315 ~ cen 

PLEASE MAAK LIOUlO LEVEl ON ALL SAMPLE BOTILES 1NI.TH GREASE PENCIL. 

SEAL TIG!-Hl Y AND RE-CHECK UPON OEUVERY TO LA8 PERSONNEL, 

Page 55 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

""""' BK 

! 

i 

i 

i 

! 

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100912 

Vet 1.0 1!:9 AUQVSI 2005 

APPENDIX PAGE No. 585 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-{800)·733·3193 

CHAIN OF CUSTODY RECORD Project No p -10124 

Run~~ •;., " -~ :. A 

CFA FILTER vos:xcose<l "" '"' ~~ Run #2-M-1 

Run #3-M-1 

'Run 

'Run 

Run 

Run #1-M-4 

Run #2·M-4 

Run 

~un 

~un 

~un 

Run " "oo 

Run #2-M-58 

Run #o ' oo 

Run #1·M-5C 

R11 ~ 

Run #3-M-SC 

I r...-tL0.-1--

NOTE: 

! c FA_ FILTER 

c 'A FILTER Exposed 

c 'A -100 mL 0.1 HNO, FH R~se 

' CFA -100 ml 0. I HNO, FH Rinse 

! CF}\_ -IQ!l_ml 0. I HNO, FH Rln•• 

: CFA C-R;;!Oml 

lmp.1&2C&R5%/10% 

! CFA Catch ,.;;,~o ml 

Imp. 1&2 C&R So/JIO% 

I 

CFA CetchR~~ml Imp. 1&2 C&R SMO" 

CFA 100mL Imp. 3 C&R wl100ml HNO, 

CFA 100ml Imp>"'"' w• •wnd HNO, 

.·· CFA 100ml Imp, 3 C&R w1 IOOml HNO, 

Catch + 100 ml 

Rinse KMN04 + 

CFA 1 oo~~n~~ H20 Imp. 4&5 C&R KMnO, Rinse 

Catdl + 100 mL ·. Rinse KMN04 + 

100mt OIH20 

CFA_ "In"" Imp. 4&5 C&R KMnO, Rln~ 

' Catch+ 100 ml 

Rinse KMN04 + 

I l00";!; H20 CFA Imp. 4&5 C&R KMnO, Rln,. 

I !2llOmL 01 H20 + 25 

i CFA mL8NHC\ SNHCI . 4&5 

f ?<l<J'Jn-L~NH~~/ 25 

' CFA 8N HCI• • 4&5 

~ 

•••••• CFA mL8NH~I• 25 

6N HCI . 4&5 

: 

·.· 

I 1/u v.>. ·"- JJ. .9-~· D •o~ 

I /"lll!f ~~~ ~ I q /;)L/ II <l ~' 'V Please analyze for standard metals list (Brick f!M.CT ICR Emissions lesting} and HG. 

Any questions contact Bill Kls:sel (704-) 241-0315. cell 

>'LEASE MARK UQ!JID LEVO:::l ON ALL SAMPLE BOTTlES W1TH GREASE PENCIL. 

SEAL T1CHTL Y AND RE-CHE.CK UPON DELIVERY TO lA8 PERSONNEL, 

Poge 56 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

A 

BK 

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Vet \.0 29 Au{IUSI 2003 

APPENDIX PAGE No. 586 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)-733-3193 

CHAIN OF CUSTODY RECORD Project No p -10124 

c"'"'~ ·;, .. -'- -·- ;. 

VOST 

Run #1-M-1 

Run #2-M-1 

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I Run ~o "<o 

lBun #1-M-5C 

I Run '"ry "rrRun #3-M-5C 

f;.;j( JJ}_ 

NOTE: 

!'<;lAW .... _ .. n:\ 

9.21.10 CFA FILTER F>c I""' '''""'. CFA FILTER 'Filler 

CFA FILTER E>pos"' o, 

.·. =A ctOOml o, 1 HN<J, FH R;n,. 

;A -tOOml 0.1 HNO, FH Rln" 

"A -100ml 0.1 HNQ, FH Rln•o 

CFA Calch ,;.: ml 

Imp. t&2C&R 6%110% 

CFA Catcn_ • 1 oo ml 

-""''" IMp. 1&2C&R 5%110% 

CFA Cal"';,~,;.,oo ml 

Imp. 1&2 C&R 5%110% 

CFA 100ml Imp. 3 C&R WIIOOml HNO, 

i GFA 100ml Imp.> C&R WI toOml HNO, 

CFA IOOmL !mp. 3 C&R WllOOml HNO, 

' Catch + 100 mL ! Rinse KMN04 ... i tOQmL 01 i-120 

CFA Rlnsa lm~ <&5 C&R KMnO, Ri""' 

Celch + 1 DO mL 

Rlnse KMN04 + 

100mL OJ H20 

CFA Rinse oRin~ 

catch + 100 ml 

R~'lSEt KMN04 + 

CFA 1~~~H20 ' 0 ' I KMnO, Rin" 

. •. 

CFA 200~L o;NH~~ · 25 _aN Hct nn,. or Imp. 4&5 

·. 

CFA 200~~ ~NH~~ o 20 •ollmp. 4&5 . 

200m;L ~NH~g • 25 CFA sN HCI n~• o/ Imp. 4&5 

I ·li'<>~ it,,•,. ~l(~ 7 b. ~o tS 

ri ~ ll6'30iqf~~lt6 r 

'-' 

Please analyze for standard metals list {Brtck MACT lCR Emissions Testing) and HG. 

Any queslions contact Bill Klssel (704) 241-0315 -<:.eJI 

PlEASE MARK LIQUID LEVEL ON All SAMPlE BOTILES WllH GREASE PENCJL. 

$EAL TIGHTLY AND RE-CHECK UP()N OE;L!VERV TO LAS PERSONNEL 

Page 57 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 D 

_illi_ 

BK 

' 

: 

! 

! 

i 

100912 

Ver1.0 2QAugust~J 

APPENDIX PAGE No. 587 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Frne-{800)-733·3193 

CHAIN OF CUSTODY RECORD Proje<t No P-10124 

~"""~ <~=-~~~~~w~~~-;"::t:~~~~~~~~ m VOST 

~un s21.1o ·. CFA FILTER •· ""'' ,.,,,., BK 

Kun 1 CF A FILTER "' •• n 'Flttar 

Run 1-1 ! CFA FILTER E•oose4 o, '»I" 

fl_un #J-M-3 CFA -100 mL 0.1 HNo, FH Rl""' 

Run #2-M-3 ! · .. _·.· · CFA -100 ml 0.1 HNO, FH Rln•• 

Run #3-M-3 ·.·· CFA -100 ml 0.1 HNO, FH Rln,. 

Run " 0 " CFA Ca~o~~n~00 ml lmp,1_&2_C&R 5%110% 

!Run"' " 1 CFA Cal<:~~n;.00 

lnl :m,. 1&2 C&R 5%110% 

!Run #1-M·5A 

!Run 

lfl.u_n .. oo 

lfl.un .. "" 

I Run "" " "" 

I Run "" " "'"' 

ifl.un ''"' 

NOTE: 

fOftotNo."ttl 

· .. 

'• 

CFA 

CFA 

CFA 

·, CFA 

CFA 

.. CFA 

· ... CFA 

I·••· ..... CFA 

CFA 

·. 

' CC<AN F ELO A<\Y' 

100 ml Imp. 3 C&R wf 100ml HNO, 

100 ml Imp. ~W/100ml HNO, 

100 ml Imp. l C&R '-l100ml HNO, 

Catch • 100 ml 

Rinse KMN04 + 

100~~0IH20 

""""' ' Imp. <&S C&R KMnO, Rln" 

~;atct~_+-100 mL 

Rinse KMN04 + 

100~LOI H20 

><OSO Imp. 4&5 C&R KMoO, Rinse 

Ca1ch ~ 100 ml 

Ril'lS& KMN04 -t 

100ml Ol H20 

Rmse Imp. ,., C&R J<MnO, Rlnoe 

.4&5 

4&5 

i 

Please analyz& f-or standarcl metals list (Brick MACT !CR Emissions 1 esting) and HG. 

Any que:!>tions contact em Kissel (704) 241-0315- cell 

PlEASE MARK :.JQUIO LEVEL ON All SAMPLE 601TLE8 WITH GREASE PENCIL. 

SEAl. T!GBTI. Y AND RE-CH!:=CK UPON OELlVEHY TO LAS Pf.R.SONNEL 

P<:~ge 58 of 1 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Wr \.0 29 Augul-121J03 

APPENDIX PAGE No. 588 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)-733-3193 

CHAIN OF CUSTODY RECORD Project No. 1.-i _.:,P_-1;,:0:..;1.=2..:.4__. 

CUENT: Bora! BriCkS O!UIIOCil~lfUfo,:II!Cl~l ( 5 J 6 ;, PLANT lOCATION; • GA 11 18 '-n 25 

""'""' """="' Plant 5 Inlet VOST '"'"I"' ~5

1 THER 

IRun 1 Filter 

!Run 1 FH 

I Run 2 FH 

!Run 3 FH 

I 61«11k 

NOTE: 

fORO! No. /I.TC' 

C:1&lral !CRICOC'$~":) COC\P!arll S lnf~l · JYIS 

ATC PROJECT No. P-10142 

9.17.10 CFA leu Tc' ;ubt 1 Filter 

CFA -100ml 

FH Ac~~~~ Rinse 

1 CFA -100 ml 

FH Ace:~~~ Rinse 

FH Acetone Rinse 

CFA -100 mL I PM\ 

h --('\, _fLJJ . f'<J>r-7 I/ 

·• CLEAN FIELD AR"{j 

PLC.ASE MARK UOU!D LEVEl ON All SAMPLE BOTTLES WlTH GREASE PENCll 

SEAL TJGHTL Y AND RE...CHECK UPON DELIVERY TO LAB PERSONNEL. 

Poge 59 of 103 

BK 

I 

~ 

Ver 1.0 29 August 2003 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PAGE No. 589 
)> Sample ID Elem Date Time Abs (Co• Cone (Cal RSD (Con• Special So Special Co Cone (Cali 

-< 0 Colib Blank As "U 

10/5/2010 8:28:06 AM 0.006 0 

;u 10 ppb As As 10/5/2010 8:33:30AM 0.011 0 0 

m 50 ppb As As 10/5/2010 8:39:17 AM 0.054 0 0 

-< 100 ppb As As 10/5/2010 8:45:02 AM 0.108 0 z 

? 200 ppb As As 10/5/2010 8:50:26 AM 0.222 0 E 

" ICY As 10/5/2010 9:07:58AM 0.112 101.55 0.23 101.3874 

.. IC8 As 10/5/2010 9:13:26 AM -0.001 -1.12 91.88 -1.84415 

"' 

1 00912.LB As 10/5/2010 9:18:51 AM -0.002 -1.79 20.97 -1.52533 

100912.LCS As 10/5/2010 9:24:19 AM 0.106 96.09 4.77 92.84928 100912.8-1 As 

)> 

10/5/2010 9:29:44 AM -0.002 -1.63 71.65 -0.80654 

c 100912.SA11-1 As 10/5/2010 9:35:11 AM 0.025 22.57 1.57 22.32252 Glm 

c., 100912.SA12-1 As 10/5/2010 9:46:07 AM 0.033 29.56 3.97 30.38986 

"1)> 

)>0 1 00912.SA13-1 As 10/5/2010 9:51:32 AM 0.031 27.73 3.96 28.50627 

(/)"U;u 

m<;;m 100912.SA01-1 As 10/5/2010 9:56:56 AM 0.002 1.73 3.85 1. 781927 

-uzs: 

-<-;- mCJ>CJ> 100912.SA02-1 As 10/5/2010 10:02:20 AM 0.001 1.17 57.06 0.696565 

1 00912.SA03-1 As 1 0/5/2010 10:07:44 AM 0.000 0.08 357.17 0.264686 

;::o .0'1 -i CCV As 10/5/2010 10:13:32 AM 0.108 98.11 2.41 96.43783 

"'CJ>m 

0)>(/) CC8 As 10/5/2010 10:19:00AM -0.005 -4.39 11.73 -4.02321 

(ii"U 

10/5/2010 10:29:44AM 0.000 0.06 1814.37 0.786739 

"'"' 100912.412-1 As co 

100912.413-1 As 10/5/2010 10:35:28 AM 0.001 0.52 43.18 0.682277 

-<m 

100912.401-1 As 10/5/2010 10:40:52 AM 0.003 2.52 23.25 2.109646 

z 100912.402-1 As 10/5/2010 10:46:17 AM 0.004 3.56 78.59 1.583732 

-< 

'" 100912.403-1 As 10/5/2010 10:51:42 AM 0.002 2.10 46.54 1.409128 

100912.512-1 As 10/5/2010 10:57:08 AM 0.008 7.20 15.14 7.967171 

100912.513-1 As 10/5/2010 11:02:34 AM 0.002 2.12 93.21 0.722418 

100912.501-1 As 10/5/201 0 11:07:59 AM 0.001 0.80 88.59 1.303703 

)> CCV As 1 0/5/2010 11:13:25 AM 0.101 91.29 6.77 95.65703 

"U "U 

m CCB As 10/5/2010 11:18:51 AM -0.005 -4.33 28.23 -5.19731 

z 

0 

x 100912.502-1 As 10/5/2010 11:24:15 AM 0.001 0.75 188.36 1.748918 

"U 100912.503-1 As 10/5/2010 11:29:39 AM 0.004 3.22 19.17 2.782951 

)> Gl 

m CCV As 10/5/2010 11:35:04 AM 0.088 80.12 0.45 80.37671 

z 

CCB As 10/5/2010 11:40:28 AM -0.004 -3.18 6.96 -3.33495 

"' "' 100912.411-1 As 10/5/2010 11:56:53 AM 0.003 2.40 10.31 2.579903 

0 

Page 60 of 1 03 
)> Sample iD Elem Dote Time Abs (Co• Cone (Col RSD (Con• Special Sa Special Cc Cone (Coli C

__, 

0 100912.411-1 As 10/5/2010 12:02:21 PM 0.084 75.93 13.17 1 75.93197 68.85817 

., 

;o CCV As 10/5/2010 12:07:43 PM 0.090 81.68 2.14 80.44496 

0 

L 

m CCB As 10/5/2010 12:13:30 PM 

0 

-0.002 -1.78 22.87 -2.06439 

__, 100912.8-2A As 10/5/2010 12:26:10 PM -0.005 -4.74 10.56 -4.38299 

z 

9 100912.5AI1-2A As 10/5/2010 12:31:36 PM 0.021 19.13 0.73 19.22348 

~ 1 00912 .SAI2-2A As 10/5/2010 12:37:01 PM 0.023 21.04 2.41 20.68477 

'" ... ~ 1 00912.5A13-2A As 10/5/2010 12:42:26 PM 0.018 15.89 0.69 15.96813 

100912.SA01-2A As 10/5/2010 12:47:49 PM -0.005 -4.76 11.54 -4.36776 

1 00912.SA02-2A As 10/5/2010 12:53:11 PM -0.004 -3.41 21.32 -3.92642 

100912.SA03-2A As 10/5/2010 12:58:33 PM -0.006 -5.00 32.80 -3.8382 

)> 

c 100912.411-2A As 10/5/2010 1:03:58 PM -0.005 -4.18 17.19 -3.66811 

Glm 

c., 1 00912.412-2A As 10/5/2010 1:15:15 PM -0.003 -3.13 12.06 -3.40054 

~)> ""o CCV As 10/5/201 0 1:51:41 PM 0.036 32.28 14.68 28.92916 

en""' m~m CC8 As 10/5/2010 1:57:07 PM 0.025 22.47 54.93 13.74218 

"Oz$ Colib Blank 10/5/2010 2:31:03 PM -0.002 0.00 __,__,_ 

mw<n As 

:s::.,..~ 

10ppbAs As 10/5/2010 2:36:29 PM 0.014 0.00 

~100~ 

10/5/2010 0.063 

::0~--i 50 ppb As As 2:42:16 PM 0.00 

~cnm 

~):>(/} 100 ppb As As 10/5/2010 2:47:43 PM 0.115 0.00 or_, 

(J>"O 200 ppb As As 10/5/2010 2:53:06 PM 0.242 0.00 "'"' co ;!JL 10/5/2010 3:03:52 PM 0.124 103.55 0.98 102.8296 

ICY As -<m 

.,o ICB As 10/5/2010 3:09:18 PM 0.001 0.86 204.23 -0.37982 

~__, z 100912.511-1 As 10/5/2010 3:14:44PM 0.023 18.94 0.42 18.88109 

__, 

"' 100912.B-2A As 10/5/2010 3:20:10 PM 0.000 -0.24 96.23 -0.41056 

100912.SAI1-2A As 10/5/2010 3:25:38 PM 0.032 26.65 1.22 26.41596 

100912.SAI1-2A As 10/5/2010 3:31:02 PM 0.159 132.06 0.17 1 105.4149 131.9046 

1 00912.SA12-2A As 10/5/2010 3:36:50 PM 0.042 34.97 2.90 34.25485 

)> 

., 1 00912.SAI3-2A As 10/5/2010 3:42:18 PM 0.032 26.44 0.49 26.53181 

., 

m 100912.SA01-2A As 10/5/2010 3:47:43 PM 0.001 0.58 101.96 0.992452 

z 

0 100912.SA02-2A As 10/5/2010 3:53:08 PM 0.002 1.78 90.44 0.641294 

x 

., 1 00912.SA03-2A As 10/5/2010 3:58:32 PM 0.002 1.52 6.13 1.452879 

)> 

Gl 

m 1 00912.411-2A As 10/5/2010 4:03:57 PM 0.001 0.75 41.60 0.526373 

z 

0 CCV As 10/5/2010 4:09:27 PM 0. 111 91.92 0.43 91.64037 

"' "1 CCB As 10/5/2010 4:14:54 PM 0.000 0.36 46.53 0.243763 

Page 61 of 103 
)> 

--< () 

" "' 0 ~ m 

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--< 

z 

0 

); 

'" ... N 

)> 

c 

Glm c., ~)> l>fi 

"'""' mt;;m -uzs: --<-;- men en !i:..,.~ ~Qog :u !-'t -1 Ncnm ~}>('/) oC-1 

cn-u 

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z 

--< 

"' 

)> 

" 

m " 

z 

0 

x 

" i!i 

m 

z ~ "' i(l 

Sample 10 

100912.412-2A 

100912.413-2A 

CCV 

CCB 

Colib Blank 

10 ppb As 

50 ppb As 

100 ppb As 

200 ppb As 

ICY 

ICB 

100912.401-2A 

1 00912.402-2A 

1 00912.403-2A 

100912.511-2A 

100912.512-2A 

100912.513-2A 

100912.501-2A 

1 00912.502-2A 

1 00912.503-2A 

CCV 

CCB 

Elem Date Time 

As 10/5/2010 4:20:17 PM 

As 10/5/2010 4:25:42 PM 

As 1 0(5/2010 4:31 :08 PM 

As 10/5/2010 4:36:35 PM 

As 10/6/2010 8:11:29 AM 

As 10/6/2010 8:16:53 AM 

As 10/6/2010 8:22:40 AM 

As 10/6/2010 8:28:06 AM 

As 10/6/2010 8:33:29 AM 

As 10/6/2010 8:44:52 AM 

As 10/6/2010 8:50:17 AM 

As 10/6/2010 8:55:39 AM 

As 10/6/2010 9:01:05 AM 

As 10/6/2010 9:06:32 AM 

As 10/6/2010 9:11:59 AM 

As 10/6/2010 9:17:26 AM 

As 10/6/2010 9:22:54AM 

As 10/6/2010 9:28:24AM 

As 10/6/2010 9:33:48 AM 

As 10/6/2010 9:39:15 AM 

As 10/6/2010 9:44:41 AM 

As 10/6/2010 9:50:28AM 

Abs (Co• Cone (Cal RSD (Con• Special So Special Co Cone (Cali 

0.002 1.72 42.36 1.206598 

0.000 0.28 206.70 -0.12921 

0.108 89.70 0.79 90.20047 

0.001 0.81 12.52 0.881699 

-0.001 0.00 

0.012 0.00 

0.059 0.00 

0.113 0.00 

0.216 0.00 

0. 111 101.19 1.67 102.3822 

0.000 0.16 177.28 -0.04031 

0.000 -0.39 186.05 -0.90905 

0.001 0.66 12.54 0.717301 

0.000 -0.34 45.95 -0.44872 

0.017 15.90 2.67 16.20371 

0.004 3.58 20.76 4.100048 

0.000 -0.12 620.93 -0.63139 

0.000 -0.38 109.56 -0.67715 

-0.001 -0.49 67.84 -0.73097 

-0.001 -1.18 72.52 -1.78678 

0.105 96.44 0.29 96.63094 

-0.001 -0.82 51.64 -1.12195 

Page 62 of 103 
::; Sample ID Date Time Elem Cone (Cali lnt (Corr) Calib Unit RSD (Corr In! (Corr)11nt 

0 

-u 

Co lib Blank 1 9/30/2010 10:46:36 AM Ag -278.801 ug/L 10.0937 -299.002 -2

:0 Standard 1 9/30/2010 10:48:10AM Ag 69018.9 ug/L 1.18152 69180.6 6

0 ~ rn Standard 2 9/30/2010 10:49:32 AM Ag 154833 ug/L 0.81269 155082 1

0 

__, ICY 9/30/2010 10:51:35 AM Ag 925.345 70082.9 ug/L 0.87285 69656.8 7

z 

? ICB 9/30/2010 10:54:06 AM Ag 0.11379 8.61819 ug/L 374.284 -22.2385 

i: 

s: ICS 9/30/2010 10:56:55 AM Ag -3.4956 -264.747 ug/L 8.44779 -263.742 -2

.. 1 00912.L8 9/30/2010 10:58:40 AM Ag -0.49744 -37.6748 ug/L 105.348 -78.2082 

"' 1 00912.LCS 9/30/2010 11:00:16 AM Ag 943.515 71459.1 ug/L 0.6289 71036 7

100912.8-1 9/30/2010 11:02:29 AM Ag 0.08874 6.72112 ug/L 403.804 -20.4213 3

100912.SA11-1 9/30/2010 11:11:35 AM Ag 0.84804 64.2281 ug/L 44.886 47.0746 4

l> 

c 100912.SAI1-1 S 9/30/2010 11:12:59AM Ag 765.805 57999.8 ug/L 0.8832 58194 5

Glrn 

c-u 100912.SA12-1 9/30/2010 11:34:05 AM Ag 0.91687 69.4413 ug/L 1.32938 70.1863 

~l> 100912.SA12-1 D 9/30/2010 11:35:42 AM Ag 0.71146 53.8842 ug/L 26.9306 37.8977 5

""i'i (/)-u;o 1 00912.SA13-1 9/30/2010 11:37:15 AM Ag 0.74132 56.1455 ug/L 38.9618 67.3605 3

rnS::m 

-uz;: 100912.SA01-1 9/30/2010 11:38:37 AM Ag 0.12885 9.75852 ug/L 209.153 21.0001 2

...,.,_ mC/lC/l 

:s::.f>.~ 1 00912.SA02-1 9/30/2010 11:40:07 AM Ag -0.27778 -21.0386 ug/L 140.545 11.0389 -4

~Qo~ 

::O!JI-1 CCV 9/30/2010 11:41:48 AM Ag 937.001 70965.7 ug/L 1.04816 70825 7

"-'C/lm ~)>Cil CC8 9/30/2010 11:47:00 AM Ag 0.3785 28.6661 ug/L 128.173 27.8374 -7

or_, 

(I)"U 100912.SA03-1 9/30/2010 12:14:10 PM Ag -0.21052 -15.9442 ug/L 117.243 -4.56274 -3

o:>:O 

co 100912.411-1 9/30/2010 12:15:44 PM Ag 0.60789 46.0399 ug/L 67.1743 45.3967 1

:0~ -<m 

-uo 100912.412-1 9/30/2010 12:17:09 PM Ag 0.0383 2.9006 ug/L 1122.92 -4.16132 -2

,......, 

l> 100912.413-1 9/30/2010 12:18:44 PM Ag 0.01678 1.27099 ug/L 2216.17 26.5319 6

z 

__, 

100912.401-1 9/30/2010 12:20:27 PM Ag 0.81981 62.0902 ug/L 4.24723 62.2184 

"' 

100912.402-1 9/30/2010 12:21:56 PM Ag -0.2402 -18.1919 ug/L 279.819 -42.6851 4

100912.403-1 9/30/2010 12:23:30 PM Ag 0.14839 11.2386 ug/L 196.025 -6.66757 3

100912.512-1 9(30/201 0 12:25:12 PM Ag -0.25681 -19.4501 ug/L 102.757 -31.0174 3

l> 100912.513-1 9/30/2010 12:28:01 PM Ag -0.19665 -14.8935 ug/L 323.72 -0.90251 

-u 

-u CCV 9/30/2010 12:29:53 PM Ag rn 946.732 71702.7 ug/L 0.74602 72234.6 7

z CCB 9/30/2010 12:35:02 PM Ag -0.32695 -24.7 625 ug/L 47.438 -33.6577 -2

0 

x Calib Blank 1 10/5/201 0 1:11:19 PM Ag -217.981 ug/L 10.52 -243.93 -2

-u 

l> Gl Standard 1 10/5/2010 1:13:25PM Ag 87223.2 ug/L 0.66 86804.2 8

m 

z Standard 2 10/5/2010 1:14:56 PM Ag 175996 ug/L 0.33 175614 

0 

"' ICY 10/5/2010 <0 1:16:23 PM Ag 993.1 87240.9 ug/L 0.95 86317.2 8

"' ICS 10/5/2010 1:18:08PM Ag -3.1 -275.517 ug/L 10.66 -248.61 -

Page 63 of 103 
)> ~ (l "1l ;o 0 ~ m ~ z 0 :!: :': .. "' 

c 

Glm c" ~)> )>() 

"'""' mS::m 

"llZS: 

-<-;- mrn"' 

S:A~ 

~120~ 

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"'"' co ;o~ -<ffi 

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s;"" 

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m 

z 

0 

x 

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eo 

m 

z ~ "' ~ Sample JD ICB 100912.511-1 100912.501-1 100912.502-1 100912.503-1 1 00912.B-2A 100912.SAI1-2A 100912.SA12-2A 1 00912.SAI2-2AD 100912.SA13-2A 100912.SA01-2A CCV CC8 1 00912.SA02-2A 1 00912.SA03-2A 100912.411-2A 1 00912 .411-2AS 100912.412-2A 1 00912.413-2A 100912.401-2A 1 00912.402-2A 100912.403-2A 100912.511-2A 1 00912.512-2A CCV CCB 100912.513-2A 100912.501-2A 100912.502-2A 1 00912.503-2A CCV CC8 Co lib Blank 1 Standard 1 Date 10/5/2010 10/5/2010 10/5/2010 10/5/201 0 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/201 0 10/5/201 0 10/5/2010 1 0/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/2010 10/5/201 0 10/5/2010 10/5/2010 10/5/201 0 10/5/2010 10/5/2010 10/5/2010 10/5/2010 9/30/2010 9/30/2010 Time 1:20:11 PM 1:22:01 PM 1:23:22 PM 1:24:50 PM 1:26:22 PM 1:28:06 PM 1:29:31 PM 1:30:55 PM 1:32:09 PM 1:33:43 PM 1:35:07 PM 1:36:28 PM 1:38:43 PM 1:43:34 PM 1:45:14PM 1:47:03 PM 1:48:30 PM 1 :50:19 PM 1 :51 :43 PM 1:53:01 PM 1:54:32 PM 1:56:39 PM 1:57:58 PM 1:59:20 PM 2:02:51 PM 2:08:19 PM 2:09:46 PM 2:11:06 PM 2:12:35 PM 2:14:07 PM 2:15:36 PM 2:18:57 PM 10:46:36 AM 10:48:10AM Elem Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ag Ba Ba Cone (Cali lnt (Corr) Calib Uni1 RSD (Corr lnt (Corr)llnt 

-0.4 -37.1978 ug/L 39.25 -51.2929 -3

0.0 -1.98286 ug/L 314.40 4.52076 -7

-0.7 -62.9531 ug/L 49.03 -44.8781 -9

0.0 0.07952 ug/L 63123.00 -9.60855 5

-0.2 -17.5262 ug/L -0.5 -41.7424 ug/L -0.1 -7.02102 ug/L -0.4 -34.5806 ug/L -0.1 -9.49972 ug/L -0.1 -12.461 ug/L -0.1 -10.405 7 ug/L 1077.3 94631.4 ug/L 0.1 5.20953 ug/L -0.1 -6.98174 ug/L -0.1 -5.91871 ug/L -0.3 -25.435 ug/L 794.1 69758.6 ug/L 0.0 -1.61584 ug/L -0.6 -52.9544 ug/L -0.4 -38.7905 ug/L -0.6 -50.9975 ug/L 0.0 0.88859 ug/L -0.6 -50.1831 ug/L -0.6 -50.6836 ug/L 895.6 78671.5 ug/L 0.3 30.2433 ug/L 0.9 77.7761 ug/L 0.2 13.867 ug/L -0.5 -42.9927 ug/L -0.7 -65.4885 ug/L 971.1 85304.6 ug/L 0.3 30.061 ug/L 72.1572 ug/L 290.65 ug/L 

Page 64 of 103 

165.66 -23.8203 1

68.57 -23.3022 -7

548.56 -1.45032 

63.02 -41.0189 -5

363.92 30.2756 -3

186.34 -17.4876 -3

66.73 -16.8134 -3

0.50 95173.9 9

405.00 -17.9196 1

305.54 17.636 -2

190.76 -1 0.5638 6

37.49 -16.0088 -2

0.37 70039.7 6

2933.36 34.1628 -5

41.80 -28.7689 -7

93.48 -2.71063 -3

45.27 -62.1031 -6

4711.01 -44.1202 8

33.86 -69.3656 -3

69.50 -10.5043 -6

1.00 78016.1 7

191.04 74.7326 5

43.90 116.715 5

315.88 63.1655 -2

65.44 -65.8249 -1

37.45 -42.8248 -9

1.09 84229 8

32.24 39.9861 2

5.19364 75.1576 6

7.75378 304.734 3
)> Sample ID Date Time Elem Cone (Cali In! (Corr) Calib Unil RSD (Carr lnt (Corr)llnt 

-< Standard 2 9/30/2010 10:49:32 AM () Ba 612.696 ug/L 3.71219 586.785 6'1l 

;u ICY 9/30/2010 10:51:35 AM Ba 903.797 274.039 ug/L 9.60593 264.898 2

0 

'-

m ICB 9/30/2010 10:54:06 AM Ba 25.9452 7.8668 ug/L 75.5786 14.4194 6

() 

-< IC8 9/30/2010 10:55:40AM Ba 9.51889 2.8S621 ug/L 79.6112 4.98516 0

z 

0 ICS 9/30/2010 10:56:55 AM Ba 10.0829 3.05721 ug/L 141.325 5.21977 5

100912.L8 9/30/2010 10:58:40AM 8a ·8. 92146 -2.70506 ug/L 175.012 ·2.83861 -7

.. 100912.LCS 9/30/2010 11:00:16 AM Ba 912.442. 276.66 ug/L 10.1931 249.905 2

"' 100912.8-1 9/30/2010 11:02:29 AM Ba 13.56S 4.11394 ug/L 161.573 -1.22558 2

100912.SA11-1 9/30/2010 11:11:35 AM Sa 213.42 64.7109 ug/L 53.3988 26.9509 7

100912.SAI1-1S 9/30/2010 11:12:59 AM Sa 1065.22 322.984 ug/L 2.65926 32S.717 3

)> 

c 100912.SAI2-l 9/30/2010 11:34:05 AM Sa 339.879 103.054 ug/L 8.42566 103.828 9Glm 

c., 100912.SAI2-1D 9/30/2010 11:35:42 AM Sa 326.469 98.9881 ug/L 13.1248 92.3844 1

100912.SAI3·1 9/30/2010 11:37:15 AM Bo 287.9 87.2936 ug/L 36.1941 86.0103 5

"'o (f)'1l;u 

m<;;m 100912.SA01-1 9/30/2010 11:38:37 AM Ba 26.84 8.13S1 ug/L 114.359 1.5029 4

'1lz;:: -<-;- 100912.SA02·1 9/30/2010 11:40:07 AM Bo 25.7711 7.81401 ug/L 85.6247 0.3731S 1

m(f)(f) 

CCV 9/30/2010 11:44:42 AM Ba 1061.32 32 1.8 0 1 ug/L 9.S277S 358.187 3

9/30/2010 11:50:49 AM 17.7218 5.37339 ug/L 81.6058 1.4334S 1

::0 _<JI -1 CC8 Ba 

"'(f)m S:>{/) 1 00912.SA03-1 9/30/2010 12:14:10 PM Ba 49.9114 15.1336 ug/L 60.2207 4.61069 2

or-< 

(ii'U 100912.411·1 9/30/2010 12:15:44 PM So 35.5616 10.7S26 ug/L 73.3071 9.318S7 1

OJ;Il 

co 100912.412-1 9/30/2010 12:17:09 PM Bo 52.3605 15.87 62 ug/L 57.4658 26.3234 

;ll'- -<m 

,o 100912.413-1 9/30/2010 12:18:44 PM Bo 49.7845 15.0951 ug/L 59.1624 23.6712 1

s;'" 100912.401-1 9/30/2010 12:20:27 PM Ba 56.5567 17.14S5 ug/L 34.1686 15.9804 1

z 

-< 100912.402-1 9/30/2010 12:21:56 PM Ba 50.6553 15.3591 ug/L 52.5917 8.S3941 2

"' 100912.403-1 9/30/2010 12:23:30 PM Bo 43.2473 13.1129 ug/L 73.7539 20.1031 1

100912.512-1 9/30/201 0 12:25:12 PM Sa 62.1459 18.8432 ug/L 39.0825 m3594 2

100912.513-1 9/30/2010 12:28:01 PM 8a 60.8078 18.4375 ug/L 59.6822 24.2557 2

)> CCV 9/30/2010 12:31:21 PM Sa 1084.36 328.787 ug/L 3.20223 317.336 3

'1l '1l CCB 9/30/2010 12:44:37 PM Bo -3.99555 -1.21149 ug/L 1237.06 -1S.1846 4

m 

z Calib Blank 1 10/5/2010 1:11:19PM Ba 76.0024 ug/L 18.86 80.5594 5

0 

x Standard 1 10/5/2010 1:13:25PM Ba 211.49 ug/L 16.86 213.323 2

'1l 

)> Gl Standard 2 1 0/5/201 0 1:14:56 PM Ba 511.692 ug/L 4.37 492.721 5

m 

z ICY 10/5/2010 1:16:23 PM 8a 912.4 225.344 ug/L 23.45 184.098 20 

"' ICS "' 10/5/2010 1:18:08 PM Ba 17.7 4.36933 ug/L 170.38 2.31673 1"' IC8 10/5/2010 1:20:11 PM 8a -21.3 -5.25889 ug/L 109.27 -9.95357 -6

Page 65 of 1 03 
, 

c ~ -u "' 0 ~ m ~ z 0 ~ 0:1 ... ~ Gl 

em 

"'" -;> >r; 

oo""' 

m<;:m 

-uz;: -<-;- moo"' 

:S::.:-.9.2 

~10'0~ 

::O.Cl -1 

~oom ~ ):.Cfl or-< 

Cii-u 

CD:O 

co ;o~ -<m -u(l 

s;:-< 

z 

-< 

"' 

, 

-u 

-u 

m 

z 

0 

x 

-u 

t; 

m 

z 

? 

"' <0 "' 

Sample ID 

100912.511-1 

1 00912.501 -1 

100912.502-1 

1 00912.503-1 

100912.8-2A 

100912.SAI1-2A 

100912.SAI2 -2A 

100912.SA12-2AD 

100912.SAI3-2A 

100912.SA01-2A 

CCB 

CCV 

1 00912.SA02-2A 

1 00912.SA03-2A 

1 00912.411-2A 

100912.411-2AS 

1 00912.412-2A 

1 00912.413-2A 

1 00912.401-2A 

100912.402-2A 

1 00912.403-2A 

1 00912.511-2A 

100912.512-2A 

CCV 

CCB 

100912.513-2A 

100912.501-2A 

1 00912.502 -2A 

100912.503-2A 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

Date 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/201 0 

10/5/2010 

10/5/201 0 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/201 0 

10/5/2010 

9/30/2010 

9/30/2010 

9/30/2010 

Time 

1:22:01 PM 

1:23:22 PM 

1:24:50 PM 

1:26:22 PM 

1:28:06 PM 

1:29:31 PM 

1:30:55 PM 

1:32:09 PM 

1:33:43 PM 

1:35:07 PM 

1:38:43 PM 

1:42:00 PM 

1:43:34 PM 

1:45:14 PM 

1:47:03 PM 

1:48:30 PM 

1:50:19 PM 

1:51:43 PM 

1:53:01 PM 

1:54:32 PM 

1:56:39 PM 

1:57:58 PM 

1:59:20 PM 

2:05:54 PM 

2:08:19 PM 

2:09:46 PM 

2:11:06 PM 

2:12:35 PM 

2:14:07 PM 

2:16:55 PM 

2:18:57 PM 

10:46:36 AM 

10:48:10 AM 

10:49:32 AM 

Elem 

Ba 

Ba 

Sa 

Sa 

Sa 

Ba 

Sa 

Ba 

Sa 

Sa 

Ba 

Ba 

So 

Sa 

Sa 

Sa 

Ba 

Ba 

Ba 

Sa 

Sa 

Sa 

Sa 

Sa 

Ba 

Ba 

Sa 

8a 

Sa 

Sa 

Ba 

p 

p 

p 

Cone (Cali In! (Carr) Calib Unil RSD (Carr In! (Carr) lint 

54.6 13.4964 ug/l 256.35 -23.1093 17

5.5 1.3676 ug/l 443.60 6.08736 3.

7.1 1.74304 ug/l 598.41 -10.2618 8

-21.0 -5.19149 ug/l 44.72 -3.37455 -7

-42.5 -10.4884 ug/l 63.52 -4.1039 -9

-10.3 -2.54643 ug/l 1594.32 43.0095 -1

57.7 14.252 ug/l 224.84 21.1433 -2

-0.1 -0.02727 ug/L 65790.27 20.6572 -1

29.3 7.24685 ug/l 57.19 6.12365 3

92.3 22.8018 ug/l 66.14 37.4266 2

9.7 2.3869 ug/l 388.79 5.94004 9

1014.3 250.496 ug/L 8.88 242.938 2

14.4 3.5578 ug/l 219.97 2.1781 -3

28.3 6.99349 ug/l 26.32 9.08719 6

5.3 1.31858 ug/l 1693.97 15.6543 

972.7 240.238 ug/l 7.30 220.857 2

104.5 25.813 ug/l 102.76 53.661 2

114.4 28.2442 ug/l 67.91 20.5169 1

-3.2 -0.79213 ug/l 1165.06 -11.4295 3

21.5 5.31147 ug/l 67.29 5.4265 

126.7 31.2956 ug/l 36.66 18.1274 3

66.9 16.5157 ug/l 141.81 7.98174 -1

-62.5 -15.4402 ug/l 79.85 -1.21249 -

1087.9 268.679 ug/l 10.52 236.066 2

15.3 3.78055 ug/l 117.28 -1.20073 7

86.0 21.242 ug/l 90.95 25.8581 3

19.8 4.89999 ug/l 30.72 3.75513 4

59.2 14.612 ug/l 22.58 11.5532 1

48.7 12.0305 ug/l 128.32 25.6493 1

1093.2 270.001 ug/l 15.18 317.187 2

-11.9 -2.93683 ug/L 593.94 16.4167 -1

108.671 ug/l 7.76157 110.801 9

880.264 ug/l 

1989.45 ug/l 

Page 66 of 103 

0.70047 877.205 8

0.34763 1981.88 1
)> Sample ID Date Time Elem Cone (Cali lnt (Corr) Calib Unit RSD (Corr lnt (Corr)llnt 

-< 

0 ICY 

, 

9/30/2010 10:51:35 AM p 4696.98 912.933 ug/L 0.72285 914.62 9

:u ICB 9/30/2010 10:54:06 AM p 18.5308 3.60176 ug/L 89.2844 6.72781 0

0 

m ICS 9/30/2010 10:56:55 AM p 0 29.0659 5.64943 ug/L 262.09 8.0577 -1

-< 

z 1 00912.LB 9/30/2010 10:58:40 AM p 67.511 13.1219 ug/L 91.6643 21.0751 

0 100912.LCS 9/30/2010 11:00:16 AM p 4517.53 878.055 ug/L 1.45885 880.685 8

100912.8-1 9/30/2010 11:02:29 AM p 104.501 20.3115 ug/L 19.4473 17.8781 1

"' .. 100912.SAI1-1S X 2 9/30/2010 11:26:01 AM p 5224.75 1015.51 ug/L 0.87959 1023.8 1"' 100912.SAI1-1 X 2 9/30/2010 11:32:35 AM p 188.676 36.6723 ug/L 30.7937 49.4965 2

100912.SAI2-1 9/30/2010 11:34:05 AM p 356.781 69.3461 ug/L 22.3586 76.5696 5

100912.SAI2-1D 9/30/2010 11:35:42 AM p 320.736 62.3403 ug/L 15.4131 69.942 6

)> c 100912.SA13-1 9/30/2010 11:37:15AM p 314.589 61.1454 ug/L 16.6772 52.7728 5

Glm c, 1 00912.SA01-1 9/30/2010 11:38:37 AM p 159.799 31.0596 ug/L 18.0532 33.6546 2

>c; 100912.SA02-1 9/30/2010 11:40:07 AM p 171.514 33.3365 ug/L 20.1399 34.3533 3

"'"""' mS::m CCV 9/30/2010 11:41:48 AM p 4962.46 964.535 ug/L 0.32328 963.452 9

-uzs: CCB 9/30/2010 11:47:00 AM p 97.5021 18.9511 ug/L 28.6974 15.1447 1

..,_,_ moo"' 

1 00912.SA03-1 9/30/2010 12:14:10 PM p 147.076 28.5867 ug/L 44.1967 41.7206 1

::ti.Ul--! 100912.411-1 9/30/2010 12:15:44 PM p 252.435 49.0648 ug/L 29.0544 37.3047 6

"'oom O)>rf> 100912.412-1 9/30/2010 12:17:09 PM p 165.487 32.165 ug/L 4.55432 33.0536 3

Oc:--1 

"'"" 100912.413-1 9/30/2010 12:18:44 PM p 272.605 52.9852 ug/L 6.13115 49.3984 5

co "'"' 100912.401-1 9/30/2010 12:20:27 PM p 195.731 38.0435 ug/L 35.2918 25.9764 3

-<m 

,o 100912.402-1 9/30/2010 12:21:56 PM p 190.494 37.0257 ug/L 26.5681 29.7055 4

s;""' 100912.403-1 9/30/2010 12:23:30 PM p 189.2 36.77 41 ug/L 37.5352 24.4927 3

z 

-< 100912.512-1 9/30/2010 12:25:12 PM p 303.596 59.0087 ug/L 18.7082 55.446 5

"' 100912.513-1 9/30/2010 12:28:01 PM p 185.344 36.0246 ug/L 25.2639 29.9842 4

CCV 9/30/2010 12:29:53 PM p 5045.98 980.7 69 ug/L 0.79882 972.16 9

CCB 9/30/2010 12:41:41 PM p 120.366 23.3951 ug/L 29.7871 31.4229 1

)> Calib Blank 1 10/5/201 0 1:11:19 PM p 26.572 ug/L 43.66 23.637 3

, Standard 1 10/5/2010 1:13:25 PM p 1235.38 ug/L 0.89 1241.25 1, m 

z Standard 2 10/5/2010 1:14:56 PM p 2451.21 ug/L 0.11 2448.59 2

0 

x 

, ICY 10/5/2010 1:16:23 PM p 5022.9 1233.19 ug/L 1.34 1247.27 1

e; ICS 10/5/2010 1:18:08 PM p 34.2 8.40564 ug/L 45.00 6.39662 1

m 

z ICB 10/5/2010 1:20:11 PM p 22.5 5.53145 ug/L 299.86 23.7323 1

0 

100912.511-1 10/5/2010 171.0 "' 1:22:01 PM p <0 41.9873 ug/L 25.18 33.5745 5

"' 100912.501-1 10/5/2010 1:23:22 PM p 76.7 18.8405 ug/L 51.05 11.5106 2

Page 67 af 103 
)> Sample 10 Date Time Elem Cone (Cali lnt (Corr) Calib Unil RSO (Corr In! (Corr)llnt (

--< 

0 100912.502-1 

" 

10/5/2010 1:24:50 PM p 89.4 21.96 ug/L 54.64 11.0943 34

" 100912.503-1 10/5/2010 1:26:22 PM p 100.4 24.6461 ug/L 19.39 19.8357 24

0 L 1 00912.B-2A 10/5/2010 1:28:06 PM p rn 

0 

42.3 10.374 ug/L 146.68 -0.02311 3.

..; 1 00912.SAI1-2A 10/5/2010 1:29:31 PM p 184.6 45.3294 ug/L 41.09 61.5197 24

z 

? 100912.SAI2-2A 10/5/2010 1:30:55 PM p 163.2 40.0622 ug/L 23.89 29.1625 47

~ 1 00912.SA12-2AD 10/5/2010 1:32:09 PM p 156.6 38.455 ug/L 8.46 38.7481 41

':l 

... 100912.SA13-2A 10/5/201 0 1:33:43 PM p 169.7 41.6655 ug/L 32.85 30.3412 56

"' 100912.SA01-2A 10/5/2010 1:35:07 PM p 146.4 35.9334 ug/L 24.77 35.3134 27

CCV 10/5/201 0 1:36:28 PM p 5352.5 1314.1 ug/L 1.31 1316.03 13

cc8 10/5/2010 1:38:43 PM p 33.7 8.2851 ug/L 85.48 14.0472 10

)> 

c 100912.SA02-2A 10/5/2010 1:43:34 PM p 115.1 28.2651 ug/L 18.13 30.8037 31

Glrn c., 100912.SA03-2A 10/5/2010 1:45:14 PM p 175.1 42.9783 ug/L 10.92 42.2211 38

~)> 1 00912 .41l-2A 10/5/2010 1:47:03 PM p 112.3 27.5812 ug/L 42.69 14.9118 38

"o cn~:u 100912.411-2AS 10/5/2010 1:48:30 PM p 3911.5 960.328 ug/L 1.96 981.873 94

rn)>rn 

-uzs: 100912.412-2A 10/5/2010 1:50:19PM p 137.4 33.7404 ug/L 21.26 36.5946 39

--<-;- rn(/)(1) 

:S:AfQ 100912.413-2A 10/5/2010 1:51:43 PM p 63.0 15.4583 ug/L 50.65 14.0403 8.

~~~ 

143.8 2.80 36.3647 

::0 _Ol __, 100912.401-2A 10/5/2010 1:53:01 PM p 35.3023 ug/L 34

"'(l)rn ~ );:.{/) 100912.402-2A 10/5/2010 1:54:32 PM p 123.0 30.2063 ug/L 6.52 28.0565 31

ac-1 

(1)'0 1 00912.403-2A 10/5/2010 1:56:39 PM p 91.0 22.3419 ug/L 30.52 25.768 14

"'" co 1 00912.511-2A 10/5/2010 1:57:58 PM p 122.8 30.1407 ug/L 9.83 33.5321 28

:OL 

-<rn 

.,o 1 00912.512-2A 10/5/2010 1:59:20 PM p 179.0 43.9516 ug/L 20.64 53.1097 43

s;:--< CCV 10/5/2010 2:02:51 PM p 4581.7 1124.87 ug/L 1.44 1115.01 11

z 

..; CCB 10/5/2010 2:08:19 PM p 47.1 11 .5546 ug/L 99.44 2.02893 8

"' 100912.513-2A 10/5/2010 2:09:46 PM p 42.1 10.3475 ug/L 92.67 7.12998 21

100912.501-2A 10/5/2010 2:11:06 PM p 136.3 33.4646 ug/L 11.93 35.5019 28

100912.502-2A 10/5/2010 2:12:35 PM p 156.5 38.4298 ug/L 29.52 27.3209 37

)> 100912.503-2A 10/5/2010 2:14:07 PM p 162.4 39.8656 ug/L 17.17 46.5805 32

" 10/5/201 0 " CCV rn 2:15:36 PM p 4836.9 1187.51 ug/L 2.47 1156.81 1

z CCB 10/5/201 0 2:18:57 PM p -7.9 -1.93136 ug/L 199.40 2.32703 -5.

0 

x 

" )> Gl 

rn 

z 

0 

"' "" "' 

Po9e 68 of 1 03 
)> 

-j 

() Sample ID Date Time Elem Cone (Calillnt (Corr) Calib Unitl RSD (Corr lnt (Corr)1 lnt (Cor

" ;o Colib Blank 1 10/5/2010 10:16:34 AM Be 24979.75 ug/L 0.746267 24935.06 25184

0 ~ m Standard 1 10/5/2010 10:18:05AM Be 1223052.84 ug/L 3.658159 1175160 12302

() 

-j Standard 2 10/5/2010 10:18:59 AM Be 2485883.46 ug/L 1.732014 2448535 24761

z ~ ICY 10/5/2010 10:22:12 AM Be 1014.94 1257476.2B ug/L 0.246379 1255005 12564

" ICB 10/5/2010 10:23:48 AM Be -0.09 -112.66 ug/L 31.79334 -152.B7 -100.9

0 

:;: ICS 10/5/2010 1 0:24:58 AM Be -0.38 -466.70 ug/L 11.43757 -501.036 -493

N 

1 00912.LB 10/5/2010 10:26:51 AM Be -0.41 -504.70 ug/L 18.20084 -431.213 -475.1

100912.LCS 10/5/2010 10:28:03 AM Be 871.44 1079680.09 ug/L 2.945141 1047071 10813

1 00912.B-1 10/5/2010 l 0:29:40 AM Be -0.62 -771.62 ug/L 20.23049 -650.271 -947.7

)> 100912.SA11-1 10/5/2010 10:30:53 AM Be -0.42 -521.7 4 ug/L 12.96059 -533.516 -582

c 100912.SA12-1 10/5/2010 10:32:10 AM Be -0.35 -436.41 ug/L 42.89968 -650.492 -355.4

"'m c, 1 00912.SA12-1 S 10/5/2010 10:35:59 AM Be 834.62 1034061.85 ug/L 1.944963 1012731 10367

~)> l>o l 00912.SA13-1 10/5/2010 10:37:38 AM Be -0.17 -208.79 ug/L 51.86936 -87.8084 -241.8

(/)"\J;o 1 00912.SA13-1 D 10/5/2010 10:38:27 AM Be -0.50 -618.37 ug/L 18.61515 -603.902 -740.0

m';m -ozs: 1 00912.SA01-1 10/5/2010 10:39:40 AM Be -0.95 -1171.81 ug/L 21.32379 -975.671 -1453

-l-j- m(l)(l) 

100912.SA02-1 10/5/2010 10:40:49 AM Be -0.97 -1196.82 ug/L 4.530319 -1211.45 -1136

~~!!? 

:;g""~ CCV 10/5/2010 10:42:00AM Be 9B0.65 1214985.81 ug/L 2.280918 1185571 12187

:::0~01 __, N(/)m 

CCB 10/5/2010 10:43:24AM Be -0.96 -1195.28 ug/L 13.79672 -13B1.46 -1136

~):>(/) 100912.SA03-1 10/5/2010 10:44:32 AM Be -0.70 -869.55 ug/L 6.624992 -B03.657 -894.6

oC:_, (1)"0 

[D;!J 100912.411-1 10/5/2010 10:45:45 AM Be -0.85 -1053.02 ug/L 7.630754 -994.70B -1019

co ;o~ 100912.412-1 10/5/2010 10:46:55 AM Be -0.93 -1155.79 ug/L 18.92245 -917.652 -1347

-<m 

,o 100912.413-1 10/5/2010 10:4B:02 AM Be -0.89 -1106.59 ug/L 8.217627 -1001.61 -1157

';-j 

z 100912.401-1 10/5/2010 10:49:15 AM Be -1.14 -1414.46 ug/L 8.063598 -1506.76 -1449

-j 100912.402-1 10/5/2010 10:50:24 AM Be -1.08 -1341.37 ug/l 19.87531 -1094.69 -1305

'" 100912.403-1 10/5/2010 10:51:33 AM Be -1.12 -1390.78 ug/L 17.83337 -1575.77 -1108

100912.512-1 10/5/2010 10:52:48 AM Be -1.10 -1364.12 ug/L 14.02859 -1277.47 -15B3

100912.513-1 10/5/2010 10:53:58 AM Be -0.93 -1153.86 ug/L 6.3083 -1154.94 -122

CCV 10/5/2010 10:55:52 AM Be 983.17 1218106.74 ug/L 1.762433 1194221 12243

)> CCB 10/5/2010 10:57:26 AM Be -1.06 -1314.05 ug/L 23.43513 -1640.37 -1028

" 

m " 100912.501-1 10/5/2010 10:58:34 AM Be -0.88 -1 089 .84 ug/L 24.38381 -1356.38 -1088

z 

D 100912.502-1 10/5/2010 10:59:45 AM Be -1.15 -1424.38 ug/L 15.49932 -1274.32 -1677

x 

" 100912.503-1 10/5/2010 11:00:52 AM Be -1.25 -1549.76 ug/L 10.57344 -1681.51 -1366

)> 

G) 100912.B-2A 10/5/2010 11:03:34 AM Be -1.39 -1721.57 ug/l 7.677297 -1569.73 -181

m 

z 1 00912.SAI1 -2A 10/5/2010 11:04:45 AM Be -1.35 -1672.02 ug/L 8.801809 -1533.03 -1826

0 

"" 100912.SAI2-2A 10/5/2010 ll:OB:52AM Be -1.40 -1731.03 ug/L 23.93414 -1309.74 -2137

"' "' 

Page 69 of 1 03 
,--~ "' -< (") Sample ID Date Time Elem Cone (Com tnt (Corr) Calib Unit! RSD (Corr lnt (Corr)1 lnt (Cor

-u 

;!l 100912.SAI2-2AD 1 0/5/201 0 11 :09 :3B AM Be -1.91 -2371.69 ug/l 2.900062 -236B.72 -2304

0 ~ m 100912.SAI3-2A 10/5/2010 11:10:57 AM Be -1.BO -2231.04 ug/l 6.B25213 -2111.23 -2179.

(") 

-< 1 00912.SA01-2A 10/5/2010 11 :12:04 AM Be -1.95 -2421.58 ug/l 2.893923 -2409.66 -2358

z 

0 CCV 10/5/2010 11:13:53AM Be 1031.04 1277425.59 ug/l 2.929239 1236472 12859

~ CCB 10/5/2010 11:15:20 AM Be -1.30 -1609.02 ug/l 1.871347 -1636.07 -1614.

'" 100912.SA02-2A 10/5/2010 11:16:25 AM Be -1.03 -1279.45 ug/l 21.45955 -1012.85 -1264

.. "' 100912.SA03-2A 10/5/2010 11:17:37 AM Be -1.39 -1718.76 ug/l 24.98555 -1262.53 -1778

100912.411-2A 10/5/2010 11:1B:45AM Be -1 .75 -2169.47 ug/l 10.79273 -2346.26 -1903

100912.411-2AS 10/5/2010 11 :21 :55 AM Be BB0.80 10912B4.57 ug/l 0.857251 10B0638 10950

1 00912.412-ZA 10/5/2010 11:23:18 AM Be -0.84 -1040.60 ug/l 14.27947 -1027.66 -898.8

"' c 100912.413-2A 10/5/2010 11:24:33 AM Be -1.32 -1639.87 ug/l B.596074 -1503.76 -1785

Glm 

c., 100912.401·2A 10/5/2010 11:25:41 AM Be -1.02 ·1261.40 ug/l 7.731743 -1149.55 -1306

~"' 1 00912.402-2A 10/5/2010 11:26:56 AM Be -1.62 -2003.52 ug/l 11.48161 -1759.18 -2215

"'o cn";o 1 00912.403-2A 10/5/2010 11 :2B:04 AM Be -1.81 -2243.1 B ug/l 6.532639 -2115.BS -2210

mr;;m 

-uzs: 1 00912.511-2A 10/5/2010 11:29:16AM Be -1.27 -1569.44 ug/l 11.62309 -1547.74 -1398.

........ - 

men en 1 00912.512-2A 10/5/2010 11:30:23 AM Be -1.7B ·2202.86 ug/L 5.752454 -2168.39 -2343

S:.:..£Q: 

~1<0~ CCV 10/5/2010 11 :35:0B AM Be 1027.58 1273131.69 ug/l 1. 980634 1244028 12B69

?J,?'""-1 -124B.15 ug/l 6.54B459 -1307.26 -1282

"'cnm CCB 10/5/2010 11:38;25 AM Be -1.01 

~)>CI> 1 00912.513-2A 10/5/2010 11:40:07 AM Be -O.BO -988.14 ug/L B.772297 -B8B.193 -1033

or-< 

cn-u 

ro;o 100912.501-2A 10/5/2010 ll:41:14AM Be -1.09 -1349.27 ug/l 15.42865 -1236.52 -122

co ;!l~ 100912.502-2A 10/5/2010 11:42:30 AM Be -1.61 -1997.B2 ug/L 5.628261 -2093.88 -2025

..:m 

.,o 1 00912.503·2A 10/5/2010 11:43:45 AM Be -1.67 ·2069.27 ug/l 9.333365 -1 B55.78 -212

r;;"""' CCV 10/5/2010 11:47:03 AM Be 1052.68 1304229.57 ug/l 0.099951 1303424 13057

z 

-< CCB 10/5/2010 11:48:50 AM Be -1.16 -1440.76 ug/l 14.B5566 -120B.B8 -1482

"' 100912.511-1 10/5/2010 12:2B:17 PM Be -O.B6 -1065.62 ug/l 8.142919 -970.339 -114

CCV 10/5/2010 12:31:24 PM Be 979.57 1213656.86 ug/l 2.31B28 1181753 12242

CCB 10/5/2010 12:32:51 PM Be -1.06 -1318.86 ug/l 1.69781 -1306.29 -1305

Calib Blank 1 10/5/2010 10:16:34AM Cd -132.49 ug/l 1.229192 -130.93 -132.3

"' Standard 1 10/5/2010 10:18:05 AM Cd 8555.16 ug/l l.B84031 8391.224 B560.8

-u -u 

m Standard 2 10/5/2010 10:1B:59AM Cd 1 7502.91 ug/l 1.772913 17154.B5 17603

z 

0 ICY 10/5/2010 10:22:12 AM Cd 1011.12 8B09 .06 ug/l 1.37123 8773.144 8710.3

x 

-u ICB 10/5/2010 1 0:23:4B AM Cd -0.74 -6.45 ug/l 83.47427 -11.3631 -0.694

"' Gl ICS 10/5/2010 10:24:58 AM Cd 0.49 4.23 ug/l 501.4904 -13.2488 27.83

m 

z 100912.LB 10/5/2010 10:26:51 AM Cd -1.28 -11.11 ug/l 111.5213 -13.7362 -21.97

0 

"' 100912.LCS 10/5/2010 10:28:03 AM Cd 8B9.B1 7752.22 ug/l 2.303731 7552.717 7897.1

0 0 

Page 70 of 1 03 
, 

-< C1 

"ll Sample ID Date Time Elem Cone (Calillnt (Corr) Calib Unit• RSD (Corr lnt (Corr)l lnt (Cor

"' 0 100912,8-1 10/5/2010 10:29:40 AM Cd -38,92 -339.05 ug/L 4.03972 -336.571 -326.7

m l00912.SAI1-1 1 0/5/201 0 1 0:30:53 AM Cd -27.94 -243.41 ug/L 4.987089 -229.76 -247.4

C1 

-< 100912.SA12-1 10/5/2010 10:32:10 AM Cd -26.54 -231.26 ug/L 3.828292 -241.321 -224.6

z 0 1 00912.SAI2-1 S 10/5/2010 10:35:59 AM Cd 776.31 6763.34 ug/L 1.668408 6666.422 6736.3

100912.SA13-1 10/5/2010 10:37:38 AM Cd -44.27 -385.72 ug/L 2.180279 -376.894 -386.6

0 

:;: 100912.SA13-1 D 10/5/2010 10:38:27 AM Cd -44.67 -389.21 ug/L 5.182776 -394.838 -405.9

"' l00912.SA01-1 10/5/2010 10:39:40 AM Cd -36.72 -319.87 ug/L 1.902689 -317.546 -326.7

100912.SA02-1 10/5/2010 10:40:49 AM Cd -37.63 -32 7.83 ug/L 5.317551 -322.515 -347.3

CCV 10/5/2010 10:42:00 AM Cd 986.47 8594.31 ug/L 1.027692 8504.876 8681.4

, CC8 10/5/2010 10:43:24 AM Cd -2.77 -24.16 ug/L 69.18013 -8.75221 -41.93

c l00912.SA03-1 10/5/2010 10:44:32 AM Cd -36.61 -318.94 ug/L 2.596308 -325.779 -321.3

Qm c"ll 100912.411-1 10/5/2010 10:45:45 AM Cd -41.66 -362.95 ug/L 4.756988 -375.774 -343.3

»r; 100912.412-1 10/5/2010 10:46:55 AM Cd -44.94 -391.56 ug/L 5.385847 -388.73 -413.9

(/)"ll:U 100912.413-1 10/5/2010 10:48:02 AM Cd -42.41 -369.50 ug/L 6.931806 -376.103 -391.1

m:>:m "llz;s: 100912.401-1 10/5/2010 10:49:15 AM Cd -44.19 -384.97 ug/L 3.742042 -368.534 -390.

.,_,_ m(l)(/) 100912.402-1 10/5/2010 10:50:24 AM Cd -43.86 -382.11 ug/L 3.429107 -381.111 -395.6

100912.403-1 10/5/2010 10:51 :33 AM Cd -44.36 -386.45 ug/L 5.305462 -392.138 -403.5

;:IJ!JI--1 "'(/)m 100912.512-1 10/5/2010 10:52:48 AM Cd -48.43 -421.91 ug/L 3.396627 -423.832 -435.1

0;,.(1) 10/5/2010 10:53:58 AM Cd -41.93 -365.26 ug/L 2.308659 -370.136 -370.1

c;c:--1 100912.513-1 (l)"ll 

"'"' CCV 10/5/2010 10:55:52 AM Cd 983.30 8566.67 ug/L 1.745077 8405.067 8594.9

co CCB 10/5/2010 10:57:26 AM Cd -4.67 -40.69 ug/L 28.16097 -27.7277 -44.85

-<m "llC1 100912.501-1 10/5/2010 10:58:34 AM Cd -42.34 -368.88 ug/L 2.201491 -375.532 -371.2

:;;"" 

z 100912.502-1 10/5/2010 10:59:45 AM Cd -49.68 -432.83 ug/L 0.699957 -434.73 -429.3

-< 100912.503-1 10/5/2010 11:00:52 AM Cd -45.39 -395.48 ug/L 3.602873 -385.415 -411.7

'" 

100912.B-2A 10/5/2010 11:03:34 AM Cd -5.75 -50.09 ug/L 11.95658 -50.166 -44.05100912.SAI1-2A 10/5/2010 11:04:45 AM Cd -5.40 -47.02 ug/L 16.66149 -44.4719 -55.8

1 00912.SA12-2A 10/5/2010 11:08:52 AM Cd -3.08 -26.81 ug/L 34.83773 -35.4668 -28.03

100912.SA12-2AD 10/5/2010 11:09:38 AM Cd ·2.55 -22.24 ug/l 25.28853 -28.7108 -19.41

, "ll 1 00912.SA13-2A 10/5/2010 11:10:57 AM Cd -0.69 -6.00 ug/l 207.8847 2.94467 -20.23

"ll 

m 100912.SA01-2A 10/5/2010 11:12:04 AM Cd -0.15 -1.29 ug/L 629.9419 -8.87348 7.3267

z 

0 CCV 10/5/2010 11:13:53 AM Cd 1045.77 9110.97 ug/L 0.633439 9044.816 9150.9

x 

, 

"ll CCB 10/5/2010 11:15:20 AM Cd -0.32 -2.80 ug/L 594.0882 -21.9545 7.7766

Q 

m 1 00912.SA02-2A 10/5/2010 11:16:25AM Cd -0.71 -6.15 ug/L 177.7339 -11.626 -13.25

z 100912.SA03-2A 10/5/2010 11:17:37 AM Cd 0.05 0.47 ug/L 2040.799 -3.06775 -6.843

0 

'" 100912.41l-2A 10/5!2010 11:18:45AM :1 Cd -0.48 -4.19 ug/L 132.6703 0.03505 -10.4

Page 71 of 103 
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Sample ID Date Time 

1 00912.411 -2AS 10/5/2010 11 :21 :55 AM 100912.412-2A 10/5/2010 11:23:18AM 100912.413-2A 10/5/2010 11:24:33 AM 1 00912.401-2A 10/5/2010 11:25:41 AM 

1 00912.402-2A 10/5/2010 11:26:56 AM 1 00912.403-2A 10/5/2010 11:28:04 AM 

100912.511-2A 10/5/2010 11:29:16 AM 

1 00912.512-2A 10/5/2010 11:30:23 AM 

CCV 1 0/5/2010 11 :35:08 AM 

CCB 10/5/2010 11 :38:25 AM 

100912.513-2A 10/5/2010 11:40:07 AM 

100912.501-2A 10/5/2010 11:41:14AM 100912.502-2A 10/5/2010 11 :42:30 AM 

1 00912.503-2A 10/5/2010 11:43:45 AM 

CCV 10/5/2010 11:47:03 AM CCB 10/5/2010 11:48:50 AM 

100912.511-1 10/5/2010 12:28:17 PM 

CCV 10/5/2010 12:31:24 PM CCB 10/5/2010 12:32:51 PM 

Elem Cone (Calil lnt (Corr) Calib Unit• RSD (Carr lnt (Corr)l lnt (Co

Cd 885.57 7715.29 ug/L 0.641719 7719.7 7762.

Cd 0.00 0.01 ug/L 79705.12 6.68496 3.411Cd 1.47 12.80 ug/L 99.85767 20.92964 19.38Cd 1.40 12.18 ug/L 46.4679 16.28239 14.5Cd 0.36 3.11 ug/l 219.9001 6.834735 -4.78Cd 0.20 1.74 ug/l 284.1597 -3.73159 3.085Cd -1.10 -9.62 ug/L 43.92717 -14.4181 -6.44Cd -0.59 -5.12 ug/L 293.8777 11.84857 -16.8Cd 1043.35 9089.87 ug/L 2.949826 8835.03 9065.

Cd 1.82 15.85 ug/L 78.85552 1.876989 25.95Cd 0.61 5.34 ug/L 307.7124 11.47876 17.81

Cd 2.39 20.81 ug/L 50.87135 31.79144 10.66Cd 0.57 4.96 ug/L 100.2765 10.61929 2. 939Cd 2.05 17.89 ug/L 13.60458 15.3726 18.06

Cd 1077.74 9389.45 ug/L 0.073816 9393.455 9393.Cd 1.89 16.44 ug/L 34.80179 9.877307 19.05Cd -36.73 -320.03 ug/L 6.571884 -299.528 -341.Cd 990.31 8627.76 ug/L 1.54554 8474.235 8694.Cd 1.04 9.05 ug/L 167.6688 26.40036 2.511

Page 72 of 1 03 
)> Sample 10 Elem Date Time Abs (Corr Cone (Calil RSD (Cone: Special So Special Co Cone (Calil C

-< Co 9/30/2010 () Calib Blank 11:37:46 AM 0.000 0 '1l 

20 ppb Co Co " 0 9/30/2010 11:43:34 AM 0.046 0 ~ m 50 ppb Co Co 9/30/2010 11:49:02 AM 0.117 0 

() 

-< 100ppbCo Co 9/30/2010 12:08:17 PM 0.225 0 

z 200 ppb Co Co 9/30/2010 12:15:29 PM 0.435 0 ~ ICY Co 9/30/2010 12:25:43 PM 0.245 107.05 1.18 106.1616 

0 ~ ICB Co 9/30/2010 12:31:11 PM -0.002 -0.65 13.53 -0.58902 

N 100912.L8 Co 9/30/2010 12:36:36 PM -0.001 -0.47 69.62 -0.237 

100912.LCS Co 9/30/2010 1:00:44 PM 0.210 91.62 13.61 100.4359 8

100912.8-1 Co 9/30/2010 1:06:10 PM 0.002 0.68 132.80 1.311698 

)> 1 00912.SAI1-1 Co 9/30/2010 1:11:37PM -0.002 -0.73 43.52 -0.95871 

c l00912.SAI1-1 Co 9/30/2010 1:17:04 PM 0.189 82.12 1.73 1 82.12016 81.11497 8

Glm 

c" 100912.SA12-1 Co 9/30/2010 1:22:34 PM 0.000 -0.02 7231.98 0.791029 

~)> "'i'i 100912 .SA13- 1 Co 9/30/2010 1:27:59 PM 0.001 0.36 71.07 0.179057 0

(/)"" m£:m 100912.SA01-1 Co 9/30/2010 1:33:24 PM -0.001 -0.39 16.76 -0.34399 

'1lzs: Co 9/30/2010 -0.92487 

-<-<- m(/)(1) 100912.SA02-1 1:38:49 PM -0.003 -1.20 32.84 

s:J:Io.'!a 100912.SA03-1 Co 9/30/2010 1:44:14PM -0.002 -0.98 9.51 -1.04227 

~12'>~ 

:::0 5-" -1 CCV Co 9/30/2010 1:55:10 PM 0.243 106.09 2.13 107.6882 

N(f)m ~):>C/) CCB Co 9/30/2010 2:00:37 PM -0.002 -0.76 60.77 -0.43555 

oc=-1 (1)'1l 

100912.411-1 Co 9/30/2010 2:06:01 PM -0.001 -0.22 256.79 -0.61746 0

"'" co 100912.412-1 Co 9/30/2010 2:11:47 PM 0.000 0.10 423.67 -0.20697 0

,~ ..;m 100912.413-1 Co 9/30/2010 2:17:11 PM -0.001 -0.44 236.46 -1.16857 0

"() 

r;;-< 100912.401-1 Co 9/30/2010 2:22:38 PM -0.002 -0.80 8.66 -0.85086 

z 

-< 100912.402-1 Co 9/30/2010 2:28:05 PM -0.001 -0.32 57.28 -0.18919 

0> 

100912.403-1 Co 9/30/2010 2:33:33 PM -0.002 -0.99 103.13 -0.2679 

100912.512-1 Co 9/30/2010 2:39:00 PM -0.003 -1.49 18.34 -1.68261 

100912.513-1 Co 9/30/2010 2:44:27 PM -0.004 -1.54 0.44 -1.53726 

100912.501-1 Co 9/30/2010 2:49:53 PM -0.005 -2.22 20.99 -1.88752 

)> CCV Co 9/30/2010 3:10:03 PM 0.198 86.17 3.94 83.76868 8

'1l '1l 

m CCB Co 9/30/2010 3:15:32 PM 0.003 1.19 6.35 1.245261 

z 

0 100912.502-1 Co 9/30/2010 3:20:58 PM 0.000 -0.15 64.91 -0.08066 

x 

'1l 100912.503-1 Co 9/30/2010 3:26:25 PM 0.000 0.13 47.43 0.084028 0

)> Gl 

m CCV Co 9/30/2010 4:27:32 PM 0.183 79.83 1.58 78.94037 

z CC8 Co 9/30/2010 4:33:21 PM 0.001 0.60 145.46 1.208041 

0 

0> Colib Blank Co 10/1/2010 7:54:20 AM 0.000 0 0 

'"' 20 ppb Co Co 10/1/2010 7:59:47 AM 0.048 0 

Page 73 of 1 03 
)> Sample ID Elem Date Time Abs (Corr Cone (Calil RSD (Cone: Special Sa Special Ca Cone (Cali' C

--< 0 50 ppb Co Co 10/1/2010 8:05:36 AM 0.120 0 

" 100 ppb Co Co 10/1/2010 8:11:02 AM 0.232 0 ;I] 0 

L m 200 ppb Co Co 10/1/2010 8:16:28 AM 0.409 0 

0 

--< ICY Co 10/1/2010 8:27:53 AM 0.235 101.3 1.4 100.278 

z 

0 ICB Co 1 0/l/201 0 8:33:22 AM 0.001 0.5 141.6 0.952 

100912.8-2A Co 10/l/2010 8:39:09 AM -0.001 -0.6 86.0 -0.222 

:l 

... 

1 00912.SA12-2A Co 10!1/2010 8:55:29 AM 0.003 1.2 56.9 1.652 

"' l00912.SAI3·2A Co 10/1/2010 9:00:56 AM 0.000 0.0 537.6 0.138 

100912.5A01-2A Co 10/1/2010 9:18:15 AM 0.003 1.1 85.3 1.758 

1 00912.SA02-2A Co 10/1/2010 9:23:41 AM 0.001 0.6 113.8 1.025 

)> 1 00912.SA03-2A Co 10/1/2010 9:29:05 AM -0.001 -0.2 258.6 0.194 

c 

Glm 100912.411·2A Co 10/1/2010 9:34:52 AM 0.001 0.3 122.5 0.609 

c, 100912.412-2A Co 10/1/2010 9:40:16 AM 0.000 0.2 120.5 0.285 

"'n 1 00912.413-2A Co 1 0/l/201 0 9:45:41 AM 0.000 0.0 2005.2 0.200 

w";ll 

m<;;m 100912.401-2A Co 10/1/2010 9:51:05 AM 0.038 15.8 5.2 15.252 

-uzs: 100912.402-2A Co 10/l/2010 9:56:31 AM O.Dl8 7.5 8.6 7.067 

--<--<- 

mwW 

CCV Co 10/l/2010 10:01:57 AM 0.232 99.7 0.2 99.903 

;;IJ_Ul -1 CCB Co 10/1/2010 10:07:25 AM -0.001 -0.5 97.3 -0.861 

"'wm 

Calib Blank Co 10/1/2010 11:21:27 AM 0.019 0 

or-< 

Cf)"U 20 ppb Co Co 10/1/2010 11:26:54 AM 0.038 0 

CD;Il 

co 50 ppb Co Co 10/l/2010 11:32:22 AM 0.103 0 ;IJL 

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,o lOOppbCo Co 10/1/2010 11:37:51 AM 0.199 0 r;;"" 200 ppb Co Co 10/l/2010 11:43:16AM 0.369 0 z 

--< ICY Co 10/l/2010 11:51:49 AM 0.192 98.9 6.9 94.030 

"' ICB Co 10/1/2010 11:57:17 AM 0.005 2.6 80.6 4.038 

100912.403-2A Co 10/1/2010 12:13:41 PM 0.011 5.4 1.0 5.445 

100912.511·2A Co 10/1/2010 12:19:10 PM -0.002 -1.2 35.2 -1.550 

1 00912.512·2A Co 10/1/2010 12:24:39 PM -0.006 -3.0 49.7 -1.939 

)> 100912.513-2A Co 10/1/2010 12:30:10 PM -0.003 -1.4 42.2 -1.007 

" " m 100912.501-2A Co 10/l/201 0 12:35:40 PM 0.001 0.4 310.3 1.363 

z 

0 1 00912.502-2A Co 10/1/2010 12:41:09 PM 0.001 0.5 39.4 0.358 

x 

" 1 00912.503·2A Co 10/1/2010 12:46:37 PM ·0.003 -1.4 186.7 -3.297 

)> Gl 

m CCV Co 10/1/2010 1:24:27 PM 0.176 90.6 1.6 89.558 

0 

z CCB Co 10/1/2010 1:30:18PM 0.001 0.6 25.6 0.522 

"' 0 100912.SAI1·2A Co 1 0/l/201 0 1:46:50 PM -0.003 -1.3 87.5 30 -0.503 ... 1 00912.SAil-2A Co 10/1/2010 1:52:16 PM 0.153 78.3 0.8 30 78.3 77.891 

Page 74 of 103 
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Sample ID Elem Date 

CCV Co 10/1/2010 

CCB Co 10/1/2010 

Calib Blank Co 10/7/2010 

20 ppb Co Co 10/7/2010 

50 ppb Co Co 10/7/2010 

100 ppb Co Co 10/7/2010 

200 ppb Co Co 10/7/2010 

ICY Co 10/7/2010 

ICB Co 10/7/2010 

100912.511-1 Co 10/7/2010 

CCV Co 10/7/2010 

CCB Co 10/7/2010 

Time Abs (Corr Cone (Calii RSD (Cone Special Sa Special Co Cone (Cali! C

1:57:42 PM 0.167 85.9 2.3 84.451 

2:03:32 PM 0.002 1.1 186.8 2.617 

1:53:28 PM 0.00043 0 

1:58:54 PM 0.03442 0 

2:04:21 PM 0.0859 0 

2:09:49PM 0.17017 0 

2:15:13 PM 0.29568 0 

2:22:52 PM 0.16752 98.4 1.4 97.416 

2:28:18 PM 0.00147 0.9 23.3 0.996 

2:33:46 PM 0.00088 0.5 16.5 0.450 

2:39:15 PM 0.16699 98.0 1.1 98.828 

2:44:41 PM 0.00015 0.1 502.5 -0.222 

Page 75 of 103 
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0 

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Sample ID 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

100912.LB 

1 00912.LCS 

100912.8-1 

1 00912.SA11-1 

1 00912.SAI2-1 

1 00912.SA12-1 S 

1 00912.SAI3-1 

100912.SAI3-1D 

100912.SA01-1 

1 00912.SA02-1 

CCV 

CCB 

1 00912.SA03-1 

100912.411-1 

100912.412-1 

100912.413-1 

100912.401-1 

100912.402-1 

100912.403-1 

100912.512-1 

100912.513-1 

CCV 

CCB 

100912.501-1 

100912.502-1 

100912.503-1 

CCV 

Date 

10/1/2010 

10/1/2010 

10/1/2010 

1 0/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

Time 

10:12:10 AM 

10:14:11 AM 

10:15:06 AM 

10:16:08 AM 

10:17:32 AM 

10:19:09 AM 

10:20:40 AM 

10/1/2010 10:21:45 AM 

1 0/1/201 0 10:24:19 AM 

1 0/1/201 0 10:26:04 AM 

10/1/2010 10:30:38 AM 

10/1/2010 10:32:37 AM 

10/1/2010 10:34:51 AM 

10/1/2010 10:35:38AM 

10/1/2010 10:37:49AM 

1 0/1/2010 

1 0/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

1 0/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

1 0/1/2010 

10:39:01 AM 

10:41:09 AM 

10:42:26 AM 

10:43:35 AM 

10:45:18 AM 

10:46:45 AM 

10:49:44 AM 

10:51:26 AM 

10:52:52 AM 

10:54:07 AM 

10:55:37 AM 

10:57:08 AM 

10:58:42 AM 

11:00:09 AM 

11:01:16 AM 

11:02:25 AM 

11:03:37 AM 

11:05:04 AM 

Elem Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr)l lnt (Corr)

Cr 168.829 ug/L 3.05 168.946 173.917

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

16303.31 ug/L 

32442.64 ug/L 

1009.60 16393.67 ug/L 

0.49 7.885636 ug/L 

0.86 13.9741 ug/L 

1.17 19.05121 ug/L 

953.66 15485.19 ug/L 

20.80 337.7138 ug/L 

16.91 274.6391 ug/L 

23.76 385.8631 ug/L 

964.69 15664.41 ug/L 

24.12 391.588 ug/L 

25.30 410.7741 ug/L 

16.40 266.3105 ug/L 

13.45 

1022.82 

1.60 

14.19 

24.19 

21.61 

22.69 

21.56 

22.26 

26.97 

18.87 

20.32 

1052.60 

2.06 

218.3945 ug/L 

16608.19 ug/L 

25.9962 ug/L 

230.4006 ug/l 

392.8074 ug/L 

350.8375 ug/L 

368.353 ug/l 

350.1555 ug/L 

3 61.4087 ug/L 

437.9897 ug/L 

306.4275 ug/L 

330.0007 ug/L 

17091.84 ug/l 

33.437 ug/L 

20.12 326.7194 ug/l 

16.28 264.3521 ug/L 

16.16 262.4098 ug/l 

1038.25 16858.82 ug/L 

Page 76 of 103 

1.21 16188.03 16190.9

0.35 32414.54 32347.3

3.10 15842.1 16845.0

135.78 19.96992 4.10453

30.86 14.93038 9.26388

102.63 36.42879 22.8450

0.53 15397.41 15560.6

3.35 337.9967 348.886

1.88 269.4557 279.783

3.78 374.824 402.412

1.47 15402.85 15750.9

4.78 380.2094 381.345

2.01 411.7394 402.094

3.14 269.2422 272.814

9.78 202.0057 242.544

0.68 16508.49 16731.1

82.53 10.12821 17.4554

4.43 242.0227 222.877

2.04 383.8103 395.422

3.20 348.5556 340.917

3.03 365.5151 380.663

4.19 363.3398 352.767

2.63 372.3882 356.068

3.67 421.0543 453.055

6.82 324.4135 311.355

1.82 332.2048 334.604

1.08 16924.49 17061.

36.91 27.01704 25.6270

2.00 329.1812 319.321

7.71 249.7263 287.630

0.85 262.8045 264.412

1.34 16614.85 17060.2
,. 

c 

,. 

-; 

0 

"0 

m 

'1 

z 0 

:!: 

:1 

t; 

Gl 

em 

(/)" -;:» 

""o 

en""' mlj;m 

-uz;:: -<-;- men'" 

oo,.,o 

- -; "-'cnm 

:;:>en or-< 

C/i"O 

"'"' co 

-<m 

.,o s;-; 

"' 

,. 

-u -u 

m 

z 

D 

x 

"0 

i!l 

m 

z 

"' 0 " 

Sample ID 

CCB Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

100912_B-2A 

1 00912_$Ail-2A 

l00912.SA12-2A 

100912.SAI2-2AS 100912_SAI3-2A 

l00912.SA13-2AD 

100912.SA01-2A 

CCV 

CCB 

l00912.SA02-2A 

1 00912.SA03-2A 1 00912.41l-2A 100912.412-2A 1 00912.413-2A 

100912.401-2A 

1 00912.402 -2A 

1 00912.403-2A 

100912.51l-2A 

1 00912.512-2A 

CCV 

CCB 

1 00912.513-2A 1 009l2_501-2A 100912_502-2A 1 00912.503-2A 

CCV 

Date Time 

1 0/1/2010 11 :06:35AM 

10/1/2010 12:17:26 PM 

10/1/2010 12:18:25 PM 

10/1/2010 12:19:17PM 10/1/2010 12:20:21 PM 10/1/2010 12:21:44 PM 

1 0/l /2010 12:22:48 PM 

10/1/2010 10/1/2010 

10/1/201 0 

10/1/2010 

1 0/l /2010 

1 0/l /2010 

10/1/2010 10/1/2010 10/1/2010 

1 0/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 10/1/2010 10/1/2010 10/1/2010 

10/1/2010 

1 0/l /2010 

10/1/2010 10/1/2010 10/1/2010 10/1/2010 

10/l/2010 

1 0/l /2010 

10/1/2010 

10/1/2010 

12:24:10 PM 12:25:25 PM 

12:26:40 PM 12:28:10 PM 

12:34:34 PM 12:35:22 PM 12:37:04 PM 

12:38:57 PM 

12:40:28 PM 

12:41:34 PM 

12:44:20 PM 12:45:50 PM 12:46:57 PM 12:48:02 PM 12:49:42 PM 12:50:47 PM 12:51:58 PM 12:53:37 PM 12:54:50 PM 12:56:26 PM 12:57:48 PM 

12:58:49 PM 

1:00:41 PM 1:01:47 PM 

1:03:20 PM 1:05:04 PM 

Elem Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr)llnt (Corr

Cr 1.76 28.51356 ug/L 6.19 30.01157 28.9602Cr 201.1937 ug/L 3.37 207.2976 202.387

Cr 17390.11 ug/L 2.06 17023.72 17405.2

Cr 35472.13 ug/L 1.49 35062.07 35284.5Cr 1009.10 17827.63 ug/L 0.47 17734.36 17850.4

Cr 0.68 12.02977 ug/L 120.09 0.775871 28.3210Cr 0.60 10.56145 ug/L 67.21 17.3671 3.20214

Cr Cr Cr Cr Cr Cr Cr Cr Cr Cr Cr Cr Cr Cr 

Cr 

Cr Cr Cr 

Cr 

Cr Cr 

Cr 

Cr 

Cr 

Cr Cr 

0.12 2.204475 ug/L 

22.29 393.8609 ug/L 

12.50 220.921 ug/L 

781.23 13801.87 ug/L 

5.54 97.79846 ug/L 

4. 77 84.23407 ug/L 

21.94 387.5539 ug/L 

1033.99 18267.29 ug/L 

-0.71 -12.493 ug/L 

3.28 57.96779 ug/L 

2.14 37.73808 ug/L 

14.86 262.4581 ug/L 

19.28 340.6149 ug/L 

9.84 173.8384 ug/L 

4.87 85.98342 ug/L 

1.56 27.58723 ug/L 

4.34 76.75599 ug/L 

21.10 372.778 ug/L 

8.81 155.5863 ug/L 

1038.96 18355.19 ug/L 

-0.15 -2.62624 ug/L 

3.86 68.20239 ug/L 3.15 55.70868 ug/L 

2. 75 48.56856 ug/L 

2.98 52.5793 ug/L 

1059.78 18722.95 ug/L 

Page 77 of 1 03 

553.89 15.9974 -2.1604

3.16 407.7862 390.025

5.52 211.9839 215.97

0.70 13843.45 13692.0

19.41 76.21264 105.285

12.17 88.52054 91.6424

2.50 398.7467 381.787

0.72 18250.52 18144.9

100.77 -7.14907 -3.4578

17.78 51.88287 52.1523

52.07 37.51562 18.1991

5.44 246.6674 266.20

4.22 326.8395 355.495

8.12 159.7773 173.723

13.72 89.03909 72.9583

53.48 11.20427 31.7326

19.00 73.50951 64.0691

2.62 361.5538 377.606

3.43 155.1646 161.120

0.84 18222.37 18523.6

451.66 8.28553 -0.9126

22.85 50.50822 79.9045

26.77 38.49928 63.8293

15.36 56.60989 47.218117.80 51.97691 62.2274

0.86 18708.49 18890.1
}> 

c ~ () "1l ;u 0 ~ m () --< z ? ~ "l .. "' 

Gl 

em cn"1l -;> 

""o "'"U;u ml:m "1lZS: -<-;- mcn"' ~ .... ~ "'"'0 ~"'z - --< "'cnm s :t.Cil 

or-< 

(ii-u 

tll;!l 

co ;u~ -<m -,Cl ~:--< z 

--< 

"' 

,. "1l "1l 

m 

z 

0 

x 

"1l 

,. 

Gl 

m 

z 

0 

"' 0 "' 

Sample 10 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

100912.511-1 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

1 00912.LB 

100912.LCS 

100912.8-1 

1 00912.SA11-1 

100912.SA12-1 

100912.SA12-1S 

100912.SA13-1 

100912.SA13-1 D 

100912.SA01-1 

100912.SA02-1 

COl 

CCB 

100912 .SA03-1 

100912.411-1 

100912.412-1 

100912.413-1 

100912.401-1 

Date Time 

1 0/1/2010 1 :06:52 PM 

10/5/2010 12:36:02 PM 

10/5/2010 12:37:15 PM 

10/5/2010 12:38:10 PM 

10/5/2010 12:39:45 PM 

10/5/2010 12:41:06PM 

1 0/5/2010 12:42:15 PM 

10/5/2010 12:43:31 PM 

10/5/2010 12:46:40 PM 

10/5/2010 12:48:13 PM 

10/1/2010 10:12:10AM 

10/1/2010 10:14:11 AM 

10/1/2010 10:15:06 AM 

10/1/2010 10:16:08AM 

10/1/201 b 10:17:32 AM 

10/1/2010 10:19:09 AM 

10/1/2010 10:20:40 AM 

10/1/2010 10:21:45AM 

10/1/2010 10:24:19 AM 

10/1/2010 10:26:04 AM 

10/1/2010 10:30:38 AM 

10/1/2010 10:32:37 AM 

10/1/2010 10:34:51 AM 

10/1/2010 10:35:38 AM 

10/1/2010 10:37:49 AM 

10/1/2010 10:39:01 AM 

10/1/2010 10:41 :09 AM 

10/1/2010 10:42:26 AM 

10/1/2010 10:43:35 AM 

10/1/2010 10:45:18AM 

10/1/2010 10:46:45 AM 

10/1/2010 10:49:44 AM 

Elem 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cr 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

10/1/2010 10:51:26AM Cu 

Cone (Calillnt (Carr) Calib RSD (Cor lnt (Corr)llnt (Corr

-0.24 -4.17557 ug/L 228.31 -5.37399 5.9000

216.6773 ug/L 9 _04189 218.4759 196.248

17964.59 ug/L 1.53719 17647.78 18154.3

37266.75 ug/L 0.87768 37034.67 37124.7

97 4.5 18027.0 ug/L 1.46822 17784.42 17987.2

-1.9 -34.9 ug/L 19.7743 -35.46 -41.460

-0.5 -9.3 ug/L 78.1822 -7.50853 -3.083

16.4 

961.8 

304.1 ug/L 4.12212 317.8263 301.101

17793.7 ug/L 1.85689 17442.12 17841.1

-0.6 -11.0 ug/L 

-2405.46 ug/L 

85129.39 ug/L 

1 68499 _1 ug/L 

1011.28 85377.63 ug/L 

-0.20 -16.5093 ug/L 

-0.28 -23.804 ug/L 

-0.74 -62.6935 ug/L 

975.39 82347.96 ug/L 

1. 77 149.4783 ug/L 

53.18 4489.779 ug/L 

52.60 4440.436 ug/L 

1046.50 88350.94 ug/L 

48.09 4059.708 ug/L 

48.98 4135.026 ug/L 

2.16 182.1629 ug/L 

3.34 281.6521 ug/L 

1036.13 87475.61 ug/L 

-0.92 -77.7574 ug/L 

2.87 242.408 ug/L 

3.09 260.6859 ug/L 

1.48 124.6719 ug/L 

2.09 1 76.4825 ug/L 

4.20 354.9151 ug/L 

Page 78 of 103 

96.5139 -20.42 -13.113

0.43 -2401.42 -2417.2

1.06 84442.34 84790.3

0.56 169593.5 167875.

4.36 81901.44 89304.5

307.12 -50.3406 41.7874

68.98 -4.84402 -33.375

45.91 -30.0508 -73.599

1.16 81649.94 83436.2

39.87 86.61381 156.660

2. 72 4360.053 4506.22

2.96 4288.743 4524.63

2.26 86071.33 89171.4

3.31 3916.907 4078

0.18 4135.781 4127.15

25.88 130.185 194.150

6.31 262.3354 285.306

1.39 86946.66 88864.7

17.59 -93.5259 -69.069

0.94 241.9934 240.371

11.14 229.046 286.122

22.47 96.28556 152.292

4.83 168.0359 176.34

3.20 356.6873 342.767
"< (l 

"1J 

;u 

0 ~ m 

(l 

--< 

z ~ ~ 0 

.. 

N 

, 

c 

Glm 

C-, "l» 

""0 

rn""' m):m "1lZS: --<-;- mrntf> 

s::"'"~ 

~?a~ 

::os.n_, Nrnm o,.rn 

0!::--i 

(f>"1J 

'""' co 

;u~ 

-<m 

,o ):--< 

z 

--< 

0> 

, 

"1J 

"1J 

m 

z 

CJ 

x 

"1J ~ m 

z 

0 

0> 

:?: 

Sample 10 

100912.402-1 

100912.403-1 

100912.512-1 

100912.513-1 

CCV 

CCB 

100912.501-1 

100912.502-1 

100912.503-1 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

100912.B-2A 

100912.5Ail-2A 

1 00912.5Al2-2A 

1 00912.SAI2-2AS 

1 00912.SAI3-2A 

1 00912.SA13-2AD 

100912.SA01-2A 

CCV 

CCB 

1 00912.SA02-2A 

100912.SA03-2A 

1 00912.411 -2A 

100912.412-2A 

1 00912.413-2A 

1 00912.401-2A 

1 00912.402-2A 

Date Time 

10/1/2010 10:52:52 AM 

1 0/1/2010 10:54:07 AM 

10/1/2010 10:55:37 AM 

10/1/2010 10:57:08 AM 

10/1/2010 10:58:42 AM 

10/1/2010 11:00:09 AM 

10/1/2010 11:01:16AM 

10/1/2010 11 :02:25AM 

1 0/1/2010 11 :03:37AM 

10/1/2010 11:05:04 AM 

10/1/2010 11:06:35 AM 

10/1/2010 12:17:26 PM 

10/1/2010 12:18:25 PM 

10/1/2010 12:19:17 PM 

10/1/2010 12:20:21 PM 

10/1/2010 12:21 :44 PM 

1 0/1/2010 12:22:48 PM 

10/1/2010 12:24:10 PM 

10/1/2010 12:25:25 PM 

10/1!2010 12:26:40 PM 

10/1/2010 12:28:10 PM 

10/1/2010 12:34:34 PM 

10/1/2010 12:35:22 PM 

10/1/2010 12:37:04 PM 

10/1!2010 12:38:57PM 

10/1/2010 12:40:28PM 

10/1/2010 12:41:34PM 

10/1/2010 12:44:20 PM 

10/1/2010 12:45:50 PM 

10/1/2010 12:46:57 PM 

10/1/2010 12:48:02 PM 

10/1/2010 12:49:42 PM 

10/1/2010 12:50:47 PM 

Elem Cone (Calillnt (Carr) Calib RSD (Cor In! (Corr)l In! (Corr

Cu 2.35 198.4596 ug/l 6. 71 199.3078 211.336

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

Cu 

3.19 

7.61 

7.89 

1042.76 

-0.86 

1.71 

2.60 

2.79 

1028.67 

-1.04 

1005.52 

0.49 

-0.12 

1.44 

26.48 

14.56 

834.77 

16.46 

18.14 

6.30 

1039.32 

0.23 

8.30 

11.12 

6.73 

7.67 

5.72 

10.12 

4.11 

269.4813 ug/L 

642.1255 ug/l 

665.7815 ug/L 

88035.7 ug/L 

-72.6476 ug/L 

144.1516 ug/l 

219.6394 ug/L 

235.8355 ug/L 

86846 ug/L 

-87.7735 ug/L 

-2546.65 ug/L 

89157.63 ug/L 

180990. 1 ug/L 

90726.04 ug/L 

43.98768 ug/L 

-11.084 ug/L 

130.2436 ug/L 

2389.449 ug/L 

1313.919 ug/L 

75319.56 ug/L 

1484.7 48 ug/l 

1637.061 ug/L 

568.309 ug/l 

93775.33 ug/l 

20.49706 ug/L 

7 48.5483 ug/l 

1003.419 ug/L 

607.1799 ug/L 

692.2285 ug/L 

516.5505 ug/l 

912.855 ug/l 

370.9525 ug/L 

Page 79 of 1 03 

2.68 276.1309 270.526

1.36 639.8957 651.724

5.39 640.7735 649.701

0.87 87155.47 88495.6

40.73 -54.3723 -106.78

18.88 17 4.5484 135.865

9.61 230.1904 233.396

6.90 217.1991 243.134

2.17 85289.7 88946.8

26.02 -70.7168 -78.887

1.05 -2529.19 -2533.2

2.11 87351.04 89018.0

1.71 179203.7 179210

0.18 90570.96 90902.8

40.58 23.72101 57.3690

310.83 -50.7804 6.50639

23.36 129.4315 100.237

3.57 2290.86 2437.29

5.82 1226.046 1349.74

1.10 75862.58 74362.1

3.87 1419.081 1525.99

0.77 1650.871 1626.10

3.80 546.3028 589.498

0.93 94046.54 92795.8

81.65 33.68301 1.6682

6.07 710.5937 798.899

5.00 945.861 1026.60

2.34 623.5869 599.813

3.06 673.9517 715.455

7.58 526.09 473.500

4.89 869.1357 911130

18.83 309.6935 356.16
)> 

c ~ (") , " 0 ~ m (") ...; z 0 :!: "' ~ "' "m c, ~)> "'C'i 

cn;!2::U m)>m -oz;;: ...;...;- m"'"' s:.f:o,.~ ~P<>~ :;u _0'1 -! 

"'"'m 0)>(/) 

c;C-i 

(1)"0 

"'" co ,~ -<m 

,n s;...; ~ "' 

)> 

, 

, 

m 

z 

0 

x 

, ~ m 

z 

0 ~ 0 

Sample 10 

100912.403-2A 

100912.511-2A 

1 00912.512-2A 

CCV 

CCB 

1 00912.513-2A 

1 00912.501-2A 

100912.502-2A 

100912.503-2A 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

ICB 

ICS 

100912.511-1 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICV 

ICB 

ICS 

100912.LB 

1 00912.LCS 

100912.8-1 

1 00912.5Ail-1 

1 00912.SA12-1 

100912.SAI2-1 S 

1 00912.SA13-1 

Date Time Elem 

10/1/2010 12:51:58 PM Cu 

1 0/1/2010 12:53:37 PM Cu 

10/1/2010 12:54:50PM Cu 

10/1/2010 12:56:26 PM Cu 

10/1/2010 12:57:48 PM Cu 

10/1/2010 12:58:49 PM Cu 

10/1/2010 1:00:41 PM Cu 

10/1/2010 1 :01:47 PM Cu 

10/1/2010 1 :03:20 PM Cu 

10/1/2010 1 :05:04 PM Cu 

10/1/2010 1 :06:52 PM Cu 

10/5/2010 12:36:02 PM Cu 

10/5/2010 12:37:15 PM Cu 

10/5/2010 12:38:1 0 PM Cu 

10/5/2010 12:39:45 PM Cu 

10/5/2010 12:41:06 PM Cu 

10/5/2010 12:42:15 PM Cu 

10/5/2010 12:43:31 PM Cu 

10/5/2010 12:46:40 PM Cu 

10/5/2010 12:48:13 PM Cu 

10/1/2010 10:12:10AM Mn 

10/1/2010 10:14:11 AM Mn 

10/1/2010 10:15:06AM Mn 

10/1/2010 10:16:08 AM Mn 

10/1/2010 10:17:32 AM Mn 

10/1/2010 10:19:09 AM Mn 

10/1/2010 10:20:40 AM Mn 

10/1/2010 10:21:45 AM Mn 

10/1/2010 10:24:19 AM Mn 

10/1/2010 10:26:04AM Mn 

10/1/2010 10:30:38AM Mn 

10/1/2010 10:32:37 AM Mn 

10/1/2010 10:34:51AM Mn 

Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr) 1 In! (Corr

14.25 1285.595 ug/L 3.35 1235.98 1312.76

7.96 717.8306 ug/L 8.64 647.0503 743.640

6.31 569.5036 ug/L 

1042.96 94103.72 ug/L 

0.18 15.83807 ug/L 

8.70 512.2923 598.691

1.04 93638.59 95223.6

407.24 86.99996 -38.773

8.88 

12.25 

10.78 

10.29 

1065.35 

0.57 

970.1 

-0.5 

-1 .1 

8.2 

960.5 

-0.2 

801.3411 ug/L 5.13 754.8 832.498

1105.417 ug/L 4.09 1054.296 1121.55

972.4859 ug/L 3.67 935.9837 974.207

928.3071 ug/L 10.82 817.0889 955.320

96124.06 ug/L 0.73 96303.53 96723.4

51.30953 ug/L 33.51 35.04834 49.5729

-2336.3 ug/L 1.29831 -2370.33 -2326.4

91537.7 ug/L 1.46043 89994.46 92340

186908.0 ug/L 1.50968 186263 184464

90289.3 ug/L 2.03278 88752.26 89794.2

-47.0 ug/L 29.3681 -34.0408 -61.528

-98.1 ug/L 16.8744 -80.4141 -113.22

765.2 ug/L 5.89608 714.05 782.195

89397.7 ug/L 1.96062 87376 90326.9

-21.6 ug/L 109.077 -35.4879 5 61082

537.3715 ug/L 4.39 538.7164 513.118

217775.9 ug/L 2.10 212518.3 220027

443798.2 ug/L 

999.61 220988.1 ug/L 

0.03 7.025472 ug/L 

-0.70 -153.739 ug/L 

0.11 23.50157 ug/L 

0.17 444245 442927

1.30 218107.3 221002

256.74 26.09894 -9.7556

10.22 -169.252 -154.12

33.64 15.17134 24.4348

946.52 209250.9 ug/L 1.71 205164.9 21182

10.88 2406.283 ug/L 

118.24 26139.4 ug/L 

121.23 26801.37 ug/L 

1042.67 230507.5 ug/L 

123.02 27195.91 ug/L 

Page 80 of 103 

1.73 2441.636 2416.89

2.09 25508.97 26470.8

2.76 25945.72 27230.1

0.62 228991.5 231802

2.40 26449.57 27473.1
)> 

c ~ 0 -u :0 0 ~ m 0 -< z 0 :!:. '" .... "' 

Gl 

em en" _,,. 

>c; (/)-u;o 

m);m 

.,_,_ -uz;:: 

m(/)(f) 

s: .... ~ ro,.o m z 

::tJ_()l --1 

"'(f)m 

~}>en 

or-< 

(ii-u 

"'"' co :o~ -<m 

-,o >"" 

z 

-< 

"' 

)> 

-u 

-u 

m 

z 

0 

x 

-u 

e; 

m 

z ~ ~ Sample ID 100912.SAI3-1D 100912.SA01-1 1 00912.SA02- 1 CCV CCB 100912.SA03-1 100912.411-1 100912.412-1 100912.413-1 100912.401-1 100912.402-1 100912.403-1 100912.512-1 100912.513-1 CCV CCB 100912.501-1 100912.502-1 100912.503-1 CCV CC8 Calib Blank 1 Standard 1 Standard 2 ICY ICB ICS 1 00912.B-2A 100912.SAI1-2A 100912.SA12-2A 1 00912.SA12-2AS 100912.SAI3-2A 1 00912.SAI3-2AD Date Time 10/1/2010 10:35:38 AM 10/1/2010 10:37:49 AM 10/1/2010 10:39:01 AM 10/1/2010 10:41:09 AM 10/1/2010 10:42:26 AM 10/1/2010 10:43:35AM 10/1/2010 10:45:18 AM 10/1/2010 10:46:45 AM 1 0/1 /201 0 1 0:49:44 AM 10/1/2010 10:51:26AM 10/1/2010 10:52:52 AM 10/1/2010 10:54:07 AM 10/1/2010 10:55:37 AM 10/1/2010 10:57:08 AM 10/1/2010 10:58:42 AM 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 10/1/2010 11:00:09 AM 11:01:16AM 11:02:25 AM 11:03:37 AM 11:05:04 AM 11:06:35 AM 12:17:26 PM 12:18:25 PM 12:19:17 PM 12:20:21 PM 12:21:44 PM 12:22:48 PM 12:24:10 PM 12:25:25 PM 12:26:40 PM 12:28:10 PM 12:34:34 PM 12:35:22 PM Elem Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Cone (Colillnt (Carr) Calib RSD (Cor lnt (Corr)llnt (Corr

125.33 27707.68 ug/L 0.29 27647.3 27675.

15.76 3484.25 ug/L 0.55 3501.615 3463.59

13.48 2980.238 ug/L 1.62 2924.573 3008.85

1014.53 224285.6 ug/L 0.39 86.34078 ug/L 19.45 4299.558 ug/L 12.99 2871.655 ug/L 11.99 2651.599 ug/L 14.87 3287.649 ug/L 12.91 2853.113 ug/L 11.79 2606.4 ug/L 12.51 2765.494 ug/L 61.65 13629.84 ug/L 36.20 8003.992 ug/L 1041.13 230167.5 ug/L 0.49 107.7565 ug/L 19.37 4281.202 ug/L 20.46 4522.416 ug/L 22.86 5054.362 ug/L 1037.55 229376.3 ug/L 0.54 118.8628 ug/L 603.3359 ug/L 231403.2 ug/L 475898.9 ug/L 1032.75 244390.9 ug/L 0.06 14.42587 ug/L -0.81 ·192.062 ug/L 0.99 234.1274 ug/L 150.49 35611.67 ug/L 44.73 10584.47 ug/L 806.99 190967.3 ug/L 44.36 10496.75 ug/L 47.23 11176.08 ug/L 

Page 81 of 103 

0.60 222915.3 225602

15.57 77.16582 101.77

1.42 4243.135 4291.36

0.18 2867.608 2877.53

2.22 2583.729 2686.13

1.62 3237.95 3281.10

0.47 2844.035 2868.67

0.70 2619.527 2585.69

1.46 2721.01 2775.46

1.18 13444.89 13723.0

1.36 7890.312 8014.52

1.61 225883.4 232219

33.80 125.2667 65.8815

1.43 4230.757 4263.57

0.85 4485.318 4519.82

0.20 5042.729 5060.43

0.45 230433 228362

4.44 119.0753 113.484

1.46 613.37 596.987

5.05 218029.5 236531

1.75 466957.6 477265

1.31 241612.1 243656

48.86 19.7 4201 6.43079

18.28 -202.12 -153.02

0.78 235.2691 235.089

1.14 35233.99 35560.2

2.74 10251.02 10726.

0.79 189258.2 191553

2.51 10205.45 10567.7

0.46 11210.88 11116.
, 

c 

, ci 

lJ 

0 " 

m 

() 

--i 

z 

p 

" .. N 

Gl 

em 

"'" _,, >() 

en"" mS::m 

lJZS: _,_,_ men"' 

""'z • --i Ncnm 

S::>(/) o!::-1 

"'" "'" co 

-<m 

,o 

r;:;--i 

z 

--i 

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, 

lJ lJ 

m 

z 

0 

x 

lJ 

, 

Gl 

m 

z 

0 

"' N 

Sample ID 

1 00912.SA01-2A 

CCV CCB 

1 00912.SA02-2A 1 00912.SA03-2A 100912.411-2A 1 00912.412-2A 

100912.413-2A 100912 .401-2A 

1 00912 .402-2A 

1 00912.403-2A 

1 00912.511-2A 

100912.512-2A 

CCV 

CCB 

1 00912.513-2A 

100912.50 1-2A 

1 00912.502-2A 

1 00912.503-2A 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Standard 2 

ICY IC8 

ICS 

100912.511-1 

CCV 

ccs 

Calib Blank 1 

Standard 1 Standard 2 

Date 

10/1/2010 

10/1/2010 10/1/2010 10/1/2010 

10/1/2010 

10/1/2010 

10/l/2010 

10/1/2010 10/1/2010 10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/l/2010 

10/1/2010 

10/1/2010 10/1/2010 

10/1/2010 10/5/2010 

1 0/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 

10/5/2010 10/5/2010 

1 0/5/2010 

10/5/2010 

1 0/1/2010 

10/1/2010 

1 0/1/2010 

Time 

12:37:04 PM 12:38:57 PM 

12:40:28 PM 

12:41:34 PM 12:44:20 PM 12:45:50 PM 12:46:57 PM 12:48:02 PM 

12:49:42 PM 

12:50:47 PM 12:51:58 PM 12:53:37 PM 12:54:50 PM 12:56:26 PM 12:57:48 PM 12:58:49 PM 

1:00:41 PM 

1:01:47 PM 1:03:20 PM 1:05:04 PM 1:06:52 PM 

12:36:02 PM 

12:37:15 PM 12:38:10 PM 12:39:45 PM 12:41:06 PM 

12:42:15 PM 

12:43:31 PM 12:46:40 PM 

12:48:13 PM 

10:12:10AM 10:14:11AM 10:15:06 AM 

Elem 

Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn Mn 

Mn 

Mn 

Mn 

Mn Mn Mn Mn Mn Mn Mn Mn Mn 

Mn Mn 

Mn 

Mn 

Mn Mn Mn 

Ni Ni Ni 

Cone (Calillnt (Corr) Calib RSD (Cor tnt (Corr)l lnt (Cor

10.05 2379.211 ug/L 1.46 2351.148 2368.52

1049.43 248337.2 ug/L 0.20 247892 248237

0.09 20.65372 ug/l 8.68 21.00933 18.709

14.44 3417.294 ug/l 2.88 3305.656 3455.

80.18 18973.42 ug/L 1.40 18684.51 19028.

31.84 7533.793 vg/L 1.39 7 41 8. 906 7558.032,89 7783.634 ug/L 1.72 7631.597 7834.14

16.05 3798.15 ug/L 1.00 3757.225 3832.717.94 4244.446 ug/L 3.09 4093.403 4311.41

8.39 1985.71 ug/L 1.33 1955.226 2001.3

17.94 

178.98 

20.72 

1051.14 

0.04 

25.53 

12.08 

108.68 

11.57 

1078.94 

0.10 

976.0 

-0.8 

-1.6 

53.6 

954.0 

-0.8 

4244.781 ug/L 

42354.8 ug/l 

4903.56 7 ug/L 

2487 41.3 ug/L 

1 0.1546 ug/l 

6042.313 ug/L 

2859.695 ug/L 

2571 8.54 ug/L 

2736.798 ug/L 255321.6 ug/L 

23.63793 ug/L 

820.3 ug/l 

249651.6 ug/L 

517926.6 vg/L 

250934.2 ug/L 

-199.2 vg/L 

-401.0 ug/L 

13770.7 ug/L 

245276.1 ug/L 

-201.2 ug/L 

83.11213 ug/L 

9962.101 ug/L 

19954.92 ug/L 

Poge 82 of 1 03 

0.79 4231.499 4219.8

4.76 40106.5 42962.2

2.39 4769.863 4951.7

1.25 245159.4 250238

338.59 46.87051 4.8776

2.62 5875.391 6060.85

3.23 2760.752 2874.5

1.86 25167.63 25965.4

2.54 2657.99 2763.0

0.96 252510.8 256448

59.67 39.49488 18.927

2.05532 820.6927 836.89

1.85034 244858.2 250022

0.8236 514565 516489

0.71784 249052.4 252642

6.11155 -185.178 -205

1.79312 -393.4 -407.69

2.6606 13384.21 13814.7

2.29655 239058.7 246730

10.6199 -214.031 -176.55

17.74 89.38467 93.680

1.26 9926.911 9857.60

0.29 20021.91 19928.
)> 

-< 

0 

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0 ~ m 

0 

-< 

z 

0 

:!: 

0 

.... ~ )> 

c 

Glm C-u 

':1l> 

l>fi 

(f)-u;o 

m't:m 

-uzs: 

-<-.<- m(f)Ul ~.,.~ mi<'O~ :;:o_c.n -1 ~U>m ~>(/) or-< (ii-u 

'""' co ,~ -<m 

-uo 

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0> 

)> 

" " m z 

0 

x ~ m 

z 

p ~ w 

Sample ID 

ICY 

ICB 

ICS 

1 00912.LB 

100912.LCS 

100912.8-1 

100912.SA11-1 

100912.SA12-1 

100912.SA12-1S 

1 00912.SA13-1 

1 00912.SA13-1 D 

100912.SA01-1 

1 00912.SA02-1 

CCV 

CCB 

100912.SA03-1 

100912.411-1 

100912.412-1 

100912.413-1 

100912.401-1 

100912.402-1 

100912.403-1 

100912.512-1 

100912.513-1 

CCV 

CCB 

100912.501-1 

100912.502-1 

100912.503-1 

CCV 

CCB 

Calib Blank 1 

Standard 1 

Date Time 

10/1/2010 10:16:08AM 

10/1/2010 10:17:32AM 

10/l/2010 10:19:09 AM 

10/1/2010 10:20:40 AM 

10/1/2010 10:21:45 AM 

10/1/2010 10:24:19 AM 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/1/2010 

10/l/2010 

10:26:04 AM 

10:30:38 AM 

10:32:37 AM 

10:34:51 AM 

10:35:38AM 

10:37:49 AM 

10:39:01 AM 

10:41:09 AM 

10:42:26 AM 

10:43:35 AM 

10:45:18 AM 

10:46:45 AM 

10:49:44 AM 

10:51:26 AM 

10:52:52 AM 

10:54:07 AM 

10:55:37 AM 

10:57:08 AM 

10:58:42 AM 

11:00:09 AM 

11:01:16AM 

11:02:25 AM 

11:03:37 AM 

11:05:04 AM 

11:06:35 AM 

12:17:26 PM 

12:18:25 PM 

Elem 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni 

Ni ~ Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr)l lnt (Corr

1004.62 1 0020.47 ug/L 4.22 9633.219 10470.9

-2.74 -27.3119 ug/L 104.23 0.610406 -56.293

-2.90 -28.9048 ug/L 41.67 -42.4607 -24.817

-2.67 -26.6271 ug/L 965.03 9625.566 ug/L 6.39 63.7 4098 ug/L 5.58 55.64485 ug/L 8.65 86.30799 ug/L 1053.60 10509.05 ug/L 9.90 98.78951 ug/L 11.35 113.2103 ug/L 6.57 65.49158 ug/L 6.67 66.48454 ug/L 1037.87 10352.12 ug/L -0.2 9 -2.88042 ug/L 8.06 80.39373 ug/L 17.43 173.8104 ug/L 10.15 101.2344 ug/L 13.66 136.2253 ug/L 11.16 111.3123 ug/L 12.64 126.0937 ug/L 16.36 163.2211 ug/L 14.49 144.5416 ug/L 10.27 102.4497 ug/L 1 046.70 1 0440.19 ug/L -2.41 -24.0084 ug/L 8.49 84.72481 ug/L 9.08 90.58308 ug/L 10.66 106.3549 ug/L 1039.52 10368.56 ug/L -0.65 -6.52264 ug/L 72.30098 ug/L 10656.64 ug/L 

Page 83 of 1 03 

95.97 -56.1345 -12.102

0.50 9576.523 9672.20

23.71 81.0845 56.7591

13.34 64.21053 51.5407

42.00 78.44649 125.841

2.23 10246.86 10582.4

11.72 109.4865 86.5007

15.86 133.9331 102.440

15.15 76.33674 56.8782

44.54 77.60399 32.9188

1.13 10306.39 10485.3

140.09 -3.70283 -6.4409

2.95 80.28117 82.8200

2.64 169.5507 178.666

18.04 88.97089 122.217

7.65 145.068 138.865

5.29 104.5966 113.724

26.70 89.99973 131.63

1.44 165.9093 161.502

4.31 151.7238 140.538

22.59 107.2966 122.785

0.79 10345.08 10483.

50.38 -28.7903 -10.253

24.60 92.14653 100.839

13.55 87.45628 80.1744

17.40 113.2798 120.39

1.82 1 0279.72 10585.1

597.64 -48.263 -0.2442

37.37 103.2749 60.0514

1.73 1 0478.32 10645.
,. Sample 10 Date Time Elem Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr)1 lnt (Cor

--< 0 

, 

Standard 2 10/1/2010 12:19:17 PM Ni 21838.99 ug/L 1.11 21641.63 21765.2

" ICY 10/1/2010 12:20:21 PM Ni 1002.38 10892.81 ug/L 0.26 10866.9 10922.6

0 ~ ICB 10/1/2010 12:21:44 PM Ni 0.48 5.265198 ug/L m 0 98.37 2.359601 2.19108

--< ICS 10/1/2010 12:22:48 PM Ni -2.64 -28.7006 ug/L 79.10 -49.7556 -31.697

z 0 

100912.8-2A 10/1/2010 12:24:10 PM Ni 1.54 16.68605 ug/L ~ 217.07 57.77417 2.90943

~ l00912.SA11-2A 10/1/2010 12:25:25 PM Ni 124.32 1351.007 ug/L 1.94 1344.796 1379.70

" '" 1 00912.SAI2-2A 10/1/201 0 12:26:40 PM Ni 24.47 265.947 ug/L 12.26 228.7127 289.376

1 00912.SAI2-2AS 10/1/2010 12:28:10 PM Ni 874.01 9497.789 ug/L 0.76 9580.339 9445.02

1 00912.SA13-2A 10/1/2010 12:34:34 PM Ni 32.49 353.0408 ug/L 8.90 385.715 350.33

100912.SAI3-2AD 

,. 

10/1/2010 12:35:22 PM Ni 36.82 400.107 ug/L 1.71 406.1725 392.708

Glm 

c 1 00912.SAO 1-2A 1 0/l/20 10 12:37:04 PM Ni 114.49 1244.109 ug/L 0.33 1246.522 1239.38

c, CCV 10/1/2010 12:38:57 PM Ni 1035.83 11256.32 ug/L 1.70 1 1438.02 11056.4

~~ CCB 1 0/l/201 0 12:40:28 PM Ni 1.79 19.45292 ug/L 138.59 17.53324 47.3205

en"" m'>m 1 00912.SA02-2A 1 0/1/2010 12:41:34 PM Ni 12.86 139.7204 ug/L 7.39 129.1435 149.779

-oz.: --<-;- 1 00912.SA03-2A 10/1/2010 12:44:20 PM Ni 9.94 108.0349 ug/L 28.50 72.93783 120.64

men en S:.:..S2 

1 00912.411-2A 10/1/2010 12:45:50 PM Ni 9.36 101.7652 ug/L 17.60 82.36591 117.677

~Qo~ 

:::o.?J _, 100912.412-2A 10/1/2010 12:46:57 PM Ni 15.79 171.6385 ug/L 5.65 182.8062 165.355

"enm 

o,.en 100912.413-2A 1 0/l/201 0 12:48:02 PM Ni 12.82 139.3656 ug/L 24.53 150.7223 166.435

c;,-1 

(ii"O 100912.401-2A 10/1/2010 12:49:42 PM Ni 11.69 127.0799 ug/L 13.65 121.5341 146.516

"'" co ,~ -<m 1 00912.402-2A 1 0/l/201 0 12:50:47 PM Ni 3.83 41.58458 ug/L 50.26 19.78833 61.4562

,o 100912.403-2A 1 0/l/201 0 12:51 :58 PM Ni 8.24 89.55354 ug/L 16.51 84.66562 106.163

,...--< ,. 

100912.51l-2A 10/1/2010 12:53:37 PM Ni 17.30 187.997 ug/L 12.99 164.2734 213.072

z --< 

"' 1 00912.512-2A 10/1/2010 12:54:50 PM Ni 7.02 76.29717 ug/L 14.18 77.04405 86.7248

CCV 10/1/2010 12:56:26 PM Ni 1045.05 11356.52 ug/L 0.69 11359.57 11433.4

CCB 10/1/2010 12:57:48 PM Ni 0.22 2.406904 ug/L 612.04 9.655177 12.1095

1 00912.513-2A 10/1/2010 12:58:49 PM Ni 6.51 70.74254 ug/L 11.45 73.34055 77.2231

,. 1 00912.501-2A 10/1/201 0 1:00:41 PM Ni 5.46 59.29589 ug/L 19.12 52.97378 52.5309

, , 

z 

m 100912.502-2A 10/1/2010 1:01:47 PM Ni 4.76 51.71881 ug/L 19.49 57.97878 57.0872

CJ 

x 100912.503-2A 10/1/2010 1:03:20 PM Ni 7.57 82.28038 ug/L 23.54 96.97914 60.3326

, CCV 10/1/2010 1:05:04 PM Ni 1067.11 11596.25 ug/L 1.06 11652.63 11681.3

,. Gl CCB 10/1/2010 1:06:52 PM Ni 0.85 9.216456 ug/L 216.95 25.97854 -12.914

m z 

Calib Blank 1 0 10/5/2010 12:36:02 PM Ni 67.2 ug/L 6.80571 69.5328 61.9101

t "' Standard 1 10/5/2010 12:37:15 PM Ni 10841.9 ug/L 0.78458 10749.29 10859.7

Page 84 of 1 03 
,. Sample ID Date Time Elem Cone (Cali lint (Corr) Calib RSD (Cor lnt (Corr)l lnt (Corr

-1 

0 

., Standard 2 10/5/2010 12:38:10 PM Ni 22365.8 ug/l 1.67618 22375.74 21985.9

:0 

0 ICY 1 0/5/201 0 12:39:45 PM Ni 971.8 10800.8 ug/l 2.10886 10560.42 10828.6

'-

ICB 10/5/2010 12:41:06 PM Ni m 0 1.4 15.2 ug/L 77.2807 1.682398 20.9860

-1 

z ICS 10/5/2010 12:42:15 PM Ni -0.7 -8.1 ug/l 270.463 -31.4295 11.9852

0 100912.511-1 10/5/2010 12:43:31 PM Ni 122.5 ug/l 21.2411 ~ 11.0 98.84044 150.360

"' CCV 10/5/2010 12:46:40 PM Ni 961.0 1 0681 .4 ug/l 1.99628 10436.72 10827.3

.. CCB 10/5/2010 12:48:13 PM Ni 1.6 18.3 ug/l 88.9252 2.270081 17.8271

"' 

Calib Blank 1 10/1/2010 10:12:10 AM Zn 222.259 ug/L 6.27 215.561 238.278

Standard 1 10/1/2010 10:14:11 AM Zn 10909.56 ug/L 1.93 10821.63 10757.

,. 

Standard 2 10/1/2010 10:15:06AM Zn 21748.74 ug/l 0.46 21769.85 21639.4

c 

Glm ICY 10/1/2010 10:16:08 AM Zn 1019.00 11088.18 ug/l 3.06 10725.53 11397.

c., ~,. ICB 10/1/2010 10:17:32 AM Zn 1.29 14.09041 ug/l 11.67 13.05439 15.9856

l>(i (}).,, ICS 10/1/2010 10:19:09 AM Zn 4.16 45.22595 ug/L 16.31 36.88456 47.9139

m<;;m 100912.LB 10/1/2010 10:20:40 AM Zn 1.21 13. 161 05 ug/L 14.08 13.40253 14.8820

'UzS: 

_,_,_ m(})(}) 100912.lCS 10/1/2010 10:21:45 AM Zn 878.45 9558.7 47 ug/l 0.88 9513.269 9655.35

s:;:AQ? 100912.8-1 1 0/1/2010 10:24:19 AM Zn 23.18 252.2405 ug/l 3.85 244.3223 263.086

~Qo~ 

;;u 5'1 -1 100912.SAI1-1 10/1/2010 10:26:04AM Zn 242.31 2636.703 ug/l 1.59 2589.315 2651.60

"'(})m o,.(}) 

100912.SA12-1 10/1/2010 10:30:38 AM Zn 240.66 2618.701 ug/L 3.04 2527.197 2657.1

Or-_, 

(})'U 1.67 11976.79 12320.4

"''" co 100912.SA12-1S 10/1/2010 10:32:37 AM Zn 1122.28 12212.02 ug/L 

:0'-

-<m 1 00912.SA13-1 10/1/2010 10:34:51 AM Zn 219.29 2386.19 ug/L 2.80 2309.177 2420.32

(l 1 00912.SA13-1 D 10/1/2010 10:35:38 AM Zn 223.02 2426.728 ug/l 0.52 2420.683 2418.34

-1 

z 100912.SA01-1 10/1/2010 10:37:49 AM Zn 29.78 324.0067 ug/L 0.38 324.2322 325.106

'" 1 00912.SA02-1 10/1/2010 10:39:01 AM Zn 29.91 325.4985 ug/L 1.53 326.2018 320.216

CCV 10/1/2010 10:41:09 AM Zn 1026.60 11170.88 ug/L 1.65 10961.8 11310.

CCB 10/1/2010 10:42:26 AM Zn -0.60 -6.57038 ug/l 29.94 -7.51514 -4.3089 

100912.SA03-1 10/1/2010 10:43:35 AM Zn 43.1 0 468.9953 ug/l 1.59 464.8466 464.532

,. 100912.411-1 10/1/2010 10:45:18 AM Zn 26.08 283.8327 ug/L 5.27 271.6744 279.296

., ., 

m 

z 100912.412-1 10/1/2010 10:46:45 AM Zn 23.77 258.6666 ug/l 3.37 253.2597 268.713

0 

x 100912.413-1 10/1/2010 10:49:44 AM Zn 23.32 253.8062 ug/l 1.71 255.8357 256.7525 

., 100912.401-1 10/1/2010 10:51:26 AM Zn 28.50 310.1117 ug/l 1.10 312.5237 306.196 

,. Gl 100912.402-1 10/1/2010 10:52:52 AM Zn 25.07 272.8099 ug/L 2.66 267.0368 270.430

m z 

0 100912.403-1 10/1/2010 10:54:07 AM Zn 24.51 266.6679 ug/l 4.18 279.4161 258.8098 

'" ~ 100912.512-1 10/1/2010 10:55:37 AM Zn 41.29 449.299 ug/l 2.28 438.6881 459.1241 

Page 85 of 1 03 
---

,. Sample ID Date Time Elem Cone (Calillnt (Corr) Calib RSD (Cor lnt (Corr)1 lnt (Corr

-< 

0 100912.513-1 10/1/2010 " 10:57:08 AM Zn 41.56 452 .1948 ug/L 0.49 453.2199 453.701

"' 0 CCV 10/1/2010 10:58:42 AM Zn 1054.35 11472.82 ug/L 0.74 11374.48 11527.5

~ 0 rn CCB 10/1/2010 11:00:09 AM Zn -1.13 -12.296 ug/L 60.72 -14.9779 -18.050

-< 

z 100912.501-1 10/1/2010 11:01:16AM Zn 39.50 429.8616 ug/L 2.50 421.0553 426.702

0 ~ 100912.502-1 10/1/2010 11:02:25 AM Zn 27.93 303.9576 ug/L 4.45 318.0971 291.153

'" 100912.503-1 10/1/2010 11:03:37 AM Zn 23.95 260.5848 ug/L 4.69 246.6914 269.661

.. N CCV 10/1/2010 11:05:04 AM Zn 1046.83 11390.96 ug/L 1.50 11211.54 11552.5

CCB 10/1/2010 11:06:35 AM Zn -1.49 -16.1793 ug/L 24.24 -16.5522 -19.90

Calib Blank 1 10/1!2010 12:17:26 PM Zn 200.7729 ug/L 2.75 206.8627 196.104

,. Standard 1 10/1/2010 12:18:25 PM Zn 11961.37 ug/L 3.06 11584.32 11985.6

c 

Glrn Standard 2 10/1/2010 12:19:17PM Zn 24359.99 ug/L 2.05 23926.03 24247.0

c., ~,. ICY 10/1/2010 12:20:21 PM Zn 1009.94 12256.89 ug/L 0.97 12122.18 12301.9

"'" IC8 10/1/2010 12:21:44 PM Zn -0.13 -1.57325 ug/L 573.42 2.044121 5.07793

(})""' rn<;rn ICS 10/1/2010 12:22:48 PM Zn 4.87 59.10245 ug/L 15.04 50.51737 58.5274

" z s: -<.,- 1 00912.8-2A 10/1/2010 12:24:10 PM Zn 2.72 32.97821 ug/L 10.16 30.73273 31.370

rn(})(}) 

s::~~ 

~go~ 1 00912.SAJ1-2A 10/1/2010 12:25:25 PM Zn 84.13 1021.043 ug/L 0.42 1021.536 1025.03

::0.01..., N(})rn 1 00912.SAJ2-2A x2 10/1/2010 12:26:40 PM Zn 15.99 194.0335 ug/L 2.63 199.6997 192.629

o,_(}) c;r--1 100912.SA12-2AS x2 10/1/2010 12:32:26 PM Zn 930.52 11293 ug/L 0.63 11215.35 11355

(ii"!J 1 00912.SAJ3-2A 10/1/2010 12:34:34 PM Zn 18.22 221.1248 ug/L 7.17 204.6397 222.491

OJJl co ,~ ..:rn 1 00912.SAI3-2AD 10/1/2010 12:35:22 PM Zn 19.46 236.1457 ug/L 8.27 242.5321 214.213

(:J 1 00912.SA01-2A 10/1/2010 12:37:04 PM Zn 13.80 167.4663 ug/L 5.00 167.0835 159.291

z CCV 10/1/2010 12:38:57 PM Zn 1027.36 12468.29 ug/L 0.80 12441.63 12384.0

-< 

"' CCB 10/1/2010 12:40:28 PM Zn -0.15 -1.81118 ug/L 185.19 2.038204 -3.3663

100912.SA02-2A 10/1!2010 12:41:34 PM Zn 22.05 267.6318 ug/l 4.48 255.0851 278.956

100912.SA03-2A 10/1/2010 12:44:20 PM Zn 18.27 221.7448 ug/l 7.05 235.9173 224.352

1 00912.411-2A 10/1/2010 12:45:50 PM Zn 23.34 283.2846 ug/l 2.47 284.3981 289.651

,. 1 00912.412-2A 10/1/2010 12:46:57 PM Zn 38.81 471.0484 ug/L 5.84 443.0748 498.088

" " rn 

z 100912.413-2A 10/1/2010 12:48:02 PM Zn 29.51 358.1905 ug/L 3.96 374.5186 348.824

0 

x 100912.401-2A 10/1/201 0 12:49:42 PM Zn 38.99 473.1439 ug/l 4.22 453.7322 472.039

" 1 00912.402-2A 10/1/2010 12:50:47 PM Zn 15.10 183.2318 ug/l 4.69 173.3014 188.318

,. Gl 

rn 100912.403-2A 10/1/2010 12:51:58PM Zn 48.34 586.7194 ug/L 2.24 573.8355 600.082

z 

? 

"' 

1 00912.511-2A 10/1/2010 12:53:37 PM Zn 23.59 286_3339 ug/L 2.40 278.3978 290.469

"' 1 00912.512-2A 10/1/2010 12:54:50 PM Zn 16.76 203.4215 ug/l 9.38 181.5919 211.702

Poga 86 of 1 03 
)> 

-< 

0 

-u 

"' 0 ~ m 

0 

-< 

z 

0 ~ 0 

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c 

Glm C-u 

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l>(j 

CJJ""' m<;;m 

-uz;:: -<.,- m())CJJ 

s::.t>.~ 

ffisto 0 "'"'z - -< 

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-u 

-u 

m 

z 

0 

x 

-u 

1) 

m 

z 

0 

"1 

... 

Sample ID 

CCV 

CCB 

1 00912.513-2A 

100912.501-2A 

100912.502-2A 

1 00912.503-2A 

CCV 

CCB 

Date Time Elem 

10/1/2010 12:56:26 PM Zn 

10/1/2010 12:57:48 PM Zn 

10/1/2010 12:58:49 PM Zn 

10/1/2010 1:00:41 PM Zn 

10/1/2010 1:01:47 PM Zn 

10/1/2010 1:03:20 PM Zn 

10/1/2010 1:05:04 PM Zn 

10/1/2010 1:06:52 PM Zn 

--

Cone (Calil int (Corr) Calib RSD (Cor lnt (Corr)1 lnt (Corr

1020.06 12379.71 ug/L 1.58 12153.23 12489.4

0.42 5.144108 ug/L 329.76 22.76797 -11.070

21.42 259.9716 ug/L 7.28 246.7618 251.502

34.99 424.61 8 ug/L 2.77 415.4229 437.876

42.18 511.9021 ug/L 1.4 7 504.8061 511.125

44.20 536.3717 ug/L 4.47 508.8126 552.432

I 038.23 12600.29 ug/L 0.87 12486.02 12705.5

-0.48 -5.857 49 ug/L 39.87 -6.72519 -3.2126

Page 87 of 1 03 
)> 

c 

)> ~ -u 

;u 

0 ~ m 

'.:l 

z 

0 ~ =: 

.. 

N 

Gl 

em rn" -;l> 

l>(i rn""' m<;;m 

-uz;:: -<-;- mrnUl 

~~~ 

m20~ 

:::0 ~01 -1 

"rnm S.J:>cn 

or-< 

u;-u 

"'"' co 

.,~ 

-<m 

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z 

-; 

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-u 

-u 

m 

z 

0 

x 

-u 

)> 

Gl 

m 

z 

0 ~ 0> 

Sample ID 

Calib Blank 1 

Standard 1 

Standard 2 

ICY 

iCB 

ICS 

100912.L8 

1 00912.LCS 

10912.8-1 

1 00912.SAI1-1 

l00912.SA12-1 

l00912.SA13-1 

100912.SA01-1 

l00912.SA02-1 

1 00912.SA03-1 

100912.411-1 

CCV 

CCB 

100912.411-1 s 

100912.412-1 

100912.412-1 D 

100912.413-1 

100912.401-1 

100912.402-1 

100912.403-1 

100912.511-1 

100912.512-1 

100912.513-1 

CCV 

CCB 

100912.501-1 

100912.502-1 

100912.503-1 

Date Time Elem Cone (Calillnt (Carr) Calib I RSD (Carr In! (Carr)11nt (Corr)21

10/6/2010 9:38:49 AM Mg 27.09564 ug/l 224.97 43.9424 -40.5131 

10/6/2010 9:39:44 AM Mg 155484.6 ug/l 1.92 152521.3 155446.9 

10/6/2010 9:40:33 AM Mg 314909.7 ug/L 0.15 315323.6 315025.5 

10/6/2010 9:41:57AM Mg 

10/6/2010 9:43:26 AM Mg 

10/6/2010 9:44:27 AM Mg 

10/6/2010 10:09:58 AM Mg 

10/6/2010 10:10:55 AM Mg 

10/6/2010 10:13:21 AM Mg 

10/6/2010 10:14:43 AM Mg 

10/6/2010 10:15:41 AM Mg 

10/6/2010 10:16:36AM Mg 

10/6/2010 10:18:08AM Mg 

10/6/2010 10:19:02 AM Mg 

10/6/2010 10:19:52 AM Mg 

10/6/2010 

10/6/2010 

10/6/2010 

10/6/2010 

10/6/2010 

10/6/2010 

10/6/2010 

10/6/201 0 

10/6/2010 

10:20:48 AM Mg 

10:22:21 AM Mg 

10:23:38AM Mg 

10:27:03AM Mg 

10:29:05 AM Mg 

10:29:57 AM Mg 

10:30:48 AM Mg 

1 0:32:11 AM Mg 

10:33:04 AM Mg 

10/6/2010 10:33:59 AM Mg 

10/6/2010 10:35:16AM Mg 

10/6/2010 10:36:05 AM Mg 

10/6/2010 10:36:54 AM Mg 

10/6/2010 10:38:21 AM Mg 

10/6/2010 10:39:43 AM Mg 

10/6/2010 10:40:31 AM Mg 

10/6/2010 10:41:21 AM Mg 

10/6/2010 10:42:11 AM Mg 

985.70 

-0.09 

-11.54 

-1.27 

870.20 

128.80 

367.50 

458.36 

507.68 

114.66 

115.71 

11,9.53 

1 S:p.03 

944.71 

-0.11 

1029.59 

157.22 

156.85 

141.49 

188.54 

185.54 

154814.8 ug/L 

-13.942 ug/L 

-1811.8 ug/L 

-1 98.88 ug/L 

136673.6 ug/L 

20229.56 ug/L 

57719.44 ug/L 

71990.69 ug/L 

79736.58 ug/L 

18008.03 ug/L 

18173.36 ug/L 

18773.97 ug/L 

2921 7.44 ug/L 

148376.1 ug/L 

-16.784 ug/L 

161708.4 ug/L 

24692.79 ug/L 

24634.96 ug/L 

22223.13 ug/L 

29613.03 ug/L 

29141.72 ug/l 

191.20 30030.49 ug/L 

305.19 47932.94 ug/L 

303.53 47 673.44 ug/L 

229.12 35985.78 ug/L 

965.16 151588 ug/L 

-0.27 -42.8323 ug/L 

216.24 33963.36 ug/L 

209.93 32972.22 ug/L 

243.62 38263.47 ug/L 

Poge 88 of 103 

2.21 152973.1 152707.9 

513.53 48.42554 -92.1227 

4.75 -1903.79 -1733.29 

12.79 -224.717 -198.047 

1.52 134689.3 136498.2 

0.90 20062.23 20203.96 2

0.46 57538.95 58021.88 5

0.67 72032.62 72451.18 7

2.06 77844.62 80828.53 

2.23 17810.74 17743.64 

0.85 18191.32 18010.46 

0.38 18706.35 18847.9 

1.67 29202.13 28738.6 2

2.62 145443.7 146893.7 1

386.10 -67.4253 -39.1717 5

1.86 158424.2 162395.3 

0.77 24756.12 24479.98 2

1.32 24378.02 24527.24 2

1.27 21998.58 22130.37 2

1.21 29401.9 29411.42 3

1.26 28732.42 29253.62 2

1.64 29750.38 297 41.85 3

1.08 47819.68 47480.77 4

0.82 47229.05 47831.08 4

1.77 35443.85 35828.35 3

2.19 147946.2 154443.9 

146.23 18.49887 -106.689 -

0.71 33704.73 34001.8 3

0.92 32757.57 33321.2 

2.55 37455.24 37990.39 3
,. Sample 10 Date Time Elem Cone (Calillnt (Corr) Calib I RSO (Corr lnt (Corr)l lnt (Corr)21

-; (") 

"1l 100912.B-2A 10/6/2010 10:44:35 AM Mg 16.60 2607.382 ug/L 0.42 2598.208 2604.276 

" 100912.SAI1-2A 10/6/2010 10:45:28AM Mg 915.14 143732.2 ug/L 1.13 142776.6 145613.5 

0 '- 1 00912.SAI2-2A 10/6/2010 10:46:22 AM Mg 286.52 45000.35 ug/L m 1.06 44551.54 4494 7.1 8 

(") -; 1 00912.SA13-2A 10/6/2010 10:47:14 AM Mg 896.73 140840.6 ug/L 2.08 137532.8 141897.8 

z 0 

:!: 1 00912.SA01-2A 10/6/2010 10:48:35 AM Mg 32.26 5066.006 ug/L 2.34 4997.54 4997.633 

':l 

... 

1 00912.SA02-2A 10/6/2010 1 0:49:27 AM Mg 47.26 7422.358 ug/L 1.87 7263.246 7518.764 

"' 1 00912.SA03-2A 10/6/2010 10:50:16 AM Mg 44.09 6925.299 ug/L 0.77 6964.999 6864.626 

CCV 10/6/2010 10:52:00 AM Mg 999.56 156991.6 ug/L 1.14 155070.4 157291.7 

CCB 10/6/2010 10:53:46 AM Mg 0.02 3.427273 ug/L 1812.00 -60.4336 7.108759 

,. 100912.411-2Ax2 10/6/2010 11 :06:02AM Mg 7 42.80 116665.3 ug/L 1.57 114697.6 11697 4.1 

G)m 

c 1 00912.411-2AS X 2 10/6/2010 11:07:20 AM Mg 1683.59 264426.3 ug/L 1.41 261064 263783.7 

c"ll 100912 .412-2A 10/6/2010 11 :09:42AM Mg 1714.1 7 269229.3 ug/L 1 .51 265695.9 268328.3 

~,. 

cn"ll" "'o 100912.412-2AD 10/6/2010 11:10:36 AM Mg 1744.63 274013.1 ug/L 1.53 269497.9 27 4791.2 

ms;m "llzS: 100912.413-2A 10/6/2010 11:11:27 AM Mg 882.83 138657.7 ug/L 0.68 138039.4 138196.1 

1.86 13358.54 13647.23 

-<-;- 100912.401-2A 10/6/2010 1l:l2:54AM Mg 86.74 13623.01 ug/L 

men"' 3:~~ 

1 00912.402-2A 10/6/2010 11:13:42 AM Mg 78.81 12377.54 ug/L 1.69 12203.63 12609.97 

~Qo~ 

::tl }'I -1 1 00912.403-2A 

10/6/2010 11:14:44 AM Mg 141.69 22254.22 ug/L 3.11 21548.66 22283.05 

"'cnm 

o,.cn CCV ]0/6/2010 11:16:17 AM Mg 1021.98 160513 ug/L 0.82 159170.4 160565.6 

;:;,-1 

(ii"ll 

"'" co CCB 10/6/2010 11:17:45AM Mg -0.23 -36.8015 ug/L 203.78 -74.2219 -85.7203 

"'" 100912.511-2A 10/6/2010 11 :18:37 AM Mg 2035.42 319684.3 ug/L 3.50 306818 325116.4 

-<m (1 100912.512-2A 10/6/2010 11:19:33AM Mg 789.63 124019.4 ug/L 0.43 123424.2 124442.5 

z 100912.513-2A 10/6/2010 11 :20:28 AM Mg 815.65 128107.3 ug/L 1.43 126190.1 128293.2 

-; a> 100912.501-2A 10/6/2010 11:21:48 AM Mg 71.83 11282.22 ug/L 3.51 10869.39 11317.59 

100912.502-2A 10/6/2010 11 :22:37 AM Mg 1100.37 172825.7 ug/L 1.48 170967.8 171769.4 

1 00912.503-2A 10/6/2010 11 :23:36 AM Mg 584.39 91785.13 ug/L 1.45 92473.85 90248.75 9

,. 

CCV 10/6/2010 11:24:59 AM Mg 1015.75 159535 ug/L 0.23 159167.7 159549.6 

CCB 10/6/2010 11:26:10AM Mg -0.11 -16.6533 ug/L 358.16 43.67224 -75.5934 

"1l "1l m 

z 

0 

x 

"1l 

,. G) 

m 

z 

? ~ <0 

Page 89 of T 03 
~ )> 

--< 

0 

" Sample_ID EL Sam_Date Sam_Time Mean_Sig Mean_ST RSD Cal_ Units Dilu Rec S

" Calib Blank Pb 9/28/2010 9:20:19 -0.004 62.6 J.lg/L 0 ~ 0 m 20 ppb Pb 9/2B/201 0 9:27:50 0.027 4.4 J.lg/L --< 

z 50 ppb Pb 9/28/2010 9:35:28 0.053 1 .1 /19/L ~ 100 ppb Pb 9/28/2010 9:43:08 0.100 3.7 /19/L 

0 ~ 200 ppb Pb 9/28/2010 9:50:48 0.1B5 1.5 J.lg/L ~ ICY Pb 9/28/2010 10:09:17 0.099 98.7 0.7 /19/L 

... N ICB Pb 9/28/2010 10:16:38 0.003 2.1 17.4 /19/L 

1 00912.LB Pb 9/2B/201 0 10:24:06 0.002 1.2 90.7 J.IQ/L 1 

1 00912.LCS Pb 9/28/2010 10:31:35 0.104 104.4 3.6 J,lg/L 1 

)> 100912.B-1 Pb 9/28/2010 10:39:02 0.004 2.2 14.0 J,lg/L 1 

c 

"'m 1 00912.SA11-1 Pb 9/28/2010 10:46:27 O.OB9 B6.6 3.7 J,lg/L 1 

C-u 

~)> 

100912.SAI1-1 Pb 9/2B/2010 10:54:07 0.166 177.5 1.1 J.lg/L 1 90.9 

"o 100912.SAI2-1 Pb 9/28/2010 11 :01:30 O.OB2 79.5 3.3 J.IQ/L 1 

mt;;m w"" 1 00912.SA13-1 Pb 9/28/2010 11 :08:50 0.075 71.1 4.9 J,lg/L 1 

"UzS: 100912.SA01-1 Pb 9/28/2010 11 :16:08 0.004 2.2 90.4 J.lg/L 1 

--<-;- mwW 100912.SA02-1 Pb 9/2B/201 0 11:23:24 0.003 1.7 13.1 J.IQ/L 1 

S,:A!:a 

~~g 1 00912.SA03-1 Pb 9/28/2010 11 :30:44 0.004 2.6 49.6 J.IQ/L 

;::o_r.n...., 1 

CCV Pb 9/2B/201 0 11 :3B:20 0.100 99.5 3.1 J.IQ/L 1 

Nwm 

0)>()) CCB Pb 9/28/2010 11 :45:43 0.001 0.9 45.4 J-19/L 1 

c_;,--1 (ii-u 

100912.411-1 Pb 9/2B/201 0 11 :53:04 0.003 l.B 104.8 1-19/L 

'"" co 1 

,~ 100912.412-1 Pb 9/2B/201 0 12:00:29 0.002 1.4 118.9 J-19/L 1 

-<m 

"0 t;;-< 100912.413-1 Pb 9/28/2010 12:07:56 0.003 2.1 4.9 /lQ/L 1 

100912.401-1 Pb 9/2B/201 0 12:15:25 0.006 4.0 58.9 J.IQ/L 1 

z --< 

"' 100912.402-1 Pb 9/2B/201 0 12:22:58 0.005 3.0 67.0 1-19/L 1 

100912.403-1 Pb 9/28/2010 12:30:32 0.005 3.0 1.0 J-19/L 1 

100912.512-1 Pb 9!2B/201 0 12:3B:11 0.010 6.3 18.4 J.IQ/L 1 

100912.513-1 Pb 9/2B/201 0 12:45:52 0.008 5.5 1B.B J.lg/L 1 

)> 

100912.501-1 Pb 9/28/2010 12:53:26 0.007 4.3 34.1 1-19/L 1 

" CCV Pb 9/28/2010 13:01 :05 0.102 102.2 0.4 /19/L 1 

" 

z 

m CCB Pb 9/2B/201 0 13:08:29 0.003 1.7 56.5 J-19/L 1 

0 

x 100912.502-1 Pb 9/2B/201 0 13:15:56 0.002 1.3 4B.7 J-19/L 1 

" 100912.503-1 Pb 9/28/2010 13:23:26 0.005 2.9 69.8 J-19/L 1 

)> 

G) 

m CCV Pb 9/28/2010 13:31 :04 0.102 101.5 0.4 1-19/L 1 

~ z CCB Pb 9!28/201 0 13:38:28 0.003 2.1 19.5 jlg/L 1 

"' N Calib Blank Pb 9/29/2010 8:11:07 -0.001 65.9 J.IQ/L 0 

Page 90 of 103 
)> 

_, 

0 

;o " Sample_ID EL Sam_Date Sam_ Time Mean_Sig Mean_ST RSD Cai_Unlts Dilu Rec S

20 ppb Pb 9/29/2010 8:18:39 0.020 2.1 !19/L 0 ~ m 

0 

_, 

50 ppb Pb 9/29/2010 8:26:18 0.051 3.2 !19/L 

z 100 ppb Pb 9/29/2010 8:33:59 0.098 1.3 !19/L 0 200 ppb Pb 9/29/2010 8:41:36 0.178 1.9 pg/L " ICY Pb 9/29/2010 8:51 :15 0.099 103.0 2.0 pg/L 

0 t ~ ICB Pb 9/29/2010 8:58:38 0.006 5.9 118.0 !19/L 

100912.B-2A Pb 9/29/2010 9:06:06 0.002 1.7 5.8 !19/L 1 

100912.SAI1-2A Pb 9/29/2010 9:13:36 0.018 17.3 9.1 !19/L 1 

100912.SAI1-2A Pb 9/29/2010 9:21:15 0.107 111.8 0.2 !19/L 1 94.5 

)> 100912.SA12-2A Pb 9/29/2010 9:28:45 0.005 5.3 19.2 !19/L 1 

c 

c., Glm 100912.SAO 1-2A Pb 9/29/2010 9:46:41 0.004 3.5 9.6 !19/L 1 

~)> 

100912.SA02-2A Pb 9/29/2010 9:54:01 0.001 0.7 407.4 !19/L 1 

l>(\ 1 00912.SA03-2A Pb 9/29/2010 10:01:19 0.002 2.3 22.3 !19/L 1 

m';m rn"'" 1 00912.411 -2A Pb 9/29/2010 10:08:38 0.003 3.2 24.6 !19/L 1 

-uz;;: 100912.412-2A Pb 9/29/2010 10:15:56 0.008 7.5 21.0 !19/L 1 

_,_,_ mrnrn CCV Pb 9/29/2010 10:23:32 0.092 95.4 4.0 !19/L 1 

S:.:..Q2 

~""~ Pb CC8 

9/29/2010 10:30:56 0.000 -0.3 25.8 !19/L 1 

::O!Jt_, 

~rnm 100912.413-2A Pb 

9/29/2010 10:38:17 0.003 2.7 73.1 !19/L 1 

o,.rn 

Oc.-1 100912.401-2A Pb 9/29/2010 10:45:42 

(f)"U 0.005 4.6 75.4 !19/L 1 

OJ;o 

co 100912.402-2A Pb 9/29/2010 10:53:09 0.002 1.9 1.3 !19/L 1 

;o~ 100912.403-2A Pb 9/29/2010 11 :00:38 0.006 5.9 23.1 !19/L 1 

-<m (1 1 00912.511 -2A Pb 9/29/2010 11:08:12 0.010 9.4 27.4 !19/L 1 

z 

_, 

1 00912.512-2A Pb 9/29/2010 11:15:46 0.005 4.7 5.8 !19/L 1 

"' 100912.513-2A Pb 9/29/2010 11:23:24 0.003 2.7 8.5 !19/L 1 

100912.501-2A Pb 9/29/2010 11 :31:05 0.006 6.3 38.0 !19/L 1 

100912.502-2A Pb 9/29/2010 11 :38:46 0.004 3.7 43.3 !19/L 1 

CCV Pb 9/29/2010 11:46:30 0.091 94.2 5.7 119/L 1 

)> 

CCB Pb 9/29/2010 11:53:53 0.002 2.2 2.7 !19/L 1 

" 1 00912.503-2A Pb 9/29/2010 12:01:22 0.005 5.3 26.5 !19/L 1 

m " CCV Pb 9/29/2010 12:09:01 0.101 104.8 2.2 !19/L 1 

z 0 

x CCB Pb 9/29/2010 12:16:26 0.001 0.9 278.0 !19/L 1 

" )> Calib Blank Pb 10/4/2010 8:59:08 0.003 185.5 !19/L Gl 

m 20 ppb Pb 10/4/2010 9:06:43 0.014 0.2 !19/L 

z 50 ppb Pb 10/4/2010 9:14:22 0.046 3.4 !19/L 0 

"' 100 ppb Pb 10/4/2010 ~ 9:22:01 0.076 1.2 !19/L 

f'Qge 91 of 103 
, 

-; 

0 

"0 

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0 ~ m 

0 

-; 

z 

p 

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0 

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-; 

"' 

, 

"0 

"0 

m 

z 

0 

x 

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, Gl 

m 

z 

0 

"' "' "' 

Sample_ID EL Sam_Date 

200 ppb Pb 10/4/2010 

ICY Pb 10/4/2010 

ICB Pb 10/4/2010 

100912.SA13-2A Pb 10/4/2010 

CCV Pb 10/4/2010 

CCB Pb 10/4/2010 

Calib Blank Pb 10/6/2010 

20 ppb Pb 1 0/6/2010 

50 ppb Pb 10/6/2010 

100 ppb Pb 10/6/2010 

200 ppb Pb 10/6/2010 

ICY Pb 10/6/2010 

ICB Pb 10/6/2010 

ICY Pb 10/6/2010 

ICB Pb 10/6/2010 

100912.511-1 Pb 10/6/2010 

CCV Pb 10/6/2010 

CCB Pb 1 0/6/201 0 

"-

Sam_ Time Mean_Sig Mean_ST RSD Cai_Units Dilu Rec S

9:29:39 0.152 4.5 J,Jg/L 

9:44:45 0.074 93.5 3.5 J,Jg/L 1 

9:52:06 -0.003 -4.3 13.6 /19/L 1 

10:14:36 -0.003 -3.8 60.3 J.ig/L 1 

11:14:00 0.088 112.1 4.1 J.ig/L 1 

11:21:23 -0.004 -4.6 59.2 Jlg/L 1 

8:13:33 0.000 534.1 Jlg/L 

8:21:03 0.015 15.4 J.ig/L 

8:28:42 0.041 2.7 Jlg/L 

8:36:21 0.076 7.8 J.ig/L 

8:43:58 0.156 6.4 J.ig/L 

8:55:54 0.087 111.7352 3.8 J,Jg/L 1 

8:59:37 -0.002 -1.90515 -1.9 J,Jg/L 1 

9:07:37 0.084 107.3257 3.9 /19/L 1 

9:14:59 -0.002 -2.32855 24.1 J.ig/L 1 

9:22:32 0.006 7.805673 0.9 J.ig/L 1 

9:30:12 0.089 

113.9833 0.4 J.ig/L 1 

9:37:36 -0.003 -3.37163 4.3 J,Jg/L 1 

Page 92 of 1 03 
, 

-l 

() Sample ID Elem Date Time Abs (Carr) Cane (Calil RSD (Cone) Special Sa Special Ca Cone (C

"1l :0 Calib Blank Sb 9/28/2010 8:41:11 AM -0.007 0 0 L 

20 ppb Sb Sb 9/28/2010 8:47:22 AM 0.017 0 m () 

-l 

z 

50 ppb Sb Sb 9/28/2010 8:53:33 AM 0.036 0 

? 100ppbSb Sb 9/28/2010 8:59:48 AM 0.060 0 :!: 200 ppb Sb Sb 9/28/2010 9:05:58AM 0.110 0 ~ ICV Sb 9/28/2010 9:34:58 AM 0.060 95.0 6.4 99.2

.. "' IC8 Sb 9/28/2010 9:41:11 AM 0.007 7.0 22.0 5.9

100912.L8 Sb 9/28/2010 9:47:21 AM 0.006 6.8 18.0 5.9

100912.LCS Sb 9/28/2010 9:53:33 AM 0.063 101.4 13.1 92.0

100912.8-1 Sb 9/28/2010 9:59:42 AM 0.002 1.6 91.7 0.5

, 

Sb "m c 100912.SA11-1 9!28/201 0 10:05:53 AM 0.008 9.1 42.4 11.8

100912.SAI1-1 Sb 9/28/2010 10:12:05 AM 0.061 97.2 4.2 1 97.2 94.2

c., ~, 1 00912.SA12-1 Sb 9/28/2010 10:18:17 AM 0.007 7.8 29.2 9.4

>fi (/).,, 

m<;m 100912.SA13-1 Sb 9/28!201 0 10:24:27 AM 0.009 9.5 12.0 10.3

"llzS: 1 00912.SA01-1 Sb 9/28!2010 10:30:35 AM 0.006 6.4 25.2 5.2

_,_,_ mrn<n 1 00912.SA02-1 Sb 9/28/2010 10:36:45 AM 0.009 9.3 38.1 11.8

s:"""~ 

~Qo~ 100912.SA03-1 Sb 9/28!2010 10:42:53 AM 0.007 7.8 7.9 

7.3

AJ.OI -i 

CCV Sb 9/28/2010 10:49:04 AM O.Q61 98.1 2.7 99.9

"'rnm 

o,.rn Or- -I CC8 Sb 9/28/2010 10:55:14AM 0.008 8.9 19.8 7.6

(i;"ll OJ:O 100912.411-1 

co Sb 9/28/2010 11:01:23 AM 0.009 9.2 20.5 7.9

100912.412-1 Sb 9/28/2010 11:07:31 AM 0.004 4.6 181.0 -1.2

:OL -<m (1 100912.413-1 Sb 9/28/201 0 11 :13:40 AM 0.008 8.6 53.2 5.3

z 100912.401-1 Sb 9/28/2010 11:19:51 AM 0.004 4.4 28.4 5.2

-l 

"' 100912.402-1 Sb 9/28/2010 11:26:01 AM 0.004 3.8 14.3 4.1

100912.403-1 Sb 9/28/2010 11:32:11 AM 0.007 7.9 13.2 8.6

100912.512-1 Sb 9/28/2010 11:38:23 AM 0.003 3.3 89.3 1.2

100912.513-1 Sb 9/28/2010 11:44:34 AM 0.004 4.7 110.7 8.3

, 

100912.501-1 Sb 9/28/2010 11:50:44 AM 0.006 6.4 15.6 5.6

CCV Sb 9/28/2010 11:56:55 AM 0.057 89.8 4.1 87.13

"1l "1l CC8 Sb 9/28/2010 12:03:07 PM 0.009 9.8 3.6 10.0

m z 

x 

0 100912.502-1 Sb 9/28/2010 12:09:18 PM 0.003 2.5 77.4 3.92

"1l 100912.503-1 Sb 9/28!2010 12:15:28 PM 0.006 5.9 3.9 5.75

, 

CCV Sb 9/28/2010 12:21:39 PM 0.061 97.6 3.6 95.1

Cl m 

z CCB Sb 9/28/2010 12:27:51 PM 0 0.006 6.2 13.5 6.78

"' 1 00912.8-2A Sb "' w 9/28/2010 1:20:39 PM 0.004 4.0 70.5 6.05

Page 93 of 103 
~· )> 

-< 

0 Sample ID Elem Date Time Abs (Corr) Cone (Cali! RSD (Cone} Special Sa Special Ca Cone (Ca

"1l " 100912.SAI1-2A Sb 9/28/2010 1:26:51 PM 0.008 8.8 19.8 9.99

0 L 

100912.SAI2-2A Sb 9/28/2010 0.007 7.0 m 0 1:40:31 PM 26.8 1 8.32

-< 

z 100912.SAI2-2A Sb 9/28/2010 1:46:42 PM 0.074 124.8 2.8 1 124.8 127.26

? 1 00912.SAI3-2A Sb 9/28/2010 1:52:53 PM 0.007 7.0 55.1 9.73

0 ~ 1 00912.SA01-2A Sb 9/28/2010 1:59:05 PM 0.008 8.7 14.1 7.83

.. 1 00912.SA02-2A Sb 9/28/2010 2:05:13 PM 0.008 8.3 34.9 6.27

"' 100912.SA03-2A Sb 9/28/2010 2:11:21 PM 0.005 4.7 1.1 4.78

100912.411-2A Sb 9/28/2010 2:17:30 PM 0.006 5.8 0.6 5.78

100912.412-2A Sb 9/28/2010 2:23:39 PM 0.007 7.4 32.1 9.1

)> 100912.413-2A Sb 9/28/2010 2:29:47 PM 0.005 5.0 38.2 6.34

c 

Glm 100912.401-2A Sb 9/28/2010 2:35:55 PM 0.007 7.3 30.5 5.73

~)> c" CCV Sb 9/28/2010 2:42:06 PM 0.069 113.6 2.4 115.50

>c; CCB Sb 9/28/2010 2:48:18 PM 0.005 5.3 63.5 7.60

en"" m);m 100912.402-2A Sb 9/28/2010 2:54:34 PM 0.009 9.7 9.3 9.10

"UzS: 1 00912.403-2A Sb 9/28/2010 3:00:48 PM 0.005 4.7 5.2 4.56

-<-;- men en 100912.511-2A Sb 9/28/2010 3:07:02 PM 0.008 8.5 45.0 5.82

s:~~ 

~s;>o~ .100912.512-2A Sb 9/28/2010 3:13:16 PM 0.007 7.7 1.7 7.80

:;:o .Ul -1 Sb 9/28/2010 0.009 9.7 9.87

"'enm 1 00912.513-2A 3:19:31 PM 3.3 

o,.en 100912.501-2A Sb 9/28/2010 3:25:47 PM 0.005 4.9 5.5 4.74

Or- -I 

'"" 6.83

co rn::O 1 00912.502-2A Sb 9/28/2010 3:32:01 PM 0.005 5.3 39.5 

Sb 9/28/2010 0.006 6.4 42.7 4.48

;oL 100912.503-2A 3:38:14 PM -<m (l CCV Sb 9/28/2010 3:44:25 PM 0.063 101.1 2.0 99.65

z CC8 Sb 9/28/2010 3:50:38 PM 0.006 6.1 37.6 7.71

-< Calib Blank Sb 10/8/2010 9:45:35 AM 0.000 0 "' 20 ppb Sb Sb 10/8/2010 9:51:44AM 0.014 0 

50 ppb Sb Sb 10/8/2010 9:57:56 AM 0.034 0 

100 ppb Sb Sb 10/8/2010 10:04:09 AM 0.069 0 

200 ppb Sb Sb 10/8/2010 10:10:18AM 0.133 0 )> ICY Sb 10/8/2010 10:17:15 AM 0.068 99.7 1.2 98.79

"1l "1l 

62.0 -0.35

m z ICB Sb 10/8/2010 10:23:26 AM 0.000 -0.6 

0 

x 100912.511-1 Sb 10/8/2010 10:29:39 AM 0.001 1.0 30.3 1.20

)> 

"1l CCV Sb 10/8/2010 10:35:52 AM 0.067 98.6 0.1 98.68

Gl 

m CCB Sb 10/8/2010 10:42:08 AM 0.000 -0.6 6.5 -0.66

z 

? 

"' .. "' 

Page 94 of 103 
, Sample ID Elem Date Time Abs (Corr) Cone (Cali! RSD (Cone) Special Sa Special Ca Cone (C

"" 0 

-u 

Calib Blank Se 9/29/2010 9:02:41 AM ..().001 0 

0 "' 20 ppb Se Se 9/29/2010 9:08:53 AM 0.018 0 ~ 50 ppb Se Se 9/29/2010 9:15:04 AM 0.045 m 0 0 

"" z 100 ppb Se Se 9/29/2010 9:21:16AM 0.090 0 

0 

200 ppb Se Se 9/29/2010 9:27:26 AM 0.176 :!: 0 

"' ICY Se 9/29/2010 9:54:29 AM 0.081 92.0 5.95 88.14

... IC8 Se 9/29/2010 10:00:41 AM 0.000 -0.2 359.77 -0.777

N 

1 00912.LB Se 9/29/2010 10:06:51 AM 0.001 0.8 73.74 0.3837

100912.LCS Se 9/29/2010 10:13:04 AM 0.090 101.3 0.62 100.81

, 

100912.8-1 Se 9/29/2010 10:19:13 AM -0.001 -0.8 96.21 -1.2696

c 

Glm 1 00912.SAil-1 Se 9/29/2010 10:25:24 AM 0.011 12.8 6.57 12.219

C-u ~, 1 00912.SA!2-1 Se 9/29/2010 10:31:36 AM 0.014 15.3 1.98 15.551

"'o 100912.SA13-1 Se 9/29/2010 10:38:55 AM 0.008 9.5 9.04 10.132

w""' Se 9/29/2010 0.000 0.5 71.81 0. 79433

m<;:m 100912.SAOl-1 10:45:03 AM -oz<: 

-<-<- mwW 

s::.j:>.~ 

100912.SA02-1 Se 9/29/2010 10:51:12 AM -0.001 -1.2 95.51 -0.3836

~!<'>~ 

1 00912.SA03-1 Se 9/29/2010 10:57:21 AM 0.000 0.5 46.78 0.31187

;u 51"' -1 CCV Se 9/29/2010 11:03:34 AM 0.089 100.8 0.77 100,263

"wm 

o,w CC8 Se 9/29/2010 11:09:47 AM 0.001 0.7 65.35 0.3642

c;r-1 

(ii"O 

co co"' 100912.411-1 Se 9/29/2010 11:18:12AM 0.012 13.1 2.43 13.3590

,~ 100912.411-1 Se 9/29/2010 11:24:26 AM 0.082 92.4 1.86 1 79.22839 93.576

..;m 0 

""" 0.005 5.63249

100912.412-1 Se 9/29/2010 11:30:35 AM 5.2 10.84 <;: 

z 100912.413-1 Se 9/29/2010 11:36:45 AM 0.003 3.2 42.91 2.23849

"" "' 100912.401-1 Se 9/29/2010 11:42:56 AM 0.000 -0.4 251.60 -1.2070

100912.402-1 Se 9/29/2010 11:49:07 AM 0.000 0.2 676.82 -0.5705

100912.403-1 Se 9/29/2010 11:55:18 AM 0.000 0.2 26.77 0.1386

, 

100912.512-1 Se 9/29/2010 12:01:32 PM 0.039 44.3 4.78 42.7682

100912.513-1 Se 9/29/2010 12:07:44 PM 0.066 74.9 2.40 76.18

"0 -u 

m 

z 100912.501-1 Se 9/29/2010 12:13:56 PM 0.002 2.0 1.48 2.01881

0 

x CCV Se 9/29/2010 12:20:09 PM 0.090 101.7 0.46 102.041

"0 CCB Se 9/29/2010 12:26:21 PM -0.001 -0.9 63.34 -0.5047

, Gl 

Se 9/29/2010 12:32:32 PM 0.002 2.7 16.63 3.04157

m 100912.502-1 z ~ 100912.503-1 Se 9/29!2010 

"' 

12:38:43 PM 0.005 5.1 6.68 4.88015

N 

"' CCV Se 9/29/2010 12:44:55 PM 0.089 100.3 0.68 100.803

Page 95 of 103 
~~ , Sample ID Elem Date Time Abs (Corr) Cone (Cali! RSD (Cone) Special Sa Special Ca Cone 

-; 

0 CCB "U Se 9/29/2010 12:51:07 PM -0.001 -0.7 105.03 -0.19

;o 

0 1 00912.B-2A Se 9/29/2010 1:00:12 PM 0.000 -0.2 345.63 -0.53

~ 1 00912.SAI3-2A Se 9/29/2010 1:24:59 PM 0.006 7.3 rn 0 22.81 8.499

-; 

z 1 00912.SAI2-2A Se 9/29/2010 1:50:06 PM 0.013 15.0 12.33 13.66

0 

1 00912.SA02-2A Se 9/29/2010 2:38:46 PM 0.006 6.9 :!: 17.19 6.07

:1 1 00912.SA03-2A Se 9/29/2010 3:12:39 PM 0.001 1.7 116.49 0.294

.... 100912.411-2A Se 9/29/2010 3:18:49 PM 0.009 9.8 3.83 9.555

"' 

1 00912.412-2A Se 9/29/2010 3:24:57 PM 0.015 17.2 23.82 14.30

100912.413-2A Se 9/29/2010 3:31 :05 PM 0.009 10.0 19.44 8.648

, 

1 00912.401-2A Se 9/29/2010 3:37:13 PM 0.002 2.7 26.90 3.164

c 1 00912.402-2A Se 9/29/2010 3:43:23 PM -0.001 -1.4 542.30 3.943

"'rn c., ~, 1 00912.403-2A Se 9/29/2010 3:49:38 PM -0.001 -1.1 58.12 -1.56

(/j"U;o >o 1 00912.511-2A Se 9/29/2010 3:55:52 PM 0.021 24.3 15.83 21.5

rn\:rn CCV Se 9/29/2010 4:02:03 PM 0.075 84.7 5.11 87.75

"UzS: 

-;-;- CCB Se 9/29/2010 4:08:14 PM -0.001 -1.0 120.01 -1.85

rn(f)(/j 

3:.::-.~ ~!«>~ Calib Blank Se 9/30/2010 8:42:30 AM -0.003 0.00 

;o _01 -I 20 ppb Se Se 9/30/2010 8:48:42 AM 0.014 0.00 

"-'(fjm 

0}>(/) 50 ppb Se Se 9/30/2010 8:54:55 AM 0.032 0.00 ~!:::--1 

(/j"U 

"'"' 100 ppb Se Se 9/30/2010 9:01:07 AM 0.070 0.00 co ,~ -<m 200 ppb Se Se 9/30/2010 9:07:18 AM 0.132 0.00 .,o ICY Se 9/30/2010 9:22:37 AM 0.067 100.3 2.41 98.58

);-; 

z ICB Se 9/30/2010 9:28:50AM -0.001 -1.5 36.90 -1.89

-; 

"' 100912.SAI1-2A Se 9/30/2010 9:35:01 AM 0.000 -0.2 536.08 -1.04

1 00912.SA11-2A Se 9/30/2010 9:41:11AM 0.062 93.2 5.26 1 93.23038 89.76

100912.SA01-2A Se 9/30/2010 9:47:20AM 0.009 13.2 2.09 13.38

1 00912.512-2A Se 9/30/2010 9:53:34AM 0.007 10.7 94.05 3.582

, 1 00912.513-2A Se 9/30/2010 9:59:49 AM 0.006 9.7 28.77 7.719

"U "U 

rn 

z 100912.501-2A Se 9/30/2010 10:06:06 AM 0.005 8.1 45.10 5.525

0 

x 1 00912.502-2A Se 9/30/2010 10:12:20AM 0.007 11 . 1 80.91 4.758

"U 1 00912.503-2A Se 9/30/2010 10:18:34 AM 0.006 8.7 13.22 9.547

, G) 

m CCV Se 9/30/2010 

z 

10:24:47 AM 0.066 99.5 6.61 94.82

~ CCB Se 9/30/2010 10:31:00 AM 

"' -0.004 -5.3 10.30 -5.71

"' Calib Blank Se 10/7/2010 2:56:46 PM 0.001 0.00 "' 

Page 96 of 103 
)> 

-< 0 

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0 ~ rn 

0 

-< 

z 

0 ~ '= 

... 

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c 

Gl 

ern 

(1)"1l _,, 

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rnS::rn 

.,_,_ -uz;;: rnC/lC/l 

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m 

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0 

'" "' .... 

Sample ID Elem Date 

20 ppb Se Se 10/7/2010 

50 ppb Se Se 10/7/2010 

100 ppb Se Se 10/7/2010 

200 ppb Se Se 10/7/2010 

ICV Se 10/7/2010 

ICB Se 10/7/2010 

100912.511-1 Se 10/7/2010 

CCV Se 10/7/2010 

CCB Se 10/7/2010 

Time 

3:02:59 PM 

3:09:13 PM 

3:15:28 PM 

3:21:40 PM 

3:30:08 PM 

3:36:21 PM 

3:42:37 PM 

3:48:51 PM 

3:55:04 PM 

-· 

Abs (Corr) Cone (Calil RSD (Cone) Special Sa Special Ca Cone 

0.018 0.00 

0.035 0.00 

0.075 0.00 

0.137 0.00 

0.071 93.6 4.42 90.66

0.002 2.0 230.13 -1.24

0.016 19.3 11.15 17.79

0.069 91.5 4.55 94.46

0.000 0.4 209.58 -0.21

Pcge 97 of 103 
--

,. Sample ID Elem Date Time Abs (Corr Cone (Cali! RSD (Cone) Special Sa Special Ca Cone (Ca

-; (l 

., Cal"tb Blank Tl 10/6/2010 11:02:28AM 0.000 0 

;o 10 ppb Tl Tl 10/6/2010 11:07:58 AM 0.008 0 0 ~ m 20 ppb Tl Tl 10/6/2010 11:13:23 AM 0.017 0 (l -; 50 ppb Tl Tl 10/6/2010 11:18:47 AM 0.042 0 z 0 

100 ppb Tl 10/6/2010 ~ Tl 11:24:11 AM 0.082 0 

'" ,. ICV Tl 10/6/2010 11:55:24 AM 0.047 56.11 1.34 55.5821

ICV Tl 10/6/2010 12:01:25 PM 0.042 50.31 1.70 49.7101

N ICB Tl 10/6/2010 12:06:52 PM 0.000 -0.34 53.66 -0.473

1 00912.LB Tl 10/6/2010 12:12:16 PM 0.000 -0.05 78.82 -0.084

,. 100912.LCS Tl 10/6/2010 12:17:41 PM 0.050 59.96 0.83 60.3176

c 

c., Glm 100912.8-1 Tl 10/6/2010 12:23:04 PM 0.000 -0.17 10.98 -0.1794

100912.SAI1-1 Tl 10/6/2010 12:28:29 PM 0.004 4.67 6.64 4.4512

~,. 

en"" 

>o 100912.SA12-1 Tl 10/6/2010 12:33:55 PM 0.004 4.88 4.86 5.04977

m>;;m 100912.SAI3-1 Tl 10/6/2010 12:39:18 PM 0.004 4.49 1.11 4.52450

"Uz;< 

-<-;- 100912.SA01-1 Tl 10/6/2010 12:44:41 PM 0.000 -0.06 396.69 0.10203

men"' 

~""""~ 

1 00912.SA02-1 Tl 10/6/2010 12:50:04 PM 0.000 -0.49 87.20 -0.187

~Qo~ 

:::0 571 __, 100912.SA03-1 Tl 10/6/2010 12:55:27 PM 0.000 -0.03 1864.91 0.33829

Ncnm 

o,.cn CCV Tl 10/6/2010 1:00:50 PM 0.044 52.70 2.25 51.86051 

~r-1 

c;;., 10/6/2010 1:06:16 PM -0.42 44.13 "'" 

CCB Tl 0.000 co ,~ -0.2894

100912.411-1 Tl 10/6/2010 1:11:38 PM 0.000 -0.03 27.11 -0.04089 

..;m 

(~ 100912.411-1 Tl 10/6/2010 1:17:18 PM 0.042 51.10 0.32 1 102.1935 50.980

z 100912.412-1 Tl 10/6/2010 1:22:40 PM 0.000 0.10 25.52 0.114479 

-; "' 100912.413-1 Tl 10/6/2010 1:28:03 PM 0.000 0.02 522.39 -0.06284 

100912.401-1 Tl 10/6/2010 1:33:28 PM 0.000 -0.45 26.79 -0.53987 

100912.402-1 Tl 10/6/2010 1:38:54 PM 0.000 -0.26 107.12 -0.46284 

,. 

100912.403-1 Tl 10/6/2010 1:44:20 PM 0.000 -0.06 278.32 0.062427 

100912.511-1 Tl 10/6/2010 1:49:45 PM 0.001 0.74 4.85 0.718394 

., " m 100912.512-1 Tl 1 0/6/2010 1:55:10 PM 0.000 0.42 37.94 0.308182 

z 0 100912.513-1 Tl 10/6/2010 2:00:35 PM 0.001 0.73 17.80 0.637492 

x ., CCV Tl 10/6/201 0 2:06:21 PM 0.043 51.72 1.24 51.26847 

,. G) 

m CCB Tl 10/6/2010 2:11:47 PM 0.000 -0.26 111.42 z -0.45947 

0 100912.501-1 Tl 10/6/2010 2:17:09 PM 0.000 -0.15 123.58 -0.27851 

"' N 100912.502-1 Tl 10/6/2010 2:22:34 PM 0.000 -0.29 77.70 -0.44423 

"" 

Page 98 of 1 03 
--

,. 

-1 Sample ID Elem Date Time Abs (Corr Cone (Cali! RSO (Cone) Special Sa Special Ca Cone (Ca

0 100912.503-1 Tl 10/6/2010 2:27:59 PM 0.000 -0.34 5.32 -0.3507

, :0 CCV Tl 10/6/2010 2:33:24 PM 0.044 52.54 0.05 52.5174

0 L CCB Tl 10/6/2010 2:38:49 PM 0.000 -0.41 39.04 m -0.5290

0 -1 1 00912.6-2A Tl 10/6/2010 2:45:08 PM -0.001 -0.70 26.84 -0.8312

z 0 100912.SAI1-2A Tl 10/6/2010 2:50:33 PM 0.000 -0.58 38.04 l -0.7412

:1 1 00912.SAI2-2A Tl 10/6/2010 2:55:58 PM 0.000 -0.59 25.16 

... 

-0.6949

1 00912.SAI3-2A Tl 10/6/2010 3:01:25 PM 0.000 -0.38 105.23 " -0.0972

100912.SA01-2A Tl 10/6/2010 3:06:50 PM 0.000 -0.29 17.42 -0.3248

100912.SA02-2A Tl 10/6/2010 3:12:13 PM 0.000 -0.07 639.80 -0.4126

,. 

1 00912.SA03-2A Tl 10/6/2010 3:17:34 PM 0.000 -0.05 232.96 -0.1280

c 

c, Glm 1 00912.4!1-2A Tl 10/6/2010 3:22:57 PM 0.000 0.09 73.40 0.0428

100912.411-2A Tl 10/6/2010 3:28:28 PM 0.041 49.69 0.02 1 99.37454 49.6787

'::1:» ""n 1 00912.412-2A Tl 10/6/2010 3:33:52 PM 0.000 -0.16 81.39 rn""' -0.0674

CCV Tl 10/6/2010 3:39:14 PM mS::m 0.041 49.98 1.62 50.547 6

-uz;s: 

-1-i- CCB Tl 10/6/2010 3:44:40 PM -0.001 -0.64 58.24 -0.9022

mrn<n 

s:~SQ 

1 00912.413-2A Tl 10/6/2010 3:50:03 PM 0.000 -0.20 19.40 ~Qo~ -0.168

::0,0'1 -1 100912.401-2A 

Tl 10/6/2010 3:55:26 PM 0.000 -0.03 244.23 0.0222

"rnm 

o,.rn 

1 00912.402-2A Tl 10/6/2010 4:00:51 PM 0.000 -0.46 3.91 -0.4456

c:::;,.--1 

(jj-u 100912.403-2A Tl 10/6/2010 4:06:19 PM 0.000 -0.17 30.93 -0.2070

OJ:O 

co :<JL 1 00912.511-2A Tl 10/6/2010 4:11.49 PM 0.000 -0.07 310.60 -0.2174

-<m (4 100912.512-2A Tl 10/6/2010 4:17:16PM 0.000 -0.29 79.96 -0.4474

z 1 00912.513-2A Tl 10/6/2010 4:22:44 PM 0.000 0.00 13092.10 0.108362 

-1 en 100912.501-2A Tl 10/6/2010 4:28:11 PM 0.000 -0.04 1385.23 -0.4269

1 00912.502-2A Tl 10/6/2010 4:33:38 PM 0.000 0.01 68.23 0.006852 

CCV Tl 10/6/2010 4:39:05 PM 0.043 51.47 0.16 51.52649 

CCB Tl 10/6/2010 4:44:30 PM 0.000 -0.57 23.61 ,. -0.47738 

1 00912.503-ZA Tl 10/6/2010 4:49:57 PM 0.000 -0.30 69.09 -0.15209 

, , m CCV Tl 10/6/2010 4:55:21 PM 0.042 50.95 0.22 50.87331 

z 0 CCB Tl 10/6/2010 5:00:48 PM 0.000 -0.44 14.68 -0.48772 

x , 

,. Gl 

m 

z 

p 

en 

" "' 

Page 99 of 1 03 
"--

, 

Method 29 Mercury 

"" Sample 10 Date Element Aliquot (mL) ConC.IJg {Reading 1) Cone. Jl9 (Reading 2) (") 

"lJ ICV 9/28/2010 Hg 4.99 ;o ICB 9/28/2010 Hg 0 -0.02 '-

m 100912.8-28 9!28/2010 Hg 5 0.01 -0.01 (") 100912.5Ail-2B 9!28!2010 Hg 5 0.15 0.17 "" 

0 

z 100912.SAI1-2BS 9!28/2010 Hg 5 5.09 5.03 100912.SAI2-2B 9/28!2010 Hg 5 0.75 0.80 :::: 100912.SAI3-2B 9/28!2010 Hg 5 0.54 0.52 :: 

,. 

100912.SA01-2B 9/28/2010 Hg 5 0.08 0.10 

"' 100912.SA0 1-28$ 9/28/2010 Hg 5 4.98 5.03 CCV 9/28/2010 Hg 5.13 

CCB 9!28/201 0 Hg 0.04 

100912.SA02-2B 9/28/2010 Hg 5 0.11 0.12 

, 

1 00912.5A03-28 9/28/2010 Hg 5 0.07 0.08 

c 100912.411-28 9/28/2010 Hg 5 0.30 0.26 

c., Glm 100912.411-285 9!28/2010 Hg 5 5.17 5.35 100912.412-28 9!28/201 0 Hg 5 0.22 0.25 

~~ 

100912.413-28 9/28!2010 Hg 5 0.17 0.19 w""' 100912.401-28 9!28!201 0 Hg 5 0.37 0.34 rn<;;m "llZS: CCV 9/28/2010 Hg 4.87 --<--<- CC8 9/28/2010 Hg -0.03 

mww s:~~ 1 00912.401-285 9!28/2010 Hg 5 

5.25 5.29 

~Ro~ 

1 00912.402·28 9/28/2010 Hg 5 0.45 0.50 

:;:o_r.n-; 100912.403-28 9/28/2010 Hg 5 0.41 0.38 

"'wrn o,w 100912.511-28 

9/28/2010 Hg 5 0.44 0.40 

;:;!::-; 100912.511-285 9/28!2010 Hg 5 5.57 5.60 

(f)"ll 

"'"' co 100912.512-28 9/28/2010 Hg 5 0.34 0.30 ;o<- 100912.513-28 9/28/2010 Hg 5 0.13 0.19 -<rn "" ,..--< CCV 9/28/2010 Hg 5.03 CC8 9/28/2010 Hg o.oo , z 100912.8-3A 9/28/2010 Hg 10 0.01 -0.03 "" "' 100912.5AI1-3A 9/28/2010 Hg 10 0.06 0.04 100912.5AI2-3A 9/28/2010 Hg 10 0.04 0.03 100912.5AI3-3A 9/28/2010 Hg 10 0.01 0.03 100912.5A01-3A 9/28!2010 Hg 10 0.01 0.03 100912.SA02-3A 9/28/2010 Hg 10 -0.03 0.00 

, 100912.SA03-3A 9/28!2010 Hg 10 -0.04 -0.01 

"lJ 

"lJ CCV 9!28/2010 Hg 4.93 

m 

z 

CC8 9/28/2010 Hg 0.04 

100912.411-3A 9!28/201 0 Hg 10 0.10 0.06 0 x 100912.412-3A 9!28/2010 Hg 10 0.08 0.08 "lJ 100912.413-3A 9/28/2010 Hg 10 0.09 0.06 , Gl 100912.401-3A 9!28/2010 Hg 10 0.03 -0.01 rn 

z 100912.402-3A 9/28/2010 Hg 10 -0.01 -0.01 ? 1 00912.403-3A 9/28/2010 Hg 10 0.00 0.03 "' "' 0 

Page 100 of 103 
~- )> Method 29 Mercury 

-< Sample JD Dote .Element Aliquot {mL} Conc.IJg (Reading l) Cone. pg (Reading 2} () 

;o 

""0 100912.511·3A 9/28/2010 Hg 10 0.04 0.03 

0 CCV 9/2812010 Hg 5.00 ~ m CCB 9/28/2010 Hg 0.07 0 1 00912.512·3A 9/28/2010 Hg 10 0.06 0.08 -< 

0 

z 100912.513·3A 9/28/2010 Hg 10 0.08 0.10 100912.501 -3A 9/28/2010 Hg 10 0.01 0.01 ~ 1 00912.502-3A 9/28/2010 Hg 10 -0.03 0.03 

.. ~ 100912.503-3A 9/28/2010 Hg 10 -O.Dl -0.01 CCV 9/28/2010 Hg 5.19 N 

CC8 9/28/2010 Hg 0.06 

100912.501-28 9/28/2010 Hg 5 0.83 0.80 100912.502-28 9/28/2010 Hg 5 0.79 0.74 

)> 

100912.503-28 9/28/2010 Hg 5 0.76 0.82 

c CCV 9/28/2010 Hg 5.05 

C-a Glm CC8 9/28/2010 Hg 0.03 

~)> 

100912.8-38 9/28/2010 Hg 20 0.01 0.00 "o 100912 .SAil-38 9/28/2010 Hg 20 0.04 0.04 

m't:m 

[/>""O;o 100912.SAI2-38 9/28/2010 Hg 20 0.06 0.03 1 00912.SAI3-38 9/28/2010 Hg 20 0.04 0.01 -azs: -<-<- l00912.SA01-3B 9/28/2010 Hg 20 0.03 0.04 

mV>V> 

S:,:..<E. 1 00912 .SA02 -3 8 9/28/2010 Hg 20 0.04 0.01 

mS(og ::0 ,?1 -1 1 00912.SA03-38 9/28/2010 Hg 20 -0.01 0.06 

CCV 9/28/2010 Hg 4.88 

'-'V>m ~}>(/) CCB 

9/28/2010 Hg -0.01 

or--< 100912.411·38 9/28/2010 Hg 20 0.01 0.00 

r/>""0 

"'"' 100912.412-38 9/28/2010 Hg 20 0.03 -0.01 co 

:o~ 100912.413-38 9/28/2010 Hg 20 0.04 0.06 -<m ""00 100912.401-38 9/28/2010 Hg 20 0.40 0.32 ,.;"" 

z 

100912.402-38 9/28/2010 Hg 20 0.35 0.38 1 00912.403-38 9/28/2010 Hg 20 0.29 0.27 -< '" 100912.511-38 9/28/2010 Hg 20 0.38 0.44 CCV 9/28/2010 Hg 5.17 CCB 9/28/2010 Hg " -0.03 

100912.512-38 9/28/2010 Hg 20 0.50 0.50 100912.513-38 9/28/2010 Hg 20 0.47 0.49 

)> 100912.501-38 9/28/2010 Hg 20 0.04 0.01 ""0 100912.502-38 9/28/2010 Hg 20 ·O.Dl -0.03 ""0 

z 

m 100912.503-38 9/28/2010 Hg 20 -0.03 0.00 0 CCV 9/28/2010 Hg 5.06 x CC8 9/28/2010 Hg 0.03 ""0 100912.501-285 9128/2010 Hg 5 6.00 5.91 )> Gl 

m CCV 9!28/201 0 Hg 5.19 

0 

z CC8 9/28/2010 Hg 0.04 

ICY 10/1/2010 Hg 5.26 '" '0 

Page 101 of 103 
}> 

Method 29 Mercury 

--< Sample 10 Date Element Aliquot (mL) Conc.~Jg (Reading 1) Conc.pg (Reading 2) 0 , ICB 10/1/2010 Hg ;u 0.04 CCV 10/1/2010 Hg 0 4.98 L cca 10/1/2010 Hg m -0.01 0 100912.8-1 10/1/2010 Hg 5 0.00 0.01 --< z 10091 2.SA11-1 10/1/2010 Hg 5 0.05 0.03 0 100912.SAI2·1 10/1/2010 Hg 5 0.04 0.03 :;: 100912.SAI3-1 10/1/2010 Hg 5 0.06 0.02 '" 100912.SA01-1 10/1/2010 Hg 5 0.03 0.00 .. "' 100912.SA02-1 10/1/2010 Hg 5 0.01 0.02 100912.SA03-1 1011/2010 Hg 5 0.00 0.04 CCV 10/1/2010 Hg 4.97 CCB 10/1/2010 Hg 0.04 100912.411-1 10/1/2010 Hg 5 0.03 0.03 }> 100912.412-1 10/1/2010 Hg 5 -0.01 -0.01 c 

c, "'m 1 00912.413-1 10/1/2010 Hg 5 0.00 0.03 100912.401-1 10/1/2010 Hg 5 0.01 -0.03 ~}> 

(1),, »o 100912.402-1 10/1/2010 Hg 5 0.02 0.04 m);m 100912.403-1 10/1/2010 Hg 5 o.oo 0.04 CCV 10/1/2010 Hg . 5.05 -uzs: --<-;- CCB 10/1/2010 Hg -0.01 

m(J)(J) 

S:.;:..~ 100912.512-1 10/1/2010 Hg 5 O.OB 0.06 

fgS?o~ 100912.513-1 

10/1/2010 Hg 5 0.01 O.D2 

:::o_c.n -I 100912.501-1 10/1/2010 Hg 5 0.03 0.01 

"-'(l)m 

~);>(/) 100912.502-1 10/1/2010 Hg 5 o.oo -0.01 

or-< 100912.503-1 10/1/2010 Hg 5 -0.03 0.03 

(jj-u 

CD>l 100912.B-3C 10/1/2010 Hg 5 0.01 0.00 co >JL 100912.SAI1-3C 10/1/2010 Hg 5 0.85 0.80 -<m ,o CCV 10/1/2010 Hg );--< 5.34 CCB 10/1/2010 Hg z -0.03 1 00912.SAI2-3C 10/1/2010 Hg 5 1.37 1.52 --< "' 1 00912.SA13-3C 10/1/2010 Hg 5 1.04 1.00 100912.SA01-3C 10/1/2010 Hg 5 0.00 0.04 100912.SA02-3C 10/1/2010 Hg 5 -0.02 0.00 1 00912.SA03-3C 10/1/2010 Hg 5 0.01 -0.03 100912 .41l-3C 10/1/2010 Hg 5 0.37 0.32 

, 

}> 1 00912.412-3C 10/1/2010 Hg 5 0.16 0.13 CCV 10/1/2010 Hg 5.19 , m CCB 10/1/2010 Hg z 0.02 10091 2.413-3C 10/1/2010 Hg 5 0.02 0.05 0 x 100912.401-JC 10/l/2010 Hg 5 0.27 0.21 , 100912.402-3C 10/1/2010 Hg 5 0.02 0.04 }> Gl 10091 2.403-3C 10/1/2010 Hg 5 0.08 0.10 m z 100912.511 -3C 10/1/2010 Hg 5 0.14 0.16 0 

"' w 1 00912.512-3C 10/1/2010 Hg 5 0.18 0.20 "' 

Poge 102 of 103 
, 

--; 

0 

"U 

0 "' L 

m 

0 

--; 

z 

? ~ s: 

.... 

"' 

, 

c 

Glm c., en,. 

~0 

en"" m';:m -uz;:: --<--;- men'" 

!§:"""~ 

~~~ 

::u 91 -1 

"'cnm 

~>(/) 

or-< 

i'ii"U 

OJ:O 

co 

:OL 

-<m 

.,o 

';:--; 

z 

--; 

"' 

, 

"U 

"U 

m 

z 

0 

x ~ m 

z 

0 

w "' w 

Method 29 Mercury 

Sample 10 Date 

100912.513-JC 10/1/2010 

CCV 10/1/2010 

CCB 10/1/2010 

100912.501-JC 10/112010 

100912.502-JC 10/1/2010 

100912.503-3C 10/112010 

CCV 10/1/2010 

CCB 10/1/2010 

ICY 10/512010 

ICB 10/5/2010 

100912.511-1 10/5/2010 

CCV 10/5/2010 

CCB 10/5/2010 

Method 29 Mercury 

Calibration Data 

True cone., 

pg/L 

BJ.ank 0.00 

Standard 1 0.50 

Standard 2 1.00 

Standard 3 2.00 

Standard 4 5.00 

Standard 5 10.00 

Element Aliquot (mL) Conc.J.Jg (Reading 1) Conc.IJg (Reading 2) Hg 5 0.11 0.09 Hg 4.88 

Hg o.oo 

Hg 5 0.22 0.20 Hg 5 0.21 0.21 Hg 5 0.26 0.22 Hg 5.13 

Hg 0.04 

Hg 5.03 

Hg 0.01 

Hg 5.00 0.04 0.04 Hg 5.20 

Hg 0.03 

Run 1 Run 2 Rvn 3 

Abs. Abs. Abs. 

0.000 0.000 0.000 

0.016 0.013 0.014 

0.034 0.026 

0.027 

0.060 0.052 

0.054 

0.151 0.125 0.135 

0.300 0.248 0.265 

Page 103 of 103 
ATC PROJECT No. P-10142 

BORAL BRICKS 

ANALYTICAL 

ANALYSIS REPORT 

NELAP Cert. No. 04053 

Method 29: Multi-metals 

Project ID: P-10124 

Prepared for: 

Analytical Testing Consultants, Inc. 

1630 Dale Earnhardt Blvd. 

Kannapolis, NC 28083 

Page 1 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 531 
( 

BORAL BRICKS 

FIRST 

AN.A.LYTICAL 

Reviewed by: 

Tara Sheehan 

Laboratory Manager 

October 11, 2010 

Reviewed and Approved by: 

Jennifer B. Feller 

Quality Assurance Manager 

October 11,2010 

Do not reproduce this report except in whole without permission oft he laboratory. 

ATC PROJECT No. P-10142 

This report meets the requirements of LAC33/NELAP. 

Page 2 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 532 
BORAL BRICKS 

CASE NARRATIVE 

Project#: 100912 

Client: Analytical Testing Consultants, Inc. 

Client Project ID: P-1 0124 

Samples: 

Report Date: 11-0ct-10 

Nineteen sets of Method 29 samples were submitted, one of which was the 

blank set. The target elements were antimony, arsenic, barium, beryllium, 

cadmium, chromium, cobalt, copper, lead, magnesium, manganese, nickel, 

phosphorus, selenium, silver, thallium, zinc, and mercury. The filter san1ple for 

Plant 5 Inlet Run I was received separately at a later date. The samples were 

received in good condition with no apparent leakage or damage, and custody seals 

intact. All of the remaining amounts of the samples and digestates will be retained 

by the laboratory for six months and then discarded. 

Preparation: 

The samples were prepared and analyzed according to EPA Method 29, 

Determination of Metals Emissions from Stationary Sources. The front and back 

halves were analyzed separately. 

Analysis: 

Antimony, arsenic, cobalt, lead, selenium, and thallium were determined by 

Graphite Furnace Atomic Absorption Spectrophotometry (GFAA). Barium, 

beryllium, cadmium, chromium, copper, magnesium, manganese, nickel, 

phosphorus, silver, and zinc were determined by Inductively Coupled PlasmaOptical Emission Spectrometry (ICP-OES). Mercury was detennined by Cold 

Vapor Atomic Absorption Spectrophotometry (CV AA). 

ATC PROJECT No. P-10142 

Page 3 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 533 
BORAL BRICKS 

FIRST 

ANALYTICAL 

Results: 

The Method 29 metals results are presented as total micrograms of each 

element present in the whole analytical fraction indicated. Antimony, beryllium, 

cadmium, and thallium were not detected in any of the samples. All other 

elements of interest were detected in most of the runs. 

Quality Control: 

Chromium, magnesium, manganese, nickel, phosphorus, and zinc were all 

detected in the blank and may be blank corrected at the user's discretion, since 

some sample levels are comparable to the blank levels. Cobalt, selenium, and 

silver all showed interferences requiring dilutions for the spikes to pass, thus, 

causing the detection limits to increase. All of the spike recoveries were within the 

normal range of75% to 125%. 

All of the samples were analyzed at least in duplicate. 

ATC PROJECT No. P-10142 

Page 4 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 534 
I 

BORAL BRICKS 

ANALYTICALLABORATORlliS 

billing POBox i 10372- ResMrch Triangle Park.. NC 27709 ,....,...,,,ipp"'g 7517 Precision Drive, Suit¢ 101 - Rnleigh, NC :r:'617 

ANALYSIS REPORT 

TEL. 919 9~2 8607 

F.<\..X: 919 882 1.60:'> 

www.tl:r!>tnnalylicollabs. CI..'>Ol 

Project#; 1 00912 Report Dale: 08-0cl-1 0 

Client: Analytical Testing Consultants, Inc. Dale Received: 24-Sep-1 0 

Client Project ID: P-10124 

Sample 

Blank Front 

Blank Back 

S. Inlet Run 1 Front 

S. Inlet Run 1 Back 

S. Inlet Run 2 Front 

S. Inlet Run 2 Back 

S. Inlet Run 3 Front 

S. Inlet Run 3 Back 

S. Outlet Run 1 Front 

S. Outlet Run 1 Back 

S. Outlet Run 2 Front 

S. Outlet Run 2 Back 

S. Outlet Run 3 Fran! 

S. Outlet Run 3 Back 

4 Inlet Run 1 Front 

4 Inlet Run 1 Back 

4 Inlet Run 2 Fran! 

4 Inlet Run 2 Back 

4 Inlet Run 3 Front 

4 Inlet Run 3 Back 

4 Outlet Run 1 Front 

4 Outlet Run 1 Back 

4 Outlet Run 2 Front 

4 Outlet Run 2 Back 

4 Outlet Run 3 Front 

4 Outlet Run 3 Back 

ATC PROJECT No. P-1 0142 

Total Micrograms in Sample 

Sb As Ba Be 

pg Jig pg Jig 

< 1.0 < 0.5 < 2.5 < 0.05 

< 1.8 < 0.9 < 4.4 < 0.09 

< 1.0 2.3 21.3 < 0.05 

< 1.4 3.9 < 3.6 < 0.07 

< 1.0 3.0 34.0 < 0.05 

< 1.4 5.0 8.2 < 0.07 

< 1.0 2.8 28.8 < 0.05 

< 1.4 3.7 4.1 < 0.07 

< 1.0 < 0.5 2.7 < 0.05 

< 1.4 < 0.7 13.2 < 0.07 

< 1.0 < 0.5 2.6 < 0.05 

< 1.5 < 0.8 < 3.8 < 0.08 

< 1.0 < 0.5 5.0 < 0.05 

< 1.4 < 0.7 3.9 < 0.07 

< 1.0 < 0.5 3.6 < 0.05 

< 1.4 < 0.7 < 3.6 < 0.07 

< 1.0 < 0.5 5.2 < 0.05 

< 1.4 < 0.7 14.8 < 0.07 

< 1.0 < 0.5 5.0 < 0.05 

< 1.4 < 0.7 16.3 < 0.07 

< 1.0 < 0.5 5.7 < 0.05 

< 1.4 < 0.7 < 3.6 < 0.07 

< 1.0 < 0.5 5.1 < 0.05 

< 1.4 < 0.7 < 3.5 < 0.07 

< 1.0 < 0.5 4.3 < 0.05 

< 1.4 < 0.7 18.4 < 0.07 

Page 5 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Cd Cr 

pg 119 

< 0.30 2.1 

< 0.53 < 0.9 

< 0.30 1. 7 

< 0.43 3.2 

< 0.30 2.4 

< 0.43 1 .8 

< 0.30 2.4 

< 0.42 0.8 

< 0.30 1 .6 

< 0.43 3.1 

< 0.30 1.3 

< 0.46 < 0.8 

< 0.30 1.4 

< 0.41 < 0.7 

< 0.30 2.4 

< 0.43 2.1 

< 0.30 2.2 

< 0.43 2.7 

< 0.30 2.3 

< 0.43 1.4 

< 0.30 2.2 

< 0.43 < 0.7 

< 0.30 2.2 

< 0.42 < 0.7 

< 0.30 2.7 

< 0.43 < 0.7 

APPENDIX PAGE No. 535 
( 

BORAL BRICKS 

FIR.':;T ANALYTICAL LABORATORIES 

~~~ 

- btiliog. PO Box 110372- Rese.."\rcb Trianll.iePark., NC 27709 

:llippiltg: 751 "!Precision Dri\·e .. Smte 101 - Rnleigh, N<.~ .}161: 

ANAlYSIS REPORT 

TEL. 919 9-12 8607 

FA.X: 919 8821603 

ww:w.ilrstattalyi~JlJbs.com. 

Project#: 1 00912 Report Date: 08-0ct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep- 10 

Client Project ID: P-10124 

Sample 

5 Inlet Run 1 Front 

5 Inlet Run 1 Back 

5 Inlet Run 2 Front 

5 Inlet Run 2 Back 

5 Inlet Run 3 Front 

5 Inlet Run 3 Back 

5 Outlet Run 1 Front 

5 Outlet Run 1 Back 

5 Outlet Run 2 Front 

5 Outlet Run 2 Back 

5 Outlet Run 3 Front 

5 Outlet Run 3 Back 

Spike, %Rec. Front 

Spike, %Rec. Back 

Duplicate, %RPD Front 

Duplicate, %RPD Back 

ATC PROJECT No. P-10142 

Total Micrograms in Sample 

Sb As Ba Be 

f.l9 f.l9 f.l9 f.l9 

< 1.0 1.9 5.5 < 0.05 

< 1.4 2.3 9.5 < 0.07 

< 1.0 0.7 6.2 < 0.05 

< 1.4 < 0.7 < 3.5 < 0.07 

< 1.0 < 0.5 6.1 < 0.05 

< 1.4 < 0.7 12.3 < 0.07 

< 1.0 < 0.5 < 2.5 < 0.05 

< 1.4 < 0.7 < 3.5 < 0.07 

< 1.0 < 0.5 < 2.5 < 0.05 

< 1.4 < 0.7 8.4 < 0.07 

< 1.0 < 0.5 < 2.5 < 0.05 

< 1.4 < 0.7 7.0 < 0.07 

QC SUMMARY 

97% 76% 85% 84% 

125% 105% 97% 88% 

N/A N/A 4% N/A 

N/A N/A N/A N/A 

Page 6 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Cd Cr 

f.l9 f.l9 

< 0.30 1.6 

< 0.43 3.0 

< 0.30 1.9 

< 0.42 1.2 

< 0.30 2.0 

< 0.43 < 0.7 

< 0.30 2.0 

< 0.42 < 0.7 

< 0.30 1 .6 

< 0.43 < 0.7 

< 0.30 1 .6 

< 0.43 < 0.7 

78% 94% 

89% 77% 

N/A 5% 

N/A N/A 

APPENDIX PAGE No. 536 
BORAL BRICKS 

FIRST ANALYTICAL LABORATORIES 

billin.r;: PO Box 110372 -Rese11rcb. Tnangle Park. NC 27709 

""'''''~'I"·""' !51' Premsj;:m Driv6. Smte J 01 - fullei._cll. NC :-:611 

ANAlYSIS REPORT 

TEL: 919 942 8607 

FA .. 'X_: 919 882 1603 

WW'i\'.tit-stanalyticalhh~.cbm 

Project#: 100912 Report Date: 08-0ct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep-1 0 

Client Project ID: P-10124 

Sample 

Blank Front 

Blank Back 

S. Inlet Run 1 Front 

S. Inlet Run 1 Back 

S. Inlet Run 2 Front 

S. Inlet Run 2 Back 

S. Inlet Run 3 Front 

S. Inlet Run 3 Back 

S. Outlet Run 1 Front 

S. Outlet Run I Back 

S. Outlet Run 2 Front 

S. Outlet Run 2 Back 

S. Outlet Run 3 Front 

S. Outlet Run 3 Back 

4 Inlet Run 1 Front 

4 Inlet Run 1 Back 

4 Inlet Run 2 Front 

4 Inlet Run 2 Back 

4 Inlet Run 3 Front 

4 Inlet Run 3 Back 

4 Outlet Run 1 Front 

4 Outlet Run 1 Back 

4 Outlet Run 2 Front 

4 Outlet Run 2 Back 

4 Outlet Run 3 Front 

4 Outlet Run 3 Back 

ATC PROJECT No. P-1 0142 

Total Micrograms in Sample 

Co Cu Pb Mg 

J-ig J-ig J-ig JJg 

< 0.3 < 0.5 < 0.5 12.9 

< 0.5 < 0.9 < 0.9 2.9 

< 0.3 5.3 8.7 36.7 

< 13.0 3.8 2.5 132 

< 0.3 5.3 7.9 45.8 

< 0.4 2.1 0.8 40.8 

< 0.3 4.8 7.1 50.8 

< 0.4 2.3 < 0.7 125 

< 0.3 < 0.5 < 0.5 11.5 

< 0.4 0.9 < 0.7 4.6 

< 0.3 < 0.5 < 0.5 11.6 

< 0.5 1.3 < 0.8 7.2 

< 0.3 < 0.5 < 0.5 12.0 

< 0.4 1.5 < 0.7 6.1 

< 0.3 < 0.5 < 0.5 18.6 

< 0.4 1.0 < 0.7 212 

< 0.3 < 0.5 < 0.5 15.7 

< 0.4 1.1 1 . 1 243 

< 0.3 < 0.5 < 0.5 14.1 

< 0.4 0.8 < 0.7 126 

< 0.3 < 0.5 < 0.5 18.9 

2.3 1.5 < 0.7 12.5 

< 0.3 < 0.5 < 0.5 18.6 

1.1 < 0.7 < 0.7 1 1.1 

< 0.3 < 0.5 < 0.5 19. I 

0.8 2.1 0.8 20.5 

Page 7 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Mn Ni 

J-ig J-ig 

1.1 0.6 

< 0.4 < 0.5 

11.B 0.6 

21.8 18.0 

12.1 0.9 

6.4 3.5 

12.3 1.0 

6.2 4.5 

1.6 0.7 

1.4 16.3 

1.3 0.7 

2.2 2.0 

1 .9 O.B 

11.0 1 .4 

1.3 1.7 

4.6 1.3 

1 .2 1.0 

4.7 2.2 

1.5 1.4 

2.3 1.8 

1.3 1.1 

2.6 1.7 

1.2 1.3 

1.2 0.5 

1.3 1.6 

2.6 1.2 

APPENOIX PAGE No. 537 
( 

BORAL BRICKS 

FIRST ANALYTICAL LABORATORIES 

biJ/tng: PO Box 1 i0372. Research Triangle Park. NC 27"70'-J 

. . .. tltippillg: 1517 Proc~i0n Dtive, Sl1ite I Ol -Raleigh. NC 27617 -~f,Z~~~f.'t 

ANALYSIS REPORT 

TEL: 919 942 8607 

FA.X: ~19 S82 1603 

\\'"\\'\Y,i\tstanalyti..:n.)l.alll> .com 

Project#: 100912 Report Date: 08-0ct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep-1 0 

Client Project ID: P-1 0124 

Sample 

5 Inlet Run 1 Front 

5 Inlet Run 1 Back 

5 Inlet Run 2 Front 

5 Inlet Run 2 Back 

5 Inlet Run 3 Front 

5 Inlet Run 3 Back 

5 Outlet Run 1 Front 

5 Outlet Run 1 Back 

5 Outlet Run 2 Front 

5 Outlet Run 2 Back 

5 Outlet Run 3 Front 

5 Outlet Run 3 Back 

Spike, %Rec. Front 

Spike, % Rec. Back 

Duplicate, %RPD Front 

Duplicate, %RPD Back 

ATC PROJECT No. P-10142 

Total Micrograms in Sample 

Co Cu Pb Mg 

Jig Jig Jig Jig 

< 0.3 0.8 0.8 30.5 

< 0.4 1.l 1.3 289 

< 0.3 0.8 0.6 30.4 

< 0.4 0.9 < 0.7 11 0 

< 0.3 0.8 0.6 22.9 

< 0.4 1.3 < 0.7 117 

< 0.3 < 0.5 < 0.5 21.6 

< 0.4 1.7 0.9 10.1 

< 0.3 < 0.5 < 0.5 21.0 

< 0.4 1.5 < 0.7 157 

< 0.3 < 0.5 < 0.5 24.4 

< 0.4 1.5 0.8 84.0 

QC SUMMARY 

82% 99% 91% 84% 

78% 82% 95% 94% 

N/A 2% N/A 0.2% 

N/A N/A N/A 2% 

Page 8 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Mn Ni 

Jig Jig 

5.4 1.1 

25.4 2.5 

6.2 1.4 

2.9 1.0 

3.6 1.0 

3.6 0.9 

1.9 0.8 

1.7 0.8 

2.0 0.9 

15.5 0.7 

2.3 1.l 

1.7 1 . 1 

92% 105% 

76% 85% 

2% N/A 

6% 13% 

APPENDIX PAGE No. 538 
( 

BORAL BRICKS 

FIRST ANALYTICAL LABORATORIES 

bt!ling: PO Bl'X 1103 72 ~ Research Trianlrle Pruic. NC 277CJ:J 

Jln}'Jiillg; 7$17 Pre(:.isionDr.h:e, Suitco 101 - :R.,teigh, NC '2761 7 ~~.~~~~~~ 

ANALYSIS REPORT 

TEL9l9 9428607 

F . ..:..:..''(: 919 882 .1603 

v. ''".,.· fn"Stan~ J:ytic.;llabs. c.om 

Project#: 100912 Report Date: 08-0ct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep- 10 

Client Project ID: P-10124 

Sample 

Blank Front 

Blank Back 

S. Inlet Run 1 Front 

S. Inlet Run 1 Back 

S. Inlet Run 2 Front 

S. Inlet Run 2 Back 

S. Inlet Run 3 Front 

S. Inlet Run 3 Back 

S. Outlet Run 1 Front 

S. Outlet Run 1 Back 

S. Outlet Run 2 Front 

S. Outlet Run 2 Back 

S. Outlet Run 3 Front 

S. Outlet Run 3 Back 

4 Inlet Run 1 Front 

4 Inlet Run 1 Back 

4 Inlet Run 2 Front 

4 Inlet Run 2 Back 

4 Inlet Run 3 Front 

4 Inlet Run 3 Back 

4 Outlet Run 1 Front 

4 Outlet Run 1 Back 

4 Outlet Run 2 Front 

4 Outlet Run 2 Back 

4 Outlet Run 3 Front 

4 Outlet Run 3 Back 

ATC PROJECT No. P-10142 

Total Micrograms in Sample 

p Se Ag Tl 

1-19 1-19 1-19 1-19 

10.5 < 1.0 < 0.5 < 0.5 

< 17.6 < 1.8 < 0.9 < 0.9 

37.7 1.3 < 2.5 < 0.5 

26.7 < 21.7 < 0.7 < 0.7 

35.7 1.5 < 0.5 < 0.5 

23.2 2.1 < 0.7 < 0.7 

31.5 < 1.0 < 0.5 < 0.5 

23.6 < 1.4 < 0.7 < 0.7 

16.0 < 1.0 < 0.5 < 0.5 

20.9 1 .9 < 0.7 < 0.7 

17.2 < 1.0 < 0.5 < 0.5 

17.6 < 1.5 < 0.8 < 0.8 

14.7 < 1.0 < 0.5 < 0.5 

24.1 < 1.4 < 0.7 < 0.7 

25.2 1.3 < 0.5 < 0.5 

16.1 < 1.4 < 0.7 < 0.7 

16.5 < 1.0 < 0.5 < 0.5 

19.5 2.4 < 0.7 < 0.7 

27.3 < 1.0 < 0.5 < 0.5 

< 14.3 1.4 < 0.7 < 0.7 

19.6 < 1.0 < 0.5 < 0.5 

20.8 < 1.4 < 0.7 < 0.7 

19.0 < 1.0 < 0.5 < 0.5 

17.4 < 1.4 < 0.7 < 0.7 

18.9 < 1.0 < 0.5 < 0.5 

< 14.5 < 1.4 < 0.7 < 0.7 

Page 9 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Zn 

1-19 

2.3 

< 0.9 

24.2 

12.2 

24.1 

4.6 

21.9 

2.5 

3.0 

2.0 

3.0 

3.4 

4.3 

2.5 

2.6 

3.3 

2.4 

5.5 

2.3 

4.2 

2.8 

5.6 

2.5 

2.1 

2.5 

7.0 

APPENDIX PAGE No. 539 
( 

BORAL BRICKS 

ANALYTICAL LABORATORIES 

blllin ... ~ PO B0.x. 110372- R~search Triangle P<lrk NC 27709 

7517 Pre-cisionDrin~. Smte 101 N Rrtleigh, NC 1i617 

ANAlYSIS REPORT 

TEL: 919 942&607 

F.<>;.X: 919 882 1603 

W\YW.firstanalyi.K-nllabs~~··(.'lU 

Project#: 100912 Report Dote: 08-0ct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep-1 0 

Client Project ID: P-10124 

Sample 

5 Inlet Run 1 Front 

5 Inlet Run 1 Bock 

5 Inlet Run 2 Front 

5 Inlet Run 2 Back 

5 Inlet Run 3 Front 

5 Inlet Run 3 Back 

5 Outlet Run 1 Front 

5 Outlet Run 1 Back 

5 Outlet Run 2 Front 

5 Outlet Run 2 Back 

5 Outlet Run 3 Front 

5 Outlet Run 3 Bock 

Spike, %Rec. Front 

Spike, %Rec. Bock 

Duplicate, %RPD Front 

Duplicate, %RPD Back 

ATC PROJECT No. P-10142 

Total Micrograms in Sample 

p Se Ag Tl 

Jig Jig Jig Jig 

17.1 1.9 < 0.5 < 0.5 

17.4 3.4 < 0.7 < 0.7 

30.4 4.4 < 0.5 < 0.5 

25.0 1.5 < 0.7 < 0.7 

18.5 7.5 < 0.5 < 0.5 

< 14.3 < 1.4 < 0.7 < 0.7 

< 10.0 < 1.0 < 0.5 < 0.5 

19.1 < 1.4 < 0.7 < 0.7 

< 10.0 < 1.0 < 0.5 < 0.5 

22.3 1.6 < 0.7 < 0.7 

10.0 < 1.0 < 0.5 < 0.5 

23.3 < 1.4 < 0.7 < 0.7 

QC SUMMARY 

101% 79% 77% 102% 

76% 93% 79% 99% 

N/A N/A N/A N/A 

N/A N/A N/A N/A 

Page 10 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Zn 

Jig 

4.9 

3.3 

4.1 

2.3 

4.2 

3.1 

4.0 

4.9 

2.8 

6.0 

2.4 

6.3 

88% 

92% 

2% 

N/A 

APPENDIX PAGE No. 540 
( 

BORAL BRICKS 

FIRST ANALYTICAL LABORATORIES 

b;iling PO Box 1103i2 ~Research Triancle Park. NC 27709 

shippmg: 7517 Precision Drive, Suite 101 - R.lleigh, NC 27617 ~"-~'1S'-k~1~"%'~ 

MERCURY ANALYSIS REPORT 

TEL: 919 942 8607 

FAX: 919 882 1603 

WW'>Y. firsbu;t<.\1) 1ica1labs. com 

Project#: 100912 Report Date: 07 -Oct-1 0 

Client: Analytical Testing Consultants, Inc. Date Received: 24-Sep-1 0 

Client Project I D: P- 1 0124 

Total Micrograms of Mercury in Sample 

Sample 

Blank 

Salisbury-Inlet-Run 1 

Salisbury-Inlet-Run 2 

Salisbury-Inlet-Run 3 

Salisbury-Outlet-Run 1 

Salisbury-Outlet-Run 2 

Salisbury-Outlet-Run 3 

Plant 4-lnlet-Run 1 

Plant 4-lnlet-Run 2 

Plant 4-lnlet-Run 3 

Plant 4-0utlet-Run 1 

Plant 4-0utlet-Run 2 

Plant 4-0utlet-Run 3 

Plant 5-lnlet-Run 1 

Plant 5-lnlet-Run 2 

Plant 5-lnlet-Run 3 

Plant 5-0utlet-Run 1 

Plant 5-0utlet-Run 2 

Plant 5-0utlet-Run 3 

BACK SPIKE Sol. Inlet 

BACK SPIKE Sal. Outlet 

BACK SPIKE-Plant 4 In 

BACK SPIKE-Plant 4 Out 

BACK SPIKE-Plant 5 In 

BACK SPIKE-Plant 5 Out 

ATC PROJECT No. P-10142 

Frac 1 Frac2B Frac3A Frac3B 

pg pg pg pg 

< 0.4 < 0.5 < 0.1 < 0.1 

< 0.4 < 1.3 < 0.3 < 0.4 

< 0.4 5.2 < 0.2 < 0.4 

< 0.4 3.8 < 0.3 < 0.4 

< 0.4 < 1.3 < 0.2 < 0.4 

<0.4 < 1.2 < 0.3 < 0.4 

< 0.4 < 1.5 < 0.3 < 0.4 

< 0.4 1.9 < 0.2 < 0.4 

< 0.4 1.6 < 0.2 < 0.4 

< 0.4 < 1.3 < 0.2 < 0.4 

< 0.4 2.3 < 0.2 0.7 

< 0.4 3.3 < 0.2 0.7 

< 0.4 2.6 < 0.2 0.6 

< 0.4 2.8 < 0.2 0.8 

< 0.4 2.3 < 0.2 1.1 

< 0.4 < 1.3 < 0.2 1.1 

< 0.4 5.7 < 0.2 < 0.4 

< 0.4 5.1 < 0.2 < 0.4 

< 0.4 5.2 < 0.2 < 0.4 

QC SUMMARY 

%Recovery 101% 

%Recovery 100% 

%Recovery 100% 

%Recovery 98% 

%Recovery 103% 

%Recovery 103% 

Page 11 of 103 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Frac3C Total 

j.lg pg 

< 0.4 < 1.5 

4.2 4.2 

7.2 12.4 

5.1 8.9 

< 1.1 < 3.4 

< 1.0 < 3.3 

< 1.0 < 3.6 

1.0 2.9 

< 1.1 1.6 

< 1.1 < 3.4 

1.2 4.2 

< 1.1 4.0 

< 1.0 3.2 

< 1.0 3.6 

< 1.0 3.4 

< 0.9 1.1 

1.0 6.1 

1.0 6.1 

1.2 6.4 

APPENDIX PAGE No. 541 
BORAL BRICKS 

ANTIMONY 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 10 IJg/l 

Proj. #: 100912 Postdig'n spike cone. = 100 IJg/l 

Date: 08-0ct-1 0 

Sample ID Test Dig'le Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

IJg/l IJg/l ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 1.6 1.6 100 < 1.0 

Salisbury Inlet Run 1 1 00912.SAI1-1 9.1 9.1 100 < 1.0 

Salisbury Inlet Run 2 100912.SAI2-1 7.8 7.8 100 < 1.0 

Salisbury Inlet Run 3 100912.SAI3-1 9.5 9.5 100 < 1.0 

Salisbury Outlet Run 1 100912.SA01-1 6.4 6.4 100 < 1.0 

Salisbury Outlet Run 2 1 00912.SA02-1 9.3 9.3 100 < 1.0 

Salisbury Outlet Run 3 100912.SA03-1 7.8 7.8 100 < 1.0 

Plant 4 Inlet Run 1 100912.411-1 9.2 9.2 100 < 1.0 

Pia nt 4 In let Run 2 100912.412-1 4.6 4.6 100 < 1.0 

Plant 4 Inlet Run 3 100912.413-1 8.6 8.6 100 < 1.0 

Plant 4 Outlet Run 1 100912.401-1 4.4 4.4 100 < 1.0 

Plant 4 Outlet Run 2 100912.402-1 3.8 3.8 100 < 1.0 

Plant 4 Outlet Run 3 100912.403-1 7.9 7.9 100 < 1.0 

Plant 5 Inlet Run 1 100912.511-1 1.0 1.0 100 < 1.0 

Plant 5 Inlet Run 2 100912.512-1 3.3 3.3 100 < 1.0 

Plant 5 Inlet Run 3 100912.513-1 4.7 4.7 100 < 1.0 

Plant 5 Outlet Run 1 100912.501-1 6.4 6.4 100 < 1.0 

Plant 5 Outlet Run 2 100912.502-1 2.5 2.5 100 < 1.0 

Plant 5 Outlet Run 3 100912.503-1 5.9 5.9 100 < 1.0 

ENERGY I ENVIRONMENTAL I ENGINEERING I CARBON MANAGEMENT 

ATC PROJECT No. P-10142 EPA I 

AUGUST; www.mmal.com 

rX PAGE No. 542 

: 
i 

\ 

BORAL BRICKS 

ANTIMONY 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL; 10 J!g/L 

Proj. #: 100912 Postdig'n spike cone. = 100 J!g/L 

Date: 08-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Total 

pg/L J1g/L ml ml ml !19 

BACK HALVES 

Blank 100912.B-2A 4.0 4.0 100 116 66 < 1.8 

Salisbury Inlet Run 1 100912.SAI1-2A 8.8 8.8 100 324 224 < 1.4 

Salisbury Inlet Run 2 100912.SAI2-2A 7.0 7.0 100 1 336 236 < 1.4 

Salisbury Inlet Run 3 100912.SA13-2A 7.0 7.0 100 1 356 256 < 1.4 

Salisbury Outlet Run 1 100912.SA01-2A 8.7 8.7 100 335 235 < 1.4 

Salisbury Outlet Run 2 100912.SA02-2A 8.3 8.3 100 288 188 < 1.5 

Salisbury Outlet Run 3 100912.SA03-2A 4.7 4.7 100 366 266 < 1.4 

Plant 4 Inlet Run 1 100912.411-2A 5.8 5.8 100 333 233 < 1.4 

Plant 4 Inlet Run 2 1 00912.412-2A 7.4 7.4 100 339 239 < 1.4 

Plant 4 Inlet Run 3 100912.413-2A 5.0 5.0 100 333 233 < 1.4 

Plant 4 Outlet Run 1 100912.401-2A 7.3 7.3 100 324 224 < 1.4 

Plant 4 Outlet Run 2 100912.402-2A 9.7 9.7 100 342 242 < 1.4 

Plant 4 Outlet Run 3 1 00912 .403-2A 4.7 4.7 100 323 223 < 1.4 

Plant 5 Inlet Run 1 100912.511-2A 8.5 8.5 100 339 239 < 1.4 

Plant 5 Inlet Run 2 100912.512-2A 7.7 7.7 100 351 251 < 1.4 

Plant 5 Inlet Run 3 1 00912.513-2A 9.7 9.7 100 333 233 < 1.4 

Plant 5 Outlet Run 1 100912.501-2A 4.9 4.9 100 350 250 < 1.4 

Plant 5 Outlet Run 2 1 00912.502 -2A 5.3 5.3 100 334 234 < 1.4 

Plant 5 Outlet Run 3 1 00912.503-2A 6.4 6.4 100 329 229 < 1.4 

FRONT SPIKE 100912.SA11-l 97.2 % REC = 97.2% 

BACK SPIKE 100912.SAI1-2A 124.8 % REC = 124.8% 

Page 13 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 543 
( 

BORAL BRICKS 

ARSENIC 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Clienf: Anoly!ical Testing Consul!ants, Inc. MDL~ 5 J.lg/L 

Proj. #: 100912 Postdig1

n spike cone. = 100 J.lg/L 

Dote: 06-0ct-1 0 

Sample ID Test Dig'fe Dil'n To!al Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd To!al 

J.lg/L J.lg/L ml ml ml J.l9 

FRONT HALVES 

Blank 1 00912.B-1 -1.6 -1.6 100 < 0.5 

Salisbury Inlet Run 1 100912.SAI1-1 22.6 22.6 100 2.3 

Salisbury Inlet Run 2 100912.SAI2-1 29.6 29.6 100 3.0 

Salisbury Inlet Run 3 10091 2 .SAI3-1 27.7 27.7 100 2.8 

Salisbury Outlet Run 1 100912.SA01-1 1.7 1.7 100 < 0.5 

Salisbury Outlet Run 2 1 00912.SA02-1 1.2 1.2 100 < 0.5 

Salisbury Outlet Run 3 100912.SA03-1 0.1 0.1 100 < 0.5 

Plant 4 Inlet Run 1 100912.411-1 2.4 2.4 100 < 0.5 

Plant 4 Inlet Run 2 100912.412-1 0.1 0.1 100 < 0.5 

Plant 4 Inlet Run 3 100912.413-1 0.5 0.5 100 < 0.5 

Plant 4 Outlet Run 1 100912.401-1 2.5 2.5 100 < 0.5 

Plant 4 Outlet Run 2 100912.402-1 3.6 3.6 100 < 0.5 

Plant 4 Outlet Run 3 100912.403-1 2.1 2.1 100 < 0.5 

Plant 5 Inlet Run 1 100912.511-1 18.9 18.9 100 1.9 

Plant 5 Inlet Run 2 100912.512-1 7.2 7.2 100 0.7 

Plant 5 Inlet Run 3 100912.513-1 2.1 2.1 100 < 0.5 

Plant 5 Outlet Run 1 100912.501-1 0.8 0.8 100 < 0.5 

Plant 5 Outlet Run 2 100912.502-1 0.7 0.7 100 < 0.5 

PlantS Outlet Run 3 100912.503-1 3.2 3.2 100 < 0.5 

Page 14 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 544 
BORAL BRICKS 

ARSENIC 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL~ 5 flg/L 

Proj. #: 100912 Postdig'n spike cone. = 100 flg/L 

Dole: 06-0ct-1 0 

Sample ID Test Dig'le Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

flg/L pg/L ml ml ml pg 

BACK HALVES 

Blank 1 00912.B-2A -0.2 -0.2 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SAI1-2A 26.6 26.6 100 324 224 3.9 

Salisbury Inlet Run 2 100912.SAI2-2A 35.0 35.0 100 336 236 5.0 

Salisbury Inlet Run 3 100912.SAI3-2A 26.4 26.4 100 356 256 3.7 

Salisbury Outlet Run 1 100912.SA01-2A 0.6 0.6 100 335 235 < 0.7 

Salisbury Outlet Run 2 1 00912.SA02-2A 1.8 1.8 100 288 188 < 0.8 

Salisbury Outlet Run 3 1 00912.SA03-2A 1.5 1.5 100 366 266 < 0.7 

Plant 4 Inlet Run 1 100912.411-2A 0.7 0.7 100 333 233 < 0.7 

Plant 4 Inlet Run 2 100912.412-2A 1.7 1.7 100 339 239 < 0.7 

Plant 4 Inlet Run 3 100912.413-2A 0.3 0.3 100 333 233 < 0.7 

Plant 4 Outlet Run 1 100912.401-2A -0.4 -0.4 100 324 224 < 0.7 

Plant 4 Outlet Run 2 100912.402-2A 0.7 0.7 100 342 242 < 0.7 

Plant 4 Outlet Run 3 100912.403-2A -0.3 -0.3 100 323 223 < 0.7 

Plant 5 Inlet Run 1 100912 .511-2A 15.9 15.9 100 339 239 2.3 

Plant 5 Inlet Run 2 100912.512-2A 3.6 3.6 100 351 251 < 0.7 

Plant 5 Inlet Run 3 1 00912.513-2A -0.1 -0.1 100 333 233 < 0.7 

Plant 5 Outlet Run 1 100912.501-2A -0.4 -0.4 100 350 250 < 0.7 

Plant 5 Outlet Run 2 100912.502-2A -0.5 -0.5 100 334 234 < 0.7 

Plant 5 Outlet Run 3 1 00912.503-2A -1.2 -1.2 100 329 229 < 0.7 

FRONT SPIKE 100912.411-1 75.9 % REC = 75.9% 

BACK SPIKE 100912.SAI1-2A 132.1 % REC = 105.4% 

Page 15 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 545 
BORAL BRICKS 

BARIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 25 jig/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 jig/l 

Date: 05-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

Jig/L Jig/L ml ml ml jig 

FRONT HALVES 

Blank 100912.8-1 13.6 13.6 100 < 2.5 

Salisbury Inlet Run 1 100912.SAI1-1 213.4 213.4 100 21.3 

Salisbury Inlet Run 2 100912.SA12-1 339.9 339.9 100 34.0 

Salisbury Inlet Run 3 100912.SA13-1 287.9 287.9 100 28.8 

Salisbury Outlet Run 1 100912.SA01-1 26.8 26.8 100 2.7 

Salisbury Outlet Run 2 1 00912.SA02-1 25.8 25.8 100 2.6 

Salisbury Outlet Run 3 1 00912.SA03-1 49.9 49.9 100 5.0 

Plant 4 Inlet Run 1 100912.411-1 35.6 35.6 100 3.6 

Plant 4 Inlet Run 2 100912.412-1 52.4 52.4 100 5.2 

Plant 4 Inlet Run 3 100912.413-1 49.8 49.8 100 5.0 

Plant 4 Outlet Run 1 100912.401-1 56.6 56.6 100 5.7 

Plant 4 Outlet Run 2 100912.402-1 50.7 50.7 100 5.1 

Plant 4 Outlet Run 3 100912.403-1 43.2 43.2 100 4.3 

Plant 5 Inlet Run 1 100912.511-1 54.6 54.6 100 5.5 

Plant 5 Inlet Run 2 100912.512-1 62.1 62.1 100 6.2 

Plant 5 Inlet Run 3 100912.513-1 60.8 60.8 100 6.1 

Plant 5 Outlet Run 1 100912.501-1 5.5 5.5 100 < 2.5 

Plant 5 Outlet Run 2 100912.502-1 7.1 7.1 100 < 2.5 

Plant 5 Outlet Run 3 100912.503-1 -21.0 -21.0 100 < 2.5 

Page 16 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 546 
BORAL BRICKS 

BARIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 25 119/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 119/L 

Date: 05-0ct-10 

Sample ID Test Di9'te DiPn Total Volume 

Client FAL Sol'n Cone FV Factor Volume Di9'd Total 

11g/L 119/L ml ml ml 119 

BACK HALVES 

Blank 1 00912.B-2A -42.5 -42.5 100 116 66 < 4.4 

Salisbury Inlet Run 1 l00912.SAI1-2A -10.3 -10.3 100 324 224 < 3.6 

Salisbury Inlet Run 2 100912.SAI2-2A 57.7 57.7 100 336 236 8.2 

Salisbury Inlet Run 3 l00912.SAI3-2A 29.3 29.3 100 356 256 4.1 

Salisbury Outlet Run 1 100912.SA01-2A 92.3 92.3 100 335 235 13.2 

Salisbury Outlet Run 2 100912.SA02-2A 14.4 14.4 100 288 188 < 3.8 

Salisbury Outlet Run 3 100912.SA03-2A 28.3 28.3 100 366 266 3.9 

Plant 4 Inlet Run 1 100912.41l-2A 5.3 5.3 100 333 233 < 3.6 

Plant 4 Inlet Run 2 100912.412-2A 104.5 104.5 100 339 239 14.8 

Plant 4 Inlet Run 3 1 00912.413-2A 114.4 114.4 100 333 233 16.3 

Plant 4 Outlet Run 1 100912.401-2A -3.2 -3.2 100 324 224 < 3.6 

Plant 4 Outlet Run 2 100912.402-2A 21.5 21.5 100 342 242 < 3.5 

Plant 4 Outlet Run 3 100912.403-2A 126.7 126.7 100 323 223 18.4 

Plant 5 Inlet Run 1 100912.51l-2A 66.9 66.9 100 339 239 9.5 

Plant 5 Inlet Run 2 100912.512-2A -62.5 -62.5 100 351 251 < 3.5 

Plant 5 Inlet Run 3 100912.513-2A 86.0 86.0 100 333 233 12.3 

Plant 5 Outlet Run 1 100912.501-2A 19.8 19.8 100 350 250 < 3.5 

Plant 5 Outlet Run 2 100912.502-2A 59.2 59.2 100 334 234 8.4 

Plant 5 Outlet Run 3 100912.503-2A 48.7 48.7 100 329 229 7.0 

FRONT SPIKE 100912.SA11-1S 1065.2 % REC = 85.2% 

BACK SPIKE l00912.411-2AS 972.7 % REC = 97.3% 

FRONT DUP 100912.SAI2-1D 326.5 RPD = 4.0% 

BACK DUP 100912.SAI2-2AD -0.1 RPD = N/A 

Page 17 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 547 
I 

\ 

BORAL BRICKS 

BERYL L I U M 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.5 J.lg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 J.lg/L 

Dote: 06-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL So/'n Cone FV Factar Volume Dig'd Total 

J.lg/L flg/l ml ml ml /19 

FRONT HALVES 

Blank 100912.8-1 -0.62 -0.6 100 < 0.05 

Salisbury Inlet Run 1 100912.SAI1-1 -0.42 -0.4 100 < 0.05 

Salisbury Inlet Run 2 100912.SAI2-1 -0.35 -0.4 100 < 0.05 

Salisbury Inlet Run 3 100912.SA13-1 -0.17 -0.2 100 < 0.05 

Salisbury Outlet Run 1 100912.SA01-1 -0.95 -0.9 100 < 0.05 

Salisbury Outlet Run 2 1 00912.SA02-1 -0.97 -1.0 100 < 0.05 

Salisbury Outlet Run 3 100912.SA03-1 -0.70 -0.7 100 < 0.05 

Plant4 Inlet Run 1 100912.411-1 -0.85 -0.8 100 < 0.05 

Plant 4 Inlet Run 2 100912.412-1 -0.93 -0.9 100 < 0.05 

Plant 4 Inlet Run 3 100912.413-1 -0.89 -0.9 100 < 0.05 

Plant 4 Outlet Run 1 100912.401-1 -1.14 - 1. 1 100 < 0.05 

Plant4 Outlet Run 2 100912.402-1 -1.08 -1.1 100 < 0.05 

Plant 4 Outlet Run 3 100912.403-1 -1.12 -1.1 100 < 0.05 

Plant 5 Inlet Run 1 100912.511-1 -0.86 -0.9 100 < 0.05 

Plant 5 Inlet Run 2 100912.512-1 -1.10 -1.1 100 < 0.05 

Plant 5 Inlet Run 3 100912.513-1 -0.93 -0.9 100 < 0.05 

Plant 5 Outlet Run 1 100912.501-1 -0.88 -0.9 100 < 0.05 

Plant 5 Outlet Run 2 100912.502-1 -1.15 -1.1 100 < 0.05 

Plant 5 Outlet Run 3 1 00912 .503-1 -1.25 -1.3 100 < 0.05 

Page 18ofl03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PlANTS 4 & 5, SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 548 
BORAL BRICKS 

BERYLLIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analyfical Testing Consultants, Inc. MDL= 0.5 J.lg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 J.lg/L 

Dale: 06-0ct-1 0 

Sample ID Test Dig'le Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

J.lg/L J.lg/L ml ml ml J.l9 

BACK HALVES 

Blank 100912.B-2A -1.39 -1.4 100 116 66 < 0.09 

Salisbury Inlet Run 1 100912.SA11-2A -1.35 -1.3 100 324 224 < 0.07 

Salisbury Inlet Run 2 1 00912.SAI2-2A -1.40 -1.4 100 336 236 < 0.07 

Salisbury Inlet Run 3 100912.SAI3-2A -1.80 -1.8 100 356 256 < 0.07 

Salisbury Outlet Run 1 100912.SA01-2A -1.95 -2.0 100 335 235 < 0.07 

Salisbury Outlet Run 2 100912.SA02-2A -1.03 -1.0 100 288 188 < 0.08 

Salisbury Outlet Run 3 1 00912.SA03-2A -1.39 -1.4 100 366 266 < 0.07 

Plant 4 Inlet Run 1 100912.411-2A -l. 75 -1 .8 100 333 233 < 0.07 

Plant 4 Inlet Run 2 100912.412-2A -0.84 -0.8 100 339 239 < 0.07 

Plant4 Inlet Run 3 1 00912.413-2A -1.32 -1.3 100 333 233 < 0.07 

Plant 4 Outlet Run 1 100912.401-2A -1.02 -1.0 100 324 224 < 0.07 

Plant 4 Outlet Run 2 1 00912.402-2A -1.62 -1.6 100 342 242 < 0.07 

Plant 4 Outlet Run 3 100912.403-2A -1.81 -1.8 100 323 223 < 0.07 

Pia nt 5 Inlet Run 1 100912.511 -2A -1.27 -1.3 100 339 239 < 0.07 

Plant 5 Inlet Run 2 100912.512-2A -1.78 -1.8 100 351 251 < 0.07 

Plant 5 Inlet Run 3 100912.513-2A -0.80 -0.8 100 333 233 < 0.07 

Plant 5 Outlet Run 1 100912.501-2A -1.09 - 1 . 1 100 350 250 < 0.07 

Plant 5 Outlet Run 2 100912.502-2A -1.61 -1.6 100 334 234 < 0.07 

Plant 5 Outlet Run 3 1 00912.503-2A -1.67 -1.7 100 329 229 < 0.07 

FRONT SPIKE 100912.SAI2-1S 834.62 % REC = 83.5% 

BACK SPIKE 1 00912.411-2AS 880.80 % REC = 88.1% 

FRONT DUP 100912.SA13-1 D -0.50 RPD = N/A 

BACK DUP 100912.SAI2-2AD -1.91 RPD = N/A 

Page 19 of 103 

ATC PROJECT No. P-1 0142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 549 
BORAL BRICKS 

CADMIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 Jlg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 Jlg/L 

Date: 06-0ct- 10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cane FY Factor Volume Dig'd Total 

Jlg/L 1'9/L ml ml ml Jig 

FRONT HALVES 

Blank 100912.8-1 -38.92 -38.9 100 < 0.30 

Salisbury Inlet Run 1 100912.SAI1-1 -27.94 -27.9 100 < 0.30 

Salisbury Inlet Run 2 100912.SAI2-1 -26.54 -26.5 100 < 0.30 

Salisbury Inlet Run 3 1 00912.SA13- 1 -44.27 -44.3 100 < 0.30 

Salisbury Outlet Run 1 100912.SA01. 1 -36.72 -36.7 100 < 0.30 

Salisbury Outlet Run 2 100912.SA02-1 -37.63 -37.6 100 < 0.30 

Salisbury Outlet Run 3 1 00912.SA03- 1 -36.61 -36.6 100 < 0.30 

Plant 4 Inlet Run 1 100912.411 "1 -41.66 -41.7 100 < 0.30 

Plant 4 In lei Run 2 100912.412-1 -44.94 -44.9 100 < 0.30 

Plant 4 Inlet Run 3 100912.413-1 -42.41 -42.4 100 < 0.30 

Plant 4 Outlet Run 1 100912.401-1 -44.19 -44.2 100 < 0.30 

Plant 4 Outlet Run 2 100912.402-1 -43.86 -43.9 100 < 0.30 

Plant 4 Outlet Run 3 100912.403-1 -44.36 -44.4 100 < 0.30 

Plant 5 Inlet Run 1 100912.511-1 -36.73 -36.7 100 < 0.30 

Plant 5 Inlet Run 2 100912.512-1 -48.43 -48.4 100 < 0.30 

Plant 5 Inlet Run 3 100912.513-1 -41.93 -41.9 100 < 0.30 

Planl 5 Outlet Run 1 100912.501 "1 -42.34 -42.3 100 < 0.30 

Plant 5 Outlet Run 2 100912.502-1 -49.68 -49.7 100 < 0.30 

Plant 5 Outlet Run 3 100912.503-1 -45.39 -45.4 100 < 0.30 

Page 20 of 1 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 550 
( 

BORAL BRICKS 

CADMIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 119/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 119/L 

Dote: 06-0ct-1 0 

Sample ID Test Di9'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

119/L 119/L ml ml ml 119 

BACK HALVES 

Blank 1 00912.8-2A -5.75 -5.7 100 116 66 < 0.53 

Salisbury Inlet Run 1 100912.SAl1-2A -5.40 -5.4 100 324 224 < 0.43 

Salisbury Inlet Run 2 100912.SAl2-2A -3.08 -3.1 100 336 236 < 0.43 

Salisbury Inlet Run 3 100912.SAl3-2A -0.69 -0.7 100 356 256 < 0.42 

Salisbury Outlet Run 1 100912.SA01-2A -0.15 -0.1 100 335 235 < 0.43 

Salisbury Outlet Run 2 100912.SA02-2A -0.71 -0.7 100 288 188 < 0.46 

Salisbury Outlet Run 3 100912.SA03-2A 0.05 0.1 100 366 266 < 0.41 

Plant 4 Inlet Run 1 1 00912.411-2A -0.48 -0.5 100 333 233 < 0.43 

Plant 4 Inlet Run 2 1 00912.412-2A 0.00 0.0 100 339 239 < 0.43 

Plant 4 Inlet Run 3 1 00912.413-2A 1.47 1.5 100 333 233 < 0.43 

Plant 4 Outlet Run 1 100912.401-2A 1.40 1.4 100 324 224 < 0.43 

Plant 4 Outlet Run 2 100912 .402-2A 0.36 0.4 100 342 242 < 0.42 

Plant 4 Outlet Run 3 100912.403-2A 0.20 0.2 100 323 223 < 0.43 

Plant 5 Inlet Run 1 100912.511-2A -1.10 -1.1 100 339 239 < 0.43 

Plant 5 Inlet Run 2 100912.512-2A -0.59 -0.6 100 351 251 < 0.42 

Plant 5 Inlet Run 3 100912.513-2A 0.61 0.6 100 333 233 < 0.43 

Plant 5 Outlet Run 1 100912.501-2A 2.39 2.4 100 350 250 < 0.42 

Plant 5 Outlet Run 2 1 00912.502-2A 0.57 0.6 100 334 234 < 0.43 

Plant 5 Outlet Run 3 1 00912.503-2A 2.05 2.1 100 329 229 < 0.43 

FRONT SPIKE 100912.SAI2-1S 776.31 % REC = 77.6% 

BACK SPIKE 1 00912.411-2AS 885.57 % REC = 88.6% 

FRONT DUP 100912.SA13-1 D -44.67 RPD = N/A 

BACK DUP 100912.SAI2-2AD -2.55 RPD = N/A 

Page 21 of 103 

ATC PROJECT No. P~ 10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 551 
BORAL BRICKS 

CHROMIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 pg/L 

Date: 05-0ct-1 0 

Sample ID Test Dig'te Diljn Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

pg/l pg/L ml ml ml J.l9 

FRONT HALVES 

Blank 100912.8-1 20.8 20.8 100 2.1 

Salisbury Inlet Run 1 100912.SAI1-1 16.9 16.9 100 1.7 

Salisbury Inlet Run 2 100912.SAI2-1 23.8 23.8 100 2.4 

Salisbury Inlet Run 3 1 00912.SAI3-1 24.1 24.1 100 2.4 

Salisbury Outlet Run 1 100912.SA01-1 16.4 16.4 100 1.6 

Salisbury Outlet Run 2 100912.SA02-1 13.4 13.4 100 1 1.3 

Salisbury Outlet Run 3 100912.SA03-1 14.2 14.2 100 1 1.4 

Plant 4 Inlet Run 1 100912.411-1 24.2 24.2 100 2.4 

Plant 4 Inlet Run 2 100912.412-1 21.6 21.6 100 2.2 

Plant4 Inlet Run 3 100912.413-1 22.7 22.7 100 2.3 

Plant 4 Outlet Run 1 100912.401-1 21.6 21.6 100 2.2 

Plant 4 Outlet Run 2 100912.402-1 22.3 22.3 100 2.2 

Pia nt 4 Outlet Run 3 100912.403-1 27.0 27.0 100 2.7 

Plant 5 Inlet Run 1 100912.511-1 16.4 16.4 100 1.6 

Plant 5 Inlet Run 2 100912.512-1 18.9 18.9 100 1.9 

Plant 5 Inlet Run 3 100912.513-1 20.3 20.3 100 2.0 

Plant 5 Outlet Run 1 100912.501-1 20.1 20.1 100 2.0 

Plant 5 Outlet Run 2 100912.502-1 16.3 16.3 100 1.6 

Plant 5 Outlet Run 3 100912.503-1 16.2 16.2 100 1.6 

Page 22 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 552 
BORAL BRICKS 

CHROMIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 Jlg/L 

Proj. #: 100912 Postdig 1

n spike cone. = 1000 Jlg/L 

Dale: 05-0ct-10 

Sample ID Test Dig'te Di11

n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

Jlg/L Jlg/L ml ml ml Jlg 

BACK HALVES 

Blank 100912.B-2A 0.1 0.1 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SAI1-2A 22.3 22.3 100 324 224 3.2 

Salisbury Inlet Run 2 100912.SA12-2A 12.5 12.5 100 336 236 1.8 

Salisbury Inlet Run 3 100912.SA13-2A 5.5 5.5 100 356 256 0.8 

Salisbury Outlet Run 1 100912.SA01-2A 21.9 21.9 100 335 235 3.1 

Salisbury Outlet Run 2 1 00912.SA02-2A 3.3 3.3 100 288 188 < 0.8 

Salisbury Outlet Run 3 100912.SA03-2A 2.1 2.1 100 366 266 < 0.7 

Planl4 Inlet Run 1 100912.411-2A 14.9 14.9 100 333 233 2.1 

Plant 4 Inlet Run 2 1 00912.412-2A 19.3 19.3 100 339 239 2.7 

Plant 4 Inlet Run 3 1 00912.413-2A 9.8 9.8 100 333 233 1.4 

Plant 4 Outlet Run 1 1 00912.401-2A 4.9 4.9 100 324 224 < 0.7 

Plant 4 Outlet Run 2 100912.402-2A 1.6 1.6 100 342 242 < 0.7 

Plant 4 Outlet Run 3 1 00912.403- 2A 4.3 4.3 100 323 223 < 0.7 

Plant 5 Inlet Run 1 1 00912.5ll-2A 21 .1 21.1 100 339 239 3.0 

Plant 5 Inlet Run 2 1 00912.512-2A 8.8 8.8 100 351 251 1.2 

Plant 5 Inlet Run 3 100912.513-2A 3.9 3.9 100 333 233 < 0.7 

Plant 5 Outlet Run 1 100912.501-2A 3.2 3.2 100 350 250 < 0.7 

Plant 5 Outlet Run 2 1 00912.502-2A 2.7 2.7 100 334 234 < 0.7 

Plant 5 Outlet Run 3 100912.503-2A 3.0 3.0 100 329 229 < 0.7 

FRONT SPIKE 100912.SA12-1 964.7 % REC ~ 94.1% 

BACK SPIKE 1 00912.SA12-2A 781.2 % REC ~ 76.9% 

FRONT DUP 1 00912.SAI3- 1 25.3 RPD = 4.8% 

BACK DUP 100912.SAI3-2A 4.8 RPD = N/A 

Page 23 of 1 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 553 
BORAL BRICKS 

COBALT 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 /lg/L 

Proj. #: 100912 Postdig'n spike cone. = 100 /19/L 

Date: 07 -Oct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

119/L pg/L ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 0.7 0.7 100 < 0.3 

Salisbury Inlet Run 1 100912.SAI1-1 -0.7 -0.7 100 < 0.3 

Salisbury Inlet Run 2 1 00912.SAI2- 1 0.0 0.0 100 < 0.3 

Salisbury Inlet Run 3 100912.SA13-1 0.4 0.4 100 < 0.3 

Salisbury Outlet Run 1 100912.SA01-1 -0.4 -0.4 100 < 0.3 

Salisbury Outlet Run 2 1 00912.SA02-1 -1.2 -1.2 100 1 < 0.3 

Salisbury Outlet Run 3 100912.SA03-1 -1.0 -1.0 100 1 < 0.3 

Plant 4 Inlet Run 1 100912.411-1 -0.2 -0.2 100 < 0.3 

Plant 4 Inlet Run 2 100912.412-1 0.1 0.1 100 < 0.3 

Plant 4 Inlet Run 3 100912.413-1 -0.4 -0.4 100 < 0.3 

Plant 4 Outlet Run 1 100912.401-1 -0.8 -0.8 100 < 0.3 

Plant 4 Outlet Run 2 100912.402-1 -0.3 -0.3 100 < 0.3 

Plant 4 Outlet Run 3 100912.403-1 -1.0 -1.0 100 < 0.3 

Plant 5 Inlet Run 1 100912.511-1 0.5 0.5 100 < 0.3 

Plant 5 Inlet Run 2 100912.512-1 -1.5 -1.5 100 < 0.3 

Plant 5 Inlet Run 3 100912.513-1 -1.5 -1.5 100 < 0.3 

Plant 5 Outlet Run 1 100912.501-1 -2.2 -2.2 100 < 0.3 

Plant 5 Outlet Run 2 100912.502-1 -0.1 -0.1 100 1 < 0.3 

Plant 5 Outlet Run 3 100912.503-1 0.1 0.1 100 1 < 0.3 

Page 24 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 554 
BORAL BRICKS 

COBALT 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 Jig/L 

Proj. #: 100912 Postdig'n spike cone. = 100 JIQ/l 

Dale: 07-0ct-10 

Sample ID Test Dig'fe Dil'n Tolal Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Toto! 

Jig/L Jig/l ml ml ml Jig 

BACK HALVES 

Blank 1 00912.B-2A -0.6 -0.6 100 1 116 66 < 0.5 

Salisbury Inlet Run 1 100912.SA11-2A -1.3 -39.6 100 30 324 224 < 13.0 

Salisbury Inlet Run 2 100912.SAI2-2A 1.2 1.2 100 336 236 < 0.4 

Salisbury Inlet Run 3 100912.SAI3-2A 0.0 0.0 100 356 256 < 0.4 

Salisbury Outlet Run 1 100912.SA01-2A 1.1 1.1 100 335 235 < 0.4 

Salisbury Outlet Run 2 1 00912.SA02-2A 0.6 0.6 100 288 188 < 0.5 

Salisbury Outlet Run 3 1 00912.SA03-2A -0.2 -0.2 100 366 266 < 0.4 

Plant 4 Inlet Run 1 1 00912.411-2A 0.3 0.3 100 333 233 < 0.4 

Plant 4 Inlet Run 2 100912.412-2A 0.2 0.2 100 339 239 < 0.4 

Plant 4 Inlet Run 3 100912.413-2A 0.0 0.0 100 1 333 233 < 0.4 

Pion! 4 Outlet Run 1 100912.401-2A 15.8 15.8 100 1 324 224 2.3 

Plant 4 Outlet Run 2 1 00912.402-2A 7.5 7.5 100 342 242 1.1 

Plant 4 Outlet Run 3 1 00912.403-2A 5.4 5.4 100 323 223 0.8 

Plant 5 Inlet Run 1 1 00912.511-2A -1.2 -1.2 100 339 239 < 0.4 

Plant 5 Inlet Run 2 1 00912.512-2A -3.0 -3.0 100 351 251 < 0.4 

Plant 5 inlet Run 3 1 00912.513-2A -1.4 -1.4 100 333 233 < 0.4 

Plant 5 Outlet Run 1 1 00912.501-2A 0.4 0.4 100 350 250 < 0.4 

Plant 5 Outlet Run 2 100912.502-2A 0.5 0.5 100 334 234 < 0.4 

Pion! 5 Outlet Run 3 1 00912.503-2A -1.4 -1.4 100 329 229 < 0.4 

FRONT SPIKE 100912.SAI1-1 82.1 % REC = 82.1% 

BACK SPIKE 1 00912.SAI1-2A 78.3 % REC = 78.3% 

Page 25 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 555 
BORAL BRICKS 

COPPER 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/l 

Proj. #: 100912 Postdig'n spike cone. = 1000 pg/l 

Date: 05-0ct-1 0 

Sample ID Test Dig'le Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Total 

pg/l pg/l ml ml ml /19 

FRONT HALVES 

Blank 100912.8-1 1.8 1.8 100 < 0.5 

Salisbury Inlet Run 1 1 00912.SAI1-1 53.2 53.2 100 5.3 

Salisbury Inlet Run 2 1 00912.SAI2-1 52.6 52.6 100 5.3 

Salisbury Inlet Run 3 100912.SA13-1 48.1 48.1 100 4.8 

Salisbury Outlet Run 1 100912.SA01-1 2.2 2.2 100 1 < 0.5 

Salisbury Outlet Run 2 1 00912.SA02-1 3.3 3.3 100 1 < 0.5 

Salisbury Outlet Run 3 1 00912.SA03-1 2.9 2.9 100 < 0.5 

Plant 4 Inlet Run 1 100912.411-1 3.1 3.1 100 < 0.5 

Plant 4 Inlet Run 2 100912.412-1 1.5 1.5 100 < 0.5 

Plant 4 Inlet Run 3 100912.413-1 2.1 2.1 100 < 0.5 

Plant 4 Outlet Run 1 100912.401-1 4.2 4.2 100 < 0.5 

Plant 4 Outlet Run 2 1 00912 .402-1 2.4 2.4 100 < 0.5 

Plant 4 Outlet Run 3 100912.403-1 3.2 3.2 100 < 0.5 

Plant 5 Inlet Run 1 100912.511-1 8.2 8.2 100 0.8 

Plant 5 Inlet Run 2 100912.512-1 7.6 7.6 100 0.8 

Plant 5 Inlet Run 3 100912.513-1 7.9 7.9 100 0.8 

Plant 5 Outlet Run 1 100912.501-1 1.7 1.7 100 < 0.5 

Plant 5 Outlet Run 2 100912.502-1 2.6 2.6 100 < 0.5 

Plant 5 Outlet Run 3 100912.503-1 2.8 2.8 100 < 0.5 

Poge 26 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 556 
BORAL BRICKS 

COPPER 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/l 

Proj. #: 100912 Posfdig'n spike cone. = 1000 pg/L 

Dale: 05-0cl-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Fodor Volume Dig'd Total 

Jlg/l Jlg/l ml ml ml Jlg 

BACK HALVES 

Blank 100912.B-2A 1.4 1.4 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SAI1-2A 26.5 26.5 100 324 224 3.8 

Salisbury Inlet Run 2 100912.SAI2-2A 14.6 14.6 100 336 236 2.1 

Salisbury Inlet Run 3 100912.SA13-2A 16.5 16.5 100 356 256 2.3 

Salisbury Outlet Run 1 100912.SA01-2A 6.3 6.3 100 335 235 0.9 

Salisbury Outlet Run 2 100912.SA02-2A 8.3 8.3 100 288 188 1.3 

Salisbury Outlet Run 3 1 00912.SA03-2A 11.1 11.1 100 366 266 1.5 

Plant 4 Inlet Run 1 100912.411-2A 6.7 6.7 100 333 233 1.0 

Plant4 Inlet Run 2 1 00912.412-2A 7.7 7.7 100 339 239 1.1 

Plant 4 Inlet Run 3 1 00912.413-2A 5.7 5.7 100 333 233 0.8 

Plant 4 Outlet Run 1 100912.401-2A 10.1 10.1 100 324 224 1.5 

Plant 4 Outlet Run 2 1 00912.402 -2A 4.1 4.1 100 342 242 < 0.7 

Plant 4 Outlet Run 3 1 00912.403-2A 14.2 14.2 100 323 223 2.1 

Plant 5 Inlet Run 1 1 00912.511-2A 8.0 8.0 100 339 239 1.1 

Plant 5 Inlet Run 2 100912.512-2A 6.3 6.3 100 351 251 0.9 

Plant 5 Inlet Run 3 1 00912.513-2A 8.9 8.9 100 333 233 1.3 

Plant 5 Outlet Run 1 1 00912.501-2A 12.3 12.3 100 350 250 1.7 

Plant 5 Outlet Run 2 100912.502-2A 10.8 10.8 100 334 234 1.5 

Plant 5 Outlet Run 3 1 00912.503-2A 10.3 10.3 100 329 229 1.5 

FRONT SPIKE 100912.SAI2-1 1046.5 %REC = 99.4% 

BACK SPIKE 1 00912.SAI2-2A 834.8 % REC = 82.0% 

FRONT DUP 100912.SA13-1D 49.0 RPD = 1.8% 

BACK DUP 1 00912.SAI3-2AD 18.1 RPD = N/A 

Page 27 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 557 
BORAL BRICKS 

LEAD 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL~ 5 J.lg/l 

Proj. #: 100912 Postdig~n spike cone. = 100 J.lg/l 

Date: 06-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

J.lg/L J.lg/L ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 2.2 2.2 100 < 0.5 

Salisbury Inlet Run 1 100912.SA11-1 86.6 86.6 100 8.7 

Salisbury Inlet Run 2 1 00912.SAI2-1 79.5 79.5 100 7.9 

Salisbury Inlet Run 3 1 00912.SAI3-1 71.1 71.1 100 7.1 

Salisbury Outlet Run 1 l00912.SA01-1 2.2 2.2 100 < 0.5 

Salisbury Outlet Run 2 1 00912.SA02-1 1.7 1.7 100 < 0.5 

Salisbury Outlet Run 3 1 00912.SA03-1 2.6 2.6 100 < 0.5 

Plant 4 Inlet Run 1 100912.411-1 1.8 1.8 100 < 0.5 

Plant 4 Inlet Run 2 100912.412-1 1.4 1.4 100 < 0.5 

Plant 4 Inlet Run 3 100912.413-1 2.1 2.1 100 < 0.5 

Plant 4 Outlet Run 1 100912.401-1 4.0 4.0 100 < 0.5 

Plant 4 Outlet Run 2 100912.402-1 3.0 3.0 100 < 0.5 

Plant 4 Outlet Run 3 100912.403-1 3.0 3.0 100 < 0.5 

Plant 5 Inlet Run 1 100912.511-1 7.8 7.8 100 0.8 

Plant 5 Inlet Run 2 100912.512-1 6.3 6.3 100 0.6 

Plant 5 Inlet Run 3 100912.513-1 5.5 5.5 100 0.6 

Plant 5 Outlet Run 1 100912.501-1 4.3 4.3 100 < 0.5 

Plant 5 Outlet Run 2 100912.502-1 1.3 1.3 100 < 0.5 

Plant 5 Outlet Run 3 100912.503-1 2.9 2.9 100 < 0.5 

Page 28 of 1 03 

ATC PROJECT No. P~10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 558 
BORAL BRICKS 

LEAD 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/L 

Proj. #: 100912 Postdig'n spike cone. == 100 pg/L 

Date: 06-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

f!g/L pg/L ml ml ml fl9 

BACK HALVES 

Blank 100912.B-2A 1.7 1.7 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SA11-2A 17.3 17.3 100 324 224 2.5 

Salisbury Inlet Run 2 1 00912.SAI2-2A 5.3 5.3 100 336 236 0.8 

Salisbury Inlet Run 3 1 00912.SAI3-2A -3.8 -3.8 100 356 256 < 0.7 

Salisbury Outlet Run 1 100912.SA01-2A 3.5 3.5 100 335 235 < 0.7 

Salisbury Outlet Run 2 100912.SA02-2A 0.7 0.7 100 28B 188 < 0.8 

Salisbury Outlet Run 3 100912.SA03-2A 2.3 2.3 100 366 266 < 0.7 

Plant 4 Inlet Run 1 1 00912.411-2A 3.2 3.2 100 333 233 < 0.7 

Plant 4 Inlet Run 2 100912.412-2A 7.5 7.5 100 339 239 1.1 

Plant 4 Inlet Run 3 100912.413-2A 2.7 2.7 100 333 233 < 0.7 

Plant 4 Outlet Run 1 100912.401-2A 4.6 4.6 100 324 224 < 0.7 

Plant 4 Outlet Run 2 100912.402-2A 1.9 1.9 100 342 242 < 0.7 

Plant 4 Outlet Run 3 100912.403-2A 5.9 5.9 100 323 223 0.8 

Plant 5 Inlet Run 1 100912.511-2A 9.4 9.4 100 339 239 1.3 

Plant 5 Inlet Run 2 100912.512-2A 4.7 4.7 100 351 251 < 0.7 

Plant 5 Inlet Run 3 1 00912.513-2A 2.7 2.7 100 333 233 < 0.7 

Plant 5 Outlet Run 1 1 00912.501-2A 6.3 6.3 100 350 250 0.9 

Plant 5 Outlet Run 2 100912.502-2A 3.7 3.7 100 334 234 < 0.7 

Plant 5 Outlet Run 3 100912.503-2A 5.3 5.3 100 329 229 0.8 

FRONT SPIKE 100912.SA11-1 177.5 % REC; 90.9% 

BACK SPIKE 100912.SAI1-2A 111.8 % REC; 94.5% 

Page 29 of 1 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 559 
BORAL BRICKS 

MAGNESIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 pg/L 

Date: 06-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cane FV Factor Volume Dig'd Total 

pg/L pg/L ml ml ml pg 

FRONT HALVES 

Blank 100912.8-1 128.8 128.8 100 12.9 

Salisbury Inlet Run 1 100912.SA11- 1 367.5 367.5 100 36.7 

Salisbury Inlet Run 2 1 00912.SAI2-1 458.4 458.4 100 45.8 

Salisbury Inlet Run 3 1 00912.SA13-1 507.7 507.7 100 50.8 

Salisbury Outlet Run 1 100912.SA01-1 114.7 114.7 100 11.5 

Salisbury Outlet Run 2 100912.SA02-1 115.7 115.7 100 11.6 

Salisbury Outlet Run 3 1 00912.SA03-1 119.5 119.5 100 12.0 

Plant 4 Inlet Run 1 100912.411-1 186.0 186.0 100 18.6 

Plant 4 Inlet Run 2 100912.412-1 157.2 157.2 100 15.7 

Plant 4 Inlet Run 3 100912.413-1 141.5 141.5 100 1 14.1 

Plant 4 Outlet Run 1 100912.401-1 188.5 188.5 100 1 18.9 

Plant 4 Outlet Run 2 100912.402-1 185.5 185.5 100 18.6 

Plant 4 Outlet Run 3 100912.403-1 191.2 191.2 100 19.1 

Plant 5 Inlet Run 1 100912.511-1 305.2 305.2 100 30.5 

Plant 5 Inlet Run 2 100912.512-1 303.5 303.5 100 30.4 

Plant 5 Inlet Run 3 100912.513-1 229.1 229.1 100 22.9 

Plant 5 Outlet Run 1 100912.501-1 216.2 216.2 100 21.6 

Plant 5 Outlet Run 2 100912.502-1 209.9 209.9 100 21.0 

Plant 5 Outlet Run 3 100912.503-1 243.6 243.6 100 24.4 

Page 30 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 560 
BORAL BRICKS 

MAGNESIUM 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 )lg/l 

Proj. #: 1 00912 Postdig'n spike cone. = 1000 )lg/l 

Dote: 06-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Total 

)lg/l )lg/l ml ml ml Jlg 

BACK HALVES 

Blank 100912.B-2A 16.6 16.6 100 116 66 2.9 

Salisbury Inlet Run 1 1 00912.SAI1-2A 915.1 915.1 100 324 224 132.4 

Salisbury Inlet Run 2 100912.SAI2-2A 286.5 286.5 100 336 236 40.8 

Salisbury Inlet Run 3 100912.SAI3-2A 896.7 896.7 100 356 256 124.7 

Salisbury Outlet Run 1 100912.SA01-2A 32.3 32.3 100 335 235 4.6 

Salisbury Outlet Run 2 100912.SA02-2A 47.3 47.3 100 288 188 7.2 

Salisbury Outlet Run 3 100912.SA03-2A 44.1 44.1 100 366 266 6.1 

Plant 4 Inlet Run 1 100912.411-2A 742.8 1485.6 100 2 333 233 212.3 

Plant 4 Inlet Run 2 100912.412-2A 1714.2 1714.2 100 339 239 243.1 

Plant 4 Inlet Run 3 100912.413-2A 882.8 882.8 100 333 233 126.2 

Plant 4 Outlet Run 1 100912.401-2A 86.7 86.7 100 324 224 12.5 

Plant 4 Outlet Run 2 100912.402-2A 78.8 78.8 100 342 242 11.1 

Plant 4 Outlet Run 3 1 00912.403-2A 141.7 141.7 100 323 223 20.5 

Plant 5 Inlet Run 1 100912.511-2A 2035.4 2035.4 100 339 239 288.7 

Plant 5 Inlet Run 2 100912.512-2A 789.6 789.6 100 351 251 110.4 

Plant 5 Inlet Run 3 1 00912.513-2A 815.7 815.7 100 333 233 116.6 

Plant 5 Outlet Run 1 100912.501-2A 71.8 71.8 100 350 250 10.1 

Plant 5 Outlet Run 2 100912.502-2A 1100.4 1100.4 100 334 234 157.1 

Plant 5 Outlet Run 3 1 00912.503-2A 584.4 584.4 100 329 229 84.0 

FRONT SPIKE 100912.411-1S 1029.6 % REC = 84.4% 

BACK SPIKE 100912.411-2AS 1683.6 % REC = 94.1% 

FRONT DUP 100912.412-1 D 156.8 RPD = 0.2% 

BACK DUP 100912.412-2AD 1744.6 RPD = 1.8% 

Page 3l of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 561 
BORAL BRICKS 

MANGANESE 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 2 pg/L 

Proj. #: 100912 Posfdig'n spike cone. = 1000 pg/L 

Date: 05-0ct-10 

Sample ID Test Dig'te Dil1

n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

pg/L pg/L ml ml ml pg 

FRONT HALVES 

Blank 100912.8-1 10.9 10.9 100 1 1.1 

Salisbury Inlet Run 1 100912.SAI1-1 118.2 118.2 100 11.8 

Salisbury Inlet Run 2 l00912.SAI2-1 121.2 121.2 100 12.1 

Salisbury Inlet Run 3 100912.SA13-1 123.0 123.0 100 12.3 

Salisbury Outlet Run 1 100912.SA01-1 15.8 15.8 100 1.6 

Salisbury Oullet Run 2 100912.SA02-1 13.5 13.5 100 1.3 

Salisbury Outlet Run 3 100912.SA03-1 19.4 19.4 100 1.9 

Plan! 4 Inlet Run 1 100912.411-1 13.0 13.0 100 1 1.3 

Plan! 4 Inlet Run 2 100912.412-1 12.0 12.0 100 1 1.2 

Plant 4 Inlet Run 3 100912.413-1 14.9 14.9 100 1.5 

Plant 4 Outlet Run 1 100912.401-1 12.9 12.9 100 1.3 

Plant 4 Outlet Run 2 100912.402-1 11.8 11.8 100 1.2 

Plant 4 Outlet Run 3 100912.403-1 12.5 12.5 100 1.3 

Plant 5 Inlet Run 1 100912.511-1 53.6 53.6 100 5.4 

Plan! 5 Inlet Run 2 100912.512-1 61.7 61.7 100 1 6.2 

Plant 5 Inlet Run 3 100912.513-1 36.2 36.2 100 1 3.6 

Plant 5 Outlet Run 1 100912.501-1 19.4 19.4 100 1.9 

Plant 5 Outlet Run 2 100912.502-1 20.5 20.5 100 2.0 

Plan! 5 Oullet Run 3 100912.503-1 22.9 22.9 100 2.3 

Page 32 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 562 
BORAL BRICKS 

MANGANESE 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 2 IJg/L 

Pro;.#: 100912 Postdig'n spike cone. = 1000 IJg/L 

Date: 05-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Toto! 

IJg/L IJg/L ml ml ml 119 

BACK HALVES 

Blank 100912.B-2A 1.0 1.0 100 116 66 < 0.4 

Salisbury Inlet Run 1 100912.SAI1-2A 150.5 150.5 100 324 224 21.8 

Salisbury Inlet Run 2 100912.SA12-2A 44.7 44.7 100 336 236 6.4 

Salisbury Inlet Run 3 100912.SA13-2A 44.4 44.4 100 356 256 6.2 

Salisbury Outlet Run 1 100912.SA01-2A 10.1 I 0.1 100 335 235 1.4 

Salisbury Outlet Run 2 1 00912.SA02-2A 14.4 14.4 100 288 188 2.2 

Salisbury Outlet Run 3 100912.SA03-2A 80.2 80.2 100 366 266 11.0 

Plant 4 Inlet Run 1 100912.411-2A 31.8 31.8 100 333 233 4.6 

Plant 4 Inlet Run 2 100912.412-2A 32.9 32.9 100 339 239 4.7 

Plant 4 Inlet Run 3 1 00912.413-2A 16.1 16.1 100 333 233 2.3 

Plant 4 Oullet Run 1 100912.401-2A 17.9 17.9 100 324 224 2.6 

Plant 4 Oullet Run 2 1 00912.402-2A 8.4 8.4 100 342 242 1.2 

Plant 4 Outlet Run 3 100912.403-2A 17.9 17.9 100 323 223 2.6 

Plant 5 Inlet Run 1 100912.511-2A 179.0 179.0 100 339 239 25.4 

Plant 5 Inlet Run 2 100912.512-2A 20.7 20.7 100 351 251 2.9 

Plant 5 Inlet Run 3 I 00912.513-2A 25.5 25.5 100 333 233 3.6 

Plant 5 Outlet Run 1 100912.501-2A 12.1 12.1 100 350 250 1.7 

Plant 5 Outlet Run 2 100912.502-2A 108.7 108.7 100 334 234 15.5 

Plant 5 Outlet Run 3 1 00912.503-2A 11.6 11.6 100 329 229 1.7 

FRONT SPIKE 100912.SAI2-1 1042.7 % REC = 92.1% 

BACK SPIKE 100912.SAI2-2A 807.0 % REC = 76.2% 

FRONT DUP I 00912.SA13-1 D 125.3 RPD = 1.9% 

BACK DUP 1 00912.SAI3-2AD 47.2 RPD = 6.3% 

Page 33 af l 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 563 
BORAL BRICKS 

NICKEL 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 119/l 

Proj. #: 100912 Postdig*n spike cone. = 1000 119/l 

Dote: 05-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Total 

119/L 119/L ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 6.4 6.4 100 0.6 

Salisbury Inlet Run 1 100912.SA11-1 5.6 5.6 100 0.6 

Salisbury Inlet Run 2 100912.SAI2-1 8.7 8.7 100 0.9 

Salisbury Inlet Run 3 100912.SAI3-1 9.9 9.9 100 1.0 

Salisbury Outlet Run 1 100912.SA01-1 6.6 6.6 100 0.7 

Salisbury Outlet Run 2 1 00912.SA02-1 6.7 6.7 100 0.7 

Salisbury Outlet Run 3 100912.SA03-1 8.1 8.1 100 0.8 

Plant 4 Inlet Run 1 100912.411-1 17.4 17.4 100 1.7 

Plant 4 Inlet Run 2 100912.412-1 10.1 10.1 100 1.0 

Plant 4 Inlet Run 3 100912.413-1 13.7 13.7 100 1.4 

Plant 4 Outlet Run 1 100912.401-1 11.2 11.2 100 1.1 

Plant 4 Outlet Run 2 100912.402-1 12.6 12.6 100 1.3 

Plant4 Outlet Run 3 100912.403-1 16.4 16.4 100 1.6 

Plant 5 Inlet Run 1 100912.511-1 11.0 11.0 100 1 . 1 

Plant 5 Inlet Run 2 100912.512-1 14.5 14.5 100 1.4 

Plant 5 Inlet Run 3 100912.513-1 10.3 10.3 100 1.0 

Plant 5 Outlet Run 1 100912.501-1 8.5 8.5 100 0.8 

Plant 5 Outlet Run 2 100912.502-1 9.1 9.1 100 0.9 

Plant 5 Outlet Run 3 100912.503-1 10.7 10.7 100 1 . 1 

Page 34 of l 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 564 
BORAL BRICKS 

NICKEL 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 3 pg/l 

Proj. #: 100912 Postdig'n spike cone. = 1000 pg/l 

Date: 05-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAl Sol'n Cone FV Factor Volume Dig'd Total 

pg/l pg/l ml ml ml !19 

BACK HALVES 

Blank 100912.B-2A 1.5 1.5 100 116 66 < 0.5 

Salisbury Inlet Run 1 100912.SA11-2A 124.3 124.3 100 324 224 18.0 

Salisbury Inlet Run 2 100912.SAI2-2A 24.5 24.5 100 336 236 3.5 

Salisbury Inlet Run 3 100912.SAI3-2A 32.5 32.5 100 356 256 4.5 

Salisbury Outlet Run 1 1 00912.SA01-2A 114.5 114.5 100 335 235 16.3 

Salisbury Outlet Run 2 100912.SA02-2A 12.9 12.9 100 288 188 2.0 

Salisbury Outlet Run 3 100912.SA03-2A 9.9 9.9 100 366 266 1.4 

Plant 4 Inlet Run 1 100912.411-2A 9.4 9.4 100 333 233 1.3 

Plant 4 Inlet Run 2 1 00912.412-2A 15.8 15.8 100 339 239 2.2 

Plant 4 Inlet Run 3 100912.413-2A 12.8 12.8 100 333 233 1.8 

Plant 4 Outlet Run 1 1 00912.401-2A 11.7 11.7 100 324 224 1.7 

Plant 4 Outlet Run 2 100912.402-2A 3.8 3.8 100 342 242 0.5 

Plant 4 Outlet Run 3 100912.403-2A 8.2 8.2 1 oo 323 223 1.2 

Plant 5 Inlet Run 1 100912.511-2A 17.3 17.3 100 339 239 2.5 

Plant 5 Inlet Run 2 100912.512-2A 7.0 7.0 100 351 251 1.0 

Plant 5 Inlet Run 3 100912.513-2A 6.5 6.5 100 333 233 0.9 

Plant 5 Outlet Run 1 100912.501-2A 5.5 5.5 100 350 250 0.8 

Plant 5 Outlet Run 2 100912.502-2A 4.8 4.8 100 334 234 0.7 

Plant 5 Outlet Run 3 1 00912.503-2A 7.6 7.6 100 329 229 1.1 

FRONT SPIKE 1 00912.SAI2·1 1053.6 % REC = 104.5% 

BACK SPIKE 100912.SAI2-2A 874.0 % REC = 85.0% 

FRONT DUP 1 00912.SAI3-1 D 11 .4 RPD = N/A 

BACK DUP 1 00912.SAI3-2AD 36.8 RPD = 12.5% 

Page 35 of 103 

ATC PROJECT No. P·10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 565 
BORAL BRICKS 

PHOSPHORUS 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 100 fJg/l 

Proj. #: 100912 Postdig'n spike cone. = 5000 Jlg/l 

Dale: 05-0ct-1 0 

Sample ID Tesl Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

Jlg/L Jlg/L ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 104.5 104.5 100 10.5 

Salisbury Inlet Run 1 100912.SAI1-1 188.7 377.4 100 2 37.7 

Salisbury Inlet Run 2 100912.SAI2-1 356.8 356.8 100 35.7 

Salisbury Inlet Run 3 1 00912 .SA13- 1 314.6 314.6 100 31.5 

Salisbury Outlet Run 1 100912.SA01-1 159.8 159.8 100 16.0 

Salisbury Outlet Run 2 1 00912.SA02-1 171.5 171.5 100 17.2 

Salisbury Outlet Run 3 1 00912.SA03-1 147.1 147.1 100 14.7 

Plant 4 Inlet Run 1 100912.411-1 252.4 252.4 100 25.2 

Plant 4 Inlet Run 2 100912.412-1 165.5 165.5 100 16.5 

Plant4 Inlet Run 3 100912.413-1 272.6 272.6 100 27.3 

Plant 4 Outlet Run 1 100912.401-1 195.7 195.7 100 19.6 

Plant 4 Outlet Run 2 100912.402-1 190.5 190.5 100 19.0 

Plant 4 Outlet Run 3 100912.403-1 189.2 189.2 100 18.9 

PlantS Inlet Run 1 100912.511-1 171.0 171.0 100 17.1 

Plant 5 Inlet Run 2 100912.512-1 303.6 303.6 100 30.4 

Plant 5 Inlet Run 3 100912.513-1 185.3 185.3 100 18.5 

Plant 5 Outlet Run 1 100912.501-1 76.7 76.7 100 < 10.0 

Plant 5 Outlet Run 2 100912.502-1 89.4 89.4 100 < 10.0 

Plant 5 Outlet Run 3 100912.503-1 100.4 100.4 100 10.0 

Paga 36 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 566 
BORAL BRICKS 

PHOSPHORUS 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 100 119/L 

Proj. #: 100912 Postdig1

n spike cone. = 5000 119/L 

Date: 05-0c!-1 0 

Sample ID Test Dig1

fe OWn Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

119/L 119/l ml ml ml 119 

BACK HALVES 

Blank 100912.B-2A 42.3 42.3 100 116 66 < 17.6 

Salisbury Inlet Run 1 1 00912.SA11-2A 184.6 184.6 100 324 224 26.7 

Salisbury Inlet Run 2 100912.SAI2-2A 163.2 163.2 100 336 236 23.2 

Salisbury Inlet Run 3 100912.SAI3-2A 169.7 169.7 100 356 256 23.6 

Salisbury Outlet Run 1 100912.SA01-2A 146.4 146.4 100 335 235 20.9 

Salisbury Outlet Run 2 100912.SA02-2A 115.1 115.1 100 288 188 17.6 

Salisbury Outlet Run 3 1 00912.SA03-2A 175.1 175.1 100 366 266 24.1 

Plant 4 Inlet Run 1 100912.411-2A 112.3 112.3 100 333 233 16.1 

Plant 4 Inlet Run 2 1 00912.412 -2A 137.4 137.4 100 339 239 19.5 

Plant 4 Inlet Run 3 1 00912.413-2A 63.0 63.0 100 333 233 < 14.3 

Plant 4 Outlet Run 1 100912.401-2A 143.8 143.8 100 324 224 20.8 

Plant 4 Outlet Run 2 100912.402-2A 123.0 123.0 100 342 242 17.4 

Plant 4 Outlet Run 3 100912.403-2A 91.0 91.0 100 323 223 < 14.5 

Plant 5 Inlet Run 1 100912.511-2A 122.8 122.8 100 339 239 17.4 

Plant 5 Inlet Run 2 100912.512-2A 179.0 179.0 100 351 251 25.0 

Plant 5 Inlet Run 3 100912.513-2A 42.1 42.1 100 333 233 < 14.3 

Plant 5 Outlet Run 1 100912.501-2A 136.3 136.3 100 350 250 19.1 

Plant 5 Outlet Run 2 100912.502-2A 156.5 156.5 100 334 234 22.3 

Plant 5 Outlet Run 3 100912 .503-2A 162.4 162.4 100 329 229 23.3 

FRONT SPIKE 100912.SAI1-1S 5224.7 % REC = 100.7% 

BACK SPIKE 1 00912.411-2AS 3911.5 % REC = 76.0% 

FRONTDUP 1 00912.SAI2-1 D 320.7 RPD = N/A 

BACK DUP 100912.SAI2-2AD 156.6 RPD = N/A 

Page 37 of l 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 567 
BORAL BRICKS 

SELENIUM 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL~ 10 J.lg/l 

Proj. #: 100912 Postdig'n spike cone. = 100 J.Ig/l 

Date: 08-0ct-10 

Sample 10 Test Dig'te Dil'n Total Volume 

Client FAL sorn Cone FV Factor Volume Dig'd Total 

J.lg/l J.lg/l ml ml ml /.19 

FRONT HALVES 

Blank 100912.8-1 -0.8 -O.B 100 < 1.0 

Salisbury Inlet Run 1 1 00912.SAI1-1 12.8 12.8 100 1.3 

Salisbury Inlet Run 2 100912.SA12-1 15.3 15.3 100 1.5 

Salisbury Inlet Run 3 100912.SAI3-1 9.5 9.5 100 < 1.0 

Salisbury Outlet Run 1 100912.SA01-1 0.5 0.5 100 < 1.0 

Salisbury Outlet Run 2 1 00912.SA02-1 -1.2 -1.2 100 < 1.0 

Salisbury Outlet Run 3 l00912.SA03-1 0.5 0.5 100 < 1.0 

Plant 4 Inlet Run 1 100912.411-1 13.1 13.1 100 1.3 

Plant 4 Inlet Run 2 100912.412-1 5.2 5.2 100 < 1.0 

Plant 4 Inlet Run 3 100912.413-1 3.2 3.2 100 < 1.0 

Plant 4 Outlet Run 1 100912.401-1 -0.4 -0.4 100 < 1.0 

Plant 4 Outlet Run 2 100912.402-1 0.2 0.2 100 < 1.0 

Plant 4 Outlet Run 3 100912.403-1 0.2 0.2 100 < 1.0 

Plant 5 Inlet Run 1 100912.511-1 19.3 19.3 100 1.9 

Plant 5 Inlet Run 2 100912.512-1 44.3 44.3 100 4.4 

Plant 5 Inlet Run 3 100912.513-1 74.9 74.9 100 7.5 

Plant 5 Outlet Run 1 100912.501-1 2.0 2.0 100 < 1.0 

Plant 5 Outlet Run 2 100912.502-1 2.7 2.7 100 < 1.0 

Plant 5 Outlet Run 3 100912.503-1 5.1 5.1 100 < 1.0 

Page 38 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 568 
BORAL BRICKS 

SELENIUM 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 10 J.lg/L 

Proj. #: 100912 Postdig'n spike cone. = 100 J.lg/L 

Dale: 08-0ct-1 0 

Sample ID Test Dig'te Dil1

n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

J.lg/L J.lg/L ml ml ml J.l9 

BACK HALVES 

Blank 100912.B-2A -0.2 -0.2 100 1 116 66 < 1.8 

Salisbury Inlet Run 1 100912 .SA11-2A -0.2 -3.3 100 15 324 224 < 21.7 

Salisbury Inlet Run 2 100912.SAI2-2A 15.0 15.0 100 336 236 2.1 

Salisbury Inlet Run 3 1 00912.SA13-2A 7.3 7.3 100 356 256 < 1.4 

Salisbury Outlet Run 1 1 00912.SA01-2A 13.2 13.2 100 335 235 1.9 

Salisbury Outlet Run 2 l00912.SA02-2A 6.9 6.9 100 288 188 < 1.5 

Salisbury Outlet Run 3 100912.SA03-2A 1.7 1.7 100 366 266 < 1.4 

Plant 4 Inlet Run 1 100912.411-2A 9.8 9.8 100 333 233 < 1.4 

Plant 4 Inlet Run 2 100912.412-2A 17.2 17.2 100 339 239 2.4 

Plant 4 Inlet Run 3 1 00912. 413-2A 10.0 10.0 100 333 233 1.4 

Plant 4 Outlet Run 1 1 00912.401-2A 2.7 2.7 100 324 224 < 1.4 

Plant 4 Outlet Run 2 100912.402-2A -1 .4 -1.4 100 342 242 < 1.4 

Plant 4 Outlet Run 3 100912.403-2A -1.1 -1.1 100 323 223 < 1.4 

Plant 5 Inlet Run 1 100912.511-2A 24.3 24.3 100 339 239 3.4 

Plant 5 Inlet Run 2 1 00912.512-2A 10.7 10.7 100 351 251 1.5 

Plant 5 Inlet Run 3 1 00912.513-2A 9.7 9.7 100 333 233 < 1.4 

Plant 5 Outlet Run 1 100912.501-2A B.l 8.1 100 350 250 < 1.4 

Plant 5 Outlet Run 2 1 00912.502-2A 11.1 11.1 100 334 234 1.6 

Plant 5 Outlet Run 3 100912.503-2A 8.7 8.7 100 329 229 < 1.4 

FRONT SPIKE 100912.411-1 92.4 % REC = 79.2% 

BACK SPIKE 100912 .SAI1-2A 93.2 % REC = 93.2% 

Page 39 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 569 
BORAL BRICKS 

SILVER 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 pg/L 

Proj. #: 100912 Postdig'n spike cone. = 1000 pg/L 

Dale: 05-0cl-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

jJg/l pg/l ml ml ml jJg 

FRONT HALVES 

Blank 100912.8-1 0.1 0.1 100 < 0.5 

Salisbury Inlet Run 1 1 00912.SAI1-1 0.8 4.2 100 5 < 2.5 

Salisbury Inlet Run 2 1 00912.SAI2-1 0.9 0.9 100 < 0.5 

Salisbury Inlet Run 3 100912.SA13-1 0.7 0.7 100 < 0.5 

Salisbury Outlet Run 1 1 00912.SA01-1 0.1 0.1 100 < 0.5 

Salisbury Outlet Run 2 1 00912.SA02-1 -0.3 .o.3 100 < 0.5 

Salisbury Outlet Run 3 1 00912.SA03-1 -0.2 -0.2 100 < 0.5 

Plant 4 Inlet Run 1 100912.411-1 0.6 0.6 100 < 0.5 

Plant 4 Inlet Run 2 100912.412-1 0.0 0.0 100 < 0.5 

Plant 4 Inlet Run 3 100912.413-1 0.0 0.0 100 < 0.5 

Plant 4 Outlet Run 1 100912.401-1 0.8 0.8 100 < 0.5 

Plant 4 Outlet Run 2 100912.402-1 -0.2 -0.2 100 < 0.5 

Plant 4 Outlet Run 3 100912.403-1 0.1 0.1 100 < 0.5 

Plant 5 Inlet Run 1 100912.511-1 0.0 0.0 100 < 0.5 

Plant 5 Inlet Run 2 100912.512-1 -0.3 -0.3 100 < 0.5 

Plant 5 Inlet Run 3 100912.513-1 -0.2 -0.2 100 < 0.5 

Plant 5 Outlet Run 1 100912.501-1 -0.7 -0.7 100 < 0.5 

Plant 5 Outlet Run 2 100912.502-1 0.0 0.0 100 < 0.5 

Plant 5 Outlet Run 3 100912.503-1 -0.2 -0.2 100 < 0.5 

Page 40 of 1 03 

ATC PROJECT No. P·10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 570 
I 

BORAL BRICKS 

SILVER 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 llg/L 

Proj. #: 100912 Postdig'n spike cone. == 1000 119/L 

Date: 05-0ct-1 0 

Sample ID Test Dig'te Dil'n Total Volume 

Clienl FAL Sol'n Cone FV Factor Volume Dig'd Total 

Jlg/l Jlg/L ml ml ml Jig 

BACK HALVES 

Blank 100912.B-2A -0.5 -0.5 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SAI1-2A -0.1 -0.1 100 324 224 < 0.7 

Salisbury Inlet Run 2 l00912.SAI2-2A -0.4 -0.4 100 336 236 < 0.7 

Salisbury Inlet Run 3 100912.SA13-2A -0.1 -0.1 100 356 256 < 0.7 

Salisbury Outlet Run 1 1 00912.SAO 1 -2A -0.1 -0.1 100 335 235 < 0.7 

Salisbury Outlet Run 2 l00912.SA02-2A -0.1 -0.1 100 288 188 < 0.8 

Salisbury Outlet Run 3 100912.SA03-2A -0.1 -0.1 100 366 266 < 0.7 

Plant 4 Inlet Run 1 100912.41l-2A -0.3 -0.3 100 333 233 < 0.7 

Plant 4 Inlet Run 2 100912 .412-2A 0.0 0.0 100 339 239 < 0.7 

Plant 4 Inlet Run 3 100912.413-2A -0.6 -0.6 100 333 233 < 0.7 

Plant 4 Ouflet Run 1 100912.401-2A -0.4 -0.4 100 324 224 < 0.7 

Plant 4 Outlet Run 2 100912.402-2A -0.6 -0.6 100 342 242 < 0.7 

Plant 4 Outlet Run 3 100912.403-2A 0.0 0.0 100 323 223 < 0.7 

Plant 5 Inlet Run 1 100912.51l-2A -0.6 -0.6 100 339 239 < 0.7 

Plant 5 Inlet Run 2 100912.512-2A -0.6 -0.6 100 351 251 < 0.7 

Plant 5 Inlet Run 3 100912.513-2A 0.9 0.9 100 333 233 < 0.7 

Plant 5 Outlet Run 1 100912.50l-2A 0.2 0.2 100 350 250 < 0.7 

Plant 5 Outlet Run 2 1 00912.502 -2A -0.5 -0.5 100 334 234 < 0.7 

Plant 5 Outlet Run 3 1 00912.503-2A -0.7 -0.7 100 329 229 < 0.7 

FRONT SPIKE 100912.SAI1-1S 765.8 % REC = 76.6% 

BACK SPIKE 100912.411-2AS 794.1 % REC = 79.4% 

FRONT DUP 100912.SA12-10 0.7 RPD = N/A 

BACK DUP 100912.SAI2-2AD -0.1 RPD = N/A 

Page 41 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 571 
( 

BORAL BRICKS 

THALLIUM 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 Jlg(l 

Praj. #: 100912 Postdig'n spike cone. = 50 Jlg(l 

Date: 07-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Foetor Volume Dig'd Total 

Jlg(l Jlg(L ml ml ml Jlg 

FRONT HALVES 

Blank 100912.8-1 -0.2 -0.2 100 < 0.5 

Salisbury Inlet Run 1 100912.SAI1-1 4.7 4.7 100 < 0.5 

Salisbury Inlet Run 2 100912.SAI2-1 4.9 4.9 100 < 0.5 

Salisbury Inlet Run 3 100912.SAI3-1 4.5 4.5 100 < 0.5 

Salisbury Outlet Run 1 100912.SA01-1 -0.1 -0.1 100 < 0.5 

Salisbury Outlet Run 2 100912.SA02-1 -0.5 -0.5 100 < 0.5 

Salisbury Outlet Run 3 1 00912.SA03-1 0.0 0.0 100 < 0.5 

Plant 4 Inlet Run 1 100912.411-1 0.0 0.0 100 < 0.5 

Plant 4 Inlet Run 2 100912.412-1 0.1 0.1 100 < 0.5 

Plant 4 Inlet Run 3 100912.413-1 0.0 0.0 100 < 0.5 

Plant 4 Outlet Run 1 100912.401-1 -0.5 -0.5 100 < 0.5 

Plant 4 Outlet Run 2 100912.402-1 -0.3 -0.3 100 < 0.5 

Plant 4 Outlet Run 3 100912.403-1 -0.1 -0.1 100 < 0.5 

Plant 5 Inlet Run 1 100912.511-1 0.7 0.7 100 < 0.5 

Plant 5 Inlet Run 2 100912.512-1 0.4 0.4 100 < 0.5 

Plant 5 Inlet Run 3 100912.513-1 0.7 0.7 100 < 0.5 

Plant 5 Outlet Run 1 100912.501-1 -0.1 -0.1 100 < 0.5 

Plant 5 Outlet Run 2 100912.502-1 -0.3 -0.3 100 < 0.5 

Plant 5 Outlet Run 3 100912.503-1 -0.3 -0.3 100 < 0.5 

Page 42 of 1 OJ 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 572 
( 

BORAL BRICKS 

THALLIUM 

GFAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 5 fJg/L 

Proj. #: 100912 Postdig 1

n spike cone. = 50 fJ9/L 

Date: 07 -Oct-1 0 

Sample ID Test Dig'te Dil1

n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

!Jg/L fJg/L ml ml ml 1'9 

BACK HALVES 

Blank 100912.B-2A -0.7 -0.7 100 116 66 < 0.9 

Salisbury Inlet Run 1 1 00912.SA11-2A -0.6 -0.6 100 324 224 < 0.7 

Salisbury Inlet Run 2 100912.SAI2-2A -0.6 -0.6 100 336 236 < 0.7 

Salisbury Inlet Run 3 100912.SA13-2A -0.4 -0.4 100 356 256 < 0.7 

Salisbury Outlet Run 1 100912 SA01-2A -0.3 -0.3 100 335 235 < 0.7 

Salisbury Outlet Run 2 100912.SA02-2A -0.1 -0.1 100 288 188 < 0.8 

Salisbury Outlet Run 3 100912.SA03-2A 0.0 0.0 100 366 266 < 0.7 

Plant4 Inlet Run 1 100912.411-2A 0.1 0.1 100 333 233 < 0.7 

Plant 4 Inlet Run 2 100912.412-2A -0.2 -0.2 100 339 239 < 0.7 

Plan! 4 Inlet Run 3 100912.413-2A -0.2 -0.2 100 333 233 < 0.7 

Plant4 Outlet Run 1 100912.401-2A 0.0 0.0 100 324 224 < 0.7 

Plant 4 Outlet Run 2 100912.402-2A -0.5 -0.5 100 342 242 < 0.7 

Plant 4 Outlet Run 3 100912.403-2A -0.2 -0.2 100 323 223 < 0.7 

Plant 5 Inlet Run 1 100912.511-2A -0.1 -0.1 100 339 239 < 0.7 

Plant 5 Inlet Run 2 100912.512-2A -0.3 -0.3 100 351 251 < 0.7 

Plan! 5 Inlet Run 3 1 00912.513-2A 0.0 0.0 100 333 233 < 0.7 

Plan! 5 Outlet Run 1 100912.501-2A 0.0 0.0 100 350 250 < 0.7 

Plant 5 Outlet Run 2 100912.502-2A 0.0 0.0 100 334 234 < 0.7 

Plan! 5 Outlet Run 3 100912.503-2A -0.3 -0.3 100 329 229 < 0.7 

FRONT SPIKE 100912.411-1 51.1 % REC ~ 102.2% 

BACK SPIKE 1 0091 2 .411-2A 49.7 % REC ~ 99.4% 

Page 43 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 573 
BORAL BRICKS 

ZINC 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants1 Inc. MDL~ 5 pg/L 

Proj. #: 100912 Postdig•n spike cone. = 1000 pg/L 

Date: 05-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

pg/L pg/L ml ml mf pg 

FRONT HALVES 

Blank 100912.8-1 23.2 23.2 100 2.3 

Salisbury Inlet Run 1 100912.SAI1-1 242.3 242.3 100 24.2 

Salisbury Inlet Run 2 1 00912.SAI2·1 240.7 240.7 100 24.1 

Salisbury Inlet Run 3 100912.SAI3-1 219.3 219.3 100 21.9 

Salisbury Outlet Run 1 100912.SA01-1 29.8 29.8 100 3.0 

Salisbury Outlet Run 2 1 00912.SA02-1 29.9 29.9 100 3.0 

Salisbury Outlet Run 3 1 00912.SA03-1 43.1 43.1 100 4.3 

Plant 4 Inlet Run 1 100912.411-1 26.1 26.1 100 2.6 

Plant 4 Inlet Run 2 100912.412-1 23.8 23.8 100 2.4 

Plant 4 Inlet Run 3 100912.413-1 23.3 23.3 100 2.3 

Plant 4 Outlet Run 1 100912.401-1 28.5 28.5 100 2.8 

Plant 4 Outlet Run 2 100912.402-1 25.1 25.1 100 2.5 

Plant 4 Outlet Run 3 100912.403-1 24.5 24.5 100 2.5 

Plant 5 Inlet Run 1 100912.511-1 49.0 49.0 100 4.9 

Plant 5 Inlet Run 2 100912.512-1 41.3 41.3 100 4.1 

Plant 5 Inlet Run 3 100912.513-1 41.6 41.6 100 4.2 

Plant 5 Outlet Run 1 100912.501-1 39.5 39.5 100 4.0 

Plant 5 Outlet Run 2 100912.502-1 27.9 27.9 100 2.8 

Plant 5 Outlet Run 3 100912.503-1 23.9 23.9 100 2.4 

Page 44 of l 03 

ATC PROJECT No. P-1 0142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 574 
BORAL BRICKS 

ZINC 

ICP ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL~ 5 pg/L 

Proj. #: 100912 Postdig' n spike cone. = 1000 pg/L 

Dale: 05-0cl-1 0 

Sample ID Test Dig1

fe Dil'n Total Volume 

Client FAL SoPn Cane FV Factor Volume Dig'd Total 

pg/L pg/L ml ml ml /19 

BACK HALVES 

Blank 100912.B-2A 2.7 2.7 100 116 66 < 0.9 

Salisbury Inlet Run 1 100912.SAI1-2A 84.1 84.1 100 324 224 12.2 

Salisbury Inlet Run 2 100912.SAI2-2A 16.0 32.0 100 2 336 236 4.6 

Salisbury Inlet Run 3 100912.SAI3-2A 18.2 18.2 100 356 256 2.5 

Salisbury Outlet Run 1 1 00912.SA01-2A 13.8 13.8 100 335 235 2.0 

Salisbury Outlet Run 2 100912.SA02-2A 22.1 22.1 100 288 188 3.4 

Salisbury Outlet Run 3 1 00912.SA03-2A 18.3 18.3 100 366 266 2.5 

Plant 4 Inlet Run 1 100912.411-2A 23.3 23.3 100 333 233 3.3 

Plant 4 Inlet Run 2 100912 .412-2A 38.8 38.8 100 339 239 5.5 

Plant4 Inlet Run 3 100912.413-2A 29.5 29.5 100 333 233 4.2 

Plant 4 Outlet Run 1 100912.401-2A 39.0 39.0 100 324 224 5.6 

Plant 4 Outlet Run 2 100912.402-2A 15.1 15.1 100 342 242 2.1 

Plant 4 Outlet Run 3 100912.403-2A 48.3 48.3 100 323 223 7.0 

Plant 5 Inlet Run 1 1 00912.511-2A 23.6 23.6 100 339 239 3.3 

Plant 5 Inlet Run 2 100912.512-2A 16.8 16.8 100 351 251 2.3 

Plant 5 Inlet Run 3 100912.513-2A 21.4 21.4 100 333 233 3.1 

Plant 5 Outlet Run 1 100912.501-2A 35.0 35.0 100 350 250 4.9 

Plant 5 Outlet Run 2 100912.502-2A 42.2 42.2 100 334 234 6.0 

Plant 5 Outlet Run 3 100912.503-2A 44.2 44.2 100 329 229 6.3 

FRONT SPIKE 100912.SAI2-1 1122.3 % REC = 88.2% 

BACK SPIKE 100912.SA12-2A 930.5 % REC = 91.5% 

FRONT DUP 1 00912 .SAI3-1D 223.0 RPD = 1.7% 

BACK DUP 100912.SAI3-2AD 19.5 RPD = N/A 

Poge 45 of 1 03 

ATC PROJECT No. P-1 0142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & s. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 575 
( 

BORAL BRICKS 

MERCURY 

CVAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.20 jlg/L 

Proj. #: 100912 Postdig 1

n spike cone. === 5.00 119/L 

Date: 07-0ct-1 0 

Sample ID Test Dig1

te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

jlg/L jlg/L ml ml ml 119 

FRONT HALVES 

Blank 100912.8-1 -0.01 -0.01 100 100 5 < 0.40 

Salisbury-Inlet-Run 1 100912.SAI1-1 0.04 0.04 100 100 5 < 0.40 

Salisbury-Inlet-Run 2 100912.SA12-1 0.04 0.04 100 100 5 < 0.40 

Salisbury-Inlet-Run 3 100912.SA13-1 0.04 0.04 100 100 5 < 0.40 

Salisbury-Outlet-Run 1 100912.SA01·1 0.02 0.02 100 100 5 < 0.40 

Salisbury-Outlet-Run 2 100912.SA02-1 0.02 0.02 100 100 5 < 0.40 

Salisbury-Outlet-Run 3 100912.SA03-1 0.02 0.02 100 100 5 < 0.40 

Plant 4-lnlet-Run 1 100912.411-1 0.03 0.03 100 100 5 < 0.40 

Plant 4-lnlet-Run 2 100912.412-1 -0.01 -0.01 100 1 100 5 < 0.40 

Plant 4-lnlet-Run 3 100912.413-1 0.02 0.02 100 1 100 5 < 0.40 

Plant 4-0utlet-Run 1 100912.401-1 -0.01 -0.01 100 100 5 < 0.40 

Plant 4-0utlet-Run 2 100912.402-1 0.03 0.03 100 100 5 < 0.40 

Plant 4-0utlet-Run 3 100912.403-1 0.02 0.02 100 100 5 < 0.40 

Plant 5-lnlet-Run 1 100912.511-1 0.04 0.04 100 100 5 < 0.40 

Plant 5-lnlet-Run 2 100912.512-1 0.07 0.07 100 100 5 < 0.40 

Plant 5-lnlet-Run 3 100912.513-1 0.02 0.02 100 100 5 < 0.40 

Plant 5-0utlet-Run 1 100912.501-1 0.02 0.02 100 100 5 < 0.40 

Plant 5-0utlet-Run 2 100912.502-1 -0.01 -0.01 100 100 5 < 0.40 

Plant 5-0utlet-Run 3 100912.503-1 0.00 0.00 100 100 5 < 0.40 

Page 46 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 576 
BORAL BRICKS 

MERCURY 

CVAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.20 Jig/L 

Proj. #: 100912 Postdig'n spike cone. = 5.00 Jig/L 

Date: 07 -Oct-1 0 

Sample ID Test Dig'fe Dil'n Total Volume 

Client FAL Sol'n Cone FV Fador Volume Dig'd Total 

Jlg/l Jlg/L ml ml ml Jig 

FRACTIONS 26 

Blank 1 00912.B-2B 0.00 0.00 100 1 116 5 < 0.46 

Salisbury-Inlet-Run 1 100912.SAI1-2B 0.16 0.16 100 1 324 5 < 1.30 

Salisbury-Inlet-Run 2 100912.SAJ2-2B 0.78 0.78 100 336 5 5.21 

Salisbury-Inlet-Run 3 1 00912.SA13-2B 0.53 0.53 100 356 5 3.77 

Salisbury-Outlet-Run 1 100912.SAO 1-28 0.09 0.09 100 335 5 < 1.34 

Salisbury-Outlet-Run 2 1 00912.SA02 -2B 0.12 0.12 100 288 5 < 1.15 

Salisbury-Outlet-Run 3 100912.SA03-2B 0.08 0.08 100 366 5 < 1.46 

Plant 4-lnlet-Run 1 1 00912.411-2B 0.28 0.28 100 333 5 1.86 

Plant 4-lnlet-Run 2 100912.412-2B 0.24 0.24 100 339 5 1.59 

Plant 4-lnlet-Run 3 100912.413-28 0.18 0.18 100 333 5 < 1.33 

Plant 4-0utlet-Run 1 100912.401-28 0.36 0.36 100 324 5 2.30 

Plant 4-0utlet-Run 2 100912.402-2B 0.48 0.48 100 342 5 3.25 

Plant 4-0utlet-Run 3 100912.403-28 0.40 0.40 100 323 5 2.55 

Plant 5-lnlet-Run 1 100912.511-28 0.42 0.42 100 339 5 2.85 

Plant 5-lnlet-Run 2 100912.512-28 0.32 0.32 100 351 5 2.25 

Plant 5-lnlet-Run 3 100912.513-2B 0.16 0.16 100 333 5 < 1.33 

Plant 5-0utlet-Run 1 100912.501-28 O.B2 0.82 100 350 5 5.71 

Plant 5-0utlet-Run 2 1 00912.502-2B 0.77 0.77 100 334 5 5.11 

Plant 5-0utlet-Run 3 100912.503-28 0.79 0.79 100 329 5 5.20 

BACK SPIKE Sal. Inlet 100912.SAI1-2BS 5.06 % REC = 101.2% 

BACK SPIKE Sal. Outlet 100912.SA01-2B~ 5.01 %REC=100.1% 

BACK SPIKE-Plant 4 In 100912.411-2BS 5.26 % REC = 99.6% 

BACK SPIKE-Plant 4 Out 100912.401-28S 5.27 % REC = 98.3% 

BACK SPIKE-Plant 5 In 100912.5tl-2BS 5.59 % REC = 103.3% 

BACK SPIKE-Plant 5 Out 100912.501-2BS 5.96 % REC = 102.8% 

Page 47 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 577 
BORAL BRICKS 

MERCURY 

CVAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.20 Jlg/l 

Proj. #: 100912 

Date: 07-0ct-1 0 

Sample ID 

Client 

FRACTIONS 3A 

Blank 

Salisbury-Inlet-Run 1 

Salisbury-Inlet-Run 2 

Salisbury-Inlet-Run 3 

Salisbury-Outlet-Run 1 

Salisbury-Outlet-Run 2 

Salisbury-Outlet-Run 3 

Plant 4-lnlet-Run 1 

Plant 4-lnlet-Run 2 

Plant 4-lnlet-Run 3 

Plant 4-0utlet-Run 1 

Plant 4-0utlet-Run 2 

Plant 4-0utlet-Run 3 

Plant 5-lnlet-Run 1 

Plant 5-lnlet-Run 2 

Plant 5-lnlet-Run 3 

Plant 5-0utlet-Run 1 

Plant 5-0utlet-Run 2 

Plant 5-0utlet-Run 3 

ATC PROJECT No. P-10142 

Postdig'n spike cone. = 5.00 Jlg/l 

Test Dig'te Dil'n Total Volume 

FAL Sol'n Cone FV Factor Volume 

Jlg/L Jlg/l ml 

1 00912.8-3A -0.01 -0.01 100 

100912.SAI1-3A 0.05 0.05 100 

100912.SA12-3A 0.04 0.04 100 

100912.SA13-3A 0.02 0.02 100 

l00912.SA01-3A 0.02 0.02 100 

1 00912.SA02-3A -0.02 -0.02 100 

100912.SA03-3A -0.03 -0.03 100 

100912.411-3A 0.08 0.08 100 

100912.412-3A 0.08 0.08 100 

1 00912.413-3A 0.08 0.08 100 

100912.401-3A 0.01 0.01 100 

100912.402-3A -0.01 -0.01 100 

1 00912.403-3A 0.02 0.02 100 

1 00912.511-3A 0.04 0.04 100 

100912.512-3A 0.07 0.07 100 

100912.513-3A 0.09 0.09 100 

100912.501-JA 0.01 0.01 100 

1 00912.502-3A 0.00 0.00 100 

1 00912.503-3A -0.01 -0.01 100 

Page 48 of 1 03 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

ml 

33 

124 

111 

153 

119 

123 

146 

118 

113 

112 

110 

11 5 

114 

107 

121 

115 

121 

108 

110 

Dig'd Total 

ml /19 

10 < 0.07 

10 < 0.25 

10 < 0.22 

10 < 0.31 

10 < 0.24 

10 < 0.25 

10 < 0.29 

10 < 0.24 

10 < 0.23 

10 < 0.22 

10 < 0.22 

10 < 0.23 

10 < 0.23 

10 < 0.21 

10 < 0.24 

10 < 0.23 

10 < 0.24 

10 < 0.22 

10 < 0.22 

APPENDIX PAGE No. 578 
BORAL BRICKS 

MERCURY 

CVAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.20 J.lg/l 

Proj. #: 100912 Postdig1

n spike cone. :::::: 5.00 J.lg/l 

Dale: 07-0ct- 10 

Sample ID Test Dig'le Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

J.lg/L J.lg/L ml ml ml J.l9 

FRACTIONS 3B 

Blank 100912.B-3B 0.01 0.01 100 87 20 < 0.09 

Salisbury-Inlet-Run 1 100912.SAI1-3B 0.04 0.04 100 386 20 < 0.39 

Salisbury-Inlet-Run 2 100912.SAI2-38 0.05 0.05 100 388 20 < 0.39 

Salisbury-Inlet-Run 3 100912.SA13-38 0.03 0.03 100 387 20 < 0.39 

Salisbury-Outlet-Run 1 100912.SA01-3B 0.04 0.04 100 408 20 < 0.41 

Salisbury-Outlet-Run 2 100912.SA02-3B 0.03 0.03 100 389 20 < 0.39 

Salisbury-Outlet-Run 3 100912.SA03-38 0.03 0.03 100 405 20 < 0.41 

Plant 4-lnlet-Run 1 100912.411-38 0.01 0.01 100 395 20 < 0.40 

Plant 4-lnlet-Run 2 100912.412-38 O.Ql 0.01 100 390 20 < 0.39 

Plant 4-lnlet-Run 3 100912.413-38 0.05 0.05 100 400 20 < 0.40 

Plant 4-0utlet-Run 1 100912.401 -3B 0.36 0.36 100 405 20 0.73 

Plant 4-0utlet-Run 2 100912.402-38 0.37 0.37 100 388 20 0.71 

Plant 4-0utlet-Run 3 100912.403-38 0.28 0.28 100 399 20 0.56 

Plant 5-lnlet-Run 1 100912.511-38 0.41 0.41 100 406 20 0.83 

Plant 5-lnlet-Run 2 100912.512-38 0.50 0.50 100 421 20 1.05 

Plant 5-lnlei-Run 3 100912.513-38 0.48 0.48 100 438 20 1.05 

Plant 5-0utlei-Run 1 100912.501-38 0.03 0.03 100 389 20 < 0.39 

Plant 5-0utlet-Run 2 100912.502-38 -0.02 -0.02 100 400 20 < 0.40 

Plant 5-0utlet-Run 3 100912.503-38 -0.02 -0.02 100 373 20 < 0.37 

Page 49 of 103 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 579 
( 

BORAL BRICKS 

MERCURY 

CVAA ANALYSIS RUN SUMMARY AND CALCULATION WORKSHEET 

Client: Analytical Testing Consultants, Inc. MDL= 0.20 pg/L 

Proj. #: 100912 Postdig'n spike cone. == 5.00 pg/L 

Date: 07-0ct-10 

Sample ID Test Dig'te Dil'n Total Volume 

Client FAL Sol'n Cone FV Factor Volume Dig'd Total 

pg/L pg/L ml ml ml Jlg 

FRACTIONS 3C 

Blank 100912.B-3C 0.01 0.01 100 107 5 < 0.43 

Salisbury-Inlet-Run 1 100912.SAI1-3C 0.83 0.83 100 255 5 4.21 

Salisbury-Inlet-Run 2 100912.SAI2-3C 1.45 1.45 100 249 5 7.20 

Salisbury-Inlet-Run 3 100912.SAJ3-3C 1.02 1.02 100 250 5 5.10 

Salisbury-Outlet-Run 1 100912.SA01-3C 0.02 0.02 100 272 5 < 1.09 

Salisbury-Outlet-Run 2 100912.SA02-3C -0.01 -0.01 100 250 5 < 1.00 

Salisbury-Outlet-Run 3 100912 .SA03-3C -0.01 -0.01 100 246 5 < 0.98 

Planl4-lnlet-Run 1 100912.411-3C 0.35 0.35 100 150 5 1.04 

Plant 4-lnlet-Run 2 1 00912.412-3C 0.15 0.15 100 263 5 < 1.05 

Plant 4-lnlet-Run 3 100912.413-3C 0.04 0.04 100 264 5 < 1.06 

Plant 4-0utlet-Run 1 100912.401-3C 0.24 0.24 100 258 5 1.24 

Plant 4-0utlet-Run 2 100912.402-3C 0.03 0.03 100 273 5 < 1.09 

Plant 4-0utlet-Run 3 100912.403-3C 0.09 0.09 100 259 5 < 1.04 

Plant 5-lnlet-Run 1 1 00912.511-3C 0.15 0.15 100 25B 5 < 1.03 

Plant 5-lnlet-Run 2 100912 .512-3C 0.19 0.19 100 253 5 < 1.01 

Plant 5-lnlet-Run 3 100912.513-3C 0.10 0.10 100 232 5 < 0.93 

Plant 5-0utlet-Run 1 100912.501-3C 0.21 0.21 100 246 5 1.03 

Plant 5-0utlet-Run 2 100912.502-3C 0.21 0.21 100 248 5 1.04 

Plant 5-0utlet-Run 3 100912.503-3C 0.24 0.24 100 243 5 1.17 

Page 50 of 1 03 

ATC PROJECT No. P·10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 580 
BORAL BRICKS 

MERCURY 

QUALITY CONTROL DATA 

Client: Analytical Testing Consultants, Inc. 

Proj. #: 100912 

Dote: 07-0ct-1 0 

Calibration Data Run 1 Run 2 

True 

cone. 

/1~/l Abs. Abs. 

Blank 0.00 0.000 0.000 

Standard 1 0.50 0.016 0.013 

Standard 2 1.00 0.034 0.026 

Standard 3 2.00 0.060 0.052 

Standard 4 5.00 0.151 0.125 

Standard 5 10.00 0.300 0.248 

Calibration Verifications Run 1 Run 2 

ATC PROJECT No. P-10142 

ICV = 5 4.99 4.99 

ICB = 0 -0.02 -0.02 

CCV1 = 5 5.13 5.13 

CCB1 = 0 0.04 0.04 

CCV2 = 5 4.87 4.87 

CCB2 = 0 -0.03 -0.03 

CCV3 = 5 5.03 5.03 

CCB3 = 0 0.00 0.00 

CCV4 = 5 4.93 4.93 

CCB4 = 0 0.04 0.04 

CCV5 = 5 5.00 5.00 

CCB5 = 0 0.01 0.01 

CCV6 = 5 5.19 5.19 

CCB6 = 0 0.06 0.06 

CCV?= 5 5.05 5.05 

CCB7 = 0 0.03 0.03 

Page 51 ofl03 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Run 3 

Abs. 

0.000 

0.014 

0.027 

0.054 

0.135 

0.265 

Run 3 

5.03 

0.01 

5.20 

0.03 

APPENDIX PAGE No. 581 
BORAL BRICKS 

MERCURY 

QUALITY CONTROL DATA 

Client: Analytical Testing Consultants, Inc. 

Proj. #: 100912 

Date: 07 -Oct-1 0 

Calibration Verifications Run 1 Run 2 

ATC PROJECT No. P-1 0142 

CCV8 = 5 4.88 

CCB8 = 0 -0.01 

CCV9 = 5 5.17 

CCB9 = 0 -0.03 

CCV10=5 5.06 

CCB10 = 0 0.03 

CCVll = 5 5.19 

CCB11 = 0 0.04 

Page 52 of 1 03 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

Run 3 

APPENDIX PAGE No. 582 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free~B00)-733-3193 

CHAIN OF CUSTODY RECORD Projoot No p -10124 

M~±=-~ ':0, ' .~ '~ f8 (,.') vosr" 

~:~:~ Run #1-M-3 

Run#2-M-3 

Run#3-M·3 

Run#1-M-4 

Run #2-M-4 

Run #3-M-4 

Run #1-1 ~ 

Run I 

Run #1-M-58 

I"' : . •n 

/Run#~" " 0 

I Run 

/Run~~ •• ~~ 

/Run'""., .. 

·SA-M 

·BB-M 

rt ·9-M 

·10-M 

'"' i ·11-M 

i ·12-M 

iv{{f l..J..-..-

NOTE: 

s.1s.1o CFA FILTeR Fmo<.d """"' Filte< 

' ' CFA FILTER Exoosed aua<tt Filte< 

: GFA iii.Tffi Exoosed' Quartz Fmer 

: CFA ·tOOml ·~;H>~<i , FH Rln><> 

CFA ·100mL 0. f HNO, FH Rln>a 

': CFA -=10cJmL 0.1 HNO, FH Rinse 

••••••••• CFA Calc~:~mL Imp_ I&:! C&R 5%/10% 

······'·.··· 

CFA catch"" 100 ml Rin~ !mo. t&Z C&R 5%110% 

' CFA CatcllR7n~.;l· >mo. t<?NO "'"'"~ 

CFA 100 ml Imp. lCOR;;, 1 

·:.··, CFA 10omL Imp. l C&R w1 100"' HNO, 

.· ·' CFA 1®mL Imp. l C&R w/100ml HNO, 

I catCh + 100 mL 

Rinse KMN04 + 

CFA 100~~~~H20 lmo. ••• 1 ,Rinse 

:· .. ·· Catch + 1 00 ml 

I < 

Rins;a KMN04 + 

CFA 1CO~n~H20 lmo. <&5 C&R KMo<'>. Rl• 

····· 

Catch+ 100 ml 

I · ... :. RJnse KMN04 + 

·: .. CFA 10~ '!H20 !mo. '"' C&R KMnO, Rln"' 

·, CFA !20o:~ ~Nil~/ 25 8N HCI . . .. : 

CFA /zoo'!L~NH~ • zo aN HCI "" 

' CFA f2o0m'li!: ~;:, SN HCI rime ollmp, 4&5 

·.··. CFA Allauol of Lot 0 f HN0 B~nk 

· ...... · CFA ~of Lot Ot WM« Blaok 

' CFA Aliquot or Lot : """' CFA Atiouot or Lol KMno,Btonk 

CFA Ali~.;.~ BN HCI Blank 

CFA -Atlquoi;;iw ·a.. • .u~a""' 

cd-'l.rf /•.1: ~f) ~ g.&J./t h t <) 1"') 

I :)l.l h<~ 

::!' 

Please Malyz.e for .standard metals list (Brick MACT ICR Emissions Testing) 01nd HG. 

Any questions. contact Bin Kissel (704) 241~0~15. cell 

PLE-'SE MARK UOUlO LEvEL ON AlllSAMPLE BOTTLES WITH GREASE PENCIL. 

SEAL nGHTL Y ft,N(l RE-CHECK UPON OEUVEAY TO l..AB PERSONNEL 

BK 

! 

c,&o.ol!CRICOC\IM2IICOCV'I~Un~·M211 Ver\.0 29Augu5\:/!00~ 

'r fi~ rn\SSi~: c\tut\: J.id.A,'t ~ lmaMs.~.Ahe<1 ~ ..ftl M<lLtR-taf parllt>-~.la:!e. m~. 1"he.y·~1 SU1cl 

c, tiJ.W-t-o..~ tJ~e.M o{-I\Q.IC{" wuU pw~"!}¥P'fo3k dl'fr/z.l/}16 J./:oaPM 

ATC PROJECT No. P-1 0142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 583 
BORAL BRICKS 

ANALYTICAL TESTING CONSULTANTS, INC. 

Toll Free-(800)·733·3193 

CHAIN OF CUSTODY RECORD Proj•ct No P-10124 

ltEQU£tTEn PARMIETB!.S 

cuan' Brm!lt Bri'*s !omlt>O 1'1-lU~ ~~ 

.......,.lh<IIL<:)CA"l!ON; 

PUWTlOC"ATIOPh Augull3, 

P1anl:4, 

A 11 " " ' ;, :a~ '" , .. VOST OTHER 

8AA'~Pl.EC: 

Run #1-M-1 

Run #2-M-1 

Run 113-M-1 

Run #1-M-3 

Run#2-M-3 

Run #3-M-3 

Run #1-M-4 

Run #2-M-4 

Run #3-M-4 

Run #1-M-SA 

Run 112-M·SA 

Run #3-M-SA 

Run#1-M-5B 

Run#2-M-5B 

Run #3'M·5B 

Run #1-M-SC 

Run 112-M-5C 

Run #3-M-SC 

I 

RfUNOUI&>Etl BY 

1..-Jtf' 

R ><DOY 

I FIEUJ REMARKS: 

NOTE: 

oAT£ """ ""'"""" _.,.,. ftiUQIIIfLftlU CONfAWER CONTENTll 

9.H.18 CFA FILTER E:q)osed Quartz Filter 

' CFA FILTER 'Exposed Quartz Filter 

! CFA FILTER Exposed Quartz Filter 

' : CFA -100 ml 0.1 H~ FH Rln9e 

' ... i CFA -100 ml 0.1 HNO~ FH Rinse 

' CFA ' -100ml 0.1 HNO:J FH Rln:IS 

i Catch + 100 ml 

! CFA Rinse Imp. 1&.2 C&R 5%/10% 

i Catch+ 100ml 

CFA Rinse Imp, 1&2 C&R 5%{10% 

I Catch+- 100 ml 

' CFA Rinse !mp. 1&2 C&R 5%f101

A:. 

' CFA 100mL Imp. 3 C.&R w/100m1 HNO,. 

i CFA 100 ml Imp. 3 C&R wl 100ml HN.03 

' CFA I100mL Imp_ 3 C&R wl 100m! HNO.!I 

Catch.- tOO ml 

I Rinse KMN04 + 

·. 1DOmL D1 H20 

CFA Rinse Imp . .4&5 C&R KMnO< RinSil: 

I Catch+- 100 ml 

Rinse KMN04 +-

I 100mL 01 H20 

l CFA R!r..se Imp . .4&5 C&R ~o. Rinse 

! Galch +- 100 ml 

Rinse KMN04 + 

i 100mLOI H20 .·. CFA RIT1$a lmp. 4&5 C&R ~0~ Rin~ 

i .· .. · 200ml. Dl H20 + 25 

i CFA ml8NHCI eN HOI rinse ot Imp. 4&5 

' 200ml 01 H20 to 25 i CFA ml8NHCJ eN HCI rinse Of /mJ). 4&5 

• 200ml Dl H20 + 25 

CFA ml.SNHCI 8N HCI rinse or Jrnp. 4&5 

''"" '""' Fii;C!!M!.Dfl'f DAn "'' ,u.,.,~ /to:.-1~9 'YftA/to l ci' <') 

""' """ ltECe.JE08V OA.TE ..... ..Ail:t h1scli'Jl:1'1 ho i CFA: CLEJ>.N FlELO AAi!f;_J 

Please analyze for standard metals list (Brtck MACT ICR EmissiOns TesUng) and HG. 

Any QUestions contact am Kissel {704) 241-0315 ·cell 

PltASE MARK UQUIO lEVEL 00 All SAMPLE AOTTL~S WITH GREASE' PENCll. 

SEAL TlGHTI. v AND RE-CHt:CK UPON. OEUVERY TO LAB PERSONNEl. 

Poge 54 of 1 03 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

~ 

BK 

i 

! 

' 

' 

j 

i 

i 

! 

' 

! 

' 

' ' 

' 

I 

: 

i 

! 

' L 

! 

I 

I 

·• 

Var 1.0 29 AU!!Us!: 20!l'l 

APPENDIX PAGE No. 584 
i 

BORAL BRICKS 

ATC EQUIPMENT CALIBRATIONS 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 634 
BORAL BRICKS 

GLASS NOZZLE CALIBRATION DATA FORM 

Re<i: Box 1 

PR!MARY DATE: 

CALIBRATED BY: 

SERIES: 

12/3012009 Black: Box 2 

Mallory P. Beam lnllials 11\() \? B 

20, 30, 40, 50, 60, 70, 80, 90, 100, 110, 120,130 Glass Sehes, Quartz Nozzles 

ATC Fonn i49 R Primary Nozzle Calibration Record 

version 1.0 January 2006 

F:\Work.V\11 FormsRFiefd Data Sheets, Calc Formulae ... 

'\149-Prlmary Nozzle Calibration Record.xls 

ATC (BOO) 733·3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 635 
PRIMARY DATE 

CALIBRATED BY: 

SERIES: 

BORAL BRICKS 

GLASS NOZZLE CALIBRATION DATA FORM 

Red: Box 1 

12/30/2009 Black: Box 2 

Mallory P. Beam Initials ro p l; 

20, 30, 40, 50, 60, 70, 80, 90, 100, 110, 120,130 Glass Series, QuartZ Nozzles 

ATC Fonn 149 ·Primary Nozzle Calibration Record 

version 1.0 January 2006 

F:\Work\AII Forms~Field Data Sheets, Calc Formulae ... 

\149-Prtmary Nozzle Calibration Recor:d.xls 

ATC (800) 733-.3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 636 
BORAL BRICKS 

GLASS NOZZLE CALIBRATION DATA FORM 

Red: Box 1 

PRIMARY DATE: 12/3012009 Black: Box 2 

CALIBRATED BY: Mallory P. Beam Initials yvy(J (3 

SERIES: 20, 30, 40, 50, 60, 70, 80, 90, 100, 110, 120,130 Glass Series, Quartz Nozzles 

NOTE· Nozzles are a ranged from smallest to gteatest average diametet 

27 MISSING MISSING MISSING #VALUE! 

28 MISSING MISSING MISSING #VALUE! 

29 MISSING MISSING MISSING #VALUE! 

30 MISSING MISSING MISSING #VALUE! 

31 MISSING MISSING MISSING #VALUE! 

33 BROKEN BROKEN BROKEN #VALUE! 

58 MISSING MISSING MISSING #VALUE! 

84 MISSING MISSING MISSING #VALUE I 

85 MISSING MISSING MISSING #VALUE! 

86 MISSING MISSING MISSING #VALUE! 

94 MISSING MISSING MISSING #VALUE! 

95 MISSING MISSING MISSING #VALUE! 

98 MISSING MISSING MISSING #VALUE! 

101 MISSING MISSING MISSING #VALUE! 

120 MISSING MISSING MISSING #VALUE! 

121 MISSING MISSING MISSING #VALUE! 

122 MISSING MISSING MISSING #VALUE! 

124 BROKEN BROKEN BROKEN #VALUE! 

125 MISSING MISSING MISSING #VALUE! 

130 MISSING MISSING MISSING #VALUE! 

0.000 

where. 

·~ Three different nozzle diameters; Each diameter must be within 0.001 inches 

...... = Maximum difference between any two diam'?ters must be less than or equal to 0.004 inches 

"'*"'::::Average of three diameters 

0.193 

0.167 

0.198 

0.211 

0.212 

0.219 

0.281 

0.346 

0.347 

0.343 

0.373 

0.379 

0.387 

0.409 

0.495 

0.497 

0.499 

0.503 

0.502 

1.023 

0.000 

ATC Form 149. Primary Nozzle Calibration Record 

version 1.0 January 2006 

F:\Wor1<\Ait Forms-Field Data Sheets, Calc Formulae .. , 

\149-Prlmary Nozzle Calibration Record.xis 

ATC (800) 733-3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 637 
BORAL BRICKS 

NOZZLE CALIBRATION DATA FORM 

Red: Box 1 

DATE: 2/24/2009 Black: Box 2 --=::...:.:.;::.:..:..::___ 

CALIBRATED BY: 

ATC Form 149- Primary Nozzle Calibration Record 

version 1.0 January 2006 

F:\Work\AII Forms-Field Data Sheets, Calc Formulae ... 

\149-Primary Nozzle Calibration Record.xls 

ATC (800) 733~3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PlANTS 4 & 5, SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 638 
( 

BORAL BRICKS 

NOZZLE CALIBRATION DATA FORM 

Red: Box 1 

DATE 2/2412009 Black: Box 2 

CALIBRATED BY: Mallory Beam Initials: 'J/t7Yi1 ___ _ All 

where: 

·=Three different nozzle diameters; Each diameter must be within 0.001 inches 

**=Maximum difference between any two diameters must be less than or equal to 0.005 inches 

***;:; Average of three diameters 

ATC Form 149- Primary Nozzle Calibration Record 

version 1.0 January 2006 

F:\Work\AII Forms-Field Data Sheets, Calc Formulae ... 

\149-Primary Nozzle Calibration Record.xls 

ATC (BOO) 733-3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 639 
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degre~ lndicEted !eve! positit.m for detennining !l1 and B2• 

Degr~e indicating ieve.l position for 

~'lclerminiug cf0. 

., .l. 

h.:o::C~Tc)!~,---

• 

D~grc~:s iadicating level position tOr dcten11ining y then C{llculate 

z. 

-- -----~--

Level mtd Perpendicular? .Y 

Obstruction? ;V 

Damaged? /1/ -----

a, (-Ill' :S a1.:S+10') -- 2" 

a2 (-111' :S a2.:S+llf') -, 

,;- "' ---- ·--·--

p, (-5'' :s fl, :s +5") /,j 

[J, (-5' .:s p, .:s +50) ;o -

r 0 

e () -- Z=A tan7 (< 0.125'') 0 

W=A tan e (_:50.03115'? 0 - ··--·-- f--

D,(J/16" :SD, :5: 318'') eJ '57S --f--· 

A I-I)· il"f s ------------- A12D,(l.OS ::;P ,.ID, ::;J.50) /. f<i3 ·--------~- ----=--

![temperature sensor isjlus!t. wit!t Y ~~tube Of!_enin!JJ is Z >'!. "? ~n---- ![temperature seusor is set back from. Jt./ 

oitot tt1be ooettitlf!, is W> 2"? i 

IsX::,:~''forDn=~" )!__ 

Is impact side o[pitot tuba ew.m witlc f-- or abo~'C noule eutrv nlane? 

Is Y;:: J"for 3116'' <Dt < 318"? QAIQC Check '---· -·-'-----~ / 

Completeness i..,...../ Legibility f.../'Accuracy _ ____.. Specificatjons Reasonableness ---· 

Certification 

I certify that the Type S pilot tube/probe ID # _ 50 meets or exceeds ali 

specifications_, criteria and/or applicable design features and is hereby assigned a pilot ttl be calibration factor CP of 

0.84 1• • . . .· • 

Ce11ified . by :;tJ'&_wvtzu - jJ~2S-01 !!.,.f(/1~._, ~ -~- iZ-'&-~-:.<:<1 redand (Signature/Date) Team Leader (Signature/Date) 

1 This certification also applies to the specifications of EPA Method 2, section 10.1.4.1. l regaiding inter-component 

spacing of pitot tube-sampling probe assemblies. Refer to the figures on the reverse side of this page for spcciflcs. 

ATC Form 37·PI·imary S-typc Pito\ Tube Calibrations-version 3.0 September 2007 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC@ (800) 733-3193 

APPENDIX PAGE No. 640 
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Reference Source2 Reference Thermocouple T

Point (Specify) Temperature Potentiometer D

Number OF Temperature, °F (calculate 

1 Ambient Air Jd/;· &:3~"' 0 -

2 Ice Bath 3 Thelco Oven 1 Reference thermometer .. mercury in glass 

2Type of calibration system used 

cf D/Jt 

~oe:,:: 

4 z. (: D. 

3CJft>~F 

o, 

{3, ~

'=[(Ref Temp, C+273) ·Test Temp., C + 273)/Ref Temp, C + 273]*100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QC Check 

Completeness /~egibility /Accuracy /specifications~easonableness 

Checked by: flcZt4.<.~ 1/·c-s -d! 

Galibra.tion Technician 

(Signature/Date) 

ATC Form 209vPrimary Them1ocouple Calibration Record 

version 2.1 May 2009 

[;J ,1{,.;.&!._ fb 11

Test Team Leader 

(Signature/Date) 

F:\Work\AII Fonns~ .. \2090-Prlmary thermocouple 

ATC (8
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degree: indicating levd posttion for dcterntin iug llt and a1. 

Degree i11dicating level p.osition for 

detcrmining of G. 

:r>~ 

r::-: :-:~~:ct,::-')'-.-.--

Degrees indicating le"vcl position for determining y then calculate. 

z 

-- ------------,--------

Level v aJJd Perpeudicular? / 

---------------i-<------1 

1-0_b_s_tr_u_ct_io_n __ ? ________________ +-- Af __ 

Damaged? -------------- N __ a 1 (-10':; al:;+IO'j 6 ~--------------------~---~--

a, (-10':5;a,:S+10') A iJ___ __ 

fl!J. 

:L _________________ ----t---'t.L)_-1 

e 1 o 

Z=A tan r (< 0.125") 0 

W=A tan e (:S 0.03125") I D ~- ------------~~----1 

D,(3/16";:;D, :;318'? 0.) 75 ~-----------------------~~----1 

(}. 9'f() 

AI2D, (1.05 :5; P ,11), :S 1.50) 1- 153 

If temperature sensor is jlus/t with y 

oitot tube openiJzg, is Z ~---4--L----~ 

lftemperattll'e sem;or is set back from 

I nftot tube oveuinf!, is W> 2"? __ _Jjj ___ _ 

. IsX~.J.4"forDn=~" ~ 

- Tshnpact side of pilot tube even wi±th - ys or above flOZ?;.le entl')!_.£1ane? __ , ..:-

Is ~3 '[or3116''<Dt<3/8·''? ;! __ QA!QC Check / 

Completeness ._-;',.... Legibility .,.....,.......7\ccmacy _..-- Speclficauons Reasonableness 

Cert!ficatioTt 

I certify that the Type S pitot h1belprobe ID # ------~5.LJ} _________ _ meets or exceeds all 

specifications, criteria a11d/or applicable design features and is hereby assigned a pitot tube calibration fJ.ctor Cp of 

os4' •. · /'j .' D _ , . ~ . · ·. /1 / ';.1 

Certifted by: ce-e..1 f)i..U.t{g!./)._, /f----s -() 1 ~~-'</( V<'__k,e_._,__--. i 2 -8-oq 

Persbfmel {Sign&rureiD::ue) · Tea~ Lc~der {Signature/Date) 

1 This cettification also applies to tht specifications of EPA Method 2. section 1 0.1.4.1.1 regarding inter-component 

spacing of pi tot tube-sampling probe assemblies. Refer to the figure.s on the reverse side of this page for specifics. 

ATC Form 37-f>rim::ll)' S-typc Pi tot Tube Ca1ibratie>l1S-ver\lion 3.0 September 2~07 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC@ (800) 733-3193 

APPENDIX PAGE No. 642 
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Calibration Date I I· zs·- 0 q 

Ambient Temp., 'F _:r:...r., 6'/<Y ____ _ 

Technician d 

., ...... '-!' X::."'-• 

Reference Source 2 

Point (Specify) 

Number 

1 Ambient Air 

2 Ice Bath 

3 Thelco Oven 

1 Reference thermometer-mercury in glass 

'Type of calibration system used 

Thermocouple Number 51 

Barometric Pressure, inches Hg ;zq i 5" 

Reference Thermometer (Lis!ID #)1 1"7, F5, r

Reference Thermocouple T

Temperature Potentiometer D

OF Temperature, 'F (calculate 

•0 (p4 F (,l/'fc o.o

1/D"F L/foF 1),

21!:'/(; .3DO"r- 6 ·l.

'=[(Ref Temp, C+273) ·Test Temp., C + 273)/Ref Temp, C + 273]'100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QC Check Completeness j Legibility__6ccuracy / Reasonableness 

Checked by: i.J (Vcle.N ti-2';·<'"1 

Calibration Technician 

(Signature/Date) 

ATC Form 209-Primary Them1ocouple Calibration Record 

version 2.1 May 2009 

t,.)- n

Test Team Leader 

(Signature/Date) 

F:\Work.\Ail Forms-... \2090-Prlmary thermocouple 

ATC (8
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degree indicuting !r.vd position for detcrminiilg Ctt and ~· 

Degree indicated l~vel position for determining p1 3Jld thDegree i11dicating lc:vel position for 

detcm)inlng of0. 

Degrees indic:l.ling level position for determining y t11en calcufate 

z 

-

- Le••el mul Perpendicular? - -~-

Obstruction.? ·----· 

Dam(lged? 

····-

l1J (-10' :5 a1:5;+J(f') 

a1 (-1(1' :5 a,:;-;+10') 

--- PI (-5' :5 fJI :5 +5") ---~--~---

p, (-5' :5 p, :5 +5") - -- )' 

e 

Z=A fan 7 (< 0.125'') 

I W=A tan@ (:5 0.03!25'7 - i D,(3/l6" :;'; D, :5 3/8'') 

r--------

A -- AI2D, (1.05 :5;P_,!D, :5;1.50) 

If temperature sensor is flush 'H!itlt 

pito-t tube openiltJ:, is Z >-x 1

7 ----- lftempel'ature sensor is set back from 

pitoc tube opeuina- is W> 2"? 

Is X?:, ¥/'fot· Dn =¥.?u 

Is impact side of pitot tube even with 

or above !lOUie entrv plane? 

lis I?_J"for3fl6"<Dt<318"? 

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y 

r-- Al_ ____ 

N 

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f.261I 

y --

N 

y 

)/ ---

/ - QAIQC Check 

Completeness legibility Accuracy Specifications Reasonableness 

Cei·tification 

I certify that the TypeS pitot tube/probe ID # -----~5-WJ~AWc----~ meets or exceeds all 

specifications, criteria and/or applicable design fealt.rres and is hC'.reby assjgned a pitot tube calibration fiactor Cp of 

o.s4'. /:1 :l . I /1 /I . 

. fi db "L.• d /)t~.· ~ I-2 ~- D9 K,·<w I (/L!..r.a cr.~ ... _. iz -B -if! Ccri.! :e y: ~ ~-~· r 

P.er.-;' nne! (Sigm,tU!'eJOat~) Team Leader (Signature/Date) 

1 This certification also applies to the specifications of EPA M~thq.~ 2, section l 0.1.4.1.1 regarding inter-component 

spacing ofpitot tube-sampling piobe as$emblics. Refer to the figlli:es on the reverse side of th:is page for specifics. 

ATC Form 37-Prlmary S-tYPe Pitol Tube C'alibr-Jtlom-verslon 3.0 September 2007 ATC@ (800) 73]-3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 644 
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Calibration Date 1/· 2'5- o"'' 

Ambient Temp., !)F r.. c.f'~ 

" 

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Reference Source2 

Point (Specify) 

Number 

1 Ambient Air 

2 Ice Bath 

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------

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Thermocouple Number 51A 

Barometric Pressure, inches Hg zCf. 1 <:; 

-

--

--~ F7 F8 

Reference Thermocouple T

Temperature Potentiometer D

OF Temperature, °F (calculate 

(,I/(.: (,_'CP ()

'-/0 1~ tfJO. 

, r- - o. 

----~~Of.?_~' _____ zqq" o. 

3:[(Ref Temp, C+273)- Test Temp., C + 273)/RefTemp, C + 273]"100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QCCheck 

Completeness ../ Legibility /Accuracy /specifications /Reasonableness 

Checked by: ~1~....., ;t·;?';,--o-:; 

C~libration Technician 

(Signature/Date) 

ATC Form 209·Prirnary Thermacouple Calibration Record 

Vf'...rslon 2.1 May 2009 

1_,_), L.& ruxL (l:

Test Team Leader 

(Signature/Date) 

F:\Work.\A(J Fonnsv.,,\2090..Prtmary tharmocouple 

1\TC (8
( 

BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet -- ---

K' 

'y Level a11d Perpe111licrdar? 

r-----

ObstructiOTt? N r~CP:n [r:---~j'i'l ' - ---, I I 

" ' ,, (-< 

LJ 

Degret! in<!ic~ting level pmit1on for dele1mining: 0.1 and a1. 

Degree indicated \evei position for det..:nnining ~~ ood . 

Degree indic:uins level position for 

delennining ore. 

:. _2 ;(' 

~-~·~~==~d;-,~--

Degrees indicating levd po.~ition tbr determining -y then calculate 

z. 

QA/QC Check , 

Damaged? 

a, (-10' S al~+IO") 

-

a, (-10' :;;;a,~+JO') 

fl; (-5' ~ p, ~ +5') - --- -·------

p, (-5" s p, ~ +5') 

r---

)' 

e 

Z=A ta11 y (< 0.125'? 

W=A t'm e (:5: 0.03125'~ 

D,(3116"~D, :5;318'? 

A 

AI2D, (1.05 :5;P,,ID, ~ 1.50) 

if temperature seJisor is }lush with 

_pilot tube ope~tin_e, is Z >¥.- "? 

lftemperauu·e sens-or is set back from 

pitot tube ope»imt, Is fV > 2"? 

JsX?:.~"fcrDit ='ll" 

Is impact side of pi tot tube even wlth 

or aboveyozz/e eJttry plmte? 

Is }~3''Jor 3116" <Dt < 3!8"? 

N 

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r --

ic 

. " l 

0 

D 

0 -- 0 

0-~75~ 

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1-23,~ 

c-y 

N ---

y 

y 

y 

Completeness ""'_,..... Legibility .!- ,_.-·Accmacy _..- SpectficatiOl.lS -:--- Reasonableness _____. 

Certificatioll 

I certify that the Type S pi tot tube/probe lD # 52 meets or exceeds all 

nel {Sign3ture/Date) Team Leader (Sigmnure-/Date) 

1 T1lis certification also applies to the specifications of EPA Method 2, section 1 0.1.4.1.1 regarding inter*component 

spacing of pitot tube-sampling probe assemblies. Refer to the figures on the reverse side of this page for specifics. 

ATC Fotm 37-Primary S-type PitOI Tt1be Calibrations-version 3.0 Sept~tJiber 2007 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PlANTS 4 & 5. SALISBURY PtA NT 6 

SEPTEMBER 2010 

ATC@ (800)733·3193 

APPENDIX PAGE No. 646 

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· Reference Source2 

Point (Specify) 

Number 

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2 Ice Bath 

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--

~-----------

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2Type of calibration system used 

Thermocouple Number 52 

Barometric Pressure, inches Hg z"t .I ~ .. - - ' ---- ' 1"''1, FB 1 ;<

Referen<>e Thermocouple T

Temperature Potentiometer D

OF Temperature, °F (calculat

6'/!= ·10 k, F o.o

'10"e 1.(0 iJ f' 0 ,0

3oz.> 30Z~ O.co

'=[(Ref Temp, C+273) ·Test Temp., C + 273)/Ref Temp, C + 273!*100<1.5% 

Kelvin= (519) * (F-32) + 273.15 

QA/QC Check 

Completeness .,/Legibility / Accuracy_..-§pecifications __ ,...ifeasonableness 

Checked by: l{,j U/dt.P> Jf-1";-0CJ 

Calibration Technician 

(Signature/Date) 

ATC Form 209-Primary Thermocouple Calibration Record 

version 2_1 May 2009 

~ · 

~-B~l""' 

-·----------·-----------

1~

Test Team Leader 

(Signature/Daie) 

F:\Work\A!I Forms~ ... \2090-Primary thermocouple 

ATC (8
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet --

_j :;·- Level and Pl!lpendicular? 

Obstruction? 

------··· 

Dam11ged? !J 

a, Hrf :'Oal:'O+lrf) {a 

L-~-

Degree indicating le.,-c! positiml for dctermining o: 1 and Q1. a, (-10' :::a,:'O+lrf) - !" --- _ ___j 

Degree indicated level position for determi;1ing p, and 0.,. 

Degree irodicating level position for 

dete1mining of<:>. 

,, ~l 

h.:-::;:~::::·::.·_ t -::>,--- " 

-. 

Degrees indicating level position for determining y the11 calcuta.re 

z 

{1, (-5"::: p, :'0 +5') 

····-· 

p, (-5' :'0 /IJ ::: +5') 

"I 

e 

Z=A tan y (.< 0.125") 

W=A tan e (S 0.03125'~ 

D, (3116" S D, :5: 318") 

A 

AI2.D, (1.05 :'OP ,/D, S 1.50) 

Iftempernture sensor isflusil witlz I 

pitot tube "''e'!~g. is Z >~"? _ 

If temperature sensor is set !Jack from ! 

pitot tube open in~, is ~V > 2"? __ 

b· X:::_-% 1

' for Dn =YJ" ....,-,------

1 Is impact side ofpitot tube even li'itlt 

! or above noz.zle entq.J!J.ane'? 

D I -- 0 

0 ·-·-·---·-

0 -~ 

0 

0 

0-'376 

(} 150 

I. ..-, ,.,...,. 

r ..,... -"'-1 

/ __ (I} 

y 

7 --

QA/QCCheck G" 7 Y;o: -~"for 3116"<Dt <318"? 

Completeness ---" ,._._..-" Legibiljty L----Accmacy - Spccific.at10ns ~ ReMonablene-ss '---· 

Certificatiou 

l certify that the TypeS pitot tllbe/probe ID # ---··--~5c.3.LLA::>.-. __ _ meets or exceeds all 

spe:cificarions-, criteria andior appllcable design features and is hcrtby assigned a pitot tube calibration factor Cp of 

o.84I _q 1. k' . ·; .~ "-c:~- '/ /. /] (S/ ~:./)"/~. w .. . ·,u r/L-.-f.q.£(/1__. l -~ ..L ~· ,r 7 

Certified by: · -- -;r:-:, /-t, . -

.L.-t - · c./{:4 ~ , ,lc J 1 ~~ "..L:..!..fJ/; 

, Personftl {Signature/Date) Te-am Leader (Signature/Date) 

1 This certification also applies to the specifications of EPA Method 2, section 10.1.4.1.1 regarding inter-component 

spacing of pitot rube-sampling probe assembhes. Refer to the figures on the reverse side of this page for specifics. 

A TC Fom1 37-Primary S-type Pitot Tube Calibrations-version 3_0 Sep!ember 2007 

ATC.PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC @ (800) 133-3193 

APPENDIX PAGE No. 648 

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Ambient Temp., °F (,<.{" 

Technician ~i("'e;;cN..:,...-C."::':"~-t-c:-t-r:JG-'""-A--·-:-'>--

Reference Source 

Point (Specify) 

Number 

1 Ambient Air 

2 Ice Bath 

3 Thelco Oven 

1 Reference thermometer~mercury in glass 

2Type of calibration system used 

Thermocouple Number 53

Barometric Pressure, inches Hg _ _.£9 ....~· .._!.;;<>;....

Reference Thermometer {List ID #)1 1"7. F8, 

Reference Thermocouple T

Temperature Potentiometer D

OF Temperature, °F {calculat

&'I; (,A';; o.o

'-}D~ 4of: o.o

3C.O'f- 2"11t= " o.:w

'=[(Ref Temp, C+273)- Test Temp., C + 273)/Ref Temp, C + 273]'100<1-5% 

Kelvin= (519) * (F-32) + 273.15 

QAJQC Check 

Completeness / Legibility~Accuracy /specifications ~easonableness 

Checked by: Jiu.i {Jjc/;,~; tt~Zt;- oCj 

~aUbration Technician 

(Signature/Date) 

ATC Form 209-Primary Thermocouple Ca!ibfation Record 

version 2.1 May 2009 

GJ ~LL, 

tJ~~ tt./t

Test Team Leader 

(Signature/Date) 

F:\Work\Ail Forms~ ... \2090·Primary thermocouple 

ATC (8
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Level and Perpendicular? 

Damaged? 

Obstruction? 

~ ,tJ 

Degree indicating level position for determining 111 and a 1• 

Degree indicated level positian for detemlinh1g fh and !h.. 

Degree indicating level positiou for 

detennin;ng of e. 

Degrees indicatillg lc.vel po.<:>ition for determiningy then calculate 

z. 

a, (-II!':::; al:::;+IIf') 

a, (-11!' :5: a2:::;+IIf') 

p, (-5":::: p, :::: -J-5D) 

p, (-5" :5: p, :5: +5D) 

---------

'I 

----------

e 

Z=A tar~ 7 (.< 0.125'') 

W=A tun 19 (::; 0.03125') 

D, (3116" :::;D, _::: 318'J 

A 

AI2D, (1.05 :5: P ,,D, :5: 1.50) 

If temperature se11sor is flush wltb 

pilot tube opening, is Z>W'? 

If temperature sensor is set back from 

pitot tube opming, is W> 2"? 

Is X2: X"for Du =M" 

Is impact side ofpitol tube evefl with 

or above nozzle ei111V vltme? 

Is l?:;3"fol'3/16" < Dt <318"? 

,c ~- / 

I c 

0 

0 

0 

\) 

0 

0 f------

(). )?D 

(). i''f 7 

t- ,.~,L 

y 

N 

N/A 

/'J/A 

OA/QC Clteck NIA 

Completeness _L- Legibility c./- Accuracy ~SpecificatiOns .-------- Reasonableness ~ 

Certification ,- __ 

7 11 I certify that the Type S pitot tube/probe ID # -> J7 meets or exceeds all 

specifications, criteria and/or applicable design featnres and is hereby assigned a pitot tube calibration factor Cp of 

o.s

4

'- rf • n , ~ - A,, I 11 i 1 VI f! • ~- L 

C oru 

'fi 1e db 

y 

. _ .. J!/8,__,7(- 15 t ~<c>f1lz [ f· j 5 - ~- 7 lA.. L l{..v~ ( y r"t •. _.;- ?"/ . 

Pcr~6nnel (Signature/Date) Te.am Leader (SignaturefDate) 

1 This certification also applies to the specifications of EPA Method 2. section 10.1.4.1.1 regarding inter-component 

spacing ?c_fpitot tube--sampling .Ptobe assemblies. Refer to the figures on the reverse side of this page for specifics. 

ATC Fonn']7-P;imary S-type Pitot TubeCalibra1ions•version 3.0 Septernber2007 

ATCPMJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PlANTS 4 & 5. SALISBURY PlANT 6 

SEPTEMBER 2010 

ATC@ (800) 733-3193 

APPENDIX PAGE No. 650 
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0> ~ Thermocouple Primary Calibration Data Form Calibration Date 12 • :Z 1- () 'f Ambient Temp., 'F 51' Technician (.B. Reference Source' Point (Specify) Number 1 Ambient Air 2 Ice Bath l Thelco Oven ----- --------- - 1 Reference thermometer-mercury in glass 'Type of calibration system used Thermocouple Number 57 A ---::-'::::--:

Barometric Pressure, inches Hg ,;2 [ '-1

Reference Thermometer (List ID #)' F·7 Reference Thermocouple Te

Temperature Potontiomater Diff

'F Temperature, 'F (calculate 

51. 50' 0. tpd,

'32"" '"5 "3 0 - 0,3?

~--· 2ft!. -· 2t??"' ···------- o.ql"'

3=[(Ref Temp, C+273)- Test Temp., C + 273)/Ref Temp, C.,. 273]'100<1.5% 

Kelvin= (5/9) • (F-32).,. 273.15 

QA/QC Check 

Completeness ~egibility /Accuracy /specifications,_..../'Reasonableness 

Checked by: r- ;;2-.J/·() r 

Calibration 1' hnician 

(Signature/Date) 

ATC Form 209~Primary Thermocouple Calibration Record 

version 2 1 May 2009 

~J. 

'-(.,__,~ 1 '1.-1 '~-l l

Test Team Teaaer-~~~ 

{Signature/Date) 

F:\W<Jrk\A!I Forms-... \2090-Primary thermocouple C

ATC (800
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Lepe[ a11d Pmpendicnlar? 

Obstruction? 

- ---------~~ /Vi I Damaged? 

, a 1 (-111' ~ aJ:!;+lll') . 

I a, (-111' ~ a2:!;+111') 

---·---------

-ft-=1 Degree i.ndic.atitlg level position for determining o: 1 Hnd o2 /" -----

{J I (-5' :S fJ1 ~ +5') 14 

. t ----·---

p, (-5' ~ p, ~ +5') '" __/__:__ ___ y 0 -- -~-· 

e 

Degree indicated level position for determining n1 and~~ 

D 

Z=A tan 1 (< 0.125'? D ·--···----

W=A tall@(~ 0.03125'7 () 

D,(3116"~D, ;SJ/8") o. -:;75 

Degree indicnting level position for 

determining of0. 

A -ro -'1ii?i 

AI2D, (1.05 < P /Dr < 1.50) c-;-;;----- - - ;. 2jJ"t 

!/temperature sensor i..r.;jlush with 

pitot tube ope~tiug, is Z >% "? _____ y 

Degrees indicating level pn!::itiOll for determining y th.:o:n calculate 

2 

If temperature se1tsor is set back from 

_p_itot tube Qpenlne, is W > 2"? 

IsX~-%"for.l)Jl =~" 

[ Is itnpact side ofpitol tobe even with 

/1/ 

y ·--

I or abQt'e nozzle ently plaue? y ___ --cQA!QCCheck y i ls 1'?:. 3" for 3/16" < Dt < 3/8"? ' . 

Completeness ::.---~ · Legibility Ac:cmacy- SpeCificatiOns Reasonableness ---- Certification 

I ce1tify that the TypeS pitot tube/probe ID # 59 meets or exc:eeds all 

specifications> criteria and/or applic.ablc de-sign features and is hereby assigned a pitot tube calibration factor ~ of 1 - - . 

0.84. . . 

,..-f -. . ,; " /j . . . 

Cel1ifiedby: (;0e.,_.-ffjt-1£t.. /1-21:,-0<j /yv/ i~~~:tRr-> 12-.:l-c:u-; 

Per_}6nncl (Signature/Date) Team Leader {Signature/Dote:) 

1 This certification a.lso applies to the specifications of EPA Method 2, section 10.1 A.l.l regarding inteT-component 

spacing of pi tot tube-sampling probe assemblies. Refer to the figures on the reverse side of this page for specifics. 

A TC Form 37-PJimary S·type PitcH Tube Cafibra\ioruH•ersion 3.0 September 2007 ATC@ (800) 733·3193 

ATC PROJECT No. P-1 0142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 652 
)> 

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Thermocouple Primary Calibration Data Form 

Calibration Date II - Z "? -oq Thermocouple Number 59 

Ambient Temp., °F c;, '-{ Barometric Pressure, inches Hg ;?'(. 1 5" 

-

Kl!5vr'/J.c::<Df3't-S ······· ·-- ···········--- ·-·-··-

.. , F 7, r-g. 

Reference Source Reference Thermocouple T

Point (Specify) Temperature Potentiometer D

Number °F Temperature, °F (calculate 

1 Ambient Air G cf'F (;, .5"" - 0. 1

2 Ice Bath '-IO'PL/Z~-:: -o. ··fo•> 

., .0 3 Thelco Oven 3 I t...;r- ::n::: •"" - o. zr:,

i.___ --- -- -------- -----------~..::...:... ----------- ------~··· ----------- L___ __ ---~-~--

1 Reference thermoineter .. mercury in glass 

"Type of calibration system used 

3=[(Ref Temp, C+273) ·Test Temp., C + 273)/Ref Temp, C + 273]'100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QC Check 

Completeness /Legibility ./Accuracy Apecifications v'Reasonableness 

• /"). I Checked by: !(t.t-;( (;.;jd,._, it- ?c:co") 

Cqlibration Technician 

(Signature/Date) 

ATC Forrn 209~Primary Thermocouple Calibration Rer,ard 

version 2.1 May 2009 

lA 

Lt.;~_ J?srb i£

Test Team Leaaer 

(Signature/Date) 

F:\Work\AJI Forms-... \2090-Primacy thermocouple C

ATC (80
( 

BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degree indicating level position for deteJmining 0::1 and U2· 

Degree indicuted level position for detetmining (h and fh. 

Degree indicating level pru.ition for 

dttcmlining ore. 

IY~ 

( .. ~- .:::':::=--.::-:~.;:; - -

.. . Degree~ indil::a1ing level position for detennining y then calculate 

7.. 

Level and Perpmdicular? 

Obstruction? 

Damaged? --

ar (-1{/' ::C::a1::C::+f(/') ··------------

a, (-1{/' :S a,::::+J 0') 

p, (-S' :5 Pr :": +5') 

p, (-5' :5 p, 5 +5') 

'Y 

e - z~A tan 7 (< 0.125") 

-· 

W~ A tan I?J ('5; 0.03125 ") 

D.(3iJ6"'5;D, '5;318") -· 

A 

AI2D, (1.05 :!;P,ID, :":1.50) 

If temperature seusor is flush with 

pitot tube openiltfl! is Z >X"? 

IftemperatuJ"c sensor is set backfrnm 

pitot tube opening, is 1¥> J»? 

1 IsX~-%-"forDn :::~" 

!Is Impact side ofpitot tnbe even with 

l or above uoule etttrp plane? 

Is ~3"for3116"<Dt<3/8"? 

·-- ·v 

/ 

N 

tJ 1---·--- ~~ 

I f-·----

/' 

z· 

2~ 

I 6 

0 -----

0 

0 

o. 37.! 

o. '115 

/. Z{<f -·-

y 

N --- y --

y 

t QAIQC C/reck 

Completeness / Legibility ... ->"'}\ccuracy ~ Spec1fications 

-· Reasonableness __ _ 

Certificatiou 

J certify that the TypeS pitot tube/probe lD # ------'-'8'"'2._ _____ _ meet~ or exceeds all 

specifications, criteria and/or appiicab1e design features and is hereby assigned a pitot tube yalibJ:ati\)11 fador Cp of 

0.84 1

• • /! ,..; . . ~ /] . . • . 

·c . ·fi db·. c?fie .i fx<~ 11 -25 -b '1 ~---~ ufaA.J__j_Z-8 -c '? .e1t1 1e y. _ .. . , · · - ~ Pcfsonne! (SJgnaturt:/Datc) Tct:nl L¢acier (Signature/Date) 

---·----------

1 This certification also applies to the ;;pecifications of EPA Method 2, section 10.1.4. 1.1 regarding int6--component 

sp:~cillg ofpitot tube--sampling probe assemblies. R~fer to the figures on the reverse side of this page for specifics. 

ATC Form 37-Primary S-type Pi tot Tube Ca.Jibrations-vcrsio~ 3.0 Sei)tember 2007 ATC@ (800) 733~3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 654 
i: 

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"' ~ ~ Thermocouple Primary Calibration Data Form Calibration Date i1 A /tf" c r Ambient Temp., °F 5{" Thermocouple Number . 1?.;2 -......,;:.

Barometric Pressure, inches Hg a 1 .. 5 I ~ .... ~'.':"' T.B- _-_ _---·------- - ··-····-··---~- \------ .. , F7 Reference Source' Reference Thermocouple Tem

Point (Specify) Temperature Potentiometer Diff

Number OF Temperature, 'F (calculate i

1 Ambient Air 56jj 5 

51' o. ;;,o "

2 Ice Bath 1-fl)' ?I" 0. 3':J.I

3 The_l_c_() Ove_flJ____-:2<1 0 "-·· 2fi'"o . - --------- __ ._ .. --- ---- _.____ ___________ 0. ~-- 3~s>''fl

. - 

1 Reference thermometer-mercury in glass 

2Type of calibration system used 

'=[(Ref Temp, C+273) ·Test Temp., C + 273)/Ref Temp, C + 273]'100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QC Check 

Completeness / Legibillty~Accuracy ./ Specifications~Reasonableness / 

,._.,:! "") 

Checked by: (1-~"'f iJ£,_:iJ&n. 12-t4·c<f 

Calibration Te$hnician 

(Signature/Date) 

ATC Form 209-Primary Thermocouple Calibrauon Record 

version 2. 1 May 2009 

f, J. ~:0\.LO~ JYl

TestTeam Leader 

(Signature/Date) 

F:\WorK\Ail Forms- .. \2090-Primary thermocouple Ca

ATC (800
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degree indicating hwel position fur delemtining 1:11 and a:1. 

D!!gree indicated level positiOli for determining ~~ and P2. 

Degree indicating level position for 

&termining of0. 

Dtgr~ indicating Je1·cl position for detennilling y tl1en calcldaie 

z. 

QAIQCC!teck 

Comp 1e-teness .....,/ 

Level and Papendicular? 

Obstruction? 

1------·-·· 

Dantaged? - a, (-!If' :5; al:;:;+l(/') 

f-· 

([2 (-1{/':;:; at::;+J(/') 

p, (-5' :5; p, :5; +.5') 

P1 (-5" :5; p, :5; +5') 

y 

@ 

Z=A tan 7 (< 0.125'') 

W=A tan e (:;:; 0.03125") 

D,(JIJ6":5D, :::;318'') 

A 

A/2D, (1. 05:::; PAID, 5 1.50) 

If temperature sensor is flush wit"-

pilot tube opening, t's Z >% "? 

lftemperaJure sensor is set back from 

_pitoJtuhe open ina, is W> 2"? 

Is X::-%" for Dll =M" 

Js impact side ofpitot tube e1-•en wftlt 

or above liOl,t.le entqp_[ane? 

Is Y?;, 3'•jor 3/16~' < Dt <318"? 

- -------

7 

N 

f/ 

;o 

i" 

C.J 

6 

D 

0 

0 

I {) 

0· 37¥ 

0.11 

f. 330 

y 

jl/ 

r--_L.. __ y 

"'-' / ------· 

1 This certification also applies to the specifications of EPA Method 2, section 1 0.1.4.1.1 regarding inter-component 

spacing ofpitot tube~sampling probe assemblies. Refer to the figures on the reverse side of this page for specifics. 

ATC Form37~Primary S·type Pilot T11be Calibrations-version 3.0 September 2007 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC@ (800) 733-3193 

APPENDIX PAGE No. 656 
J> 

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z ~ "' "' ... ~ Thermocouple Primary Calibration Data Form Calibration Date 11 ~/4·~0'1 Ambient Temp., °F SY;;. -- -- •. - ·-rg J •• , Reference Source Point (Specify) Number 1 Ambient Air 2 Ice Bath 3 Thelco Oven 1 Reference thermometer-mercury in glass 'Type of calibration system used Thermocouple Number ?{ 1-f Barometric Pressure, inches Hg ----io~

2 <:J, S 1 - --.- • -''.'""'~·- ••• -· ••• - •• ·-·-· \-,~- ·- •· I .F1 Reference Thermocouple Tem

Temperature Potentiometer Diff

OF Temperature, °F (calculate i

5'1° s~-t ,. 0&/

40p ·""")Q <; )1 0. :J...~

2~d"' 271?" 0. ?Ji.:e 

'~[(Ref Temp, C+273)- Test Temp., C + 273)/RefTemp, C + 273]"100<1.5% Kelvin= (5/9) • (F-32) + 273.15 QA/QC Check Completeness ,/Legibility__L_Accuracy~pecifications__::::Reasonableness / Checked by: d'l.~,;r !5liMq.n /1-lt..;-tr'l - - - - - } - - (Signature/Date) ATC Form 209-.Prim.ary ThermocoupJe Calfbratton Record version 2.1 May 2009 (A)_ tL~~ f~ l~/

Test Team L..eaoer (Signature/Date) F:\Work\Aif Forms-... \2:00Q..Primary tl1ermoco!Jple C

ATC (800
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet -- Level and Perpeltdicular? y --

Obstructimt? N 

Damaged? N 

a, (-10"::; al:':;+lf!') IC 

I 1---

Degree indicating !evt:l pmition for determining o1 and a1• a1 (-If!' :5;az:5;+lf!') I c 

f-----

h (-5" :':; p, :':; +)~) ?" 

p, (-5" 5 pl 5 +5") !" --

Degree indkated le~·eJ position for determining~~ llild ~lDegree indi"nring level po:c;ltion for 

detem1iJ1ing ore. 

,, _,1. 

::-

r;:::-::-: :::,:..:=..d, --

• 

Degrees uHiit;ating le-.·el position fur determining y thl!n ca\clllate 

Z. 

'l 

e 

-----~----------·-· ·-··------

Z=A tan y (< 0.125 '? 

W=A tan @(:5;0.03125i") 

D, (3116" :5;D, 5 318'? ·-------------····--------

A 

A/2D, (!.05 5 p_,!D, :5; 1.50) 

If temperature sensor is flush with 

pr'tof tube oe.ening, i!l' Z >Yt'"? 

lftempetature sensor is set backf,.om 

oitot tube ope11i11~, is W > 1"? 

ls X2: %''for Dtt =V:r·'' 

ls impact side of pitot tube even with 

o1· above nozzle entry J!..~mre? 

.l.r:; Y?:. 3" for 1116" <Dt < 318''? 

0 

{) 1----------

1) 

0 

0.375 

o. 'I '-{-2 

{2S6-

y 

/'/ 

y 

y 

QAIQC Check / f 

Completeness ~ Legibility ~__......,.,.Accuracy ·- Specifications ___.., Reasonableness ---··· 

Certification 

1 certify that the Type S pitot tubefprobe ID # 85 meets or exceeds all 

·specifications, criteria and/or applicable design features and is hereby assigned a pilOt tube calibration factor Cr of 

~·r.db .. "--:v. qf;. 1/-15 ··C>/ J?A (~/j-"-"~ Jz-ff ~r.:Jfi' . enLte y. t. 

Te«m Leader (Sign~:~ture/Date) 

t This certification also apphes to the :>pecifications of EPA Method 2, section 10, 1.4. 1.1 regarding inter-component 

spacing of pi tot tube-sampling probe assm11blies. Refer to the figures on the reverse side of this page for specifics. 

ATC Fom1 :l7-PrimaJ)' S-typc Pitot Tube Calibralions-ven;io.n 3.0 September 2007 ATC@ (800) 133-3!93 

. 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 658 

1 
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Calibration Date /2 '1'/ - (,!J 

Ambient Temp., "F '?•i" 

Technician T.l3 

Reference Source2 

Point (Specify) 

Number 

1 Ambient Air 

2 Ice Bath 

3 Thelco Oven 

1 Reference thermometer-mercury in glass 

'Type of calibration system used 

Thermocouple Number ?5 

Barometric Pressure, inches Hg---~:-:,,::::9;-."'l.J

Reference Thermometer (List ID #)1 ;:·7 

Reference Thermocouple Tem

Temperature Potentiometer Diffe

"F Temperature, "F (calculate in 

SLJ~> .) '-.("' , ·- ('). lo

i-11)0 37" () . ?:>

2. '10. 4)7~0 

----- ...:; " I ---- - - .. - Q, S__'2

3 

. =[(Ref Temp, C.,.273)- Test Temp., C .,. 273)/Ref Temp, C + 273]'100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QA/QC Check 

Completeness o/iegibilityLAccuracy~pecifications ._/'Reasonableness / 

;•-' 7 Checked by: i-..;.,.1 /5 •. ~ !1-14-0J 

Calibration T4nician 

(Signature/Date) 

ATC Form 209-Prirnary Thermocouple Calibration Record 

version 2. '1 May 2009 

/;, ). ~L R/191._,.___ r:-f 

Test Team Leacfer 

(Signature/Date) 

F:\WorkWI Forms-... \2090-Prlmary 1hennocouple Ca

ATC (800) 
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

D~!gree indiclltirtg level position for determining o.1 ood a,.. 

Dcg,tee indicated level position for determinir.gfJJ and }h. 

Degree indicating level position for 

determining of B. 

Degrees indicating levd position for determining 1 then calculate 

z. 

QAIQC Check 

Level and Perpendicular? ----- Obstmctio11? 

~· 

Damaged? 

a, (-iff ::: a]:::+ 1 (/') 

a, (-10' ;:;u.,;:;+lff) 

p, (-5' 5 PI::: +5') 

p, (-5'::: p,::: +5') 

7 

@ -- Z=A ta117 {.< 0.125") 

W~A tell!@(::; 0.031Z5") 

D, (3116" 5 D, ::; 318'? 

A 

A/2D, (1.05 :!;P#D1 ::,1.50) 

lftempmtture seusor is flush with . oitot l!the oveninJ!. is z >'),"? 

I[temperature sensor is set back from 

Ditot tube open!!J:& f.s W> 2"? 

Is X?:, "A"for Du ~" 

Is impact side of pilot tube even with 

or above noa;le entrv plane? 

u Y?:. :!"for 3/lli" <Dt < 318"? 

y 

N 

N 

I , -----

r 

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14 

0 

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l.?d 

y 

N 

tJ/A 

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All4 

Completeness ~- - Legibility~- Accuracy ...-· Specifications -- Reasonableness -- Catificatiolt 

v 3 

I certifY that the Type S pitot tube/probe ID # ~--_:d::_:----~---~ 

meets or exceeds all 

specificatioru, crite-ria and/or apPlicable design features and is hereby assigned a pitot tube caHbration factor Cp of 

0. 84l "1" 

v /::' :/, 

/_.? . .o : · ...: r \("- L J · ... l / { 

C "fi • · ,11 ~ l OU/ { f- 2 ::> ·-t• 1 1 :.uA , /,_v'("'-'-i/1 I 'L tl ;1 

--~~ . Team Leader (Signalure/Oate) 

- 1

._'_This certification also applies to the spedtications l)fEPA Method 2, section t 0.\ .4. \.1 regarding inter~component 

:~;-~pacing of pitot tube-sampling probe assemblies. Refer to the figures on the reverse side of this page for specifics. 

·:·\~\KTc Form 37-Primary S-typc PitotTube Calibrations-version 3.0 Septemher 2007 

ATC@ {800} 733-3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 660 
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Calibration Date t:Z-ZI-<>'1 

Ambient Temp., °F 5;z.o 

Technician T G. 

Reference Source' 

Point (Specify) 

Number 

1 Ambient Air 

2 lee Bath 

3 Thelco Oven 

· 

1 Reference thermometer-mercury in glass 

2Type of calibration system used 

Thermocouple Number ?I 

Barometric Pressure, inches Hg J"/. '79

Reference Thermometer (List ID #) 1 ;::::" -7 

Reference Thermocouple 

Temperature Potentiometer Diffe

OF Temperature, oF (calculate i

sJ· 5o¥ D. VJ,#

32• 33' - 0. 53°/

/J'{>o 1774 v wf.c% 

·-· --- ----------•------------

·'=[(Ref Temp, C+273)- Test Temp., C,. 273)/Ref Temp, C + 273].100<1.5% 

Kelvin= (519) • (F-32) + 273.15 

QAJQC Check 

Completeness /Legibility /.Accuracy 

Checked by: ' , /J -:2/-tl i /M..... jOUv.t.- (l.0-J 

Calibration hnician est earn Leader 

(Signature/Date) (Signature/Date) 

ATC Form 209-Primary Thermocouple Calibration Record 

version 2.1 May 2009 

..t 

F;\Work.\AU Forms-, .. \2090-Primary thermocouple C

ATC (BOO
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

Degree indicating- kvel position fur detemllning £4 and n1. 

.-. ·._· -. . 

Dc:gtee indicated level positio11 for determining ~~ and fh. 

Degree indicating level position for 

determining of e. 

77EJ 

Level and Perpendicular? 

Obstruction? ·--- Danza .. !fed? 

a, (-10":: al::;+l 0") 

a2 (-10".::; a,.::;+JO") 

p, (-5'.::: fJ,::: +5') 

P1 (-5'::: p,::: +5') 

y 

e 

Z=A tan 7 (< 0.125") 

W= A tan fJ (:5; 0. 03125'') 

D, (3116" ::;D, ::;318") 

A 

AI2D1 (1.05 .S P,,ID, :5: 1.50) 

If temperature sensor is flus II wit/r. 

pilot tube openin~, b;. Z>~"? 

If temperature sensor is set hack from 

pitot tube openina, is W > 2"? 

1-tX~ %;"for Dn =%,, 

I 

Degrees indicating Je\'el position for cleterntining y tlltO calcl1late 

z. Is impact side ofpitot tube even with--

or above nozzle entry plf!pe? 

y 

N 

N 

;o 

I" 

c.> 

0 

0 

0 

0 

{) 

(). 3 7¥ 

0.1'15 

f. 330 

y 

f\1 

_L __ 

/ 

QA/QC Check Is Y?. 3"for 3/16" < Dt < 318"? / J --. -------------· ----·- Completeness / Legibility SpecificatiOns ~-~ Reasonableness~ 

Certification '"?u 

l certify that the Type S pitot rube/probe lD # ¥o meets or exceeds all 

specifications, criteria and/or applicable design features and is hereby assigned a pi tot tube calibration factor CP of 

0.841

. /"- ~- {:' /, ·it -kn. !f-2~"-o . ' I _"· 1

:c.../_ -cr.:? Certified by: ~ · - ' :l ' ~ - ·-fC:L.i'r1 /2--- 6 ' 7 

el (Sig.nature!Droe) Team Leader (Signahlre/Date) 

1 This certification also applies to the specifications of EPA Method 2, section 1 0.1.4.1.1 regarding inter-component 

spacing ofpitot tube~sampling probe assemblies. Refer to the figures on the reverse side ofthls page for specifics. 

ATC Form 37·Primary S-type Pltot Tube Calibrations-versiorJ 3.0 September 2007 

ATC PROJECT No. P-10142 EPA JCR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & s. SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC@ (800) 733-3!93 

APPENDIX PAGE No. 656 · 
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

,, 

Degree indicating level position for detem1ining a1 a.'ld a2-

Degree indicated level position for detenninlng ~~ and Pl.> 

Degree indicating level position for 

detcrulining of e. 

;;.--z 

~-- +~-- .• . Dtgrees i11dlcating level position fQr detcnnining y then celculate 

z. 

QA/QC Clteck 

----

Level and Perpendicular? 

Obstruction? 

Damaged? 

a, (-10':::: a1:::+10') 

a, (-lrl':::: a2:0+lrl') 

PI (-5':::: p,:::: +5") 

p, (-5' :5 Pz :5 +5") 

'! 

e 

z~A tan 7 (.< 0.115'~ 

w~ A tan e (:5 0.03115'~ 

D, (3116" :5D, :::: 318'? 

A 

AI2D, (LOS:::: P,.ID,:::: 1.50) 

Iftempernture sensor is jluslt wltlt 

pilot ftlbe opem'u,f(, Is Z >%"? 

Ifumperature sensor is set hack from 

pilot tube opening, is W> 2"? 

h X;! Y-t"for Dn ='h" 

Is Impact slue ofplto/ /t{be eve1r will! or above 11oule e11tn nlane? 

Is f?:.3"for3!16"<Dt<318"? 

y 

IV 

IV 

'0 ' 

,c 

I 

_......., t. 

.i. 

'I.> I 

A 

(/ 

i./ 

0 

"'' v 

. ~--x 0.5 /...., _ ...... ....,. .. 0. ~ I{. 

s i{C /-. . ) 

/ 

;J 

'/ 

/ 

y 

/ -

I l 

Completeness v/ / _.-- Legibility .,./ Accuracy vr Specifications ~ .. Reasonableness ..,..,..-

Certification """' 

I certify thatthe Type S pitot tube/probe l.D # 6 i meets or exceeds all 

specifications. criteria andlor appllcable design featw·es and is hereby assigned a pitot tube calibration factor Cp of 

0.841 

/';f r. 0 /f··JL~.-,•j<'7J 

C <'fi db , .;.·LJ.:..""-'"'"~t-e<·if,_. _:.:V:..'.:.[7V.fi"P.:.V_.:1:_Z.:.,·_· __ o __ ~_·_,;_ Chi 1e y.- Pers~nel (Signature/Date) Team Leader (Signature/Date) 

'This certification also applies to the specifications ofEPA Method 2, section10.L4.L I regmding inter-component 

spacing ofpitot tube-sampling probe assemblies. Refer to the figures on the reverse side of this page for specifics. 

ATC Fonn .37·Primary S-type Pilot Tube Calibrations~version 3.0 September 2007 ATC@ (800} 733-3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 

APPENDIX PAGE No. 662 
> 

"'< () 

" "' 0 

~ 

m 

<::1 

" ? 

-;o 

:l 

.. 

~ 

§ em (fl'TJ __,, 

>c; 

"'""' mc;;m 'Tlz;;: __,__,_ men"' 

s:J>.~ 

01 .. 0 

~""z - --1 

~cnrn 

~>"' or-< 1i)"<J "'"' co ,~ 

-<m 

'TJ() 

c;;..; 

" ..; "' 

!(; 

'TJ 

m 

" 0 x 

~ 

m 

2 

? 

"' !:!: 

Thermocouple Primary Calibration Data Form 

Calibration Date I 1 ~ 14~ () '1 

Ambient Temp., "F S'-1 c 

Technician ''1":-B. ' .,r 

Reference Source 

Point (Specify) 

Number 

1 Ambient Air 

2 lee Bath 

3 Thelco Oven 

---- -----------------------------

1 Reference thermometer-mercury in glass 

'Type of calibration system used 

Thermocouple Number )? l-f -~i--

Barometric Pressure, inches Hg 2 q, <; 1 

Reference Thermometer (List ID #)1 F "' 

Reference Thermocouple Tem

Temperature Potentiometer Diffe

"F Temperature, oF (calculate in 

5'1¢ Stt '' oct,

40P 

·~Q~ o.~·;.

)l 

-;; 9<) 6 "27f't} 0 :;l• 

..-' ·' 

------

------- -· 

--- . -

-------- -------~ 

"----"-- __ _,_:::.2_\g 

3=[(Ref Temp, C+273)- Test Temp., C + 273)1Ref Temp, C + 273]"100<1 .5% 

Kelvin= (519) • (F-32) + 273.1$ 

QA/QC Check 

Completeness v'Legibility_LAccuracy~pecifications___::::Reasonabteness 

/'-;/ - /7 

Checked by: d\t~,;r 6t.:'M1 • canoratlon TeFJinlcian 

(Signature/Date) 

A IC Form 209-Pr!mary Thermocouple CaliOratlon Record 

version 2.1 May 2009 

l'l-JI..J-IJ'I \A} 4JJ- f~ 

Test Team Leader 

(Signature/Date) 

F':\Work\AI! Forms-... t2090.Primary thermoGoup

ATC 
, 

c ~ , e: L m 0 -< z 0 ~ :1 .... N 

Gl em 

"'"" _., 

"n 

"'"""' m);m "1JZS:: 

-<-<-

mUJUJ 

m,.o ~"""~ "'"'z . -< 

NUJm ~ ):.Cil 

or--< 

u;, 

"'"' co 

::tJL 

--:m 

,o 

>"""' ~ 0> 

, 

, 

, 

m 

z 

0 

x 

, 

11 

rn 

z 

0 

0> 

0> 

'"' 

Thermocouple Primary Calibration Data Form 

Calibration Date ;2 -2;- Oy 

Ambient Temp., °F 59• 

.n T.i3. 

Reference Source2 

Point (Specify) 

Number 

i Ambient Air 

2 Ice Bath 

3 Thelco Oven 

1 Reference thermometer-mercury in glass 

2Type of calibration system used 

Thermocouple Number [/9 

Barometric Pressure, inches Hg ---=~~

2 '1. S I 

. ·-·-· ----- . -·------------· \------ .. , F] 

Reference Thermocouple Tem

Temperature Potentiometer Diffe

OF Temperature, °F (calculate in 

5'1" Sir ...\l3.1J"

2 'Jo 31° -0 jg_to"/

; 8o· li'20 - Q,_J.jlj <J

'=[(Ref Temp, C+273) ·Test Temp., C + 273)/RefTemp, C + 273]'100<1.5% 

Kelvin" (519) • (F-32) + 273.15 

QAJQC Check 

Compieteness_i Legibility · VAccuracy_LSpecifications /Reasonableness / 

Checked by: fk,,a-Cv::;;;en, 12-21·tJ7 

Calibration · · · 

(Signature/Date) 

ATC Form 209-Primary Thermocouple Calibration Record 

version 2.1 May 2009 

Test 

lJ t~P. 

Team Leader 

='2/w

(Signature/Date) 

F:\Work.\All Fonns-... 1.2090~Pfimary thermocouple Ca

ATC (BOO
BORAL BRICKS 

Analytical Testing Consultants, Inc. 

Primary Type S Pitot Tube Inspection Sheet 

,-~-r 

~~ U--~ U' 

" ' I L_~ 

Degree indic-.1ting levd position for determining 1,11 and u.2• 

Degree indicated level pmition for dctcm"rinin.g P1 and fu. 

Degree indicating level pusilion for 

determining of e. 

0 

-li· 1 .------- ,_____ <-( 

·'------------

"-! 

jL~~el ami Perpmdicular? 

Obstntction? 

-- -----------------·---~--

Damaged? 

a1 (-Iff :5;ai:S+lff) 

a, (-Iff :5 a,:':; +I If') 

r--

/JI (-$" :5: /JJ :5 +$") 

p, (-5' :5 p, :5: +5') .. 

y 

e 

Z=A tnn y (< 0.125 ") _____ ._ 

W=A tune (:5 0.03125") 

D, (3116" :5 D, :5 3/8 ,, --------- A 

------

A/2D, (1.05 :5;P ,.ID, :5: 1.50) 

If temperature sensor is flush with 

l!...itot tube oneni.nv. is Z >'4"? 

If temperature sensor i's set back. from 

y 

N 

il 

r 

;c 

I 0 

6 

0 

C) 

0 

6 

o. 37') ---

,1, J"('f 

j. t=/'2. 

y 

N 

-

·--

_p_j_tot tube opell!iJ:,~ W > 1"? ------~ 

J~- X?:. Y.t" fiJr Dn =!6" .L ! Degree:; indicating le"l'el position for detcm1ming "!then cakulaLe 

Z. Is impact side of pitot tube eveJJ with 

or above Itt! We entt:f.J!!p.ne? _)" _ __] 

QA/QCCheck Is Y?:. 3" for 3116" < Dt <3/8"? y 

Completet1ess V 

~- -- Legibl"Jity "-./ Acc.macy ;._/ Specifications ~ Reasonable-ness t_.../ 

Certification 

1 certlfy that the TypeS pitot tube/probe ID # 89a meets or exceeds all 

specifications, criteria and/or applicable design features_and is hereby assigned a pitot tube calibrailon factor Cp of 

0.841

. · .. ..¢ . . ·.. . .. -, 

d/'e.,i ,bc•AU.",n- I{--2 £; -o '1 !{.j (~~~ 12 ··if -o9 Certified by: ---L. "--L-"""-"-'-!-""':::.;71";;p;.-""''-'-L1...-'"-·-'---='---'- _ - . Pet·s~el (Signature/Dale) Team Lcaqcr (Signature/Date) 

1 Tills certification also applies to the specifications of EPA Method 2, section 10. L4.L 1 regarding U,.ter-component 

spacing ofpltot tube-san1pling probe assemblies. Refer to the figures on the reverse slde of this page for specifics. 

ATC F~.<rm 37hPrimat)' Shtypt:: Pi tot Tube Cu!ibrations-veuion 3.0 September 2007 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC@ (SOO) 733-3193 

APPENDIX PAGE No. 664 

I 

! 
)> 

c ~ -u ~ ~ m '1 z 0 ~ '= .. N 

Gl 

em 

"'" -;» l>o 

"'""' m);m -uzs: 

-<-;- mUlUl 

~,f:o~ 

m"'o "'"'z . -< 

NUlm 

~)>CI.l 

or-< 

(ji'O 

"'"' co ::o~ -<m ~'1 z 

-< 

"' 

)> 

'0 

'0 

m 

z 

0 

x ~ m 

z 

? 

"' "' "' 

Thermocouple Primary Calibration Data Form 

Calibration Date / Z -f 7 ~ 6 /' 

Ambient Temp., °F 6do 

Technician -r: S 

·-

Reference Source' 

Point (Specify) 

Number 

1 Ambient Air 

2 Ice Bath 

3 Thelco Oven 

1 Reference thermometer~mercury in glass 

2Type of calibration system used 

Thermocouple Number ?1 <'1. 

Barometric Pressure, inches Hg 2 '/ .. 51 

Reference Thermometer (List ID #) 1 t=.,.. ' ' 

Reference Thermocouple Tem

Temperature Potentiometer Diffe

'F Temperature, 'F (calculate I

cg~ 

. .J 60c - (:) l.c!

'10 {) 36~ 0 0 t,L

2'ftJ Q 2ST' o. S3

'=[(Ref Temp, C+273)- Test Temp., C + 273)/Ref Temp, C + 273].100<1.5% 

Kelvin= (5/9) • (F-32) + 273.15 

QAJQC Check 

Completeness / Legibility~Accuracy~Specifications~Reasonableness_::::

,r-.7 -?':1 

Checked by: ?~.-;/ t:Jt-v/.ft?.t !.2 ·/tf -t/1 

Calibration Technician 

(Signature/Date) 

ATC form 209-Primary Thermocouple Calibration Record 

version 2.1 May 2009 

't· 

kJ ~ P~ iz./

Test Team Leader 

(Signature/Date) 

F:\Work\Ail Forms· ... \2090·i>rimary thermocouple C

ATC (80
BORAL BRICKS 

Primary Module Calibration Calculation 

bate:r.n== 

Pbar. 

Calibrations by Mallory Beam 

Wet Test Mete( Sertal No.: 175$2 

Module ID:L-"=-'-l Prewtest Calibration Factor 0.963 

Orifice 

t.H~~~es 

0.5( 

1.0( 

1.5( 

2.00 

3.00 

4.00 

Orifice 

A.H (inches 

Vw,rt' 

Jnitlal 

109.41 

113.8: 

126.3: 

133.2' 

151.11 

161.1! 

I 

minutes 

Ending 

113.50 

119.56 

133.04 

i~ ~.4 

dH@1 

Vd, ft3 

tnitlaJ Ending 

;~~ 32911 

39.097 

46.070 52.957 

53.154 61.277 

71.585 81.618 

81.995 93.653 

1.781 0.975l 

Specifications. (QA Handbook~Vollll CD5·1, 9130/94) 

Tw, ~f 

Initial 

55 

55 

55 

55 

55 

551 

1) No value of .8.H@i shall vary from the average AH@ by more than 0.20. 

2) No value of Yl shatt vary from Yavg by more than 0.02. 

( li.H) 0.031961! I;+- r J' dH@~ ' 13.6 (t.+459.69)e 

~J + 459.69) L V,.P. . 

QNQC Ch~X:k 

Ending 

55 

55 

55 

55 

55 

55 

Td, ~F 

!nUl a! Ending 

57.0 57.0 

57.0 5JUl 

59.0 59.0 

59.0 60.0 

61.0 61.0 

61.0 61.0 

• 

/ 

Completeness __ ,_1_ 

Clleck.ed by: 

,~,.,-·· ( ;: v:::;::_r;~/1 /_d;o Reasonableness ___ _ 

Team Leader (Signature/Date} • 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 666 
BORAL BRICKS 

Primary Module Calibration Calculation 

Date· 

Pbar: 

Calibr a lions by: Mallory Beam 

Wei Test Meter Serial No.: 175$2 

Module 10: '-'-"''-=----' Pre-test Calibration Factor'---_o,.oc97"7'-----' 

Orifice 

~H (inches 

H20) 

0.50 

1.00 

1.50 

2.00 

3.00 

4.00 

Ormes 

.O.H (inches 

vw,te 

Initial Ending 

56.39 61.87 

62.43 70.24 

70.47 79.71 

79.91 90.93 

91.37 104.98 

105.16 120.86 

minutes dH@. 

2.084 

vd,te 

Initial Ending 

275.837 281.567 

282.149 290.294 

290.537 300.188 

300.391 311.915 

312.371 326.604 

326.792 343.233 

y, 

0.969J 

Specifications {QA HandbookNollll CDS..1, 9/30194) 

Tw, °F 

initial 

58 

58 

58 

58 

58 

58 

1} No value of .61-!@i shall vary from the average 6H@ by m<Jre than 0.20. 

2) No value o~~~:h~::(ro;. Y:v~:m)olrethan 0.0:. ~]' Y 

dH@ = --~----13.6 (t,, + 4)9.69 )e ; 

(t" +459.69J. V,,Pb 

QA/QC Check 

Check~ by. 

A.TC Fotm 34c.·P<Imary MocMe C•libr.alioo1 Recore! 

~e.·~WO\ 4.0 Hove1nbt!r 2001} 

Ending 

58 

58 

58 

58 

58 

58 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

I Td, 11F 

Initial Ending 

66.0 66.0 

66.0 66.0 

66.0 67.0 

67.0 68.0 

68.0 69.0 

69.0 70.0 

APPENDIX PAGE No. 667 
BORAL BRICKS 

PRIMARY MODULE CALIBRATION CALCULATION 

Module 1.0. ;-f r-::.:_ '-/ 

Barometric Pressure, P 2. c.? , 1 J ::J 

Pre·test Calibration Factor, v~l I .DJ 0 

Personn e 

Oat 

Wet Test Meter Selia! 

e 

i<C.F..-r (.;, C'-QG<.<, 

'2.- iO- .2 .;>; ... ) 

i 75-l z 

v. v, T. 

Final, 'F ~ Initial, 'F 

r, 

Orifice Setting 

Initial, ft3 FIMI, ft iai.ft,l Flnal, ft.l Initial, °F Final, ~F 

0.50 Z7.6~ I JlVi'l (1~'3. :J& I <;{.··· 36 ,' ~..,L. . ~ (.· r,.o (.,tJ &I &3 

1.00 3'f. 2<11 ]'t.tJ30 13>-3. 0/0 !Ski'-573 fPh v &o r:. 3 ks 

1.50 <f(}.IJ:;- 'fl. G<lo -&!3. t&-11o {i 75~ . .)-.zz._ t;o ;;_, 0 {.:) r.,·:t-

-:-

2.00 i-ffo•·"11"1 s~r. 'if3o 87<;,/3Z,;- b'i3 3. ·'I'R (,.D 40 (.,'f b'f 

3.00 -'"- 8'1'1 t,'( csO sil3. 6ZS !3'-73.2..4:;: &o {p() (:;y 7:? 

4.00 G'i. 'ibO Jr{. 131J t'/'13. t.-30 lt.fol/.37:> &~ (,0 72 7'-f 

Speclflcatlons {QA Handbook-Volllt CDS-1 9130/94) 

1) No value of ilH@! shall vary from the average llH@ by more thom 0.20 

~ ~:~· TIME 

~ Y; 

2) No value of Y1 shall vary from the average Y by mor£J than 0.02. ng min. 

' 

I 

I 

0.03191lli ( P,+--- ~H) 2 

dH@ _ 13.6 [ (t, +459.69)0] 

Va + 459.69) VwP, .. 

Y; VwPJtd +459.69) -

-

vd(pb+ ~)tw +459.69) 

legend 

Vw =Volume of WetTest Meter. fe 

Vd = Volume of Dry Gas Meter, rf 

Tw =Temperature of Wet Test Meter, °F 

Td::: Temperature of Dry Gas Meter, °F 

6.H@i = Pressure differentia! across the orifce meter, lr'l. !i.O 

Yi = Drj Gas Meter Calibration Coefficient, dirnenstonless 

0.50 /() I, 770 

1.00 /0 /. 67i} 

1.50 !0 i.tlas 

2.00 jO ;z.. Cll (, 

3.00 (() 7-t:<J§ 

4.00 /0 ;z.o6o 

I I qt;l 

Ccmpleteness lsgibilily /- . Accuracy Spe.cificafions 

•/ .1,/..j'j - .·\tt•·( ( ~~t.{IJU.i<·l 2 -I 0 .:_' i_cc'·-' -- [

' . ' ' ("' [) 

.A ) • ~- t't.N•<-·-

Signaturw: Technician (Signat\Jre/Date) Project Manager {S!gnatu:e/DEte) 

f, 0()'2-

!) . '?CJ::l 

t!.q<J<;" 

(1. 9'9</ 

o.'ro/Z 

0 .ql?l"f 

II o. qq,-1 

/ 

v 

Reasonableness 

ATC Fonn 34·f'rimary r.md!?.e CaHOr3tl<ul Record 

version 3.1 May 20(;5 

F:\Wgr'~\An !"QfOIS·Flekl D<1lll ~-Calc FD!!llUi:se .. J34·Pri~ Mcdule C~~b..">16on Rueord Slaii",qpH 

ATC (000) 73J-:3t93 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 669 
BORAL BRICKS 

PRIMARY MODULE CALIBRATION CALCULATION 

Orifice Setting v. v, 

Initial, ft! F(n.al, tt' Initial, tt' Fi11al, ft3 

0.50 ~n~ ~~~-'\;:}o w9nst 76/.ciJ3 

1.00 ~~.a11\ wn. OiO J::J. rf7S 7ut{.lJI7 

1.50 ~\lf.J\o ~Jf.ll3~ []vz. H"'ilb 'rl;t;H)!o 

2.00 at..'7tc 'fJ>J. no l7ts-_q'\5 i7Jt.llll'l 

3.00 ~3'5.<.1.o S'ID~tl 7iJI/.4t"i' !735. '/i).<;' 

4.00 rb%- 730 1\)]. 73~ 735:757 il/7. [.ilo 

Specifications (QA Handboak-Vollll C05-1 9130/94) 

i] No va\tle of AH@i shall vary from !he average li.H~ by more then 0.20 

2) No value of Y; shail var-; from !he average Y by more than o.a2. 

dH@ 

0 0319AH[P, + ~:) [ 0. :45969)e i 

&d +459.69J VwP• 

Y. I 

- vw~(td +459.69) -

V,{Pb+ ~-}tw +459.69) 13.6 

Legend 

Vw =Volume of Wet Test Meter, fe 

Vd =Volume of Dry Gas Meter, ff 

Tw::: Temperature of Wet Test Meter, °F 

Td::::: Temperature of Dry Gas Meter, °F 

Personne~l Rtii{iiJ\ii. 

Date J J JJ~IJJ. ¢1.'0 lO 

Wet Test Meter Serial oil /75'/o :J 

r. r, 

lniJJa.l, Dp Final, ~F' lniti'lll, "F Fin:~!,~ 

7ff 97 ;o;;L tn·z. ' LJ 'l 'i9 JO) JDll 

9"'1 I '1 l o'-1 1 o')~ 

tfln I 'DO 105' !D7 

100 loo \0( \09 

)()i) tllO [O'i \\0 

Orifice 

c:J~ Y, 

Sctdng 

. 

0.50 10 If o ?,/o 0. <ii21 

1.00 )f) '\. ,[\<\ D.q&D 

1.50 il! \.lS) In CJT7 

2.00 tn tl11 I fl c1 I r/1 

3.00 fO 1- 7'70 o.%5 

4.00 !0 J /. fDJ. {),q~')' 

I !l!Jiw I o,q-p 

II Pf\-55 

.6.H@i = Pressure differential across the orlfce meter, in.I}O 

Y1 =' Dry Gas Meter Calibration Coefficient, dimensionless 

Q,.'\/QCChy· 

Cnmpletene!ls 

ATC Form 34-Prim;;~;y Module CalitraliOn Record 

version~- t May 20o."lS 

ATC PROJECT No. P-1 0142 

Reasonableness 

7/t/1~ Project Manager {Signature/Dale} 

F.IWorkWI Ftom•-Fleld Data St-eels, Calc f~rmulae ... 13~·Prinulry W"'dule: Cal!tn;ion R ~COfd Slarit tW<f 

A'fC (SOO) 7.l3-3193 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 670 
BORAL BRICKS 

Primary Module Calibration Calculation 

Date: Calibrations by: Kirkman 

Pbar. Wet Test Meter Serial No.: 17562 

MOdule 10:'---"="'--' Pre-test Calibration FactorL__,"o"'.9""99~8'--..J 

Orifice Vw.te Vd, re Tw,°F Td, °F 

AH~~n~~GS Initial Ending Jnltlal Ending Initial Ending Initial Ending 

0.5( 808.61 8129? 701.772 9t 99 102.( 103.( 

1.( 813.22 819.01 702.075 7( 1.01 1 104.0 

1 119. 826.4: 7' 

2.( 

3.( 135 

126. 834.9: 

7. 

715. 

~4. 15 

\5 

7: 

7: 

;.425 

~ 1 

1 ~ )7 109. 

4.0 1145.7. 857.3< 7 !5. 27 7 >7.84( 10( 100 1o\l:c 110.( 

Orifice minutes dH@; Vt 

1.766 0.9721 

Speclflcatloru;. (QA Handbook-Val ill CDS-1, 9/36194) 

1) No value of fiH@i shall vary from the average AH@ by more than 0.20. 

2) No value of Yl shall vary from Yavg by more than 0.02. 

0.0319Llli(P,+ l'lH) ' ~- VJ~(t" +459.69) dH@= l3.6 (tw+459.69}e ; - Ml 

Vd+459.69) [ V.P, J . Va(Pb+-)(tw+459.69) 

QAIQG Check 

. .1\.TC Fcr.n 34e-Pr~tngry MOdule Ca!ibrallon Record 

\8!<IC>O l_ij Novernller 2009 

ATC PROJECT No. P-10142 

1 13.6 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

ATC(800j73H193 

APPENDIX PAGE No. 671 
BORAL BRICKS 

PRIMARY MODULE CALIBRATION CALCULATION 

Module I.D /J"T ,.-: b Personne - rff {i~r::c.o...~ 

Barometric Pressure, P Z 8 ""1 3 sPre-test Calibration Factor, Y~l [) /fl(, 

Date I 2 -~tO· :;zotd 

Wet Test Meter Serial •·1 bd,,f,,d,E.~==dl 

Orifice Setting v. v, 

lnHial, te Final, fil lnltlal, ftl Flnal,te 

0.50 £!;0.(,2.0 !N.S'i'l 3q'),JI,<; 35.::1. 7(,'! 

1.00 6>/.'fB<I qo. </L2 35•('-.30 35'77?4 

1.50 o/0. 760 '17.4-60 36tl12'r 3-·',/;,8$1} 

2.00 q7510 !tJ'I. 870 367110 37'/.7'{8 

3.00 /o.5~ z.;;o l!t'l 1'/o 375:/'ls- 36</.,?t.C 

4.CO 1/'1'. 'fBo J;t-/.Bo5 3cN·b7o _?<J>; 3''5 . SpecJtiC:atlons (QA Handbool<.Vol 1!1 CD5·1 9"/30194) 

1) No va;lue of AH@i shall vary from the average ll.H@ by more than 020 

2) No value of '11 shall vary fium the average Y by mote than 0.02 

( Mi) 0.0319Mi P,+-- ' 

dH@=---L n.6 [(t,.+459.69)e] 

f!a +459.~ V,.P, 

yi - VwPb (t d + 459.69) -

vd(pb+ ~)iw +459.69) 

Legend 

Vw::: Volume of Wet Test Meter, tf 

Vd :::; Volume of Dry Gas Meter, ff 

Tw::: Temperature of Wet Test Meter, °F 

Td = Temperature of Dry Gas Meter, I)F 

Initial, 3

F 

Go 

r:o 

{:;(} 

{;0 

60 

&0 

Orifice 

Settlng 

0.50 

1.00 

1.50 

2.00 

3.00 

4.00 

ll.H@i = Pressure differential across the orifce meter, ln. 110 

Y1::: Dry Gas Meter Calibration Coefficient, dimensionless 

/ 

Completeness Accuracy 

r. T, 

r!nal, QF lnitiai,"F Final,~ 

c,o &o .f, z_ 

iS&' r;, z (_. 3 

(,() ~3 6'( 

6:,0 6•1 ~b 

{;.0 &{, :;; 

(o.O (, '7 t.!J 

TIME ll.H@I Y, 

min. 

/0 J.t:Js<: o.qe;; 

It' /.Cf3? o.c;gz 

fO -;z. c:?8 o.1M3 

!0 J. ·lOb tO. qb8 

[0 :J...N'> o.qJ'I 

iO :J..N/ 0·17<; 

lz.o.?s-~ Cl.'775l 

II II 

Legibility specifications Reasonableness 

~'LI-='G"":"'~·,{L":. ~"'"---',:"'-~~"-=l"""''l'-"!..:::c.i'--- {,.). kV\- f1.,,J.-~ z p., /; 0 

sign;;!!ures: Technlc!an (Signamre!Dete) 

ATC Fctm 34-Primary Modur,:~ Calibration Re~:ocd 

~'{!tsiU'l 5.1 May 2C<l6 

Project Man01ger (Signature!Oa:e) 

F:\WOI~V'.tl f~s-i"i~rd O.;ta.Shee!S. Cali: Formulae.. .. '.!l4--Pr~nal)' ~100\JJe Calillro.G~n RllCOid Blanl<_qp\Y 

ATC (000) 733·3193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5. SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 672 
BORAL BRICKS 

PRIMARY MODULE CALIBRATION CALCULATION 

Module 1.0 A·r -:: b Personn e ll~Nr L ;.J. C<.O_f2._ 

Barometric Pressure, P j Z 8 - -1 3 s-' 

Prevtest Calibration Factor, Y~l [) /f9'b 

Oat 

Wet Test Meter Serial 

e 2 -JO -· ::ZO! ,_) 

I 

Oriflc-e Setting v. v, 

Initial, ft3 Final, ftl lnitial,te Finai, tt' lnitlaf, DF 

0.50 BIJ, &20 fNS'i1 3'/'i.tb<' .3:>.3, 7/A t;,o 

1.00 M-98'1 C[IJ. 'IL?. 35•/.?.30 3<;'?.77<1 &o 

1.50 'fa 760 11. J.-60 360.125- 3t.~r...85""8 6(} 

2.00 q7510 1/J'I 8}0 367110 :J7i.J'1E (:,0 

3.00 tos:z60 I !!<I /"Jo 37.'>-1'15 39•/.:;:bt 60 

4,00 II'{ '(/3o !.P/.Bo'S l.::?ii'/ "n _<:tW3os (;,D 

'" Specifications 00 - 0 . ' {QA H db k v 1111 cos 1 9/30/94) 

1) No value or t.H@! shall \lary from the averaga lt.H@ by more lhan 0.20 Orifice 

2) No \lalue ofY1a-hall vary from the average Y by more than 0.02. I Setting 

( Mf) 0.50 

0.0319Mf P, +- _ ' 

dH@!.= 13.6 [(t,.+4)9.69)e] 1.00 

~· Va +459.69) V,.P, 1,50 

VwPb(td + 459.69) 

2.00 

yi 3.00 --

v{Pb+ ~~)tw + 459.69) 

4.00 

. 

Legend 

Vvv =Volume of Wet Test Meter, ft3 

Vd = Volume of Dry Gas Meter, ff 

Tw = Temperature of Wet Test Meter, °F 

Td = Temperature of Dry Gas Mete1·, °F 

llH@i:: Pressure differential across the orifce meter, in. }10 

Y1;; Dry Gas Meter Cal!bratlon Coefficient, dimensionless 

OAJQC Chep-1(: 

./ / ·' 

Completeness lagibl!ity 

x~~Ji C:t4~" 7/lt:'/ /{.) 

/ 

Accuracy l I ;.,_/, 

I t.. 7 s--~, z.. I 

r. r, 

Final, "F Initial, '"F F~naf, °F 

c;.o (,,o f .. , '(.:.. 

hi? L1 ;:__ 63 

r;,o ~3 61 

6;,0 (,'{ &.~~ 

r;.o r;_.(, {,j 

(.,0 0'7 It: e 

TIME AH@i 

min .. c:J 

/{) l85<; o-'hor 

/0 /."131 t)-9§Z 

;o 2- c.?t} t1-'1M3 

!0 J.. rot;. I!J, qt·8 

{0 :;;..N<: o."!J'I 

lo J.. i'll o.qJS: 

lz.o.<:d O-'t7il 

II 

Specifications Reasonableness 

Signa\ures: Technlc!an (Signature/Date} Project Manager {SlgnaturetDate} 

AlC Form 34-Primary Morlula Calibfali~;~o'l Rw.:cn:l 

~<etslro 3.1 M~y zc-os 

f:l~"\lorkl/1~ Fu•=·Ft~ld Oal.;l Shee~. C~lc ForrroU~e....\3.1;-Prlmij<y Moduli! Calibr.lti0t1 RSI;;Ofd Blank.QPIV 

ATC (600) 13-3-3-193 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 673 
BORAL BRICKS 

Report on Calibration of Field Barometers 

The following barometers were calibrated: 

By: Keith Poole 

Date: August 27, 2010 

Barometer ID 

ATC#l .. 

ATC#2 

Pre-Calibration Reading 

:J-9- 3f5 

·';A ~- '3 3 

Adjustment Needed 

--·u.o'j) 

- o. a'-f{ 

----- ATC#3 I {"\;), iW'(;\ub k ------------ -j ATC#4 dv Of.5Y -O-J.)(; I 

! I I Barometer adjusted to reading obtained from National Weather Service website. Reading j 

adjusted for elevation of 835 ft. 

L------------------~ational Weathe1· Service Barometer reading, actual = I 30.12 

1---_E!~vation Ad'ustment (ATC Office=835 ft., NWS elevation=836 ft). 

Adjusted Station Pressure for correction of A TC Barometers 

-0.835 

29.285 

ATC Form 53-Barometer Calibrations 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

vefsion l.l February 2007 

Analytical Testing Consultants, Inc. 

(800) 733-3193 

APPENDIX PAGE No. 674 
~ -u 

e "' 

m 

0 

-; 

z 

? ~ :: 

.... 

"' 

)> 

c 

Glm C-u 

~)> 

l>(j 

rn""' mS::m 

-uzs: 

-<-;- mrn<f> 

;g:.f>-22 ro..,o 

~c.nz 

. -; "'rnm 

~;p.cn 

or--< 

(jj'U 

co "'"' 

-<m "'~ 

.,o s;"" ~ "' 

)> 

-u 

-u 

m 

z 

0 

x 

;! 

Gl 

m 

z 

0 

"' ~ "' 

Dare 

717/2009 

817/2009 

9118/2009 

10/12/2009 

11112/2009 

12/23/2009 

1/512010 

2/212010 

41812010 

6/28/2010 

8127/2010 

I 

! Date 

717/2009 

8nl20o9 

9/18/2009 

10/1212009 

11/1212009 

12123/2009 

11512010 

212/2010 

4/812010 

6128/2010 

8/27/2010 

Calibration of ATC Field Barometers 1 

Barometer #1 Barometer #2 

Station Barometer Adjustment Pressure, in. Reading. in. Technician 

Hg Hg Needed 

Station Barometer AdJ

Date Pressure, in. Reading, in. 

Hg Hg N

29.005 29.000 0.005 Childers, K 7nl2009 29.005 29.150 

29,356 29.480 0.125 Childers, K 8n12009 29.355 29.300 

29.305 29.320 O.G15 Childers. K 9/18/2009 29.305 29.380 

29.385 29.340 O.G45 Burgess, T 10/1212009 29.385 29.440 

29.035 29.100 0.065 Burgess, T 29.035 

29.455 29.430 0.025 Burgess, 'T 1212312009 29.455 29.490 

29.175 29.200 0.025 Burgass, T 115/2010 29.175 29.190 

29.275 29.200 0.075 Burgess, T 212/2010 29.275 29.180 

29.035 29.020 0.015 Burgess, T 4/8/2010 29.035 29.200 

29.035 29.000 0.035 Burgess, T 6/2812010 29.035 29.020 

29.285 29.380 0.095 812712010 

----- ------------ ---- -~---- --·-~ _P~I~IS: ----------··· -- ~--~9.285 ---. 29.330 --

UOIVUit:C.O:H fro) Barometer #4 

Station Barometer Adjustment Pressure, in. Reading, in. Technician Station Barometer Adju

Dare Pressure, in. Reading, in. Hg Hg 

29.005 29.150 

29.355 29.500 

Z9.305 29.400 

29.385 29.500 

29.035 29.060 

29.455 29.510 

29.175 29.290 

29.275 29.300 

29.036 29.150 

29.035 29.050 

29.285 n1a 

Needed 

0.145 

0.14S 

0.095 

0.115 

0.025 

0.055 

0.115 

O.Q25 

0.115 

0.015 

Childers. K 

Childers, K 

Childers, K 

Burgess, T 

Burgess, T 

Burgess. T 

Burgess, T 

Burgess. T 

Burgess~ T 4/8/2010 

Burgess, T 6/28/2010 

8127/2010 

Shop Eleva1ion = 

Charlotte-Douglas Airport Elevation= 

' Data provided by NOAA National Weather 

Service for Charlotte-Douglas Airport. 

Hg 

29.035 

29.035 

29.285 

835 

836 

Hg Ne

29.210 

28.070 

29.540 
BORAL BRICKS 

Precision Weighing 

1949 Evans Road 

Cary, North Carolina 27513 

Phone: (919) 678-0077 * Fax: (919) 678-0075 

Email: pweighing@aol.com 

BALANCE CERTIFICATE OF CALIBRATION 

Calibration Date: 

Balance ID #: 

Dept: 

W#fit! 

lfjtl 

Calibration due date: .4vr/( 

Type/Model: Preafa J.t8ff . I . ' '--«;fr 

Weight set ID# 

. ,Pt,{tz, P/7-l/ 

·----== 

Room Number: 

NIST Test Number 

1~'7!7111./tJ:..·l:.'/ifJ 

h - ItA-"· f)!) 

' ''/ ' 

g!i In . I . 

Cal Date 

&ifJf'Ul'l 

SOP: 2000 Rev L JTolerance +/· : 0.1% 

Cal Due 

IA'"ll) 

-........ 

B"ef'ore CalibJcatlon Readings: d After Calibration Readings: 

In Tolerance: In Tolerance: 

Out of Tolerance: 0 

0 

Out of Tolerance: 

N/A: N/A: 

Co!:'jments: 

This certifies that the balance listed above has been serviced and calibrated to manufacturer 

specifications and/or Precision Weighing Standard Operating Procedures with weights traceable 

to the National Institute of Standards and Technology (NIST). 

Oate of Service 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Customer Signature (Review) 

Dale of Review 

APPENDIX PAGE No. 676 
BORAL BRICKS 

Contractor: Precision Weighing Inc 

1949 Evans Rd 

Ca_!)', NC 27513-2041 

Purchase Order II: 10JCI 

Client: Precision Weighing Inc 

Address: 1949 Evans Rd 

City & State: Cary, NC 27513 

Date Received: 25 NOV 2009 

Date Calibrated: 01 DEC 2009 

Temperature Ranga: 20.91 to 21.40 ·c 

Pressure Range: 720.8 l<l 722.6 mmHg 

Relative Humidity Range: 50% 

AirOensfty: 1.1312 to 1.1358 mg/cm~ 

Traceable Report#: 1575793 

NIST Certificate#: 8221272801-06 8221274081-08 

Tested By: 12 

Procedure: Modified Substitution {WI05-0023l 

Contractor Req Rl3cal! Data: 12131/2010 

Primary Standard Calibration Date: 111031{)6 Due: 11/03110 

Description of Weights: 1mg·100g Polished Kil. Class "1~, S/N F824 

Allkl1.1gh \hen! are two NISi numbe~. 

rJJ'le 01 both m.11y apply 

~onventlonal Mass Corr. Unc. 

Nnminal 

V.:!ue Ia. 

1 mg 

2 mg 

2 mg 

5 mg 

10 mg 

20 mg 

20 mg 

50 mg 

100 mg 

200 mg 

200 mg 

500 mg 

1 g 

2 g 

2 g 

5 g 

10 g 

20 g 

20 g 

50 g 

100 g 

Prep;:; red By: 

;htte'i&C~~~~~ 

!RiiCE I!I.AKIE v .. -~ICt-::r-.:c, ~y~rEMS 

t:orMJnnem Be;·or.d Mt'ttillJ~fil!'Jtt~ 

As Found 

(mg) 

0.00229 

0.00194 

0.00354 

0.00392 

0.0001 

0.0037 

0.0052 

0.0005 

0.0081 

-0.0009 

-0.0011 

0.0016 

0.0035 

0.0150 

0.0111 

-0.0166 

0.0129 

-0.002 

0.011 

-0.056 

-0.006 

230 Wes~ Co!o'll;::n .S!reo?l • Rice Lr.ke, '~N[ 5•!668 •lJSi; 

TEL: f 16-20-J.-Dl.~ 1 " FAX: -;:·15-23<l-6S'IJ7 

As Left K•2 Tol. 

(mg) (mg) (mg) 

0.00229 0.00078 0.010 

0.0(}194 0.00066 0.010 

0.00354 0.00066 0.010 

0.00392 0.00097 0.010 

0.0001 0.0013 0.010 

0.0037 0.0012 0.010 

0.0052 0.0012 0.010 

0.0005 0.0014 0.010 

0.0081 0.0015 0.010 

-0.0009 0.0014 0.010 

-0.0011 0.0014 0.010 

0.0016 0.0017 0.010 

0.0035 0.0026 0.034 

0.0150 0.0027 0.034 

0.0111 0.0027 0.034 

-0.0166 0.0053 0.034 

. 0.0129 0.0099 0.050 

-0.002 0.010 0.074 

0.011 0.010 0.074 

-0.056 0.021 0.12 

·0.006 0.034 0.25 

Page 1 of 1 Page 

r ' I r, Y, "J_:- r ! [/ 1-

( . ' 

Standafd Set Used Assumed 

Balance Cafibrated/due Density 

Used MM·DO-YYIMM-DD·YY (glcm') 

5010 K5940 11-20-09/02·19·1 0 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09/02·19-10 7.95 

5010 K594Q 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09102-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09102-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K594Q 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

5010 K594Q 11·20-09/02-19-1 0 7.95 

5010 K594Q 11-20-09/02-19-10 7.95 

5010 K594Q 11-20-09/02-19-10 7.95 

5010 K5940 11-20-09/02-19-10 7.95 

6760 K5940 11-20-09/02-19-10 "1.95 

6760 K5940 11-20-09/02-19-10 7.95 

6760 K5940 11-20-09/02-19-10 7.95 

1i83Q K5940 11-20-09102-19-10 7.95 

1183Q K594Q 11-20-09/02-19-10 7.95 

9(lted 01 DEC 2009 ' \ (\ \! to .. _... V. · ~ lj ...... % y,..~ Dan Demers. M:irologist 

Ti1:s rt;po:l ;!, •·-ot kl 01~ •• s:l.i to cia~~~ pr>J:~,:;:;: er ... i,11't>f:\fl'l<tnt by Ri~ Lah!! 'i'li'·g~·~::•~ .S/>t;;:r;-.;, C• <Jntage!',Gy t') t!i::, U.S. G0-,;s;nmer.t. 

ATC PRoJ~Cf'N~!.'F~':i'il1~4f'1 bofrtK~rx;J~te~d- ~~~~;,~,~~ EiJISJts 1bN''fE'~iPPRbJ~~~f Lc~~; ··N;;irt·M>< s:,-•i\£:'n~-k~~~1~'6T~bPA~:~ No. 677 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 201 0 
Contractor: 

Purchase Order#; 

Client; 

Address~ 

Ci!y & Stata: 

Date Received: 

Date Calibrated: 

Temperatura Range: 

Pressure Range: 

Relative Humidity Range-: 

Air Density: 

Traceable Report#: 

NIST Certificate I: 

Testad By: 

Procedure: 

Contractor Req li:eca/1 Date: 

Prlmary Standard Calibration Date: 

Description of Weights: 

A.lthO(.lgh t,"lere are Lwo N!ST numbers, 

one or OO!h rna-J appry. 

Precision Weighing Inc 

1949 Evans Rd 

Cary, NC 27513-2041 

10301 

Precision Weighing Inc 

1949 Evans Rd 

Cary, NC 27513 

25 NOV2009 

01 DEC 2009 

20.95"' 2145 ·c 

?20. 7 to 721.2 mmHg 

50 % 

1.1309!Q 1.1~27 rngtcm3 

1575793A 

822/272801-06 822!274081-06 

12 

Modmed Subs•Jtuiion (WJ05-0023) 

12!31/2010 

11/03106 Due: 11/03110 

100g-5kg Satln Finis/1. Kit, Class "1", SIN F822 

Conventional M~ss Corr. Unc. Standard Set Used Assumed 

Nominal 

Value I d. 

100 g 

200 9 

200 9 

500 g 

1 kg 

2 kg 

2 kg 

5 kg 

P~ep::-.::ed 8y: 

--

RifCE LAKEr W~_IGHINC S\~STF.M$ 

C(l(Ml.i;nM?Jl> lb.i~:lli Mca.~nrcmem· 

As Found 

(mg) 

.0.057 

0.228 

-0.161 

0.303 

0.17 

-0.53 

1.87 

2.3 

TE::...: ?15-2J·J·9~ r1 • Fr-\X· 715-234-69(17 

As Left K=2 Tot. Balance CalibratedJdue Density 

(mg) (mg) (mg) Usad MM·DD·YYIMM·DD·YY (g/cm') 

-0.057 

"' 0.034 0.25 11830 K594Q 11·20-09/02-19-10 

0.228 

"' 0.064 0.50 619Q K5940 11-20-09/02·19-1 0 

·0.161 * 0.064 0.50 619Q K594Q 11·20.09/02-19-1 0 

0.303 a 0.091 1.2 6190 K594Q 11·20-09/02-19-1 0 

0.17 a 0.15 2.5 6190 K5940 11·20-09/02-19-1 0 

·0.53 * 0.71 5.0 9750 K5940 11·20-09/02-19-1 0 

1.87 

" 0.71 5.0 975Q K594Q 11·20-09/02·1 9-10 

2.3 * 1.0 12 9750 K594Q 11-20-09/02·19-1 0 

Page 1 of 1 Page i;iated 01 DEC 2009 

* Although this lest weight has beenlesled lor the 

tolerance of the Cia~s fo' which it was s:;t.mitted. H 

does r.ot rnee1 .:::!! lhe reauirements for\hat class. 

; ' C\ ··r..J<::'-·""-~ 4-.,• !?~--~ Dan Oe:r.&rs MltrolOg!st 

7.84 

7.84 

7.84 

7.84 

7.84 

7.84 

7.84 

7.84 

lh!s r:;;i>~~11s no~ !o b<Ol ;.rs~i J'j ,%;r~t oroG.Jct cmlcr~rn,or:t r_,,. Rir;e l,<:t<-.e W-?.igl1ir;g s:.-st~M>= or !lf1/ <>ge:1(;t otl!;e U.S. C'io'<':'rr~l\l.<ftL .ii;:s dt~...::urner,t sr.al! ~:Ot t;a rc:prcducc-cl. e<Gtl}! lll f.]!, wftXut :t;-o; •:.tl!t~n ap,)<·.Jva:' of Fl:.;:f< L;,k:: 'Ni:•Qhi;>J S~'St.e:-;•s' M,;;tr·~'~C9J." Lab~retor~;. 

ATC PROJECT No. P·1 014~)& e.bcvn .,~~;certa:..~ty ~X f'Ct~Etm~~ltf~ff~t~rpworrt't'f~ped:t ~ i·;a."V.1fing a:ld vs&APPENDIX PAGE No. If~;:, a:c.e 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 
BORAL BRICKS 

Precision Weighing 

1949 .Evans Road 

Cary, North Carolina 27513 

PJ10nc: (919) 678-0077 *fax: (919) 678-0075 

Email~ pweighing@aol.com 

Weight Set Verification Certificate 

cneflt_-_, 

Analytical TestiOg Consultants 

-r;,.;,_rita~_t:t .. , Keith Poole 

:';-:i~e;paftm.en:ft ,:-.; 

Lab 

Dfi):S_cliP.tli>n~ 

Class 1 weights 

'Wi>.i9htlO#: 

See below 

!Verification Date: 19-Apr-10 !verification Due Date: Apr-11 

CaUimHIOD SO~ Metr-ology 2190 

StamJard s) Used 

Class I wei ht set 

Precisa balance model 303A 

Comme11ts: 

ID 

F822, F824 

43108 

Ex imlion Date 

Dee-10 

A r-11 

Readings of welght(s) taken on balance(s) listed after balance(s) calibrated with NIST traceable weight sel{s) noted. 

T~ellnicianm~te: 

19-Api·-IO, 

ATC PROJECT No. P-10142 

Cusrumer.: 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 679 
BORAL BRICKS 

ISO 

17025 Thermo fisher lf.OiliOllll Certlfj~~~l,3.01 

SCIENTIFIC Thermometer Calibration Report In serving sdet'lte 

This Is to certify that the Instrument described below has been examined and tested by dlrect measurement of generated temperatures in our· 

calibration laboratory using high precision temperature calibraflon equipment. The calibration methods used are based on the technical 

Information contained in NIST Technical note 1265, "Guldellnes for Realizing the International Temperature Scale of 1990 (ITS·90)" and NIST 

Special Publlcallon 250-23, ~uquld In Glass Thermometer Calibration Services". This calibration meets the requirements of the ISO 9001 series 

of quality standards. 

Instrument Description 

Serial Number: 1548 

Product: 1 005-BFC-BF 

Results of Physical Examination 

Inscription: 1 0058-BF 

Scale Range: -1 TO 101 

Immersion: TOTAL 

Scale Divisions: 0.2 Units: oc 

This InstrUment has been examfned under a polariscope for strains In the glass. If any, were fudged to be minimal and of no detriment to the 

functionality of the Instrument. 

The capilfar; of this thennometer has been examined under magnification and no foreign material, moisture, or other evldence of 

contamination were discovered. No discernible capillary irregularities were noted. 

Upon completion of physical examination, it has bean determined the instrument is In good working order and is therefore suitable for 

calibration. 

Calibration Results Unless othetwfse noted1 these results are considered "as found" and "as left", 

Results In Target Test Actual Test Reading Of This Emergent Column System 

Engineering Units: oc Temperature Temperature Instrument Correction Temperature Uncertainty 

0.00 0.000 0.000 0.000 NA 0.0277 

20.00 19.998 20.000 ·0.002 NA 0.0267 

40.00 40.002 40.000 0.002 NA 0.0267 

60.00 59.991 60.040 ·0.049 NA 0.0267 

80.00 80.007 80.100 ·0.093 NA 0.0267 

100.00 100.001 100.200 -0.199 NA 0.0357 

"'"'IMPORTANT NOTE: If no sign Is given on the correction, the true temperature Is higher then the indicated temperature. If the sign given Is 

negative, the true temperatura Is lower than the Indicated temperature. 

The estimated system uncertainties as stated above (k = 2) were determined In accordance with the guldeUnes given In NIST Publica1ion IR 

5341, take ln1o account the type or thennometer tested, the precision with which Its reading can be resolVed, and the degree of confidence one 

can have In its Indications under similar conditions of usage. 

For further discussion of accuracies attainable with such thermometers, see NIST Special Publication 250-23 and NIST Publication IR 5341. 

The caUbralion performed and documented by this report of test is a full scale calibration and no !Imitations of use are Imposed on this inslrument. 

The Instrument mentioned In this report was tested In accordance with Barnstead International procedure number CPM105 which is based upon 

standard test method ASTM E-77 and N.I.S.T. Special Publication SP250-23 

Traceability Information 

The measurement standards used in thts calibration are given below: 

Test Point: 0.00 Model No. Serial Numbe~ Description 

2563 A36152 Thermister Meter 

5640 

N/A 

Test Point: 20.00 Mode! No. 

1590 

5699 

7007 

Page 1of2 

ATC PROJECT No. P-10142 

1047 

N/A 

Serial Number 

A27184 

1476 

A33016 

2555 Kerpar Blvd Oubt~que. lA 

52001 

Thermister 

Ice Bath 

Description 

PRT Thermometer 

PRT 

Calibration Bath 

(563)556-1241 

{563}58~0516 fax 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

Recall Date 

11/4/2009 

11/4/2009 

Recall Date 

3/20/2009 

11/4/2009 

RECEIVED 

FEB 1 0 2009 

BY: ~-n<f Calibration Traceability No.: 1282719442 

w.vw.t!\ermofisher.tllm 

Rlrm No,: CC-300 

Revls!on: 10{05 

APPENDIX PAGE No. 680 
Test Point: 

Test Point: 

40.00 

60.00 

80.00 

100.00 

Model No. 

5680 

7007 

Model No. 

1590 

5628 

6054 

BORAL BRICKS 

Serial Number 

1475 

A33017 

Serial Number 

A27184 

1477 

A33014 

Description Recall Date 

PRT 11/4/2009 

Calibration Bath 

Descriotion Recall Date 

PRT Thermometer 3120/2009 

PRT 11/4/2009 

Calibration Bath 

The results Indicated in this report relate only to the item{s) calibrated. If addltlonallnfonnatlon regarding this calibration Is required, please 

contact this laboratory. 

Results of this calibration are traceable to NIST. 

Appoved 

. By. 

~u~ Jeff Welly 

Quanty Operations Manager 

Calibration Date: 01126/2009 

Calibration Due: Not Defined 

Batch No.: M714760 

This certificate may not be reproduCfJd except In run without the written approval of Barnstead International. 

Page 2 of 2 

ATC PROJECT No. P-10142 

End Of Report 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

RECEIVED 

BY: FEBG~ tf __ 

Calibration Traceability No.: 1282719442 

Form No.: CC-300 

Revision: 10/0S 

APPENDIX PAGE No. 681 
84/08/2618 11:05 7049829705 ST D GAS METER 

BORAL BRICKS 

ST A.l'IDARD GAS METER SALES AM> REP AIR INC 

537 WEST MAIN ST 

POBOX273 

ALBEMARLE NC 28001 

704-982-%01 FAX 704-982-9705 

stlmdardgllll@windsmam.net 

PAGE !'Jl 

To: Analytical Tming 

Keith Poole 

03-10.10 

704-932.0570 

Te§ting and Calibration: American Wet Teat Meter AL19#17562 

Conditions: 69F, l.S"WC, Barometric P..-ure 31).1" 

Meter w1111 preclflely 

removed from the wat~ 

leveled, t:hecked for lealu and proper operation. A foreign objttct wu 

and the minbcus gauge adjusted 

reservoir. Calibration was efl'eeted at the termination off"ln cycles 

aecordl.!lgiy. 

Calibrated on RW Prover lfflt, Certlfiod Tape 1#26727, 

/1/.,.~dfJ~ 

ATC PROJECT No. P-10142 

~p Miller-SGM 

EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 682 
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STATE OF LOUISIANA 

DEPARTMENT OF ENVIRONMENTAL QUALITY 

Is hereby granting a Louisiana Environmental I.aboratot-y Accreditation to 

Analytical .. :r e$tip~'¥? ?S qltan ts Inc. 

19~p-jaie 

Ear~il~riit 

igiy~ .. 

~nnapolis, NC 28083<{21:9 

Agency Interest No. 94216 

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,

According to the Louisiana Administrative Code, Title ~~{Part~!lifup~,t 3, LA~G)~ y{ilR~~)i;ACCREDIT A TION, the State 

recognizes that this laboratory is technically competent!<o perf41'ffi'"fh<)[i:invli·o~~al ijllalys"i,s listed on )he scope of accred

attachment. .,, ;•,.. i/ '' " 

The laboratory agrees to perfomt all analyses listed on this scope of accreditation accordi1~,;,tb .the Part I, Subpar

acknowledges that continued accreditation is )lependent on successful ongoing compliance with 'the applicable requirem

contact the Department of Enviromnental Quality, Louisiana Environmental Laboratory Acctcdjul.j)bnProgram (LELAP) to 

scope of accreditation and accreditation status. 

Accreditation by the State of Louisiana is not an end~bnent or a guarantee pf validity0gfthe data generated by the laborat

initially and maintain accreditation, the laboratory agrees lf:P?r!Jcip;tt<:in.,two.~J?gl~cbli'hd, single-concentration PT studies

year for each field of testing for which it seeks accreditationor'nfuint.'li~Si:\i4~~~di!1itlori asreqnired in LAC 33:L47l J. 

Cl::!:::Z::il~en~:Ler 

Notifications and Accreditations Section 

Pennit Support Sen·ices Division 

Certificate Number: 04

Expiration Date: June 

Issued On: July 1, 2010 
BORAL BRICKS 

This is the last page 

of this report. 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 684