Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2050 ENTERGY MS, BAXTER W ILSON 1 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description

No.6 Fuel Oil (residual or bunker C)EIA

Facility Code Facility Name Boiler ID Basis Analyte

2050 ENTERGY MS, BAXTER WILSON 1 As Received Higher Heating Value 2050 ENTERGY MS, BAXTER WILSON 1 As Received % Moisture 2050 ENTERGY MS, BAXTER WILSON 1 As Received % Ash 2050 ENTERGY MS, BAXTER WILSON 1 As Received % Sulfur 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Higher Heating Value 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis % Ash 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis % Sulfur 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Antim ony 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Arsenic 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Beryllium 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Cadmium 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Chlorine 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Chromium 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Cobalt 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Fluorine 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Lead 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Manganese 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Mercury 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis Nickel 2050 ENTERGY MS, BAXTER WILSON 1 Dry basis SeleniumAnalysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6721 ASTM D 6357 ASTM D 6357 ASTM D 3761 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2050 ENTERGY MS, BAXTER WILSON 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1A 5/11/2010 5/11/2010 17700.00 Btu/lb 1B 5/11/2010 5/11/2010 17800.00 Btu/lb 3A 5/12/2010 5/12/2010 17700.00 Btu/lb 3B 5/12/2010 5/12/2010 17600.00 Btu/lb 4A 5/12/2010 5/13/2010 17600.00 Btu/lb 4B 5/12/2010 5/13/2010 17600.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.0702 NA NA NA NA NA 0.091 NA NA NA NA NA 0.0714 NA NA NA NA NA 0.0889 NA NA NA NA NA 0.0449 NA NA NA NA NA 0.0568 NA NA NA NA NAChlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 61.6 ppm <0.031 ppm <5.9 ppm <2 ppm <0.98 62.7 ppm <0.032 ppm <5.6 ppm <1.9 ppm <0.94 110 ppm <0.031 ppm <5.1 ppm <1.7 ppm <0.85 114 ppm <0.031 ppm <5.9 ppm <2.0 ppm <0.98 110 ppm <0.031 ppm <5.5 ppm <1.8 ppm <0.91 239 ppm <0.033 ppm <5.3 ppm <1.8 ppm <0.88Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units ppm <0.49 ppm <1.5 ppm <1.5 ppm <1.5 ppm ppm <0.47 ppm <1.4 ppm <1.4 ppm 0.2 ppm ppm <0.42 ppm <1.3 ppm <1.3 ppm <1.3 ppm ppm <0.49 ppm <1.5 ppm <1.5 ppm <1.5 ppm ppm <0.46 ppm <1.4 ppm <1.4 ppm <1.4 ppm ppm <0.44 ppm <1.3 ppm <1.3 ppm <1.3 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 4.5 ppm 0.91 ppm <150 ppm 0.28 ppm 4.4 ppm 0.78 ppm <150 ppm 0.3 ppm 4.1 ppm 0.67 ppm <150 ppm 0.26 ppm 6.9 ppm 0.82 ppm <150 ppm 0.32 ppm 3.9 ppm 0.7 ppm <150 ppm 0.26 ppm 3.9 ppm 0.69 ppm <150 ppm 0.29 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

Analysis Not PerformedNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

OxygenUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm