Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1 Fuel Type 2 Fuel Type 3 Other Fuel Description

3148 Martins Creek3 No.6 Fuel Oil (residual or bunker C)
EIA Facility Code Facility Name Boiler ID Basis Analyte

Analysis Method for each Analyte 

(example: ASTM D5865-04)

3148 Martins Creek 3 As Received Heat of Combustion ASTM D240

3148 Martins Creek 3 As Received Water by Distillation ASTM D95

3148 Martins Creek 3 As Received Metals EPA 3040A 6010B

3148 Martins Creek 3 As Received Anions EPA 5050 9056

3148 Martins Creek 3 As Received Mercury EPA 245.1

3148 Martins Creek 3 As Received Carbon, Hydrogen, Nitrogen ASTM D5291

3148 Martins Creek 3 As Received Oxygen ASTM D5291_MOD

3148 Martins Creek 3 As Received Sulfur ASTM D4294
EIA Facility Code Facility Name Boiler ID HAPs Test Group

3148 Martins Creek 3 Acid gas HAPs

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

2010-PHIL-002077-001 7/13/2010 7/13/2010 18231 Btu/lb n/a n/a 0.621 151937 Btu/gallon n/a

2010-PHIL-002077-009 7/14/2010 7/14/2010 18324 Btu/lb n/a n/a 0.627 152602 Btu/gallon n/a

2010-PHIL-002077-013 7/15/2010 7/15/2010 18229 Btu/lb n/a n/a 0.63 151811 Btu/gallon n/a

 Fuel Testing Results
% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis)

n/a 20.1 ppm < 0.2 μg/g 2.73 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 16.1

n/a 21.7 ppm < 0.2 μg/g 2.99 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.7

n/a 20.5 ppm < 0.2 μg/g 2.92 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.6
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

μg/g < 1.16 μg/g < 17.4 ppm 0.626 μg/g

μg/g < 1.16 μg/g < 17.4 ppm 0.837 μg/g

μg/g < 1.16 μg/g < 17.4 ppm < 0.573 μg/g

Proximate Analyses, % by wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

3148 Martins Creek 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

2010-PHIL-002077-001 7/13/2010 7/13/2010 18231 Btu/lb n/a n/a 0.621 151937 Btu/gallon n/a

2010-PHIL-002077-009 7/14/2010 7/14/2010 18324 Btu/lb n/a n/a 0.627 152602 Btu/gallon n/a

2010-PHIL-002077-013 7/15/2010 7/15/2010 18229 Btu/lb n/a n/a 0.63 151811 Btu/gallon n/a

 Fuel Testing Results
% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis)

n/a 20.1 ppm < 0.2 μg/g 2.73 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 16.1

n/a 21.7 ppm < 0.2 μg/g 2.99 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.7

n/a 20.5 ppm < 0.2 μg/g 2.92 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.6
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

μg/g < 1.16 μg/g < 17.4 ppm 0.626 μg/g

μg/g < 1.16 μg/g < 17.4 ppm 0.837 μg/g

μg/g < 1.16 μg/g < 17.4 ppm < 0.573 μg/g

Proximate Analyses, % by wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

3148 Martins Creek 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

2010-PHIL-002077-001 7/13/2010 7/13/2010 18231 Btu/lb n/a n/a 0.621 151937 Btu/gallon n/a

2010-PHIL-002077-009 7/14/2010 7/14/2010 18324 Btu/lb n/a n/a 0.627 152602 Btu/gallon n/a

2010-PHIL-002077-013 7/15/2010 7/15/2010 18229 Btu/lb n/a n/a 0.63 151811 Btu/gallon n/a

 Fuel Testing Results
% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis)

n/a 20.1 ppm < 0.2 μg/g 2.73 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 16.1

n/a 21.7 ppm < 0.2 μg/g 2.99 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.7

n/a 20.5 ppm < 0.2 μg/g 2.92 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.6
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

μg/g < 1.16 μg/g < 17.4 ppm 0.626 μg/g

μg/g < 1.16 μg/g < 17.4 ppm 0.837 μg/g

μg/g < 1.16 μg/g < 17.4 ppm < 0.573 μg/g

Proximate Analyses, % by wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

3148 Martins Creek 3 Dioxin/furan HAPs

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

2010-PHIL-002077-001 7/13/2010 7/13/2010 18231 Btu/lb n/a n/a 0.621 151937 Btu/gallon n/a

2010-PHIL-002077-009 7/14/2010 7/14/2010 18324 Btu/lb n/a n/a 0.627 152602 Btu/gallon n/a

2010-PHIL-002077-013 7/15/2010 7/15/2010 18229 Btu/lb n/a n/a 0.63 151811 Btu/gallon n/a

 Fuel Testing Results
% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis)

n/a 20.1 ppm < 0.2 μg/g 2.73 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 16.1

n/a 21.7 ppm < 0.2 μg/g 2.99 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.7

n/a 20.5 ppm < 0.2 μg/g 2.92 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 15.6
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

μg/g < 1.16 μg/g < 17.4 ppm 0.626 μg/g

μg/g < 1.16 μg/g < 17.4 ppm 0.837 μg/g

μg/g < 1.16 μg/g < 17.4 ppm < 0.573 μg/g

Proximate Analyses, % by wt Ultimate Analyses, % by wt