### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

990 AES Harding Street Boiler 60 3/7/2010Fuel Type 1 Fuel Type 2 Fuel Type 3

bitum inousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

990 AES Harding Street Boiler 60 As Received Higher Heating Value 990 AES Harding Street Boiler 60 As Received % Moisture 990 AES Harding Street Boiler 60 As Received % Ash 990 AES Harding Street Boiler 60 As Received % Sulfur 990 AES Harding Street Boiler 60 Dry

basis Higher Heating Value 990 AES Harding Street Boiler 60 Dry

basis % Moisture 990 AES Harding Street Boiler 60 Dry

basis % Ash 990 AES Harding Street Boiler 60 Dry

basis % Sulfur 990 AES Harding Street Boiler 60 Dry

basis Antim ony 990 AES Harding Street Boiler 60 Dry

basis Arsenic 990 AES Harding Street Boiler 60 Dry

basis Beryllium 990 AES Harding Street Boiler 60 Dry

basis Cadmium 990 AES Harding Street Boiler 60 Dry

basis Chlorine 990 AES Harding Street Boiler 60 Dry

basis Chromium 990 AES Harding Street Boiler 60 Dry

basis Cobalt 990 AES Harding Street Boiler 60 Dry

basis Fluorine 990 AES Harding Street Boiler 60 Dry

basis Lead 990 AES Harding Street Boiler 60 Dry

basis Manganese 990 AES Harding Street Boiler 60 Dry

basis Mercury 990 AES Harding Street Boiler 60 Dry

basis Nickel 990 AES Harding Street Boiler 60 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) D4809 D3173 D482 D1552 / D4239 D5865 D3173 D3174 D4239 6020 6020 6020 6020 9056 6020 6020 9056 6020 6020 D3684 6020 6020EIA Facility Code Facility Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 990 AES Harding Street Boiler 60 M30B, M3B, M5/29, OTM-027/028

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Unit 60 30B Run 1 3/7/2010 10788.00 Btu/lb 15 Unit 60 30B Run 2 3/7/2010 10347.00 Btu/lb 15 Unit 60 30B Run 3 3/7/2010 10358.00 Btu/lb 16 Unit 60 PM/Metals Run 1 3/13/2010 10500.00 Btu/lb 16 Unit 60 PM/Metals Run 2 3/13/2010 10720.00 Btu/lb 15 Unit 60 PM/Metals Run 3 3/14/2010 11016.00 Btu/lb 16 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 8.65 12692 Btu/lb 10.18 1.818 10.94 12173 Btu/lb 12.87 1.985 9.22 12331 Btu/lb 10.97 1.783 8.17 12500 Btu/lb 9.72 3.23 9.1 12612 Btu/lb 10.7 2.672 8 13115 Btu/lb 9.52 2.591Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 150 ppm 0.0496 mg/Kg 7.2 mg /Kg 3 mg /Kg 2.8 170 ppm 0.0709 mg/Kg 7.3 mg /Kg 2.7 mg /Kg 0.75 150 ppm 0.053 mg/Kg 6.2 mg /Kg 2.8 mg /Kg 0.84 110 ppm 0.0673 mg/Kg 7.1 mg /Kg 2.4 mg /Kg 0.92 120 ppm 0.072 mg/Kg 7 mg /Kg 2.7 mg /Kg 1.1 120 ppm 0.0526 mg/Kg 6.8 mg /Kg 2.4 mg /Kg 0.81Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units mg/Kg 9.7 mg/Kg 25 mg /Kg 16 mg /Kg 28 mg /Kg mg/Kg 11 mg/Kg 12 mg /Kg 19 mg /Kg 32 mg /Kg mg/Kg 10 mg/Kg 13 mg /Kg 18 mg /Kg 30 mg /Kg mg/Kg 10 mg/Kg 9 mg /Kg 14 mg /Kg 19 mg /Kg mg/Kg 10 mg/Kg 9.5 mg /Kg 16 mg /Kg 20 mg /Kg mg/Kg 10 mg/Kg 7.9 mg /Kg 16 mg /Kg 18 mg /KgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units [<0.6] mg/Kg [<3] ppm 6.6 mg /Kg 1.1 mg/Kg [<3] ppm 8 mg /Kg 1 mg/Kg [<3] ppm 6.6 mg /Kg 1.3 mg/Kg [<3] ppm 4.3 mg /Kg 1.6 mg/Kg [<3] ppm 4.5 mg /Kg 1.3 mg/Kg [<3] ppm 4.4 mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm