### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

1374 Elm er Smith Station Units 1 and 2 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel Description



### petroleum coke other TDFEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 1374 Elmer Smith Station Units 1 and 2

As Received Higher Heating Value 

### 1374 Elmer Smith Station Units 1 and 2

As Received % Moisture 

### 1374 Elmer Smith Station Units 1 and 2

As Received % Ash 

### 1374 Elmer Smith Station Units 1 and 2

As Received % Sulfur 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Higher Heating Value 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis % Ash 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis % Sulfur 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Antim ony 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Arsenic 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Bery llium 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Cadmium 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Chlorine 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Chromium 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Cobalt 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Fluorine 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Lead 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Manganese 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Mercury 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis Nickel 

### 1374 Elmer Smith Station Units 1 and 2

Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3173 ASTM D3174 ASTM D4293 ASTM D5865 ASTM D4293 ASTM D3174 ASTM 6357 ASTM 6357 ASTM 6357 ASTM 6357 ASTM 6721 ASTM 6357 ASTM 6357 ASTM 5987 ASTM 6357 ASTM 6357 ASTM 6722 ASTM 6357 ASTM 4606EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 1374 Elmer Smith Station Units 1 and 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Unit 1 Run 1 

### 6/29/2010 6/29/2010 11117.00 Btu/lb Unit 2 Run 1 6/29/2010 6/29/2010 11056.00 Btu/lb Unit 1 Run 2 6/30/2010 6/30/2010 11187.00 Btu/lb Unit 2 Run 2 6/30/2010 6/30/2010 10849.00 Btu/lb Unit 1 Run 3 6/30/2010 6/30/2010 11202.00 Btu/lb Unit 2 Run 3 6/30/2010 6/30/2010 11118.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 12.26 10.91 3.94 12670 Btu/lb 12.43 4.49 12.27 10.69 3.63 12602 Btu/lb 12.18 4.14 12.16 10.46 3.9 12736 Btu/lb 11.91 4.44 12.83 11.48 3.55 12446 Btu/lb 13.17 4.07 11.51 10.79 4.15 12659 Btu/lb 12.19 4.69 12.07 10.62 3.68 12644 Btu/lb 12.08 4.18Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.129 ppm 1.18 ppm 18.6 ppm 1.9 0.142 ppm 1.15 ppm 33.5 ppm 2.2 0.118 ppm 1.25 ppm 17.2 ppm 2.1 0.126 ppm 1.34 ppm 20.2 ppm 2.2 0.131 ppm 1.2 ppm 21.1 ppm 2.1 0.136 ppm 1.15 ppm 35.1 ppm 2.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm 1.69 ppm 25 ppm 8.5 ppm 51 ppm ppm 0.67 ppm 23 ppm 9.8 ppm 47 ppm ppm 1.68 ppm 24 ppm 8.1 ppm 43 ppm ppm 1.26 ppm 26 ppm 9.5 ppm 46 ppm ppm 1.8 ppm 24 ppm 8.1 ppm 48 ppm ppm 0.56 ppm 24 ppm 9 ppm 43 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 58 ppm 3.9 ppm 8.3 ppm 12.26 35 ppm 3.5 ppm 13.3 ppm 12.27 62 ppm 3.9 ppm 8.3 ppm 12.16 29 ppm 3.8 ppm 9.5 ppm 13.17 60 ppm 3.8 ppm 9.2 ppm 11.51 35 ppm 3.3 ppm 14.5 ppm 12.07 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 35.78 12.43 51.79 69.31 4.64 1.52 4.49 37.95 12.18 49.87 68.68 4.77 1.65 4.14 35.44 11.19 52.65 69.5 4.61 1.51 4.44 39.17 13.17 47.66 67.34 4.75 1.53 4.07 35.35 12.19 52.46 68.91 4.64 1.47 4.69 38.67 12.08 49.25 68.88 4.82 1.62 4.18 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 7.61 8.58 8.03 9.14 8.1 8.42EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 1374 Elmer Smith Station Units 1 and 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units Unit 1 Run 1 

### 6/29/2010 6/29/2010 11117.00 Btu/lb Unit 2 Run 1 6/29/2010 6/29/2010 11056.00 Btu/lb Unit 1 Run 2 6/30/2010 6/30/2010 11187.00 Btu/lb Unit 2 Run 2 6/30/2010 6/30/2010 10849.00 Btu/lb Unit 1 Run 3 6/30/2010 6/30/2010 11202.00 Btu/lb Unit 2 Run 3 6/30/2010 6/30/2010 11118.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 12.26 10.91 3.94 12670 Btu/lb 12.43 4.49 12.27 10.69 3.63 12602 Btu/lb 12.18 4.14 12.16 10.46 3.9 12736 Btu/lb 11.91 4.44 12.83 11.48 3.55 12446 Btu/lb 13.17 4.07 11.51 10.79 4.15 12659 Btu/lb 12.19 4.69 12.07 10.62 3.68 12644 Btu/lb 12.08 4.18Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 130 ppm 129 ppm 76 ppm 118 ppm 80 ppm 97 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 86 ppm 85 ppm 92 ppm 93 ppm 86 ppm 85 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 12.26 35.78 12.43 51.79 69.31 4.64 1.52 4.49 12.27 37.95 12.18 49.87 68.68 4.77 1.65 4.14 12.16 35.44 11.19 52.65 69.5 4.61 1.51 4.44 13.17 39.17 13.17 47.66 67.34 4.75 1.53 4.07 11.51 35.35 12.19 52.46 68.91 4.64 1.47 4.69 12.07 38.67 12.08 49.25 68.88 4.82 1.62 4.18 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 7.61 8.58 8.03 9.14 8.1 8.42EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 1374 Elmer Smith Station Units 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 1374 Elmer Smith Station Units 1 and 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm