### Name: Paul Plotkin

Title: Plant General Manager Company: Florida Power & Light Sign Date: 8/23/2010 Name: Thomas K. Graham Title: Director of Operations Company: Air Hygiene International, Inc. Sign Date: 7/27/2010 Permitted Facility Representative / Date Testing Company Representative / Date



## Manatee Energy Center, Unit #1, Information Collection Request Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Monday, February 14, 2011 Page 1 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Facility Information: Manatee Energy Center
19050 State Road 62

Parrish FL 34219 Contact: Augie De La Vega Phone: (305) 242-3896 Fax: Email: augie.de.la.vega@fpl.com Testing Company: Air Hygiene International, Inc. 5634 S. 122nd East Ave, Suite F

Tulsa OK 74146 Contact: Thomas Graham Phone: (918) 307-8865 Fax: (918) 307-9131 Email: tom@airhygiene.com

Air Permit Number: 0810010-014-AV Permitted Source ID/Name: Foster Wheeler, Wall Fired Boiler PMT1 Permitted Maximum Process Rate: 863.3 MW Max. Normal Operation Process Rate: 800 MW Target Process Test Rate 800 MW

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Florida Power and Light Company (FPL) operates two oil fired electric utility steam generating units of Foster Wheeler design, designated as Units PMT1 and PMT2. The facility is located at 19050 State Road 62 in Parrish, Florida. Unit PMT1 and PMT2 are of identical design and consists of two wall fired boilers and ancillary equipment designed to generate 863.3 megawatts (MW) of electricity each with rated heat inputs of 8,650 million British thermal units per hour (MMBtu/hr) based on high heating value (HHV). Fuel oil consumption is rated at 600,000 pounds per hour. Unit PMT1 and PMT2 utilize low nitrogen oxide (NOx) burner technology to control NOx emissions and cyclone separators to control particulate matter (PM) emissions. Emission testing will be conducted from platforms on the independent stacks of each unit. Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: 0810010 FRS #: 110000496776

SCC / Description 10100401 External Combustion Boilers - Electric Generation - Residual Oil - Grade 6 Oil: Normal Firing

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width PMT1 - D/F 357.4 4524 876 4 0 24 0 0 PMT1 - Gases 357.4 4524 876 4 0 1 0 0 PMT1 - Metals 357.4 4524 876 4 0 24 0 0 PMT1 - PM 357.4 4524 876 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Regulation Description Compound Limit Unit Not applicable.



### Monday, February 14, 2011 Page 2 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location % H2O Method 1 - 4 3 480 24 PMT1 - D/F 2,3,7,8-TCDD Method 23 3 480 24 PMT1 - D/F 1,2,3,7,8-PeCDD Method 23 3 480 24 PMT1 - D/F 1,2,3,4,7,8-HxCDD Method 23 3 480 24 PMT1 - D/F 1,2,3,6,7,8-HxCDD Method 23 3 480 24 PMT1 - D/F 1,2,3,7,8,9-HxCDD Method 23 3 480 24 PMT1 - D/F 1,2,3,4,6,7,8-HpCDD Method 23 3 480 24 PMT1 - D/F OCDD Method 23 3 480 24 PMT1 - D/F 2,3,7,8-TCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,7,8-PeCDF Method 23 3 480 24 PMT1 - D/F 2,3,4,7,8-PeCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,4,7,8-HxCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,6,7,8-HxCDF Method 23 3 480 24 PMT1 - D/F 2,3,4,6,7,8-HxCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,7,8,9-HxCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,4,6,7,8-HpCDF Method 23 3 480 24 PMT1 - D/F 1,2,3,4,7,8,9-HpCDF Method 23 3 480 24 PMT1 - D/F OCDF Method 23 3 480 24 PMT1 - D/F Total Dioxins Method 23 3 480 24 PMT1 - D/F Total Furans Method 23 3 480 24 PMT1 - D/F 3,3',4,4'-TCB (PCB77) Method 23 3 480 24 PMT1 - D/F 3,4,4',5-TCB (PCB81) Method 23 3 480 24 PMT1 - D/F 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 24 PMT1 - D/F 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 24 PMT1 - D/F 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 24 PMT1 - D/F 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 24 PMT1 - D/F 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 24 PMT1 - D/F 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 24 PMT1 - D/F

2,3',4,4',5,5'-HxCB (PCB167) Method 23 3 480 24 PMT1 - D/F 3,3',4,4',5,5'-HxCB (PCB169) Method 23 3 480 24 PMT1 - D/F 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 24 PMT1 - D/F

O2 Method 3A O2 3 480 24 PMT1 - D/F Co2 Method 3A CO2 3 480 24 PMT1 - D/F % H2O Method 1 - 4 3 120 1 Determined after initial stratification test PMT1 - Gases

Carbon Monoxide Method 10 3 120 1 Determined after initial stratification test PMT1 - Gases
Total organic compounds

(TOC) as Propane Method 25A 3 120 1 Determined after initial stratification test PMT1 - Gases

Co2 Method 3A CO2 3 120 1 Determined after initial stratification test PMT1 - Gases

O2 Method 3A O2 3 120 1 Determined after initial stratification test PMT1 - Gases

Sulfur Dioxide Method 6C 3 120 1 Determined after initial stratification test PMT1 - Gases
Nitrogen oxides (NOx) Method 7E 3 120 1 Determined after initial stratification test PMT1 - Gases

% H2O Method 1 - 4 3 240 24 PMT1 - Metals Nickel Method 29 3 240 24 PMT1 - Metals Filterable Particulate Method 29 3 240 24 PMT1 - Metals


### Monday, February 14, 2011 Page 3 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. PM Run All - reduced to 2 hour runs to avoid high vacuum, did not pull required volumes.
PM Run 3 - oily substance in organic backhalf.

Cobalt Method 29 3 240 24 PMT1 - Metals Chromium Method 29 3 240 24 PMT1 - Metals Cadmium Method 29 3 240 24 PMT1 - Metals Manganese Method 29 3 240 24 PMT1 - Metals Selenium Method 29 3 240 24 PMT1 - Metals Lead Method 29 3 240 24 PMT1 - Metals Co2 Method 3A CO2 3 240 24 PMT1 - Metals O2 Method 3A O2 3 240 24 PMT1 - Metals % H2O Method 1 - 4 3 120 12 Run times vary based on method calculations PMT1 - PM
Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM

Filterable PM2.5 OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM
Organic Condensible

Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM

Total PM2.5 OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM

Total Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM

Filterable Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMT1 - PM

O2 Method 3A O2 3 120 12 Run times vary based on method calculations PMT1 - PM

Co2 Method 3A CO2 3 120 12 Run times vary based on method calculations PMT1 - PM



### Monday, February 14, 2011 Page 4 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Sampling / Stack Data Results Summary



### Location PMT1 - D/F - Method 23 Average Run Number PMT1-23-1 PMT1-23-2 PMT1-23-3
Test Date 5/17/2010 5/18/2010 5/20/2010 Run Start Time 9:37:00 AM 11:05:00 AM 11:10:00 AM

Run Finish Time 5:37:00 PM 7:05:00 PM 7:10:00 PM Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 370.084 370.760 356.228 365.691 Moisture Content of Stack Gas, % 9.26 9.44 9.07 9.257 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 12.79 12.66 12.86 12.770 Oxygen, % 5.26 5.36 5.28 5.300 Average Stack Gas Temperature, °F 323.33 328.50 329.38 327.070 Dry Volumetric Flow Rate, dry scfm 1,577,964.0 1,598,210.6 1,558,820.1 1,578,331.56 7 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,580,799.9 2,636,395.4 2,573,275.7 2,596,823.66 7 Percent Isokinetic of Sampling Rate, % 99.9 98.8 97.3 98.667 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location PMT1 - Gases - Method 10 Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Monday, February 14, 2011 Page 5 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 25A Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Location PMT1 - Gases - Method 3A CO2 Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Monday, February 14, 2011 Page 6 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 3A O2 Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Location PMT1 - Gases - Method 6C Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Monday, February 14, 2011 Page 7 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 7E Average Run Number
Test Date Run Start Time
Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Location PMT1 - Metals - Method 29 Average Run Number
Test Date Run Start Time
Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Monday, February 14, 2011 Page 8 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - PM - OTM - 27/28 Average Run Number
Test Date Run Start Time
Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Monday, February 14, 2011 Page 9 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Emissions Summary



### Location: PMT1 - D/F - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000072 0.0000000099 0.000000007 0.000 lb/mmBtuO2 5.27E-13 7.28E-13 5.33E-13 0.000 ng/dscm 6.87E-04 9.43E-04 6.94E-04 0.001 ng/dscm@7%O2 6.11E-04 8.43E-04 6.18E-04 0.001 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000037 0.0000000056 0.000000003 0.000 lb/mmBtuO2 2.71E-13 4.12E-13 2.28E-13 0.000 ng/dscm 3.53E-04 5.33E-04 2.97E-04 0.000 ng/dscm@7%O2 3.14E-04 4.77E-04 2.64E-04 0.000 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000051 0.0000000077 0.0000000041 0.000 lb/mmBtuO2 3.73E-13 5.66E-13 3.12E-13 0.000 ng/dscm 4.87E-04 7.34E-04 4.07E-04 0.001 ng/dscm@7%O2 4.33E-04 6.57E-04 3.62E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000052 0.0000000049 0.0000000073 0.000 lb/mmBtuO2 3.80E-13 3.60E-13 5.56E-13 0.000 ng/dscm 4.96E-04 4.67E-04 7.24E-04 0.001 ng/dscm@7%O2 4.41E-04 4.18E-04 6.44E-04 0.001 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000012 0.0000000027 0.0000000037 0.000 lb/mmBtuO2 8.78E-13 1.98E-13 2.82E-13 0.000 ng/dscm 1.15E-03 2.57E-04 3.67E-04 0.001 ng/dscm@7%O2 1.02E-03 2.30E-04 3.27E-04 0.001 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000044 0.0000000041 0.0000000061 0.000 lb/mmBtuO2 3.22E-13 3.01E-13 4.64E-13 0.000 ng/dscm 4.20E-04 3.91E-04 6.05E-04 0.000 ng/dscm@7%O2 3.73E-04 3.50E-04 5.38E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDF Average



### Monday, February 14, 2011 Page 10 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000021 0.0000000024 0.0000000033 0.000 lb/mmBtuO2 1.54E-13 1.76E-13 2.51E-13 0.000 ng/dscm 2.00E-04 2.29E-04 3.27E-04 0.000 ng/dscm@7%O2 1.78E-04 2.05E-04 2.91E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000046 0.0000000042 0.0000000063 0.000 lb/mmBtuO2 3.37E-13 3.09E-13 4.79E-13 0.000 ng/dscm 4.39E-04 4.00E-04 6.25E-04 0.000 ng/dscm@7%O2 3.90E-04 3.58E-04 5.56E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000027 0.0000000031 0.0000000042 0.000 lb/mmBtuO2 1.98E-13 2.28E-13 3.20E-13 0.000 ng/dscm 2.58E-04 2.95E-04 4.16E-04 0.000 ng/dscm@7%O2 2.29E-04 2.64E-04 3.70E-04 0.000 

### Compound: 1,2,3,7,8-PeCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000051 0.0000000072 0.0000000047 0.000 lb/mmBtuO2 3.73E-13 5.29E-13 3.58E-13 0.000 ng/dscm 4.87E-04 6.86E-04 4.66E-04 0.001 ng/dscm@7%O2 4.33E-04 6.14E-04 4.15E-04 0.000 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.00000003 0.0000000052 0.0000000063 0.000 lb/mmBtuO2 2.19E-12 3.82E-13 4.79E-13 0.000 ng/dscm 2.86E-03 4.95E-04 6.25E-04 0.001 ng/dscm@7%O2 2.54E-03 4.43E-04 5.56E-04 0.001 

### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000053 0.0000000022 0.000000066 0.000 lb/mmBtuO2 3.88E-12 1.62E-13 5.02E-12 0.000 ng/dscm 5.06E-03 2.10E-04 6.54E-03 0.004 ng/dscm@7%O2 4.50E-03 1.88E-04 5.82E-03 0.004 

### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000159 0.0000000278 0.00000017 0.000 lb/mmBtuO2 1.16E-11 2.04E-12 1.29E-11 0.000 ng/dscm 1.52E-02 2.65E-03 1.69E-02 0.012 ng/dscm@7%O2 1.35E-02 2.37E-03 1.50E-02 0.010



### Monday, February 14, 2011 Page 11 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000855 0.000000271 0.00000144 0.000 lb/mmBtuO2 6.25E-11 1.99E-11 1.10E-10 0.000 ng/dscm 8.16E-02 2.58E-02 1.43E-01 0.083 ng/dscm@7%O2 7.25E-02 2.31E-02 1.27E-01 0.074 

### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000223 0.000000026 0.00000024 0.000 lb/mmBtuO2 1.63E-11 1.91E-12 1.83E-11 0.000 ng/dscm 2.13E-02 2.48E-03 2.38E-02 0.016 ng/dscm@7%O2 1.89E-02 2.22E-03 2.12E-02 0.014 

### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000412 0.000000017 0.000000105 0.000 lb/mmBtuO2 3.01E-12 1.25E-12 7.99E-12 0.000 ng/dscm 3.93E-03 1.62E-03 1.04E-02 0.005 ng/dscm@7%O2 3.49E-03 1.45E-03 9.25E-03 0.005 

### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.00000205 0.000000693 0.00000291 0.000 lb/mmBtuO2 1.50E-10 5.09E-11 2.21E-10 0.000 ng/dscm 1.96E-01 6.60E-02 2.89E-01 0.184 ng/dscm@7%O2 1.74E-01 5.90E-02 2.57E-01 0.163 

### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000342 0.000000028 0.0000000666 0.000 lb/mmBtuO2 2.50E-12 2.06E-12 5.07E-12 0.000 ng/dscm 3.26E-03 2.67E-03 6.60E-03 0.004 ng/dscm@7%O2 2.90E-03 2.39E-03 5.87E-03 0.004 

### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000023 0.0000000026 0.0000000035 0.000 lb/mmBtuO2 1.68E-13 1.91E-13 2.66E-13 0.000 ng/dscm 2.20E-04 2.48E-04 3.47E-04 0.000 ng/dscm@7%O2 1.96E-04 2.22E-04 3.09E-04 0.000 

### Compound: 2,3,4,7,8-PeCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000047 0.000000005 0.000000006 0.000 lb/mmBtuO2 3.44E-13 3.67E-13 4.57E-13 0.000



### Monday, February 14, 2011 Page 12 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 ng/dscm 4.49E-04 4.76E-04 5.95E-04 0.001 ng/dscm@7%O2 3.99E-04 4.26E-04 5.29E-04 0.000 

### Compound: 2,3,7,8-TCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000041 0.0000000062 0.0000000057 0.000 lb/mmBtuO2 3.00E-13 4.56E-13 4.34E-13 0.000 ng/dscm 3.91E-04 5.91E-04 5.65E-04 0.001 ng/dscm@7%O2 3.48E-04 5.29E-04 5.03E-04 0.000 

### Compound: 2,3,7,8-TCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000362 0.0000000051 0.000000006 0.000 lb/mmBtuO2 2.65E-12 3.75E-13 4.57E-13 0.000 ng/dscm 3.45E-03 4.86E-04 5.95E-04 0.002 ng/dscm@7%O2 3.07E-03 4.35E-04 5.29E-04 0.001 

### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000063 0.0000000027 0.0000000071 0.000 lb/mmBtuO2 4.61E-13 1.98E-13 5.40E-13 0.000 ng/dscm 6.01E-04 2.57E-04 7.04E-04 0.001 ng/dscm@7%O2 5.34E-04 2.30E-04 6.26E-04 0.000 

### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.00000001 0.000000021 0.0000000483 0.000 lb/mmBtuO2 7.32E-13 1.54E-12 3.68E-12 0.000 ng/dscm 9.54E-04 2.00E-03 4.79E-03 0.003 ng/dscm@7%O2 8.48E-04 1.79E-03 4.26E-03 0.002 

### Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000148 0.000000037 0.000000282 0.000 lb/mmBtuO2 1.08E-11 2.72E-12 2.15E-11 0.000 ng/dscm 1.41E-02 3.52E-03 2.80E-02 0.015 ng/dscm@7%O2 1.25E-02 3.15E-03 2.49E-02 0.014 

### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000211 0.000000007 0.0000000183 0.000 lb/mmBtuO2 1.54E-12 5.14E-13 1.39E-12 0.000 ng/dscm 2.01E-03 6.67E-04 1.81E-03 0.001 ng/dscm@7%O2 1.79E-03 5.97E-04 1.61E-03 0.001 

### Compound: OCDD Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3


### Monday, February 14, 2011 Page 13 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Mass_mg 0.00000006 0.000000036 0.000000018 0.000 lb/mmBtuO2 4.39E-12 2.65E-12 1.37E-12 0.000 ng/dscm 5.73E-03 3.43E-03 1.78E-03 0.004 ng/dscm@7%O2 5.09E-03 3.07E-03 1.58E-03 0.003 

### Compound: OCDF Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.000000022 0.0000000089 0.000000016 0.000 lb/mmBtuO2 1.61E-12 6.54E-13 1.22E-12 0.000 ng/dscm 2.10E-03 8.48E-04 1.59E-03 0.002 ng/dscm@7%O2 1.87E-03 7.59E-04 1.41E-03 0.001 

### Compound: Total Dioxins Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000000906 0.0000000725 0.0000000551 0.000 lb/mmBtuO2 6.63E-12 5.33E-12 4.19E-12 0.000 ng/dscm 8.65E-03 6.91E-03 5.46E-03 0.007 ng/dscm@7%O2 7.69E-03 6.18E-03 4.86E-03 0.006 

### Compound: Total Furans Average RunNumber PMT1-23-1 PMT1-23-2 PMT1-23-3 Mass_mg 0.0000001208 0.0000000483 0.0000000561 0.000 lb/mmBtuO2 8.84E-12 3.55E-12 4.27E-12 0.000 ng/dscm 1.15E-02 4.60E-03 5.56E-03 0.007 ng/dscm@7%O2 1.02E-02 4.11E-03 4.95E-03 0.006



### Location: PMT1 - Gases - Method 10 Compound: Carbon Monoxide Average Run 1-CO-1 1-CO-2 1-CO-3 lb/mmBtuO2 1.06E-01 9.59E-02 5.35E-02 0.085 ppm 1.18E+02 1.07E+02 5.95E+01 94.833 ppm@7%O2 1.05E+02 9.52E+01 5.32E+01 84.467



### Location: PMT1 - Gases - Method 25A Compound: Total organic compounds (TOC) as Average Run 1-THC-1 1-THC-2 1-THC-3 lb/mmBtuO2 4.70E-05 0.00E+00 0.00E+00 0.000 ppm 3.35E-02 0.00E+00 0.00E+00 0.011 ppm@7%O2 2.97E-02 0.00E+00 0.00E+00 0.010



### Location: PMT1 - Gases - Method 6C Compound: Sulfur Dioxide Average Run 1-SO2-1 1-SO2-2 1-SO2-3 lb/mmBtuO2 8.31E-01 8.10E-01 9.44E-01 0.862 ppm 4.08E+02 3.96E+02 4.59E+02 421.000 ppm@7%O2 3.62E+02 3.52E+02 4.11E+02 375.000



### Monday, February 14, 2011 Page 14 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010

Process Run Data Location: PMT1 - Gases - Method 7E 

### Compound: Nitrogen oxides (NOx) Average Run 1-NOx-1 1-NOx-2 1-NOx-3 lb/mmBtuO2 0.000 ppm 0.000 ppm@7%O2 #Num!



### Monday, February 14, 2011 Page 15 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Process Run Data



### Run Name Value UOM Comments Target Value 1 Residual Oil (No. 6) Burned 59626 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 5/17/2010; Start - 13:28; End - 15:27 0



### 10 Residual Oil (No. 6) Burned 59619 gal/hr Method 027/028; Run PM-1; Date - 5/17/2010; Start - 18:31; End - 21:39 0

11 Residual Oil (No. 6) Burned 59927 gal/hr Method 027/028; Run PM-2; Date - 5/19/2010; Start - 16:43; End - 18:15 0

12 Residual Oil (No. 6) Burned 59736 gal/hr Method 027/028; Run PM-3; Date - 5/20/2010; Start - 15:22; End - 18:00 0

2 Residual Oil (No. 6) Burned 59685 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 5/17/2010; Start - 15:52; End - 17:52 0

3 Residual Oil (No. 6) Burned 59714 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 5/18/2010; Start - 13:04; End - 15:03 0



### 4 Residual Oil (No. 6) Burned 59649 gal/hr Method 23; Run D/F-1; Date - 5/17/2010; Start - 09:37; End - 20:16 0

5 Residual Oil (No. 6) Burned 59722 gal/hr Method 23; Run D/F-2; Date - 5/18/2010; Start - 11:05; End - 19:58 0

6 Residual Oil (No. 6) Burned 59985 gal/hr Method 23; Run D/F-3; Date - 5/20/2010; Start - 11:10; End - 20:03 0

7 Residual Oil (No. 6) Burned 59649 gal/hr Method 29; Run M-1; Date - 5/17/2010; Start - 13:16; End - 17:59 0



### Monday, February 14, 2011 Page 16 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 8 Residual Oil (No. 6) Burned 59649 gal/hr Method 29; Run M-2; Date - 5/18/2010; Start - 08:02; End - 12:42 0

9 Residual Oil (No. 6) Burned 59736 gal/hr Method 29; Run M-3; Date - 5/18/2010; Start - 12:57; End - 17:32 0

1 Average Heat Input 7426 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 5/17/2010; Start - 13:28; End - 15:27 0



### 10 Average Heat Input 7427 MMBtu/hr Method 027/028; Run PM-1; Date - 5/17/2010; Start - 18:31; End - 21:39 0

11 Average Heat Input 7465 MMBtu/hr Method 027/028; Run PM-2; Date - 5/19/2010; Start - 16:43; End - 18:15 0

12 Average Heat Input 7441 MMBtu/hr Method 027/028; Run PM-3; Date - 5/20/2010; Start - 15:22; End - 18:00 0

2 Average Heat Input 7433 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 5/17/2010; Start - 15:52; End - 17:52 0

3 Average Heat Input 7438 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 5/18/2010; Start - 13:04; End - 15:03 0



### 4 Average Heat Input 7430 MMBtu/hr Method 23; Run D/F-1; Date - 5/17/2010; Start - 09:37; End - 20:16 0

5 Average Heat Input 7440 MMBtu/hr Method 23; Run D/F-2; Date - 5/18/2010; Start - 11:05; End - 19:58 0

6 Average Heat Input 7471 MMBtu/hr Method 23; Run D/F-3; Date - 5/20/2010; Start - 11:10; End - 20:03 0



### Monday, February 14, 2011 Page 17 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
7 Average Heat Input 7430 MMBtu/hr Method 29; Run M-1; Date - 5/17/2010; Start - 13:16; End - 17:59 0

8 Average Heat Input 7429 MMBtu/hr Method 29; Run M-2; Date - 5/18/2010; Start - 08:02; End - 12:42 0

9 Average Heat Input 7442 MMBtu/hr Method 29; Run M-3; Date - 5/18/2010; Start - 12:57; End - 17:32 0

1 Steam Output 5353 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 5/17/2010; Start - 13:28; End - 15:27 0



### 10 Steam Output 5351 1000 lb Method 027/028; Run PM-1; Date - 5/17/2010; Start - 18:31; End - 21:39 0

11 Steam Output 5362 1000 lb Method 027/028; Run PM-2; Date - 5/19/2010; Start - 16:43; End - 18:15 0

12 Steam Output 5354 1000 lb Method 027/028; Run PM-3; Date - 5/20/2010; Start - 15:22; End - 18:00 0

2 Steam Output 5356 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 5/17/2010; Start - 15:52; End - 17:52 0

3 Steam Output 5366 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 5/18/2010; Start - 13:04; End - 15:03 0

4 Steam Output 5354 1000 lb Method 23; Run D/F-1; Date - 5/17/2010; Start - 09:37; End - 20:16 0

5 Steam Output 5365 1000 lb Method 23; Run D/F-2; Date - 5/18/2010; Start - 11:05; End - 19:58 0



### Monday, February 14, 2011 Page 18 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
6 Steam Output 5354 1000 lb Method 23; Run D/F-3; Date - 5/20/2010; Start - 11:10; End - 20:03 0

7 Steam Output 5354 1000 lb Method 29; Run M-1; Date - 5/17/2010; Start - 13:16; End - 17:59 0

8 Steam Output 5363 1000 lb Method 29; Run M-2; Date - 5/18/2010; Start - 08:02; End - 12:42 0

9 Steam Output 5367 1000 lb Method 29; Run M-3; Date - 5/18/2010; Start - 12:57; End - 17:32 0

1 Unit Gross Electrical Output 798 MWg Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 5/17/2010; Start - 13:28; End - 15:27 0



### 10 Unit Gross Electrical Output 798 MWg Method 027/028; Run PM-1; Date - 5/17/2010; Start - 18:31; End - 21:39 0

11 Unit Gross Electrical Output 798 MWg Method 027/028; Run PM-2; Date - 5/19/2010; Start - 16:43; End - 18:15 0

12 Unit Gross Electrical Output 798 MWg Method 027/028; Run PM-3; Date - 5/20/2010; Start - 15:22; End - 18:00 0

2 Unit Gross Electrical Output 798 MWg Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 5/17/2010; Start - 15:52; End - 17:52 0

3 Unit Gross Electrical Output 798 MWg Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 5/18/2010; Start - 13:04; End - 15:03 0

4 Unit Gross Electrical Output 798 MWg Method 23; Run D/F-1; Date - 5/17/2010; Start - 09:37; End - 20:16 0



### Monday, February 14, 2011 Page 19 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 5 Unit Gross Electrical Output 798 MWg Method 23; Run D/F-2; Date - 5/18/2010; Start - 11:05; End - 19:58 0

6 Unit Gross Electrical Output 798 MWg Method 23; Run D/F-3; Date - 5/20/2010; Start - 11:10; End - 20:03 0

7 Unit Gross Electrical Output 798 MWg Method 29; Run M-1; Date - 5/17/2010; Start - 13:16; End - 17:59 0

8 Unit Gross Electrical Output 798 MWg Method 29; Run M-2; Date - 5/18/2010; Start - 08:02; End - 12:42 0

9 Unit Gross Electrical Output 798 MWg Method 29; Run M-3; Date - 5/18/2010; Start - 12:57; End - 17:32 0

1 Unit Net Electric Generation 766 MWn Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 5/17/2010; Start - 13:28; End - 15:27 0



### 10 Unit Net Electric Generation 766 MWn Method 027/028; Run PM-1; Date - 5/17/2010; Start - 18:31; End - 21:39 0

11 Unit Net Electric Generation 766 MWn Method 027/028; Run PM-2; Date - 5/19/2010; Start - 16:43; End - 18:15 0

12 Unit Net Electric Generation 766 MWn Method 027/028; Run PM-3; Date - 5/20/2010; Start - 15:22; End - 18:00 0

2 Unit Net Electric Generation 766 MWn Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 5/17/2010; Start - 15:52; End - 17:52 0

3 Unit Net Electric Generation 766 MWn Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 5/18/2010; Start - 13:04; End - 15:03 0



### Monday, February 14, 2011 Page 20 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010

APCD Run Data

Process Lab Run Data 4 Unit Net Electric Generation 766 MWn Method 23; Run D/F-1; Date - 5/17/2010; Start - 09:37; End - 20:16 0

5 Unit Net Electric Generation 766 MWn Method 23; Run D/F-2; Date - 5/18/2010; Start - 11:05; End - 19:58 0

6 Unit Net Electric Generation 766 MWn Method 23; Run D/F-3; Date - 5/20/2010; Start - 11:10; End - 20:03 0

7 Unit Net Electric Generation 766 MWn Method 29; Run M-1; Date - 5/17/2010; Start - 13:16; End - 17:59 0

8 Unit Net Electric Generation 766 MWn Method 29; Run M-2; Date - 5/18/2010; Start - 08:02; End - 12:42 0

9 Unit Net Electric Generation 766 MWn Method 29; Run M-3; Date - 5/18/2010; Start - 12:57; End - 17:32 0



### Run Name Value UOM Comments Target Value 1 LOW NOX BURNERS 165 NOx Emissions 0


### 2 LOW NOX BURNERS 168 NOx Emissions 0
3 LOW NOX BURNERS 154 NOx Emissions 0
1 CYCLONE SEPARATORS 13.9 Opacity 0


### 2 CYCLONE SEPARATORS 15.2 Opacity 0
3 CYCLONE SEPARATORS 11.4 Opacity 0

Run Name Value UOM Comments 

### 1 Fuel Higher Heating Value 17800 Btu/lb 1 Fuel Moisture 0.112 % 1 Fuel Mercury Content 0.001 mg/kg 1 Fuel Chlorine Content 194 mg/kg 

### 1 Fuel Fluorine Content 74 mg/kg 1 Fuel Antimony Content 0.87 mg/kg 1 Fuel Arsenic Content 0.08 mg/kg 

### 1 Fuel Beryllium Content 0.008 mg/kg
Monday, February 14, 2011 Page 21 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 1 Fuel Cadmium Content 0.008 mg/kg 

### 1 Fuel Chromium Content 0.083 mg/kg 1 Fuel Cobalt Content 1.1 mg/kg 1 Fuel Lead Content 0.15 mg/kg 1 Fuel Manganese Content 0.3 mg/kg 

### 1 Fuel Nickel Content 22.3 mg/kg 1 Fuel Selenium Content 0.03 mg/kg 1 Fuel Sulfur Content 10700 mg/kg 

### 1 Fuel Proximate Analysis (Carbon) 88.51 % 1 Fuel Proximate Analysis (Hydrogen) 10.06 % 1 Fuel Proximate Analysis (Nitrogen) 0.57 % 1 Fuel Proximate Analysis (Oxygen) 0.5 % 

### 1 Fuel Proximate Analysis (Sulfur) 1.06 % 2 Fuel Higher Heating Value 17800 Btu/lb 2 Fuel Moisture 0.083 % 

### 2 Fuel Mercury Content 0.002 mg/kg 2 Fuel Chlorine Content 217 mg/kg 2 Fuel Fluorine Content 78 mg/kg 2 Fuel Antimony Content 1 mg/kg 

### 2 Fuel Arsenic Content 0.069 mg/kg 2 Fuel Beryllium Content 0.008 mg/kg 2 Fuel Cadmium Content 0.008 mg/kg 

### 2 Fuel Chromium Content 0.092 mg/kg 2 Fuel Cobalt Content 1 mg/kg 2 Fuel Lead Content 0.17 mg/kg 2 Fuel Manganese Content 0.4 mg/kg 

### 2 Fuel Nickel Content 22.5 mg/kg 2 Fuel Selenium Content 0.03 mg/kg 2 Fuel Sulfur Content 10500 mg/kg 

### 2 Fuel Proximate Analysis (Carbon) 87.72 % 2 Fuel Proximate Analysis (Hydrogen) 9.97 % 2 Fuel Proximate Analysis (Nitrogen) 0.59 % 2 Fuel Proximate Analysis (Oxygen) 0.5 % 

### 2 Fuel Proximate Analysis (Sulfur) 1.2 % 3 Fuel Higher Heating Value 17900 Btu/lb 3 Fuel Moisture 0.22 % 

### 3 Fuel Mercury Content 0.003 mg/kg 3 Fuel Chlorine Content 213 mg/kg 3 Fuel Fluorine Content 78 mg/kg 3 Fuel Antimony Content 1.2 mg/kg 

### 3 Fuel Arsenic Content 0.056 mg/kg 3 Fuel Beryllium Content 0.008 mg/kg 3 Fuel Cadmium Content 0.009 mg/kg



### Monday, February 14, 2011 Page 22 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 3 Fuel Chromium Content 0.1 mg/kg 

### 3 Fuel Cobalt Content 0.94 mg/kg 3 Fuel Lead Content 0.19 mg/kg 3 Fuel Manganese Content 0.5 mg/kg 3 Fuel Nickel Content 22.3 mg/kg 

### 3 Fuel Selenium Content 0.03 mg/kg 3 Fuel Sulfur Content 10000 mg/kg 3 Fuel Proximate Analysis (Carbon) 87.96 % 

### 3 Fuel Proximate Analysis (Hydrogen) 10.57 % 3 Fuel Proximate Analysis (Nitrogen) 0.68 % 3 Fuel Proximate Analysis (Oxygen) 0.5 % 3 Fuel Proximate Analysis (Sulfur) 1.16 %



### Monday, February 14, 2011 Page 23 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010 Sampling / Stack Data Results Detail



### Location PMT1 - D/F - Method 23 Average Run Number PMT1-23-1 PMT1-23-2 PMT1-23-3 Test Date 5/17/2010 5/18/2010 5/20/2010 Run Start Time 9:37:00 AM 11:05:00 AM 11:10:00 AM Run Finish Time 5:37:00 PM 7:05:00 PM 7:10:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.25 0.25 0.25 0.250 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.987 0.987 0.987 0.987 Barometric Pressure, inches of Mercury 30.01 30.01 29.9 29.973 Average Orifice Meter Differential, inches H2O 2.16 2.24 2.06 2.153 Dry Gas Meter Volume Sampled, cubic feet 376.740 379.760 366.460 374.320 Average Dry Gas Meter Temperature, °F 74.92 78.33 78.46 77.237 Dry Gas Meter Volume Sampled, dscf 370.084 370.760 356.228 365.691 Total Moisture Liquid collected, g 802.6 821.1 754.9 792.867 Volume of Water Vapor, standard cubic feet 37.78 38.65 35.53 37.320 Moisture Content of Stack Gas, % 9.26 9.44 9.07 9.257 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9074 0.9056 0.9093 0.907 Carbon Dioxide, % 12.79 12.66 12.86 12.770 Oxygen, % 5.26 5.36 5.28 5.300 Carbon Monoxide & Nitrogen, % 81.95 81.98 81.86 81.930 Fuel Factor 1.22 1.23 1.21 Dry Molecular Weight, lb/lb-Mole 30.26 30.24 30.27 30.257 Wet Molecular weight, lb/lb-Mole 29.12 29.08 29.16 29.120 Flue Gas Static Pressure, inches of H2O -1.4 -1.4 -1.4 -1.400 Absolute Flue Gas Pressure, inches of Mercury 29.91 29.91 29.80 29.873 Average Stack Gas Temperature, °F 323.33 328.50 329.38 327.070 Average Velocity Head, inches of H2O 0.8219652069 63952 0.850952866

417075 0.808911559

550721 0.827
Average Stack Gas Velocity, feet/second 61.74 63.07 61.56 62.123 Stack Cross-Sectional Area, square feet 696.685 696.685 696.685 696.685 Dry Volumetric Flow Rate, dry scfm 1,577,964.0 1,598,210.6 1,558,820.1 1,578,331.5 67 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,580,799.9 2,636,395.4 2,573,275.7 2,596,823.6 67 Percent Isokinetic of Sampling Rate, % 99.9 98.8 97.3 98.667 Percent Excess Air, % 32.1 32.9 32.3 32.433 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 357.4 357.4 357.4 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 10320 10,320.000 Fc 1420 1420 1420 1,420.000



### Monday, February 14, 2011 Page 24 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 10 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 25 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 25A Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 26 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 3A CO2 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 27 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 3A O2 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 28 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 6C Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 29 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Gases - Method 7E Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Monday, February 14, 2011 Page 30 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - Metals - Method 29 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Monday, February 14, 2011 Page 31 of 32

### Manatee Energy Center, Unit #1, Information Collection Request

8/23/2010
Location PMT1 - PM - OTM - 27/28 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



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