### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8



### Client Sample ID: FG1075-01R \ SAMPLES #1 @ Lab ID: R10030049-01 Matrix: OIL Analyses Result Qual Units Date Analyzed Limit DF Date Sampled: 02/23/2010 0:00 Date Received: 03/15/2010

ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony 3/17/2010 3.00 mg/Kg 1 BRL Arsenic 3/17/2010 2.00 mg/Kg 1 BRL Beryllium 3/17/2010 1.00 mg/Kg 1 BRL Cadmium 3/17/2010 1.00 mg/Kg 1 BRL Chromium 3/17/2010 1.00 mg/Kg 1 BRL Cobalt 3/17/2010 0.100 mg/Kg 1 BRL Lead 3/17/2010 1.00 mg/Kg 1 BRL Manganese 3/17/2010 1.00 mg/Kg 1 1.58 Nickel 3/17/2010 1.00 mg/Kg 1 1.84 Selenium 3/17/2010 2.00 mg/Kg 1 BRL 

### MERCURY, TOTAL D3684/SW7471 Anal yst: SUB

Mercury 3/19/2010 0.100 mg/Kg 1 BRL 

### ASH, OIL D482 Anal yst: VJO

Ash 3/18/2010 0.0100 % 1 0.150 

### CHLORINE E776/9253 Anal yst: VJO

Chlorine 3/22/2010 0.0100 % 1 0.0200 

### CARBON, HYDROGEN, NITROGEN (OIL) D5291 Anal yst: VJO

Carbon 3/18/2010 0.01 % 1 86.6 Hydrogen 3/18/2010 0.01 % 1 11.2 Nitrogen 3/18/2010 0.01 % 1 0.45 

### FLUORINE D3761 Anal yst: VJO

Fluorine 3/22/2010 0.0100 mg/Kg 1 13.0
Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 1 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search

### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8

HEATING VALUE BTU/LB D240 Anal yst: VJO

Heating Value 3/22/2010 50 Btu/lb 1 18,310 

### OXYGEN BY DIFFERENCE D5291 Anal yst: VJO

Oxygen 3/18/2010 0.0100 % 1 0.190 

### SULFUR D1552 Anal yst: VJO

Sulfur 3/18/2010 0.0100 % 1 1.35

Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 2 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search

### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8



### Client Sample ID: FG1076-01R \ SAMPLES #2 @ Lab ID: R10030049-02 Matrix: OIL Analyses Result Qual Units Date Analyzed Limit DF Date Sampled: 02/23/2010 0:00 Date Received: 03/15/2010

ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony 3/17/2010 3.00 mg/Kg 1 BRL Arsenic 3/17/2010 2.00 mg/Kg 1 BRL Beryllium 3/17/2010 1.00 mg/Kg 1 BRL Cadmium 3/17/2010 1.00 mg/Kg 1 BRL Chromium 3/17/2010 1.00 mg/Kg 1 1.14 Cobalt 3/17/2010 0.100 mg/Kg 1 BRL Lead 3/17/2010 1.00 mg/Kg 1 1.39 Manganese 3/17/2010 1.00 mg/Kg 1 1.52 Nickel 3/17/2010 1.00 mg/Kg 1 2.90 Selenium 3/17/2010 2.00 mg/Kg 1 BRL 

### MERCURY, TOTAL D3684/SW7471 Anal yst: SUB

Mercury 3/19/2010 0.100 mg/Kg 1 BRL 

### ASH, OIL D482 Anal yst: VJO

Ash 3/18/2010 0.0100 % 1 0.0800 

### CHLORINE E776/9253 Anal yst: VJO

Chlorine 3/22/2010 0.0100 % 1 0.0300 

### CARBON, HYDROGEN, NITROGEN (OIL) D5291 Anal yst: VJO

Carbon 3/18/2010 0.01 % 1 86.4 Hydrogen 3/18/2010 0.01 % 1 11.4 Nitrogen 3/18/2010 0.01 % 1 0.44 

### FLUORINE D3761 Anal yst: VJO

Fluorine 3/22/2010 0.0100 mg/Kg 1 17.0
Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 3 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search

### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8

HEATING VALUE BTU/LB D240 Anal yst: VJO

Heating Value 3/22/2010 50 Btu/lb 1 18,240 

### OXYGEN BY DIFFERENCE D5291 Anal yst: VJO

Oxygen 3/18/2010 0.0100 % 1 0.360 

### SULFUR D1552 Anal yst: VJO

Sulfur 3/18/2010 0.0100 % 1 1.40

Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 4 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search

### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8



### Client Sample ID: FG1077-01R \ SAMPLES #3 @ Lab ID: R10030049-03 Matrix: OIL Analyses Result Qual Units Date Analyzed Limit DF Date Sampled: 02/24/2010 0:00 Date Received: 03/15/2010

ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony 3/17/2010 3.00 mg/Kg 1 BRL Arsenic 3/17/2010 2.00 mg/Kg 1 BRL Beryllium 3/17/2010 1.00 mg/Kg 1 BRL Cadmium 3/17/2010 1.00 mg/Kg 1 BRL Chromium 3/17/2010 1.00 mg/Kg 1 BRL Cobalt 3/17/2010 0.100 mg/Kg 1 BRL Lead 3/17/2010 1.00 mg/Kg 1 BRL Manganese 3/17/2010 1.00 mg/Kg 1 1.41 Nickel 3/17/2010 1.00 mg/Kg 1 2.89 Selenium 3/17/2010 2.00 mg/Kg 1 BRL 

### MERCURY, TOTAL D3684/SW7471 Anal yst: SUB

Mercury 3/19/2010 0.100 mg/Kg 1 BRL 

### ASH, OIL D482 Anal yst: VJO

Ash 3/18/2010 0.0100 % 1 0.0800 

### CHLORINE E776/9253 Anal yst: VJO

Chlorine 3/22/2010 0.0100 % 1 0.0200 

### CARBON, HYDROGEN, NITROGEN (OIL) D5291 Anal yst: VJO

Carbon 3/18/2010 0.01 % 1 86.6 Hydrogen 3/18/2010 0.01 % 1 11.3 Nitrogen 3/18/2010 0.01 % 1 0.46 

### FLUORINE D3761 Anal yst: VJO

Fluorine 3/22/2010 0.0100 mg/Kg 1 15.0
Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 5 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search

### Project: B026217-Vienna Lab Order: R10030049 Date: 29-Mar-10 

## Certificate of Analytical Results
CLIENT: Maxxam Analy tical Services 6740 Campobello Road Mississauga, Ontario L5N 2L8

HEATING VALUE BTU/LB D240 Anal yst: VJO

Heating Value 3/22/2010 50 Btu/lb 1 18,330 

### OXYGEN BY DIFFERENCE D5291 Anal yst: VJO

Oxygen 3/18/2010 0.0100 % 1 0.150 

### SULFUR D1552 Anal yst: VJO

Sulfur 3/18/2010 0.0100 % 1 1.46

Qualifiers: J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank S - Spike Recovery outside accepted recovery limits R - RPD outside accepted recovery limits BRL - Below Reporting Limit E - Value above quantitation range * - Value exceeds Maximum Contaminant Level 

### Page 6 of 6 H - Hold Time excedance N - Tentatively identified compound based on mass spectral library search