Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

Client Sample ID: FG1075-01R \ SAMPLES #1 @

Lab ID: R10030049-01

Matrix: OIL

Analyses Result Qual Units Limit DF Date Analyzed

Date Received:03/15/2010 Date Sampled: 02/23/2010 0:00

 ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony BRL 3.00 mg/Kg 1 3/17/2010

Arsenic BRL 2.00 mg/Kg 1 3/17/2010

Beryllium BRL 1.00 mg/Kg 1 3/17/2010

Cadmium BRL 1.00 mg/Kg 1 3/17/2010

Chromium BRL 1.00 mg/Kg 1 3/17/2010

Cobalt BRL 0.100 mg/Kg 1 3/17/2010

Lead BRL 1.00 mg/Kg 1 3/17/2010

Manganese 1.58 1.00 mg/Kg 1 3/17/2010

Nickel 1.84 1.00 mg/Kg 1 3/17/2010

Selenium BRL 2.00 mg/Kg 1 3/17/2010

MERCURY, TOTAL D3684/SW7471 Analyst: SUB

Mercury BRL 0.100 mg/Kg 1 3/19/2010

ASH, OIL D482 Analyst: VJO

Ash 0.150 0.0100 % 1 3/18/2010

CHLORINE E776/9253 Analyst: VJO

Chlorine 0.0200 0.0100 % 1 3/22/2010

CARBON, HYDROGEN, NITROGEN (OIL) D5291 Analyst: VJO

Carbon 86.6 0.01 % 1 3/18/2010

Hydrogen 11.2 0.01 % 1 3/18/2010

Nitrogen 0.45 0.01 % 1 3/18/2010

FLUORINE D3761 Analyst: VJO

Fluorine 13.0 0.0100 mg/Kg 1 3/22/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 1 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search
Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

HEATING VALUE BTU/LB D240 Analyst: VJO

Heating Value 18,310 50 Btu/lb 1 3/22/2010

OXYGEN BY DIFFERENCE D5291 Analyst: VJO

Oxygen 0.190 0.0100 % 1 3/18/2010

SULFUR D1552 Analyst: VJO

Sulfur 1.35 0.0100 % 1 3/18/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 2 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search
Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

Client Sample ID: FG1076-01R \ SAMPLES #2 @

Lab ID: R10030049-02

Matrix: OIL

Analyses Result Qual Units Limit DF Date Analyzed

Date Received:03/15/2010 Date Sampled: 02/23/2010 0:00

 ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony BRL 3.00 mg/Kg 1 3/17/2010

Arsenic BRL 2.00 mg/Kg 1 3/17/2010

Beryllium BRL 1.00 mg/Kg 1 3/17/2010

Cadmium BRL 1.00 mg/Kg 1 3/17/2010

Chromium 1.14 1.00 mg/Kg 1 3/17/2010

Cobalt BRL 0.100 mg/Kg 1 3/17/2010

Lead 1.39 1.00 mg/Kg 1 3/17/2010

Manganese 1.52 1.00 mg/Kg 1 3/17/2010

Nickel 2.90 1.00 mg/Kg 1 3/17/2010

Selenium BRL 2.00 mg/Kg 1 3/17/2010

MERCURY, TOTAL D3684/SW7471 Analyst: SUB

Mercury BRL 0.100 mg/Kg 1 3/19/2010

ASH, OIL D482 Analyst: VJO

Ash 0.0800 0.0100 % 1 3/18/2010

CHLORINE E776/9253 Analyst: VJO

Chlorine 0.0300 0.0100 % 1 3/22/2010

CARBON, HYDROGEN, NITROGEN (OIL) D5291 Analyst: VJO

Carbon 86.4 0.01 % 1 3/18/2010

Hydrogen 11.4 0.01 % 1 3/18/2010

Nitrogen 0.44 0.01 % 1 3/18/2010

FLUORINE D3761 Analyst: VJO

Fluorine 17.0 0.0100 mg/Kg 1 3/22/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 3 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search
Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

HEATING VALUE BTU/LB D240 Analyst: VJO

Heating Value 18,240 50 Btu/lb 1 3/22/2010

OXYGEN BY DIFFERENCE D5291 Analyst: VJO

Oxygen 0.360 0.0100 % 1 3/18/2010

SULFUR D1552 Analyst: VJO

Sulfur 1.40 0.0100 % 1 3/18/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 4 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search
Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

Client Sample ID: FG1077-01R \ SAMPLES #3 @

Lab ID: R10030049-03

Matrix: OIL

Analyses Result Qual Units Limit DF Date Analyzed

Date Received:03/15/2010 Date Sampled: 02/24/2010 0:00

 ICP METALS, TOTAL SW6010B Analyst: CBP

Antimony BRL 3.00 mg/Kg 1 3/17/2010

Arsenic BRL 2.00 mg/Kg 1 3/17/2010

Beryllium BRL 1.00 mg/Kg 1 3/17/2010

Cadmium BRL 1.00 mg/Kg 1 3/17/2010

Chromium BRL 1.00 mg/Kg 1 3/17/2010

Cobalt BRL 0.100 mg/Kg 1 3/17/2010

Lead BRL 1.00 mg/Kg 1 3/17/2010

Manganese 1.41 1.00 mg/Kg 1 3/17/2010

Nickel 2.89 1.00 mg/Kg 1 3/17/2010

Selenium BRL 2.00 mg/Kg 1 3/17/2010

MERCURY, TOTAL D3684/SW7471 Analyst: SUB

Mercury BRL 0.100 mg/Kg 1 3/19/2010

ASH, OIL D482 Analyst: VJO

Ash 0.0800 0.0100 % 1 3/18/2010

CHLORINE E776/9253 Analyst: VJO

Chlorine 0.0200 0.0100 % 1 3/22/2010

CARBON, HYDROGEN, NITROGEN (OIL) D5291 Analyst: VJO

Carbon 86.6 0.01 % 1 3/18/2010

Hydrogen 11.3 0.01 % 1 3/18/2010

Nitrogen 0.46 0.01 % 1 3/18/2010

FLUORINE D3761 Analyst: VJO

Fluorine 15.0 0.0100 mg/Kg 1 3/22/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 5 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search
Project: B026217-Vienna

Lab Order: R10030049

Date: 29-Mar-10

Certificate of Analytical Results

CLIENT: Maxxam Analytical Services

6740 Campobello Road

Mississauga, Ontario L5N 2L8 

HEATING VALUE BTU/LB D240 Analyst: VJO

Heating Value 18,330 50 Btu/lb 1 3/22/2010

OXYGEN BY DIFFERENCE D5291 Analyst: VJO

Oxygen 0.150 0.0100 % 1 3/18/2010

SULFUR D1552 Analyst: VJO

Sulfur 1.46 0.0100 % 1 3/18/2010

Qualifiers: 

J - Analyte detected below quantitation limits

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

BRL - Below Reporting Limit

E - Value above quantitation range

* - Value exceeds Maximum Contaminant Level

Page 6 of 6

H - Hold Time excedance

N - Tentatively identified compound based on mass

 spectral library search