Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

54755 Westmoreland Partners Roanoke Valley Boiler 2 bituminous Energy Authority
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received Higher Heating Value

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Moisture

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Ash

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Sulfur

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Higher Heating Value

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis % Ash

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis % Sulfur

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Antimony

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Arsenic

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Beryllium

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Cadmium

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Chlorine

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Chromium

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Cobalt

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Fluorine

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Lead

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Manganese

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Mercury

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Nickel

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D3302

ASTM D3174/D5142

ASTM D4239 Method B

ASTM D5865

ASTM D3174/D5142

ASTM D4239 Method B

ASTM D3683

ASTM D3683

ASTM D3683

ASTM D3683

ASTM D6721

ASTM D3683

ASTM D3683

ASTM D3761

ASTM D3683

ASTM D3683

ASTM D6722

ASTM D3683

ASTM D3683
EIA Facility Code Facility Name Boiler ID HAPs Test Group

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

19 6/20/2010 6/20/2010 12271.00 Btu/lb

20 6/20/2010 6/20/2010 12454.00 Btu/lb

21 6/20/2010 6/20/2010 12408.00 Btu/lb

22 6/20/2010 6/20/2010 12286.00 Btu/lb

28 6/29/2010 6/29/2010 12841.00 Btu/lb

29 6/29/2010 6/29/2010 12611.00 Btu/lb

30 6/30/2010 6/30/2010 12943.00 Btu/lb

31 6/30/2010 6/30/2010 12992.00 Btu/lb

32 7/1/2010 7/1/2010 12924.00 Btu/lb

33 7/1/2010 7/1/2010 12839.00 Btu/lb

 Fuel Testing Results


metalic HAPs

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

5.03 12.65 0.81 12922 Btu/lb 13.32 0.85

4.61 12.1 0.81 13056 Btu/lb 12.69 0.85

4.32 12.39 0.81 12968 Btu/lb 12.95 0.84

4.69 12.88 0.84 12890 Btu/lb 13.51 0.88

5.03 9.39 1.3 13521 Btu/lb 9.89 1.37

5.14 10.77 1.27 13293 Btu/lb 11.35 1.34

4.88 8.92 1.14 13607 Btu/lb 9.38 1.2

4.57 9.05 1.32 13615 Btu/lb 9.48 1.38

4.76 9.59 1.23 13570 Btu/lb 10.07 1.29

4.87 9.46 1.19 13497 Btu/lb 9.84 1.25


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

790 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 3

840 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 3

860 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 3

770 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 4

1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

1000 ppm 0.07 μg/g <2.0 μg/g 6 μg/g 4

1000 ppm 0.09 μg/g <2.0 μg/g 11 μg/g 4

1100 ppm 0.09 μg/g <2.0 μg/g 6 μg/g 4

1100 ppm 0.08 μg/g <2.0 μg/g 7 μg/g 4


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g <2.0 μg/g 28 μg/g 13 μg/g 11 μg/g

μg/g <2.0 μg/g 28 μg/g 20 μg/g 11 μg/g

μg/g <2.0 μg/g 25 μg/g 13 μg/g 63 μg/g

μg/g <2.0 μg/g 28 μg/g 14 μg/g 12 μg/g

μg/g <2.0 μg/g 15 μg/g 11 μg/g 12 μg/g

μg/g <2.0 μg/g 15 μg/g 12 μg/g 14 μg/g

μg/g <2.0 μg/g 15 μg/g 10 μg/g 11 μg/g

μg/g <2.0 μg/g 14 μg/g 11 μg/g 9 μg/g

μg/g <2.0 μg/g 17 μg/g 12 μg/g 11 μg/g

μg/g <2.0 μg/g 16 μg/g 11 μg/g 12 μg/g


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

15 μg/g <2.0 μg/g 70 ppm 12 μg/g

16 μg/g <2.0 μg/g 63 ppm 13 μg/g

14 μg/g <2.0 μg/g 62 ppm 12 μg/g

14 μg/g <2.0 μg/g 68 ppm 13 μg/g

12 μg/g <2.0 μg/g 82 ppm 10 μg/g

12 μg/g <2.0 μg/g 63 ppm 10 μg/g

11 μg/g <2.0 μg/g 91 ppm 9 μg/g

10 μg/g <2.0 μg/g 62 ppm 9 μg/g

13 μg/g <2.0 μg/g 74 ppm 10 μg/g

11 μg/g <2.0 μg/g 69 ppm 9 μg/g

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Oxygen


EIA Facility Code Facility Name Boiler ID HAPs Test Group

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

28 6/29/2010 6/29/2010 12841.00 Btu/lb

29 6/29/2010 6/29/2010 12611.00 Btu/lb

30 6/30/2010 6/30/2010 12943.00 Btu/lb

31 6/30/2010 6/30/2010 12992.00 Btu/lb

32 7/1/2010 7/1/2010 12924.00 Btu/lb

33 7/1/2010 7/1/2010 12839.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

5.03 9.39 1.3 13521 Btu/lb 9.89 1.37

5.14 10.77 1.27 13293 Btu/lb 11.35 1.34

4.88 8.92 1.14 13607 Btu/lb 9.38 1.2

4.57 9.05 1.32 13615 Btu/lb 9.48 1.38

4.76 9.59 1.23 13570 Btu/lb 10.07 1.29

4.87 9.46 1.19 13497 Btu/lb 9.84 1.25


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

1000 ppm 0.07 μg/g <2.0 μg/g 6 μg/g 4

1000 ppm 0.09 μg/g <2.0 μg/g 11 μg/g 4

1100 ppm 0.09 μg/g <2.0 μg/g 6 μg/g 4

1100 ppm 0.08 μg/g <2.0 μg/g 7 μg/g 4


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g <2.0 μg/g 15 μg/g 11 μg/g 12 μg/g

μg/g <2.0 μg/g 15 μg/g 12 μg/g 14 μg/g

μg/g <2.0 μg/g 15 μg/g 10 μg/g 11 μg/g

μg/g <2.0 μg/g 14 μg/g 11 μg/g 9 μg/g

μg/g <2.0 μg/g 17 μg/g 12 μg/g 11 μg/g

μg/g <2.0 μg/g 16 μg/g 11 μg/g 12 μg/g


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

12 μg/g <2.0 μg/g 82 ppm 10 μg/g

12 μg/g <2.0 μg/g 63 ppm 10 μg/g

11 μg/g <2.0 μg/g 91 ppm 9 μg/g

10 μg/g <2.0 μg/g 62 ppm 9 μg/g

13 μg/g <2.0 μg/g 74 ppm 10 μg/g

11 μg/g <2.0 μg/g 69 ppm 9 μg/g


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analyses, % by wt Ultimate Analyses, % by wt


 basis (including ash).

Oxygen


EIA Facility Code Facility Name Boiler ID HAPs Test Group

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

23 6/28/2010 6/28/2010 12513.00 Btu/lb

24 6/28/2010 6/28/2010 12558.00 Btu/lb

25 6/28/2010 6/28/2010 12386.00 Btu/lb

26 6/28/2010 6/28/2010 12320.00 Btu/lb

27 6/28/2010 6/28/2010 12583.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

4.9 11.29 0.96 13158 Btu/lb 11.87 1.01

4.43 11.45 1.03 13141 Btu/lb 11.98 1.08

4.67 12.24 0.98 12993 Btu/lb 12.84 1.03

4.76 12.67 0.97 12935 Btu/lb 13.3 1.02

4.37 11.42 0.96 13158 Btu/lb 11.94 1.01


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

910 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 3

900 ppm 0.11 μg/g <2.0 μg/g <2.0 μg/g 4

970 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

860 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4

910 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g <2.0 μg/g 24 μg/g 15 μg/g 10 μg/g

μg/g <2.0 μg/g 25 μg/g 14 μg/g 10 μg/g

μg/g <2.0 μg/g 23 μg/g 13 μg/g 11 μg/g

μg/g <2.0 μg/g 25 μg/g 14 μg/g 11 μg/g

μg/g <2.0 μg/g 24 μg/g 13 μg/g 21 μg/g


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

14 μg/g <2.0 μg/g 85 ppm 14 μg/g

14 μg/g <2.0 μg/g 121 ppm 13 μg/g

15 μg/g <2.0 μg/g 71 ppm 13 μg/g

14 μg/g <2.0 μg/g 90 ppm 13 μg/g

15 μg/g <2.0 μg/g 69 ppm 13 μg/g

Proximate Analyses, 


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm