EMISSION TEST REPORT 

Performance Test 

Of the 

Lime Scrubber System 

Associated with the 

Plant 2 Kiln (EPN NK-1) 

At the 

Tiffany Brick Company LP dba Hanson Brick 

Located in 

Elgin, Texas 

Prepared for 

Hanson Brick, Inc. 

October 2007 

TRC Project No. 154785 
EMISSION TEST REPORT 

Performance Testing 

Of the 

Lime Scrubber System 

Associated with the 

Plant 2 Kiln (EPN NK-1) 

At the 

Tiffany Brick Company LP dba Hanson Brick 

Located in 

Elgin, Texas 

Prepared for 

Hanson Brick, Inc. 

October 2007 

TRC Project No. 154785 
TABLE OF CONTENTS 

INTRODUCTION 1 

Table 1: Background Data 2 

SUMMARY OF RESULTS 4 

Table 2: Summary of Results Plant 2 Kiln Scrubber 5 

PROCESS DESCRIPTION 6 

ANALYTICAL TECHNIQUE 7 

Table 3: Analytical Instrumentation 11 

Figure 1: Sample System Diagram 12 

Figure 2: PM System Diagram 12 

QUALITY ASSURANCE ACTIVITIES 13 

APPENDICES 

A. Field Data Sheets 

B. Example Calculations 

C. Quality Assurance Activities 

D. Calibration Certifications 

E. Data Acquisition/Gas Chromatograms/Ion Chromatograms 

F. Process Data 
INTRODUCTION 

A performance test of the Lime Scrubber associated with the Plant 2 Kiln designated as 

EPN NK-1 (Plant 2 Kiln Scrubber) was conducted at the Tiffany Brick Company LP dba 

Hanson Brick (Hanson Brick) Elgin Facility, located at 506 Highway 290 East, Elgin, 

Bastrop County, Texas. The purpose of this test was to satisfy pennit requirements for 

Texas Commission on Environmental Quality (TCEQ) Permit #48992, Special Condition 

12. TRC of Austin, Texas conducted the testing on October 21, 2007. 

TCEQ Pennit #48992 requires that the Plant 2 Kiln Scrubber be tested to establish the 

actual quantities of nitrogen oxides (NOx), carbon dioxide (CO), sulfur dioxide (S02), 

particulate matter (PM), and opacity being emitted from the Plant 2 Kiln Scrubber. In 

addition, the removal efficiency of hydrogen fluoride (HF), hydrogen chloride (HCl), and 

S02 was determined as required. The tests followed the procedures set forth in the Code 

of Federal ReQulations, Title 40, Part 60, Appendix A Methods 1, 2, 3A, 4, 5, 6C, 7E, 9, 

10, 18, 25A and 26. Table 1 summarizes the background information pertinent to these 

tests. 

This report has been reviewed and approved for submittal to the TCEQ by the following 

representatives: 

TR : 

;V

ared by 

,~/ 

Hanson Brick 

~~C ~~ 

TRC: Reviewed by 
TABLE 1 

BACKGROUND DATA 

Facility Owner/Operator: Tiffany Brick Company LP 

Dba Hanson Brick 

506 Highway 290 East 

Elgin, Texas 78621 

Attn: Brad George 

TEL (713) 466-6306 

FAX (713) 466-6357 

Test Contractor: TRC 

9225 U. S. Highway 183 South 

Austin, Texas 78747 

Attn: Jason Grizzle 

TEL (512) 243-0202 

FAX (512) 243-0222 

Test Participants: Hanson Brick 

Brad George 

Kevin Emberton 

Paul Anderson 

TRC 

Jason Grizzle 

ShunilJacob 

Jeff Militar 

Thor Olsen 

Paul Campbell 

Ryan McDonald 

Cody Jaysek 

Test Dates: October 21, 2007 

Location: Elgin, Bastrop County, Texas 

Emission Points: Feed Rates from the Plant 2 Kiln Scrubber Inlet 

were measured from a 41.75-inch internal diameter 

duct. See diagrams in Appendix A. 

Emissions from the Plant 2 Kiln Scrubber Exhaust 

were measured from a 55-inch internal diameter 

exhaust stack. See diagrams in Appendix A. 

2 
Test Methods: EPA Method 1 for traverse point location 

EPA Method 2 for stack volumetric flow 

EPA Method 3A for 02 / COz concentrations 

EPA Method 4 for stack gas moisture content 

EPA Method 5 for particulate matter emissions 

EPA Method 6 for S02 concentrations 

EPA Method 7E for NOx concentrations 

EPA Method 9 for opacity determinations 

EPA Method 10 for CO concentrations 

EPA Method 18 for methane and ethane concentrations 

EPA Method 25A for stack THC concentrations 

EPA Method 26 for HF and HCl concentrations 
SUMMARY OF RESULTS 

On October 21, 2007, a performance test was conducted on the Lime Scrubber associated 

with the Plant 2 Kiln designated as EPN NK-1 (Plant 2 Kiln Scrubber), at the Tiffany 

Brick Company LP dba Hanson Brick (Hanson Brick) Elgin Facility, located in Elgin, 

Bastrop County, Texas. The purpose of the performance tests was to measure the nitrogen 

oxides (NOx), carbon monoxide (CO), sulfixr dioxide (SOz), particulate matter (PM), 

volatile organic compounds (VOC), and opacity emissions from the Plant 2 Kiln 

Scrubber as required by the Texas Commission on Environmental Quality (TCEQ) Permit 

#48992. In addition, the removal efficiencies of hydrogen fluoride (HF), hydrogen 

chloride (HCl) and S02 were determined as required by TCEQ Pennit #48992. 

The test matrix consisted of three one-hour test runs conducted on the Plant 2 Kiln 

Scrubber while operating at maximum conditions. During each test run, quantities of HF, 

HCl, and S02 were measured at the inlet and exhaust of the scrubber in conjunction with 

the volumetric flow rates of each. The feed and emission rates for HF, HCl, and S02 

were calculated using the concentration and corresponding volumetric flow rates 

measured during each run. The removal efficiencies of HF, HCI, and SOZ were 

calculated from the feed and emission rates using the following equation. 

CE (%) =(Inlet Loadine (lb/hr) - Outlet Emission Rate (lb/hr) x 100 

Inlet Loading (lb/hr) 

In conjunction with the determination of the removal efficiencies, the emission rates of 

NOx, CO, PM, and VOC were detennined over three, one-hour test runs. During each 

run the quantities of NOx, CO, PM, and VOC were measured from the exhaust of the 

Plant 2 Kiln Scrubber along with the volumetric flow rates. The emission rates of NOx, 

CO, PM, and VOC were calculated using the concentrations and corresponding 

volumetric flow rate measured during each run. The visible emissions from the Plant 2 

Kiln Scrubber were determined over a six-minute period during each test run to 

determine the compliance status with the TCEQ Permit # 48992. 

For the determination of VOCs being emitted from the Plant 2 Kiln Scrubber, the 

methane and ethane concentrations as propane were subtracted from the concentrations of 

total hydrocarbons (THC) during each test run. The THC concentrations are determined 

on a propane basis. 

Table 2 provides the summary for these performance tests of the Plant 2 Kiln Scrubber 

while being operated at the maximum conditions. All field data sheets utilized in this 

testing are presented in Appendix A of this report. Example calculations are located in 

Appendix B. Quality assurance activities are documented in Appendix C. Calibration 

certifications supporting the results are in Appendix D. Data acquisition and 

chromatograms records from TRC instrumentation can be found in Appendix E. Process 

data is contained in Appendix F. 

10 
TABLE 2 

Summary of Results 

Hanson Brick 

Elgin, Texas 

Technicians: JSG, SJ, JM, PC, TO, RAM, CJ 

Project Number: 154785 

SOURCE HIln 2 Scrubber 

TEST RUN 1 2 3 Avera es 

Date 10/21/2007 10/21/2007 10/21/2007. 

Star[ Time 10:53 13:05 16:02 

Stop Time,~~'* 11:53 1tA4:0a5t 17:02 

~ C~$Su.".L , ~ A ll ..t

~ 

Lime Feed Rate (lb/hr) 167 167 167 167 

Number of Cars (Cars/Day) 28 28 28 28 

Tons of Brlck Fired (tons/hr) 10.56 10.56 10.56 10.56 

Kiln Combustible Air Pressure (PSIG) 15.13 13.65 ND 14.39 

Kiln Natrual Gas Pressure (PSIG) 42 42 42 42 

Kiln Overpressure Fan Speed (RPM) 2,508 2,508 2,508 2,508 

Itiln P*,ressure (inH2O)Y -0.15~$ -0.08 ND -0.11 

Atmospheric Pressure (in. Hg) 29.37 29.35 29.31 29.35 

Wet Bulb (°F) 70 70 71 70 

Dry Bulb (°F) 84 84 87 85 

Humidity ~(~](bs/.Ib of air) . ~~qp~ 0.50283 0.0283g 0.0314 0.0293 

uv~u.p.9.'~1' ~~ ~~F„~ 3'+i {~C d~ E~~' ., I"S'St ry,.. HaCtf}'~w^.'k'"~C°' ..~ ... 

Volumetric Flow (DSCFH) 1,333,675 1,357,007 1,293,257 1,327,980 

Volumetric Flow (WSCFH) 1,415,149 1,447,621 1,375,350 1,412,707 

HF (ppmv, dry) 27.5 44.2 46.5 39.4 

HCI (ppmv, dry) 9.01 17.9 35.7 20.8 

SOi (ppmv, dry) 193 153 161 169 

HF Qb/]v) 1.90 3.11 3.1 2.71 

HCl (Ib/hr) 1.14 2.29 4.4 2.60 

SOi (]b/hr) { ~ 42.8 34.4 34.7 37.3 

~1 Te ~.`~a~t''~ 

Volumetric Flow (DSCFH) 1,333,675 1,357,007 1,293,257 1,327,980 

Volumetric Flow (WSCFH) 1,415,149 1,447,621 1,375,350 1,412,707 

Oi (vol %, dry) 18.4 18.3 18.4 18.4 

COz (vol %, dry) 1.9 1.8 1.7 1.8 

NOx (ppmv, dry) 8.8 9.8 10.2 9.6 

CO (ppmv, dry) 120 116 118 118 

SOi (Ppmv, dry) 19.3 21.9 24.6 21.9 

HF (ppmv, dry) 0.12 0.05 0.07 0.08 

HCl (ppmv, dry) 0.17 0.09 0.38 0.21 

VOC (ppmv, wet) 4.64 2.85 5.06 4.18 

NOx (Ib/hr) 1.40 1.59 1.57 1.52 

CO (Ib/]v) 11.6 11.4 11.1 11.4 

SOi (Ib/Iv) 4.27 4.93 5.29 4.83 

HF (]b/lv) 0.0080 0.0035 0.0050 0.0055 

'HCI (lb/hr) 0.021 0.011 0.046 0.026 

VOC (Ib/Iv) 0.75 0.47 0.79 0.67 

Filterable PM (Ib/hr) 0.62 0.59 0.55 0.59 

Filterable PM (Ib/tons of Fired Brick) 0.06 0.06 0.05 0.06 

Total Suspended PM (]b/hr) 2.55 2.44 2.25 2.42 

Opacity (%) 0.63 0.00 0.21 0.28 v,yu Wffp,~ , .~P~C~: ~ ;:s, 4 ;x:.n. I: 

SOi (%) 90.01 85.68 84.73 86.81 

HF ((%) 99.58 99.89 99.84 99.77 

HC1(%) _. .. 98.16 99.52 . 98.95 98.88 

ND- No Data 

4.33 

14.73 

51.97 

0.40 

0.81 

1.51 

5.13 

0.12 

5.13 

5 

> 

31 

95 

97 

TRC s 
PROCESS DESCRIPTION 

Tiffany Brick Company LP dba Hanson Brick owns and operates a brick manufacturing 

facility located at 506 Highway 290 East, Elgin, Bastrop County, Texas. Within the 

facility is a Lime Scrubber associated with the Plant 2 Kiln designated as EPN NK-1, 

which controls the hydrogen fluoride (HF), hydrogen chloride (HF) and sulfur dioxide 

(S02) emissions. 

The Elgin Plant 2 kiln was built in 1999 by Ceric hic. Bricks are set on the kiln cars in the 

green state and proceed from the extrusion and setting department to the holding room. 

The holding room holds the brick until the dryer needs a car of bricks. The bricks exit the 

dryer with less than %2 % moisture and proceed into the kiln. 

The cars are pushed through the kiln with a large hydraulic cylinder. A car of brick is 

charged into the kiln approximately every 51 minutes, 24 hours per day, seven days per 

week. The kiln can be described as a large counter flow heat exchanger. The first 2/3 of 

the kiln is the firing section. The heat is inputed into the brick by gradually increasing 

temperature zones until it reaches top temperature of approximately 2060 F. The heat is 

supplied by a number of natural gas burners installed in the roof and sides of the kiln. 

The hot gases from the burners in the first 2/3 of the kiln flow counter to the brick travel 

from the hottest zone to the exhaust section of the kiln. The air from the beginning of the 

cooling zone and the firing zone is drawn to the front of the kiln and out the kiln exhaust. 

The exhaust temperature of the gases is approximately 350 F. 

The last 1/3 of the tunnel kiln is the cooling section. The brick are cooled quickly as they 

exit the hottest firing zone until they reach 1300 F. The ambient air from the exit of the 

kiln is passed over the brick with the exit end fan and lowers the brick temperature and 

heats the air to approximately 600F. The 600F air is ducted to the dryer to dry the 

extrusion water from our brick. No additional gas or fuel is required to dry the brick. 

The exhaust gases of the Plant 2 Kiln are routed to the scrubber by the automatic valve 

system. The recirculated lime material is fed into the flue gas piping using frequencycontrolled metering screws, and the fresh lime using a frequency-controlled metering 

screw, at various positions, and therefore into the flue gases. The sorption process 

commences when the material is fed in. There is a process air connection in the flue gas 

piping upstream of the filter unit which is fitted with an automatic valve. This valve is 

used to ensure that the flue gas temperature is reduced to the maximum permissible 

operating temperature of the filter medium if necessary before entering the filter unit. 

The flue gases enriched by the absorbing agents are fed into the filter unit, where the 

bound pollutants are filtered out of the flue gases together with the absorption material 

using the filter media. The flue gases (clean gases) are fed to the fan and then, to the 

exhaust downstream of the filter unit. 

C 
ANALYTICAL TECHNIQUE 

The sampling and analysis procedures used during these tests conformed in principle with 

those outlined in the Code of Federal Regulations, Title 40, Part 60, Appendix A, 

Methods 1, 2, 3A, 4, 5, 6C, 7E, 9, 10, 18, 25A and 26. 

The sampling and analysis system used to determine exhaust emission concentrations is 

depicted in Figure 1. Stack gas entered the sample system through a heated stainless steel 

probe with a glass wool filter. The sample was transported via 3/8-inch heat-traced 

Teflon® tubing using a stainless steel/Teflon® diaphragm pump to the wet portion of the 

sample manifold. The sample was then delivered to a specially designed stainless steel 

minimum-contact condenser that dried the sample without removing the pollutants of 

interest before being passed back to the dry portion of the sample manifold. From the dry 

manifold, the sample was partitioned to the analyzers through glass rotameters that 

controlled the flow of the sample. 

Figure 1 shows that the sampling system was equipped with a separate path through 

which a calibration gas could be delivered to the probe and back through the entire 

sampling system. This allowed for convenient performance of system bias checks and 

calibrations as required by the testing methods. 

All instruments were housed in an air-conditioned trailer-mounted mobile laboratory. 

Gaseous calibration standards were provided in aluminum cylinders with the 

concentrations certified by the vendor, where applicable. 

All data from the continuous monitoring instruments were recorded by a computer data 

acquisition system. The data was recorded at one-minute intervals. 

Velocity determinations using EPA Methods 1 and 2 were conducted during each test 

run. The number and locations of the traverse points were determined according to the 

procedures outlined in EPA Method 1. Velocity measurements at the outlet location were 

made using a Type S pitot tube conforming to the geometric specifications outlined in 

EPA Method 2. Differential pressures were measured with an oil-inclined manometer. 

Gas temperatures were measured with a K-type thermocouple equipped with digital 

readouts. The configuration of the system is such that the outlet flow rates and the inlet 

flow rates are equivalent, so no inlet flow rates were determined during the testing series. 

The stack gas analyses for CO2 and 02 concentrations were performed by Method 3A. 

This analysis was performed on the exhaust outlet samples collected during the testing. A 

nondispersive infrared analyzer was used for CO2 concentration analyses. 02 

concentration analyses were performed by a paramagnetic analyzer. 

Exhaust stack moisture was determined by US EPA Method 4. Stack gas was extracted 

and pulled through a series of iced standard impingers. The dry gas volume was 

measured with a dry gas meter after the impinger train and sampling pump. The amount 

7 
of moisture collected was determined gravimetrically. This sampling train was combined 

with the US EPA Method 5 sampling train depicted in Figure 2. 

US EPA Method 5 was used to determine concentrations of particulate matter, with the 

addition of condensable particulate recovered as required by the TCEQ regulations. 

Figure 2 shows that a gaseous sample was pulled through a stainless steel nozzle and 

heated borosilicate glass lined probe to a heated glass fiber filter. This portion of the 

sample train is utilized to determine filterable particulate matter. The nozzle was sized 

such that an isokinetic sampling rate (i.e. sampling at the same rate as the stack velocity) 

could be maintained within the capabilities of the sample pump. Following the filter, the 

sample was pulled through an impinger train to a dry gas meter and sample pump. The 

impingers were charged with de-ionized water. Filter and probe temperatures were 

maintained at the temperature range specified in the method [248 f 25°F] for each PM 

test run on the Plant 2 Kiln Scrubber. 

The weight gain of the acetone rinse plus the weight gain of the filter constitute the 

filterable PM analysis. The back half of the filter holder, connecting glassware and 

impingers constitute the condensable PM assembly. The first impinger contents from 

each test run were saved after weighing the impingers for moisture content determination. 

The solutions from the first impinger were combined with the back half of the filter 

holder and connecting glassware and saved. Each of these solutions was measured for 

volume. The collection was then evaporated and weighed at TRC's Austin laboratory to 

determine weight gain. The weight gain of these impinger evaporations constitutes the 

condensable, PM analyses. 

All EPA Method 5 particulate matter weights were determined with an AND HR-120 

analytical balance. This balance has a 120-gram capacity and 0.0001-gram sensitivity. 

The balance was leveled and zeroed before each series of weighing. All weighing of 

filters and beakers were repeated until a"constant weight" was obtained. A"constant 

weight" is defined in EPA Method 5 as a difference of no more than 0.5 mg or 1 percent 

of the total weight less tare weight, whichever is greater. This definition applies to two 

consecutive measurements with no less than 6 hours of desiccation time between weights. 

The sample recovery data sheets in Appendix A describe the weighing times and dates. 

The difference between weighing is recorded to establish that a constant weight had been 

obtained. In cases where a weight loss is apparent, the minimum detection limit of the 

scale as described above is recorded. 

All S02 concentrations contained in this report were obtained using the procedures of US 

EPA Method 6C (i.e. instrumental analysis). The instrument used for this analysis is 

based on the principle of ultraviolet absorption. 

Concentrations of NOx were determined using the instrumental analyzer procedure 

described in US EPA Method 7E. Sample gas was continuously extracted from the 

source and a portion of the sample was directed to a chemiluminescent analyzer for 

analysis of NOx. All NOx is reported as NO2 as per EPA convention. 

9 
Opacity was determined using the procedures of US EPA Method 9. These tests were 

conducted during daytime hours that met the sun angle specifications of the method. A 

certified visible emission observer conducted these test run, a certificate of the individual 

can be found in Appendix D. Appendix A provides the opacity observation sheets. 

Concentrations of CO were quantified during the tests in accordance with procedures set 

forth in US EPA Method 10. A continuous non-dispersive infrared (NDIR) analyzer was 

used for this purpose. This analyzer is equipped with a gas correlation filter, which also 

removes any interference from CO2 or other combustion products, eliminating the need 

for ascarite traps, and the associated con-ection factors. 

hiterference response tests on the instruments were conducted by the instrument vendors 

and TRC on the analyzers. The sum of the interference responses for H2O, methane, 

NH3, S02, Hz, NOZ, NOx, CO, COz and 02 (as appropriate for each analyzer) are less 

than t2 percent of the applicable full-scale span value. The instruments used for the tests 

meet the performance specifications for US EPA Methods. The results of these direct 

interference tests are available in Appendix C of this report. 

Methane and ethane concentrations of the exhaust gases were determined by US EPA 

Method 18. The methane and ethane concentrations were detennined by a gas sample 

that was continuously extracted from the source and injected onto a gas chromatograph. 

The Hewlett Packard 5890 Series lI gas chromatograph is equipped with a dual channel; 

heated gas sampling valve for sample injections, 1.0 cc sample loop, split/splitless 

injector, capillary column, and a flame ionization detector. The capillary column used for 

organic compound separation was a 30 meter SGE capillary column (30BP-1-1.0). 

Conditions for the separation were as follows: 

Head pressure: 3 psig 

Sample loop Temp: 160°C 

hiitial Oven Temp: 40°C 

Initial Time: l Omin 

Prior to the collection of data, TRC used calibration standards containing propane to 

confum compound relative retention times. Pollutant concentrations were determined 

using sample detector response to propane. All methane and ethane concentrations were 

based on the propane calibration curves. These concentrations were used to con•ect the 

THC concentrations for the methane and ethane portion to calculate the VOC 

concentrations of the exhaust stream. 

THC concentrations were determined according to the procedures outlined in US EPA 

Method 25A. A continuous sample of stack gas was directed into a heated hydrocarbon 

analyzer. This instrument operates on the principle of flame ionization, in which 

combustion of hydrocarbons results in the generation of carbon ions. This process yields 

a current directly proportional to the carbon content of the molecules in the gas stream. 

The current is converted to voltage output and recorded continuously with a computerized 

data acquisition system. 

~ 
Concentrations of HF and HCl were determined using the procedures of US EPA Method 

26. A sample of stack gas was pulled through a series of chilled impingers and then 

through calibrated dry gas meter with a pump. A series of four impingers were used in 

the sample train with the first two containing 100m1 of a O.1N H2SO4 solution, the third 

impinger was empty, and the fmal impinger contained an indicating silica gel before 

being drawn through the dry gas meter. Leak checks of the sampling train were 

conducted prior to and following each test run. Following testing, the samples were 

recovered in the TRC's mobile laboratory. 

The contents of the first two impingers were transferred to a graduated cylinder. The 

iinpingers and connecting glassware were rinsed three times with Deionized water and 

these rinses were added to the graduated cylinder. The total volume of liquid collected 

was recorded and the sample were transferred to a HPDE bottle and sealed for analysis by 

ion chromatogram. 

Analysis of the halogens was performed by US EPA Method 26 (analysis by ion 

chromatography). Samples were analyzed using a Dionex ion chromatograph. Sample 

analysis was performed in the TRC mobile laboratory following collection. A five-point 

standard curve was generated to quantify each of the ions (fluoride and chloride). 

Conditions for the Dionex Model ICS-90 ion chromatograph were as follows: 

Eluent Flow: 

Eluent Pressure 

Loop Size: 

Pre-Column: 

Column: 

Eluent: 

Regen: 

2.0 ml/min 

5 psig 

10 μl 

IonPac AG14A 37042 

IonPac AS 14A 4mm 10-32 

18 mM Na2CO3/ 10 mM NaHCO3 

0.01 N H2SO4 

10 
TABLE 3 

LIST OF ANALYTICAL INSTRUMENTATION 

Models antl Calibration Minimum Serial 

Parameter Manufacturers Span Sensitivity Number Detection Principle 

NOx CalifomiaAnalytical 0-50.6ppm O.lppm 6MI2004 ThertnalreductionofNOi [oNO. 

400-CLD Chemiluminescent reaction ofNO with excess of 

ozone. Detectionbyphotomultiplierarphotodiode. 

Inherently linear for ranges listed 

CO TEC048C 0-496 ppm 0.2 ppm 48C-73966-375 Infrared absorption, gas filter correlatfon deteclor 

Microprocessor based linearization. 

COz Servomex1400 0-10.07% 0.02% 01415C/2650 Infraredabsorption,analoglinearizaitonsolid 

state detector 

02 Servomex1400 0-10.05% 0.10% 01420Cl/2534 Paramagneticcell,orelectrochemicalcell 

all detection pdncipals are inherently 

Iinear uver a wide range. 

SOz Ametek 921 0-44.3 ppm 0.5 ppm AW-921-6232 Absorbance ofUV light at two frequencies 

Dual cell instrument with matched photo 

detectors and lamp currenl conlol. Calculation 

of concentration by Beer Lambert Law 

Hydrocarbon HewlettPackard 0-lOppm 0.5ppm Flame ionization of hydrocarbons. Capillary 

Species 5890aGasChroma- 0-100ppm CH4 analyticalcolunmforcompoundsepamtion. 

togmph with dual 0-1000 ppm Gas sample size variable with sample loops 

channel FIDs 0-100 % and split mtios. 

THC Model 3-100 0-100 ppm 0.5 ppm 9309261-33 Flame ionization ofhydrocarbons 

Inherently linear over 4 orders of magnitude. 

Temperature Omega HH-26K -I20 to 2000 °F 0.1 °F n/a Chromel-alumel K-Type thennocouple with digitial 

thertnometer. Respnse time based on thermocouple 

design 

Opera[ing range is defined by the calibration gzses used during the test (per EPA Methods 3A, 6C, 7E, 10, 20, and 25A). 

11 
FIGURE 1: SAMPLE SYSTEM DIAGRAM 

FIGURE 2: PM SYSTEM DIAGRAM 

TemperaNreSensor 

HealeE 

Zone 

~ 

Mammeier 

Thermometer 

Slack Wall 

~

f—TemperaNre Sensor 

~Probe 8 Noule 

rPiWtTube 

12 
QUALITY ASSURANCE ACTIVITIES 

A number of quality assurance activities were undertaken before, during, and after this 

testing project to ensure the accuracy of results obtained. This section of the report and 

the documentation contained in Appendices C and D describe each quality assurance 

activity that was performed. 

Sampling and analyses, where appropriate, were conducted on-site to afford any 

interested parties the opportunity to observe all aspects of the test and to circumvent the 

possibility of sample loss or contamination during transport. 

Each instrument's response was checked and adjusted in the field prior to the collection of 

data via multi-point calibration (calibration error). The instrument's linearity was 

checked by first adjusting the zero and span responses to zero (nitrogen) and an upscale 

calibration gas in the range of the expected concentrations. The instrument response was 

then challenged with other calibration gases of known concentration and accepted as 

linear if the response of the other calibration gases agreed within t2 percent of range (t5 

percent of calibration gas for THC only) of the predicted values. The data acquisition 

logs that present the results of the initial multi-point linearity test are provided in 

Appendix E. 

Before and after each test run, the sample system was checked for zero and upscale bias 

(Except for THC). This allowed each test run to be bracketed by calibrations and 

documented the precision of the collected data. The criterion for acceptable data is that 

the sample system bias is within t5 percent for both the zero and upscale calibration 

gases. Documentation of sample system bias also allowed for the use of Equation 7E-4 to 

assess drift. The criterion for acceptable data is that the drift assessment not exceed 3 

percent for both the zero and upscale calibration gases. The Quality Assurance 

worksheets in Appendix C summarize all multipoint calibration checks and the zero and 

upscale checks performed during the tests. Equation 7E-5 was used for the correction of 

gas concentrations for sample system bias. 

When two consecutive test runs were conducted one after the other, the final bias test for 

the previous run was used for the initial bias test of the subsequent run. In cases where 

there was a sufficient delay between test runs to deem this strategy invalid, a separate 

initial calibration was conducted and the response from this calibration was used in 

Equation 7E-5. 

Prior to testing a NOx converter efficiency check was conducted as required by EPA 

Method 7E. To conduct this test, a NO2 calibration gas in nitrogen balance was used as 

allowed by method. The NOx response of the analyzer is monitored until the 

concentration reading stabilizes. The response of the analyzer is then recorded and the 

converter efficiency is calculated using the response of the analyzer and the actual 

concentration of the certified NO2 gas. The converter is acceptable if the analyzer 

indicates a response of 90% or greater. 

13 
The instrumental sampling system was leak checked by demonstrating that a vacuum 

greater than 10" Hg could be held for at least 1 minute with a decline of less than 1" Hg. 

A leak test was conducted after a sample system was set up and before that system was 

dismantled. These tests were conducted to ensure that ambient air had not diluted the 

sample. No leaks were found during the post-test leak checks. 

The absence of leaks in the sampling system was also verified by sample system bias 

checks. The sampling system's integrity was tested by comparing the responses of each 

of the analyzers used to a calibration gas introduced via two paths. The first path was 

into the analyzer via the zero/span calibration manifold (direct to the analyzers). The 

second path was to introduce a calibration gas into the sample system at the sample probe 

via the calibration line and switching valve. Any difference in the instrument responses 

by these two methods was attributed to sampling system bias. Quality Assurance 

worksheets in Appendix C show that the analyzer responses via both sample paths agreed 

within acceptable limits. All bias check results are summarized in the Quality Assurance 

Worksheets in Appendix C. 

Response time tests were conducted on site on the sample system utilized during the tests. 

The control gases used to calibrate the instruments were analyzed and certified by the 

compressed gas vendors to tl% accuracy or EPA Protocol Procedure Gl, as applicable. 

The gas calibration sheets as prepared by the vendor are contained in Appendix D. 

Appendix D also contains calibration data on the altimeter, dry gas meter, and pitot tubes. 

The dry gas meters used for the methods that require one were calibrated prior to testing 

in accordance with EPA methodology. A post test calibration check was also conducted 

on the meter. Calibration certification documentation of the dry gas meters can be found 

in Appendix C. That documentation shows that the difference between the pre and post 

test calibrations differed by less than 5% as required 

All glassware was thoroughly washed, rinsed, dried, and stored with protection to prevent 

contamination. Pre-weighed filters were sealed against contamination and packed safely. 

Reagent grade acetone (HPLC grade) and Deionized water were used for the washing of 

the sampling train as appropriate to the method. A blank of the acetone and the water 

were treated in the same manner as the samples and retained for evaporation and 

weighing for contaminants. A blank filter was also weighed after treating it in the same 

manner as the filters used during sampling. 

Each Method 5 sample train was leak-checked in accordance with Method 5, before and 

after each test run. If leaks were found prior to the test they were corrected before the test 

run started. No leaks were found after the test runs; therefore, no leak compensation was 

performed, and no test runs were voided. 

Isokinetic sampling rates were achieved and checked in the field at each traverse point as 

well as over the entire test run period. Isokinetics between 90% and 110% over the test 

run are required for Method 5. The isokinetic calculation spreadsheets of Appendix A 

show that the sample rate was within acceptable limits. 

14 
The nozzles utilized for isokinetic sampling were checked prior to the sampling event per 

the stipulations of EPA Method 5, §5.1. The nozzles were measured with a micrometer 

upon the completion of sampling, and the post-test nozzle area was used for data 

reduction. 

VOC concentrations were determined by US EPA Method 18. Provisions were made to 

introduce the calibration gases to the instruments under the same conditions as that of the 

samples. Propane standards were injected to establish a calibration standard curve prior 

to sample analysis. Calibration standards injections were repeated until area counts of 

propane from three separate injections agreed to within 5% of their average. Each test 

run consists of a minimum of 5 inj ections of sample gas. Upon completion of testing, the 

mid-range standard was injected to verify the absence of instrument dri8. This 

calibration check was used to ensure that the instrument response had not varied by more 

than 5%. If a variance of greater than 5% was observed, the calibration process was 

repeated and the average of the two calibration curves would be used to determine 

concentrations. All calibrations for the US EPA Method 18 were conducted through the 

entire sample system. 

The dry gas meters used for the HF and HCl sample trains were calibrated prior to testing 

in accordance with EPA Method 5. A post test calibration check was also conducted on 

the dry gas meters. A standard dry gas meter traceable to NIST was used for the initial 

annual calibration and critical orifices used for the post test checks. Calibration 

certification documentation of the dry gas meter can be found in Appendix C. That 

documentation shows that the difference between the pre and post test calibrations 

differed by less than 5% as required by the regulations. 

Each Method 26 sample train was leak-checked in accordance with Method 5, before and 

after each test run. If leaks were found prior to the test, they were corrected before the 

test run started. No leaks were found after the test runs; therefore, no leak compensation 

was performed, and no test runs were voided. 

HF and HCl concentrations were detennined by US EPA Method 26. Calibration 

standards injections were repeated until area counts of each ion from duplicate injections 

agreed to within 5% of their average. Sample runs consist of a minimum of two 

injections that agreed to within 5% of their average. Upon completion of testing 

standards were injected to verify the instrument drift. Duplicate injections were made 

until the areas agreed to within 5% of their average. The average of the pre and post 

calibration curves was used to determine the concentrations of HF and HCI. 

TRC collected and reported the enclosed test data in accordance with the procedures and 

quality assurance activities described in this test report. TRC makes no wan -anty as to the 

suitability of the test methods. TRC assumes no liability relating to the interpretation and 

use of the test data. 

15 
APPENDIX A: 

FIELD DATA SHEETS 
1— 

FIELD TEST PARTICIPANT SIGN IN SHEET 

Job Name: 00,A^5VII ~r` Cle DATE(S): 1 /a /Zl ( e-rJoli Number: /S-q PERMIT# 4 8 9 9a 

Plant Name/Location: cC 

Emission Source(s): 40~ 2 Svt,~ 

PARTICIPANTS: TRC Environmental Corporation Test Contractor 

/',a..."S un T>riL Owner/Operator 

TGFQ 3egulatory Agency 

Name: Affiliation: Position: Telepbone 

Number 

. ~so,-, Cyr, 2zle, 772\,e. P a~ C,U~,_ SiZ -zyf-oznz 

I ~ 0 L rc ~23020 

ul COV4 Pb2ll C Field 16 k_ 52 2Y3 o2a 

0 --F'LL 

-C"PC "Tc~[n 

~ G GUrLGU qqkY&j ErvJ. ,4wa4l ? l3-c 6 _ 766 

U,~ &nA,6 r46ti 14 x li9t, 512-563 -W 

~./ w~JI~ vSU ~tl CtGr, S ~✓' Z 

~ TRC v3.0_052007 
Stack Diagram 

(Draw side view showing major compones, dimensions, upstream/downstream Flow disturbances) 

(NvriZ~ ankal vte..>3 

,n_.k 

t

!i~ 

plr5-~l~iCe I 

iD 

AIow/ 

d i54',n- 6artGQ 

0 

\ F 

- E- - -- as30~ 

~ Z

~I 

( ToppSrapl.~ cal vte:./ ) 

~ et 

I I ,/~d lIrP 

te 

dls 

*Calculated 

Traverse 

Point 

....... ._.. .-_.. E 

*Stack diameters > 24 in shall have no traverse points located wli'n 1 in of the stack wall 

*Stack diameters 5 24 in shall have no traverse points located w!n 0.5 in of the stack wall 

50 '5 

1.0 1.5 2.0 2.5 

Particulate Traverses 

t

40 

30 

24 u ~ 25• 

20 20 slacktllameter>24in 

,2 

10 -Lar9ernumnermr eors~ 

reaanaaiarslaoks siackdizmeler,2-2ein 

0 2 3 4 5 6 7 8 9 10 

outldzmeurs aownNwem Rcm nowa stoNZnm lo¢dnce el 

ouvtaam.mrs upso-exm flcm new asWmanre (oistlnceFl 

50.5 1.0 1.5 2 0 1.5 

Non-Particulale Traverses °"'"" 

40 

30 - cuB I 

20 ~ s sraekniameler>2ain 

z 

10 'LarOernumbertor or 

reclangmarslacks slacBJiamelert2-24in 

6 9 3 6 S fi ] fl 9 1n 

r 

oua 6.m.ma eo.in,o-e.m xom now nimrrbano. (oi.m- el 

*Port 

Length ° 

Offset ~ 

s 

E 

s fi 

Traverse Number of Traverse Points 

Point 4 6 8 

Number I Percent distances 

1 6.7 4.4 3.2 2.1 

2 25.0 14.6 10.5 6.7 

3 75.0 29.6 19.4 11.8 

4 93.3 70.4 32.3 17.7 

5 85.4 67.7 25.0 

6 95.6 80.6 35.6 

7 89.5 64.4 

8 96.8 75.0 

9= 82.3 

10 - 88.2 

11 = 93.3 

12 = - 97.9 

Circular Stack Sampling Traverse Point Layout 

(EPA Method 1) 

Date: /D~~P~~ 

Plant: 1~2n9~~ ~iicLe 

Source: 

Technician(s): Ts~j 

Port+ Stack ID (in): 

Port Extension (in): ~ 

Stack ID (in): 2~y, :75- " 

Stack Area (ft2):9. S 

Duct Diameters upstream from flow disturbance (A):~ 

Duct Diameters downstream from flow disturbance (B): ~ 

Total Required Traverse Points: 17- 

No. of Traverse Points per Diameter: 61 

Stack cross section 

.. . 

~ 

~ 

\ 

Draw traverse point layout above 

Unit Information 

._ _. <- - E- -° ✓F-- ~--I- <- 

+ 3ot 2ti / 

r 1 

misemPonl 

OTRC 
Stratification Test (Method 7E ) 

Company: Hanson Brick 

Plant: Elgin Facility 

Location: Elgin, Texas 

Technicians: JSG, JM, SJ, RAM, PC, TO, CJ 

Source: Plant 2 Kiln Scrubber Inlet 

Is Stack Diameter or Equivalent Diameter greater than 7.8 ft? 

S02 

Point (ppmv) 

1 185.55 

2 194.63 

3 193.23 

Averages 191.14 

Minimum Number of Sampling Points Required: 

Single Point 

FE—M-0—M-1 

Stratification determination by Method 7E, Section 8.1.2 

Testing by TRC 
~ 

SAMPLING DATA FOR : EPA METHOD 26 

Date: t 0

(2t(a

ftest Rurl: ej~ 

Plant: 14an5on _B04 04rometric Pressure (m Hg) 0-1,37 

Location: L ~',A T~ ;&M ID: 

Source: ;(A a Scr bbu (;ntdIDGM Correction Factor: 6. 96~ 

Technicians: p{y) Probe Material/Size: 

d154Z45 

Pre-Test Leak Check Results 

Rate of $3/min 

at a vacuum of 

Leakage rate must be less than 0.02 ft3/min 

at a vacuum of at least 15 in Hg 

.. .. ... . . . ~~K: 

gs @ 10 min intervals 

mipling Clock I DGM 

Time I Time Reading 

)GM/IN I DGM/OUT 

Temp Temp 

7 

~ ~ ~ 

; 

i ~ 

Z -iXH 

SD _ i1 ~ 43 

I: 48 

r.n I I -53 

, 

Post-Test Leak Check Results 

Rate of ('j,p0 ( ft3/min °- 

at a vacuum of +9Z `S 

Leakage rate must be less than 0.002 ft3/miu at a vacuum of at least 15 in 

Final vol' 

Imp ml 

H2SO4 

NaOH. 

WEIGHTS Imp #1 Imp--#2 Imp #3 Imp #4 Imp #5 Imp #6 

Contents IDA \ S:, , 

Begirnning 

Endin 
SAMPLING DATA FOR : EPA METHOD 26 

Date: Test Run:(~Z 

Plant: } Ice o.(3r c k Barometric Pressure (in Hg) Qq, 3-~j 

Location: 1 T X DGM3D: T-3 l39 ~73q 

Source: ~(; ~~ S h,~ t~ ~le~ DGM Correction Factor: (-g--C •q- ® ~ 9 g 7~ !e 

Technicians: Probe Material/Size: ahon 

Pre-Test Leak Check Results 

Rate of 6,),6?0 p ft3/min 

at a vacuum of _,rE 20 

Leakage rate must be less than 0.02 $3/min 

at a vacuum of at least 15 in Hg 

~ . ~ ®~ 

. I 

• 

:. _ 

- 

• ~ u. • • 

: ~ . 

. 

:u. I ~ ~~~- `I~~~L~7~ ` . • / 

~ 

LTiN M Il!+,~ ~t~~WE" 

.~~ • a -~~'/'~~' • ✓ 

~,~~~c~~~ ~. s~~,>~■ 

~ • G, ~-~~~ 

-~

------- 

----- 

------- 

~-----® 

------ 

------- 

Post-Test Leak Check Results 

Rate ,600 ft3/min 

at a v~ 

(~ 

iitlm of 1sLeakage rate must be less than 0.002 113/min at a vacuum of at least 15 in 

Final Vol 

Imp nil 

H2SO4 --~ 

NaOH 

WEIGHTS Imp #1 Imp #2 Imp #3 Imp #4 Imp #5,~; ~ np #6 

Contents 1 n 1 fU N n't r S; Co 

Begmning lD0 w1 1 6 k. I — — — ~ 

Ending --~ 
SAMPLING DATA FOR : EPA METHOD 26 

~ 

Date: /6-7- Test Run:C-3 

Plant: R„c_ k Barometric Pressure (in Hg) 3 ~ 

Location: CI ~ ti -~ x DGM ID:T- ~3 C3ySs73q 

Source: ~<~~ 4 (,~~ 1,,~\DGM CorrectionFac tor: ~~ e, q t~ Lo 

Technicians: (~ M y ~ ~~Probe Material/Size: Te~'/a n 

6ib1'a•<E-AR 

Pre-Test Leak Check Results 

Rate of 0/min 

at a vacuum of /5 ; ~ t-(a 

akage rate must be less than 0.02 ft3/min 

a vacuum of at least 15 in Hg 

readings @ 10 min intervals 768°F 

Sampling 

Time 

(min) 

Clock 

Time 

(24 hr) 

DGM 

Reading 

(ft3) 1 

DGM/IN 

Temp 

DGM/oUT 

Temp 

(°F) 

Last Imp 

Temp 

(°F) 

D 6= 03 y(, X.f 71 

P6-~ ~43.~f5 ! l0 54.5 

(o - 945.133 1 160.3 5'Y5 

t5 16: (8 `i'l1.605 I jo?_ 9U Y 

20 (6= 23 8:935 oz f m 0 '5. 6 

25 b=2?, 0.750 !e2 &.g 

0 6= 33 452.585 loz ial. M'.D 

S 112zw SY. vo 5 02 iol,t 576 

o 16<Y3 6.?1i2 Go2 fof.6 5.(2 

o Z o•6 S. 

55 loz fDo 

o ( :0 6 -5W 102- 101.5 7 

Post-Test Leak Check Results 

Rate of ft3/min 

at a vacuuni of 

Leakage rate must be less than 0.002 ft3/min at a vacuum of at least 15 in 

Fina1 Vol 

Imp ml 

H2SO4 ~ 

~ 

NaOH 

WEIGHTS Imp #1 Imp #2 Imp #3 Imp #4 Imp #5 Imp #6 

Contents 

l Ending 

~ 
q 

~ 

®, 

/ 

~ 

T 

~ T rn lek 

~ 

ilet 1 Lee- 

~ 

m 

M 

nCe 

pr,arpae~ 

 n a ,n 

, a, 

~ 

C 

s 

~ 

50 'S 

1.0 1.5 2.0 2.5 

Non-Particulate Traverses °"•^^ 

40 a sk 

30 

6 I 

ZO 16 slackaiamemr>z4in 

1z 

10 •1-arser moerror 

ar:ra=k: ecaeiamecarl2za'in renaaew =k 

n 

O 

L% 

2 3 4 5 6 7 8 9 10 

oen ei.meea aow=:ve.m nam now ai:mre.=<e (oi:u=r. e) 

b 

oun ai.mm.rs u>mr.zm rtom now aawmznw lowi 

50 'S 1.0 1.5 2.0 2.5 

Particulate Traverses q p ~ 

ao = ~ • 

e I 

30 

24 or 25- 

20 20 sracktliameler>24in 

16 

12 

10 -Laraernemeermr eorsrananeuiarera=ka slackaiamerer,z-zaib 

0 

9 z a 5 a 7 

oula,m,r,B ae..,a„m,ram aa. a s,imm.- roerarr 

ew, - tb.nmi 

Circular Stack Sampling Traverse Point Layout 

/ (EPA Method 1) 

Date: /dlZO/ O~- 

Plant: 119,60n &;c 

Source: ~;an.~~iv~ Erhavs 

Technician(s): 

Port+ Stack ID (in):54 

Port Extension (in):y,y 

Stack ID (in): ~ 

Stack Area (ft2): 

Duct Diameters upstream from flow disturbance (A): :~L 

Duct Diameters downstream from flow disturbance (B):13 

Total Required Traverse Points: 7b 

No. of Traverse Points per Diameter: ;5Y 

Stack Diagram 

(Draw side view showing major components, dimensions, upstream/downstream flow disturbances) 

tacK cross secnon 

Mv 

~

.'. 

\, 

..: ~~ .. 

Draw traverse point layout above 

Unit Information 

Traverse Number of Traverse Points on a Diamete *Calculated *Port 

Point ~4 6 8 12 Traverse Length 

Number I Percentdistances(%) Point Offset 

2 25.0 14.6 10.5 6.7 

3 75.0 29.6 19.4 11.8 

____...,......__... 

4 93.3 70.4 32.3 17.7 

_ _. ..... _.. _ _._. _.... 

5 85.4 67.7 25.0 

6 95.8 80.6 35.6 

7 89.5 64.4 

8 96.8 75.0 

9 82.3 

1088.2 

12 97.9 

*Stack diameters > 24 in shall have no traverse points located wi n 1 in of the stack wall 

'Stack diameters <_ 24 in shall have no traverse points located w/in 0.5 in of the stack wall 

TRC 
Stratification Test (Method 7E ) 

Company: Hanson Brick 

Plant: Elgin Facility 

Location: Elgin, Texas 

Technicians: JSG, JM, SJ, RAM, PC, TO, CJ 

Source: Plant 2 Kiln Scrubber Outlet 

Is Stack Diameter or Equivalent Diameter greater than 7.8 ft? 

02 

Point (%) 

1 18.52 

2 18.46 

3 18.38 

Averages 18.45 

Minimum Number of Sampling Points Required: 

Single Point 

Stratification determination by Method 7E, Section 8.1.2 

Testing by TRC 
SAMPLING DATA FOR : EPA METHOD 26 

Date: / o/21 1 o7 Test Run: G — ~ 

Plant: 9uh54, 8 Barometric Pressure (in Hg) 21 37 7

Location: E1 ;A ( DGM ID: 95 y 9$ Q 

Source: I 1 r ~„ ~P„ au}le} DGM Correction Fac tor: 

Technicians: 7~ To ProbeMateriaUSize: 

-4F t5H'1'65 

-e-Test Leak Check Results 

ite of 0 • ob ( ft3/min 

a vacuum of 

Leakage rate must be less than 0.02 $3/min 

at a vacuum of at least 15 in Hg 

. ~ 

~~ 

~ ~ 

-~~~' 

• i • • . 

M~= rNE - ~ r~ 

®~~ ~ ~ • -~~ ~~~ ~.' 

------- 

------- 

------- 

------- 

------- 

------® 

-~----- 

--- ~- -- 

Post-Test Leak Check Results 

Rate of p,poN ft3/min 

at a vacuum of + t~ 

Leakage rate must be less than 0.002 ft3/min at a vacuum of at least 15 in 

Final Vol 

Imp ml 

H2SO4 .~ 

NaOH ~ 

WEIGHTS Imp #1 Imp #2 Imp #3 Ilp #4 Imp #5 Imp #6 

Contents .10 FFzsd .1 N &9e em S` t✓f 

Bng l oo vv,L ioo ,.nL — °— 

Qi — 
SAMPLING DATA FOR : EPA METHOD 26 

Date: 1 0 r2i jd9 Test Run: C- Z 

Plant: Hc~ sc,, gc~ ~,k Barometric Pressure (in Hg) 

Location: C_~~T?x DGM ID: 9549go 

Source: DGM Correction Fac tor: ~~[,a ~ 

Technicians: NSJ EL 3~ PL, Probe Material/Size: 

~ 

Pre-Test Leak Check Results 

Rate of ~ . 001 ft3/min 

at a vacuum of 2 ~ 

Leakage rate must be less than 0.02 ft3/min 

at a vacuum of at least 15 in Hg 

readings @ 10 min intervals ;;3; a68°F 

Sampling 

Time 

(min) 

Clock 

Time 

(24 hr) 

DGIV4 

Re40ing 

DGM/iN 

Temp 

(°F) 

DGM/oIIT 

Temp 

(°F) 

Last Imp 

Temp 

(°F) 

2 £s - 7 Y . q. 

( ff)14.137 8 .$ -7 6 •S 

l0 1 7 166.36' fS41. 2. 7 6`1. s 

4S4.1• 51 Aag3,n 6`!. g;~, 

Oz 27 jf0,qqC fs .9 s. 

2 133 1 J1 .1 . 11 Ss Sy 7 3- a S. 

30 1337 II'1.S39, x S. 

31- 1 1 1 4, . 5ti -7 ~s5. S by • 3 ~ 

Ll o V3 4 7 fi$•6HA 

r3 12-0 -1E j 

so 13.5-7 l.-7 i 96.3 Li•5r 6S, 

5 S" I H f ,5 S S- D S. 5s 

D Iq o -7 SIX 13 0 

Post-Test Leak Check Results 

Rate of (), oo\ ft3/min 

at a vacuum of a. o 

Leakage rate must be less than 0.002 ft3/min at a vacuum of at least 15 in 

Final Vol 

Imp ml 

H2SO4 -- — 

NaOH 

WEIGHTS Imp #1 Imp #2 Imp #3 Imp #4 Imp #5 Imp #6 

Contents , (V 4 D , i N .2 e 

Begnining 100 onL Io0 AL ^ -- ✓ 
SAMPLING DATA FOR : EPA METHOD 26 

Date: 10121 109 TestRun: C-3 

Plant: k4Asw, (~ , ;c[~ Barometric Pressure (in Hg) a g, 3( 

Location: [I ~; ^ ~X DGMID: 95 ~ 9g0 

Source: K;T 6,14DGM Correction Factor: 

Technicians: & GS; To ProbeMateriaUSize:-je qor, 

Test Leak Check Results 

ite of 0,00( ft3/min 

a vacuum of 0 

Leakage rate must be less than 0.02 ft3/min 

at a vacuum of at least 15 in Hg 

readings @ 10 min intervals <68°F 

Sampling 

Time 

(min) 

Clock 

Time 

(24 hr) 

DGM 

Reading 

($3) 

DGM/IN 

Temp 

(°F) 

DGM/oUT 

Temp 

(°F) 

Last Imp 

Temp 

(°F) 

O tsS 1 ` 6 . 9 6ztl 3 

a 5.3ti 3~ •fs 

O f 31 .3 - 6 8~5. q 

3.y~IfS 4. ;L 6 

0 16 '35°.15 12. 2.6 . ~ S.p 

7 '3l.s'Sr 3. ly 1/.S-- 6s. 

'?O 3 3. S 2 53. g/, Ff 66_. 

3 s f 7 l ~ll .? ~s 3. ~r T2 . P, 6S. 

Lt0 /6 q ~L M171C 1~~_, S, y 

NS 16 If7 iys,fs7 S, ( 

50 t6Sa !`f .`1 $ 9 . e/3 `2 

~S 16 S 7 tso.o3 k I / A~ ^. -7 

C~ 1 -70 1' . 

Post-Test Leak Check Results 

Rate of 0,00 'k ft3/min 

at a vacuum of 0-0 

Leakage rate must be less than 0.002 ft3/min at a vacuymziTat least 15 in 

Final Vol 

Imp ml 

H2SO4 

NaOH 

WEIGHTS Imp 41 ~` jilp #3 Imp #4 Imp #5 Imp #6 

Contents 

AImp#2 

Beginmuing (d0 L _ ~ 
Preliminary Velocity/Cyclonic Flow Measurement 

PLANT: f/a's ,, -&> JeDATE: /p Zo o ~ 

TEST RUN #: p- j Start Time: so End Time: J260 

TECHNICIANS T7k6 PC., 

SAMPLING POINT AP CYCLONIC ANGLE (°) °F 

1 0. i91 9 

2 0. /V 309 

3 6, /y 0 3/0 

4 046 3 ,3o8 

5 3a:i6 3d& 

7 D, r8 8 d.i 

8 a, /9 d 30(0 

9 2os' 

10 0. i ~ -3 30 

11 o./f C) 3 

12 0, /(. q 306 

14 6,16 0 30 

15 o./G 3©S' 

16 o.iS 1 ~a 

17 

18 

19 

20 

21 

22 

23 

24 

AVG. AP AVG. AVG. °F 

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Plant: Hanson Brick 

Location: Elgin, Texas 

Source: Kiln 2 Lime Scrubber 

Technicians: TO, CJ, PC 

Test Run Designation Run 1 Run 2 Run 3 

Date 10/21/2007 10/21/2007 10/21/2007 

Start Time (24 hr) 11:03 13:09 16:06 

Stop Time (24 hr) 12:13 14:23 17:18 

Stack Gas Sampling Data 

Box No. A A A 

Sample Time Length (min) 64 64 64 

Atmospheric Pressure (" Hg) 29.37 29.37 29.37 

Avg. Stack Temperature (°F) 324 324 324 

Avg. Meter Temperature (°F) 82.8 82.8 82.8 

Average ~AP 0.518 0.518 0.518 

Average AH 1.41 1.41 1.41 

Sample Volume at STP (DSCF) 42.363 42.363 42.363 

Moisture (% volume) 5.76 5.76 5.76 

Dry Gas Fraction (unitless) 0.942 0.942 0.942 

Molecular Weight (]b/Ib-mole) 28.40 28.401 28.401 

Static Pressure (in. H20) -0.40 -0.40 -0.40 

Stack Velocity (ft/min @ stack conditions) 2164 2164 2164 

Stack Flow, dry (DSCFH) 1.33E+06 1.33E+06 1.33E+06 

% Isokinetic 99.2 99.6 100.3 

Calculated Particulate Emissions Average 

Filterable Particulate Matter Collected (g) 0.0090 0.0085 0.0080 8.47E-03 

Condensable Particulate Matter Collected (g) 0.0278 0.0267 0.0245 2.63E-02 

FilterableAnalysis(Ib/dscfl 4.68E-07 4.40E-07 4.14E-07 4.41E-07 

Filterable Analysis (lb/hr) 0.62 0.59 0.55 0.59 

Total Suspended Particulate Analysis (lb/dscf) 1.92E-06 1.83E-06 1.69E-06 1.81E-06 

Total Suspended Particulate Analysis (gr/dsco 0.0134 0.0128 0.0118 0.013 

Total Suspended Particulate Analysis (lb/hr) 2.55 2.44 2.25 2.42 

Total Suspended Particulate Anal sis (tons/yr) 11.19 10.69 9.86 10.58 

OTRC 
Plant: Hanson Brick 

Locatfon: Elgin, Texas 

Source: Kiln 2 Lime Scrubber 

1'echnicians: TO, CJ, PC 

Test Run Desi nation Run 1 Run 2 Run 3 

Date 10/21/2007 10/21/2007 10/21/2007 

Start Time (24 hr) 11:03 13:09 16:06 

Stop Time (24 hr) 12:13 14:23 17:18 

BLANK Filter # 79586 79586 79586 

Avg. Tare Wt. (g) 0.3590 0.3590 0.3590 

Avg. Final Wt.(g) 0.3588 0.3588 0.3588 

Filter Blank Weight Gain (g) -0.0002 -0.0002 -0.0002 

SAMPLE Fflter # 79582 79583 79584 

Avg. Tare Wt. (g) 0.3591 0.3597 0.3620 

Avg. Final Wt. (g) 0.35925 0.3599 0.3622 

Filter Weight Gain (g) 0.0002 0.0002 0.0003 

Filter Weight Gain, Blank Corrected (g) 0.0004 0.0004 0.0005 

BLANK Filterable Rfnse Beaker # 139 139 139 

Volume Acetone (ml) 277.3 277.3 277.3 

Avg. Tare Wt. (g) 7.7222 7.7222 7.7222 

Avg. Final Wt. (g) 7.7229 7.7229 7.7229 

Front Half Rinse Blank Weight Gain (g) 0.0007 0.0007 0.0007 

Blank Weight Concentration (mg/liter) 2.52 2.52 2.52 

SAMPLE Filterable Rfnse Beaker # 129 171 128 

Volume Acetone (ml) 218.9 138.6 174.0 

Avg. Tare Wt. (g) 7.9317 7.9478 7.7234 

Avg. Final Wt. (g) 7.9409 7.9562 7.7313 

Filterable Rinse Weight Gain (g) 0.0092 0.0084 0.0080 

Filterable Rinse Wei t Gain, Blank Corrected (g) 0.0086 0.0081 0.0075 

Filterable Particulate Matter Collected 0.0090 0.0085 0.0080 

AQUEOUS BLANK Condensable Impinger Contents Beaker # 142 142 142 

Volume H20 (ml) 312.1 312.1 312.1 

Avg. Tare Wt. (g) 7.8235 7.8235 7.8235 

Avg. Final Wt. (g) 7.8242 7.8242 7.8242 

Impinger Contents Blank Weight Gain (g) 0.0007 0.0007 0.0007 

D.I. Water Blank Particulate Concentration (mg/liter) 2.24 2.24 2.24 

AQUEOUS SAMPLE Condensable Impinger Beaker # 114 124 133 

Volume H20 (ml) 153.8 131.4 146.8 

Avg. Tare Wt. (g) 7.7721 7.7142 7.7584 

Avg. Final Wt. (g) 7.8003 7.7412 7.7832 

Impinger Contents Weight Gain (g) 0.0282 0.0270 0.0248 

Impinger Contents Weight Gain, Blank Corrected O 0.0278 0.0267 0.0245 

Condensable Particulate Matter Collected ) 0.0278 0.0267 0.0245 

OTRC 
M-5 Beaker Weighing Data Sheet 

COMPANY/JOB #: 154785 Hanson Brick 

PLANT: Elgin, Texas 

DATE: 10/21/2007 

EMISSION POINT: Lime Scrubber Page: 

TARE WEIGHTS 

Date: 9/4/2007 9/5/2007 

Time: 4:00 4:00 

Weight 

#1 ( ) 

Weight 

#2 (g) 

Weight 

#3 (g) 

Weight 

#4 (g) 

Final 

Avg. Wt. 

Absolute 

Beaker# Diff. (mg) 

139 7.7222 7.7222 7.7222 0.0000 

129 7.9317 7.9317 7.9317 0.0000 

171 7.9477 7.9478 7.9478 0.0001 

128 7.7235 7.7232 7.7234 0.0003 

0.0000 0.0000 

0.0000 0.0000 

142 7.8234 7.8235 7.8235 0.0001 

114 7.7722 7.7720 7.7721 0.0002 

124 7.7142 7.7142 7.7142 0.0000 

133 7.7583 7.7584 7.7584 0.0001 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

FINAL WEIGHTS 

Date: 

Time: 

10/24/2007 10/25/2007 

3:30 9:30 

Weight 

#1 (g) 

Weight 

#2 ( ) 

Weight 

#3 (g) 

Weight 

#4 (g) 

Final 

Avg. Wt. 

Absolute 

DESCRIPTION Beaker # Vol. (ml) Diff. (mg) 

Blank Acetone 139 277.3 7.7229 7.7229 7.7229 0.0000 

Cl P/N Rinse 129 218.9 7.9410 7.9408 7.9409 0.0002 

C2 P/N Rinse 171 138.6 7.9561 7.9562 7.9562 0.0001 

C3 P/N Rinse 128 174.0 7.7313 7.7313 7.7313 0.0000 

0.0000 0.0000 

0.0000 0.0000 

Blank DI H20 142 312.1 7.8242 7.8241 7.8242 0.0001 

CI BackHalf 114 1 153.8 7.8004 7.8001 7.8003 0.0003 

C2 Back Half 124 131.4 7.7412 7.7412 7.7412 0.0000 

C3 Back Half 133 146.8 7.7831 7.7832 7.7832 0.0001 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

Notes: 

OTRC 
M-5 Filter Weighing Data Sheet 

COMPANY: 154785 Hanson Brick 

PLANT: Elgin, Texas 

DATE: 10/21 /2007 

11SSION POINT: Lime Scrubber 

TARE WEIGHTS 

Date: 8/13/2007 8/14/2007 

Time: 1 4:00 I 1:00 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

----- 

1 1111 1 1111 

FINAL WEIGHTS 

Date: 

Time: 

10/24/2007 1 0/25/2007 

4:30 10:00 

Weight 

#1 ( ) 

Weight 

#2 (g) 

Weight 

93 (g) 

Weight 

#4 ( ) 

Final 

Avg. Wt. 

Absolute 

DESCRIPTION Filter # Diff. (mg) 

Blank 79586 0.3588 0.3588 0.3588 0.0000 

FilterCl 79582 0.3593 0.3592 0.3593 0.0001 

Filter C2 79583 0.3599 0.3599 0.3599 0.0000 

Filter C3 79584 0.3622 0.3622 0.3622 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

0.0000 0.0000 

Notes: 

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APPENDIX B: 

EXAMPLE CALCULATIONS 
Example Calculations 

Method 7E Concentration Correction 

Example for Run: Run 1 

Observe_d Measurements: 

 50.40 NOx, Gas Range (CS) 

8.69 NOx r, ave.reading for run (ppm) 

0.40 Co;, reading for zero gas before run (ppm) 

-0.01 Cof, reading for zero gas after run (ppm) 

24.87 CMi, reading for span gas before run (ppm) 

24.55 CMf, reading for span gas aRer run (ppm) 

25.30 C., actual cal. gas concentration (ppm) 

-0 13 Caic o, direct zero gas cnncentration (ppm) 

24.70 Ca ,,, M , direct span gas concentration (ppm) 

Bias Check (SBo) 

Eq 7E-2 

Bias Check (SB M) 

Eq 7E-2 

Drift Check (D) 

Eq 7E-4 

Initial zero gas 

_ (Coi - Cd', o ) 

CS 

= 0.40 - -0.13 

50.4 

= 1.05 % 

Initial span gas 

- (CMI - CEir,M) 

CS 

= 24.87 - 24.70 

50.4 

= 0.34 % 

Zero gas 

= ABS I SBor - SBo; I 

= ABS 10.24 - 1.05 1 

= 0.81 % 

Final zero gas 

_ (Cor - Ceic o ) 

CS 

_ -0.01 - -0.13 

50.4 

= 0.24 °fo 

Finalspan gas 

- (CMf - CCIGM ) 

CS 

= 24.55 - 24.70 

50.4 

_ -0.30 % 

Span gas 

= ABS I SBM( - SBMi I 

_ -ABS 10.30 - 0.34 1 

= 0.63 % 

NOx Correction (CNO,): 

Eq 7E-5 _ (NOx,r- Co)x C~ 

CM -C'o 

Average zero bias (Co) Average span bias (C M) 

_ (Coi + Cof ) (CMi * CMi ) 

2 2 

= 0.40 + -0.01 = 24.87 + 24.55 

2 2 

= 0.20 (ppm) = 24.71 (ppm) 

( 8.69 - 0.20 ) x 25.30 

( 24.71 - 0.20 ) 

= 8.77 (ppm) 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

Method 7E Concentration Correction 

Example for Run: Run 1 

Observed Measurements: 

496.00 CO, Gas Range (CS) 

118.42 COr, ave. reading for run (ppm) 

. 0.05 Coi, reatling for zero gas tiefore run (ppm) 

-0.05 Cof, reading for zero gas after run (ppm) 

 251.75 Cmi, reading for span gas before run (ppm) 

 246.75 Cmf, reading for span gas after run (ppm) 

253.00 Cma, actual cal. gas concentration (ppm) 

Initial zero gas 

Bias Check (SBo) _ (Coi - Cao-, o ) 

Eq 7E-2 CS 

. = 0.05 - 0.05 

496.0 

= 0.00 % 

 Initial span gas 

Bias Check (SB M) _ (CM, - Cd;,,M ) 

Eq 7E-2 CS 

= 251.75 . - 251.75 

496.0 

= 0.00 % 

Zero gas 

Drift Check (D) = ABS I SBor - SBo; I 

Eq 7E-4 

_ -ABS 10.02 - 0.00 ~ 

= 0.02 °!o 

0.05 Ca;,, o , direct zero gas concentration (ppm) 

251.75 Cm,, M. direct span gas concentration (ppm) 

Final zero gas 

_ (Cor - Cdv,a ) 

CS 

_ -0.05 - 0.05 

496.00 

_ -0.02 % 

Finalspan gas 

(CMf - Ctlly M) 

CS 

= 246.75 - 251.75 

496.0 

_ -1.01 % 

Span gas 

= ABS I SBMf- SB, I 

= ABS 11.01 - 0.00 ~ 

= 1.01 % 

CO Correction (Cco) 

Eq 7E-5 = (CO,r- Co) x CMg 

CM - Co 

Average zero bias (C o) 

_ (Coi + Cor ) 

2 

. = 0.05 + -0.05 

2 

 = 0.00 (ppm) 

118.42 - 0.00 ) x 253.00 

 ( 249.25 - 0.00 ) 

= 120.20 (ppm) 

 Values may differ from Summary Tables due to rounding and truncation. 

Average span bias (C M ) 

(CMI + CMf ) 

2 

= 251.75 + 246.75 

2 

= 249.25 (pprn) 
Example Calculations 

Method 7E Concentration Correction 

Example for Run; Run 1 

Observed M easurements: 

21.10 Oz , Gas Range (CS) . -0.08 Cai,, o, direct zero gas concentration (ppm) 

18.42 Oz r, ave. reading for run (vol. %) I. 10.12 Caic m, direct span gas concentration (ppm) 

-0.07 Coi, reading for zero gas tiefore run (vol %) i 

 -0.03 Cof, reading for zero gas after run (vol %) '. 

 9.91 CMi, reading for span gas before run (vol %) ' 

 10.04 CMf, reading for span gas after run (vol %) 

 10.00 CMA, actual cal. gas concentration (vol %) , 

Initial zero gas 

Bias Check (SBo) _ (COi - Cdo-, o ) 

Eq 7E-2 CS 

_ -0.07 - -0.08 

21.1 

= 0.05 % 

Initial span gas 

Bias Check (SBa) (GMi - CCiy M ) 

Eq 7E-2 CS 

= 9.91 - 10.12 

21.1 

_ -1.00 % 

Zero gas 

Drift Check (D) = ABS I SB, - SBoi I 

Eq 7E-4 

 = ABS 10.00 - 0.05 ~ 

= 0.19 % 

Final zero gas 

_ (Cof - Cdv. o ) 

CS 

_ -0.03 - -0.08 

21.1 

= 0.24 % 

Finalspan gas 

(CM( - CdiG M ) 

CS 

= 10.04 - 10.12 

21.1 

_ -0.38 % 

Span gas 

= ABS I SB Mf - SBMi I 

_ -ABS 10.38 - - 1.00 ~ 

= 0.62 % 

02 Correction (Co2) 

Eq7E-5 = (Oi,r-Co) x CMp 

CM - Go 

Average zero bias (Co) 

_ (Coi + Cof ) 

2 

_ -0.07 + -0.03 

2 

 _ -0.05 (ppm) 

_ ( 18.42 - -0.05 ) x 10.00 

( 9.98 - -0.05 ) 

 = 18.42 (vol %) 

- Values may differ from Summary Tables due to rounding and truncation. 

Average span bias (C M) 

(CiMi ~ CMf ) 

2 

= 9.91 + 10.04 

2 

= 9.98 (ppm) 
Example Calculations 

Method 7E Concentration Correction 

Example for Run: Run 1 

Observ ed Measurements: 

--- 10.07 COz , Gas Range (CS) -- _ 0.10 Cd,,, o , direct zero gas concentration (ppm) 

1.89 COzr, ave. reading for run (vol. %) '~, 10.05 C, M , direct span gas concentration (ppm) 

 -0.09 Coi, reatling for iero gas before run (vol %) 

0.16 Cc, reading for zero gas after run (vol %) 

I 

9.95 CMi, reading for span gas before run (vol %) ' 

10.10 C,, reading for span gas after run (vol %) I, 

10.07 Cw„ actual cal. gas concentration (vol %) 

Initial zero gas Final zero gas 

Bias Check (SBo) _ (Col - Cmc O ) _ (Cof - Cdico ) 

Eq 7E-2 CS CS 

-0.09 - 0.10 = 0.16 - 0.10 

10.1 10.1 

_ -1.89 % = 0.60 % 

 Initial span gas Final span gas 

Blas Check (SBM) - (CMi - CtlicM ) _ (CMt - cmgM) 

Eq 7E-2 CS CS 

= 9.95 - 10.05 = 10.10 - 10.05 

10.1 10.1 

_ -0.99 % = 0.50 % 

 Zero gas Span gas 

Dri$ Check (D) = ABS I SBor - SBoi I = ABS I SBMI - SBMi I 

Eq 7E-4 

= ABS 10.60 -- 1.89 I = ABS 10.50 -- 0.99 ~ 

= 2.48 % = 1.49 % 

Op Correction (CO2): 

Eq 7E-5 = (Oz ,r- Co) x CMg 

CM - Co 

Average zero bias (Co) Average span bias (CM) 

- (COi + COI ) _ (CMi + CMf ) 

2 2 

_ -0.09 + 0.16 = 9.95 + 10.10 

2 2 

` = 0.04 (ppm) = 10.03 (ppm) 

_ ( 1.89 - 0.04 ) x 10.07 

( 10.03 - 0.04 ) 

= 1.87 (vol %) 

- Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

Method 7E Concentration Correction 

Example for Run: Run 1 

Observed Measurements: 

101.50 SOz , Gas Range (CS) 

19.54 SOz r, ave. reading for run (vol. %) 

1.30 Cc;, reading for zero gas before run (vol %) 

 2:28 Ccr, reading for zeio gas aRer run (vol %) 

. 44.50 CM„ reading for span gas before run (vol %) 

43.01 CMr, reading for span gas aRer mn (vol %) 

45.60 CMq, actual cal. gas concentration (vol %) 

Initial zero gas 

Bias Check (SBo) _ (Coi - Cm,.o ) 

Eq 7E-2 CS 

= 1.30 - -0.13 

101.5 

= 1.41 % 

Initial span gas 

Blas Check (SBM) _ (CMi - Cein M ) 

Eq 7E-2 CS 

= 44.50 - 44.48 

-0.13 Ce,c o , direct zero gas cuncentration (ppm) 

44.48 Caic M, direct span gas concentraflon (ppm) 

Finalzero gas 

(Cor - Cdv.O ) 

CS 

= 2.28 - -0.13 

101.5 

= 2.37 % 

Final span gas 

(CM( - CEiO M ) 

cS 

= 43.01 - 44.48 

Drift Check (D) 

Eq 7E-4 

Oz Correction (Coz): 

Eq 7E-5 

101.5 

= 0.02 % 

Zero gas 

= ABS I SBor - SBOI I 

= ABS 10.00 - 1.41 1 

= 0.97 % 

_ (Oz ,r- Ca) x CMg 

Cm - Co 

Average zero bias (Co) 

' (Coi + Cor.) 

2 

= 1.30 + 2.28 

101.5 

_ -1.45 % 

Span gas 

= ABS I SB Mr - SBMi I 

_ -ABS 11.45 - 0.02 1 = 1.47 % 

Average span bias (CM) 

(CMi + CMI ) 

2 

= 44.50 + 43.01 

2 

= 1.79 (ppm) _ 

_ ( 19.54 - 1.79 ) x 45.60 

( 43.76 - 1.79 ) 

= 19.29 (vol %) 

Values may differ from Summary Tables tlue to rounding and truncation. 

2 

43.76 (ppm) 
Example Calculations 

NOx Emission Rates 

Example for Run: Run 1 

Observed Measurements: 

8.77 corrected NOx concentration (ppm) 

1333458 stack exhaust flow rate (DSCFH) 

Co nstants/Co nversi o ns/Stan da rds: 

385.15 ideak gas constant @ EPA STP (68 OF and 29.92 "Hg); 

 (scf / Ib-mol) 

46.01 Molecular weight of NOX as NO2 (Ib/Ib-mol) 

29.92 EPA STP (" Hg); Prer 

CNOxcorrected NOx concentration 

Coz corrected Oz concentration 

Qd stack exhaust flow rate 

DNox NOx density factor 

NOx density factor 

— 46.01 Ib/Ib-mol x 10 

385.15 scf/Ib-mol 

= 11.95E-081b/scf 

NOx mass emission rates (Ibs/hr) 

— QNOx x Qd x DNOX 

= 8.77 x 1.33E+06 

= 1.40 Ibs/hr 

x 1.19E-07 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

CO Emission Rates 

Example for Run: Run 1 

Observed Measurements: 

120.20 corrected CO cancentration (ppm) 

1.33E+06 stack exhaust flow rate (DSCFH) 

. CO densityfactor 

_ — 28.01 Ib/Ib-mol x 10 

385.15 scf/Ib-mol 

= 7.27E-081b/sd 

CO mass emission rates 

= Cco x Qd x Dco 

= 120.20 x 1.33E+06 x 7.27E-08 

= 11.661bs/hr 

C on sta nts/Co nversi o ns/Stan d ards: 

385.15 ideak gas constant @ EPA STP (68 OF and 29.92 "Hg); 

(scf / Ib-mol) 

28.01 Molecular weight of CO (Ib/Ib-mol) 

29.92 EPASTP("Hg) 

Cco corrected CO concentration 

COZcorrected 02 concentration 

Qd stack exhaust flow rate 

Dco CO density factor 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

S02 Emission Rates 

Example for Run: Run 1 

Observed Measurements: 

19.3 corrected SOz concentration (ppm) 

 - 1.33E+06 stack exhaust flow rate (DSCFH) 

Constants/Conversions/Standards: 

385.15 ideak gas constant @ EPA STP (68 OF and 29.92 "Hg); 

(scf/Ib-mol) 

64.06 MolecularweightofSOz (Ib/Ib-mol) 

29.92 EPASTP("Hg) 

I Csoz corrected SOz concentration 

Coi corrected 02 concentration 

Qd stack exhaust flow rate 

' Dsoz SOz density factor 

S02density factor 

 = 64.06 Ib/Ib-mol x 10" s 

 = 1.66E-071b/scf 

S02 mass emission rates 

= Csoz x Qd x Dsoz 

= 19.30 x 

= 4.281bs/hr 

S02 Removal Efficiency 

1.33E+06 x 1.66E-07 

_ [1 _SO, Outlet (Ibs/hrl] x 100 

SOz Inlet (Ibs/hr) 

_ [1 - 4'28 ] x 100 42.8 

= 90.00 i 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

HCI Emission Rates 

Example forRun: Run 1 

Observed Measurements: 

0.17 HCI concetltration (ppm) 

1333458 stack exhaust flow rate (WSCFH) 

HCI density factor 

= 36.46 Ib/Ib-molx 10 

385.15 scf/Ib-mol 

= 9.47E-081b/scf 

HCI mass emission rates 

= CHq x Qd x DHCi 

= 0.17 X 1.33E+06 x 9.47E-08 

= 0.021 Ibs/hr 

HCI Removal Efficiency 

HCI Outlet (Ibs/hr) 

(1 HCI Inlet (Ibs/hr) 1 x 100 

0.021 ) x 100 

1.14 

= 98.12 % 

I Constants/Conversions/Standards: 

li 385.15 ideal gas constant @ EPA STP (68 OF and 29.92 "Hg); 

(scf / Ib-mol) 

36.46 MolecularweightofHCl (Ib/Ib-mol) 

29.92 EPA STP ( " Hg) 

' CHci HCI concentration 

, Coz corrected 02 concentration 

I, Qd stack exhaust flow rate 

DHci HCI density factor 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

HF Emission Rates 

Example forRun: Run 1 

Otiserved Measurements: 

0.12 HF concentration (ppm) 

1333458 stack exhaustflow rate (WSCFH) 

Consta 

385.15 

20.01 

29.92 

QHF 

Q02 

Qd 

DHF 

its/Conversions/Standards: 

ideal gas constant @ EPA STP (68 OF and 29.92 "Hg) 

(scf / Ib-mol) 

Molecular weight of HF (Ib/Ib-mol) 

EPA STP ( " Hg) 

HF concentration 

corrected 02 concentration 

stack exhaust flow rate 

HF density factor 

HF density factor 

= 20.01 Ib/Ib-molx 10 

385.15 scf/Ib-mol 

= 5.20E-081b/scf 

HF inass emission rates 

— QHFxQ'dxDHF 

= 0.12 x 

= 0.00831bs/hr 

HF Removal Efficiency 

_ HF Outlet Ilbs/hrl 

(1 HF Inlet (Ibs/hr) ) x 100 

_ (1 0.0083 

1.9 

) x 100 

= 99.56 °fo 

1.33E+06 x 5.20E-08 

Values may differ from Summary Tables due to rounding and truncation. 
Example Calculations 

VOC Emission Rates 

Example for Run: Run 1 

Observed Measurements: 

4.64 VOC concentration (ppm) 

1415149 stack exhaust flow rate (WSCFH) 

Constants/Conversions/Standards: 

385.15 ideal gas constant @ EPA STP (68 OF and 29.92 "Hg); 

(scf / Ib-mol) 

44.10 Molecular weight of VOC as C3 (Ib/Ib-mol) 

29.92 EPASTP("Hg) 

G1r,, VOC concentration 

Co: corrected 02 concentration 

Qd stack exhaust flow rate 

Dvoc VOC density factor 

VOC density factor 

— 44.10 Ib/Ib-molx 10 

385.15 scf/Ib-mol 

= 1.14E-07 Ib/scf 

VOC mass emission rates 

- = Cvoc x Qd x Dvoc 

= 4.64 x 1.42E+06 

= 0.75 Ibs/hr 

x 1.14E-07 

Values may differfrom Summary Tables due to rounding and lruncation. 
Example Calculations Stack Moisture and Molecular Weight 

Example for Run: Run 1 

Observed Measurements: 

_ 

161.945 beginning DGM reading (ft3) 

204.925 ending DGM reading (ft3) 

2731.2 beginning impinger weight (g) 

2786.1 ending impinger weight (g) 

1.0286 Y, DGM factor (unitless) 

542.5 Tm, ave. DGM temperature (R = F+ 460) 

29.37 Pm, barometric pressure (in. Hg) 

1.87 CO2 (%) 

18.42 02 (%) 

0.0 H2 (%) 

0.0 CO (%) 

C o nsta nts/Co nve rs i o ns/Sta n dards: 

-- ---- 

~I 528 Tstd, EPA standard temperature (R) 

i, 29.92 Pstd, EPA standard pressure (in. Hg) 

0.04715 water (ft3/g) 

i 1.335 water (L/g) 

I 28.3 conversion factor, (L/ft3) 

Impinger Wt. Gain (IWG): = ending impinger wt. (g) - beginning impinger wt. (g) 

= 2786.1 - 2731.2 

= 54.9 (g) 

Volume Metered (Vm): = ending DGM reading (0) - beginning DGM reading (113) 

= 204.925 - 161.945 

= 42.98 (ft3) 

Standard 

Volume Metered (Vstd): _ (Vm) (Y) (Pm) (Tstd) 

(Pstd) (Tm) 

= 42.98 x 1.0286 x 29.37 x 528 

 29.92 x 542.5 

= 42.237 (SCF) 

Moisture Content (Bws): = IWG (g) x 0.04715 (ft3/g) 

( (IWG (g) x 0.04715 (ft3/g) )+ ( Vstd (ft3) ) ) 

= 2.5885 

(2.5885 + 42.237) 

= 0.058 

= 5.8 (%) 

Dry Gas Fraction: = 1- Bws 

= 1 - 0.058 

= 0.942 

Molecular Wt. (Ms): Total Molecular Moisture or Partial 

Compound Percent Weight Dry Fraction Mol. Wt. 

H20 n/a 18 0.058 1.039 

02 18.4 32 0.942 5.554 

CO2 1.9 44 0.942 0.775 

CO 0.0 28 0.942 0.000 

H2 0.0 2 0.942 0.000 

N2 79.7 28 0.942 21.030 

28.40 (Ib/Ib-mole) 

Values may diNerfrom SummaryTables due to rounding and truncation. Ex.CaICB- Stack MOiBture/MOI.Wt. 1 
Example Calculations 

Example for Run: Run 1 

Observed Measurements: 

0.84 Cps, pitot tube factor (unitless) 

29.37 Pb, barometric pressure (in. Hg) 

783.7 Ts(abs), ave. stack temperature (R, F+460) 

28.40 Ms, stack gas molecular wt. (Ib/Ib-mole) 

-0.4 Pg, stack static pressure (in. H20) 

16.50 A, stack area (ft2) 

16 Number of traverse Points 

0.942 Fd, stack dry gas fraction 

Stack Gas Flow Rate 

Constants/Convers io ns/Sta nda rds: 

528 Tstd, EPA standard temperature (R) 

29.92 Pstd, EPA standard pressure (in. Hg) 

85.49 Kp, (ft/s) [(Ib/Ib-mole) (in. Hg) / (R)(in.H2O)]"0.5 

5129.4 Kp, (ft/min) [(Ib/Ib-mole) (in. Hg) / (R)(in.H20)]^0.5 

60 conversion factor, (s/min) 

60 conversion factor, (min/hr) 

0.07355 conversion factor, (in Hg/in H20) 

Point# dP Point# dP Point# dP ' Point# dP 

1 0.24 'I 10 0.31 19 28 

2 0.25 '~~. 11 0.3 20 29 

3 0.28 ', 12 0.28 I 21 I, 30 

4 0.28 ''~, 13 0.29 22 'I 31 

5 0.3 I, 14 0.3 23 32 

6 0.33 '' 15 0.25 ''~ 24 'il 33 

7 0.31 16 0.19 I 25 34 

8 0.17 ~. 17 'I 26 , 35 

9 0.24 18 ''~, 27 ; 36 

Absolute Static Pressure (Ps): = Pb x(Pg x 0.07355) 

= 29.37 + ( -0.4 x 0.07355) 

= 29.34 (in. Hg) 

Average Square Root of DiP (p1): = 8.285 

16 

= 0.5178 

Stack Velocity (Vs): = Kp x Cp x p1 x[Ts(abs) /(Ps x Ms)]^0.5 

(ft/min) = 5129.4 x 0.84 x 0.5178 1783.7 I (29.34 x 28.40 )]^0.5 

= 2163.8 (ft/min) 

Stack Velocity (Vs): = Vs / 60 (s/min) 

(ft/Sec) = 2163.8 / 60 

= 36.06 (ft/sec) 

Stack Volumetric Flow (Qa): = Vs x A 

= 2163.8 x 16.50 

= 35700 (ACFM) 

Stack Volumetric Flow (Qd): = Qa x 60 (Tstd/Pstd) x(Ps/Ts(abs)) x Fd 

= 35700 x 60 x 528 x 29.34 x 0.942 

29.92 783.7 

= 1333458 DSCFH 

Values may differ from Summary Tables due to rounding and truncation. Ex.Calcs- Stack Gas Flowrate 1 
Example Calculations 

Particulate Matter weights 

Exampfe for Run: Run 1 

Observed Measurements: 

Blank Analyses: 

-0.0002 Bf, filter blank weight gain (g) 

0.0007 Bw, back half blank weight gain (g) 

0.0007 Ba, front half blank weight gain (g) 

312.1 Vw, back half aqueous volume (ml) 

277.3 Va, front half acetone volume (ml) 

Front Half Filter Analysis: 

0.0002 F,weightgainofflter(g) 

Front Half Probe/Hozzle R7nse Analysis: 

0.0092 Ra, weight gain of front half rinse (g) 

218.9 Vm, front half rinse volume (ml) 

Back Half Impinger/Rinse Analysis: 

0.02815 I, weight gain of back half rinse (g) 

454 conversion factor,(g/Ib) 

7000 conversion factor, (grains/Ib) 

1000000 conversion factor, (ml-mg/g-L) 

1000000 conversion factor, (ml-mg/g-L) 

153.8 Vit, back half aqueous rinse total volume (ml) 

Front Half Filter = F - Bf 

Blank Correction (PMf): = 0.0002 -- 0.0002 

= 0.0004 (g) 

PM conc in front half = Ba / Va x 1000000 (mg-ml/g-L) 

acetone blank (Cba): = 0.0007 / 277.3 x 1000000 (ml-mg/g-L) 

= 2.52 (mg/L) 

PM conc. in front half = Ra / Vra x 1000000 (ml-mg/g-L) 

rinse sample (Cra): = 0.0092 / 218.9 x 1000000 (ml-mg/g-L) 

= 42.0 (mg/L) 

Front Half Rinse Blank = Cra - Cba 

Correction (Crac): = 42.0 - 2.52 

= 39.5 (mg/L) 

Total Front Half rinse = Crac x Vra / 1000000 (ml-mg/g-L) 

PM Mass (PMra): = 39.5 x 218.9 I 1000000 (ml-mg/g-L) 

= 0.0086 (g) 

PM conc in back half = Bw/ Vw x 1000000 

aqueous blank (Cbw): = 0.0007 / 312.1 x 1000000 (ml-mg/g-L) 

= 2.24 (mg/L) 

 PM conc. in back half = I/ Vit x 1000000 (ml-mg/g-L) 

sample (Ci): = 0.0282 / 153.8 x 1000000 (ml-mg/g-L) 

= 183.0 (mg/L) 

Back Half Aqueous Rinse = Ci - Cbw 

Blank Correction (Cic): = 183.0 - 2.24 

= 180.8 (mg/L) 

Total Back Half Aqueous = Cic x Vit / 1000000 (ml-mg/g-L) 

PM Mass (PMi): = 180.8 x 153.8 / 1000000 (ml-mg/g-L) 

= 0.0278 (g) 

Total PM Catch: Front Halt = Pmf + PMra + PMi 

Aqueous Back Half (PMtot1; = 0.0004 + 0.0086 + 0.0278 

= 0.0368 (g) 

Values may differ from Summary Tables due to rounding and truncation. 

' Front Half Analyses: 

(filter + front half rinses) 

Back Half Analysis: 

(impinger(s) + back 

half rinses) 

Ex.Calcs-Particulate Matter 1 
Example Calculations 

Particulate Matter Emissions / Isokinetics 

Example for Run: Run 1 

Observed Measurements: 

42.237 Vstd, gaseous volume collected (DSCF) 

1333458 Qtl,stackvolumetricflowrate(DSCFH) 

0.0368 PMtotal, total PM catch (g) 

0.000495 An, nozzle area (R2) 

0.942 Fd, tlry gas fraction (unitless) 

1.400 dH, average dH of DGM (in. H20) 

29.34 Ps, stack absolute pressure (in. Hg) 

783.7 Ts, ave. stack temperature (R, F+460) 

64 ts, sample time (min) 

2163.8 Vs, stack gas velocity (ft/min) 

528 Tstd, EPA standard temperature (R) 

29.92 Pstd, EPA standard pressure (in. Hg) 

454 wnversion factor, (g/Ib) 

7000 conversion factor, (grains/Ib) 

2000 conversion factor, (Ib/ton) 

8780 conversion factor, (hr/year) 

Filterable PM Conc. ln Stack 

Total PM Conc. in Stack: 

(Ib/DSCI) 

Total PM Conc. in Stack: 

(grains/DSCF) 

Filterable PM Emissions: 

(Ib/hr) 

Total PM Emissions: 

(Ib/hr) 

Filterable PM Emissions: 

(tons/yr) 

= Filterable PM / 454 / Vstd 

= 0.0086 / 454 / 42.237 

= 4.48E-07 (IbIDSCF) 

= PMtotal / 454 / Vstd 

= 0.0368 / 454 / 42.237 

= 1.92E-06 (IbtDSCF) 

= Total PM Conc. in Stack x 7000 (greins/Ib) 

= 1.91925E-06 x 7000 

= 0.0134 (grains/DSCF) 

= Filterable PM Conc. in Stack x Qd 

= 4.48E-07 x 1333458 

= 0.60 (Ib/hr) 

= Total PM Conc. in Stack x Qd 

= 1.92E-06 x 1333458 

= 2.56 (Ib/hr) 

Note: Conc. in (Ib/DSCF) 

Note: Conc. in (Ib/DSCF) 

= Filterable PM Emissions x Tons of Brick Firetl (tons/hr) Note: Fllterable PM Emissions in (Ib/hr) 

= 0.60 / 10.56 

= 0.06 (Ibs/ton of Fired Brick) 

Ave. Sampling 

Isokinetics ( % ): 

— (Ts x Vstd x Pstd x 100) 

(Tstd x Vs x ts x An x Ps x Fd) 

= 783.7 x 42.237 x 29.92 x 100 

528 x 2163.8 x 64 x 0.000495 x 00029 x 0.942 

= 98.9 (%) 

Values may differ from Summary Tab/es due to rounding and truncation. Ex.Calcs-Particulate Matter 2 
APPENDIX C: 

QUALITY ASSURANCE ACTIVITIES 
Barometer/Altimeter Calibration Check 

Date: 10/19/2007 

Location: Austin, TX south location 

Technician: Neal Afflerbach 

Manufacturer: United Instruments 

Type: Aneroid 

Units: in Hg and ft 

Cubix Lab Assign.: T-8 

Serial No.: GH438 

standarci 6arometer 

Lab Standard Barometer 

Manufacturer: Princo 

Type: Fortin Type Mercurial 

Units: in. Hg and mm Hg 

ID Number: NOVA 453x 

Uncorrected (Observed) Lab Barometer Reading 29.39 in. Hg 

Temperature of Lab Barometer 70 °F 

Multiplier for Temperature Correction (+ or -) -0.003742 unitless 

Multiplier for Laftitude Correction (Austin =-30.5°N) (+ or -) -0.001327 unitless 

Temperature Corrected Laboratory Barometer Reading 29.28 in. Hg 

Temperature & Latitude Corrected Laboratory Barometer Reading 29.24 in. Hg 

Corrected Laboaratory Barometer Reading 743 mm Hg 

Corrected Laboaratory Barometer Reading 990 mb 

Corrected Laboaratory Barometer Reading 625 ft 

Field Barometer/Altimeter 

Field Barometer Reading (temperature compensated) 560 ft 

Field Barometer Reading (temperature compensated) 29.31 in. Hg 

Calibration Test Results 

`Difference (in Hg) -0.07 

Pass/Fail PASS 

Accentance Criteria 

Agreement within 0.1 in. Hg or 2.5 mm Hg, or 100 ft 

signature 

12&uh 

~~ TRC 
Barometer/Altimeter Calibration Check 

Date: 

Location: 

Technician: 

Manufacturer: 

Type: 

Units: 

Cubix Lab Assign.: 

Serial No.: 

10/22/2007 

Austin, TX south location 

RAM 

United Instruments 

Aneroid 

in Hg and ft 

T-8 

GH438 

Lab Standard Barometer 

Manufacturer: Princo 

Type: Fortin Type Mercurial 

Units: in. Hg and mm Hg 

ID Number: NOVA 453x 

Laooratory stanaara tsarometer 

Uncorrected (Observed) Lab Barometer Reading 29.65 in. Hg 

Temperature of Lab Barometer 70 °F 

Multiplier for Temperature Correction (+ or -) -0.003742 unitless 

Multiplier for Lattitude Correction (Austin =-30.5°N) (+ or -) -0.001327 unitless 

Temperature Corrected Laboratory Barometer Reading 29.54 in. Hg 

Temperature & Latitude Corrected Laboratory Barometer Reading 29.50 in. Hg 

Corrected Laboaratory Barometer Reading 749 mm Hg 

Corrected Laboaratory Barometer Reading 999 mb 

Corrected Laboaratory Barometer Reading 390 ft 

Field Barometer/Altimeter 

=ield Barometer Reading (temperature compensated) 315 ft 

Field Barometer Reading (temperature compensated) 29.58 in. Hg 

Calibration Test Results 

Acceptance Criteria 

Agreement within 0.1 in. Hg or 2.5 mm Hg, or 100 ft 

signature 

TRC 
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ooa rc ~~~r 
Nozzle Inspection and Measurement Data Sheet 

Company Name: TW— 

Nozzle Number: FL(D p.30~ 

Measure three diameters (in inches) as shown below. Average the diameters and calculate the Nozzle 

area according to the calculations below. 

*Diameter 1 (in): p--W Date: 10 

*Diameter 2 (in): 03O2 

*Diameter 3 (in): D•3o 

Average Diameter (in): ©• 3!D\5 =(Sum of Diameters 1-3) / 3 

Average Radius (in): Average Diameter (in) / 2 

Average Radius (ft): D• (a5$3 = Average Radius (in) / 12 

Nozzle Area (ft2): 0, d6n 4q 52.5 =Tr x radius (ft) ^2 

at 

*Diameter 1 (in): fl.3o ( Date: (0 

*Diameter 2 (in): D• 3~ 1 

*Diameter 3 (in): 0.302 

Average Diameter (in): D,30lCj =(Sum of Diameters 1-3) / 3 

Average Radius (in): 0, l 5l = Average Diameter (in) / 2 

Average Radius (ft): 0• LaT°j~ °~ = Average Radius (in) / 12 (ft) 

Nozzle Area (ft2):p, Qjpq'A 5 ~)-S = Tr x radius (ft) ^2 

*Maximum allowable difference between largest diameter and smallest 

diameter is 0.004 inches. Noale must be round, sharp-edged, free of nicks an< <r 

i 

N 

signature 

C- TRC nozzle_insp_measure_v1.1.x1t 
Dry Gas Meter Calibration 

WORKING METER REFERENCE METER 

Date: 1015I2007 

Prev. Calib. Dale: 7/2512007 Calibration Date: 7130/2007 

Location: TRC South Auslin Loeation: TRC Austin Lab 

Technician: RAM Technician: KRH 

MeterSerial No: 1348739 Meter9edal Nu: P164240 

Cubix DGM ID T-3 Cubix DGM ID American 

Prev. Calib Factor(Y): 0.9901 Calib. Factor Y: 0.9780 

REFERENCE METER ~n~ Corr Vo

Calibration 

Run# 

Time 

min 

SlartTemp 

de F 

StopTemp 

tle F 

Vol(initial) 

wft 

Vol(final) 

wft 

Vol.Total 

cufl 

MeterRate 

w•R/min 

EPASTP 

cuft 

1 1 31 0.000 8.4930 a.306 0.2679 8.134 

2 31.5 0.0000 13.3020 13.009 0.4130 12.740 

3 15.5 

a77. M77 

0.0000 8.8510 8.656 0.5585 8.445 

4 21.5 0.0000 14.2990 13.984 D.6504 13643 

5 15 0.0000 115440 1 13.246 1 0.8831 12.827 

WORKING METER ICOM. Vol @ 

EPA STP 

(cuft) 

Calculated 

DGM Pactor 

(Y) 

Dry Gas Meter (DGM Factor) 

Calibration Test Results 

Calibration 

Run# 

Time 

(min) 

Start Temp 

(tlegF) 

Stop Temp 

(degF) 

Vol (initial) 

(wft) 

Vol (rnaq 

(wft) 

V.I. Total 

(cuft) 

Meter Rate 

(w•ft/min) 

1 31 81.0 78 824.775 833.327 8.552 O.Z]6 8.243 0.9868 "AVerageY:,. .-0,9876 

2 31.5 78.0 78 834.923 848.315 13.392 0.425 12.944 0.9842 :'AVe YwfinS%oFpFevlousvalue. YES - 

~ PASS; ~-. 

..-Ind Y~ value3kl<0i02fromAve: PASSe 

3 15.5 78.0 79 849.167 858.038 1 8.871 1 0.572 

4 1 21.5 1 79.0 1 79 859.191 871472 14.281 0.664 13.778 09903 

5 1 15 79.0 79 877.347 890168 1 13.421 1 0.895 1 12.948 0.9906 

cnreria: 

' Y- ratio of the reading of the reference meter to the working DGM. Acceptable tolerance of intlividual values from the avera9e is+l- 0.02, wilh a value between 0.95 and 1.05. 

DGM Factor vs. Flow rate 

1.0500 

1.0400 

1.0300 

1.0200 

1.0100 

~ 1.0000 

0.9900 

0.9800 

0.9700 

0.9600 

0.9500 

0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 

 Flow Rate (cfin) 

F",0 7k I 
10/22/2007 

10/5/2007 

TRC South Austin 

RAM 

1348739 

T-3 

0.9876 

WORKING METER 

Date: 

Prev. Calib. Date: 

Loeation: 

Technician: 

MeterSerial No: 

Cubix DGM ID 

Prev. Calib Factor (Y) 

REFERENCE METER 

Calibration Date: 7/3012007 

Location: TRCAustinLab 

Technician: KRH 

MeterSerial No: P164240 

Cubix DGM ID American 

Calib. Factor 0.9780 

Dry Gas Meter Calibration 

REFERENCE METER ~~ Cnn. vn

Calibratian 

Run# 

Time 

min 

StartTemp 

tle F 

StopTemp 

de F 

Vol(initiap 

wR 

Vol(fnap 

cufi 

Vol.TOtal 

wft 

MeterRate 

w•ft/min 

EPASTP 

wft 

t 29 72.0 72 0.000 8.3280 t1.t45 0.2809 7.961 

2 21.5 72.0 72 0.0000 10.5120 10.281 0.4782 10.049 

3 12.5 72.0 71 0.0000 7.5350 7.369 0.5895 7.210 

4 1 t 71.0 71 0.0000 7.3550 7.193 0,6539 7.044 

5 17.5 71.0 71 0.0000 10.3540 10.126 0.8805 1 9 916 

WORKING METER Corr. Vol g 

EPA STP 

(cuft) 

Calculated 

DGM Factor 

(Y) 

Dry Gas Meter (DGM Factor) 

Calibration Test Results 

Calibration 

Run# 

Time 

(min) 

Start Temp 

(degF) 

Stop Temp 

(tlegF) 

Vol (initial) 

(cuft) 

Vol (finap 

(wft) 

Vol. Total 

(cuft) 

Meter Rate 

cu•ft/min) 

1 29 66.5 72.1 972.607 980.845 8.238 0.284 8.093 0.9837 * Aveiage Y ~ ; '. ' U.9921 

qve Yw(r~ 5°lofpranousvalue 

I 

 YES ' 

£Ave YbetweenO9Send705: ,IPASSf` 

2 21.5 72.0 75 981.420 991.850 10.430 0.485 10.766 0.9885 

3 12.5 75.0 76 992.371 999.847 7.476 0.598 7.260 0.9931 

4 11 76.0 76 1.375 8.670 7.295 0.663 7.077 0.9953 Ihd Y9aluea+/ 0,02fromAVe.: iRASS'F 

5 11.5 ]6.0 76 10266 20.488 1 10.222 1 0.989 1 9.917 1.0000 

crnerla: 

• Y- ralio of the reading of the reference meterto the worfling OGM. Acaeptable tolerance of individual values from the avera9e is+/- 0.02, with a value between 0.95 and 1.05. 

DGM Factor vs. Flow rate 

1.0500 

1.0400 

1.0300 

1.0200 

1.0100 

Y 1.0000 

0.9900 

0.9800 

0.9700 

0.9600 

0.9500 

0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 

Flow Rate (cfin) 

TRC 
Dry Gas Meter Calibration 

WORKING METER 

Date: 101812007 

Prev. Calib. Date: 8/30/2007 

Location: TRC Austin 

Technician: RAM 

MeterSerial No: 954980 

TRC Meter ID T-8 

Prev. Calib Factor (Y) 0.9995 

P bar (in Hg) : uncorrected: 30.17 -> 30.17 

REPERENCE METER 

REFERENCE METER 

Calibration Date: 7/3012007 

Location: TRC Austin 

Technician: KRH 

MeterSerial No: P164240 

Calib. Factor Y : 0.9780 

frnrr vM 

Calibration 

Run # 

Time 

min 

Start Temp 

de F 

Stop Temp 

de F 

Vol (initial) 

cu ft 

Vol (fnal) 

cu ft 

I Vol. Total 

cu ft 

Meter Rate 

cu ft/min 

EPA STP 

in, ~Jjj ft 

1 1 21.5 71 71 0.000 6.577 6.432 0.2992 6.352 

2 29 71 71 0.000 13.069 12.781 0.4407 12.622 

3 22.5 71 71 0.000 13.389 13.094 0.5820 12.932 

4 27 71 71 0.000 18.904 18.488 0.6847 18.258 

5 7.5 71 71 0.000 1 6.714 1 6.566 1 0.8755 1 6.485 

WORKING METER Corr. Vol @ 

EPA STP 

(cu ft) 

I Calculatetl 

DGM Factor 

(Y) 

Dry Gas Meter (DGM Factor 

Calibration Test ResultS 

Calibretion 

Run # 

Time 

(min) 

Start Temp 

(deg F) 

Stop Temp 

(deg F) 

Vol (initial) 

(cu ft) 

Vol (final) 

(cu ft) 

Vol. Total 

(cu ft) 

Meter Rate 

(cu•ft /min) 

1 21.5 80 80 9.131 15.708 6.577 0.306 6.386 0.9947 :` Vera90 r 

2 29 80 80 16.702 29.682 12.980 0.448 12.604 1.0015 Ave. YS9(1115%of pfevious value: , YES 

3 22.5 80 80 31.744 1 45.029 1 13.285 0.590 12.900 1.0025 "AY2-Yb9twBef10,95Snd7.05' RASS ~ ". 

4 27 80 80 46.650 67.390 18.740 0.694 18.197 1.0034 ,- IOd; Y'YdIUeS'*Y- 0.92 from AVe: PASS I 

7.5 80 8 69.620 76.227 6.60 0.881 6.415 1 1.0108 

.rnenz: 

' Y- ratio of the reading uf the reference meter to lhe working DGM. Acceptable tolerance of intlivitlual values from the average is +/- 0.02, with a value between 0.95 antl 1.05. 

DGM Factor vs. Flow rate 

1.0500 

1.0400 

1.0300 

1.0200 

1.0100 

> 1.0000 

0.9900 

0.9800 

0.9700 

0.9600 

0.9500 

0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 1.10 1.20 1.30 

Flow Rate (cfm) 

TRC Air Measurements, Austin, TX 
Dry Gas Meter Calibration 

WORKING METER 

Date: 1012212007 

Prev. Calib. Date: 10/812007 

Location: TRCAustin 

Technician: RAM 

MeterSerial No: 954980 

TRC Meter ID T-8 

Prev. Calib Factor (Y) 1.0026 

P bar (in Hg) : uncoffected: 30.17 --> 30.17 

REFERENCE METER 

REFERENCE METER 

Calibration Date: 7/30/2007 

Location: TRC Austin 

Technician: KRH 

MeterSerial No: P164240 

Calib. Factor 0.9780 

Corr. Vol @ 

Calibration 

Run # 

Time 

min 

Start Temp 

d F 

Stop Temp 

de F 

Vol (initial) 

cu ft 

Vol (final) 

cu ft 

Vol. Total 

cu ft 

Meter Rate 

cu ft/min 

EPA STP 

cu ft 

1 29.5 70 70 0.000 8.773 8.521 0.2889 8.431 

2 22.5 70 71 0.000 10.259 10.033 0.4459 1 918 

3 1 12 77 72 0.000 7.197 7.039 0.5866 1 6.945 

4 . 10.5 72 72 0.000 7.164 7.006 0.6673 6.908 

5 13 1 73 1 73 1 0.000 11.655 1 11.399 1 0.8768 1 11.216 

WORKING METER Corr. Vol @ 

EPA STP 

(cu ft) 

Calculated 

DGM Facto 

Y) 

Dry Gas Meter (DGM Facto 

Callbration Teet ReSDlts 

Calibration 

Run # 

Time 

(min) 

Start Temp 

(deg F) 

Stop Temp 

(deg F) 

Vol (initial) 

(cu ft) 

Vol (final) 

(cu ft) 

Vol. Total 

(cu ft) 

Meter Rate 

(cu•ft/min) 

1 29.5 76 77 157.307 165.808 8.501 0.288 8.308 1.0148 ,-. Veraye. : 

2 22.5 78 82 167.833 177.698 ;vQnS%ofpfeV[oGBYalue.YES

3 

10.085 Q447 9.771 1.0150 

12 82 85 178.475 185543 7068 ;AvQ:Ybetweefl(1,95and1,05: PHSS

4 

0589 6819 10184 

10. 201.272 7.046 0.671 6.767 1.0209 P.ASS~ 

13 89 uu 205.252 216.551 11.399 I0.877 10.877 1.0311 

Criteria: 

' Y- ratio of the reading of the reference meter to the working DGM. Acceptable tolemnce of intlivitlual values from the average is +/_ 0.02, with a value between 0.95 antl 1.05. 

DGM Factor vs. Flow rate 

1.0500 

1.0400 

1.0300 

1.0200 

1.0100 

> 1.0000 

0.9900 

0.9800 

0.9700 

0.9600 

0.9500 

0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 1.10 1.20 1.30 

Flow Rate (cfm) 

TRC Air Measurements, Austin, TX 
Meter Box: Orifice Full Calibration 

Date: 

Prev. Calib. Date: 

Location: 

Technician: 

MeterSerial No: 

TRC Meter Box ID 

Atm. Pressure (corr. In Hg): 

Critical Vacuum+2 in Hg: 

Prev. Calib Factor (Y): 

10/17/2007 

8/9/2007 

TRC Austin south 

NTA 

A 

uncarrectetl: 29.14 --> 29.14 

16 in. Hg. (required minimum) 

1.0333 

Reference Orifice Set Orikce # K' Factor 

Manufacturer: Nutech Instruments 40 0.2398 

Model: LA40-73 48 0.3524 

Tested By: OMD 55 0.4635 

63 0.6026 

Initial Tem eratures iFinal Temperaturesl 

Orifce 

Serial # 

K' coefficient 

see above 

dH 

in. H20) min 

I Vol (initlal) 

cu ft 

Vol (fnal) 

cu ft 

Vol. Total 

cu k 

Inlet 

tleg F 

Oullet 

de F 

Inlet 

tle F 

Outlet 

de F 

Vacuum 

in H 

Initiai 

tle F 

Final 

de F 

40 0.2398 0.29 17.5 124.224 129.683 5.459 80 79 81 79 23 74.0 74.0 

48 0.3524 0.63 77 129.683 737.376 7.693 80 79 81 80 22 75.0 74.0 

55 0.4635 1.1 13 137.376 745.069 7.693 82 80 84 81 20 74.0 76.0 

63 0.6026 1.7 14 145.069 155.90fi 10.837 83 81 85 82 18.5 76.0 75.0 

Meter Box Dry Gas Meter Critical Orifice Dry Gas Meter 

Calibration 

Onfice 

Volume Volume Volume Volume Calibration 

Corrected Corrected Flow Corrected Correctetl Factor (Y) Factor (dH@) 

Vm (std) Vm (std) Rate Vcr (std) Vm (std) Value Variation Value Variation 

cu ft liters CFM cu k liters # # in H20 in H20 

510 147.34 0.312 1 5.29 149.87 7.017 -0.011 1.655 0.02 

7.34 207.72 0.453 7.55 213.85 1.029 0.001 1.670 0.04 

7.32 207.30 0.592 7.59 214.99 1.037 0.009 1.678 0.04 

10.31 297.92 0.774 10.62 300.86 1.031 0.002 7.535 -0.10 

Meter Box 

Criteria: 

' V- ralio of the reading of the calibration meter (cntical orifice) to the Meler Box DGM. Acceptable toterance of individual values from lhe average is +/- 0.02. 

" tlH- the orifice tlifferential pressure in inches of H20 that equates tu 0.75 cfm of air fiow at 68 F antl 29.92 in Hg, acceptable lolerance of intlivitlual values from the average is +/- 0.2. 

DifPerential Pressure vs. Flow Rate 

1.6 

1.6 

1.4 

1.2 O ~ 

_ c 

= 0.8 

D 

0.6 

0.4 

0.2 

0 

0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 .. Flow Rate (cfm) 

-1 

TRC Air Measurements Austin, TX 
Meter Box: Orifice Full Calibration 

Date: 10122/2007 

Prev. Calib. Date: 10/17/2007 

Location: TRC Austin Lab 

Technician: RAM 

MeterSerial No: 80715.00 

Cubix Meter Box ID A 

Atm. Pressure (corr. In 129.49 unconected: 29.65 

Critical Vacuum+2 in H 16 in. Hg. (required minimum) 

Prev. Calib Factor (Y): 1.0286 

Reference Orifice Set OriFice (#) K' Factor 

Manufacturer: Apex Instruments 40 0.2398 

Model: LA40-73 1 48 0.3524 

Tested By: SH 55 0.4635 

63 0.6026 

73 0.8162 

Initial Temnemfiires lFinni Tcmnorafurc. 

Orifce 

Serial # 

K'wefficienQ 

see above 

dH 

in. H20 

Time 

min 

Vol (initial) 

cu ft 

Vol (fna0 

cu k 

Vol. Total 

cu k 

Inlet 

de F 

Outiet 

tle F 

Inlet 

de F) 

Outlet 

de F 

Vacuum 

in H 

Initial 

de F 

Final 

(de F 

40 0.2398 03 24 298.200 1 305.439 1 7.239 1 70 69 75 72 23 71.0 72.0 

48 0.3524 0.69 17 305.439 312.948 7.509 75 72 79 75 21.5 72.0 74.0 

55 0.4635 1.1 12 312.948 319.965 7.017 79 75 80 78 20 74.0 74.0 

63 0.6026 1.8 8 319.965 326.060 6.095 80 76 1 82 78 19 74.0 74.0 

73 0.8162 3.9 8 326.060 1 333.834 1 7.774 1 82 78 1 85 1 74.0 1 74.0 

Meter Box 

Calibration Test Results Pass/Fail 

, ".AverageY: 1.0407 t PASS ~ 

:AVe,YW/In5°/eufpreviousvalue - YES 

,0,95 -Y=1.05- - -PASS - 

•"AVera eEH 1.738 PASS . 

Criteria: 

' Y- ratio of the reading of the calibration meter (cntical orifice) to the Meter Box DGM. Acceptabte tulerence of individual values from the averege is +/_ 0.02. 

"dH- the onfce differential pressure in inches of H20 that equates to 0.75 cfm of air Bow at 68 F antl 29.92 in Hg, acceptable tolerance of individual values from the average is +/- 0. 

Differential Pressure vs. Flow Rate 

4.5 

4 

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x 

c 

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0 

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1 

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0 

0.20 0.30 0.40 0.50 0.60 0.70 0.80 0.90 1.00 

Flow Rate (cfm) 

Meter Box Dry Gas Meter Critical Odfice Dry Gas Meter 

Calibration 

Orifce 

Volume Volume Volume Volume Calibration 

Conected Conected Flow Corrected Corrected Factor ff) Factor(dH 

Vm (sttl) Vm (sttl) Rate Vcr (std) Vm (std) Value VariaBon Value Variation 

cu k liters CFM cu k liters # # in H20 in H20 

7.09 200.79 0.302 7.36 208.47 1.038 -0.002 1.748 0.01 

7.31 206.99 0.442 7.65 216.70 1.047 0.006 1.708 -0.03 

6.81 192.84 0.585 7.10 201.00 1.042 0.002 1.689 -0.05 

5.91 167.33 0.762 6.15 174.21 1.041 0.000 1.627 -0.11 

7.55 213.74 1.037 7.81 22112 1.035 -0.008 1.920 0.18 

102207 Box A Full Cal.xls 
Quality Assurance Worksheet 

NOx Conversion Efficiency, System Bias, Response Time, Sample System Leak Checks 

Date: 10/21/2007 

Client: Hanson Brick 

Location: Elgin, Texas 

Tecbnician: JSG, JM, SJ, CJ, RAM, PC, TO 

Source: Lime Scrubber 

i`O, - NO Connersio€a l:fficie¢iss 

Certified concentration, NO zstandard: 45.90 

Measured concentration, NO Zstandard: 41.9 

E'ITxoi 91.3% 

Resuonse Time 

2X SYSTEM RESPONSE TIME: 

Saninle Svstem Leak Cliecl: 

Sample 

System ID 

Vacuum 

(in. Hg) 

Leak Rate 

(in. Hg/min) 

Pre test A 21.0 0.00 

Post test A 21.0 0.00 

Pre test B 21.0 0.00 

Post test B 21.0 0.25 

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Interference Response Test 

Date of Test: 1/16/2007 

Manufacture: California Analytical 

Model No.: 400-CLD 

Serial No.: 6412004 

Calibration Span: 100.5 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

Oz/COz 4.99/21.0 % 0.02 

02/CO2 21.1/5.04 % 0.00 

H20 i 4.50% 0.01 

CO/CH4 45.4/45.5 ppm 0.02 

NH3/SF6 10.2/10.0 ppm I 0.03 

S02 44.3 ppm 0.00 

1-12/He2 40/60 % 0.01 

Sum of Responses 0.09 

% of Calibration Span 0.09 

* Interferance must be less than 2.50% of calibration span 

OTRC 
Interference Response Test 

Date of Test: 1/16/2007 

Manufacture: Thermo Environmental 

Model No.: CO 48 

Serial No.: 48-27403-228 

Calibration Span: 99.9 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

Oz/COz 4.99/21.0 % 0.03 

02/CO2 21.1/5.04 % -0.01 

H20 4.50% 0.02 

CH4 50.5 ppm 0.02 

NH3/SF6 10.2/10.0 ppm 0.00 

S02 44.3 ppm 0.00 

H2/He2 40/60 % 0.04 

NO 15.16 ppm 0.01 

NOz 55.9 ppm 0.10 

Sum of Responses 0.21 

% of Calibration Span 0.21 

* Interferance must be less than 2.50% of calibration span 

AiiaLi 
Interference Response Test 

Date of Test: 1/16/2007 

Manufacture: Servomex 

Model No.:1400 02 1440 

Serial No.:01420C1/2534 

Calibration Span:21.1 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

H20 4.50% 0.00 

CO/CH4 45.4/45.5 ppm 0.00 

NH3/SF6 10.2/10.0 ppm 0.00 

S02 44.3 ppm 0.00 

H2/He2 40/60 % 0.00 

NO 15.16 ppm 0.00 

NOz 55.9 ppm 0.01 

Sum of Responses 0.01 

% of Calibration Span 0.05 

* Interferance must be less than 2.50% of calibration span 

OTRC 
Interference Response Test 

Date of Test: 1/16/2007 

Manufacture: Servomex 

Model No.: 1400 CO2 1440 

Serial No.: 1415C/2650 

Calibration Span: 21.0 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

H20 4.50% 0.00 

CO/CH4 45.4/45.5 ppm 0.01 

NH3/SF6 10.2/10.0 ppm 0.01 

S02 44.3 ppm 0.00 

H2/He2 40/60 % 0.00 

NO 15.16 ppm 0.00 

NO2 55.9 ppm 0.00 

Sum of Responses 0.02 

% of Calibration S an 0.10 

* Interferance must be less than 2.50% of calibration span 

~~ 
Interference Response Test 

Date of Test: 1/16/2007 

Manufacture:Western Research Ametek 

Model No.:S02 921 

Serial No.:AZ-921N-9088-1 

Calibration Span:44.3 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

H20 4.50% 0.04 

CO/CH4 45.4/45.5 ppm 0.01 

NH3/SF6 10.2/10.0 ppm 0.01 

H2/He2 40/60 % 0.06 

NO 15.16 ppm 0.00 

NOZ 55.9 ppm 0.00 

02/CO2 4.99/21.0 % 0.02 

02/CO2 21.1/5.04 % 0.00 

Sum of Responses 0.14 

% of Calibration S an 0.32 

* Interferance must be less than 2.50% of calibration span 

OTRC 
Interference Response Test 

Date of Test: 1/16/2007 

Manufacture: JUM Engineering 

Model No.: FID 3-300 

Serial No.: 9303161-33 

Calibration Span: 100.6 propane 

Technician: JSG 

Test Gas Type Concentration Analyzer Response 

HZO 4.50% 0.04 

CO 43.9 ppm 0.01 

NH3/SF6 10.2/10.0 ppm 0.03 

NO 15.16 ppm 0.00 

NOz 55.9 ppm 0.05 

02/CO2 4.99/21.0 % 0.10 

OZ/COz 21.1/5.04 % 0.01 

Sum of Responses 0.24 

% of Calibration S an 0.24 

* Interferance must be less than 2.50% of calibration span 

~~ 
Calibration Curves 

60 

50 

■ Propane 

40 

> 

E 

n 

n 

N 

C 0 30 .q 

G 

N 

u 

c 0 

U 

20 

— Linear(Propane) 

10 

01 ~ 

0.0 20.0 OV.V BV.V 1UU.0 1LU.0 14U.0 1bU.0 36U.0 CVU.V 

Area Counts 

Concentration = (Slope(m) x Area Counts ~ 

Initial Calibration Curve Finai Calibration Curve (Combination of all Calibrations) 

Com ound Slo e m R° Com ound Slo e m R' 

1 Pro ane t 0 270279 ':' 0 9998I3 l Pro ane s::0 295902 

Calibrafion Datz 

Initial Cal Gas Concentrations Finai Cal Gas Concentrations 

S 2311 ' 507 

Initial Area Counts Final Area Counfs 

1 Pco ane ; .21.8181 ~ 931798 S e 187,I067 ;_ 18.4301 ;. . 75.7512 " " -1502929, `. 
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.; 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 10:17:48 

Description: 5ppm C1-C6 

Data file: 102107_11.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785t 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

~ 

Component Retention Area Area % 

Methane 0.996 3.7446 3.5278 

Ethane 1.058 11.0501 10.4103 

Propane 1.211 22.0645 20.7871 

36.8591 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 10:32:37 

Description: 5ppm C1-C6 

Data file: 102107_13.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

, 

~ 

Component Retention Area Area % 

Methane 0.990 4.0471 3.1512 

Ethane 1.051 10.7147 8.3430 

Propane 1.202 21.0014 16.3527 

35.7631 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 10:39:45 

Description: 5ppm C1-C6 

Data file: 102107_14.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785f 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.990 3.2546 2.4218 

Ethane 1.052 10.7945 8.0321 

Propane 1.203 20.8884 15.5429 

34.9376 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 10:46:50 

Description: 50.7ppm C3 

Data file: 102107_15.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Locatlon: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

0.061 0.6446 0.1059 

0.505 22.5787 3.7096 

Methane 1.005 14.9608 2.4580 

Ethane 1.044 6.3398 1.0416 

Propane 1.204 188.5709 30.9815 -- 

C 

- 1.908 0.3412 0.0561 

- 2.030 1.5389 0.2528 

- 2.181 187.5732 30.8176— 

- 2.934 0.2531 0.0416 ~ 

- 3.031 0.6800 0.1117 

- 3.204 185.1759 30.4237 — 50. + ~– c3 

608.6570 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/2112007 10:51:21 

Description: 25.1ppm C3 

Data file: 102107_16.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

0.064 23.0271 3.5795 

0.164 115.2593 17.9169 

Ethane 

Propane 

1.051 

1.200 

1.3993 

92.8100 

0.2175 

14.4272 

C 

- ZS, ( p~^ } 

- 2.057 23.8366 3.7054 

2.226 94.1376 14.6336 

- 2.346 0.1598 0.0248 

3.692 92.5919 14.3933 - 

- 4.540 0.1237 0.0192 

- 4.565 0.1276 0.0198 

- 4.583 0.1591 0.0247 

- 4.695 94.1239 14.6315- Z~•~ ~r ~j 

- 5.254 0.1382 0.0215 

- 5.517 0.1284 0.0200 

- 5.587 0.1560 0.0243 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 U-95-4 -7- JO53 

Description: Kiln 2 Scrubber 

Data file: 102107_17.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785t 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.982 14.1878 67.7056 $~ n 

Ethane 1.030 3.3347 15.9138 

Propane 1.188 0.3371 1.6087 

17.8596 100.0000 

" ' 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 16:58:24 

Description: 25.1ppm C3 

Data file: 102107_40.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.957 12.7106 65.6739 

Ethane 1.005 3.4196 17.6688 

Propane 1.146 0.4982 2.5741 

Propane 1.200 1.4127 7.2989 

18.0411 100.0000 

FQ(LA3 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 17:14:53 

Description: 25.1 ppm C3 

Data file: 102107_41.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Ethane 

Propane 

1.016 

1.149 

0.1110 

75.3333 

0.0468 

31.7428 

2.346 0.2516 0.1060 

2.417 0.3393 0.1430 f 

31.8372 ' ~s 

P 

ly 

N25 

Pentane 2.591 75.5575 

3.945 9.0955 3.8325 

3.987 0.2735 0.1152 

4.169 76.3627 32.1765 y ZS• ~~ ~ 

~~ZS 

237.3245 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 17:28:05 

Description: 50.7 ppm C3 

Data file: 102107_42.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

~ 

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~ 

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Component Retention Area Area % 

Propane 1.145 149.9910 39.4677 

2.352 0.1125 0.0296 

2.432 2.8124 0.7400 3 

Pentane 2.590 149.5898 39.3621 

- 4.084 0.1742 0.0458 

- 4.132 0.1160 0.0305 

- 4.325 71.7971 18.8922 

- 5.378 2.3371 0.6150 

- 7.305 0.6041 0.1590 

- 7.445 1.1548 0.3039 

- 7.595 0.8493 0.2235 

- 7.740 0.4969 0.1308 

380.0351 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 17:36:45 

Description: 50.7 ppm C3 

Data file: 102107_43.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Propane 1.148 151.2953 49.7213 

2.382 0.1983 0.0652 

Pentane 2.485 0.9808 0.3223 

Pentane 2.625 151.8124 49.8912 

(<i~LlV~:i:1/iGbxrPPIr] 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 17:43:01 

Description: 5ppm c1-c6 

Data file: 102107_44.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Ethane 1.014 9.5578 12.3612 

Propane 1.155 19.0783 24.6741 

Butane 1.561 20.2575 26.1992 

Pentane 2.609 25.9508 33.5624 

5.299 1.5709 2.0317 

5.306 0.9058 1.1715 

77.3212 100.0000 
Lab name: TRC 

Client: Hanosn Brick 

Client ID: 154785 

Analysis date: 10/21/2007 17:52:23 

Description: 5ppm c1-c6 

Data file: 102107_45.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Ethane 1.012 9.5961 9.2536 

Propane 1.155 18.0910 17.4454 

Butane 1.565 20.0796 19.3630 

Pentane 2.620 25.4088 24.5020 

5.321 30.5254 29.4360 

103.7009 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 18:00:06 

Description: 5ppm c1-c6 

Data file: 102107_46.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785t 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Ethane 1.012 4.9596 4.7997 

Ethane 1.032 3.2264 3.1224 

Propane 1.154 18.1210 17.5369 

Butane 1.565 20.5963 19.9324 

Pentane 2.625 25.8936 25.0589 

5.355 30.5340 29.5497 

MRIrkIII%7i Bbx4rIIII] 
Method 26A Quality Assurance 

Fluoride Calibration 

Company Name Hanson Brick Source Kiln #2 Scrubber 

Facility Elgin, Texas Job No. 154785 

Sampling Date 10/21/2007 

Technicians JSG 

Calibration Curves Via US EPA Method 26 Section 5.2 

Initial Curve 

Scale=0 • 10n IC Calihra}inn Curvn- Fhinrldn 

Date Time Area 1 Area 2 Precision % Mean Area Conc /m L Calc /mL 

10/21/2007 08:31 1.0057 1.0524 2.27 1 6.25 6 

10/21/2007 0902 2.1385 2.1254 0.31 2 12.5 12 

10121/2007 09:36 4.3161 4.3194 0.04 4 25 25 

10121/2007 10:08 8.7842 8.8773 0.53 9 50 51 

10121/2007 11:44 17.3019 17.4534 0.44 17 100 100 

unecorreiarnon: u.auaaaeis 

120 

100 

y'5.7262x+0.1702 

- R

2 = 0.9999 

E 80 

ca 

d 60 

0 40 

U 

20 

0 

0 2 4 6 8 10 12 14 16 18 20 

Area(eounts( 

Final Curve IC Calihratinn Grtva Fhmridc 

Date Time Area 1 Area 2 Precision °/ Mean Area I Conc /mL Calc /mL I Drift % 

10/22/2007 15:37 1.0963 1.0961 0.01 1 6.25 6 0.54 

10/22/2007 16:08 2.1515 2.1463 0.12 2 12.5 12 0.24 

10122/2007 16:41 4.3246 4.3500 0.29 4 25 25 0.11 

10/22/2007 17:10 9.0120 9.0183 0.03 9 50 52 1.06 

10/22/2007 17:51 17.8693 17.8926 0.07 18 100 103 2.88 

Line Gorreianon: u.y8894bzbtl 

120 

100 

E 80 rn 

2. 60 y= 5.5616x+ 0.3972 

0 40 R' = 0.9999 

U 

20 

0 

0 2 4 6 8 10 12 14 16 18 20 

IArea (counts 

TRC 
Method 26A Qualit~ Assurance 

Chloride Calibratio 

Company Name Hanson Brick Source Kiln #2 Scrubber 

Facility Elgin, Texas Job No. 154785 

Sampling Date 10/21/2007 

Technicians JSG 

Calibration Curves Via US EPA Method 26 Section 5.2 

Initial Curve 

a,.re=n -inn ir 

Date Time Area 1 Area 2 Precision % Mean Area Conc /mL Calc /mL 

10/21/2007 0831 1.6369 1.6718 1.05 2 6.25 6 

10/21/2007 09:02 2.7004 2.6914 0.17 3 12.5 14 

10/2112007 09:36 4.1760 4.1714 0.06 4 25 24 

10/21/2007 10:08 7.6027 7.4650 0.91 8 50 49 

10/2112007 11:44 14.6233 14.8332 0.71 15 100 101 

LlneCorrelatlon: 0.999ti5336/ 

y = 7.216x - 5.6807 

120 R' = 0.9993 

100 

E 80 

a 

- 60 '

`o 40 

U 

20 

0 

0 2 4 6 8 10 12 14 16 

Area(counts) 

Final Curve Ir: rAllllfA}jnn r:nNP' r:hlnflfrP 

Date Time Area 1 Area 2 Precision % Mean Area Conc /mL Calc /mL Drift % 

10/2212007 15:37 1.8681 1.9084 1.07 2 6.25 8 1.69 

10/2212007 16:08 2.5964 2.6288 0.62 3 12.5 13 0.60 

10/2212007 16:41 4.0675 4.1071 0.48 4 25 24 0.62 

10/2212007 17:10 7.4187 7.3551 0.43 7 50 48 1.06 

10/2212007 1751 14.8919 15.0299 0.46 15 100 102 1.68 

Line Correlation: 0.998754567 

120 

100 

E 80 

~ y = 7.1289x - 5.3587 

60 R' = 0.9975 

0 40 

U 

20 

0 

0 2 4 6 8 10 12 14 16 

)Area (counts 

/ ~ ~t ~ ~ 
lon Chromatograph Analysis 

Sample Name: 6.25ug/mi STD Client: Hanson8rick 

Control Program. Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121/2007 8:31 Location: Elgin, Texas 

53826Hanson #28 modiied by TRC-Cubix Em lo ee ECD 1 100 

NS 3-414.8 S80 

88 

7 

il 

i 

6 

i 

5 

i 

38 

25 

13 

1 - Floride2 3QhlDride - 4.507 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.22 Floride 2.635 1.0057 1.66 

2 4.51 Chloride 2.932 1.6369 2.70 

3 11.33 n.a. 62.830 3.8025 6.27 

4 11.68 n.a. 131.111 54.1980 89.37 

Total: 199.508 60.6431 100.00 

Testing Pertormed by TRC 
lon Chromatograph Analysis 

Sample Name: 6.25ug/ml STD Client Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 8:46 Location: Elgin, Texas 

153826Hanson #29 6.25u /ml STD ECD 1 100 

N S 4 -91.P 27 

88 

7 

63 

5 

38 

2 

13 

1 - Floride2 3Qbbride - 4.500 

3 - 7.693 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.23 Floride 2.780 1.0524 1.72 

2 4.50 Chloride 2.909 1.6718 2.74 

3 7.69 n.a. 0.009 0.0022 0.00 

4 11.27 n.a. 64.084 3.8862 6.36 

5 11.63 n.a. 131.445 54.4591 89.17 

Total: 1 201.226 61.0717 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 12.5ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2112007 9:02 Location: Elgin, Texas 

153826Hanson#30 12.5u /mISTD ECD 1 10D 

uS 4-91. 73 

88 

7 

63 

5 

3 

2 

1 - Floride2 30130de - 4.470 

3 - 7.543 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

S 

Area 

S`min 

Rel.Area 

% 

1 3.21 Floride 5.709 2.1385 3.40 

2 4.47 Chloride 5.599 2.7004 4.29 

3 7.54 n.a. 0.166 0.2112 0.34 

4 11.22 n.a. 66.680 4.0189 6.39 

5 11.57 n.a. 130.844 53.8647 85.59 

Total: 208.998 62.9336 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 12.5ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121/2007 9:18 Location: Elgin, Texas 

153826Hanson#31 12.5u /mISTD ECD 1 1W 

NS 

88 

7 

63 

5 

4 51aL38 

25 

13 

1 - Floride2•3C11fl8ride - 4.417 

3 - 7.297 

min -10- 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

S 

Area 

S'min 

Rel.Area 

% 

1 3.18 Floride 5.794 2.1254 0.49 

2 4.42 Chloride 5.534 2.6914 0.62 

3 7.30 n.a. 0.174 0.2192 0.05 

4 11.13 n.a. 511.120 58.0012 13.34 

5 11.44 n.a. 509.760 371.7754 85.50 

Total: 1032.383 434.8126 100.00 

Testing PerFormed by TRC 
lon Chromatograph Analysis 

Sample Name: 25ug/mi STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 9:36 Location: Elgin, Texas 

153826Hanson #32 25u /ml STD ECD 1 

10 

NS A 3111 7 

88 

75 

63 

5 

3 

25 

13 1 - Floride2 3dgAride - 4.430 

3 - 7.467 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 1 2.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.17 Floride 11.908 4.3161 1.00 

2 4.43 Chloride 10.934 4.1760 0.97 

3 7.47 n.a. 0.166 0.2013 0.05 

4 11.14 n.a. 511.078 58.2823 13.51 

5 11.45 n.a. 509.779 364.4433 84.48 

Total: 1 1043.865 431.4190 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 25ug/mi STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2112007 9:52 Location: Elgin, Texas 

153826Hanson #33 25u /ml STD ECD 1 10 

N S 4511. .873 

88 

7 

63 

5 

38 

2 

1 g 1- Floride2 3CtQride - 4.387 

; 3 - 7.380 ' 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S'min 

Rel.Area 

% 

1 3.15 Floride 12.055 4.3194 1.00 

2 4.39 Chloride 10.894 4.1714 0.97 

3 7.38 n.a. 0.176 0.2206 0.05 

4 11.07 n.a. 511.255 57.7796 13.41 

5 11.37 n.a. 509.787 364.3584 84.57 

Totai: 1044.167 430.8492 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 50ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 10:08 Location: Elgin, Texas 

153826Hanson #34 50u /mISTD ECD 1 100 

N S 3 41-11 0 

88 

7 

63 

5 

38 

i - Floride - 3.037 

2 2 - Chloride - 4.333 

1 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.04 Floride 28.318 8.7842 2.07 

2 4.33 Chloride 22.906 7.6027 1.79 

3 11.04 n.a. 510.941 60.0603 14.17 

4 11.31 n.a. 509.775 347.5216 81.97 

Total: 1071.939 423.9688 100.00 

Testing Pertormed by TRC 
lon Chromatograph Analysis 

Sample Name: 50ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 10:23 Location: Elgin, Texas 

10 153826Hanson #35 50u /mISTD ECD 1 

NS M1bF71 0 

88 

il 

75 

63 

5 

38 

1 - Floride - 3.050 

2 2 - Chloride - 4.350 

13 

3 - 7.230 ' 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.05 Floride 28.211 8.8773 2.09 

2 4.35 Chloride 22.335 7.4650 1.76 

3 7.23 n.a. 0.157 0.1844 0.04 

4 11.04 n.a. 510.982 61.8144 14.54 

5 11.31 n.a. 509.783 346.9300 81.58 

Total: 1071.468 425.2711 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 100ug/mi STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2112007 11:44 Location: Elgin, Texas 

10 153826Hanson #36 100u /ml STD ECD 1 

NS 34311. ED7 

8 

7 

63 1 - Floride - 3.013 

5 2 - Chloride - 4.290 

38 

2 

1 

-1 min 

0.0 1.3 2.5 3.8 5.0 6.3 7.5 8.8 10.0 11.3 13.4 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.01 Floride 61.327 17.3019 4.31 

2 4.29 Chloride 48.432 14.6233 3.64 

3 11.01 n.a. 510.225 341.9576 85.23 

4 11.21 n.a. 83.321 27.3479 6.82 

Total: 703.305 401.2307 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 100ug/ml STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121/2007 11:58 Location: Elgin, Texas 

1538261-lanson #37 100u /ml STD ECD 1 10 

PS 34111. M 

88 

7 

63 1 - Floride - 3.037 

5 2 - Chloride - 4.323 

38 

2 

13 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S'min 

Re1.Area 

% 

1 3.04 Floride 61.867 17.4534 4.33 

2 4.32 Chloride 47.022 14.8332 3.68 

3 11.09 n.a. 510.308 343.4519 85.24 

4 11.28 n.a. 82.901 27.1945 6.75 

Total: 702.097 402.9331 100.00 

Testing PerFormed by TRC 
lon Chromatograph Analysis 

Sample Name: 6.25ug/ml STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/22/2007 15:37 Location: Elgin, Texas 

100,153826Hanson #57 6.25u /ml STD ECD 1 

NS I 4-90.6 0390 

88 

75 

63 

5 

38 

25 

13 

1 - Floride - 29,407hloride - 4.403 

3 - 7.167 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S'min 

Rel.Area 

% 

1 2.95 Floride 2.985 1.0963 1.74 

2 4.40 Chloride 3.144 1.8681 2.96 

3 7.17 n.a. 0.120 0.1295 0.21 

4 10.63 n.a. 49.295 5.2211 8.28 

5 10.99 n.a. 138.541 54.7409 86.81 

Total: 1 194.085 63.0559 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 6.25ug/ml STD Clienf: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/22/2007 15:51 Location: Elgin, Texas 

10 153826Hanson #58 6.25u /ml STD ECD 1 

FS 4-50.6 ®20 

88 

7 

63 

5 

38 

2 

13 

1 - Floride - 2.94~loride - 4.373 3 - 7.117 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S`min % 

1 2.94 Floride 2.834 1.0961 1.68 

2 4.37 Chloride 3.094 1.9084 2.93 

3 7.12 n.a. 0.139 0.1619 0.25 

4 10.55 n.a. 51.914 5.1659 7.93 

5 10.92 n.a. 141.853 56.7929 87.21 

Total: 199.833 65.1253 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 12.5ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10122/2007 16:08 Location: Elgin, Texas 

10 153826Hanson #59 12.5u /mISTD ECD 1 

uS 4-98. ®37 

88 

7 

63 

5 

38 

2 

13 ,''.. 

1 - Floride - a. 9rghloride - 4.380 '. 

3 - 7.127 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 2.95 Floride 5.988 2.1515 0.48 

2 4.38 Chloride 5.365 2.5964 0.58 

3 7.13 n.a. 0.136 0.1572 0.04 

4 10.61 n.a. 510.642 74.7076 16.80 

5 10.94 n.a. 509.888 364.9620 82.09 

Total: 1032.019 444.5746 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 12.5ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif Method: Hanson Project #: 154785 

Recording Tlme: 10/2212007 16:23 Location: Elgin, Texas 

10 153826Hanson i180 12.5u /mISTD ECD 1 

NS 4-90.5 3330 

6 

7 

63 

5 

38 

2 

13 

1 - Floride - VVhloride - 4.367 . 3 - 7.107 . 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S*min % 

1 2.94 Floride 5.885 2.1463 3.27 

2 4.37 Chloride 5.440 2.6288 4.01 

3 7.11 n.a. 0.146 0.1773 0.27 

4 10.57 n.a. 53.951 5.9896 9.13 

5 10.93 n.a. 138.935 54.6718 83.32 

Total: F 204.356 65.6137 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 25ug/ml STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012212007 16:41 Location: Elgin, Texas 

10 153826Hanson #61 25u /ml STD ECD 1 

NS 4-98. 867 

88 

7 

63 

5 

38 

25 

1 - Floride - 2.943 

13 2 - Chloride - 4.377 

3 - 7.140 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

ps 

Area 

S`min 

Rel.Area 

% 

1 2.94 Floride 13.564 4.3246 6.56 

2 4.38 Chloride 10.344 4.0675 6.17 

3 7.14 n.a. 0.139 0.1581 0.24 

4 10.63 n.a. 51.821 6.2482 9.48 

5 10.97 n.a. 132.930 51.1390 77.56 

Total: 1 208.797 65.9373 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 25ug/mi STD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2212007 16:56 Location: Elgin, Texas 

100 153826Hanson #62 25u /ml STD ECD 1 

uS 4-90. A87 

88 

7 

6 

5 

38 

25 

13 1 - Floride - 2.957 

2 - Chloride - 4.390 

3 - 7.160 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

IJS 

Area 

S*min 

Rel.Area 

% 

1 2.96 Floride 13.113 4.3500 6.36 

2 4.39 Chloride 10.026 4.1071 6.01 

3 7.16 n.a. 0.135 0.1539 0.23 

4 10.64 n.a. 57.858 6.1919 9.06 

5 10.99 n.a. 136.553 53.5475 78.34 

Total: 1 217.686 68.3504 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 50ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012212007 17:10 Location: Elgin, Texas 

153826Hansoni163 50u /mISTD ECD 1 I, 10 

N S 45141. 917 . 

88 

75 

63 

5 

38 

1 - Floride - 2.960 

2 

2 - Chloride - 4.400 

1 

6.963 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14. 0 

No. Ret.Time 

min 

Peak Name Height 

IJS 

Area 

S'min 

Rel.Area 

% 

1 2.96 Floride 31.442 9.0120 2.10 

2 4.40 Chloride 21.080 7.4187 1.73 

3 6.96 n.a. 0.132 0.1534 0.04 

4 10.63 n.a. 510.832 68.2457 15.92 

5 10.92 n.a. 509.895 343.7748 80.21 

Total1 1073.381 428.6046 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 50ug/mISTD Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10122/2007 17:36 Location: Elgin, Texas 

153826Hanson #64 50u /mISTD ECD 1 10 

NS ~ 4-99. 333 

8 

7 

63 

5 

38 

i - Floride - 2.947 

2 2 - Chloride - 4.407 

13 

6.970 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S`min 

Re1.Area 

% 

1 2.95 Floride 32.740 9.0183 12.50 

2 4.41 Chloride 21.912 7.3551 10.19 

3 6.97 n.a. 0.111 0.1215 0.17 

4 10.60 n.a. 62.900 6.5671 9.10 

5 10.93 n.a. 129.377 49.1084 68.05 

Total: 247.040 72.1704 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 100ug/ml STD Client Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2212007 17:51 Location: Elgin, Texas 

1538261-lanson #65 100u /ml STD ECD 1 100 

N S 4 51-0I 3370 

8 

7 

1 - Floride - 2.947 

6 

5 2 - Chloride - 4.403 

38 

25 

1 

3 - 6.973 i . ._— L _ 1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 2.95 Floride 65.546 17.8693 4.44 

2 4.40 Chloride 48.403 14.8919 3.70 

3 6.97 n.a. 0.109 0.1165 0.03 

4 10.64 n.a. 510.609 334.5583 83.07 

5 10.87 n.a. 105.364 35.3277 8.77 

Total: 730.031 402.7637 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: 100uglml STD Client Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10122/2007 18:05 Location: Elgin, Texas 

10 153826Hanson i166 100u !ml STD ECD 1 

OS 4 5101 . 0 

88 

7 

1 - Floride - 2.923 

6 

2 - Chloride - 4.373 

5 

38 

25 

13 

6.940 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 2.92 Floride 66.198 17.8926 4.38 

2 4.37 Chloride 51.181 15.0299 3.68 

3 6.94 n.a. 0.108 0.1155 0.03 

4 10.64 n.a. 510.487 339.9618 83.24 

5 10.88 n.a. 104.996 35.4315 8.68 

Total: 732.970 408.4312 100.00 

Testing Performed by TRC 
APPENDIX D: 

CALIBRATION CERTIFICATIONS 
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3434 Route 22 West, Branchburg, New Jersey 08876 USA 

,/7`Cctra ISO 9001:2000 

/~ Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0114982 

ITEM# : 1 

P.O.# : 2007141. T-8 Jason 

CERTIFICATION DATE: 9113/2007 

EXPIRATION DATE: 9/1112009 

CERTIFICATION HISTORY 

CYLINDER # : CC-187589 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

PRODUCT CODE: TRC-25 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Monoxide 8/29/2007 

9/1312007 

25.29 ppm 

25.39 ppm 

25.3 ppm +/- 1% 

Nitric Oxide 

NOx 

8/30/2007 

9/11/2007 

25.28 ppm 

25.27 ppm 

25.3 ppm 

25.3 ppm 

+/- 1% 

Reference Value Only 

Propane 9/1212007 25.4 ppm 25.4 ppm +/- 1% 

I3ALANGE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Carbon Monoxide NTRM-81679 CC-134736 101.0 ppm 

Nitric Oxide NTRM-81684 CC-202693 98.8 ppm 

Propane GMIS-1 CC-113884 100.3 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Carbon Monoxide Horiba VIA-510 1-100021-2Y NDIR 9/5/2007 

Nitric Oxide CAI-400-CLD 6L09004 Cheml 8/28/2007 

Propane H. Packard 6890 US00001434 GC - FID 9/412007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST:&/ )a DATE: 9/13/2007 

CODY HAMLIN 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

,pEctP~a 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0114982 

ITEM# : 2 

P.O.# : 2007141, T-8 Jason 

CERTIFICATION DATE: 9/13/2007 

EXPIRATION DATE: 9/11/2009 

CERTIFICATION HISTORY 

ISO 9001:2000 

EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CYLINDER # : CC-250142 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

PRODUCT CODE: TRC-25 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Monoxide 8/29/2007 

9/13/2007 

50.66 ppm 

50.57 ppm 

50.6 ppm +/_ 1% 

Nitric Oxide 

NOx 

8/30/2007 

9/11/2007 

50.26 ppm 

50.31 ppm 

50.3 ppm 

50.4 ppm 

+/- 1% 

Reference Value Only 

Propane 9/12/2007 45.2 ppm 45.2 ppm +/- 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCESTANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Carbon Monoxide NTRM-81679 CC-134736 101.0 ppm 

Nitric Oxide NTRM-81684 CC-202693 98.8 ppm 

Propane GMIS-1 CC-113884 100.3 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Carbon Monoxide Horiba VIA-510 1-1000212Y NDIR 9/5/2007 

Nitric Oxide CAI-400-CLD 6L09004 Cheml 8/28/2007 

Propane H. Packard 6890 US00001434 GC - FID 9/4/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: ~

A4 

DATE: 9/13/2007 

CODY HAMLIN 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

;pEctra ISO 9001:2000 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: Cubix Corporation 

SGI ORDER # : 0086921 

ITEM# : 4 

P.O.#: 2006136,T8TREY 

CERTIFICATION DATE: 3/29/2006 

EXPIRATION DATE: 3/28/2008 

CERTIFICATION HISTORY 

CYLINDER # : CC-126734 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Monoxide 3/21/2006 

3/28/2006 

84.82 ppm 

84.44 ppm 

84.6 ppm +/-1% 

Nitric Oxide 

NOx 

3/15/2006 

3/28/2006 

85.90 ppm 

85.67 ppm 

85.8 ppm 

85.8 ppm 

+/_ 1% 

Reference Value Only 

Propane 3/29/2006 85.8 ppm 85.8 ppm +/_ 1% 

tlALANC:t Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCESTANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Carbon Monoxide NTRM-81679 CC-135126 101 ppm 

Nitric Oxide NTRM-81684 CC-202720 98.8 ppm 

Propane GMIS-1 CC-113884 100.3 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Carbon Monoxide Horiba VIA-510 570423011 NDIR 3/23/2006 

Nitric Oxide CAI-400-CLD 6L09004 Cheml 3/22/2006 

Propane H. Packard 6890 US00001434 GC - FID 3/6/2006 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: DATE: 3/2912006 

CHERYL PATINO 

Tel: +1908-252-9300 Fax:+1 908-252-0811 

www.spectragases.com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

pECI~ a ISO 9001:2000 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0106245 

ITEM# : 4 

P.O.# : 2006666,T8GRIZZ 

CERTIFICATION DATE: 4/5/2007 

EXPIRATION DATE: 4/2/2009 

CERTIFICATION HISTORY 

CYLINDER # : CC-98984 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Monoxide 3/2712007 

4/5/2007 

252.2 ppm 

253.1 ppm 

253 ppm +/- 1% 

Nitric Oxide 

NOx 

3/26/2007 

4/2/2007 

249.6 ppm 

249.6 ppm 

250 ppm 

250 ppm 

+/- 1% 

Reference Value Only 

Propane 3/28/2007 251 ppm 251 ppm +/-1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Carbon Monoxide GMIS-1 CC-106962 505 ppm 

Nitric Oxide GMIS-1 CC-135383 251 ppm 

Propane GMIS-1 CC-20010 1013 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Calbon Monoxide Horiba VIA-510 H0002L2Y NDIR 3/27/2007 

Nitric Oxide CAI-400-CLD 6L09004 Cheml 3/29/2007 

Propane H. Packard 6890 US00001434 GC - FID 3/13/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: DATE: 4/5/2007 

CHERYL PATINO 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www. spectragases. com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

pE' tra ISO 9001:20000 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0106245 

ITEM# : 5 

P.O.# : 2006666,T8GRI77 

CERTIFICATION DATE: 4/5/2007 

EXPIRATION DATE: 4/4/2009 

CERTIFICATION HISTORY 

CYLINDER # : CC-85249 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Monoxide 3/28/2007 

4/5/2007 

496.1 ppm 

496.3 ppm 

496 ppm +/- 1% 

Nitric Oxide 

NOx 

3/27/2007 

4/4/2007 

506.1 ppm 

505.4 ppm 

506 ppm 

506 ppm 

+/- 1% 

Reference Value Only 

Propane 3/2812007 450 ppm 450 ppm +/_ 1% 

Lt9ALANGt Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRMINTRM# CYLINDER# CONCENTRATION 

Carbon Monoxide GMIS-1 CC-106962 505 ppm 

Nitric Oxide NTRM-81687 CC-131062 992 ppm 

Propane GMIS-1 CC-20010 1013 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Carbon Monoxide Horiba VIA-510 1-100021-2Y NDIR 3/27/2007 

Nitric Oxide CAI-400-CLD 6L09004 Cheml 4/4/2007 

Propane H. Packard 6890 US00001434 GC - FID 3/13/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: DATE: 4/5/2007 

CHERYL PATINO 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

t

Eetra ISO 9001:2000 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0106245 

ITEM# : 2 

P.O.#: 2006666,T8GRI77 

CERTIFICATION DATE: 4/3/2007 

EXPIRATION DATE: 4/3/2010 

CERTIFICATION HISTORY 

CYLINDER # : CC-131257 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 590 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Dioxide 4/3/2007 10.07 % 10.07 % +/- 1% 

Oxygen 4/3/2007 10.00 % 10.00 % +/- 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# I CYLINDER# CONCENTRATION 

Carbon Dioxide NTRM-82745x CC-79933 20.0 % 

Oxygen NTRM-82659x CC-83906 22.8 % 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL# DETECTOR CALIBRATION 

DATE(S) 

Carbon Dioxide CIA-300 S03001 NDIR 4/3/2007 

Oxygen CAI-300 S03001 PM 3/29/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: DATE: 4/3/2007 

TED NEEME 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
t

POE"Ctre 

Spectra Gases Inc. 

3434 Route 22 West, Branchburg, New Jersey 08876 USA 

ISO 9001:2000 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0098632 

ITEM# : 4 

P.O.# : 2006465,T8GRI77 

CERTIFICATION DATE: 11/3/2006 

EXPIRATION DATE: 11/312009 

CERTIFICATION HISTORY 

EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CYLINDER # : CC-94734 

CYLINDER PRES: 1900 PSIG 

CGA OUTLET: 590 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Carbon Dioxide 11/3/2006 5.04 % 5.04 % +/- 1% 

Oxygen 11/3/2006 21.1 % 21.1 % +/_ 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Carbon Dioxide GMIS-1 CC-85169 5.02 % 

Oxygen NTRM-82659x CC-83906 22.8 % 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Carbon Dioxide CAI-300 S03001 NDIR 11/1/2006 

Oxygen CAI-300 S03001 PM 10/16/2006 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: DATE: 11/3/2006 

JAMES SCHMIDT 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
3434 Route 22 West, Branchburg, New Jersey 08876 USA 

t

Octra ISO 9001:2000 

Spectra Gases Inc. 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

RECERTIFICATION OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: Cubix Corporation 

SGI ORDER # : 103425 

ITEM# : 1 

P.O.# : 2006589, T8Jason 

CERTIFICATION DATE: 2/6/2007 

EXPIRATION DATE: 2/6/2009 

CERTIFICATION HISTORY 

CYLINDER # : CC-133266 

CYLINDER PRES: 1800 PSIG 

CGA OUTLET: 660 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Nitrogen Dioxide 6/2072006 

2/6/2007 

46.10 ppm 

45.73 ppm 

45.9 ppm +/- 3% 

13ALANGE Air 

PREVIOUS CERTIFICATION DATES: 6/2712006 by Spectra Gases 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Nitrogen Dioxide NTRM-82660 CC-200753 97.6 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL# DETECTOR CALIBRATION 

DATE(S) 

NitrogenDioxide Thermo42i-HL 621417605 Cheml 2/6/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: ~ i' DATE: 2/6/2007 

FRED PIKULA 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
hka SPECTRR CASES INC. 

3434 Route 22 West • Sranehburg, Nd 08878 USA Tel.: (908) 252-9300 •(S00) 932-0624 • Faxi (908) 252-0811 

Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

RECERTIFICATION OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CUSTOMER: Cubix Corporation CYLINDER # : CC-143342 

SGI ORDER # 0072957 CYLINDER PRES: 1200 PSIG 

ITEM# : CGA OUTLET: 660 

P.O.# : 2005477,T8Shane 

CERTIFICATION DATE: 6/22/2005 

EXPIRATION DATE: 6/2212008 

CERTIFICATION HISTORY 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Sulfur Dioxide 4/23/2003 

6/22/2005 

45.80 ppm 

45.31 ppm 

45.6 ppm +/- 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: 4/23/2003 by Spectra Gases 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Sulfur Dioxide NTRM-81694 CC-162874 96.1 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL# DETECTOR CALIBRATION 

DATE(S) 

Sulfur Dioxide Horiba VIA-510 851221093 NDIR 612/2005 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF T/HE C~ YLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: ~ 1' DATE: 6/22/2005 

FRED PIKULA 
t

P2tra 

Spectra Gases Inc. 

3434 Route 22 West, Branchburg, New Jersey 08876 USA 

ISO 9001:2000 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0108271 

ITEM# : 3 

P.O.# : 2007023,T1 1 TREY 

CERTIFICATION DATE: 5/11/2007 

EXPIRATION DATE: 5/11/2009 

CERTIFICATION HISTORY 

EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CYLINDER # : CC-94390 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

PRODUCT CODE: TRC 17 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Sulfur Dioxide 5/3/2007 

5/11/2007 

101.8 ppm 

101.3 ppm 

101.5 ppm +/- 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCESTANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Sulfur Dioxide GMIS-1 CC-143657 193.4 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Sulfur Dioxide Horiba VIA-510 851221093 NDIR 5/9/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: 

/' - 

DATE: 5/11/2007 

FRED PIKULA 

Tel:+1 908-252-9300 Fax:+1 908-252-0811 

www.spectragases.com 
SPECTRA GASES INC. 

!3 ki 3434 Route 22 Wesfy Branchburg, Nd 08876 USA Tel.' (908) 252-9300 •(800) 932-0624 • Fax (908) 25220811 

Shipped From: 80 Intlustrial Drive • Alpha, NJ 08865 

RECERTIFICATION OF ANALYSIS EPA PROTOCOL MIXTURE 

PROCEDURE#: G2 

CUSTOMER: Cubix Corporation CYLINDER #: CC-130956 

SGI ORDER #: 0072957 CYLINDER PRES: 2000 PSIG 

ITEM# : 1 CGA OUTLET: 660 

P.O.# : 2005477.T8Shane 

CERTIFICATION DATE: 6/22/2005 

EXPIRATION DATE: 6/22/2008 

CERTIFICATION HISTORY 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Sulfur Dioxide 4/2412003 

6/22/2005 

257.0 ppm 

255.8 ppm 

256 ppm +/_ 1% 

tfALANGt Nitrogen 

PREVIOUS CERTIFICATION DATES: 412412003 by Spectra Gases 

REFERENCESTANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Sulfur Dioxide GMIS-1 CC-135535 202 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Sulfur Dioxide Horiba VIA-510 851221093 NDIR 618/2005 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: ~ I'?' DATE: 6/22/2005 

FRED PIKULA 
L

Ctra 

Spectra Gases Inc. 

3434 Route 22 West, Branchburg, New Jersey 08876 USA 

ISO 9001:2000 

Shipped from: 80 Industrial Drive, Alpha, NJ 08865 

RECERTIFICATION OF ANALYSIS 

CUSTOMER: TRC Air Measurements 

SGI ORDER # : 0105188 

ITEM# : 1 

P.O.# : 2006625, T6 Ross 

CERTIFICATION DATE: 4/3/2007 

EXPIRATION DATE: 4/312010 

CERTIFICATION HISTORY 

EPA PROTOCOL MIXTURE 

PROCEDURE#: G1 

CYLINDER # : CC-65912 

CYLINDER PRES: 1700 PSIG 

CGA OUTLET: 660 

COMPONENT 

DATE OF 

ASSAY 

MEAN 

CONCENTRATION 

CERTIFIED 

CONCENTRATION 

ANALYTICAL 

ACCURACY 

Sulfur Dioxide 1/3/2005 

4/3/2007 

447.0 ppm 

445.1 ppm 

446 ppm +/- 1% 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: 11312005 by Spectra Gases 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# CYLINDER# CONCENTRATION 

Sulfur Dioxide NTRM-81662 CC-143755 990 ppm 

INSTRUMENTATION 

COMPONENT MAKE/MODEL SERIAL # DETECTOR CALIBRATION 

DATE(S) 

Sulfur Dioxide Horiba VIA-510 851221093 NDIR 4/3/2007 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

v! 

'

1 J~) 

ANALYST: ~ 1'

, 

DATE: 4/3/2007 

FRED PIKULA 

Tel: +1 908-252-9300 Fax: +1 908-252-0811 

www.spectragases.com 
APPENDIX E: 

DATA ACQUISITION RECORDS, 

GAS CHROMATOGRAMS, 

AND 

ION CHROMATOGRAMS 
Data Acquisition Records 

154785 Hanson Brick 

Source Run Number Date Time NOx (pmmv) CO (ppmv) 02 (%) CO2 (%) THC (ppmv) S02in (ppmv) S02out (ppmv) 

Kiln 2 Scrubber 10/21/2007 846:20 7.06 115.20 18.92 1.27 0.00 10.70 6.46 

Kiln 2 Scrubber 10/21/2007 8:47:20 0.31 96.65 18.33 1.60 0.00 12.20 8.10 

Kiln 2 Scrubber 10/21/2007 8:48:20 0.09 0.55 -0.01 -0.10 0.00 5.70 0.68 

Kiln 2 Scrubber 10/21/2007 8:49:20 0.04 0.55 -0.02 -0.11 0.00 4.55 0.62 

Kiln 2 Scrubber 10/21/2007 8:50:20 0.05 0.00 -0.04 0.07 0.00 0.00 0.62 

Kiln 2 Scrubber 10/21/2007 8:51:20 0.02 0.00 -0.05 0.05 0.00 -0.10 0.62 

Kiln 2 Scrubber 10/21/2007 8:52:20 0.00 0.05 -0.06 0.07 0.00 -0.10 -0.08 

Kiln 2 Scrubber 10/2112007 8:53:20 0.01 0.05 -0.06 0.05 0.00 -0.10 -0.14 

Kiln 2 Scrubber 10/21/2007 8:50:16 0.01 0.00 -0.06 0.05 0.00 -0.20 -0.14 

Kilu 2 Scrubber 10/21/2007 85113 -0.14 0.00 -0.07 0.04 0.00 0.10 -0.14 

Kiln 2 Scrubber CE 10/21/2007 8:52:13 -0.13 0.05 -0.08 0.05 0.00 0.10 -0.20 

Kiln 2 Scrubber 10/21/2007 853:13 43.47 165.55 6.15 4.78 0.00 0.00 -0.14 

Kiln2Scrubber 10/21/2007 8:54:13 49.83 480.75 9.95 10.01 0.00 346.55 84.64 

Kiln 2 Serubber 10/2112007 8:55:13 50.21 485.30 9.96 10.02 0.00 363.00 100.80 

Kiln 2 Scrubber 10/21/2007 8:56:13 50.26 488.30 9.96 10.05 -0.10 363.80 101.12 

Kiln2Scrubber 10/21/2007 8:57:13 50.42 501.90 9.97 10.03 0.00 364.10 101.22 

Kiln 2 Scrubber 10/21/2007 8:58:13 50.36 496.35 10.02 10.06 0.00 373.25 101.28 

Kiln 2 Scrubber 10/21/2007 8:59:13 50.23 495.85 10.06 10.06 -0.10 444.09 101.30 

Kiln 2 Scrubber 10/21/2007 8:59:47 50.18 500.90 10.06 10.07 0.00 444.27 101.36 

Kiln 2 Scrubber CE 10l21l2007 9:00:47 50.29 496.35 10.06 10.05 0.00 444.39 101.30 

Kiln 2 Scrubber 10/21/2007 9:01:47 17.93 500.90 10.07 10.06 0.00 444.51 101.42 

Kiln 2 Scrubber 10/21/2007 9:02:47 24.41 249.80 21.20 5.09 0.00 417.62 101.42 

Kiln 2 Scrubber 10/21/2007 9:03:47 24.71 250.75 21.20 5.08 0.00 417.26 101.22 

Kiln 2 Scrubber - 10/21/2007 9:04:47 24.71 249.20 21.21 5.07 4.80 254.51 101.24 

Kiln 2 Scrubber 10/21/2007 9:05:47 24.70 251.25 21.23 5.07 0.00 254.57 101.24 

Kiln2Scrubber 10/21/2007 9:06:47 24.82 249.20 21.22 5.08 0.00 254.21 100.86 

Kiln 2 Scrubber 10/21/2007 9:07:42 24.78 250.30 21.21 5.08 0.00 254.39 44.38 

Ki1n 2 Scrubber CE 10/21/2007 9:08:42 24.70 251.75 21.23 5.08 0.00 254.45 44.48 

Kiln 2 Scrubber 10/21/2007 9:09:42 24.77 250.70 21.23 5.09 0.00 254.57 44.56 

Kiln 2 Scrubber CE 10/21/2007 9:10:27 56.32 237.60 10.12 10.07 0.00 253.23 5.68 

Kiln 2 Scrubber 10/21/2007 9:11:27 10.86 135.10 10.09 10.08 0.00 253.48 1.72 

Kiln 2 Scrubber 10/21/2007 9:12:27 82.90 120.55 10.10 10.07 0.00 247.80 1.78 

Kdn 2 Scrubber 10/21/2007 9:13:27 2.11 4.55 -0.03 0.10 0.00 46:65 196.48 

Kiln 2 Scrubber 10/21/2007 9:14:27 0.20 0.05 -0.05 0.11 0.00 47.20 198.92 

Kiln 2 Scrubber 10/21/2007 9:14:57 0.10 0.05 -0.05 0.09 8.20 47.20 198.92 

Kiln 2 Scrubber 10/21/2007 9:15:57 0.15 0.05 -0.05 0.08 10.30 50.61 198.92 

Kiln 2 Scrubber 10/21/2007 9:16:57 0.44 0.05 -0.07 0.10 4.60 236.16 53.36 

Kiln 2 Scrubber SSB 10l21/2007 9:17:56 0.40 0.05 -0.07 0.09 -2.30 245.00 44.50 

Kiln 2 Scrubber 10/21/2007 9:18:56 0.46 0.05 -0.07 0.08 4.00 246.83 42.18 

KOn 2 Scrubber 10/21/2007 9:19:56 0.45 0.05 -0.08 0.12 -6.80 247.38 41.58 

Kiln 2 Scrubber 10/21/2007 9:20:56 36.94 24.00 -0.08 0.12 -1.60 63.41 24.26 

Kiln 2 Scrubber 10/21/2007 9:21:56 49.10 46.60 -0.09 0.10 4.80 20.91 11.02 

Kiln 2 Scrubber 10/21/2007 9:22:56 27.80 30.55 -0.07 0.10 4.80 14.39 6.52 

Kiln 2 Scrubber SSB 10/21/2007 9:23:42 24.87 24.00 -0.09 0.11 4.70 12.07 4.82 

Kiln2Scrubber 10/21/2007 9:24:42 24.57 24.00 -0.08 0.10 -103.80 10.43 4.16 

Kiln 2 Scrubber 10/21/2007 9:25:42 24.63 24.00 -0.08 0.09 0.00 10.00 3.96 

Kiln 2 Scrubber 10/21/2007 9:26:42 6.63 8.10 7.42 7.76 0.00 11.04 4.02 

Kiln 2 Scrubber 10/21/2007 9:27:42 1.42 1.10 9.53 9.58 0.00 11.16 3.84 

Kiln 2 Scrubber 10/21/2007 9:28:03 0.88 0.55 9.71 9.72 0.00 11.59 3.72 

Kiln 2 Scmbber SSB 10/2112007 9:29:03 0.42 0.05 9.91 9.95 0.00 12.07 3.42 

Kiln 2 Scrubber 10/21/2007 9:30:03 120.58 118.60 3.86 3.46 -135.49 12.87 2.64 

Kiln 2 Scrubber 10/21 /2007 9:31:03 121.72 231.05 0.45 0.69 133.14 13.48 2.02 

Kiln 2 Scrubber 10/21/2007 9:31:57 121.72 247.25 0.02 0.22 129.64 14.33 1.72 

Kiln 2 Scrubber SSB 10/21/2007 9:32:57 121.72 251.75 -0.04 0.13 127.65 15.85 1.60 

Kiln 2 Scrubber 10/21/2007 9:33:57 121.73 156.05 -0.07 0.11 0.00 16.40 1.48 

Kiln 2 Scrubber 10/21/2007 9:34:27 49.46 54.75 -0.07 0.12 0.00 16.65 1.42 

Kiln 2 Scrubber SSB 10/21/2007 9:35:27 7.00 7.65 -0.07 0.13 0.00 17.13 1.30 

Kiln 2 Scrubber 10/21/2007 9:36:27 24.83 13.70 -0.08 0.13 22.06 17.20 1.24 

Kiln 2 Scrubber 10/21/2007 9:37:27 60.62 47.65 -0.06 0.13 83.55 17.38 2.02 

Kiln 2 Scrubber 10/21/2007 9:37:58 71.94 67.25 -0.07 0.12 85.74 17.38 1.78 

Kiln 2 Scrubber SSB 10/21/2007 9:38:58 80.37 76.75 -0.08 0.12 86.48 17.68 1.60 

1 C: TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scmbber 10212007 9:39:52 79.74 76.75 -0.07 0.11 50.43 17.80 1.54 

Kdn 2 Serubber 1021/2007 9:40:52 59.89 57.25 -0.07 0.13 50.11 17.62 1.48 

Kiln 2 Scrubber 10212007 9:41:52 50.60 48.60 -0.07 0.12 21.14 18.05 1.42 

Kiln 2 Scrubber 10212007 9:42:52 33.44 32.05 -0.08 0.11 21.33 18.41 1.36 

Kiln 2 Scrubber 10/21/2007 9:43:52 27.68 26.60 -0.09 0.12 21.45 18.17 1.30 

Kilu 2 Scrubber 10/21/2007 9:44:52 25.70 24.55 -0.08 0.11 21.31 18.23 1.24 

Kiln 2 Scrubber 10212007 9:45:52 24.97 24.10 -0.07 0.12 86.31 18.23 0.92 

Kiln 2 Scrubber THC CE 10212007 9:46:52 57.65 54.35 -0.08 0.13 85.85 18.48 1.12 

Kiln 2 Scrubber 10212007 9:47:52 76.19 73.40 -0.08 0.12 86.93 18.60 1.12 

Kiln 2 Scrubber 10212007 9:48:23 80.10 76.85 -0.08 0.11 87.46 18.48 1.06 

Kibt 2 Scrubber 10212007 9:49:23 83.01 79.85 -0.08 0.12 86.71 18.78 1.00 

Kilu 2 Scrubber 10/212007 9:50:23 84.19 81.35 -0.08 0.13 50.80 18.78 1.06 

Kiln 2 Scrubber TT-IC CE ] 0212007 9:51:08 62.89 62.25 -0.09 0.12 48.88 18.72 0.94 

Kiln 2 Scrubber 10212007 9:52:08 51.26 49.70 -0.09 0.13 48.23 18.84 0.94 

Kiln 2 Scrubber 10212007 9:53:08 34.71 40.65 -0.08 0.14 20.71 18.90 0.74 

Kiln 2 Scrubber 1 0212007 9:54:08 25.07 24.60 -0.08 0.14 24.36 18.96 0.62 

Kiln 2 Scrubber THC CE 10212007 9:54:10 24.94 24.60 -0.08 0.12 24.50 19.09 0.56 

Kiln 2 Scrubber 10212007 9:55:10 24.69 24.05 -0.09 0.13 23.52 18.96 0.56 

Kiln 2 Scrubber 102112007 9:56:10 24.69 24.05 -0.09 0.12 23.74 19.02 0.50 

Kiln 2 Scrubber 10212007 9:57:10 24.67 24.10 -0.08 0.14 24.61 18.96 0.50 

Kiln 2 Scrubber 10/21/2007 9:58:10 24.62 24.05 -0.08 0.14 25.33 19.21 0.44 

Kiln 2 Scmbber 10/21/2007 9:58:22 24.62 24.05 -0.09 0.14 25.27 19.15 0.50 

Kiln 2 Scrubber 10212007 9:59:22 24.67 24.05 -0.09 0.13 23.75 19.51 0.44 

Kiln 2 Scrubber 1 0/212007 10:00:22 24.55 24.05 -0.09 0.13 25.60 19.45 0.44 

KiW 2 Scrubber 10212007 10:01:22 24.60 24.05 -0.08 0.15 26.05 19.63 0.44 

Kiln 2 Scrubber 10212007 10:02:22 24.52 24.05 -0.08 0.14 25.03 19.57 0.44 

Kiln 2 Scrubber 10212007 10:03:22 39.75 24.05 -0.09 0.14 5.52 19.82 0.44 

Ktln 2 Scrubber 10212007 10:04:22 37.02 24.05 -0.09 0.17 5.40 19.45 0.44 

Kiln 2 Scrubber 10212007 10:05:22 38.40 24.05 -0.09 0.16 4.26 19.82 0.44 

Kiln 2 Scrubber 10212007 10:06:22 38.83 67.80 9.74 1.24 5.13 19.82 3.96 

Ki]n 2 Scmbber 10212007 1 0:07:22 39.59 103.80 14.98 1.71 5.43 19.63 5.06 

Kiln 2 Scrubber 10212007 10:08:22 40.12 115.80 16.96 1.90 5.07 20.06 5.48 

Kiln 2 Scrubber 10212007 10:09:22 40.49 118.65 18.11 1.91 9.39 20.00 8.88 

Kiln 2 Scrubber 10212007 10:10:22 40.71 125.10 18.22 1.96 9.16 20.00 10.16 

Kiln 2 Scrubber 10212007 10:11:22 40.88 126.65 18.16 2.00 8.66 19.76 10.90 

Kiln 2 Scrubber 10212007 10:12:22 40.95 123.15 18.37 1.91 8.60 20.00 11.20 

Kiln 2 Scrubber 10/21/2007 10:13:22 41.12 123.00 18.38 1.91 9.18 20.00 11.08 

Kiln 2 Scrubber 10/21/2007 10:14:22 41.18 126.00 18.24 1.98 9.23 20.06 10.40 

Kiln 2 Scrubber 1021/2007 10:15:22 41.28 126.05 18.33 1.93 8.88 20.37 9.44 

Kiln 2 Scrubber 10/21/2007 10:16:22 41.41 123.50 18.38 1.90 8.64 20.18 8.96 

Kiln 2 Scmbber 10212007 10:17:22 41.41 123.50 18.35 1.94 9.44 20.30 8.76 

Kilu 2 Scrubber 10212007 10:18:22 41.41 128.00 18.30 1.96 9.01 20.37 8.16 

Kiin 2 Scmbber 10212007 10:19:22 41.63 123.95 18.36 1.93 8.87 20.24 8.16 

Kiln2Scrubber ]0212007 10:20:22 41.49 122.45 18.39 1.89 9.36 20.67 8.40 

Kiln 2 Scrubber 10212007 10:21:22 41.52 122.95 18.45 1.86 9.36 20.37 8.70 

Kiln 2 Scrubber 10212007 10:22:22 41.55 122.95 18.44 1.86 9.42 153.96 8.90 

Kiln 2 Scrubber 10212007 10:23:22 41.49 106.65 19.11 1.46 7181 78.35 8.16 

Kiln 2 Scrubber 10212007 10:24:22 41.68 119.95 19.56 1.26 10.55 141.04 5.86 

Kiln 2 Scrubber 10/21/2007 10:25:22 41.82 114.15 18.98 1.59 8.81 156.71 6.58 

Kiln 2 Scrubber 10212007 10:26:22 41.79 100.60 18.49 1.84 8.60 160.18 7.74 

Kiln 2 Scrubber NOx CCE 10212007 10:27:22 41_93 98.60 18.44 1.86 8.71 162.32 8.82 

Kiln 2 Scrubber NOx CCE 10212007 10:28:22 41_84 98.15 18.45 1.87 9.04 166.46 9.32 

Kiln 2 Scrubber NOx CCE 10/21/2007 10:29:22 41_91 103.15 18.30 1.95 9.24 188.23 10.78 

Kiln 2 Scrubber 10/21/2007 10:30:22 41.91 112.65 18.31 1.94 9.33 193.72 11.20 

Kiln 2 Scrubber 10/21/2007 10:31:22 41.98 120.95 18.17 2.03 9.29 197.56 10.34 

Kiln 2 Scrubber 10/21/2007 10:32:22 41.83 121.00 18.14 2.05 9.26 189.82 10.22 

Kiln 2 Scrubber 10212007 10:33:22 42.00 118.50 18.30 1.95 9.00 187.32 10.48 

Kiln 2 Scrubber 10212007 10:34:22 39.83 119.50 18.31 1.96 9.85 191.22 10.60 

Kiln 2 Scrubber 10212007 10:35:22 13.16 123.45 18.14 2.05 9.58 194.70 10.28 

Kiln 2 Scrubber 10212007 10:36:22 10.75 120.40 18.30 1.95 9.45 187.32 11.26 

Kiln 2 Scrubber 10212007 10:37:22 9.69 121.50 18.37 1.94 9.68 186.46 11.74 

Kiln 2 Scrubber 10212007 10:38:22 9.38 120.00 18.30 1.95 10.13 189.02 12.10 

2 ~'TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln2Scrubber 10/21/2007 10:39:22 8.98 126.50 18.32 1.94 10.13 192.07 12.54 

Kiln 2 Saubber 10/21/2007 10:40:22 8.97 123.50 18.36 1.96 9.53 188.05 13.02 

Kiln 2 Scrubber 10/21/2007 10:41:22 8.97 120.95 18.37 1.92 9.67 185.91 13.46 

Kiln 2 Scrubber 10/21/2007 10:42:22 8.53 121.50 18.44 1.90 10.25 187.50 13.50 

Kiln2Scrubber 10/21/2007 10:43:22 8.55 126.50 18.30 1.97 10.14 194.27 13.26 

Kiln 2 Scmbber 10/21/2007 10:44:22 8.77 122.05 18.31 1.95 9.92 189.15 14.12 

Kiln 2 Scrubber 10/21/2007 10:45:22 8.33 120.05 18.44 1.91 9.91 187.32 14.92 

Kiln2Scrubber 10/21/2007 10:46:22 7.99 124.00 18.39 1.92 10.23 194.51 14.72 

Kiln 2 Scrubber 10121/2007 10:47:22 8.10 126.05 18.34 1.95 9.97 194.76 15.34 

Kiln 2 Scrubber 10/21/2007 10:48:22 8.43 121.55 18.39 1.93 6.83 173.78 16.12 

Kiln 2 Scmbber 10/21/2007 104922 5.29 99.65 19.36 1.37 27.02 106.77 10.96 

Kiln 2 Scrubber 10/21/2007 10:50:22 4.42 119.50 19.42 1.35 9.84 168.84 8.64 

Kiln 2 Scrubber 10/21/2007 10:51:22 8.31 120.00 18.45 1.91 9.35 183.29 11.38 

Kiln 2 Scmbber 10/21/2007 10:52:22 9.52 115.15 18.14 2.06 9.04 185.67 11.14 

Ki1n2Scrubber 10/21/2007 10:53:00 9.92 114.15 18.13 2.07 9.47 185.06 10.96 

Kiln 2 Scrubber c] 10/21/2007 10:54:00 9.51 114.65 18.20 2.03 9.63 182.50 11.44 

KiIn2Scrubber Cl 10/21/2007 10:55:00 9.55 121.50 18.12 2.06 9.54 182.32 11.26 

Kiln 2 Saubber Cl 10/21/2007 10:56:00 9.43 118.45 18.24 1.98 9.50 185.18 11.68 

Kiln 2 Scrubber Cl 10/21/2007 10:57:00 9.27 118.45 18.28 1.98 9.76 188.48 12.28 

Kiln2Scmbber Cl 10/21/2007 10:58:00 9.04 119.50 18.27 1.97 10.16 192.87 12.90 

Kiln 2 Scrubber cl 10/21/2007 10:59:00 8.84 124.00 18.25 2.00 10.22 194.82 13.14 

Kiln2Scrubber Cl 10/21/2007 11:00:00 9.25 120.95 18.23 2.02 10.00 192.50 13.88 

Kiln 2 Scrubber Cl 10/21/2007 11:01:00 8.95 120.00 18.41 1.91 9.76 189.27 14.72 

Kiln2Scrubber cl 10/21/2007 11:02:00 8.38 124.50 18.40 1.93 10.84 195.18 14.78 

KiIn2Scmbber Cl 10/21/2007 11:03:00 8.67 126.00 18.30 1.99 10.34 195.18 15.32 

Kiln2Scrubber Cl 10/21/2007 11:04:00 8.45 122.00 18.43 1.88 10.32 191.34 15.94 

Kiln2Scrubber Cl 10/21/2007 11:05:00 8.10 122.05 18.49 1.86 10.53 190.61 17.04 

Kiln2Scmbber Cl 10/21/2007 11:06:00 8.30 124.45 18.34 1.96 10.97 197.38 17.16 

Kiln 2 Scrubber cl 10/21/2007 11:07:00 8.44 125.55 18.38 1.93 10.15 193.72 17.58 

Kiln 2 Scmbber Cl 10/21/2007 11:08:00 8.10 122.50 18.50 1.85 10.20 192.32 19.04 

Kiln 2 Scrubber cl 10/21/2007 11:09:00 9.57 122.05 18.43 1.91 10.64 192.44 28.88 

Kiln 2 Scrubber Cl 10/21/2007 11:10:00 10.37 124.45 18.37 1.94 10.66 195.98 23.54 

KiIn2Scrubber Cl 10/21/2007 11:11:00 9.56 126.55 18.41 1.92 10.46 196.04 29.42 

Kiln 2 Scrubber cl 10/21/2007 11:12:00 9.54 124.50 18.38 1.94 10.83 196.28 29.92 

Kiln2Saubber Cl 10/21/2007 11:13:00 9.11 125.00 18.44 1.88 10.36 194.88 26.76 

Kiln2Scrubber cl 10/21/2007 11:14:00 8.99 121.00 18.52 1.85 7.83 185.55 26.08 

Kiln 2 Scrubber Cl 10/21/2007 11:15:00 5.74 101.70 1931 1.38 39.60 111.59 17.70 

Kiln 2 Scmbber Cl 10/21/2007 11:16:00 4.11 113.75 19.54 1.28 9.87 141.28 13.52 

Kiln 2 Scrubber cl 10/21/2007 11:17:00 7.51 110.20 18.81 1.71 9.19 157.56 19.76 

Kiln 2 Scmbber Ci 10/21/2007 11:18:00 9.04 99.70 18.45 1.88 8.56 162.93 22.14 

Kiln2Scmbber cl 10/21/2007 11:19:00 9.24 97.20 18.44 1.87 9.09 164.63 22.98 

Kiln 2 Scmbber CI 10I21/2007 11:20:00 8.92 97.20 18.50 1.85 9.81 165.43 23.30 

Kiln 2 Scrubber cl 10121/2007 11:21:00 9.69 101.75 18.31 1.96 9.75 187.44 25.66 

Kiln2Scrubber CI 10/21/2007 11:22:00 9.42 110.20 18.30 1.93 10.39 191.10 24.44 

Kiln 2 Scmbber Cl 10/212007 11:23:00 9.26 119.05 18.18 2.03 10.66 196.40 22.62 

Ki1n2Scrubber cl 10/21/2007 11:24:00 9.12 120.50 18.22 2.00 10.28 195.73 22.02 

Kiln 2 Scmbber Cl 10/21/2007 11:25:00 9.00 122.55 18.26 1.97 10.05 196.59 20.86 

Kiln2Scrubber cl 10/21/2007 11:26:00 9.27 119.55 18.22 1.98 10.27 195.98 21.54 

Kiln2Scrubber Cl 10/21/2007 11:27:00 8.76 117.55 18.39 1.91 10.63 192.99 21.66 

K8n 2 Scmbber Cl 10/21/2007 11:28:00 8.19 123.55 18.40 1.89 10.69 196.89 20.38 

Kiln 2 Scrubber Cl 10/21/2007 11:29:00 8.86 124.50 18.25 1.99 10.46 198.96 19.88 

Kiln 2 Scmbber Ci 10/21/2007 11:30:00 8.47 120.50 18.42 1.88 10.00 192.87 19.94 

Kiln 2 Scrubber cl 10121/2007 11:31:00 7.94 120.50 18.49 1.86 10.50 192.80 19.94 

Kiln 2 Scrubber cl 10/21/2007 11:32:00 8.20 121.05 18.39 1.93 10.86 197.44 20.26 

Kiln 2 Scmbber CI 10/21/2007 11:33:00 8.29 124.50 18.33 1.93 10.51 198.23 19.16 

Kiln2Scrubber cl 10/21/2007 11:34:00 7.84 122.55 18.46 1.86 10.07 194.63 19.52 

Kiln 2 Saubber Cl 10/21/2007 11:35:00 8.19 120.50 18.41 1.91 10.50 195.30 19.22 

Kiln2Scrubber CI 10/21/2007 11:36:00 8.08 119.50 18.45 1.88 10.43 194.21 18.54 

Kiln 2 Scmbber Cl 10/21/2007 11:37:00 7.77 119.55 18.51 1.83 10.23 194.15 17.82 

Kiln2Scrubber cl 10/21/2007 11:38:00 8.20 120.05 18.51 1.83 10.28 193.90 18.18 

Kiln 2 Scrubber Cl 10/21/2007 11:39:00 8.44 120.45 18.45 1.87 10.42 197.01 18.56 

Kiln 2 Scrubber Cl 10/21/2007 11:40:00 8.15 122.00 18.54 1.81 7.64 151.40 17.82 

3 IC)TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scmbber Cl 10/21@007 11:41:00 4.81 102.15 19.45 1.28 17.66 107.20 11.92 

Kiln 2 Scrubber Ci 10/2112007 11:42:00 5.03 122.00 19.29 1.42 9.96 183.35 15.16 

Kiln2Scmbber G 10/21/2007 11:43:00 8.89 119.95 18.30 1.95 9.82 193.48 20.26 

Kiln 2 Scrubber C] 10/21/2007 11:44:00 9.76 115.65 18.03 2.09 9.68 196.28 20.50 

Ki1n2Scrubber Cl 10/21/2007 11:45:00 9.81 116.10 18.05 2.07 9.63 196.95 20.44 

KiIn2Scrnbber Cl 10/21/2007 11:46:00 10.05 118.05 18.07 2.06 9.49 198.05 20.56 

Kiln 2 Scmbber Cl 10/21/2007 11:47:00 9.81 115.65 18.27 1.96 9.39 191.40 21.34 

Kiln 2 Scmbber Cl 10/21/2007 11:48:00 9.65 115.15 18.30 L96 9.75 192.87 21.52 

Kiln 2 Scmbber Cl 10/21/2007 11:49:00 9.68 118.05 18.33 1.93 9.58 194.33 22.08 

Kiln 2 Scrubber Ci 10/21/2007 11:50:00 9.77 120.00 18.30 1.97 9.80 195.24 22.44 

Kiln2Scmbber Cl 10121/2007 11:51:00 9.65 121.55 18.30 1.94 9.12 196.83 22.20 

Kiln 2 Scrubber C] 10121/2007 11:52:00 9.58 121.50 18.33 1.96 9.40 195.79 21.96 

Kiln 2 Scrubber Cl 10/21/2007 11:53:00 9.58 121.00 18.38 1.90 9.25 193.23 22.08 

Average 8.69 118.42 18.42 1.89 10.60 186.95 19.54 

Kiln 2 Scrubber 10/21/2007 11:54:00 9.66 121.00 18.31 1.94 9.42 196.28 21.84 

Kiln 2 Scmbber 10/21/2007 11:55:00 9.26 121.00 18.36 1.93 9.30 195.00 21.72 

Kiln 2 Scrubber 10/21/2007 11:56:00 4.66 77.70 4.05 0.52 -0.93 70.55 157.90 

Kiln 2 Scmbber 10/21/2007 11:57:00 0.63 1.95 0.12 0.20 -0.95 36.16 194.12 

Kiln 2 Scrubber 10/21/2007 11:58:00 0.56 -0.05 -0.02 0.16 -0.96 25.06 49.84 

Kiln 2 Scrubber 10/21/2007 11:59:00 0.74 -0.05 -0.02 0.18 -0.95 21.95 41.94 

KiIn2Scrubber 10/21/2007 11:59:01 0.71 -0.05 -0.03 0.17 -0.95 21.95 41.88 

Kiln 2 Scrubber SSB 10/21/2007 12:00:01 0.60 -0.05 -0.03 0.16 -0.98 20.49 43.01 

Kiln 2 Scrubber 10/21/2007 12:01:01 0.39 -0.05 -0.03 0.17 0.68 93.35 42.60 

Kiln 2 Scrubber 10/21/2007 12:02:01 0.03 -0.05 0.03 0.18 1.21 217.13 43.34 

Kiln 2 Scrubber 10/21/2007 12:03:01 0.23 -0.05 6.86 6.27 -0.99 30.98 26.76 

Kiln 2 Scmbber 10/21/2007 12:04:01 0.20 -0.50 9.53 9.35 -0.98 21.71 12.48 

Kiln 2 Saubber 10/21/2007 12:05:01 0.20 -0.45 9.95 9.94 -1.00 19.51 7.56 

Kiln 2 Sernbber 10/21/2007 12:06:01 0.00 -0.45 10.03 10.07 -0.99 18.11 4.58 

Kiln 2 Scrubber 10/21/2007 12:07:01 0.01 -0.50 10.04 10.08 -1.01 17.56 3.30 

Kiln 2 Scrubber 10/21/2007 12:08:01 -0.04 -0.50 10.05 10.09 -1.01 16.89 2.70 

Kiln 2 Scmbber 10/21/2007 12:0825 0.01 -0.50 10.05 10.10 -1.03 16.77 2.58 

Kiln 2 Scrubber SSB 10/21/2007 12:09:25 -0.01 -0.50 10.04 10.10 -1.02 16.46 2.28 

Kiln 2 Scmbber 10/21/2007 12:10:25 0.07 -0.45 10.05 10.11 -1.04 15.98 2.64 

Kiln 2 Scrubber 10/21/2007 12:11:25 0.18 -0.05 0.34 0.60 -1.03 18.90 198.30 

Kiln 2 Scrubber 10/21/2007 12:12:25 19.08 10.50 -0.03 0.23 31.28 159.02 57.74 

Kiln2Scrubber 10/21/2007 12:13:25 24.45 23.45 -0.04 0.18 25.00 233.90 9.92 

Kiln 2 Sernbber 10/21/2007 12:13:55 24.49 23.45 -0.04 0.17 24.93 238.35 6.04 

Kiln 2 Scrubber SSB 10/21/2007 12:14:55 24.55 23.40 -0.05 0.18 24.63 243.11 3.12 

Kiln 2 Scrubber . 10/21/2007 12:15:55 24.58 23.40 -0.06 0.18 14109 244.33 2.52 

Kiln 2 Scmbber 10/21/2007 12:16:55 121.75 221.60 -0.04 0.19 143.04 261.16 2.40 

Kiln 2 Scrubber SSB 10/21/2007 12:17:40 121.76 246.75 -0.05 0.18 143.02 282.01 2.16 

Kiln 2 Scrnbber 10/21/2007 12:18:40 121.76 249.25 -0.05 0.17 143.01 305.30 1.84 

Kiln 2 Scrubber 10/21/2007 12:19:40 23.88 247.30 -0.04 0.20 26.90 303.05 2.02 

Kiln 2 Scr¢bber 10/21/2007 12:20:40 85.96 197.75 12.08 1.46 7.42 294.94 20.80 

Kiln 2 Scrubber 10/21/2007 12:21:40 24.65 129.60 17.12 1.84 7.46 279.02 24.82 

Kiln 2 Scmbber 10/21/2007 12:22:40 13.77 122.50 18.04 1.90 7.48 268.23 23.18 

Kiln 2 Scrubber 10/21/2007 12:23:40 10.96 123.05 18.19 1.93 7.18 254.21 20.44 

Kiln 2 Scrubber 10/21/2007 12:24:40 10.51 121.60 18.24 1.96 7.15 231.77 18.92 

Kiln 2 Scmbber 10/21/2007 12:25:40 10.11 121.55 18.33 1.90 7.14 198.23 18.06 

Kiln 2 Scrubber 10/21/2007 12:26:40 9.87 121.05 18.32 1.94 7.23 158.90 16.74 

Kiln 2 Scrubber 10/21/2007 12:27:40 9.65 121.00 18.29 1.96 7.08 175.98 16.06 

Kiln 2 Scrubber 10/21/2007 12:28:40 9.57 121.60 18.35 1.90 7.07 180.00 15.58 

Kiln 2 Saubber 10/21/2007 12:29:40 9.41 121.55 18.33 1.95 7.11 180.98 15.28 

Kiln 2 Scmbber 10/21/2007 12:30:40 9.37 120.05 18.31 1.93 6.87 178.78 15.02 

Kiln 2 Scmbber 10/21/2007 12:31:40 8.28 117.60 18.64 1.74 22.30 90.06 14.18 

Kiln 2 Scmbber 10/21/2007 12:32:40 5.13 102.65 19.43 1.31 10.29 112.68 10.34 

Kiln 2 Scrubber 10/21/2007 12:33:40 5.91 119.50 19.21 1.46 6.78 163.41 12.24 

Kiln 2 Scmbber 10/21/2007 12:34:40 9.47 119.00 18.37 1.94 6.64 170.55 14.66 

Kiln 2 Scmbber 10/21/2007 12:35:40 10.65 116.15 18.12 2.06 6.52 173.41 15.04 

Kiln 2 Scmbber 10/21/2007 12:36:40 10.41 114.70 18.20 1.99 6.18 166.28 16.18 

Kiln 2 Scrubber 10/21/2007 12:37:40 10.11 113.75 18.23 1.99 6.44 163.05 17.34 

Kiln 2 Scrubber 10/21/2007 12:38:40 10.33 114.65 18.23 1.99 6.49 166.89 18.68 

4 iC'TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scrubber 10212007 12:39:40 10.36 120.05 18.18 2.01 6.34 167.38 1964. 

Kiln 2 Scrubber 1021/2007 12:40:40 10.44 118.50 18.26 1.98 6.40 160.43 20.86 

Kiln 2 Scrubber 10212007 12:41:40 10.12 118.05 18.36 1.90 6.40 156.16 21.22 

Kiln 2 Scrubber 10/212007 12:42:40 9.91 118.45 18.34 1.94 6.35 157.07 21.40 

Kiln 2 Scrubber 10/21/2007 12:43:40 10.35 119.00 18.26 1.96 6.73 160.73 21.22 

Kiln 2 Scrubber 10/21 /2007 12:44:40 10.07 123.50 18.32 1.93 6.27 162.93 21.16 

Kiln 2 Scrubber 10/21/2007 12:45:40 9.88 121.55 18.34 1.93 6.35 161.40 22.26 

Kiln 2 Scrubber 1021/2007 12:46:40 10.15 118.05 18.33 1.91 6.37 160.98 22.62 

Kiln 2 Scrubber 10212007 12:47:40 9.46 119.05 18.53 1.86 6.08 160.06 22.68 

Kfln 2 Scrubber 10212007 12:48:40 9.46 120.00 18.46 1.86 6.57 162.74 22.26 

Kiln 2 Scnrbber 10212007 12:49:40 9.87 123.50 18.33 1.94 6.07 165.37 20.98 

Kiln 2 Scrubber 10212007 12:50:40 9.66 122.00 18.48 1.83 6.38 160.00 20.50 

Kiln 2 Scrubber 10/21/2007 12:51:40 9.39 120.45 18.47 1.83 5.98 159.21 18.74 

Kiln 2 Scrubber 10/21/2007 12:52:40 9.75 118.50 18.49 1.86 6.04 156.83 17.64 

Kiln 2 Scrubber 10/21/2007 12:53:40 9.46 122.45 18.48 1.85 5.99 158.90 16.48 

Kiln 2 Scrubber 10/21/2007 12:54:40 9.49 124.45 18.42 1.89 5.92 158.48 15.94 

Kiln 2 Scrubber 10212007 12:55:40 9.37 119.45 18.46 1.86 5.78 155.06 15.88 

Kiln 2 Scrubber 1 021/2007 12:56:40 9.23 118.50 18.55 1.80 5.57 153.23 16.00 

Kiln 2 Scrubber 10212007 12:57:40 6.20 107.65 19.13 1.45 23.24 93.66 13.02 

Kiln 2 Scrubber 10/212007 12:58:40 4.17 106.15 19.60 1.21 5.65 102.50 9.02 

Kiln 2 Scrubber 1021/2007 12:59:40 7.17 113.15 18.97 1.60 4.34 122.38 13.94 

Kiln 2 Scrubber 10212007 13:00:40 9.37 99.60 18.42 1.87 4.73 128.05 17.34 

Kiln 2 Scrubber 10212007 13:01:40 10.32 95.65 18.35 1.92 4.75 130.12 17.88 

Kiln 2 Scrubber 10212007 13:02:40 10.04 94.65 18.43 1.84 4.72 130.24 18.24 

Kiln 2 Scmbber 10/21/2007 13:03:40 10.95 97.15 18.26 1.96 4.92 146.34 20.62 

Kiln 2 Scrubber 10/21/2007 13:04:40 10.56 106.65 18.25 1.96 5.02 150.00 20.50 

Kiln 2 Scrubber 10212007 13:05:02 10.51 109.70 18.27 1.94 5.00 149.76 20.32 

Kiln 2 Sombber C2 10212007 13:06:02 10.62 110.65 18.22 1.97 5.17 151.34 19.76 

Kiln 2 Scrubber C2 10212007 13:07:02 10.43 113.20 18.24 1.98 5.39 15184 19.70 

Kiln 2 Scrubber C2 10/21/2007 13:08:02 10.43 119.00 18.21 1.99 5.30 156.40 19.70 

Kiln 2 Scrubber C2 10212007 13:09:02 10.38 115.65 18.18 2.00 5.09 155.00 20.70 

Kiln 2 Scmbber C2 10212007 13:10:02 10.15 113.70 18.27 1.95 5.25 153.41 20.74 

Kiln 2 Scrubber C2 10212007 13:11:02 9.55 114.70 18.39 1.88 5.12 152.20 21.04 

Kiln 2 Scrubber C2 10212007 13:12:02 9.75 115.70 18.25 1.97 5.45 157.50 21.72 

Kiln 2 Scrubber C2 10212007 13:13:02 9.70 119.05 18.26 1.96 5.67 159.15 21.28 

Kiln 2 Scrubber C2 10212007 13:14:02 9.13 115.70 18.45 1.88 5.41 156.95 21.40 

Kilu 2 Scmbber C2 10212007 13:15:02 9.26 115.75 18.36 1.90 5.60 157.44 22.20 

Kiln 2 Scrubber C2 10212007 13:16:02 9.33 115.75 18.38 1.90 5.60 156.10 22.44 

Kilu 2 Scrubber C2 10121/2007 13:17:02 8.76 116.20 18.48 1.87 5.89 154.15 22.32 

Kiln 2 Scmbber C2 10212007 13:18:02 9.36 118.55 18.38 1.92 6.07 157.20 21.40 

Kiln 2 Scmbber C2 10/212007 13:19:02 9.04 119.55 18.38 1.91 5.89 158.29 21.60 

Kiln 2 Scmbber C2 10212007 13:20:02 9.72 119.55 18.38 1.93 5.79 157.38 22.76 

Kiln 2 Scmbber C2 10/212007 13:21:02 8.94 115.75 18.56 1.81 5.78 148.78 22.50 

Kiln 2 Scrubber C2 10212007 13:22:02 9.50 116.70 18.38 1.88 5.62 154.57 21.10 

K0n 2 Scrubber C2 10/21/2007 13:23:02 8.15 114.20 18.71 1.69 12.22 117.44 18.98 

Kiln 2 Scrubber C2 10/212007 13:24:02 4.52 103.70 19.52 1.24 9.90 89.21 12.12 

Kiln 2 Scmbber C2 10212007 13:25:02 6.22 120.50 19.15 1.49 5.81 138.54 19.10 

Kiln 2 Scrubber C2 10/212007 13:26:02 9.76 114.75 18.21 2.00 5.65 151.83 21.60 

Kiln 2 Scrubber C2 10212007 13:27:02 11.00 109.80 18.05 2.10 5.50 152.26 22.26 

Kiln 2 Saubber C2 10/212007 13:28:02 10.77 109.30 18.15 2.03 5.32 150.61 22.68 

Kiln 2 Scmbber C2 10212007 13:29:02 10.51 110.25 18.19 2.00 5.43 149.57 22.80 

Kiln 2 Scrubber C2 10/212007 13:30:02 10.40 111.25 18.21 2.01 5.52 149.15 24.20 

Kiln 2 Scmbber C2 10212007 13:31:02 10.62 112.80 18.21 2.01 5.67 151.04 24.76 

Kiln 2 Serubber C2 10212007 13:32:02 10.25 112.70 18.27 1.99 6.38 152.13 25.12 

Kiln 2 Scrubber C2 10212007 13:33:02 10.38 113.25 18.33 1.95 6.04 151.95 26.20 

Kiln 2 Scmbber C2 10212007 13:34:02 10.24 113.25 18.23 2.03 6.02 153.78 27.00 

Kiln 2 Scrubber C2 10/2112007 13:35:02 10.50 113.25 18.29 1.99 5.29 152.50 27.18 

Kiln 2 Scrubber C2 10212007 13:36:02 9.93 114.75 18.40 1.92 5.84 150.85 27.36 

Kilu 2 Scrubber C2 10212007 13:37:02 10.33 114.70 18.32 1.97 6.08 154.15 27.66 

Kiln 2 Scmbber C2 10212007 13:38:02 9.93 115.20 18.40 1.93 6.32 153.78 28.58 

Kiln 2 Sctubber C2 10/21/2007 13:39:02 9.69 115.70 18.45 1.89 6.16 153.48 28.34 

Kiln 2 Scrubber C2 102112007 13:40:02 9.49 115.70 18.39 1.94 6.11 154.76 28.02 

5 C;TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scrubber C2 1021/2007 13:41:02 

Kiln 2 Scrubber C2 102112007 13:42:02 

Kiln 2 Scmbber C2 10/212007 13:43:02 

Kiln 2 Scmbber C2 10/212007 13:44:02 

Kiln 2 Scrubber C2 10212007 13:45:02 

Kiln 2 Scrubber C2 1021/2007 13:46:02 

Kiln 2 Scrubber C2 10212007 13:47:02 

Kiln 2 Scrubber C2 10212007 13:48:02 

Kiln 2 Scmbber C2 10/212007 13:49:02 

Kiln 2 Scrubber C2 1021/2007 13:50:02 

Kiln 2 Scrubber C2 10212007 13:51:02 

Kiln 2 Scrubber C2 10212007 13:52:02 

Kiln 2 Scrubber C2 10/212007 13:53:02 

Kiln 2 Scmbber C2 10212007 13:54:02 

Kiln 2 Scrubber C2 10212007 13:55:02 

Kiln 2 Scrubber C2 10212007 13:56:02 

Kiln2Scrubber C2 ]021/2007 13:57:02 

Kiln 2 Scrubber C2 10/212007 13:58:02 

Kiln 2 Scrubber C2 10/212007 13:59:02 

Kiln 2 Scrubber C2 1021/2007 14:00:02 

Kiln 2 Scrubber C2 ] 0212007 14:01:02 

Kiln 2 Scrubber C2 10212007 14:02:02 

Kiln 2 Scmbber C2 10212007 14:03:02 

Kiln 2 Scrubber C2 10212007 14:04:02 

Kiln 2 Scrubber C2 10/212007 14:05:02 

Average 

Kiln 2 Scrubber 10212007 14:06:02 

Kiln 2 Scrubber 10/212007 14:07:02 

Kiln 2 Scrubber 10212007 14:08:02 

Kiln 2 Scmbber 10212007 14:09:02 

Kiln 2 Scmbber 10212007 14:10:02 

Kiln 2 Scrubber 10/21/2007 14:11:02 

Kiln 2 Scrubber 10212007 14:12:02 

Kiln 2 Scmbber SSB 10/21/2007 14:12:18 

Kiln 2 Scmbber 10212007 14:13:18 

Kiln 2 Scrubber ] 0212007 14:14:18 

Kiln 2 Scrubber 10212007 14:15:18 

Kiln 2 Scrubber 10212007 14:16:18 

Kiln 2 Scrubber 10212007 14:17:18 

Kiln 2 Scmbber 10212007 14:17:23 

Kiln 2 Scmbber SSB 10212007 14:18:23 

Kiln 2 Scrubber 10212007 14:19:23 

Kiln 2 Scrubber 10212007 14:20:23 

Kiln 2 Scrubber 10212007 14:21:04 

Kiln 2 Scrubber SSB 1021/2007 14:22:04 

Kiln 2 Scrubber 10212007 14:23:04 

Kiln 2 Scrubber 10212007 14:24:04 

Kiln 2 Scrubber 10212007 14:25:04 

Kiln 2 Scrubber 10212007 14:26:04 

Kiln 2 Scrubber SSB 10212007 14:26:08 

Kiln 2 Scrubber 10212007 14:27:08 

Kiln 2 Scmbber 10212007 14:28:08 

Kiln 2 Scrubber 10212007 14:29:08 

Kiln 2 Scmbber 10212007 14:30:08 

Kiln 2 Scrubber ] 0212007 14:31:08 

Kiln 2 Scrubber 10212007 14:32:08 

Kiln 2 Scrubber 10212007 14:33:08 

Kiln 2 Scrubber 10212007 14:34:08 

Kiln 2 Scrubber 10212007 14:35:08 

Kiln 2 Scmbber 10212007 14:36:08 

Kiln 2 Scrubber 10212007 14:37:08 

Kilu2Scrubber 1021/2007 14:38:08 

10.11 114.70 18.38 1.94 6.49 154.21 28.20 

9.33 117.55 18.49 1.86 6.28 152.87 26.28 

9.98 115.70 18.45 1.90 6.21 152.44 27.30 

9.53 115.70 18.47 1.88 6.87 152.50 25.90 

10.09 116.70 18.41 1.91 6.69 153.60 25.00 

9.22 116.70 18.50 1.88 6.61 153.23 23.24 

10.13 115.75 18.40 1.91 6.82 154.15 23.30 

9.99 115.75 18.47 1.86 6.78 153.35 21.96 

7.77 100.10 18.99 1.55 31.42 101.83 17.40 

4.57 102.65 19.56 1.20 7.29 102.38 11.14 

6.97 108.15 19.04 1.57 6.48 125.18 14.60 

9.66 97.15 18.45 1.87 6.30 131.95 16.66 

10.83 94.05 18.37 1.93 6.26 133.17 17.46 

10.34 94.00 18.43 1.86 5.72 132.38 18.26 

10.94 98.55 18.18 2.04 6.73 151.65 21.40 

10.80 106.60 18.22 1.99 6.89 154.09 20.26 

10.51 114.60 18.12 2.07 6.31 160.24 18.12 

10.43 114.60 18.15 2.04 6.10 158.90 17.58 

10.25 114.20 18.26 1.98 7.02 156.83 17.70 

10.27 114.15 18.31 1.95 6.71 155.98 17.04 

9.70 115.25 18.33 1.96 7.04 155.61 16.74 

9.72 116.25 18.37 1.92 6.90 155.18 16.48 

9.75 118.65 18.26 1.99 7.30 160.24 16.42 

9.87 119.65 18.25 2.00 6.71 158.90 16.54 

9.46 116.80 18.37 1.90 6.55 156.95 15.82 

9.62 113.07 18.41 1.90 6.66 149.08 21.45 

9.91 116.25 18.38 1.91 6.41 156.71 15.76 

1.29 115.30 18.33 1.91 2.36 157.07 16.36 

121.77 128.15 7.25 0.78 143.10 149.76 8.72 

121.78 242.75 0.25 0.19 143.06 131.59 2.28 

121.78 248.40 0.02 0.14 143.04 207.74 1.12 

121.78 248.45 0.00 0.17 143.03 228.23 0.62 

121.78 249.50 -0.01 0.16 143.03 234.27 0.44 

121.78 248.50 -0.01 0.14 143.03 236.83 0.38 

121.79 247.50 -0.02 0.16 143.03 234.27 0.26 

98.04 166.20 6.02 6.71 -0.37 94.15 0.38 

10.07 16.05 9.63 9.83 -0.67 31.22 0.32 

1.51 1.60 9.98 10.18 -0.80 23.60 0.32 

0.36 0.00 10.02 10.16 -0.86 20.85 0.32 

0.34 -0.45 10.02 10.18 -0.85 20.73 0.32 

0.23 -0.45 10.02 10.16 -0.92 19.15 0.32 

0.29 -0.45 10.03 10.13 17.29 18.23 0.26 

23.76 21.50 0.31 0.49 16.98 17.38 -0.02 

24.54 23.45 -0.01 0.21 24.73 16.71 -0.02 

24.60 23.50 -0.03 0.15 24.25 16.04 -0.08 

7.86 12.00 -0.04 0.17 -1.42 17.26 128.68 

0.32 0.45 -0.04 0.17 0.40 25.12 198.92 

0.38 0.00 -0.05 0.14 -0.07 37.50 60.04 

0.19 0.00 -0.05 0.16 -0.04 50.06 43.96 

0.21 0.00 -0.05 0.13 -0.07 50.85 43.70 

037 -0.05 -0.05 0.15 -0.09 58.96 41.28 

0.23 -0.05 -0.06 0.16 1.21 64.88 41.28 

-0.07 0.00 -0.04 0.18 1.93 71.46 41.94 

-0.23 0.00 -0.03 0.23 1.88 80.12 41.94 

-0.17 0.00 -0.02 0.25 1.95 96.16 41.94 

-0.18 0.00 -0.01 0.31 1.99 115.79 41.94 

-0.21 0.00 0.01 0.38 1.99 121.59 41.94 

-0.13 0.00 0.04 0.46 2.01 126.22 41.94 

-0.30 0.00 0.07 0.56 2.03 129.15 41.94 

-0.25 0.00 0.10 0.61 2.17 125.37 41.88 

-0.28 0.00 0.13 0.65 2.13 118.84 41.94 

-0.36 0.00 0.15 0.68 2.18 106.52 41.88 

6 ~'TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scrubber 10212007 14:39:08 -0.12 0.00 0.18 0.70 2.12 97.01 41.88 

Kiln 2 Scrubber 10212007 14:40:08 -0.04 0.00 0.20 0.73 2.17 87.32 41.88 

Kiln 2 Scrubber 10/212007 14:41:08 -0.13 0.00 0.23 0.76 2.21 81.77 41.88 

Kiln 2 Scrubber 10212007 14:42:08 -0.21 0.00 0.26 0.79 2.27 75.98 41.82 

Kiln 2 Scmbber 10212007 14:43:08 -0.24 0.00 0.29 0.82 2.28 71.22 41.82 

Kilu 2 Scrubber 10/212007 14:44:08 -0.21 0.00 0.33 0.83 2.06 66.83 41.88 

Kiln 2 Scrubber 10212007 14:45:08 -0.25 0.00 0.35 0.83 2.13 63.41 41.82 

Kilu 2 Scrubber 10212007 14:46:08 -0.27 0.05 0.36 0.86 2.14 60.24 41.76 

Kiln 2 Scrubber 10212007 14:47:08 -0.28 0.05 0.38 0.83 2.04 57.80 41.76 

Kiln 2 Scrubber 10212007 14:48:08 -0.26 0.05 0.38 0.83 2.08 50.37 41.76 

Kiln 2 Scrubber 10212007 14:49:08 -0.16 0.05 0.33 0.70 2.11 47.01 41.76 

Kiln 2 Scrubber 10212007 14:50:08 -0.24 0.05 0.26 0.37 2.04 54.88 41.76 

Kiln 2 Scrubber 10212007 14:51:08 -0.27 0.05 0.23 0.31 1.96 53.72 41.76 

Kiln 2 Scrubber 10/21/2007 14:52:08 -0.29 0.10 0.20 0.27 2.01 43.90 41.76 

Kiln 2 Scmbber 10/21/2007 14:53:08 -0.20 0.10 0.18 0.26 1.94 43.48 41.70 

Kiln 2 Scrubber 10/21/2007 14:54:08 -0.27 0.05 0.18 0.27 2.04 39.57 41.64 

Kiln 2 Scrubber 10212007 14:55:08 -0.06 0.10 0.20 0.26 2.02 35.55 41.58 

Kiln 2 Scmbber 10212007 14:56:08 -0.01 0.10 0.21 0.26 2.06 32.80 41.52 

Kiln 2 Scrubber 10212007 14:57:08 0.10 0.10 0.22 0.25 2.13 30.85 41.52 

Kiln 2 Scmbber 10212007 14:58:08 -0.12 0.05 0.23 0.26 2.11 30.24 41.40 

Kiln 2 Scrubber 10212007 14:59:08 -0.18 0.05 0.23 0.25 2.10 30.55 41.34 

Kiln 2 Scmbber 10212007 15:00:08 -0.01 0.05 0.22 0.26 2.13 30.00 41.28 

Kiln 2 Scrubber 1021/2007 15:01:08 0.03 0.05 0.21 0.25 2.06 29.33 41.22 

Kiln 2 Scrubber 10212007 15:02:08 -0.14 0.00 0.21 0.25 2.09 28.23 41.10 

Kiln 2 Scrubber 10/21/2007 15:03:08 0.00 0.00 0.20 0.26 2.04 26.95 41.04 

Kiln 2 Scrubber 10/212007 15:04:08 -0.12 0.05 0.19 0.24 2.09 26.10 40.92 

Kiln 2 Scrubber 10/21/2007 15:05:08 -0.11 0.00 0.19 0.25 2.10 24.82 40.72 

Kiln 2 Scrubber 10/21/2007 15:06:08 0.21 0.05 0.19 0.24 2.25 24.27 40.48 

Kiln 2 Scmbber 1 0212007 15:07:08 -0.32 0.05 0.23 0.22 2.18 23.60 40.12 

Kiln 2 Scrubber 10212007 15:08:08 -0.13 0.05 0.36 0.22 2.25 22.80 39.76 

Kiln 2 Scmbber 10212007 15:09:08 -0.03 0.00 0.75 0.21 2.32 22.20 39.40 

Kiln 2 Scrubber 10/212007 15:10:08 0.07 0.05 1.62 0.22 2.37 21.71 38.96 

Kiln 2 Scrubber 10212007 15:11:08 -0.11 0.05 3.10 0.21 2.35 21.52 38.54 

Kiln 2 Scrubber 10212007 15:12:08 -0.01 0.05 5.15 0.20 2.46 20.91 38.12 

Kiln 2 Scmbber 10212007 15:13:08 -0.03 0.05 7.53 0.19 2.45 20.67 37.70 

Kiln 2 Scmbber 10212007 15:14:08 0.20 0.05 9.93 0.20 2.42 20.30 37.20 

Kiln 2 Scrubber 10/21/2007 15:15:08 -0.14 0.05 12.12 0.19 2.50 20.06 36.78 

Kiln 2 Scrubber 10212007 15:16:08 -0.04 0.05 13.95 0.21 2.55 19.63 36.42 

Kiln 2 Scrubber 10/21/2007 15:17:08 -0.05 0.00 15.42 0.18 2.64 19.27 35.98 

Kiln 2 Scmbber 10212007 15:18:08 0.04 0.05 16.54 0.21 2.63 19.09 35.50 

Kiln 2 Scrubber 10/21/2007 15:19:08 0.10 0.00 17.40 0.19 2.58 18.84 35.08 

Kiln 2 Scrubber 1021/2007 15:20:08 0.17 0.00 18.04 010 2.55 18.54 34.66 

Kiln 2 Scrubber 10/21/2007 15:21:08 -0.14 0.00 18.51 0.19 2.49 18.05 34.28 

Kiln 2 Scrubber 1021/2007 15:22:08 0.10 0.00 18.87 0.18 2.45 18.05 33.92 

Kiln 2 Scmbber 10212007 15:23:08 -0.1 1 0.00 19.14 0.18 2.45 17.87 33.56 

Kiln 2 Scrubber 1021/2007 15:24:08 0.73 0.05 19.20 0.19 2.66 17.62 33.26 

Kiln2Scmbber 1021/2007 15:25:08 -0.01 0.50 0.83 0.34 2.50 50.30 36.54 

Kiln 2 Scrubber 10/21/2007 15:26:08 0.01 0.05 0.85 0.35 2.35 44.88 36.24 

Kiln 2 Scrubber 10212007 15:27:08 -0.03 0.50 0.87 0.33 2.40 40.12 36.12 

Kiln 2 Scrubber ]0212007 15:28:08 -0.13 0.00 0.90 0.35 2.45 37.38 36.04 

Kiln 2 Scrubber 10212007 15:29:08 -0.17 0.00 0.94 0.33 2.37 36.83 35.98 

Kiln 2 Scmbber 10212007 15:30:08 -0.23 0.00 1.05 0.34 2.32 37.01 35.92 

Kiln 2 Scrubber 10212007 15:31:08 -0.25 0.05 1.11 0.37 2.26 37.44 35.86 

Kiln 2 Scrubber 10212007 15:32:08 -0.18 0.00 1.25 0.33 17.62 37.68 35.80 

Kiln 2 Scrubber 10212007 15:33:08 -0.17 -0.10 1.40 0.35 15.34 37.93 35.74 

Kiln 2 Scmbber 10212007 15:34:08 -0.12 -0.05 1.56 0.36 14.66 38.17 35.70 

Kiln 2 Scrubber 1021/2007 15:35:08 -1.95 -0.05 1.72 0.35 14.10 38.11 35.56 

Kiln 2 Scrubber 10212007 15:36:08 -0.06 -0.10 1.86 0.36 12.60 62.07 35.56 

Kiln 2 Scrubber 10212007 15:37:08 1.06 0.40 0.87 0.41 10.54 152.56 29.68 

Kiln 2 Scrubber 10212007 15:38:08 9.44 72.65 15.26 1.62 10.44 176.59 26.46 

Kiln 2 Scrubber 10212007 15:39:08 10.31 104.65 17.50 1.84 10.40 185.73 26.40 

Kiln 2 Scrubber 10/212007 15:40:08 10.47 114.20 18.02 1.90 10.40 189.39 26.40 

7 

~`TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scrubber 10/21/2007 15:41:08 10.39 117.55 18.09 1.94 10.15 188.66 26.34 

Kiln 2 Scrubber 10/21/2007 15:42:08 10.62 118.55 18.17 1.89 9.93 185.37 26.46 

Kilu 2 Scmbber 10/21/2007 15:43:08 10.25 119.55 18.21 1.91 10.21 182.62 26.52 

Kiln 2 Scrubber 10/21/2007 15:44:08 10.45 120.10 18.17 1.94 10.06 182.38 26.34 

Kiln2Scrubber 10/21/2007 15:45:08 10.56 120.05 18.20 1.90 10.11 181.34 25.72 

Kiln 2 Scrubber 10/21/2007 15:46:08 10.34 118.50 18.29 1.87 10.00 179.39 24.20 

Kiln 2 Scrubber 10/21/2007 15:47:08 10.29 115.20 18.34 1.83 10.11 179.88 23.30 

Kiln 2 Scmbber 10/21/2007 15:48:08 10.26 119.55 18.27 1.87 10.06 180.06 24.44 

Kilu 2 Scrubber 10/21/2007 15:49:08 10.05 121.00 18.29 1.87 9.86 180.49 25.90 

Kiln 2 Scrubber 10/21/2007 15:50:08 9.94 121.05 18.23 1.89 9.75 181.65 26.22 

Kiln 2 Scrubber 10/21/2007 15:51:08 9.82 118.55 18.27 1.89 9.35 177.44 26.88 

Kiln 2 Scmbber 10/21/2007 15:52:08 9.55 115.75 18.35 1.83 9.59 175.98 27.60 

Kiln 2 Scrubber 10/21/2007 15:53:08 9.72 117.60 18.30 1.85 9.45 176.28 27.12 

Kiln 2 Scrubber 10/21/2007 15:54:08 9.59 118.10 18.33 1.84 9.66 175.98 25.24 

Kiln 2 Scrubber 10/2112007 15:55:08 9.12 118.50 18.41 1.79 9.41 173.41 24.14 

Kiln 2 Scrubber 10/21/2007 15:56:08 9.33 118.55 18.37 1.84 9.45 172.80 24.32 

Kiln 2 Scrubber 10/21/2007 15:57:08 8.95 118.05 18.50 1.74 6.97 143.72 23.30 

Kiln 2 Scmbber 1 0/21/2007 15:58:08 4.88 97.70 19.45 1.18 20.07 96.95 12.60 

Kiln 2 Scrubber 10/21/2007 15:59:08 4.76 119.05 19.27 1.33 9.44 14154 19.10 

Kiln 2 Scmbber 10/21/2007 16:00:08 9.34 117.55 18.21 1.91 8.98 161.28 23.42 

Kiln 2 Scrubber 10/21/2007 16:01:08 10.54 113.20 17.92 2.08 9.07 166.52 23.18 

Kdn 2 Scrubber C3 10/21/2007 16:02:00 10.83 114.70 17.99 2.03 8.55 167.07 23.00 

Kiln 2 Scrubber C3 10/21/2007 16:03:00 10.61 111.75 18.14 1.96 8.41 163.29 23.84 

Kiln 2 Scrubber C3 10/21/2007 16:04:00 10.39 111.70 18.19 1.93 8.77 165.18 23.90 

Kiln2Scmbber C3 10/21/2007 16:05:00 10.52 118.10 18.12 1.96 8.80 170.18 23.60 

Kiln 2 Scmbber C3 10/21/2007 16:06:00 10.91 118.55 18.12 1.96 8.35 169.70 23.42 

Kiln 2 Scrubber C3 10/21/2007 16:07:00 10.74 116.70 18.28 1.88 8.44 165.43 25.18 

Kiln 2 Scmbber C3 10/21/2007 16:08:00 10.39 116.15 18.24 1.90 9.00 168.78 24.94 

Kiln 2 Scrubber C3 10/21/2007 16:09:00 10.45 120.05 18.14 1.95 9.03 170.61 23.78 

Kiln 2 Scrubber C3 10/21/2007 16:10:00 10.10 120.05 18.30 1.88 8.36 166.46 24.38 

Kiln 2 Scrubber C3 10/21/2007 16:11:00 9.85 116.70 18.31 1.88 8.71 164.88 23.30 

Kiln 2 Scrubber C3 10/21/2007 16:12:00 10.79 116.70 18.26 1.92 9.21 166.89 22.08 

Kiln 2 Scrubber C3 10/21/2007 16:13:00 10.34 120.50 18.28 1.90 8.83 167.93 21.66 

Kiln 2 Scrubber C3 10/21/2007 16:14:00 10.30 118.55 18.31 1.87 8.84 164.45 22.88 

Kiln 2 Scmbber C3 10/21/2007 16:15:00 10.54 117.55 18.30 1.87 9.15 165.12 23.30 

Kiln 2 Scmbber C3 10/21/2007 16:16:00 9.96 121.00 18.32 1.89 9.21 166.95 22.88 

Kiln 2 Scmbber C3 10/21/2007 16:17:00 10.10 120.50 18.32 1.88 8.87 165.73 23.30 

Kiln 2 Scrubber C3 10/21/2007 16:18:00 10.03 117.55 18.39 1.82 9.31 163.23 23.84 

Kiln 2 Scrubber C3 10/21/2007 16:19:00 10.07 118.50 18.37 1.85 9.82 165.18 24.22 

Kiln 2 Scrubber C3 10/21/2007 16:20:00 9.73 121.60 18.36 1.87 9.43 167.07 23.66 

Kiln 2 Scrubber C3 10/21/2007 16:21:00 9.88 120.50 18.36 1.86 9.38 164.51 24.26 

Kiln 2 Scrubber C3 10/21/2007 16:22:00 9.92 117.55 18.44 1.80 9.54 161.71 24.44 

Kiln 2 Scrubber C3 10121/2007 16:23:00 9.21 118.55 18.56 1.72 11.90 131.28 23.96 

Kiln 2 Scrubber C3 10/21/2007 16:24:00 5.50 102.70 19.30 1.30 17.82 95.98 15.16 

Kiln2Scmbber C3 10/21/2007 16:25:00 4.90 114.70 19.34 1.31 9.59 124.21 17.28 

Kilu 2 Scrubber C3 10/21/2007 16:26:00 7.99 105.25 18.67 1.71 9.21 135.73 22.56 

Kikt 2 Scrubber C3 10/21/2007 16:27:00 9.57 96.65 18.39 1.86 8.92 142.26 23.84 

Kiln 2 Scmbber C3 10/21/2007 16:28:00 9.99 95.20 18.37 1.85 8.89 143.48 24.70 

Kiln 2 Scrubber C3 10/21@007 16:29:00 10.09 95.15 18.38 1.85 8.63 154.94 25.12 

Kiln 2 Scrubber C3 10/21/2007 16:30:00 10.72 99.15 18.25 1.89 8.75 158.48 27.60 

Kiln 2 Scrubber C3 10/21/2007 16:31:00 10.24 108.15 18.28 1.89 8.75 161.83 25.72 

Kiln 2 Scrubber C3 10/21/2007 16:32:00 10.47 112.70 18.22 1.94 8.78 162.56 24.94 

Kiln 2 Scrubber C3 10/21/2007 16:33:00 11.13 112.20 18.26 1.93 8.97 161.10 24.02 

Kiln 2 Scrubber C3 10121/2007 16:34:00 11.39 116.20 18.21 1.94 9.32 164.33 23.78 

Kiln 2 Scrubber C3 10/21/2007 16:35:00 10.84 119.10 18.16 1.99 8.83 165.79 23.96 

Kiln 2 Scrubber C3 10/21/2007 16:36:00 11.77 115.25 18.25 1.92 8.80 161.40 24.52 

Kiln 2 Scmbber C3 10/21/2007 16:37:00 10.55 115.70 18.34 1.89 8.97 160.49 24.82 

Kilu2Scrubber C3 10/21/2007 16:38:00 10.16 119.05 18.23 1.97 9.24 167.07 23.66 

Kiln 2 Scrubber C3 10/21/2007 16:39:00 11.06 118.10 18.20 1.94 9.02 164.82 2184 

Kiln 2 Scmbber C3 10/21/2007 16:40:00 10.28 116.70 18.36 1.86 9.48 162.07 23.72 

Kiln 2 Scrubber C3 10/21/2007 16:41:00 10.22 116.15 18.35 1.89 9.62 162.56 24.44 

Kiln 2 Scrubber C3 10/21/2007 16:42:00 10.18 115.75 18.33 1.88 9.51 160.67 24.44 

8 C,TRC 
Data Acquisition Records 

154785 Hanson Brick 

Kiln 2 Scmbber C3 10/21/2007 16:43:00 

Kiln 2 Scmbber C3 10/21/2007 16:44:00 

Kiln 2 Scrubber C3 10/21/2007 16:45:00 

Kiln 2 Scrubber C3 10/21/2007 16:46:00 

KBn 2 Scrubber C3 10/21/2007 16:47:00 

Kiln 2 Scrubber C3 10/21/2007 16:48:00 

Kiln 2 Scrubber C3 10/21/2007 16:49:00 

Kiln 2 Scrubber C3 10/21/2007 16:50:00 

Kiln 2 Scrubber C3 10/21/1007 16:51:00 

Kiln 2 Scrubber C3 10/21/2007 16:52:00 

Kiln 2 Scmbber C3 10/21/2007 16:53:00 

Kiln 2 Scrubber C3 10/21/2007 16:54:00 

Kiln 2 Scrubber C3 10/21/2007 16:55:00 

Kiln 2 Scrubber C3 10/21 /2007 16:56:00 

Kiln 2 Scrubber C3 10/21/2007 16:57:00 

Kiln 2 Scrubber C3 10/21/2007 16:58:00 

Kiln 2 Scrubber C3 10/21/2007 16:59:00 

Kiln 2 Scrubber C3 10/21/2007 17:00:00 

Kiln 2 Serubber C3 10/21/2007 17:01:00 

Kiln 2 Scrubber C3 10/21/2007 17:02:00 

Average 

Kiln 2 Scrubber 10/21/2007 17:03:00 

Kiln 2 Scrubber 10/21/2007 17:04:00 

Kiln 2 Scrubber 10/21/2007 17:05:00 

Kiln 2 Scrubber 10/21/2007 17:06:00 

Kiln 2 Scrubber SSB 10/21/2007 17:06:31 

Kiln2Scrubber 10/21/2007 17:07:31 

Kiln 2 Scmbber 10/21/2007 17:08:31 

Kiln 2 Scrubber 10/21/2007 17:09:24 

Kiln 2 Scrubber SSB 10/21/2007 17:10:24 

Kiln 2 Scrubber 10/21/2007 17:11:24 

Kiln 2 Scrubber 10/21/2007 17:12:24 

Kiln 2 Scrubber SSB 10/21/2007 17:12:28 

Kiln 2 Scrubber 10/21/2007 17:13:28 

Kiln 2 Scrubber 10/2112007 17:14:28 

Kiln 2 Scrubber 10/21/2007 17:15:28 

Kiln 2 Scrubber 10/21/2007 17:16:28 

Kiln 2 Scrubber 10/21/2007 17:16:44 

Kiln 2 Scrubber SSB 10/21/2007 17:17:44 

Kiln 2 Scrubber 10/21/2007 17:18:44 

Kiln 2 Scrubber 10/21/2007 17:19:44 

Kilu 2 Scrubber 10/21/2007 17:20:44 

Kiln 2 Scrubber 10/21/2007 17:21:44 

Kiln2Scrubber 10/21/2007 17:22:44 

Kiln 2 Scrubber 10/21/2007 17:23:44 

Kiln 2 Scrubber 10/21/2007 17:24:44 

Kiln 2 Scrubber 10/21l2007 17:25:44 

9.72 117.60 18.42 1.83 9.34 160.55 24.08 

9.81 120.10 18.35 1.88 9.57 164.94 23.30 

10.06 121.60 18.33 1.90 9.32 163.78 23.36 

9.44 119.10 18.54 1.78 9.13 159.51 23.90 

9.30 119.10 18.57 1.77 9.26 157.68 24.52 

9.57 119.60 18.59 1.73 9.22 155.43 25.00 

7.71 112.20 19.00 1.49 35.23 110.49 22.14 

4.58 103.75 19.59 1.18 10.39 102.20 15.04 

6.34 119.55 19.14 1.46 8.47 140.91 23.96 

10.09 114.70 18.41 1.84 8.21 150.85 25.48 

11.58 113.70 18.26 1.94 7.92 152.99 25.00 

11.09 114.70 18.29 1.90 7.94 152.93 24.44 

11.51 116.15 18.33 1.91 8.13 153.84 24.08 

11.80 116.15 18.26 1.92 8.34 153.78 24.20 

11.89 117.55 18.37 1.87 8.33 15156 24.26 

10.81 119.05 18.40 1.86 8.58 154.21 23.72 

11.08 118.05 18.36 1.89 8.85 154.63 24.02 

10.58 123.00 18.36 1.90 8.82 158.11 24.02 

10.47 122.50 18.36 1.89 8.75 156.28 25.18 

11.15 119.55 18.34 1.91 8.49 155.30 25.60 

10.02 115.33 18.40 1.84 9.56 156.43 23.66 

6.71 120.05 18.43 1.84 3.48 153.41 26.10 

121.79 165.05 5.31 0.55 -0.82 179.51 9.14 

121.80 243.25 0.35 0.23 -0.96 224.51 2.52 

121.80 247.90 0.04 0.18 -1.01 237.20 1.06 

121.80 247.85 0.02 0.17 -1.04 242.74 0.68 

121.80 248.85 0.00 0.18 -0.18 238.60 0.32 

60.33 98.15 -0.01 0.18 -0.18 124.21 20.98 

3.78 2.90 -0.02 0.17 -0.21 43.96 32.58 

0.78 -0.10 -0.03 0.18 -0.21 28.05 43.16 

18.25 16.45 -0.03 0.20 -0.21 22.80 12.66 

24.43 23.40 -0.03 0.18 25.22 20.67 2.82 

24.78 23.40 -0.03 0.19 24.64 20.37 2.56 

24.61 23.45 -0.04 0.17 24.15 18.84 1.00 

12.40 15.50 5.52 6.10 0.73 17.68 0.94 

1.75 1.50 9.38 9.38 0.72 16.83 0.88 

0.10 -0.05 9.92 9.93 0.72 16.04 0.76 

0.11 -0.50 9.96 9.97 0.71 15.91 0.68 

0.04 -0.45 10.01 10.04 0.71 15.37 0.50 

0.07 -0.50 10.01 10.03 0.72 14.63 0.38 

0.01 -0.40 10.03 10.06 0.71 14.39 0.32 

-0.03 -0.50 10.03 10.04 0.74 15.85 0.20 

0.09 -0.50 9.99 9.96 2.20 19.21 0.38 

-0.28 -0.50 10.00 9.89 2.09 20.91 0.44 

-0.13 -0.50 9.99 9.92 2.17 21.40 0.38 

-0.19 -0.50 10.00 9.90 2.11 22.50 0.44 

-0.25 -0.50 10.01 9.85 2.03 23.23 0.46 

9 C--.TRC 
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Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 11:16:09 

Description: Kiln 2 Scrubber 

Data file: 102107_18.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.983 14.5534 67.3666 

Ethane 1.031 3.4276 15.8659 

Propane 1.185 0.4842 2.2413 

18.4651 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 11:34:45 

Description: Kiln 2 Scrubber 

Data file: 102107_20.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785f 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.984 13.2982 64.3967 

Ethane 1.032 3.4019 16.4738 

Propane 1.185 0.5480 2.6537 

17.2481 100.0000 
Lab name: TRC 

Client: Hanson Brick 

ClientlD: 154785 

Analysis date: 10/21/2007 11:49:07 CI-~ ~ 

Description: Kiln 2 Scrubber 

Data file: 102107_24.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

cz- 

;' 

Component Retention Area Area % 

Methane 0.975 11.0813 55.8525 

Ethane 1.025 3.9014 19.6640 

Propane 1.174 0.5718 2.8823 

15.5546 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 11:54:52 

Description: Kiln 2 Scrubber 

Data file: 102107_25.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785t 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.974 10.4674 47.5192 

Ethane 1.023 3.7628 17.0821 

Propane 1.175 0.6272 2.8473 

14.8574 100.0000 

` \ 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10121/2007 13:05:26 

Description: Kiln 2 Scrubber 

Data file: 102107_26.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.970 8.1921 47.3857 / -A 

Methane 1.001 0.4076 2.3577 

Ethane 1.018 3.0056 17.3851 

Propane 1.171 0.5132 2.9682 

i f'~i fi f:1.Yi NI~xrPUIrI 

ku.,,\ a 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 13:25:44 

Description: Kiln 2 Scrubber 

Data file: 102107_28.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.965 12.6903 69.1766 

Ethane 1.013 3.0400 16.5717 

Propane 1.159 0.6043 3.2941 

16.3347 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10121/2007 13:47:57 

Description: Kiln 2 Scrubber 

Data file: 102107_30.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.964 8.7411 68.2726 

Ethane 1.013 2.2174 17.3191 

Propane 1.160 0.5222 4.0783 

Propane 1.223 1.1092 8.6636 

12.5899 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 13:59:35 

Description: Kiln 2 Scrubber 

Data file: 102107_31.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

:` 

Component Retention Area Area % 

Methane 0.960 13.0506 62.9219 

Methane 1.008 3.1638 15.2539 

Propane 1.158 0.6168 2.9736 

Propane 1.217 1.3539 6.5277 

18.1850 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 14:06:31 

Description: Kiln 2 Scrubber 

Data file: 102107_32.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.963 10.3433 62.7841 

Ethane 1.012 2.3570 14.3068 

Propane 1.162 0.6515 3.9545 

Propane 1.225 1.2414 7.5351 

JF 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 16:10:32 

Description: Kiln 2 Scrubber 

Data file: 102107_34.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.958 12.6175 70.8261 

Ethane 1.005 3.1244 17.5384 tey' 

Propane 1.145 0.4723 2.6515 

Propane 1.199 1.0860 6.0958 

1.377 0.5145 2.8882 

17.8148 100.0000 

ew~43 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/2112007 16:17:50 

Description: Kiln 2 Scrubber 

Data file: 102107_35.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

;' 

Component Retention Area Area % 

Methane 0.957 13.0801 73.3341 

Methane 1.006 3.0219 16.9427 

Propane 1.145 0.5492 3.0788 

Propane 1.202 1.1851 6.6444 

17.8363 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10/21/2007 16:26:06 

Description: Kiln 2 Scrubber 

Data file: 102107_36.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\154785f 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

;' 

Component Retention Area Area % 

Methane 0.957 12.0719 69.0776 

Methane 1.005 2.9749 17.0230 

Propane 1.146 0.4503 2.5767 

Propane 1.200 1.1891 6.8044 

16.6862 100.0000 
Lab name: TRC 

Client: Hanson Brick 

Client ID: 154785 

Analysis date: 10121/2007 16:44:18 

Description: Kiln 2 Scrubber 

Data file: 102107_38.CHR (C:\Documents and Settings\Data Logger\My Documents\PeakSimpleData\1547851 

Comments: Location: Elgin, Texas 

Source: Lime Kiln Scrubber 

Technicians: JSG 

Component Retention Area Area % 

Methane 0.955 13.3000 68.6607 

Ethane 1.005 3.1692 16.3612 

Propane 1.145 0.5718 2.9522 

Propane 1.198 1.4388 7.4278 

18.4799 100.0000 
Method 26A Data 

Fluoride Data 

Company Name Hanson Bnck Source Kiln #2 Scrubber 

Facillty Elgin, Tems Job No. 154785 

Sampling Date 10/2112007 

Technicians JSG 

Calibra0on Curves Va US EPA Method 26 Sec[ion 5.2 

Inidal Curve 

Scale=0 - 100 IC Calibration Curve: Fluoritle 

Date Time I Area 1 Anz 2 Precision % Mean Area Calc /mL 

10121/2007 08:31 1.0057 1.0524 2.27 1 6 

10/21/2007 0902 2.1385 2.1254 0.31 2 T 12 

10/21/2007 09:36 4.3161 4.3194 0.04 4 25 

10/21/2007 10:08 8.7842 8.8773 0.53 9 51 

10/21/2007 11:44 17.3019 17.4534 0.44 17 100 

Line Correlation: 0.99993913 

120 

100 y=5.726E+00x+1.702EE 80 a 

3 60 

o 40 

U 

20 

0 

0 2 4 6 8 1➢ 12 14 16 t8 20 

Area (comka) 

ExoerimnMalOafae Flnnrida 

Date Time RUN Area1 1 Area2 1 Pmcision % MeanArea I Conc Imh 

10/21/2007 12:13 Blank 0.0082 0.0076 3.75 0.0079 0.05 N/A 

10/21/2007 12:46 C-i lnlet 8.3601 8.2488 0.67 83045 4763 1 

10/21/2007 15:29 C-2lnlet 10.8779 10.7806 0.45 10.8293 62.12 1 

10/22/2007 15:04 C-3lnlet 8.3396 8.4931 0.91 8.4164 48.27 

I Diluti70.18 2 

10/21/2007 13:15 C-1 Outlet 0.0545 0.0502 4.10 0.0524 0.26 1 

10/21/2007 15:59 C-20u8et 0.0265 0.0278 2.39 0.0272 0.11 1 

10/21/2007 17:48 C-30u0et 0.0386 0.0402 2.03 0.0394 0.18 1 

C' TRC 
Method 26A Data 

Chloride Data 

Company Name Hanson Brick Source Kiln #2 Scrubber 

Facility Elgin, Texas Job No. 154785 

Sampling Date 10/21/2007 

Technicians JSG 

Calibration Curves Via US EPA Method 26 Seetion 5.2 

Initial Curve 

Scale=0 - 100 IC Calibration Curve: Chloritle 

Date Time Area 1 Area 2 Precision (%I Mean Area I Conc /mL Calc /mL 

10121/2007 0831 1.6369 1.6718 1.05 2 6.25 6 

10121/2007 0902 2.7004 2.6914 0.17 3 12.5 14 

10/21/2007 09:36 4.176 4.1714 0.06 4 25 24 

10/2112007 10:08 7.6027 7.465 0.91 8 50 49 

10/21/2007 11:44 14.6233 14.8332 0.71 15 100 101 

Line Correlation: 0.999653387 

120 

100 y= 7.216E+00x - 5.681 E+ 

E 80 

= 60 

o` 40 

~ 

20 

0 

0 2 4 6 8 10 12 14 16 

Area (counts) 

Exnerimental Data: Chloritle 

Date Time RUN Area 1 1 Area 2 Precision % Mean Area Conc /ml Dilution Conc /ml 

10121/2007 12:13 Blank 0.0410 0.0451 4.75 0.0431 0.29 N/A 0.29 

10/21/2007 12:46 C-1lnlet 4.3533 4.2994 0.62 4.3264 28.42 1 28.42 

10/21/2007 15:29 C-2lnlet 7.0171 6.8640 1.10 6.9406 45.77 1 45.77 

10/22/2007 15:04 C-3lnlet 9.9334 10.4694 2.63 10.2014 67.40 2 134.81 

10/21/2007 13:15 C-1 Outlet 0.1367 0.1489 4.27 0.1428 0.66 1 0.66 

10121/2007 15:59 C-20utlet 0.0935 0.0973 1.99 0.0954 0.35 1 0.35 

10/21/2007 17:48 C-30utlet 0.2941 0.2927 0.24 0.2934 1.66 1 1.66 

TRC 
lon Chromatograph Analysis 

Sample Name: Blank Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/2112007 12:13 Location: Elgin, Texas 

100 153826Hanson #38 modified by TRC-Cubix Em lo ee ECD 1 

NS 3-40.9 1297 

88 

7 

63 

5 

38 

25 

13 

1 - Floride - 2 1 aloride - 4.587 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S'min 

Rel.Area 

% 

1 3.17 Floride 0.045 0.0082 0.01 

2 4.59 Chloride 0.181 0.0410 0.07 

3 10.94 n.a. 65.186 3.8633 6.51 

4 11.30 n.a. 135.297 55.4690 93.41 

Total: 200.708 59.3816 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: Blank Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121/2007 12:28 Location: Elgin, Texas 

153826Hanson #39 modified by TRC-Cubix Em lo ee ECD 1 

100 

uS 4-90.8 0163 

8 

75 

63 

5 

38 

25 

13 

1- Floride - loride - 4.507 3- 9,44 

min 

-1 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.15 Floride 0.035 0.0076 0.01 

2 4.51 Chloride 0.189 0.0451 0.07 

3 9.44 n.a. 0.000 0.0002 0.00 

4 10.80 n.a. 65.436 4.0984 6.81 

5 11.16 n.a. 135.579 56.0613 93.11 

Total: 201.239 60.2127 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-1 Inlet Client Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 12:46 Location: Elgin, Texas 

153826Hanson #40 C-1 Inlet ECD 1 

100 

uS 6-710. 010 

88 

7 

6 

5 

38 

2 1 - Floride - 3.027 

13 2 - Chloride - 4.243 

5 10.173 3-5.457 4-7.097 

_1 min ' 

0.0 2.0 4.0 610 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

IJS 

Area 

S*min 

Rel.Area 

% 

1 3.03 Floride 23.923 8.3601 12.85 

2 4.24 Chloride 10.720 4.3533 6.69 

3 5.46 n.a. 0.584 0.6674 1.03 

4 7.10 n.a. 0.023 0.0063 0.01 

5 10.17 n.a. 1.089 0.2549 0.39 

6 10.79 n.a. 60.445 4.3087 6.62 

7 11.11 n.a. 122.333 47.1091 72.41 

Total: F 219.118 65.0598 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-1 Inlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recordfng Time: 1012112007 13:00 Location: Elgin, Texas 

153826Hanson #41 C-1 Inlet ECD 1 100 

N S 6 -710. 070 

88 

7 

63 

5 

3 

25 1 - Floride - 2.990 

13 2 - Chloride - 4.210 

5 10.133 3-5.407 4-7.043 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 2.99 Floride 24.464 8.2488 13.05 

2 4.21 Chloride 10.529 4.2994 6.80 

3 5.41 n.a. 0.543 0.6252 0.99 

4 7.04 n.a. 0.022 0.0061 0.01 

5 10.13 n.a. 1.042 0.2459 0.39 

6 10.76 n.a. 57.467 4.2381 6.71 

7 11.07 n.a. 119.568 45.5378 72.05 

Total: 1 213.636 63.2014 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-1 Outlet CIlent: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 13:15 Location: Elgin, Texas 

53826Hanson #42 modifed by TRC-Cubix Em lo ee ECD 1 100 

N S 461018 0 

8 

7 

63 

5 

38 

25 

13 

1- Floride -J. 0,Qh1onde - 4.503 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S'min 

Rel.Area 

% 

1 3.05 Floride 0.138 0.0545 0.01 

2 4.50 Chloride 0.300 0.1367 0.03 

3 9.08 n.a. 0.000 0.0000 0.00 

4 10.80 n.a. 510.245 76.2795 18.59 

5 11.04 n.a. 509.664 333.8208 81.36 

Total: F 1020.346 410.2915 100.00 

Testing Performed by TRC 
Ion Chromatograph Analysis 

Sample Name: C-1 Outlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121/2007 13:32 Location: Elgin, Texas 

153826Hanson #43 modified by TRC-Cubix Em lo ee ECD 1 

6N Ns 

4101$.`,i3$7 

50 

40 

30 ,1 

20 

10 

1 - Flodd - 2.0Q~loride - 4.460 

min 

10 

0.0 2.0 4.0 6.0 8.0 1 0.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.04 Floride 0.118 0.0502 0.01 

2 4.46 Chloride 0.342 0.1489 0.04 

3 10.85 n.a. 510.003 375.7880 91.50 

4 11.09 n.a. 99.866 34.7141 8.45 

Total: 610.328 410.7012 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: DiH2O Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121t2007 13:53 Location: Elgin, Texas 

153826Hanson #44 modifed by TRC-Cubix Em lo ee ECD 1 

0.6 NS 

1 - 11.380 

0.5 

0.4 

0.3 

0.2 

0.1 

0.0 

-0.1 

-0.2 

-0.3 

min 

-0.4 

0.0 2.0 4.0 6.0 8.0 1 0.0 12.0 14. 0 ~~. No. Ret.Time Peak Name Height 

min IJS 

Area 

S*min 

Rel.Area 

% 

1 11.38 n.a. 0.551 0.2869 100.00 

Total: 0.551 0.2869 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: DIH2O Client' Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 14:08 Location: Elgin, Texas 

153826Hanson ri45 modified by TRC-Cubix Em lo eel ECD 1 0.300 NS 

0.20 1 - 11.370 

0.10 

0.00 —" 

-0.10 

-0.20 

-0.30 

min -0.40 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height 

min PS 

Area 

S'min 

Re1.Area 

% 

1 11.37 n.a. 0.185 0.0975 100.00 

Total: 0.185 0.0975 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-2 Inlet Client: HansonBrick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 15:29 Location: Elgin, Texas 

153826Hanson i146 modified by TRC-Cubix Em lo ee ECD 1 ~ 100 

N S 4-10.7 0 ' 

88 

7 

63 

5 

38 

1 - Floride - 2.913 

2 

2 - Chloride - 4.337 

1 

3 - 5.330 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 1 4.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Re1.Area 

% 

1 2.91 Floride 30.714 10.8779 2.40 

2 4.34 Chloride 16.418 7.0171 1.55 

3 5.33 n.a. 0.796 0.7559 0.17 

4 10.76 n.a. 509.594 434.5007 95.88 

Total: 557.522 453.1516 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-2 Inlet Client Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012112007 15:44 Location: Elgin, Texas 

153826Hanson#47 C-2lnlet ECD 1 10 

N S 6 - 10 950 

88 

7 

6 

5 

38 

1 - Floride - 2.937 

2 

2 - Chlodde -4.327 

1 

3 - 5. 9f- .137 6.850 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 2.94 Floride 31.328 10.7806 2.35 

2 4.33 Chloride 17.019 6.8640 1.50 

3 5.30 n.a. 0.607 0.5151 0.11 

4 6.14 n.a. 0.022 0.0047 0.00 

5 6.85 n.a. 0.019 0.0050 0.00 

6 10.95 n.a. 509.507 440.2927 96.04 

Total: 558.503 458.4622 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-2 Outlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 15:59 Location: Elgin, Texas 

100 53826Hanson #48 modified by TRC-Cubix Em lo ee ECD 1 

NS 5 - 10 927 

88 

7 

63 

5 

38 

25 

il 

13 

1- Florid -:0bloride - 4.3 7 3- 6.817 4 9. ------- ___.___ 

1 min 

0.0 2.0 410 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S'min % 

1 3.00 Floride 0.074 0.0265 0.01 

2 4.34 Chloride 0.314 0.0935 0.02 

3 6.82 n.a. 0.229 0.0510 0.01 

4 9.24 n.a. 0.000 0.0005 0.00 

5 10.93 n.a. 509.474 422.0610 99.96 

Total: 510.091 422.2325 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-2 Outlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10121t2007 16:13 Location: Elgin, Texas 

53826Hanson #49 modified by TRC-Cubix Em lo ee ECD 1 100 

N S 3 - 10 887 

88 

75 

63 

I 

i 

5 

ii 

38 

25 

13 

1 - Florid - bloride - 4.333 

_ 1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S'min % 

1 2.98 Floride 0.064 0.0278 0.01 

2 4.33 Chloride 0.324 0.0973 0.02 

3 10.89 n.a. 509.459 419.5222 99.97 

Total: 509.847 419.6473 100.00 

Testing PerPormed by TRC 
lon Chromatograph Analysis 

Sample Name: C-3 Outlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 17:48 Location: Elgin, Texas 

153826Hanson #52 rmodified by TRC-Cubix Em lo ee ECD 1 10 

PS 3 - 10 837 

88 

7 

63 

5 

38 

25 

13 

1- Flor de - B~Ehloride - 4.280 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name 

min 

Height 

PS 

Area 

S`min 

Re1.Area 

% 

1 2.86 Floride 0.108 0.0386 0.01 

2 4.28 Chloride 0.646 0.2941 0.07 

3 10.84 n.a. 484.550 427.3754 99.92 

Total: 485.304 427.7082 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-3 Outlet Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10/21/2007 18:03 Location: Elgin, Texas 

53826Hanson #53 modifed by TRC-Cubix Em lo ee ECD 1 100 

N S 4 - 10. 27 

88 

75 

63 

5 

38 

25 

13 

1- Flo id~ ~pfslrtide - 4.31,7 3- 6.873 

._.__._.—~.. _ .......—.........— 

1 min 

0. 0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time 

min 

Peak Name Height 

PS 

Area 

S*min 

Rel.Area 

% 

1 3.26 Floride 0.037 0.0165 0.00 

2 4.32 Chloride 0.617 0.2927 0.07 

3 6.87 n.a. 0.202 0.0451 0.01 

4 10.83 n.a. 486.395 425.7016 99.92 

Total: 487.252 426.0558 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-3 Inlet 2:1 Client: HansonBrick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 1012212007 15:04 Location: Elgin, Texas 

100 1538261-lanson #55 C-3 Inlet 2:1 ECD 1 

NS 6 -71U 000 

8 

7 

6 

5 

38 

2 - Chloride - 4.450 '. 

1 - Floride - .960 

2 

13 

3 - 5.4 04 -i 307.023 ' --. 

1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S`min % 

1 2.96 Floride 28.056 8.3396 1.87 

2 4.45 Chloride 31.846 9.9334 2.23 

3 5.48 n.a. 0.445 0.3807 0.09 

4 6.51 n.a. 0.026 0.0069 0.00 

5 7.02 n.a. 0.134 0.1278 0.03 

6 10.72 n.a. 510.495 83.5606 18.74 

7 11.00 n.a. 509.976 343.4542 77.04 

Tota1: 1080.979 445.8033 100.00 

Testing Performed by TRC 
lon Chromatograph Analysis 

Sample Name: C-3 Inlet 2:1 Client: Hanson8rick 

Control Program: Hanson Source: Multiple 

Quantif. Method: Hanson Project #: 154785 

Recording Time: 10122/2007 15:19 Location: Elgin, Texas 

100 153826Hanson #56 C-3 Inlet 2:1 ECD 1 

us 5 -610. 087 

88 

i 

7 

i 

63 

5 

38 

2 - Chloride - 4.423 

1 - Floride - .947 

2 

13 

3-6. 9b-7.270 

-1 min 

0.0 2.0 4.0 6.0 8.0 10.0 12.0 14.0 

No. Ret.Time Peak Name Height Area Rel.Area 

min PS S'min % 

1 2.95 Floride 27.863 8.4931 1.87 

2 4.42 Chloride 32.056 10.4694 2.31 

3 6.39 n.a. 0.222 0.2361 0.05 

4 7.27 n.a. 0.017 0.0046 0.00 

5 10.68 n.a. 510.501 79.9926 17.65 

6 10.99 n.a. 509.786 353.9736 78.11 

Total: 1080.444 453.1694 100.00 

Testing PerFormed by TRC 
APPENDIX F: 

PROCESS DATA 
Process Data 

DateTime Kiln Comb Air Kiln_Gas_ Kiln_OverPre Kiln_Press Kiln_Push_Car Kiln_Pusher Kiln_Pushing Brick 

Press Top ~ Press ssure_Fan_Sp s_per_Day Pushes_Today Production 

eed_Out (tons/lu') 

10/21/20077:00 11.74 42 2600 -0.17 28 19 0 10.56 

10/21/2007 7:01 12.05 42 2600 -0.17 28 19 0 10.56 

10/21/2007 7:02 12.02 42 2600 -0.18 28 19 0 10.56 

10/21/2007 7:03 11.99 42 2600 -0.16 28 19 0 10.56 

10/21/2007 7:04 11.93 42 2600 -0.17 28 19 0 10.56 

10/21/2007 7:05 11.82 42 2600 -0.13 28 19 0 10.56 

10/21/2007 7:06 11.88 42 2600 -0.15 28 19 0 10.56 

10/21/20077:07 11.87 42 2600 -0.19 28 19 0 10.56 

10/21/20077:08 11.79 42 2600 -0.15 28 19 0 10.56 

10/21/2007 7:09 11.61 42 2600 -0.18 28 19 0 10.56 

10/21/2007 7:10 30.83 42 1200 -0.06 28 19 1 10.56 

10/21/20077:11 29.36 42 1200 -0.07 28 20 0 10.56 

10/21/2007 7:12 11.21 42 2600 -0.14 28 20 0 10.56 

10/21/2007 7:13 11.85 42 2600 -0.17 28 20 0 10.56 

10/21/2007 7:14 11.67 42 2600 -0.18 28 20 0 10.56 

10/21/2007 7:15 11.8 42 2600 -0.16 28 20 0 10.56 

10/21/2007 7:16 11.73 42 2600 -0.17 28 20 0 10.56 

10/21/2007 7:17 11.72 42 2600 -0.17 28 20 0 10.56 

10/21/2007 7:18 13.65 42 2600 -0.2 28 20 0 10.56 

10/21/20077:19 13.31 42 2600 -0.13 28 20 0 10.56 

10/21/20077:20 12.54 42 2600 -0.17 28 20 0 10.56 

10/21/20077:21 12.29 42 2600 -0.18 28 20 0 10.56 

10/21/2007 7:22 12.09 42 2600 -0.16 28 20 0 10.56 

10/21/20077:23 12.12 42 2600 -0.16 28 20 0 10.56 

10/21/20077:24 12.08 42 2600 -0.16 28 20 0 10.56 

10/21/2007 7:25 12.11 42 2600 -0.17 28 20 0 10.56 

10/21/2007 7:26 12.22 42 2600 -0.15 28 20 0 10.56 

10/21/2007 7:27 12.16 42 2600 -0.19 28 20 0 10.56 

10/21/2007 7:28 12.35 42 2600 -0.18 28 20 0 10.56 

10/21/2007 7:29 12.44 42 2600 -0.16 28 20 0 10.56 

10/21/2007 7:30 12.45 42 2600 -0.17 28 20 0 10.56 

10/21/20077:31 12.41 42 2600 -0.16 28 20 0 10.56 

10/21/2007 7:32 12.58 42 2600 -0.18 28 20 0 10.56 

10/21/2007 7:33 12.38 42 2600 -0.17 28 20 0 10.56 

10/21/2007 7:34 12.67 42 2600 -0.16 28 20 0 10.56 

10/21/2007 7:35 14.43 42 2600 -0.17 28 ' 20 0 10.56 

10/21/2007 7:36 30.68 42 1200 -0.09 28 20 1 10.56 

10/21/2007 7:37 13.39 42 2600 -0.13 28 21 0 10.56 

10/21/20077:38 11.42 42 2600 -0.09 28 21 0 10.56 

10/21/2007 7:39 12.23 42 2600 -0.1 28 21 0 10.56 

10/21/2007 7:40 12.11 42 2600 -0.03 28 21 0 10.56 

10/21/2007 7:41 13.42 42 2600 -0.06 28 21 0 10.56 

10/21/2007 7:42 13.3 42 2600 -0.19 28 21 0 10.56 

10/21/20077:43 13.11 42 2600 -0.16 28 21 0 10.56 

10/21/2007 7:44 1142 42 2600 -0.18 28 21 0 10.56 

10/21/2007 7:45 13.42 42 2600 -0.16 28 21 0 10.56 

10/21/2007 7:46 13.14 42 2600 -0.15 28 21 0 10.56 

10/21/20077:47 13.39 42 2600 -0.15 28 21 0 10.56 

10/21/2007 7:48 14.83 42 2600 -0.15 28 21 0 10.56 

10/21/2007 7:49 13.39 42 2600 -0.14 28 21 0 10.56 

10/21/2007 7:50 13.67 42 2600 -0.12 28 21 0 10.56 

10/2112007 7:51 13.86 42 2600 -0.14 28 21 0 10.56 

10/21/2007 7:52 13.37 42 2600 -0.11 28 21 0 10.56 

10/21/2007 7:53 13.8 42 2600 -0.18 28 21 0 10.56 

10/21/2007 7:54 13.75 42 2600 -0.12 28 21 0 10.56 

10/21/2007 7:55 13.66 42 2600 -0.15 28 21 0 10.56 

10/21/2007 7:56 13.41 42 2600 -0.17 28 21 0 10.56 

10/21/2007 7:57 14.8 42 2600 -0.13 28 21 0 10.56 

1 
Process Data 

10/21/2007 7:58 13.85 42 2600 -0.16 28 21 0 10.56 

30/21/2007 7:59 13.55 42 2600 -0.14 28 21 0 10.56 

10/21/2007 8:00 13.96 42 2600 -0.11 28 21 0 10.56 

10/21/2007 8:01 14.1 42 2600 -0.13 28 21 0 10.56 

10/21/2007 8:02 30.45 42 1200 -0.06 28 21 1 10.56 

10/21/20078:03 11.34 42 2600 -0.17 28 22 0 10.56 

10/21/2007 8:04 11.86 42 2600 -0.15 28 22 0 10.56 

10/21/2007 8:05 12.31 42 2600 -0.05 28 22 0 10.56 

10/21/2007 8:06 14.01 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:07 13.73 42 2600 -0.15 28 22 0 10.56 

30/21/20078:08 14.22 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:09 14.27 42 2600 -0.12 28 22 0 10.56 

10/21/2007 8:10 14.53 42 2600 -0.12 28 22 0 10.56 

10/21/2007 8:11 14.81 42 2600 -0.12 28 22 0 10.56 

10/21/2007 8:12 14.37 42 2600 -0.15 28 22 0 10.56 

10/21/2007 8:13 14.74 42 2600 -0.14 28 22 0 10.56 

10/21/2007 8:14 14.43 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:15 13.57 42 2600 -0.11 28 22 0 10.56 

10/21/20078:16 14.39 42 2600 -0.15 28 22 0 10.56 

10/21/2007 8:17 14.84 42 2600 -0.13 28 22 0 10.56 

10/21/20078:18 13.42 42 2600 -0.12 28 22 0 10.56 

10/21/2007 8:19 14.47 42 2600 -0.09 28 22 0 10.56 

10/21/2007 8:20 14.04 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:21 14.14 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:22 14.08 42 2600 -0.1 28 22 0 10.56 

10/21/2007 8:23 14.19 42 2600 -0.12 28 22 0 10.56 

10/21/2007 8:24 14.04 42 2600 -0.08 28 22 0 10.56 

10/21/2007 8:25 13.84 42 2600 -0.13 28 22 0 10.56 

10/21/2007 8:26 13.73 42 2600 -0.09 28 22 0 10.56 

10/21/2007 8:27 29.38 42 1200 0.04 28 22 0 10.56 

10/21/2007 8:28 29.72 42 1200 -0.06 28 23 0 10.56 

10/21/2007 8:29 11.89 42 2600 0.03 28 23 0 10.56 

10/21/2007 8:30 12.77 42 2600 -0.03 28 23 0 10.56 

10/21/2007 8:31 11.94 42 2600 0 28 23 0 10.56 

10/21/2007 8:32 13.42 42 2600 -0.01 28 23 0 10.56 

10/21/2007 8:33 12.04 42 2600 -0.13 28 23 0 10.56 

10/21/2007 8:34 15.73 42 2600 -0.15 28 23 0 10.56 

10/21/2007 8:35 13.96 42 2600 -0.11 28 23 0 10.56 

10/21/2007 8:36 13.09 42 2600 -0.06 28 23 0 10.56 

10/21/2007 8:37 15.67 42 2600 -0.13 28 23 0 10.56 

10/21/2007 8:38 14.05 42 2600 -0.12 28 23 0 10.56 

10/21/2007 8:39 14.44 42 2600 -0.03 28 23 0 10.56 

10121/2007 8:40 14.77 42 2600 -0.05 28 23 0 10.56 

10/21/2007 8:41 13.57 42 2600 -0.08 28 23 0 10.56 

10/21/2007 8:42 15.38 42 2600 -0.06 28 23 0 10.56 

10/21/2007 8:43 14.32 42 2600 -0.13 28 23 0 30.56 

10/21/2007 8:44 13.56 42 2600 -0.11 28 23 0 10.56 

10/21/2007 8:45 15.01 42 2600 -0.09 28 23 0 10.56 

10/21/2007 8:46 15.52 42 2600 -0.16 28 23 0 10.56 

10/21/20078:47 15.38 42 2600 -0.13 28 23 0 10.56 

10/21/2007 8:48 14.79 42 2600 -0.05 28 23 0 10.56 

10/21/20078:49 15.47 42 2600 -0.07 28 23 0 10.56 

10/21/2007 8:50 14.56 42 2600 -0.08 28 23 0 10.56 

10/21/2007 8:51 15.14 42 2600 -0.14 28 23 0 10.56 

10/21/2007 8:52 15.86 42 2600 -0.14 28 23 0 10.56 

10/21/2007 8:53 30.32 42 1200 0.08 28 23 1 10.56 

10/21/20078:54 29.58 42 1200 -0.01 28 24 0 10.56 

10121/2007 8:55 11.67 42 2600 -0.07 28 24 0 10.56 

10/21/2007 8:56 12.41 42 2600 -0.08 28 24 0 10.56 

10/21/2007 8:57 12.66 42 2600 -0.07 28 24 0 10.56 

10/21/2007 8:58 12.53 42 2600 -0.04 28 24 0 10.56 

2 
Process Data 

10/21/20078:59 15.35 42 2600 -0.1 28 24 0 10.56 

10/21/2007 9:00 13.79 42 2600 -0.04 28 24 0 10.56 

10/21/2007 9:01 14.63 42 2600 -0.09 28 24 0 10.56 

10/21/2007 9:02 15.46 42 2600 -0.04 28 24 0 10.56 

10/21/2007 9:03 13.71 42 2600 -0.01 28 24 0 10.56 

10/21/2007 9:04 15.3 42 2600 -0.1 28 24 0 10.56 

10/21/20079:05 15.38 42 2600 -0.05 28 24 0 10.56 

10/21/2007 9:06 13.87 42 2600 -0.03 28 24 0 10.56 

10/21/2007 9:07 15.51 42 2600 0.03 28 24 0 10.56 

10/21/2007 9:08 15.56 42 2600 0.01 28 24 0 10.56 

10/21/20079:09 13.86 42 2600 -0.04 28 24 0 10.56 

10/21/2007 9:10 15.64 42 2600 0.03 28 24 0 10.56 

10/21/2007 9:11 15.62 42 2600 0.08 28 24 0 10.56 

10/21/20079:12 14.26 42 2600 0 28 24 0 10.56 

10/21/20079:13 15.67 42 2600 -0.03 28 24 0 10.56 

10/21/20079:14 15.64 42 2600 -0.04 28 24 0 10.56 

10/21/2007 9:15 14.37 42 2600 0 28 24 0 10.56 

10/21/20079:16 15.68 42 2600 -0.03 28 24 0 10.56 

10/21/20079:17 15.7 42 2600 0 28 24 0 10.56 

10/21/20079:18 15.66 42 2600 -0.03 28 24 0 10.56 

10/21/20079:19 30.1 42 1200 0.1 28 24 1 10.56 

10/21/20079:20 11.47 42 2600 0.06 28 25 0 10.56 

10/21/20079:21 11.77 42 2600 0.11 28 25 0 10.56 

10/21/2007 9:22 12.83 42 2600 0.07 28 25 0 10.56 

10/21/2007 9:23 - 12.83 42 2600 0.08 28 25 0 10.56 

10/21/2007 9:24 12.7 42 2600 0.05 28 25 0 10.56 

10/21/2007 9:25 15.06 42 2600 -0.02 28 25 0 10.56 

10/21/2007 9:26 14.27 42 2600 -0.03 28 25 0 10.56 

10/21/2007 9:27 14.13 42 2600 -0.03 28 25 0 10.56 

10/21/2007 9:28 15.79 42 2600 -0.06 28 25 0 10.56 

10/21/2007 9:29 15.77 42 2600 -0.02 28 25 0 10.56 

10/21/2007 9:30 14.12 42 2600 0 28 25 0 10.56 

10/21/20079:31 15.72 42 2600 -0.02 28 25 0 10.56 

10/21/20079:32 15.75 42 2600 0.08 28 25 0 10.56 

10/21/2007 9:33 14.1 42 2600 0 28 25 0 10.56 

10/21/2007 9:34 15.77 42 2600 -0.03 28 25 0 10.56 

10/21/2007 9:35 15.68 42 2600 -0.12 28 25 0 10.56 

10/21/2007 9:36 14.07 42 2600 -0.09 28 25 0 10.56 

10/21/2007 9:37 15.74 42 2600 -0.1 28 25 0 10.56 

10/21/20079:38 15.72 42 2600 -0.01 28 25 0 10.56 

10/21/2007 9:39 13.99 42 2600 -0.09 28 25 0 10.56 

10/21/20079:40 15.66 42 2600 -0.11 28 25 0 10.56 

10/21/2007 9:41 15.69 42 2600 -0.09 28 25 0 10.56 

10/21/20079:42 15.77 42 2600 -0.09 28 25 0 10.56 

10/21/20079:43 14.11 42 2600 -0.09 28 25 0 10.56 

10121/20079:44 15.67 42 2600 -0.14 28 25 0 10.56 

10/21/20079:45 29.94 42 1200 -0.04 28 26 0 10.56 

10/21/2007 9:46 11.65 42 2600 -0.16 28 26 0 10.56 

10/21/20079:47 11.8 42 2600 -0.14 28 26 0 10.56 

10/21/20079:48 12.85 42 2600 -0.14 28 26 0 10.56 

10/21/20079:49 14.12 42 2600 -0.13 28 26 0 10.56 

10/21/2007 9:50 12.75 42 2600 -0.14 28 26 0 10.56 

10/21/2007 9:51 13.18 42 2600 -0.14 28 26 0 10.56 

10/21/20079:52 14.05 42 2600 -0.08 28 26 0 10.56 

10/21/2007 9:53 14.55 42 2600 -0.15 28 26 0 10.56 

10/21/2007 9:54 15.9 42 2600 -0.17 28 26 0 10.56 

10/21/2007 9:55 12.96 42 2600 -0.16 28 26 0 10.56 

10/21/2007 9:56 15.81 42 2600 -0.19 28 26 0 10.56 

30/21/20079:57 15.78 42 2600 -0.12 28 26 0 10.56 

10/21/2007 9:58 14.18 42 2600 -0.14 28 26 0 10.56 

10/21/2007 9:59 15.78 42 2600 -0.2 28 26 0 10.56 

3 
Process Data 

10/21/2007 10:00 15.79 42 2600 -0.16 28 26 0 10.56 

10/21/200710:01 14.06 42 2600 -0.18 28 26 0 10.56 

10/21/200710:02 15.71 42 2600 -0.16 28 26 0 10.56 

10/21/200710:03 15.7 42 2600 -0.17 28 26 0 10.56 

10/21/200710:04 13.98 42 2600 -0.13 28 26 0 10.56 

10/21/200710:05 15.75 42 2600 -0.16 28 26 0 10.56 

10/21/200710:06 15.63 42 2600 -0.16 28 26 0 10.56 

10/21/2007 10:07 14.27 42 2600 -0.16 28 26 0 10.56 

10/21/200710:08 15.71 42 2600 -0.19 28 26 0 10.56 

10/21/200710:09 15.57 42 2600 -0.19 28 26 0 10.56 

10/21/200710:10 29.95 42 1200 -0.06 28 26 1 10.56 

10/21/200710:11 29.91 42 1200 -0.1 28 27 0 10.56 

10/21/200710:12 11.64 42 2600 -0.12 28 27 0 10.56 

10/21/2007 10:13 11.84 42 2600 -0.09 28 27 0 10.56 

10/21/200710:14 12.73 42 2600 -0.08 28 27 0 10.56 

10121/200710:15 12.7 42 2600 -0.06 28 27 0 10.56 

10/21/200710:16 11.64 42 2600 -0.22 28 27 0 10.56 

10/21/200710:17 14.31 42 2600 -0.21 28 27 0 10.56 

10/21/200710:18 14.01 42 2600 -0.17 28 27 0 10.56 

10/21/200710:19 14.74 42 2600 -0.05 28 27 0 10.56 

10/21/200710:20 14.43 42 2600 -0.18 28 27 0 10.56 

10/21/2007 10:21 12.88 42 2600 -0.2 28 27 0 10.56 

10/21/2007 10:22 15.49 42 2600 -0.15 28 27 0 10.56 

10/2112007 10:23 15.63 42 2600 -0.15 28 27 0 10.56 

10/21/2007 10:24 12.99 42 2600 -0.19 28 27 0 10.56 

10/21/200710:25 15.54 42 2600 -0.17 28 27 0 10.56 

10/21/2007 10:26 15.6 42 2600 -0.2 28 27 0 10.56 

10/21/2007 10:27 13.92 42 2600 -0.18 28 27 0 10.56 

10/21/200710:28 15.49 42 2600 -0.16 28 27 0 10.56 

10/21/2007 10:29 15.58 42 2600 -0.14 28 27 0 10.56 

10/21/200710:30 13.97 42 2600 -0.11 28 27 0 10.56 

10/21/2007 10:31 15.6 42 2600 -0.17 28 27 0 10.56 

10/21/200710:32 15.72 42 2600 -0.21 28 27 0 10.56 

10/21/200710:33 15.57 42 2600 -0.16 28 27 0 10.56 

10/21/200710:34 13.97 42 2600 -0.15 28 27 0 10.56 

10/21/2007 10:35 15.61 42 2600 -0.13 28 27 0 10.56 

10/21/200710:36 29.76 42 1200 -0.07 28 27 1 10.56 

10/21/200710:37 17.62 42 2600 -0.23 28 28 0 10.56 

10/21/200710:38 11.82 42 2600 -0.22 28 28 0 10.56 

10/21/2007 10:39 11.77 42 2600 -0.19 28 28 0 10.56 

10/21/200710:40 12.73 42 2600 -0.13 28 28 0 10.56 

10/21/200710:41 11.79 42 2600 -0.17 28 28 0 10.56 

10/21/200710:42 13 42 2600 -0.18 28 28 0 10.56 

10/21/200710:43 11.55 42 2600 -0.21 28 28 0 10.56 

10/21/2007 10:44 14.04 42 2600 -0.16 28 28 0 10.56 

10/21/200710:45 12.93 42 2600 -0.09 28 28 0 10.56 

10/21/2007 10:46 13.84 42 2600 -0.18 28 28 0 10.56 

10/21/2007 10:47 14.1 42 2600 -0.19 28 28 0 10.56 

10/21/2007 10:48 15.49 42 2600 -0.19 28 28 0 10.56 

10/21/200710:49 12.95 42 2600 -0.18 28 28 0 10.56 

10/21/2007 10:50 15.42 42 2600 -0.16 28 28 0 10.56 

10/21/200710:51 15.71 42 2600 -0.19 28 28 0 10.56 

10/21/2007 10:52 13.37 42 2600 -0.14 28 28 0 10.56 

10/21/200710:53 15.64 42 2600 -0.13 28 28 0 10.56 

10/21/200710:54 15.66 42 2600 -0.13 28 28 0 10.56 

10/21/200710:55 14.21 42 2600 -0.18 28 28 0 10.56 

10/21/200710:56 14.06 42 2600 -0.19 28 28 0 10.56 

10/21/2007 10:57 15.73 42 2600 -0.16 28 28 0 10.56 

10/21/200710:58 15.55 42 2600 -0.16 28 28 0 10.56 

10/21/2007 10:59 13.99 42 2600 -0.18 28 28 0 10.56 

10/21/2007 11:00 15.72 42 2600 -0.21 28 28 0 10.56 

4 
Process Data 

10/21/200711:01 15.71 42 2600 -0.12 28 28 0 10.56 

10/21/2007 11:02 29.86 42 1200 -0.06 28 28 1 10.56 

10/21/200711:03 11.71 42 2600 0 28 29 0 10.56 

10/21/200711:04 11.94 42 2600 -0.1 28 29 0 10.56 

10/21/200711:05 11.91 42 2600 -0.09 28 29 0 10.56 

10/21/200711:06 13.74 42 2600 -0.11 28 29 0 10.56 

10/21/2007 11:07 11.85 42 2600 -0.09 28 29 0 10.56 

10/21/2007 11:08 14.31 42 2600 -0.14 28 29 0 10.56 

10/21/200711:09 12.48 42 2600 -0.17 28 29 0 10.56 

10/21/200711:10 12.88 42 2600 -0.16 28 29 0 10.56 

10/21/200711:11 14.25 42 2600 -0.17 28 29 0 10.56 

10/21/2007 11:12 14.71 42 2600 -0.12 28 29 0 10.56 

10/21/200711:13 12.97 42 2600 -0.24 28 29 0 10.56 

10/21/200711:14 14.16 42 2600 -0.19 28 29 0 10.56 

10/21/2007 11:15 15.78 42 2600 -0.18 28 29 0 10.56 

10/21/2007 11:16 12.77 42 2600 -0.14 28 29 0 10.56 

10/21/2007 11:17 14.89 42 2600 -0.2 28 29 0 10.56 

10/21/200711:18 15.45 42 2600 -0.15 28 29 0 10.56 

10/21/200711:19 14.06 42 2600 -0.21 28 29 0 10.56 

10/21/200711:20 14.26 42 2600 -0.21 28 29 0 10.56 

10/21/200711:21 15.77 42 2600 -0.16 28 29 0 10.56 

10/21/200711:22 14.03 42 2600 -0.17 28 29 0 10.56 

10/21/2007 11:23 14.51 42 2600 -0.16 28 29 0 10.56 

10/21/200711:24 15.81 42 2600 -0.14 28 29 0 10.56 

10/21/200711:25 13.99 42 2600 -0.19 28 29 0 10.56 

10/21/2007 11:26 15.7 42 2600 -0.17 28 29 0 10.56 

10/21/200711:27 29.21 42 1200 -0.07 28 29 0 10.56 

10/21/200711:28 29.84 42 1200 -0.04 28 30 0 10.56 

10/21/200711:29 11.79 42 2600 -0.11 28 30 0 10.56 

10/21/200711:30 11.7 42 2600 -0.17 28 30 0 10.56 

10/21/200711:31 12.24 42 2600 -0.12 28 30 0 10.56 

10/21/2007 11:32 12.71 42 2600 -0.17 28 30 0 10.56 

10/21/200711:33 11.8 42 2600 -0.18 28 30 0 10.56 

10/21/200711:34 11.66 42 2600 -0.16 28 30 0 10.56 

10/21/20071135 12.4 42 2600 -0.13 28 30 0 10.56 

10/21/200711:36 14.02 42 2600 -0.12 28 30 0 10.56 

10/21/200711:37 14.44 42 2600 -0.19 28 30 0 10.56 

10/21/200711:38 13.21 42 2600 -0.16 28 30 0 10.56 

10/21/200711:39 14.22 42 2600 -0.1 28 30 0 10.56 

10/21/2007 11:40 15.92 42 2600 -0.13 28 30 0 10.56 

10/21/200711:41 13.06 42 2600 -0.17 28 30 0 10.56 

10/21/200711:42 14.34 42 2600 -0.19 28 30 0 10.56 

10/21/200711:43 15.82 42 2600 -0.2 28 30 0 10.56 

10/21/200711:44 14.23 42 2600 -0.15 28 30 0 10.56 

10/21/200711:45 14.6 42 2600 -0.13 28 30 0 10.56 

10/21/200711:46 15.85 42 2600 -0.19 28 30 0 10.56 

10/21/200711:47 14.07 42 2600 -0.17 28 30 0 10.56 

10/21/200711:48 14.45 42 2600 -0.18 28 30 0 10.56 

10/21/2007 11:49 15.93 42 2600 -0.13 28 30 0 10.56 

10/21/2007 11:50 14.26 42 2600 -0.17 28 30 0 10.56 

10/21/2007 11:51 15.64 42 2600 -0.19 28 30 0 10.56 

10/21/2007 11:52 15.74 42 2600 -0.14 28 30 0 10.56 

10/21/200711:53 29.78 42 1200 0.02 28 30 1 10.56 

10/21/200711:54 29.8 42 1200 -0.1 28 31 0 10.56 

10/21/200711:55 11.87 42 2600 -0.09 28 31 0 10.56 

10/21/200711:56 11.95 42 2600 -0.15 28 31 0 10.56 

10/21/200711:57 11.82 42 2600 -0.1 28 31 0 10.56 

10/21/200711:58 11.6 42 2600 -0.07 28 31 0 10.56 

10/21/200711:59 11.63 42 2600 -0.24 28 31 0 10.56 

10/21/200712:00 11.64 42 2600 -0.21 28 31 0 10.56 

10/21/200712:01 11.75 42 2600 -0.17 28 31 0 10.56 

5 
Process Data 

10/21/2007 12:02 13.99 42 2600 -0.17 28 31 0 10.56 

10/21/200712:03 13.19 42 2600 -0.2 28 31 0 10.56 

10/21/200712:04 13.21 42 2600 -0.18 28 31 0 10.56 

10/21/200712:05 14.23 42 2600 -0.19 28 31 0 10.56 

10/21/200712:06 15.82 42 2600 -0.18 28 31 0 10.56 

10/211200712:07 12.86 42 2600 -0.17 28 31 0 10.56 

10/21/2007 12:08 14.45 42 2600 -0.18 28 31 0 10.56 

10/21/200712:09 15.77 42 2600 -0.21 28 31 0 10.56 

10/21/200712:10 13.15 42 2600 -0.16 28 31 0 10.56 

101211200712:11 14.65 42 2600 -0.18 28 31 0 10.56 

10/21/2007 12:12 15.79 42 2600 -0.15 28 31 0 10.56 

10/21/200712:13 14.08 42 2600 -0.19 28 31 0 10.56 

10/21/2007 12:14 14.16 42 2600 -0.15 28 31 0 10.56 

10/21/2007 12:15 13.06 42 2600 -0.14 28 31 0 10.56 

10/21/200712:16 15.69 42 2600 -0.2 28 31 0 10.56 

10/21/200712:17 12.61 42 2600 -0.12 28 31 0 10.56 

10/21/2007 12:18 15.74 42 2600 -0.18 28 31 0 10.56 

10/21/200712:19 29.69 42 1200 -0.03 28 31 1 10.56 

10/21/200712:20 10.46 42 2600 -0.19 28 32 0 10.56 

10/21/200712:21 11.76 42 2600 -0.14 28 32 0 10.56 

10/21/200712:22 11.65 42 2600 -0.18 28 32 0 10.56 

10/21/200712:23 12.74 42 2600 -0.19 28 32 0 10.56 

10/21/200712:24 12.68 42 2600 -0.18 28 32 0 10.56 

10/21/2007 12:25 11.49 42 2600 -0.21 28 32 0 10.56 

10/21/200712:26 11.64 42 2600 -0.19 28 32 0 10.56 

10/21/200712:27 12.57 42 2600 -0.17 28 32 0 10.56 

10/21/2007 12:28 12.56 42 2600 -0.15 28 32 0 10.56 

10/21/2007 12:29 12.87 42 2600 -0.16 28 32 0 10.56 

10/21/200712:30 13.33 42 2600 -0.19 28 32 0 10.56 

10/21/200712:31 15.79 42 2600 -0.2 28 32 0 10.56 

10/21/200712:32 11.11 42 2600 -0.17 28 32 0 10.56 

10/21/200712:33 14.25 42 2600 -0.18 28 32 0 10.56 

10121/200712:34 13.34 42 2600 -0.19 28 32 0 10.56 

10/21/200712:35 14.08 42 2600 -0.15 28 32 0 10.56 

10/21/200712:36 13.26 42 2600 -0.15 28 32 0 10.56 

10/21/200712:37 15.57 42 2600 -0.13 28 32 0 10.56 

10/21/2007 12:38 12.91 42 2600 -0.17 28 32 0 10.56 

10/21/200712:39 14.01 42 2600 -0.01 28 32 0 10.56 

10/21/200712:40 11.53 42 2600 -0.2 28 32 0 10.56 

10/21/200712:41 15.73 42 2600 -0.19 28 32 0 10.56 

10/21/200712:42 11.59 42 2600 -0.17 28 32 0 10.56 

10121/200712:43 15.31 42 2600 -0.21 28 32 0 10.56 

10/21/200712:44 14.28 42 2600 -0.16 28 32 0 10.56 

10/21/200712:45 29.72 42 1200 -0.05 28 32 1 10.56 

10/21/200712:46 11.78 42 2600 -0.12 28 33 0 10.56 

10/21/200712:47 11.79 42 2600 -0.09 28 33 0 10.56 

10/21/200712:48 11.68 42 2600 -0.03 28 33 0 10.56 

10/21/2007 12:49 12.74 42 2600 -0.09 28 33 0 10.56 

10/21/200712:50 11.7 42 2600 -0.23 28 33 0 10.56 

10/21/200712:51 11.73 42 2600 -0.19 28 33 0 10.56 

10/21/200712:52 12.66 42 2600 -0.13 28 33 0 10.56 

10/21/200712:53 12.53 42 2600 -0.17 28 33 0 10.56 

10/21/200712:54 11.49 42 2600 -0.23 28 33 0 10.56 

10/21/200712:55 12.45 42 2600 -0.17 28 33 0 10.56 

10/21/200712:56 12.56 42 2600 -0.14 28 33 0 10.56 

10/21/200712:57 13.34 42 2600 -0.2 28 33 0 10.56 

10/21/200712:58 12.95 42 2600 -0.18 28 33 0 10.56 

10/21/200712:59 13.59 42 2600 -0.19 28 33 0 10.56 

10/21/200713:00 14.09 42 2600 -0.15 28 33 0 10.56 

10/21/200713:01 13.26 42 2600 -0.19 28 33 0 10.56 

10/21/200713:02 13.91 42 2600 -0.18 28 33 0 10.56 

a] 
Process Data 

10/21/2007 13:03 13.9 42 2600 -0.13 28 33 0 10.56 

10/21/2007 13:04 13.74 42 2600 -0.19 28 33 0 10.56 

10/21/200713:05 13.35 42 2600 -0.17 28 33 0 10.56 

10/21/200713:06 14.21 42 2600 -0.17 28 33 0 10.56 

10/21/200713:07 13.63 42 2600 -0.13 28 33 0 10.56 

10/21/200713:08 13.34 42 2600 -0.15 28 33 0 10.56 

10/21/2007 13:09 13.17 42 2600 -0.14 28 33 0 10.56 

10/21/200713:10 28.59 42 1200 -0.06 28 33 1 10.56 

10/21/200713:11 29.54 42 1200 -0.02 28 34 0 10.56 

10/21/200713:12 11.76 42 2600 •-0.13 28 34 0 10.56 

10/21/200713:13 11.82 42 2600 -0.1 28 34 0 10.56 

10/21/2007 13:14 12.02 42 2600 -0.12 28 34 0 10.56 

10/21/200713:15 11.75 42 2600 -0.14 28 34 0 10.56 

10/21/200713:16 11.62 42 2600 -0.15 28 34 0 10.56 

10/21/2007 13:17 11.75 42 2600 -0.13 28 34 0 10.56 

10/21/200713:18 11.38 42 2600 -0.11 28 34 0 10.56 

10/21/200713:19 11.62 42 2600 -0.03 28 34 0 10.56 

10/21/200713:20 11.4 42 2600 -0.11 28 34 0 10.56 

10/21/200713:21 11 42 2600 -0.09 28 34 0 10.56 

10/21/2007 13:22 12.47 42 2600 -0.09 28 34 0 10.56 

10/21/2007 13:23 11.86 42 2600 -0.03 28 34 0 10.56 

10/21/2007 13:24 14.07 42 2600 -0.1 28 34 0 10.56 

10/21/200713:25 10.68 42 2600 -0.14 28 34 0 10.56 

10/21/200713:26 14.03 42 2600 0.02 28 34 0 10.56 

10/21/2007 13:27 11.85 42 2600 -0.14 28 34 0 10.56 

10/21/2007 13:28 15.28 42 2600 -0.1 28 34 0 10.56 

10/21/2007 13:29 13.27 42 2600 -0.09 28 34 0 10.56 

10/21/2007 13:30 13.5 42 2600 -0.12 28 34 0 10.56 

10121/200713:31 11.74 42 2600 -0.15 28 34 0 10.56 

10/21/200713:32 15.48 42 2600 -0.1 28 34 0 10.56 

10/21/200713:33 11.92 42 2600 -0.13 28 34 0 10.56 

10/21/200713:34 13.47 42 2600 -0.08 28 34 0 10.56 

10/21/200713:35 12.91 42 2600 -0.09 28 34 0 10.56 

10/21/200713:36 29.49 42 1200 -0.01 28 34 1 10.56 

10/21/2007 13:37 20.72 42 2600 -0.12 28 35 0 10.56 

10/21/2007 13:38 11.87 42 2600 -0.03 28 35 0 10.56 

10/21/200713:39 11.78 42 2600 -0.03 28 35 0 10.56 

10/21/200713:40 11.6 42 2600 -0.01 28 35 0 10.56 

10/21/2007 13:41 11.85 42 2600 -0.03 28 35 0 10.56 

10/21/200713:42 11.48 42 2600 -0.08 28 35 0 10.56 

10/21/200713:43 12.27 42 2600 -0.07 28 35 0 10.56 

10/21/200713:44 11.3 42 2600 -0.08 28 35 0 10.56 

10/21/200713:45 11.61 42 2600 -0.07 28 35 0 10.56 

10/21/200713:46 11.32 42 2600 -0.06 28 35 0 10.56 

10/21/200713:47 11.04 42 2600 -0.07 28 35 0 10.56 

10/21/2007 13:48 12.06 42 2600 -0.05 28 35 0 10.56 

10/21/200713:49 13.27 42 2600 -0.09 28 35 0 10.56 

10/21/200713:50 11.01 42 2600 -0.05 28 35 0 10.56 

10/21/200713:51 13.29 42 2600 -0.05 28 35 0 10.56 

10/21/200713:52 12.96 42 2600 -0.06 28 35 0 10.56 

10/21/200713:53 12.92 42 2600 -0.07 28 35 0 10.56 

10/21/200713:54 12.26 42 2600 -0.06 28 35 0 10.56 

10/21/200713:55 14.59 42 2600 -0.05 28 35 0 10.56 

10/21/200713:56 11.49 42 2600 -0.1 28 35 0 10.56 

10/21/200713:57 12.88 42 2600 -0.02 28 35 0 10.56 

10/21/200713:58 11.93 42 2600 -0.07 28 35 0 10.56 

10/21/200713:59 12.73 42 2600 -0.07 28 35 0 10.56 

10/21/200714:00 11.23 42 2600 -0.04 28 35 0 10.56 

10/21/2007 14:01 14.89 42 2600 -0.04 28 35 0 10.56 

10/21/200714:02 29.58 42 1200 0.09 28 35 1 10.56 

10/21/200714:03 11.47 42 2600 -0.12 28 36 0 10.56 

7 
Process Data 

10/21/200714:04 11.71 42 2600 -0.05 28 36 0 10.56 

10/21/2007 14:05 11.87 42 2600 -0.04 28 36 0 10.56 

10/21/2007 14:06 11.68 42 2600 -0.04 28 36 0 10.56 

10/21/2007 14:07 11.13 42 2600 0 28 36 0 10.56 

10/21/2007 14:08 11.39 42 2600 -0.1 28 36 0 10.56 

10/21/2007 14:09 11.15 42 2600 -0.01 28 36 0 10.56 

10/21/2007 14:10 12.04 42 2600 -0.03 28 36 0 10.56 

10/21/2007 14:11 11.15 42 2600 -0.03 28 36 0 10.56 

10/21/200714:12 11.27 42 2600 -0.05 28 36 0 10.56 

10/21/200714:13 11.98 42 2600 0.05 28 36 0 10.56 

10/21/200714:14 11.05 42 2600 -0.08 28 36 0 10.56 

10/21/200714:15 11.2 42 2600 -0.07 28 36 0 10.56 

10/21/2007 14:16 10.95 42 2600 -0.07 28 36 0 10.56 

10/21/200714:17 12.55 42 2600 -0.03 28 36 0 10.56 

10/21/200714:18 11.13 42 2600 0.01 28 36 0 10.56 

10/21/2007 14:19 12.51 42 2600 -0.04 28 36 0 10.56 

10/2112007 14:20 12.38 42 2600 -0.02 28 36 0 10.56 

10/21/200714:21 12.41 42 2600 -0.03 28 36 0 10.56 

10/21/200714:22 11.07 42 2600 -0.04 28 36 0 10.56 

10/21/2007 14:23 13.05 42 2600 -0.06 28 36 0 10.56 

10/21/200714:24 11.06 42 2600 -0.07 28 36 0 10.56 

10/21/200714:25 12.38 42 2600 0.01 28 36 0 10.56 

10/21/200714:26 11.16 42 2600 -0.04 28 36 0 10.56 

10/21/200714:27 25.92 42 1200 0.06 28 36 0 10.56 

10/21/2007 14:28 29.4 42 1200 0 28 37 0 10.56 

10/21/200714:29 11.76 42 2600 0.11 28 37 0 10.56 

10/21/200714:30 11.72 42 2600 0.05 28 37 0 10.56 

10/21/200714:31 11.66 42 2600 0.06 28 37 0 10.56 

10/211200714:32 11.7 42 2600 0.01 28 37 0 10.56 

10/21/200714:33 11.44 42 2600 -0.16 28 37 0 10.56 

10/21/200714:34 11.66 42 2600 -0.08 28 37 0 10.56 

10/21/200714:35 11.59 42 2600 -0.05 28 37 0 10.56 

10/21/200714:36 11.63 42 2600 -0.07 28 37 0 10.56 

10/21/200714:37 11.68 42 2600 -0.03 28 37 0 10.56 

10/21/200714:38 11.19 42 2600 -0.04 28 37 0 10.56 

10/21/2007 14:39 11.15 42 2600 -0.03 28 37 0 10.56 

10/21/200714:40 11.49 42 2600 -0.07 28 37 0 10.56 

10/21/200714:41 10.87 42 2600 -0.04 28 37 0 10.56 

10/21/200714:42 10.84 42 2600 -0.1 28 37 0 10.56 

10/21/200714:43 10.92 42 2600 -0.07 28 37 0 10.56 

10/21/2007 14:44 11.12 42 2600 -0.04 28 37 0 10.56 

10/21/200714:45 10.92 42 2600 0 28 37 0 10.56 

10/21/200714:46 11.49 42 2600 0.03 28 37 0 10.56 

10/21/200714:47 10.9 42 2600 -0.1 28 37 0 10.56 

10/21/2007 14:48 12.03 42 2600 -0.06 28 37 0 10.56 

10/21/200714:49 10.84 42 2600 -0.04 28 37 0 10.56 

10/21/200714:50 11.94 42 2600 -0.08 28 37 0 10.56 

10/21/2007 14:51 10.92 42 2600 -0.03 28 37 0 10.56 

10/21/200714:52 11.93 42 2600 -0.09 28 37 0 10.56 

10/21/200714:53 29.58 42 1200 0.04 28 37 1 10.56 

10/21/200714:54 29.68 42 1200 0.06 28 38 0 10.56 

10/211200714:55 11.62 42 2600 -0.02 28 38 0 10.56 

10/21/200714:56 11.64 42 2600 -0.05 28 38 0 10.56 

10/21/200714:57 11.11 42 2600 -0.07 28 38 0 10.56 

10/21/200714:58 11.55 42 2600 -0.05 28 38 0 10.56 

10/21/200714:59 11.56 42 2600 -0.07 28 38 0 10.56 

10/21/200715:00 11.19 42 2600 -0.04 28 38 0 10.56 

10/21/200715:01 10.93 42 2600 -0.06 28 38 0 10.56 

10/21/200715:02 10.85 42 2600 -0.07 28 38 0 10.56 

10/21/200715:03 11 42 2600 -0.03 28 38 0 10.56 

10/21/2007 15:04 11.04 42 2600 -0.04 28 38 0 10.56 

8 
Process Data 

10/21/200715:05 12.92 42 2600 0 28 38 0 10.56 

10/21/200715:06 10.72 42 2600 -0.06 28 38 0 10.56 

10/21/200715:07 11.66 42 2600 -0.05 28 38 0 10.56 

10/21/200715:08 11.93 42 2600 -0.06 28 38 0 10.56 

10/21/200715:09 11.47 42 2600 -0.05 28 38 0 10.56 

10/21/200715:10 10.67 42 2600 -0.01 28 38 0 10.56 

10/21/200715:11 11.91 42 2600 -0.04 28 38 0 10.56 

10/21/200715:12 10.81 42 2600 -0.06 28 38 0 10.56 

10/21/2007 15:13 12.83 42 2600 -0.12 28 38 0 10.56 

10/21/200715:14 10.67 42 2600 -0.06 28 38 0 10.56 

10/21/200715:15 11.98 42 2600 0.02 28 38 0 10.56 

10/21/2007 15:16 11.4 42 2600 -0.03 28 38 0 10.56 

10/21/200715:17 12.33 42 2600 -0.07 28 38 0 10.56 

10/21/2007 15:18 12.2 42 2600 -0.03 28 38 0 10.56 

10/21/200715:19 29.52 42 1200 0.03 28 38 1 10.56 

10/21/200715:20 11.74 42 2600 0.03 28 39 0 10.56 

10/21/200715:21 11.67 42 2600 0.08 28 39 0 10.56 

10/21/200715:22 11.65 42 2600 -0.01 28 39 0 10.56 

10/21/200715:23 11.64 42 2600 0 28 39 0 10.56 

10/21/200715:24 11.57 42 2600 0.03 28 39 0 10.56 

10/21/200715:25 11.42 42 2600 -0.08 28 39 0 10.56 

10/21/200715:26 11.21 42 2600 -0.08 28 39 0 10.56 

10/21/200715:27 11.45 42 2600 -0.07 28 39 0 10.56 

10/211200715:28 10.86 42 2600 -0.06 28 39 0 10.56 

10/21/200715:29 11 42 2600 -0.03 28 39 0 10.56 

10/21/200715:30 11.22 42 2600 -0.02 28 39 0 10.56 

10/21/200715:31 10.59 42 2600 -0.06 28 39 0 10.56 

10/21/200715:32 10.5 42 2600 -0.06 28 39 0 10.56 

10/21/2007 15:33 10.72 42 2600 0 28 39 0 10.56 

10/21/2007 15:34 10.44 42 2600 -0.05 28 39 0 10.56 

10/21/200715:35 11.71 42 2600 -0.06 28 39 0 10.56 

30/21/200715:36 10.5 42 2600 -0.05 28 39 0 10.56 

10/21/200715:37 10.51 42 2600 -0.06 28 39 0 10.56 

10/21/200715:38 11.93 42 2600 -0.01 28 39 0 10.56 

10/21/200715:39 10.7 42 2600 -0.01 28 39 0 10.56 

10/211200715:40 10.6 42 2600 -0.04 28 39 0 10.56 

10/21/2007 15:41 12.49 42 2600 -0.08 28 39 0 10.56 

10/21/2007 15:42 10.45 42 2600 -0.04 28 39 0 10.56 

10/211200715:43 11.22 42 2600 -0.06 28 39 0 10.56 

10/21/200715:44 11.13 42 2600 -0.05 28 39 0 10.56 

10/21/2007 15:45 29.7 42 1200 0.08 28 39 1 10.56 

10/21/200715:46 11.07 42 2600 -0.09 28 40 0 10.56 

10/21/200715:47 11.38 42 2600 -0.01 28 40 0 10.56 

10/21/200715:48 10.6 42 2600 -0.08 28 40 0 10.56 

10/21/200715:49 10.81 42 2600 -0.05 28 40 0 10.56 

10/21/200715:50 10.76 42 2600 -0.07 28 40 0 10.56 

10/21/200715:51 10.45 42 2600 -0.08 28 40 0 10.56 

10/21/2007 15:52 11.57 42 2600 -0.05 28 40 0 10.56 

10/21/200715:53 11.22 42 2600 -0.03 28 40 0 10.56 

10/21/200715:54 11.24 42 2600 -0.08 28 40 0 10.56 

10/21/200715:55 10.43 42 2600 -0.06 28 40 0 10.56 

10/21/200715:56 10.63 42 2600 -0.08 28 40 0 10.56 

10/21/200715:57 11.28 42 2600 -0.03 28 40 0 10.56 

10/21/200715:58 11.6 42 2600 -0.07 28 40 0 10.56 

10/21/200715:59 10.43 42 2600 -0.01 28 40 0 10.56 

10/21/200716:00 10.45 42 2600 -0.1 28 40 0 10.56 

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