ANALYTICAL REPORT

Job Number: 500-53342-1

Job Description: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, SC 29651

Attention: Mr. Robert Stevens

_____________________________________________

Approved for release.

Donna L Ingersoll

Project Manager II

1/4/2013 2:22 PM

Donna L Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

01/04/2013

cc: Mr. David Kirby

Mr. Robert Malcomson

These test results meet all the requirements of NELAC for accredited parameters.

The Lab Certification ID# is 100201.

All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears

on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be

reproduced only in its entirety.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

TestAmerica Laboratories, Inc.

TestAmerica Chicago 2417 Bond Street, University Park, IL 60484

Tel (708) 534-5200 Fax (708) 534-5211 www.testamericainc.com

Page 1 of 332 01/04/2013
Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83

Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104

Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 108

Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 108

Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 138

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 159

Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 159

Page 2 of 332 01/04/2013
Table of Contents

Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 162

Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 165

Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 171

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174

Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174

Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 175

Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 176

Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 179

Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 179

Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187

Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 190

Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 203

Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 209

Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 214

Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 226

Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 229

Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 234

Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 243

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 249

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 250

Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 251

Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 254

Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 254

Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 258

Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 259

Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 261

Page 3 of 332 01/04/2013
Table of Contents

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 263

Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 281

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 289

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 327

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 330

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332

Page 4 of 332 01/04/2013
Job Narrative

500-53342-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/18/2012 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 2.4o C.

GC/MS VOA 

Method(s) 8260B: One internal standard response was outside of acceptance limits for the following sample:FC Composite 5 

(500-53342-2). The sample was re-analyzed at a dilution for Acetone with all internal standard areas within limits. Both sets of data have 

been provided.

No other analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

Page 5 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53342-1

Instrument ID: CMS16 Analysis Batch Number: 170196

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD1 500-170196/6 IC

11/19/12 12:14 16I1119A.D GC Column: DB624 ID: 0.2(mm)

Acetone 1.91 Poor chromatography wernerb 11/19/12 13:19

8260B

Page 6 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53342-1

Instrument ID: CMS22 Analysis Batch Number: 172614

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD01 500-172614/2 IC

12/11/12 14:23 22I1211A.D GC Column: DB624 ID: 0.2(mm)

Trichloroethene 7.55 Baseline alikpalae 12/11/12 19:50

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD02 500-172614/3 IC

12/11/12 14:51 22I1211B.D GC Column: DB624 ID: 0.2(mm)

Bromomethane 2.01 Baseline alikpalae 12/11/12 19:54

Acetonitrile 3.59 Split Peak alikpalae 12/11/12 19:54

Tetrachloroethene 9.75 Split Peak alikpalae 12/11/12 19:54

8260B

Page 7 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53342-1

Instrument ID: CMS22 Analysis Batch Number: 172615

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD01 500-172615/2 IC

12/11/12 14:23 22I1211A.D GC Column: DB624 ID: 0.2(mm)

Trichloroethene 7.55 Baseline alikpalae 12/11/12 19:50

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD02 500-172615/3 IC

12/11/12 14:51 22I1211B.D GC Column: DB624 ID: 0.2(mm)

Bromomethane 2.01 Baseline alikpalae 12/11/12 19:54

Acetonitrile 3.59 Split Peak alikpalae 12/11/12 19:54

Tetrachloroethene 9.75 Split Peak alikpalae 12/11/12 19:54

8260B

Page 8 of 332 01/04/2013
SAMPLE SUMMARY

Client: Project Integration, Inc Job Number: 500-53342-1

Lab Sample ID Client Sample ID Client Matrix Sampled Received

Date/Time Date/Time

500-53342-1 FC Composite 5 Solid 12/17/2012 1450 12/18/2012 0940

500-53342-2 FC Composite 5 Solid 12/17/2012 1440 12/18/2012 0940

500-53342-3 FC EB 5 Water 12/17/2012 1430 12/18/2012 0940

500-53342-4 Trip Blank Water 12/17/2012 0000 12/18/2012 0940

TestAmerica Chicago Page 9 of 332 01/04/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53342-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53342-1 FC COMPOSITE 5

Barium 409 3.01 mg/Kg 6010B

Copper 693 3.01 mg/Kg 6010B

Chromium 14200 3.01 mg/Kg 6010B

Nickel 77.4 B 3.01 mg/Kg 6010B

Lead 250 B 1.50 mg/Kg 6010B

Vanadium 238 1.50 mg/Kg 6010B

Zinc 441 6.02 mg/Kg 6010B

Mercury 0.321 0.0540 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Cyanide, Total 0.905 J 1.59 mg/Kg 9014

Sulfide 798 82.8 mg/Kg 9034

pH 9.59 0.200 SU 9045C

HEM (Oil & Grease) 13200 1650 mg/Kg 9071B

Percent Moisture 70 0.10 % Moisture

Percent Solids 30 0.10 % Moisture

% Moisture 70.0 0.100 % SM 2540G

Total Solids 30.0 0.100 % SM 2540G

TCLP

Chromium 0.166 0.0250 mg/L 6010B

Nickel 0.531 0.0250 mg/L 6010B

Vanadium 0.00669 J 0.0250 mg/L 6010B

Zinc 0.0502 J 0.100 mg/L 6010B

500-53342-2 FC COMPOSITE 5

Acetone 3200 928 ug/Kg 8260B

2-Butanone (MEK) 28.2 18.6 ug/Kg 8260B

Percent Moisture 73 0.10 % Moisture

Percent Solids 27 0.10 % Moisture

500-53342-3 FC EB 5

Copper 0.00616 J 0.0100 mg/L 6010B

Lead 0.00245 J B 0.00500 mg/L 6010B

Zinc 0.00789 J 0.0200 mg/L 6010B

TestAmerica Chicago Page 10 of 332 01/04/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53342-1

Description Lab Location Method Preparation Method

Matrix: Solid

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Metals TAL CHI SW846 3050B

Metals (ICP) TAL CHI SW846 6010B

TCLP Extraction TAL CHI SW846 1311

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

TCLP Extraction TAL CHI SW846 1311

Preparation, Mercury TAL CHI SW846 7470A

Mercury (CVAA) TAL CHI SW846 7471A

Preparation, Mercury TAL CHI SW846 7471A

Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010

Chromium, Hexavalent TAL CHI SW846 7196A

Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

pH TAL CHI SW846 9045C

HEM and SGT-HEM TAL CHI SW846 9071B

Preparation, HEM and SGT-HEM TAL CHI SW846 9071B

Percent Moisture TAL CHI EPA Moisture

Total, Fixed, and Volatile Solids TAL CHI SM SM 2540G

Matrix: Water

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

Preparation, Mercury TAL CHI SW846 7470A

HEM and SGT-HEM TAL CHI 1664A 1664A

HEM and SGT-HEM (SPE) TAL CHI 1664A 1664A

Chromium, Hexavalent TAL CHI SW846 7196A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

TestAmerica Chicago Page 11 of 332 01/04/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53342-1

Description Lab Location Method Preparation Method

Lab References:

TAL CHI = TestAmerica Chicago

Method References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago Page 12 of 332 01/04/2013
METHOD / ANALYST SUMMARY

Client: Project Integration, Inc Job Number: 500-53342-1

Method Analyst Analyst ID

SW846 8260B Alikpala, Elaine EA

SW846 8260B Werner, Brian D BDW

SW846 6010B Smith, Todd D TDS

SW846 7470A Bills, Brandon J BJB

SW846 7471A Bills, Brandon J BJB

SW846 1010 Wasowicz, Andrew P APW

1664A 1664A Brogan, Mary T MTB

SW846 7196A Deb, Khona KD

SW846 7196A Wasowicz, Andrew P APW

SW846 9014 Treadwell, Eliane A EAT

SW846 9034 Boyd, Cheryl L CLB

SW846 9034 Moore, Colleen L CLM

SW846 9045C Moore, Colleen L CLM

SW846 9071B Brogan, Mary T MTB

EPA Moisture Veldhuizen, Chris M CMV

SM SM 2540G Veldhuizen, Chris M CMV

TestAmerica Chicago

Page 13 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix: % Moisture: 73.1

500-53342-2

Solid

Date Sampled: 12/17/2012 1440

Date Received: 12/18/2012 0940

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/20/2012 1352

12/20/2012 1352

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53342-02.D

5 g

5 mL

5030B

CMS16

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173515

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 28.2 6.72 18.6

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 112 70 - 134

Toluene-d8 (Surr) 100 75 - 122

4-Bromofluorobenzene (Surr) 83 70 - 122

Dibromofluoromethane 111 75 - 120

TestAmerica Chicago Page 14 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix: % Moisture: 73.1

500-53342-2

Solid

Date Sampled: 12/17/2012 1440

Date Received: 12/18/2012 0940

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/19/2012 1300

12/21/2012 2240

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53342-02.D

5 g

Run Type: DL 5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173708

500-173454

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 3200 241 928

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 94 75 - 125

Toluene-d8 (Surr) 96 75 - 120

4-Bromofluorobenzene (Surr) 86 75 - 120

Dibromofluoromethane 95 75 - 120

TestAmerica Chicago Page 15 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC EB 5

Client Matrix:

500-53342-3

Water

Date Sampled: 12/17/2012 1430

Date Received: 12/18/2012 0940

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/24/2012 1425

12/24/2012 1425

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53342-03.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173827

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 94 75 - 125

Toluene-d8 (Surr) 100 75 - 120

4-Bromofluorobenzene (Surr) 90 75 - 120

Dibromofluoromethane 96 75 - 120

TestAmerica Chicago Page 16 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

Trip Blank

Client Matrix:

500-53342-4

Water

Date Sampled: 12/17/2012 0000

Date Received: 12/18/2012 0940

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/24/2012 1359

12/24/2012 1359

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53342-04.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173827

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 95 75 - 125

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 92 75 - 120

Dibromofluoromethane 96 75 - 120

TestAmerica Chicago Page 17 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix: % Moisture: 70.0

500-53342-1

Solid

Date Sampled: 12/17/2012 1450

Date Received: 12/18/2012 0940

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51219A

Dilution: 1.0 Initial Weight/Volume: 1.1079 g

12/19/2012 1339 Final Weight/Volume: 100 mL

12/18/2012 1600

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173517

Prep Batch: 500-173339

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 409 0.358 3.01

Copper 693 0.815 3.01

Chromium 14200 0.502 3.01

Nickel 77.4 B 0.659 3.01

Lead 250 B 0.517 1.50

Vanadium 238 0.228 1.50

Zinc 441 2.06 6.02

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51219B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/19/2012 2241 Final Weight/Volume: 50 mL

12/19/2012 0820

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173518

500-173406

500-173323

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/18/2012 1400

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium 0.166 0.0100 0.0250

Nickel 0.531 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium 0.00669 J 0.00500 0.0250

Zinc 0.0502 J 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 122012R.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/20/2012 0942 Final Weight/Volume: 25 mL

12/19/2012 1400

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173572

500-173428

500-173323

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/18/2012 1400

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 18 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix: % Moisture: 70.0

500-53342-1

Solid

Date Sampled: 12/17/2012 1450

Date Received: 12/18/2012 0940

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 122012B.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6182 g

12/20/2012 1021 Final Weight/Volume: 50 mL

12/19/2012 1445

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-173574

Prep Batch: 500-173393

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.321 0.0206 0.0540

TestAmerica Chicago Page 19 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

Client Sample ID:

Lab Sample ID:

FC EB 5

Client Matrix:

500-53342-3

Water

Date Sampled: 12/17/2012 1430

Date Received: 12/18/2012 0940

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51219A

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/19/2012 1503 Final Weight/Volume: 50 mL

12/18/2012 1530

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173517

Prep Batch: 500-173349

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Barium <0.0100 0.000440 0.0100

Copper 0.00616 J 0.00106 0.0100

Chromium <0.0100 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead 0.00245 J B 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc 0.00789 J 0.00472 0.0200

7470A Mercury (CVAA)

7470A Instrument ID:

Lab File ID: 122012R.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/20/2012 1029 Final Weight/Volume: 25 mL

12/19/2012 1400

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173572

Prep Batch: 500-173428

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000710 0.000200

TestAmerica Chicago Page 20 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix:

500-53342-1

Solid

Date Sampled: 12/17/2012 1450

Date Received: 12/18/2012 0940

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-173625 Analysis Date (Start): 12/20/2012 1100 (End) 12/20/2012 1200 DryWt Corrected: N

Chromium, hexavalent <3.33 mg/Kg 1.30 3.33 1.0 7196A

Analysis Batch: 500-174027 Analysis Date (Start): 12/27/2012 1250 (End) 12/27/2012 1251 DryWt Corrected: Y

Prep Batch: 500-173790 Prep Date: 12/22/2012 1200

Cyanide, Total 0.905 J mg/Kg 0.524 1.59 1.0 9014

Analysis Batch: 500-174173 Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1531 DryWt Corrected: Y

Prep Batch: 500-174096 Prep Date: 12/28/2012 1120

Sulfide 798 mg/Kg 13.2 82.8 1.0 9034

Analysis Batch: 500-173474 Analysis Date: 12/19/2012 1338 DryWt Corrected: Y

Prep Batch: 500-173291 Prep Date: 12/19/2012 1125

Sulfide, Reactive <48.7 mg/Kg 3.80 48.7 1.0 9034

Analysis Batch: 500-173472 Analysis Date: 12/19/2012 1219 DryWt Corrected: N

Prep Batch: 500-173290 Prep Date: 12/19/2012 1050

pH 9.59 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173479 Analysis Date (Start): 12/20/2012 1710 (End) 12/20/2012 1810 DryWt Corrected: N

HEM (Oil & Grease) 13200 mg/Kg 732 1650 1.0 9071B

Analysis Batch: 500-173330 Analysis Date: 12/19/2012 1123 DryWt Corrected: Y

Prep Batch: 500-173324 Prep Date: 12/19/2012 0510

Percent Moisture 70 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173404 Analysis Date: 12/19/2012 0840 DryWt Corrected: N

Percent Solids 30 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173404 Analysis Date: 12/19/2012 0840 DryWt Corrected: N

% Moisture 70.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173229 Analysis Date: 12/18/2012 0957 DryWt Corrected: N

Total Solids 30.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173385 Analysis Date: 12/19/2012 0731 DryWt Corrected: N

TestAmerica Chicago Page 21 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC Composite 5

Client Matrix:

500-53342-2

Solid

Date Sampled: 12/17/2012 1440

Date Received: 12/18/2012 0940

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 73 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173667 Analysis Date: 12/21/2012 0720 DryWt Corrected: N

Percent Solids 27 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173667 Analysis Date: 12/21/2012 0720 DryWt Corrected: N

TestAmerica Chicago Page 22 of 332 01/04/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53342-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC EB 5

Client Matrix:

500-53342-3

Water

Date Sampled: 12/17/2012 1430

Date Received: 12/18/2012 0940

Analyte Result Qual Units MDL RL Dil Method

HEM (Oil & Grease) <5.36 mg/L 1.55 5.36 1.0 1664A

Analysis Batch: 500-173459 Analysis Date: 12/21/2012 1035

Prep Batch: 500-173450 Prep Date: 12/21/2012 0709

Chromium, hexavalent <0.0100 mg/L 0.00325 0.0100 1.0 7196A

Analysis Batch: 500-173293 Analysis Date (Start): 12/18/2012 1122 (End) 12/18/2012 1122

Cyanide, Total <0.0100 mg/L 0.00331 0.0100 1.0 9014

Analysis Batch: 500-174042 Analysis Date (Start): 12/27/2012 1444 (End) 12/27/2012 1444

Prep Batch: 500-173980 Prep Date: 12/27/2012 0950

Sulfide <1.00 mg/L 0.230 1.00 1.0 9034

Analysis Batch: 500-173846 Analysis Date (Start): 12/24/2012 1358 (End) 12/24/2012 1400

Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034

Analysis Batch: 500-173845 Analysis Date: 12/24/2012 1340

Prep Batch: 500-173844 Prep Date: 12/24/2012 0830

TestAmerica Chicago Page 23 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53342-2 FC Composite 5 111 112 100 83

MB 500-173515/4 103 106 113 107

LCS 500-173515/5 103 98 111 102

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

TestAmerica Chicago

Page 24 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53342-2 DL FC Composite 5 DL 95 94 96 86

MB 500-173708/6 88 90 97 88

LCS 500-173708/4 96 94 97 103

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 25 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Water

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53342-3 FC EB 5 96 94 100 90

500-53342-4 Trip Blank 96 95 99 92

MB 500-173827/6 92 90 96 88

LCS 500-173827/4 92 92 97 94

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 26 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173515

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16M1220.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173515/4 CMS16

Analysis Date: 12/20/2012 0900

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173515

Prep Date:

Leach Date:

12/20/2012 0900

N/A

Analyte Result Qual MDL RL

Acetone <5.00 2.16 5.00

2-Butanone (MEK) <5.00 1.81 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 106 70 - 134

Toluene-d8 (Surr) 113 75 - 122

4-Bromofluorobenzene (Surr) 107 70 - 122

Dibromofluoromethane 103 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-173515

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16S1220.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-173515/5 CMS16

Analysis Date: 12/20/2012 0923

Analysis Batch:

Prep Batch:

Leach Batch:

500-173515

N/A

N/A

Prep Date:

Leach Date:

12/20/2012 0923

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 43.68 87 50 - 138

2-Butanone (MEK) 50.0 45.67 91 58 - 133

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 98 70 - 134

Toluene-d8 (Surr) 111 75 - 122

4-Bromofluorobenzene (Surr) 102 70 - 122

Dibromofluoromethane 103 75 - 120

TestAmerica Chicago Page 27 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173708

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22M1221.D

Units: ug/Kg

Method: 8260B

Preparation: N/A

MB 500-173708/6 CMS22

Analysis Date: 12/21/2012 1316

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173708

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.30 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 90 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 88 75 - 120

Dibromofluoromethane 88 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-173708

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22S1221.D

Units: ug/Kg

Method: 8260B

Preparation: N/A

LCS 500-173708/4 CMS22

Analysis Date: 12/21/2012 1223

Analysis Batch:

Prep Batch:

Leach Batch:

500-173708

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 46.74 93 46 - 153

2-Butanone (MEK) 50.0 41.90 84 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 94 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 103 75 - 120

Dibromofluoromethane 96 75 - 120

TestAmerica Chicago Page 28 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173827

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22M1224.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173827/6 CMS22

Analysis Date: 12/24/2012 1333

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173827

Prep Date:

Leach Date:

12/24/2012 1333

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 90 75 - 125

Toluene-d8 (Surr) 96 75 - 120

4-Bromofluorobenzene (Surr) 88 75 - 120

Dibromofluoromethane 92 75 - 120

Water

1.0

Lab Control Sample - Batch: 500-173827

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22S1224.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-173827/4 CMS22

Analysis Date: 12/24/2012 1235

Analysis Batch:

Prep Batch:

Leach Batch:

500-173827

N/A

N/A

Prep Date:

Leach Date:

12/24/2012 1235

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 48.03 96 46 - 153

2-Butanone (MEK) 50.0 50.18 100 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 92 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 92 75 - 120

TestAmerica Chicago Page 29 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173339

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

MB 500-173339/1-A ICP5

Analysis Date: 12/19/2012 1033

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173517

500-173339

Prep Date:

Leach Date:

12/18/2012 1600

N/A

Analyte Result Qual MDL RL

Barium <1.00 0.119 1.00

Copper <1.00 0.271 1.00

Chromium <1.00 0.167 1.00

Nickel 0.3300 J 0.219 1.00

Lead 0.2580 J 0.172 0.500

Vanadium <0.500 0.0759 0.500

Zinc <2.00 0.686 2.00

Solid

1.0

Lab Control Sample - Batch: 500-173339

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

LCS 500-173339/2-A ICP5

Analysis Date: 12/19/2012 1039

Analysis Batch:

Prep Batch:

Leach Batch:

500-173517

500-173339

N/A

Prep Date:

Leach Date:

12/18/2012 1600

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 200 199.5 100 80 - 120

Copper 25.0 25.15 101 80 - 120

Chromium 20.0 20.20 101 80 - 120

Nickel 50.0 49.95 100 80 - 120

Lead 10.0 10.14 101 80 - 120

Vanadium 50.0 50.42 101 80 - 120

Zinc 50.0 49.15 98 80 - 120

TestAmerica Chicago Page 30 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173349

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

MB 500-173349/1-A ICP5

Analysis Date: 12/19/2012 1352

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173517

500-173349

Prep Date:

Leach Date:

12/18/2012 1530

N/A

Analyte Result Qual MDL RL

Barium 0.002710 J 0.000440 0.0100

Copper <0.0100 0.00106 0.0100

Chromium 0.001210 J 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead 0.002720 J 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

Water

1.0

Lab Control Sample - Batch: 500-173349

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173349/2-A ICP5

Analysis Date: 12/19/2012 1358

Analysis Batch:

Prep Batch:

Leach Batch:

500-173517

500-173349

N/A

Prep Date:

Leach Date:

12/18/2012 1530

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.955 98 80 - 120

Copper 0.250 0.2524 101 80 - 120

Chromium 0.200 0.1989 99 80 - 120

Nickel 0.500 0.4934 99 80 - 120

Lead 0.100 0.1010 101 80 - 120

Vanadium 0.500 0.4993 100 80 - 120

Zinc 0.500 0.4858 97 80 - 120

TestAmerica Chicago Page 31 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-173406

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

TCLP

LB2 500-173323/1-B ICP5

Analysis Date: 12/19/2012 2113

Analysis Batch:

Prep Batch:

Leach Batch: 500-173323

500-173518

500-173406

Prep Date:

Leach Date:

12/19/2012 0820

12/18/2012 1400

Analyte Result Qual MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel <0.0250 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

Water

1.0

Lab Control Sample - Batch: 500-173406

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173406/3-A ICP5

Analysis Date: 12/19/2012 2120

Analysis Batch:

Prep Batch:

Leach Batch:

500-173518

500-173406

N/A

Prep Date:

Leach Date:

12/19/2012 0820

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.975 99 80 - 120

Copper 0.250 0.2464 99 80 - 120

Chromium 0.200 0.1969 98 80 - 120

Nickel 0.500 0.4873 97 80 - 120

Lead 0.100 0.09785 98 80 - 120

Vanadium 0.500 0.4959 99 80 - 120

Zinc 0.500 0.4782 96 80 - 120

TestAmerica Chicago Page 32 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173428

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122012R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-173428/7-A HG6

Analysis Date: 12/20/2012 0932

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173572

500-173428

Prep Date:

Leach Date:

12/19/2012 1400

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000200 0.000200

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-173428

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122012R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

LB2 500-173323/1-C HG6

Analysis Date: 12/20/2012 0940

Analysis Batch:

Prep Batch:

Leach Batch: 500-173323

500-173572

500-173428

Prep Date:

Leach Date:

12/19/2012 1400

12/18/2012 1400

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000200 0.000200

Water

1.0

Lab Control Sample - Batch: 500-173428

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122012R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-173428/8-A HG6

Analysis Date: 12/20/2012 0938

Analysis Batch:

Prep Batch:

Leach Batch:

500-173572

500-173428

N/A

Prep Date:

Leach Date:

12/19/2012 1400

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002086 104 80 - 120

TestAmerica Chicago Page 33 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173393

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122012A.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

MB 500-173393/7-A HG5

Analysis Date: 12/20/2012 0916

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173573

500-173393

Prep Date:

Leach Date:

12/19/2012 1445

N/A

Analyte Result Qual MDL RL

Mercury <0.0167 0.00637 0.0167

Solid

1.0

Lab Control Sample - Batch: 500-173393

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122012A.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

LCS 500-173393/8-A HG5

Analysis Date: 12/20/2012 0918

Analysis Batch:

Prep Batch:

Leach Batch:

500-173573

500-173393

N/A

Prep Date:

Leach Date:

12/19/2012 1445

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.167 0.1467 88 80 - 120

TestAmerica Chicago Page 34 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173450

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

MB 500-173450/1-A No Equipment 

Analysis Date: 12/21/2012 0955

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173459

500-173450

Prep Date:

Leach Date:

12/21/2012 0505

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <5.00 1.45 5.00

Water

1.0

Lab Control Sample - Batch: 500-173450

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

LCS 500-173450/2-A No Equipment 

Analysis Date: 12/21/2012 0958

Analysis Batch:

Prep Batch:

Leach Batch:

500-173459

500-173450

N/A

Prep Date:

Leach Date:

12/21/2012 0516

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 40.0 36.70 92 78 - 114

TestAmerica Chicago Page 35 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173293

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 7196A

Preparation: N/A

N/A

MB 500-173293/3 SPEC5

Analysis Date: 12/18/2012 1121

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173293

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <0.0100 0.00325 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173293

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 7196A

Preparation: N/A

N/A

LCS 500-173293/4 SPEC5

Analysis Date: 12/18/2012 1121

Analysis Batch:

Prep Batch:

Leach Batch:

500-173293

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 0.250 0.2652 106 85 - 115

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

Method: 7196A

Preparation: N/A

N/A

N/A

SPEC5

SPEC5

500-53342-3

500-53342-3

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173293

12/18/2012 1122

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173293

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1123

N/A

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173293

N/A

N/A

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Chromium, hexavalent 100 102 85 - 115 2 20

TestAmerica Chicago Page 36 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Water

12/18/2012 1122 12/18/2012 1123

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 7196A

Preparation: N/A

MS Lab Sample ID: 500-53342-3 Units: mg/L MSD Lab Sample ID: 500-53342-3

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173293

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Chromium, hexavalent <0.0100 0.250 0.250 0.2502 0.2555

TestAmerica Chicago Page 37 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173790

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

MB 500-173790/1-A SPEC5

Analysis Date: 12/27/2012 1241

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174027

500-173790

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <1.00 0.389 1.00

Solid

1.0

Lab Control Sample - Batch: 500-173790

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173790/2-A SPEC5

Analysis Date: 12/27/2012 1242

Analysis Batch:

Prep Batch:

Leach Batch:

500-174027

500-173790

N/A

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 10.0 9.188 92 80 - 120

Solid

50

Lab Control Sample - Batch: 500-173790

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173790/3-A SPEC5

Analysis Date: 12/27/2012 1242

Analysis Batch:

Prep Batch:

Leach Batch:

500-174027

500-173790

N/A

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 676 669.0 99 80 - 120

TestAmerica Chicago Page 38 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173980

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-173980/1-A SPEC5

Analysis Date: 12/27/2012 1440

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174042

500-173980

Prep Date:

Leach Date:

12/27/2012 0950

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.0100 0.00331 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173980

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-173980/2-A SPEC5

Analysis Date: 12/27/2012 1440

Analysis Batch:

Prep Batch:

Leach Batch:

500-174042

500-173980

N/A

Prep Date:

Leach Date:

12/27/2012 0950

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 0.100 0.1066 107 80 - 120

TestAmerica Chicago Page 39 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174096

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-174096/12-A SPEC5

Analysis Date: 12/28/2012 1530

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174173

500-174096

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.500 0.165 0.500

Solid

1.0

Lab Control Sample - Batch: 500-174096

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-174096/13-A SPEC5

Analysis Date: 12/28/2012 1530

Analysis Batch:

Prep Batch:

Leach Batch:

500-174173

500-174096

N/A

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 5.00 5.325 107 80 - 120

TestAmerica Chicago Page 40 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173290

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-173290/1-A No Equipment 

Analysis Date: 12/19/2012 1215

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173472

500-173290

Prep Date:

Leach Date:

12/19/2012 1005

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <50.0 3.90 50.0

Solid

1.0

Lab Control Sample - Batch: 500-173290

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-173290/2-A No Equipment 

Analysis Date: 12/19/2012 1215

Analysis Batch:

Prep Batch:

Leach Batch:

500-173472

500-173290

N/A

Prep Date:

Leach Date:

12/19/2012 1010

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 180 168.6 94 80 - 120

TestAmerica Chicago Page 41 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173291

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

MB 500-173291/1-A No Equipment 

Analysis Date: 12/19/2012 1335

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173474

500-173291

Prep Date:

Leach Date:

12/19/2012 1125

N/A

Analyte Result Qual MDL RL

Sulfide <25.0 4.00 25.0

Solid

1.0

Lab Control Sample - Batch: 500-173291

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

LCS 500-173291/2-A No Equipment 

Analysis Date: 12/19/2012 1335

Analysis Batch:

Prep Batch:

Leach Batch:

500-173474

500-173291

N/A

Prep Date:

Leach Date:

12/19/2012 1125

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 180 168.3 93 80 - 120

TestAmerica Chicago Page 42 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173844

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-173844/1-A No Equipment 

Analysis Date: 12/24/2012 1319

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173845

500-173844

Prep Date:

Leach Date:

12/24/2012 0800

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <1.00 1.00 1.00

Water

1.0

Lab Control Sample - Batch: 500-173844

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-173844/2-A No Equipment 

Analysis Date: 12/24/2012 1329

Analysis Batch:

Prep Batch:

Leach Batch:

500-173845

500-173844

N/A

Prep Date:

Leach Date:

12/24/2012 0815

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 3.60 3.767 105 80 - 120

TestAmerica Chicago Page 43 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173846

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 9034

Preparation: N/A

N/A

MB 500-173846/1 No Equipment 

Analysis Date: 12/24/2012 1319

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173846

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Sulfide <1.00 0.230 1.00

Water

1.0

Lab Control Sample - Batch: 500-173846

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 9034

Preparation: N/A

N/A

LCS 500-173846/2 No Equipment 

Analysis Date: 12/24/2012 1320

Analysis Batch:

Prep Batch:

Leach Batch:

500-173846

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 3.60 3.760 104 80 - 120

TestAmerica Chicago Page 44 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173324

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

MB 500-173324/1-A No Equipment 

Analysis Date: 12/19/2012 0920

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173330

500-173324

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <500 222 500

Solid

1.0

Lab Control Sample - Batch: 500-173324

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

LCS 500-173324/2-A No Equipment 

Analysis Date: 12/19/2012 0931

Analysis Batch:

Prep Batch:

Leach Batch:

500-173330

500-173324

N/A

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 4000 4090 102 80 - 120

TestAmerica Chicago Page 45 of 332 01/04/2013
DATA REPORTING QUALIFIERS

Client: Project Integration, Inc Job Number: 500-53342-1

Lab Section Qualifier Description

Metals

B Compound was found in the blank and sample.

ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: 

Instrument related QC exceeds the control limits. ^ Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

General Chemistry

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

TestAmerica Chicago Page 46 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA

Prep Batch: 500-173454

500-53342-2DL FC Composite 5 T Solid 5030B

Analysis Batch:500-173515

LCS 500-173515/5 Lab Control Sample T Solid 8260B

MB 500-173515/4 Method Blank T Solid 8260B

500-53342-2 FC Composite 5 T Solid 8260B

Analysis Batch:500-173708

LCS 500-173708/4 Lab Control Sample T Solid 8260B

MB 500-173708/6 Method Blank T Solid 8260B

500-53342-2DL FC Composite 5 T Solid 8260B 500-173454

Analysis Batch:500-173827

LCS 500-173827/4 Lab Control Sample T Water 8260B

MB 500-173827/6 Method Blank T Water 8260B

500-53342-3 FC EB 5 T Water 8260B

500-53342-4 Trip Blank T Water 8260B

Report Basis

T = Total

TestAmerica Chicago

Page 47 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 500-173323

LB2 500-173323/1-B TCLP SPLPW Leachate Blank P Solid 1311

LB2 500-173323/1-C TCLP SPLPW Leachate Blank P Solid 1311

500-53342-1 FC Composite 5 P Solid 1311

Prep Batch: 500-173339

LCS 500-173339/2-A Lab Control Sample T Solid 3050B

MB 500-173339/1-A Method Blank T Solid 3050B

500-53342-1 FC Composite 5 T Solid 3050B

Prep Batch: 500-173349

LCS 500-173349/2-A Lab Control Sample T Water 3010A

MB 500-173349/1-A Method Blank T Water 3010A

500-53342-3 FC EB 5 T Water 3010A

Prep Batch: 500-173393

LCS 500-173393/8-A Lab Control Sample T Solid 7471A

MB 500-173393/7-A Method Blank T Solid 7471A

500-53342-1 FC Composite 5 T Solid 7471A

Prep Batch: 500-173406

LCS 500-173406/3-A Lab Control Sample T Water 3010A

LB2 500-173323/1-B TCLP SPLPW Leachate Blank P Solid 3010A 500-173323

500-53342-1 FC Composite 5 P Solid 3010A 500-173323

Prep Batch: 500-173428

LCS 500-173428/8-A Lab Control Sample T Water 7470A

MB 500-173428/7-A Method Blank T Water 7470A

LB2 500-173323/1-C TCLP SPLPW Leachate Blank P Solid 7470A 500-173323

500-53342-1 FC Composite 5 P Solid 7470A 500-173323

500-53342-3 FC EB 5 T Water 7470A

Analysis Batch:500-173517

LCS 500-173339/2-A Lab Control Sample T Solid 6010B 500-173339

MB 500-173339/1-A Method Blank T Solid 6010B 500-173339

LCS 500-173349/2-A Lab Control Sample T Water 6010B 500-173349

MB 500-173349/1-A Method Blank T Water 6010B 500-173349

500-53342-1 FC Composite 5 T Solid 6010B 500-173339

500-53342-3 FC EB 5 T Water 6010B 500-173349

Analysis Batch:500-173518

LB2 500-173323/1-B TCLP SPLPW Leachate Blank P Solid 6010B 500-173406

LCS 500-173406/3-A Lab Control Sample T Water 6010B 500-173406

500-53342-1 FC Composite 5 P Solid 6010B 500-173406

TestAmerica Chicago

Page 48 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Analysis Batch:500-173572

LB2 500-173323/1-C TCLP SPLPW Leachate Blank P Solid 7470A 500-173428

LCS 500-173428/8-A Lab Control Sample T Water 7470A 500-173428

MB 500-173428/7-A Method Blank T Water 7470A 500-173428

500-53342-1 FC Composite 5 P Solid 7470A 500-173428

500-53342-3 FC EB 5 T Water 7470A 500-173428

Analysis Batch:500-173573

LCS 500-173393/8-A Lab Control Sample T Solid 7471A 500-173393

MB 500-173393/7-A Method Blank T Solid 7471A 500-173393

Analysis Batch:500-173574

500-53342-1 FC Composite 5 T Solid 7471A 500-173393

Report Basis

P = TCLP

T = Total

TestAmerica Chicago

Page 49 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-173229

500-53342-1 FC Composite 5 T Solid SM 2540G

Prep Batch: 500-173290

LCS 500-173290/2-A Lab Control Sample T Solid 7.3.4

MB 500-173290/1-A Method Blank T Solid 7.3.4

500-53342-1 FC Composite 5 T Solid 7.3.4

Prep Batch: 500-173291

LCS 500-173291/2-A Lab Control Sample T Solid 9030B

MB 500-173291/1-A Method Blank T Solid 9030B

500-53342-1 FC Composite 5 T Solid 9030B

Analysis Batch:500-173293

LCS 500-173293/4 Lab Control Sample T Water 7196A

MB 500-173293/3 Method Blank T Water 7196A

500-53342-3 FC EB 5 T Water 7196A

500-53342-3MS Matrix Spike T Water 7196A

500-53342-3MSD Matrix Spike Duplicate T Water 7196A

Prep Batch: 500-173324

LCS 500-173324/2-A Lab Control Sample T Solid 9071B

MB 500-173324/1-A Method Blank T Solid 9071B

500-53342-1 FC Composite 5 T Solid 9071B

Analysis Batch:500-173330

LCS 500-173324/2-A Lab Control Sample T Solid 9071B 500-173324

MB 500-173324/1-A Method Blank T Solid 9071B 500-173324

500-53342-1 FC Composite 5 T Solid 9071B 500-173324

Analysis Batch:500-173385

500-53342-1 FC Composite 5 T Solid SM 2540G

Analysis Batch:500-173404

500-53342-1 FC Composite 5 T Solid Moisture

Prep Batch: 500-173450

LCS 500-173450/2-A Lab Control Sample T Water 1664A

MB 500-173450/1-A Method Blank T Water 1664A

500-53342-3 FC EB 5 T Water 1664A

Analysis Batch:500-173459

LCS 500-173450/2-A Lab Control Sample T Water 1664A 500-173450

MB 500-173450/1-A Method Blank T Water 1664A 500-173450

500-53342-3 FC EB 5 T Water 1664A 500-173450

TestAmerica Chicago

Page 50 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-173472

LCS 500-173290/2-A Lab Control Sample T Solid 9034 500-173290

MB 500-173290/1-A Method Blank T Solid 9034 500-173290

500-53342-1 FC Composite 5 T Solid 9034 500-173290

Analysis Batch:500-173474

LCS 500-173291/2-A Lab Control Sample T Solid 9034 500-173291

MB 500-173291/1-A Method Blank T Solid 9034 500-173291

500-53342-1 FC Composite 5 T Solid 9034 500-173291

Analysis Batch:500-173479

500-53342-1 FC Composite 5 T Solid 9045C

Analysis Batch:500-173625

500-53342-1 FC Composite 5 T Solid 1010

Analysis Batch:500-173667

500-53342-2 FC Composite 5 T Solid Moisture

Prep Batch: 500-173790

LCS 500-173790/2-A Lab Control Sample T Solid 3060A

LCS 500-173790/3-A Lab Control Sample T Solid 3060A

MB 500-173790/1-A Method Blank T Solid 3060A

500-53342-1 FC Composite 5 T Solid 3060A

Prep Batch: 500-173844

LCS 500-173844/2-A Lab Control Sample T Water 7.3.4

MB 500-173844/1-A Method Blank T Water 7.3.4

500-53342-3 FC EB 5 T Water 7.3.4

Analysis Batch:500-173845

LCS 500-173844/2-A Lab Control Sample T Water 9034 500-173844

MB 500-173844/1-A Method Blank T Water 9034 500-173844

500-53342-3 FC EB 5 T Water 9034 500-173844

Analysis Batch:500-173846

LCS 500-173846/2 Lab Control Sample T Water 9034

MB 500-173846/1 Method Blank T Water 9034

500-53342-3 FC EB 5 T Water 9034

Prep Batch: 500-173980

LCS 500-173980/2-A Lab Control Sample T Water 9010B

MB 500-173980/1-A Method Blank T Water 9010B

500-53342-3 FC EB 5 T Water 9010B

TestAmerica Chicago

Page 51 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-174027

LCS 500-173790/2-A Lab Control Sample T Solid 7196A 500-173790

LCS 500-173790/3-A Lab Control Sample T Solid 7196A 500-173790

MB 500-173790/1-A Method Blank T Solid 7196A 500-173790

500-53342-1 FC Composite 5 T Solid 7196A 500-173790

Analysis Batch:500-174042

LCS 500-173980/2-A Lab Control Sample T Water 9014 500-173980

MB 500-173980/1-A Method Blank T Water 9014 500-173980

500-53342-3 FC EB 5 T Water 9014 500-173980

Prep Batch: 500-174096

LCS 500-174096/13-A Lab Control Sample T Solid 9010B

MB 500-174096/12-A Method Blank T Solid 9010B

500-53342-1 FC Composite 5 T Solid 9010B

Analysis Batch:500-174173

LCS 500-174096/13-A Lab Control Sample T Solid 9014 500-174096

MB 500-174096/12-A Method Blank T Solid 9014 500-174096

500-53342-1 FC Composite 5 T Solid 9014 500-174096

Report Basis

T = Total

TestAmerica Chicago

Page 52 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Laboratory Chronicle

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 14:50 Received Date/Time: 500-53342-1 FC Composite 5

P:3050B 500-53342-A-1-E 500-173517 500-173339 12/18/2012 16:00 1 TAL CHI RL

A:6010B 500-53342-A-1-E 500-173517 500-173339 12/19/2012 13:39 1 TAL CHI TDS

P:3010A 500-53342-A-1-F 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B 500-53342-A-1-F 500-173518 500-173406 12/19/2012 22:41 1 TAL CHI TDS

P:7470A 500-53342-A-1-H 500-173572 500-173428 12/19/2012 14:00 1 TAL CHI BJB

A:7470A 500-53342-A-1-H 500-173572 500-173428 12/20/2012 09:42 1 TAL CHI BJB

P:7471A 500-53342-A-1-G 500-173574 500-173393 12/19/2012 14:45 1 TAL CHI BJB

A:7471A 500-53342-A-1-G 500-173574 500-173393 12/20/2012 10:21 1 TAL CHI BJB

A:1010 500-53342-A-1 500-173625 12/20/2012 11:00 1 TAL CHI APW

P:3060A 500-53342-A-1-I 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A 500-53342-A-1-I 500-174027 500-173790 12/27/2012 12:50 1 TAL CHI APW

P:9010B 500-53342-A-1-J 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 500-53342-A-1-J 500-174173 500-174096 12/28/2012 15:31 1 TAL CHI EAT

P:7.3.4 500-53342-A-1-A 500-173472 500-173290 12/19/2012 10:50 1 TAL CHI CLM

A:9034 500-53342-A-1-A 500-173472 500-173290 12/19/2012 12:19 1 TAL CHI CLM

P:9030B 500-53342-A-1-B 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 500-53342-A-1-B 500-173474 500-173291 12/19/2012 13:38 1 TAL CHI CLM

A:9045C 500-53342-A-1 500-173479 12/20/2012 17:10 1 TAL CHI CLM

P:9071B 500-53342-A-1-D 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B 500-53342-A-1-D 500-173330 500-173324 12/19/2012 11:23 1 TAL CHI MTB

A:Moisture 500-53342-A-1 500-173404 12/19/2012 08:40 1 TAL CHI CMV

A:SM 2540G 500-53342-A-1 500-173229 12/18/2012 09:57 1 TAL CHI CMV

A:SM 2540G 500-53342-A-1 500-173385 12/19/2012 07:31 1 TAL CHI CMV

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 14:40 Received Date/Time: 500-53342-2 FC Composite 5

P:5030B 500-53342-A-2 500-173515 12/20/2012 13:52 1 TAL CHI BDW

A:8260B 500-53342-A-2 500-173515 12/20/2012 13:52 1 TAL CHI BDW

P:5030B 500-53342-A-2-A DL 500-173708 500-173454 12/19/2012 13:00 50 TAL CHI WRE

A:8260B 500-53342-A-2-A DL 500-173708 500-173454 12/21/2012 22:40 50 TAL CHI EA

A:Moisture 500-53342-A-2 500-173667 12/21/2012 07:20 1 TAL CHI CMV

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 53 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Laboratory Chronicle

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 14:30 Received Date/Time: 500-53342-3 FC EB 5

P:5030B 500-53342-A-3 500-173827 12/24/2012 14:25 1 TAL CHI EA

A:8260B 500-53342-A-3 500-173827 12/24/2012 14:25 1 TAL CHI EA

P:3010A 500-53342-E-3-A 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B 500-53342-E-3-A 500-173517 500-173349 12/19/2012 15:03 1 TAL CHI TDS

P:7470A 500-53342-E-3-B 500-173572 500-173428 12/19/2012 14:00 1 TAL CHI BJB

A:7470A 500-53342-E-3-B 500-173572 500-173428 12/20/2012 10:29 1 TAL CHI BJB

P:1664A 500-53342-H-3-A 500-173459 500-173450 12/21/2012 07:09 1 TAL CHI MTB

A:1664A 500-53342-H-3-A 500-173459 500-173450 12/21/2012 10:35 1 TAL CHI MTB

A:7196A 500-53342-F-3 500-173293 12/18/2012 11:22 1 TAL CHI KD

P:9010B 500-53342-D-3-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 500-53342-D-3-A 500-174042 500-173980 12/27/2012 14:44 1 TAL CHI EAT

P:7.3.4 500-53342-G-3-A 500-173845 500-173844 12/24/2012 08:30 1 TAL CHI CLB

A:9034 500-53342-G-3-A 500-173845 500-173844 12/24/2012 13:40 1 TAL CHI CLB

A:9034 500-53342-G-3 500-173846 12/24/2012 13:58 1 TAL CHI CLB

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 14:30 Received Date/Time: 500-53342-3 MS FC EB 5

A:7196A 500-53342-F-3 MS 500-173293 12/18/2012 11:22 1 TAL CHI KD

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 14:30 Received Date/Time: 500-53342-3 MSD FC EB 5

A:7196A 500-53342-F-3 MSD 500-173293 12/18/2012 11:23 1 TAL CHI KD

12/18/2012 09:40

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/17/2012 00:00 Received Date/Time: 500-53342-4 Trip Blank

P:5030B 500-53342-A-4 500-173827 12/24/2012 13:59 1 TAL CHI EA

A:8260B 500-53342-A-4 500-173827 12/24/2012 13:59 1 TAL CHI EA

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 54 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

P:5030B MB 500-173515/4 500-173515 12/20/2012 09:00 1 TAL CHI BDW

A:8260B MB 500-173515/4 500-173515 12/20/2012 09:00 1 TAL CHI BDW

A:8260B MB 500-173708/6 500-173708 12/21/2012 13:16 1 TAL CHI EA

P:5030B MB 500-173827/6 500-173827 12/24/2012 13:33 1 TAL CHI EA

A:8260B MB 500-173827/6 500-173827 12/24/2012 13:33 1 TAL CHI EA

P:3050B MB 500-173339/1-A 500-173517 500-173339 12/18/2012 16:00 1 TAL CHI RL

A:6010B MB 500-173339/1-A 500-173517 500-173339 12/19/2012 10:33 1 TAL CHI TDS

P:3010A MB 500-173349/1-A 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B MB 500-173349/1-A 500-173517 500-173349 12/19/2012 13:52 1 TAL CHI TDS

P:7470A MB 500-173428/7-A 500-173572 500-173428 12/19/2012 14:00 1 TAL CHI BJB

A:7470A MB 500-173428/7-A 500-173572 500-173428 12/20/2012 09:32 1 TAL CHI BJB

P:7471A MB 500-173393/7-A 500-173573 500-173393 12/19/2012 14:45 1 TAL CHI BJB

A:7471A MB 500-173393/7-A 500-173573 500-173393 12/20/2012 09:16 1 TAL CHI BJB

P:1664A MB 500-173450/1-A 500-173459 500-173450 12/21/2012 05:05 1 TAL CHI MTB

A:1664A MB 500-173450/1-A 500-173459 500-173450 12/21/2012 09:55 1 TAL CHI MTB

A:7196A MB 500-173293/3 500-173293 12/18/2012 11:21 1 TAL CHI KD

P:3060A MB 500-173790/1-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A MB 500-173790/1-A 500-174027 500-173790 12/27/2012 12:41 1 TAL CHI APW

P:9010B MB 500-173980/1-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 MB 500-173980/1-A 500-174042 500-173980 12/27/2012 14:40 1 TAL CHI EAT

P:9010B MB 500-174096/12-A 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 MB 500-174096/12-A 500-174173 500-174096 12/28/2012 15:30 1 TAL CHI EAT

P:7.3.4 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 10:05 1 TAL CHI CLM

A:9034 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 12:15 1 TAL CHI CLM

P:9030B MB 500-173291/1-A 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 MB 500-173291/1-A 500-173474 500-173291 12/19/2012 13:35 1 TAL CHI CLM

P:7.3.4 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 08:00 1 TAL CHI CLB

A:9034 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 13:19 1 TAL CHI CLB

A:9034 MB 500-173846/1 500-173846 12/24/2012 13:19 1 TAL CHI CLB

P:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 09:20 1 TAL CHI MTB

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LB2 N/A

P:3010A LB2 500-173323/1-B 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B LB2 500-173323/1-B 500-173518 500-173406 12/19/2012 21:13 1 TAL CHI TDS

P:7470A LB2 500-173323/1-C 500-173572 500-173428 12/19/2012 14:00 1 TAL CHI BJB

A:7470A LB2 500-173323/1-C 500-173572 500-173428 12/20/2012 09:40 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 55 of 332 01/04/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53342-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCS N/A

P:5030B LCS 500-173515/5 500-173515 12/20/2012 09:23 1 TAL CHI BDW

A:8260B LCS 500-173515/5 500-173515 12/20/2012 09:23 1 TAL CHI BDW

A:8260B LCS 500-173708/4 500-173708 12/21/2012 12:23 1 TAL CHI EA

P:5030B LCS 500-173827/4 500-173827 12/24/2012 12:35 1 TAL CHI EA

A:8260B LCS 500-173827/4 500-173827 12/24/2012 12:35 1 TAL CHI EA

P:3050B LCS 500-173339/2-A 500-173517 500-173339 12/18/2012 16:00 1 TAL CHI RL

A:6010B LCS 500-173339/2-A 500-173517 500-173339 12/19/2012 10:39 1 TAL CHI TDS

P:3010A LCS 500-173349/2-A 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B LCS 500-173349/2-A 500-173517 500-173349 12/19/2012 13:58 1 TAL CHI TDS

P:3010A LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 21:20 1 TAL CHI TDS

P:7470A LCS 500-173428/8-A 500-173572 500-173428 12/19/2012 14:00 1 TAL CHI BJB

A:7470A LCS 500-173428/8-A 500-173572 500-173428 12/20/2012 09:38 1 TAL CHI BJB

P:7471A LCS 500-173393/8-A 500-173573 500-173393 12/19/2012 14:45 1 TAL CHI BJB

A:7471A LCS 500-173393/8-A 500-173573 500-173393 12/20/2012 09:18 1 TAL CHI BJB

P:1664A LCS 500-173450/2-A 500-173459 500-173450 12/21/2012 05:16 1 TAL CHI MTB

A:1664A LCS 500-173450/2-A 500-173459 500-173450 12/21/2012 09:58 1 TAL CHI MTB

A:7196A LCS 500-173293/4 500-173293 12/18/2012 11:21 1 TAL CHI KD

P:3060A LCS 500-173790/2-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A LCS 500-173790/2-A 500-174027 500-173790 12/27/2012 12:42 1 TAL CHI APW

P:3060A LCS 500-173790/3-A 500-174027 500-173790 12/22/2012 12:00 50 TAL CHI APW

A:7196A LCS 500-173790/3-A 500-174027 500-173790 12/27/2012 12:42 50 TAL CHI APW

P:9010B LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 14:40 1 TAL CHI EAT

P:9010B LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 15:30 1 TAL CHI EAT

P:7.3.4 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 10:10 1 TAL CHI CLM

A:9034 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 12:15 1 TAL CHI CLM

P:9030B LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 13:35 1 TAL CHI CLM

A:9034 LCS 500-173846/2 500-173846 12/24/2012 13:20 1 TAL CHI CLB

P:7.3.4 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 08:15 1 TAL CHI CLB

A:9034 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 13:29 1 TAL CHI CLB

P:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 09:31 1 TAL CHI MTB

Lab References:

TAL CHI = TestAmerica Chicago

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 56 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1664 HEM_00060 04/26/13 Mallin / JTBaker, Lot E50600 / K19H00 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L

SGT-HEM 4000 mg/L

8260 IS WK_00381 12/03/12 11/19/12 1, Lot NA 5 mL 8260 IS SK_00026 5 mL 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

.8260 IS SK_00026 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW IS_00104 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 IS SK_00027 4000 uL 1,4-Dichlorobenzene-d4 50 ug/mL

1,4-Difluorobenzene 50 ug/mL

Chlorobenzene-d5 50 ug/mL

Pentafluorobenzene 50 ug/mL

.8260 IS SK_00027 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW SS_00106 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 LOW SS_00107 12/27/12 12/13/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

.8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

Page 57 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

Page 58 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Page 59 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Page 60 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

Page 61 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Page 62 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

5 mL 8260 SS WK_00385 0.8656 1,2-Dichloroethane-d4 (Surr) 43.28 ug/L

uL

INST16 IS/SS_00223 01/01/13 12/18/12 1, Lot NA

4-Bromofluorobenzene (Surr) 43.28 ug/L

Dibromofluoromethane 43.28 ug/L

Toluene-d8 (Surr) 43.28 ug/L

.8260 SS WK_00385 01/01/13 12/18/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

Page 63 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

level 1_00011 12/31/16 03/20/12 1, Lot CY647 1 mL level1std5ppm_00006 100 uL Benzene 0.5 ug/mL

Ethylbenzene 0.5 ug/mL

m-Xylene & p-Xylene 1 ug/mL

o-Xylene 0.5 ug/mL

Toluene 0.5 ug/mL

Trichloroethene 0.5 ug/mL

Vinyl chloride 0.5 ug/mL

.level1std5ppm_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level18260wk_00006 100 uL Benzene 5 ug/mL

Ethylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

o-Xylene 5 ug/mL

Toluene 5 ug/mL

Trichloroethene 5 ug/mL

level1gaswk_00006 100 uL Vinyl chloride 5 ug/mL

..level18260wk_00006 06/30/12 03/22/11 1, Lot NA 1 mL level18260sk_00001 1 mL Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

...level18260sk_00001 06/30/12 Restek, Lot AO67921 (Purchased Reagent) Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

..level1gaswk_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level1gaspt_00005 100 uL Vinyl chloride 100 ug/mL

...level1gaspt_00005 02/28/12 03/22/11 MEOH, Lot NA 1 mL level1gassk_00001 1 mL Vinyl chloride 2000 ug/mL

....level1gassk_00001 02/28/12 SUPELCO, Lot LB65254 (Purchased Reagent) Vinyl chloride 2000 ug/mL

Page 64 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

LOW8260SS WK_00042 12/03/12 11/19/12 1, Lot DA057 1 mL 8260 SS WK_00378 200 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

LOW8260STD WK_00209 11/26/12 11/19/12 1, Lot DG596 1 mL 8260 STD WK_00212 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Page 65 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00244 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00180 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00175 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

Page 66 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

Page 67 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

Page 68 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOW8260STD WK_00215 12/18/12 12/11/12 1, Lot DG860 1 mL 8260 STD WK_00216 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

Page 69 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00254 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Page 70 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00184 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00179 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Page 71 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Page 72 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Page 73 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOWACRSTD WK_00189 11/26/12 11/19/12 MEOH, Lot DG596 1 mL ACR/NITRSTDWK_00205 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

LOWACRSTD WK_00193 12/18/12 12/11/12 MEOH, Lot DG860 1 mL ACR/NITRSTDWK_00212 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

M11FSTKHG_00001 05/31/17 ULTRA, Lot L00365 (Purchased Reagent) Mercury 1000 ug/mL

M12ASTKHG_00001 01/01/13 Inorganic Ventures, Lot E2-HG02091 (Purchased Reagent) Mercury 1000 ug/mL

M12JSPKIC_00002 05/23/13 10/04/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Page 74 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Page 75 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12KSPKIC_00001 05/23/13 11/20/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

Page 76 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12LCCVIC_00001 07/10/13 12/10/12 1, Lot N/A 1000 mL M12GSTKIC_00002 10 mL Barium 0.5 ug/mL

Chromium 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.5 ug/mL

Nickel 0.5 ug/mL

Vanadium 5 ug/mL

Zinc 0.5 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Page 77 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Zinc 50 ug/mL

M12LCRIIC_00001 06/01/13 12/03/12 1, Lot NA 1000 mL M12ESTKIC_00002 2 mL Barium 20 ug/L

Chromium 20 ug/L

Copper 20 ug/L

Lead 10 ug/L

Nickel 20 ug/L

Vanadium 10 ug/L

Zinc 40 ug/L

.M12ESTKIC_00002 06/01/13 IV, Lot F2-MEB423074 (Purchased Reagent) Barium 10 ug/mL

Chromium 10 ug/mL

Copper 10 ug/mL

Lead 5 ug/mL

Nickel 10 ug/mL

Vanadium 5 ug/mL

Zinc 20 ug/mL

M12LICVIC_00001 07/10/13 12/06/12 1, Lot N/A 1000 mL M12GSTKIC_00002 8 mL Barium 0.4 ug/mL

Chromium 0.4 ug/mL

Copper 0.4 ug/mL

Lead 0.4 ug/mL

Nickel 0.4 ug/mL

Vanadium 4 ug/mL

Zinc 0.4 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LISAIC_00001 12/01/13 12/03/12 1, Lot na 1000 mL M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

M12LISBIC_00001 09/01/13 12/03/12 1, Lot B51037 1000 mL M12ISTKIC_00003 10 mL Ag 0.2 ug/mL

As 0.1 ug/mL

Barium 0.5 ug/mL

Be 0.5 ug/mL

Cd 1 ug/mL

Chromium 0.5 ug/mL

Co 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.05 ug/mL

Page 78 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Mn 0.5 ug/mL

Nickel 1 ug/mL

Sb 0.6 ug/mL

Se 0.05 ug/mL

Tl 0.1 ug/mL

Vanadium 0.5 ug/mL

Zinc 1 ug/mL

M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12ISTKIC_00003 09/01/13 IV, Lot E2-MEB399019 (Purchased Reagent) Ag 20 ug/mL

As 10 ug/mL

Barium 50 ug/mL

Be 50 ug/mL

Cd 100 ug/mL

Chromium 50 ug/mL

Co 50 ug/mL

Copper 50 ug/mL

Lead 5 ug/mL

Mn 50 ug/mL

Nickel 100 ug/mL

Sb 60 ug/mL

Se 5 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 100 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VOC/THF SPK_00124 12/03/12 11/19/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

Page 79 of 332 01/04/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00127 12/25/12 12/11/12 1, Lot DG860 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

WSTCR1_00008 04/30/15 ERA, Lot 160412 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTCR13_00629 12/29/12 STL, Lot Lead(II)Chrom_00001 (Purchased Reagent) Chromium, hexavalent 16.9 mg/L

WSTCR2_00008 05/31/17 Ultra Scientific, Lot L00439 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTINCN1_00571 12/27/12 12/27/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN1_00572 12/28/12 12/28/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN2_00563 12/27/12 12/27/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTINCN2_00564 12/28/12 12/28/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTSF1_00036 11/15/13 NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL (Purchased Reagent) Sulfide 180 mg/L

Sulfide as H2S 209.1 mg/L

Sulfide, Reactive 180 mg/L

Page 80 of 332 01/04/2013
Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago Alabama State Program 4 40461

TestAmerica Chicago California NELAP 9 01132CA

TestAmerica Chicago Georgia State Program 4 939

TestAmerica Chicago Georgia State Program 4 N/A

TestAmerica Chicago Hawaii State Program 9 N/A

TestAmerica Chicago Illinois NELAP 5 100201

TestAmerica Chicago Indiana State Program 5 C-IL-02

TestAmerica Chicago Iowa State Program 7 82

TestAmerica Chicago Kansas NELAP 7 E-10161

TestAmerica Chicago Kentucky State Program 4 90023

TestAmerica Chicago Kentucky (UST) State Program 4 66

TestAmerica Chicago L-A-B DoD ELAP L2304

TestAmerica Chicago L-A-B ISO/IEC 17025 L2304

TestAmerica Chicago Louisiana NELAP 6 30720

TestAmerica Chicago Massachusetts State Program 1 M-IL035

TestAmerica Chicago Mississippi State Program 4 N/A

TestAmerica Chicago North Carolina DENR State Program 4 291

TestAmerica Chicago North Dakota State Program 8 R-194

TestAmerica Chicago Oklahoma State Program 6 8908

TestAmerica Chicago South Carolina State Program 4 77001

TestAmerica Chicago Texas NELAP 6 T104704252-09-TX

TestAmerica Chicago USDA Federal P330-12-00038

TestAmerica Chicago Virginia NELAP 3 460142

TestAmerica Chicago Wisconsin State Program 5 999580010

TestAmerica Chicago Wyoming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s 

current list of certified methods and analytes.

Page 81 of 332 TestAmerica Chicago 01/04/2013
Method 8260B

Volatile Organic Compounds (GC/MS) 

by Method 8260B

Page 82 of 332 01/04/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53342-1

SDG No.:

Matrix: Solid Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC Composite 5 500-53342-2 111 112 100 83

MB 500-173515/4 103 106 113 107

LCS 500-173515/5 103 98 111 102

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B

# Column to be used to flag recovery values

Page 83 of 332 01/04/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53342-1

SDG No.:

Matrix: Solid Level: Medium

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC Composite 5 DL 500-53342-2 DL 95 94 96 86

MB 500-173708/6 88 90 97 88

LCS 500-173708/4 96 94 97 103

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 84 of 332 01/04/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53342-1

SDG No.:

Matrix: Water Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC EB 5 500-53342-3 96 94 100 90

Trip Blank 500-53342-4 96 95 99 92

MB 500-173827/6 92 90 96 88

LCS 500-173827/4 92 92 97 94

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 85 of 332 01/04/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53342-1

Solid Lab File ID: 16S1220.D

Lab ID: LCS 500-173515/5 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 43.68 87 50-138

2-Butanone (MEK) 50.0 45.67 91 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 86 of 332 01/04/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Medium

500-53342-1

Solid Lab File ID: 22S1221.D

Lab ID: LCS 500-173708/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 46.74 93 46-153

2-Butanone (MEK) 50.0 41.90 84 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 87 of 332 01/04/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53342-1

Water Lab File ID: 22S1224.D

Lab ID: LCS 500-173827/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/L)

SPIKE

ADDED

(ug/L)

#

LCS LCS

COMPOUND

Acetone 50.0 48.03 96 46-153

2-Butanone (MEK) 50.0 50.18 100 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 88 of 332 01/04/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/21/2012 13:16

DB624

Heated Purge:(Y/N) N

CMS22

Lab File ID: 22M1221.D Lab Sample ID: MB 500-173708/6

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173708/4 22S1221.D 12/21/2012 12:23

FC Composite 5 DL 500-53342-2 DL 53342-02.D 12/21/2012 22:40

FORM IV 8260B

Page 89 of 332 01/04/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/20/2012 09:00

DB624

Heated Purge:(Y/N) Y

CMS16

Lab File ID: 16M1220.D Lab Sample ID: MB 500-173515/4

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173515/5 16S1220.D 12/20/2012 09:23

FC Composite 5 500-53342-2 53342-02.D 12/20/2012 13:52

FORM IV 8260B

Page 90 of 332 01/04/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53342-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/24/2012 13:33

DB624

Heated Purge:(Y/N) N

CMS22

Lab File ID: 22M1224.D Lab Sample ID: MB 500-173827/6

Matrix: Water

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173827/4 22S1224.D 12/24/2012 12:35

Trip Blank 500-53342-4 53342-04.D 12/24/2012 13:59

FC EB 5 500-53342-3 53342-03.D 12/24/2012 14:25

FORM IV 8260B

Page 91 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

16B1119c.D

CMS16

11/19/2012

11:14

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 170196

50 15.0 - 40.0 % of mass 95 19.7 

75 30.0 - 60.0 % of mass 95 53.5 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.7 (1.0)1

174 50.0 - 120.00 % of mass 95 75.9 

175 5.0 - 9.0 % of mass 174 5.3 (6.9)1

176 95.0 - 101.0 % of mass 174 74.4 (98.0)1

177 5.0 - 9.0 % of mass 176 5.8 (7.8)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-170196/6 16I1119A.D 11/19/2012 12:14

STD2 500-170196/7 16I1119B.D 11/19/2012 12:37

STD3 500-170196/8 16I1119C.D 11/19/2012 13:00

STD4 500-170196/9 16I1119D.D 11/19/2012 13:23

STD5 500-170196/10 16I1119E.D 11/19/2012 13:46

STD6 500-170196/11 16I1119F.D 11/19/2012 14:09

ICV 500-170196/19 16S1119.D 11/19/2012 17:14

FORM V 8260B Page 92 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

16B1220a.D

CMS16

12/20/2012

07:38

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173515

50 15.0 - 40.0 % of mass 95 21.7 

75 30.0 - 60.0 % of mass 95 47.1 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 8.2 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 79.5 

175 5.0 - 9.0 % of mass 174 5.2 (6.5)1

176 95.0 - 101.0 % of mass 174 77.5 (97.5)1

177 5.0 - 9.0 % of mass 176 5.2 (6.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173515/2 16C1220.D 12/20/2012 08:13

CCV 500-173515/3 16D1220.D 12/20/2012 08:36

MB 500-173515/4 16M1220.D 12/20/2012 09:00

LCS 500-173515/5 16S1220.D 12/20/2012 09:23

FC Composite 5 500-53342-2 53342-02.D 12/20/2012 13:52

FORM V 8260B Page 93 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

22B1211.D

CMS22

12/11/2012

13:45

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172614

50 15.0 - 40.0 % of mass 95 22.6 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 86.2 

175 5.0 - 9.0 % of mass 174 5.9 (6.8)1

176 95.0 - 101.0 % of mass 174 86.4 (100.2)1

177 5.0 - 9.0 % of mass 176 4.9 (5.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD01 500-172614/2 22I1211A.D 12/11/2012 14:23

STD02 500-172614/3 22I1211B.D 12/11/2012 14:51

STD03 500-172614/4 22I1211C.D 12/11/2012 15:20

STD04 500-172614/5 22I1211D.D 12/11/2012 15:48

STD05 500-172614/6 22I1211E.D 12/11/2012 16:16

STD06 500-172614/7 22I1211F.D 12/11/2012 16:44

STD07 500-172614/8 22I1211G.D 12/11/2012 17:13

STD08 500-172614/9 22I1211H.D 12/11/2012 17:41

STD09 500-172614/10 22I1211I.D 12/11/2012 18:09

ICV 500-172614/23 22S1211.D 12/12/2012 00:17

FORM V 8260B Page 94 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

22B1211.D

CMS22

12/11/2012

13:45

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172615

50 15.0 - 40.0 % of mass 95 22.6 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 86.2 

175 5.0 - 9.0 % of mass 174 5.9 (6.8)1

176 95.0 - 101.0 % of mass 174 86.4 (100.2)1

177 5.0 - 9.0 % of mass 176 4.9 (5.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD01 500-172615/2 22I1211A.D 12/11/2012 14:23

STD02 500-172615/3 22I1211B.D 12/11/2012 14:51

STD03 500-172615/4 22I1211C.D 12/11/2012 15:20

STD04 500-172615/5 22I1211D.D 12/11/2012 15:48

STD05 500-172615/6 22I1211E.D 12/11/2012 16:16

STD06 500-172615/7 22I1211F.D 12/11/2012 16:44

STD07 500-172615/8 22I1211G.D 12/11/2012 17:13

STD08 500-172615/9 22I1211H.D 12/11/2012 17:41

STD09 500-172615/10 22I1211I.D 12/11/2012 18:09

ICV 500-172615/23 22S1211.D 12/12/2012 00:17

FORM V 8260B Page 95 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

22B1221.D

CMS22

12/21/2012

10:53

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173708

50 15.0 - 40.0 % of mass 95 27.5 

75 30.0 - 60.0 % of mass 95 49.0 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 8.2 

173 Less than 2.0 % of mass 174 0.4 (0.4)1

174 50.0 - 120.00 % of mass 95 92.1 

175 5.0 - 9.0 % of mass 174 6.7 (7.3)1

176 95.0 - 101.0 % of mass 174 92.3 (100.3)1

177 5.0 - 9.0 % of mass 176 6.0 (6.5)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173708/2 22C1221.D 12/21/2012 11:31

CCV 500-173708/3 22D1221.D 12/21/2012 11:57

LCS 500-173708/4 22S1221.D 12/21/2012 12:23

MB 500-173708/6 22M1221.D 12/21/2012 13:16

FC Composite 5 DL 500-53342-2 DL 53342-02.D 12/21/2012 22:40

FORM V 8260B Page 96 of 332 01/04/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53342-1

Lab File ID:

Instrument ID:

22B1224.D

CMS22

12/24/2012

11:02

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173827

50 15.0 - 40.0 % of mass 95 24.4 

75 30.0 - 60.0 % of mass 95 44.1 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.8 

173 Less than 2.0 % of mass 174 1.9 (1.9)1

174 50.0 - 120.00 % of mass 95 101.2 

175 5.0 - 9.0 % of mass 174 9.0 (8.9)1

176 95.0 - 101.0 % of mass 174 97.2 (96.0)1

177 5.0 - 9.0 % of mass 176 5.2 (5.3)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173827/2 22C1224.D 12/24/2012 11:43

CCV 500-173827/3 22D1224.D 12/24/2012 12:09

LCS 500-173827/4 22S1224.D 12/24/2012 12:35

MB 500-173827/6 22M1224.D 12/24/2012 13:33

Trip Blank 500-53342-4 53342-04.D 12/24/2012 13:59

FC EB 5 500-53342-3 53342-03.D 12/24/2012 14:25

FORM V 8260B Page 97 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

464716

116179 170040

680160

134826

539304

INITIAL CALIBRATION MID-POINT 3.42 3.99 6.38

3.92

2.92

4.49

3.49

6.88

5.88

232358 340080 269652

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 258949 3.42 378895 3.99 285510 6.38

CCV 500-173515/2 306031 3.42 446450 3.99 343252 6.38

CCV 500-173515/3 299433 3.42 436791 3.99 334061 6.38

MB 500-173515/4 281103 3.42 405415 3.99 311525 6.38

LCS 500-173515/5 299125 3.42 434722 3.99 333232 6.38

500-53342-2 FC Composite 5 241093 3.42 359760 3.99 232539 6.38

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 98 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

283260

70815

INITIAL CALIBRATION MID-POINT 8.21

8.71

7.71

141630

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 139276 8.21

CCV 500-173515/2 162988 8.21

CCV 500-173515/3 161510 8.22

MB 500-173515/4 157163 8.21

LCS 500-173515/5 157933 8.21

500-53342-2 FC Composite 5 58638* 8.22

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 99 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD06 500-172614/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10829

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

1409738

352435 493044

1972176

417716

1670864

INITIAL CALIBRATION MID-POINT 6.27 7.24 10.64

6.77

5.77

7.74

6.74

11.14

10.14

704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172614/23 772269 6.26 1099840 7.24 931671 10.64

CCV 500-173708/2 687278 6.26 977657 7.24 817789 10.64

CCV 500-173708/3 687212 6.26 935438 7.24 801033 10.64

LCS 500-173708/4 680014 6.26 968230 7.24 803959 10.64

MB 500-173708/6 675524 6.26 913201 7.24 797068 10.64

500-53342-2 DL FC Composite 5 DL 553196 6.26 775796 7.24 655962 10.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 100 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD06 500-172614/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10829

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

1003186

250797

INITIAL CALIBRATION MID-POINT 13.08

13.58

12.58

501593

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172614/23 542063 13.08

CCV 500-173708/2 512733 13.08

CCV 500-173708/3 451000 13.07

LCS 500-173708/4 489137 13.08

MB 500-173708/6 423190 13.08

500-53342-2 DL FC Composite 5 DL 344276 13.07

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 101 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

1409738

352435 493044

1972176

417716

1670864

INITIAL CALIBRATION MID-POINT 6.27 7.24 10.64

6.77

5.77

7.74

6.74

11.14

10.14

704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 772269 6.26 1099840 7.24 931671 10.64

CCV 500-173827/2 690066 6.26 966119 7.24 829756 10.64

CCV 500-173827/3 718212 6.26 976330 7.24 827808 10.64

LCS 500-173827/4 678203 6.26 926614 7.24 799281 10.64

MB 500-173827/6 646307 6.26 901906 7.24 766183 10.64

500-53342-4 Trip Blank 670114 6.26 929055 7.24 794089 10.64

500-53342-3 FC EB 5 629756 6.27 877752 7.24 760147 10.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 102 of 332 01/04/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53342-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

1003186

250797

INITIAL CALIBRATION MID-POINT 13.08

13.58

12.58

501593

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 542063 13.08

CCV 500-173827/2 505828 13.07

CCV 500-173827/3 467889 13.08

LCS 500-173827/4 489029 13.08

MB 500-173827/6 424583 13.08

500-53342-4 Trip Blank 435535 13.08

500-53342-3 FC EB 5 410915 13.08

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 103 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Composite 5

SDG No.:

500-53342-1

Lab Sample ID: 500-53342-2

Matrix: Lab File ID: 53342-02.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/17/2012 14:40

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

73.1

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/20/2012 13:52

DB624 ID:

Analysis Batch No.: 173515 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 28.2 18.6 6.72

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 112 70-134

2037-26-5 Toluene-d8 (Surr) 100 75-122

460-00-4 4-Bromofluorobenzene (Surr) 83 70-122

1868-53-7 Dibromofluoromethane 111 75-120

FORM I 8260B

Page 104 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Composite 5 DL

SDG No.:

500-53342-1

Lab Sample ID: 500-53342-2 DL

Matrix: Lab File ID: 53342-02.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/17/2012 14:40

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

73.1

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/21/2012 22:40

DB624 ID:

Analysis Batch No.: 173708 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 3200 928 241

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 94 75-125

2037-26-5 Toluene-d8 (Surr) 96 75-120

460-00-4 4-Bromofluorobenzene (Surr) 86 75-120

1868-53-7 Dibromofluoromethane 95 75-120

FORM I 8260B

Page 105 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC EB 5

SDG No.:

500-53342-1

Lab Sample ID: 500-53342-3

Matrix: Lab File ID: 53342-03.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/17/2012 14:30

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/24/2012 14:25

DB624 ID:

Analysis Batch No.: 173827 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 94 75-125

2037-26-5 Toluene-d8 (Surr) 100 75-120

460-00-4 4-Bromofluorobenzene (Surr) 90 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 106 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

Trip Blank

SDG No.:

500-53342-1

Lab Sample ID: 500-53342-4

Matrix: Lab File ID: 53342-04.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/17/2012 00:00

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/24/2012 13:59

DB624 ID:

Analysis Batch No.: 173827 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-125

2037-26-5 Toluene-d8 (Surr) 99 75-120

460-00-4 4-Bromofluorobenzene (Surr) 92 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 107 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Dichlorodifluoromethane 0.5101 0.4328 0.4745 0.4472 0.4791 Ave 5.9

0.4553

0.4665 0.0100 15.0

Chloromethane 0.6409 0.5486 0.6042 0.5514 0.5726 Ave 6.2

0.5611

0.5798 0.1000 15.0

Vinyl chloride 0.5489 0.4879 0.5232 0.4889 0.5055 Ave 4.9

0.4889

0.5072 0.0100 15.0

Bromomethane 0.2173 0.1622 0.1619 0.1577 0.1599 Lin2 0.9990

0.1594

0.3023 0.1550 0.0100 0.9900

Chloroethane 0.2848 0.2512 0.2658 0.2550 0.2653 Ave 4.4

0.2627

0.2641 0.0100 15.0

Trichlorofluoromethane 0.6410 0.5479 0.5898 0.5813 0.5855 Ave 5.1

0.5792

0.5875 0.0100 15.0

Acrolein 0.0833 0.0649 0.0739 0.0632 0.0635 Lin2 0.9920

0.0576

4.1129 0.0627 0.0010 0.9900

1,1-Dichloroethene 0.3883 0.3810 0.3940 0.3681 0.3657 Ave 4.2

0.3520

0.3748 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.4271 0.3940 0.4076 0.3784 0.3788 Ave 6.6

0.3531

0.3898 0.0100 15.0

Acetone 0.2177 0.1065 0.1169 0.1078 0.1047 Lin1 0.9950

0.0952

0.5599 0.0976 0.0100 0.9900

Carbon disulfide 1.2281 1.2015 1.3462 1.3937 1.2778 Ave 5.7

1.2592

1.2844 0.0100 15.0

Acetonitrile 0.0349 0.0327 0.0349 0.0328 0.0329 Ave 6.1

0.0294

0.0330 0.0010 15.0

Methylene Chloride 0.4402 0.4262 0.4539 0.4254 0.4228 Ave 4.4

0.3973

0.4276 0.0100 15.0

Acrylonitrile 0.1608 0.1223 0.1370 0.1213 0.1263 Lin2 0.9950

0.1142

1.5562 0.1209 0.0010 0.9900

trans-1,2-Dichloroethene 0.4687 0.4410 0.4603 0.4325 0.4314 Ave 4.6

0.4139

0.4413 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 108 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Methyl tert-butyl ether 1.2409 1.0967 1.2053 1.0887 1.1030 Ave 7.6

1.0084

1.1238 0.0100 15.0

1,1-Dichloroethane 0.9158 0.8754 0.8985 0.8573 0.8580 Ave 4.0

0.8171

0.8704 0.1000 15.0

Vinyl acetate 0.7794 0.7899 0.8439 0.8848 0.9027 Ave 6.1

0.8075

0.8347 0.0100 15.0

2,2-Dichloropropane 0.5123 0.4762 0.4910 0.4760 0.4692 Ave 5.5

0.4333

0.4764 0.0100 15.0

cis-1,2-Dichloroethene 0.5178 0.4752 0.4900 0.4699 0.4727 Ave 4.9

0.4468

0.4787 0.0100 15.0

2-Butanone (MEK) 0.1907 0.1661 0.1744 0.1666 0.1738 Ave 7.0

0.1547

0.1710 0.0100 15.0

Propionitrile 0.0377 0.0303 0.0325 0.0300 0.0310 Ave 10.0

0.0283

0.0316 0.0010 15.0

Bromochloromethane 0.2134 0.1810 0.1955 0.1835 0.1826 Ave 7.7

0.1724

0.1881 0.0100 15.0

Tetrahydrofuran 0.1362 0.1110 0.1157 0.1060 0.1101 Lin2 0.9970

0.0981

0.1550 0.1053 0.0100 0.9900

Chloroform 0.8071 0.7676 0.7909 0.7569 0.7592 Ave 3.9

0.7200

0.7669 0.0100 15.0

1,1,1-Trichloroethane 0.6379 0.6227 0.6514 0.6248 0.6266 Ave 3.7

0.5828

0.6244 0.0100 15.0

Carbon tetrachloride 0.3601 0.3514 0.3626 0.3590 0.3620 Ave 1.9

0.3457

0.3568 0.0100 15.0

1,1-Dichloropropene 0.6628 0.6440 0.6397 0.6320 0.6326 Ave 3.2

0.6014

0.6354 0.0100 15.0

Benzene 1.2960 1.2332 1.2212 1.1893 1.1679 Ave 5.2

1.1124

1.2033 0.0100 15.0

1,2-Dichloroethane 0.4036 0.3828 0.3925 0.3773 0.3822 Ave 3.7

0.3615

0.3833 0.0100 15.0

Trichloroethene 0.3071 0.2871 0.2880 0.2787 0.2819 Ave 4.3

0.2706

0.2856 0.0100 15.0

1,2-Dichloropropane 0.2945 0.3110 0.2983 0.3002 0.3013 Ave 2.3

0.2903

0.2993 0.0100 15.0

Dibromomethane 0.1499 0.1401 0.1448 0.1410 0.1445 Ave 3.6

0.1346

0.1425 0.0100 15.0

Bromodichloromethane 0.3131 0.3276 0.3492 0.3570 0.3677 Ave 5.9

0.3548

0.3449 0.0100 15.0

2-Chloroethyl vinyl ether 0.1275 0.1289 0.1333 0.1400 0.1446 Ave 5.1

0.1302

0.1341 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 109 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

cis-1,3-Dichloropropene 0.3823 0.3878 0.3955 0.4081 0.4277 Ave 4.1

0.4075

0.4015 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.2134 0.2212 0.2438 0.2360 0.2310 Ave 5.2

0.2176

0.2272 0.0100 15.0

Toluene 0.7563 0.7457 0.7103 0.7065 0.7016 Ave 4.3

0.6724

0.7155 0.0100 15.0

trans-1,3-Dichloropropene 0.3019 0.3263 0.3366 0.3455 0.3644 Ave 6.4

0.3505

0.3375 0.0100 15.0

1,1,2-Trichloroethane 0.2720 0.2647 0.2830 0.2757 0.2832 Ave 2.6

0.2710

0.2749 0.0100 15.0

Tetrachloroethene 0.3877 0.3857 0.3641 0.3770 0.3714 Ave 3.1

0.3585

0.3741 0.0100 15.0

1,3-Dichloropropane 0.4386 0.4678 0.4537 0.4585 0.4651 Ave 2.7

0.4404

0.4540 0.0100 15.0

2-Hexanone 0.1953 0.1931 0.1955 0.2045 0.1961 Ave 2.7

0.1880

0.1954 0.0100 15.0

Dibromochloromethane 0.2040 0.2329 0.2507 0.2602 0.2677 Ave 9.7

0.2616

0.2462 0.0100 15.0

1,2-Dibromoethane 0.1811 0.1775 0.1848 0.1786 0.1848 Ave 2.7

0.1720

0.1798 0.0100 15.0

1-Chlorohexane 0.6093 0.5831 0.5505 0.5582 0.5737 Ave 4.3

0.5435

0.5697 0.0100 15.0

Chlorobenzene 0.9184 0.9225 0.9033 0.9116 0.9054 Ave 2.2

0.8681

0.9049 0.3000 15.0

1,1,1,2-Tetrachloroethane 0.2930 0.2979 0.3101 0.3188 0.3208 Ave 3.6

0.3132

0.3090 0.0100 15.0

Ethylbenzene 0.5544 0.5503 0.5126 0.5352 0.5171 Ave 4.1

0.5009

0.5284 0.0100 15.0

m&p-Xylene 1.3686 1.3827 1.3012 1.2861 1.2289 Ave 6.9

1.1453

1.2855 0.0100 15.0

o-Xylene 1.3495 1.4372 1.3698 1.3557 1.3252 Ave 4.5

1.2528

1.3484 0.0100 15.0

Styrene 0.9608 1.0612 1.0145 1.0388 1.0303 Ave 3.6

0.9843

1.0150 0.0100 15.0

Bromoform 0.1125 0.1362 0.1408 0.1514 0.1643 Ave 13.0

0.1539

0.1432 0.1000 15.0

Isopropylbenzene 3.1539 3.6540 3.1572 3.3315 3.1688 Ave 6.7

3.0455

3.2518 0.0100 15.0

Bromobenzene 0.6695 0.7563 0.7093 0.7420 0.7361 Ave 4.2

0.7199

0.7222 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 110 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,1,2,2-Tetrachloroethane 0.5452 0.5696 0.5597 0.5706 0.5758 Ave 3.0

0.5328

0.5589 0.3000 15.0

1,2,3-Trichloropropane 0.1912 0.1794 0.1660 0.1701 0.1701 Ave 6.1

0.1622

0.1732 0.0100 15.0

N-Propylbenzene 3.9287 4.2993 3.7879 3.9367 3.7362 Ave 6.3

3.5832

3.8787 0.0100 15.0

2-Chlorotoluene 2.3554 2.5038 2.2305 2.3361 2.2656 Ave 4.9

2.1830

2.3124 0.0100 15.0

1,3,5-Trimethylbenzene 2.6219 2.9360 2.6333 2.7109 2.6361 Ave 5.3

2.5201

2.6764 0.0100 15.0

4-Chlorotoluene 2.6491 2.9401 2.6216 2.7188 2.6440 Ave 5.1

2.5353

2.6848 0.0100 15.0

tert-Butylbenzene 2.2801 2.5455 2.2199 2.2982 2.2247 Ave 6.1

2.1418

2.2850 0.0100 15.0

1,2,4-Trimethylbenzene 2.7631 3.0061 2.6438 2.7255 2.6458 Ave 5.8

2.5511

2.7226 0.0100 15.0

sec-Butylbenzene 3.5331 3.8935 3.3623 3.4462 3.3180 Ave 7.1

3.1870

3.4567 0.0100 15.0

1,3-Dichlorobenzene 1.4471 1.5053 1.3813 1.4255 1.3778 Ave 4.0

1.3501

1.4145 0.0100 15.0

p-Isopropyltoluene 2.9586 3.2474 2.8310 2.8845 2.8017 Ave 6.6

2.6869

2.9017 0.0100 15.0

1,4-Dichlorobenzene 1.3977 1.4878 1.3669 1.4117 1.3954 Ave 3.8

1.3295

1.3982 0.0100 15.0

n-Butylbenzene 2.8602 3.1543 2.7994 2.7899 2.7599 Ave 6.2

2.6239

2.8313 0.0100 15.0

1,2-Dichlorobenzene 1.2797 1.3306 1.2155 1.2573 1.2376 Ave 3.9

1.1916

1.2521 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0873 0.0832 0.0794 0.0812 0.0900 Ave 4.7

0.0826

0.0839 0.0100 15.0

1,2,4-Trichlorobenzene 0.9789 0.9823 0.8678 0.7520 0.7794 Ave 13.0

0.7396

0.8500 0.0100 15.0

Hexachlorobutadiene 0.6292 0.6291 0.5100 0.4198 0.4138 Qua1 0.9940

+++++

0.7417 0.5403 -0.001 0.0100 0.9900

Naphthalene 1.6968 1.5945 1.4268 1.3407 1.4423 Lin2 0.9970

1.3291

1.6628 1.3908 0.0100 0.9900

1,2,3-Trichlorobenzene 0.7531 0.7667 0.6080 0.5315 0.5708 Qua2 0.9900

0.5407

0.4654 0.6784 -0.001 0.0100 0.9900

Dibromofluoromethane 0.4012 0.4120 0.3878 0.4079 Ave 4.3

0.3703

0.3958 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 111 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,2-Dichloroethane-d4 (Surr) 0.3252 0.3396 0.3092 0.3325 Ave 6.0

0.2918

0.3196 0.0100 15.0

Toluene-d8 (Surr) 1.0538 1.0512 0.9999 1.0425 Ave 4.8

0.9393

1.0174 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5024 0.5042 0.4741 0.5018 Ave 5.3

0.4456

0.4856 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 112 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Dichlorodifluoromethane PFB Ave 12902 50070 127370 264568 422626

553924

5.00 20.0 50.0 100 150

200

Chloromethane PFB Ave 16213 63463 162200 326211 505093

682571

5.00 20.0 50.0 100 150

200

Vinyl chloride PFB Ave 13885 56436 140448 289222 445896

594740

5.00 20.0 50.0 100 150

200

Bromomethane PFB Lin2 5496 18758 43458 93314 141095

193922

5.00 20.0 50.0 100 150

200

Chloroethane PFB Ave 7205 29060 71345 150837 234006

319655

5.00 20.0 50.0 100 150

200

Trichlorofluoromethane PFB Ave 16215 63387 158331 343881 516513

704692

5.00 20.0 50.0 100 150

200

Acrolein PFB Lin2 84258 300252 793200 1494545 2240120

2801943

200 800 2000 4000 6000

8000

1,1-Dichloroethene PFB Ave 9821 44072 105755 217759 322621

428198

5.00 20.0 50.0 100 150

200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 10804 45578 109401 223828 334178

429549

5.00 20.0 50.0 100 150

200

Acetone PFB Lin1 5507 12315 31383 63749 92368

115814

5.00 20.0 50.0 100 150

200

Carbon disulfide PFB Ave 31066 138989 361364 824494 1127201

1531938

5.00 20.0 50.0 100 150

200

Acetonitrile PFB Ave 7059 30299 75012 155141 232468

286410

40.0 160 400 800 1200

1600

Methylene Chloride PFB Ave 11136 49301 121856 251650 373003

483310

5.00 20.0 50.0 100 150

200

Acrylonitrile PFB Lin2 32531 113188 294241 574185 891617

1111839

40.0 160 400 800 1200

1600

trans-1,2-Dichloroethene PFB Ave 11855 51013 123566 255847 380526

503496

5.00 20.0 50.0 100 150

200

Methyl tert-butyl ether PFB Ave 31388 126868 323557 644017 972967

1226790

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 113 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

1,1-Dichloroethane PFB Ave 23166 101272 241193 507139 756847

994036

5.00 20.0 50.0 100 150

200

Vinyl acetate PFB Ave 19714 91380 226543 523396 796266

982422

5.00 20.0 50.0 100 150

200

2,2-Dichloropropane PFB Ave 12960 55088 131791 281610 413914

527180

5.00 20.0 50.0 100 150

200

cis-1,2-Dichloroethene PFB Ave 13099 54969 131526 277962 416945

543539

5.00 20.0 50.0 100 150

200

2-Butanone (MEK) PFB Ave 4823 19213 46819 98580 153328

188153

5.00 20.0 50.0 100 150

200

Propionitrile DFB Ave 11092 40835 102296 208849 323908

406897

40.0 160 400 800 1200

1600

Bromochloromethane PFB Ave 5399 20944 52481 108571 161097

209785

5.00 20.0 50.0 100 150

200

Tetrahydrofuran PFB Lin2 3446 12837 31053 62700 97150

119315

5.00 20.0 50.0 100 150

200

Chloroform PFB Ave 20416 88794 212306 447767 669705

875928

5.00 20.0 50.0 100 150

200

1,1,1-Trichloroethane PFB Ave 16137 72040 174862 369627 552754

709015

5.00 20.0 50.0 100 150

200

Carbon tetrachloride DFB Ave 13245 59272 142459 312633 472055

620557

5.00 20.0 50.0 100 150

200

1,1-Dichloropropene PFB Ave 16767 74498 171713 373900 558058

731603

5.00 20.0 50.0 100 150

200

Benzene DFB Ave 47671 208006 479794 1035802 1523052

1996925

5.00 20.0 50.0 100 150

200

1,2-Dichloroethane DFB Ave 14847 64572 154226 328584 498369

649012

5.00 20.0 50.0 100 150

200

Trichloroethene DFB Ave 11297 48428 113149 242684 367651

485784

5.00 20.0 50.0 100 150

200

1,2-Dichloropropane DFB Ave 10834 52448 117184 261424 392941

521104

5.00 20.0 50.0 100 150

200

Dibromomethane DFB Ave 5515 23635 56895 122814 188390

241667

5.00 20.0 50.0 100 150

200

Bromodichloromethane DFB Ave 11517 55249 137199 310916 479512

636972

5.00 20.0 50.0 100 150

200

2-Chloroethyl vinyl ether DFB Ave 4691 21736 52381 121903 188565

233764

5.00 20.0 50.0 100 150

200

cis-1,3-Dichloropropene DFB Ave 14063 65411 155392 355410 557705

731626

5.00 20.0 50.0 100 150

200

4-Methyl-2-pentanone (MIBK) DFB Ave 7850 37307 95785 205560 301187

390574

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 114 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Toluene DFB Ave 27820 125770 279057 615277 914875

1207131

5.00 20.0 50.0 100 150

200

trans-1,3-Dichloropropene DFB Ave 11105 55044 132225 300866 475199

629293

5.00 20.0 50.0 100 150

200

1,1,2-Trichloroethane PFB Ave 6881 30616 75972 163072 249804

329645

5.00 20.0 50.0 100 150

200

Tetrachloroethene CBZ Ave 11739 49681 113412 247302 371178

488872

5.00 20.0 50.0 100 150

200

1,3-Dichloropropane CBZ Ave 13281 60253 141339 300730 464793

600568

5.00 20.0 50.0 100 150

200

2-Hexanone CBZ Ave 5913 24867 60900 134127 195945

256358

5.00 20.0 50.0 100 150

200

Dibromochloromethane CBZ Ave 6176 29991 78104 170673 267577

356811

5.00 20.0 50.0 100 150

200

1,2-Dibromoethane DFB Ave 6662 29944 72598 155572 240952

308703

5.00 20.0 50.0 100 150

200

1-Chlorohexane PFB Ave 15413 67451 147771 330227 506094

661180

5.00 20.0 50.0 100 150

200

Chlorobenzene CBZ Ave 27808 118815 281396 597934 904889

1183858

5.00 20.0 50.0 100 150

200

1,1,1,2-Tetrachloroethane CBZ Ave 8870 38367 96602 209122 320615

427140

5.00 20.0 50.0 100 150

200

Ethylbenzene CBZ Ave 16785 70876 159684 351002 516773

683074

5.00 20.0 50.0 100 150

200

m&p-Xylene CBZ Ave 82877 356156 810673 1687130 2456378

3123829

10.0 40.0 100 200 300

400

o-Xylene CBZ Ave 40858 185102 426723 889192 1324449

1708514

5.00 20.0 50.0 100 150

200

Styrene CBZ Ave 29090 136679 316041 681314 1029721

1342275

5.00 20.0 50.0 100 150

200

Bromoform CBZ Ave 3407 17540 43862 99282 164184

209852

5.00 20.0 50.0 100 150

200

Isopropylbenzene DCB Ave 51019 228406 516591 1065124 1575324

2017775

5.00 20.0 50.0 100 150

200

Bromobenzene DCB Ave 10830 47272 116055 237235 365963

476962

5.00 20.0 50.0 100 150

200

1,1,2,2-Tetrachloroethane DCB Ave 8819 35605 91578 182439 286268

352978

5.00 20.0 50.0 100 150

200

1,2,3-Trichloropropane DCB Ave 3093 11214 27159 54392 84576

107459

5.00 20.0 50.0 100 150

200

N-Propylbenzene DCB Ave 63553 268743 619776 1258627 1857403

2373990

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 115 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

2-Chlorotoluene DCB Ave 38102 156509 364951 746878 1126306

1446295

5.00 20.0 50.0 100 150

200

1,3,5-Trimethylbenzene DCB Ave 42413 183522 430864 866728 1310538

1669636

5.00 20.0 50.0 100 150

200

4-Chlorotoluene DCB Ave 42853 183778 428943 869237 1314457

1679760

5.00 20.0 50.0 100 150

200

tert-Butylbenzene DCB Ave 36885 159113 363220 734777 1106000

1419051

5.00 20.0 50.0 100 150

200

1,2,4-Trimethylbenzene DCB Ave 44697 187908 432579 871394 1315353

1690213

5.00 20.0 50.0 100 150

200

sec-Butylbenzene DCB Ave 57153 243374 550146 1101803 1649521

2111505

5.00 20.0 50.0 100 150

200

1,3-Dichlorobenzene DCB Ave 23410 94092 226011 455769 684977

894523

5.00 20.0 50.0 100 150

200

p-Isopropyltoluene DCB Ave 47861 202992 463212 922211 1392838

1780196

5.00 20.0 50.0 100 150

200

1,4-Dichlorobenzene DCB Ave 22610 92998 223660 451341 693731

880833

5.00 20.0 50.0 100 150

200

n-Butylbenzene DCB Ave 46268 197168 458033 891981 1372078

1738419

5.00 20.0 50.0 100 150

200

1,2-Dichlorobenzene DCB Ave 20701 83175 198883 401981 615248

789503

5.00 20.0 50.0 100 150

200

1,2-Dibromo-3-Chloropropane DCB Ave 1412 5199 12985 25946 44755

54754

5.00 20.0 50.0 100 150

200

1,2,4-Trichlorobenzene DCB Ave 15835 61405 141991 240412 387497

490028

5.00 20.0 50.0 100 150

200

Hexachlorobutadiene DCB Qua1 10179 39324 83450 134222 205730

+++++

5.00 20.0 50.0 100 150

+++++

Naphthalene DCB Lin2 27448 99668 233455 428628 717029

880550

5.00 20.0 50.0 100 150

200

1,2,3-Trichlorobenzene DCB Qua2 12182 47927 99479 169921 283755

358235

5.00 20.0 50.0 100 150

200

Dibromofluoromethane PFB Ave 46408 110602 229403 359839

450525

20.0 50.0 100 150

200

1,2-Dichloroethane-d4 (Surr) DFB Ave 54848 133405 269262 433613

523883

20.0 50.0 100 150

200

Toluene-d8 (Surr) DFB Ave 177743 413010 870860 1359449

1686334

20.0 50.0 100 150

200

4-Bromofluorobenzene (Surr) CBZ Ave 64705 157084 310979 501486

607718

20.0 50.0 100 150

200

FORM VI 8260B Page 116 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend:

Ave = Average ISTD

Lin1 = Linear 1/conc ISTD

Lin2 = Linear 1/conc^2 ISTD

Qua1 = Quadratic 1/conc ISTD

Qua2 = Quadratic 1/conc^2 ISTD

FORM VI 8260B Page 117 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172614/2 22I1211A.D

Level 2 STD02 500-172614/3 22I1211B.D

Level 3 STD03 500-172614/4 22I1211C.D

Level 4 STD04 500-172614/5 22I1211D.D

Level 5 STD05 500-172614/6 22I1211E.D

Level 6 STD06 500-172614/7 22I1211F.D

Level 7 STD07 500-172614/8 22I1211G.D

Level 8 STD08 500-172614/9 22I1211H.D

Level 9 STD09 500-172614/10 22I1211I.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883 Ave 9.9

0.5798 0.5632 0.5150 0.5364

0.5420 0.0100 15.0

Chloromethane 0.8256 0.7243 0.6267 0.6890 Ave 7.9

0.7182 0.7230 0.6810 0.7012

0.7111 0.1000 15.0

Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130 Ave 8.0

0.6517 0.6618 0.6041 0.6323

0.6381 0.0100 15.0

Bromomethane 0.1659 0.2203 0.1716 0.1726 Ave 13.0

0.2077 0.2258 0.2110 0.2234

0.1998 0.0100 15.0

Chloroethane 0.4113 0.3289 0.3175 0.3315 Ave 10.0

0.3369 0.3333 0.3044 0.3069

0.3338 0.0100 15.0

Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079 Ave 6.3

0.9817 1.0066 0.9437 0.9571

0.9993 0.0100 15.0

Acetone +++++ +++++ 0.0554 0.0635 Ave 7.8

0.0614 0.0672 0.0690 0.0671

0.0639 0.0100 15.0

Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319 Ave 7.9

0.8320 0.8249 0.7635 0.7796

0.8265 0.0100 15.0

Acrolein 0.0331 0.0421 0.0314 0.0388 Ave 13.0

0.0392 0.0429 0.0450 0.0450

0.0397 0.0010 15.0

1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008 Ave 4.7

0.3938 0.3925 0.3935 0.4040

0.4001 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785 Ave 6.7

0.4739 0.4784 0.4696 0.4829

0.4862 0.0100 15.0

Methylene Chloride +++++ 0.4011 0.3629 0.4004 Ave 4.0

0.3719 0.3777 0.3682 0.3859

0.3812 0.0100 15.0

Carbon disulfide 1.5962 1.3713 1.3219 1.4559 Ave 6.5

1.5313 1.5882 1.4767 1.4979

1.4799 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 118 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Acetonitrile 0.0371 0.0333 0.0243 0.0295 Ave 13.0

0.0262 0.0281 0.0299 0.0295

0.0297 0.0010 15.0

Acrylonitrile 0.0750 0.0912 0.0677 0.0823 Ave 9.0

0.0764 0.0821 0.0846 0.0849

0.0805 0.0010 15.0

trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560 Ave 4.4

0.4456 0.4511 0.4430 0.4552

0.4499 0.0100 15.0

2-Butanone (MEK) +++++ +++++ 0.0823 0.0919 Ave 6.1

0.0908 0.0953 0.0973 0.0970

0.0924 0.0100 15.0

Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577 Ave 5.4

0.7230 0.7592 0.7369 0.7564

0.7369 0.0100 15.0

Vinyl acetate +++++ 0.6129 0.5650 0.6423 Ave 5.2

0.6107 0.6494 0.6338 0.6642

0.6255 0.0100 15.0

Tetrahydrofuran +++++ +++++ 0.0538 0.0611 Ave 4.2

0.0583 0.0572 0.0571 0.0595

0.0578 0.0100 15.0

1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189 Ave 6.2

0.8749 0.8925 0.8704 0.9084

0.8857 0.1000 15.0

2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515 Ave 5.5

0.7243 0.7285 0.7200 0.7474

0.7341 0.0100 15.0

cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663 Ave 6.4

0.4508 0.4630 0.4488 0.4652

0.4554 0.0100 15.0

Propionitrile 0.0230 0.0200 0.0163 0.0205 Ave 10.0

0.0191 0.0201 0.0217 0.0219

0.0203 0.0010 15.0

Bromochloromethane 0.2191 0.1652 0.1606 0.1825 Ave 10.0

0.1747 0.1747 0.1737 0.1772

0.1785 0.0100 15.0

Chloroform 0.7988 0.7465 0.6742 0.7604 Ave 4.9

0.7195 0.7370 0.7200 0.7434

0.7375 0.0100 15.0

1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390 Ave 4.7

0.7317 0.7368 0.7320 0.7583

0.7394 0.0100 15.0

Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871 Ave 3.4

0.4883 0.4750 0.4767 0.4948

0.4834 0.0100 15.0

1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649 Ave 6.9

0.6479 0.6478 0.6435 0.6685

0.6488 0.0100 15.0

Benzene 1.2306 1.3508 1.2179 1.1306 1.2550 Ave 4.7

1.2277 1.2183 1.1975 1.2355

1.2293 0.0100 15.0

1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618 Ave 5.6

0.3558 0.3552 0.3521 0.3644

0.3536 0.0100 15.0

4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561 Ave 5.1

0.1535 0.1552 0.1604 0.1580

0.1536 0.0100 15.0

2-Hexanone +++++ +++++ 0.1035 0.1187 Ave 7.3

0.1220 0.1257 0.1256 0.1271

0.1204 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 119 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516 Ave 4.9

0.3434 0.3325 0.3291 0.3406

0.3450 0.0100 15.0

1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264 Ave 6.4

0.3130 0.3110 0.3089 0.3197

0.3152 0.0100 15.0

Dibromomethane 0.1457 0.1306 0.1153 0.1288 Ave 6.9

0.1238 0.1238 0.1224 0.1261

0.1271 0.0100 15.0

Bromodichloromethane 0.3875 0.3507 0.3319 0.3726 Ave 4.6

0.3533 0.3599 0.3552 0.3686

0.3600 0.0100 15.0

2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096 Ave 3.2

0.1015 0.1078 0.1021 0.1054

0.1054 0.0100 15.0

cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222 Ave 4.1

0.4033 0.4109 0.4067 0.4210

0.4091 0.0100 15.0

Toluene 0.9341 0.8388 0.7909 0.7458 0.8161 Ave 6.2

0.8023 0.8060 0.7995 0.8258

0.8177 0.0100 15.0

trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412 Ave 8.6

0.3304 0.3383 0.3448 0.3521

0.3392 0.0100 15.0

1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681 Ave 7.7

0.1638 0.1667 0.1692 0.1728

0.1723 0.0100 15.0

Tetrachloroethene 0.5511 0.4482 0.4255 0.4568 Ave 9.0

0.4446 0.4384 0.4251 0.4400

0.4537 0.0100 15.0

1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542 Ave 4.9

0.3407 0.3413 0.3399 0.3540

0.3491 0.0100 15.0

Dibromochloromethane 0.2702 0.2371 0.2274 0.2693 Ave 6.9

0.2630 0.2690 0.2675 0.2786

0.2603 0.0100 15.0

1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607 Ave 10.0

0.1572 0.1634 0.1626 0.1665

0.1651 0.0100 15.0

Chlorobenzene 1.1305 1.0221 0.9605 1.0363 Ave 5.3

0.9949 0.9884 0.9670 0.9960

1.0120 0.3000 15.0

1-Chlorohexane 0.7176 0.7070 0.6491 0.6984 Ave 3.1

0.6765 0.6760 0.6835 0.6837

0.6865 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448 Ave 5.0

0.3425 0.3461 0.3458 0.3585

0.3400 0.0100 15.0

Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796 Ave 3.4

0.5801 0.5769 0.5619 0.5822

0.5753 0.0100 15.0

m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876 Ave 4.5

1.4534 1.4554 1.3960 1.3942

1.4275 0.0100 15.0

o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780 Ave 5.5

1.4493 1.4706 1.4590 1.5151

1.4564 0.0100 15.0

Styrene 1.1505 1.0719 0.9871 1.1405 Ave 5.6

1.1318 1.1478 1.1460 1.1845

1.1200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 120 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1602 0.1366 0.1243 0.1553 Ave 10.0

0.1546 0.1600 0.1660 0.1720

0.1536 0.1000 15.0

Isopropylbenzene 3.8233 3.3535 3.0653 3.4816 Ave 7.4

3.1927 3.1639 3.1360 3.2790

3.3119 0.0100 15.0

Bromobenzene 0.8632 0.7552 0.6812 0.7730 Ave 8.2

0.6922 0.7028 0.6972 0.7345

0.7374 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089 Ave 6.0

0.3542 0.3640 0.3676 0.3874

0.3844 0.3000 15.0

1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046 Ave 6.1

0.2704 0.2691 0.2728 0.2923

0.2827 0.0100 15.0

N-Propylbenzene 4.4856 4.0360 3.6439 4.1493 Ave 6.5

3.8858 3.8875 3.7881 3.8936

3.9712 0.0100 15.0

4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065 Ave 7.0

2.1662 2.2029 2.1653 2.2760

2.2416 0.0100 15.0

1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026 Ave 5.8

2.6929 2.7638 2.7107 2.8237

2.7652 0.0100 15.0

2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174 Ave 6.4

2.5627 2.6413 2.6089 2.7193

2.6625 0.0100 15.0

tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552 Ave 7.3

2.4553 2.4418 2.4420 2.5773

2.5582 0.0100 15.0

1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710 Ave 6.3

2.6381 2.7234 2.6840 2.8189

2.7134 0.0100 15.0

sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075 Ave 5.8

3.6796 3.6591 3.6577 3.7738

3.7828 0.0100 15.0

1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907 Ave 8.4

1.4814 1.5187 1.5128 1.5667

1.5748 0.0100 15.0

p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705 Ave 6.4

3.1719 3.2121 3.1807 3.2836

3.2868 0.0100 15.0

1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651 Ave 6.9

1.4798 1.5043 1.4758 1.5340

1.5559 0.0100 15.0

1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033 Ave 6.4

1.2786 1.2876 1.2674 1.3183

1.3233 0.0100 15.0

n-Butylbenzene 3.1126 2.8700 2.6461 2.9480 Ave 4.7

2.8772 2.9149 2.9548 3.0267

2.9188 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678 Ave 12.0

0.0613 0.0622 0.0635 0.0659

0.0661 0.0100 15.0

1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999 Ave 5.3

0.8675 0.9149 0.9059 0.9063

0.8970 0.0100 15.0

Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351 Ave 9.3

0.7318 0.6946 0.7407 0.7100

0.7568 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 121 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0319 0.9651 0.8910 1.0003 Ave 5.7

0.9350 0.9776 1.0179 1.0659

0.9856 0.0100 15.0

1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392 Ave 5.4

0.6972 0.7092 0.7197 0.7238

0.7171 0.0100 15.0

Dibromofluoromethane 0.4088 Ave 3.6

0.3747 0.4105 0.3974 0.4034

0.3990 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2898 Ave 2.8

0.2681 0.2786 0.2783 0.2818

0.2793 0.0100 15.0

Toluene-d8 (Surr) 1.2317 Ave 3.0

1.1353 1.2008 1.1689 1.1817

1.1837 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5022 Ave 2.5

0.4792 0.5117 0.5010 0.5085

0.5005 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 122 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172614/2 22I1211A.D

Level 2 STD02 500-172614/3 22I1211B.D

Level 3 STD03 500-172614/4 22I1211C.D

Level 4 STD04 500-172614/5 22I1211D.D

Level 5 STD05 500-172614/6 22I1211E.D

Level 6 STD06 500-172614/7 22I1211F.D

Level 7 STD07 500-172614/8 22I1211G.D

Level 8 STD08 500-172614/9 22I1211H.D

Level 9 STD09 500-172614/10 22I1211I.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 8283 14019 34084 128973

408706 762307 1110898 1572519

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 10611 19121 44725 181982

506217 978702 1468998 2055922

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 2072 9537 16111 40052 161885

459341 895799 1302949 1853836

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2132 5817 12250 45578

146376 305638 455210 654905

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 5286 8684 22657 87550

237436 451232 656528 899737

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 14493 27342 66676 266205

691989 1362610 2035639 2806119

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave +++++ +++++ 3957 16764

43292 90934 148822 196769

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 12483 22039 55227 219705

586466 1116585 1646914 2285626

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 16997 44508 89671 410157

1104663 2325112 3885554 5276134

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 5414 11300 26186 105858

277562 531364 848798 1184587

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 7210 13042 32193 126370

334028 647515 1013020 1415755

1.00 2.00 5.00 20.0

50.0 100 150 200

Methylene Chloride PFB Ave +++++ 10588 25901 105736

262156 511318 794285 1131397

+++++ 2.00 5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 20516 36202 94343 384523

1079379 2149891 3185269 4391617

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3815 7023 13902 62328

147511 304606 515971 692080

8.00 16.0 40.0 160

400 800 1200 1600

FORM VI 8260B Page 123 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7715 19252 38635 173831

430688 889127 1460725 1990459

8.00 16.0 40.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 6143 12190 29175 120435

314119 610637 955652 1334459

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave +++++ +++++ 5877 24272

64002 128968 209900 284336

+++++ +++++ 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 10253 18092 48485 200118

509651 1027632 1589481 2217547

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave +++++ 16181 40320 169641

430488 879019 1367143 1947324

+++++ 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave +++++ +++++ 3843 16127

41123 77379 123251 174315

+++++ +++++ 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 12660 21793 57801 242674

616675 1208102 1877461 2663163

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 10444 18966 47829 198464

510518 986077 1552961 2191135

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 6562 11093 29875 123154

317732 626799 968176 1363967

1.00 2.00 5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 3274 5826 13049 61580

150541 311165 533857 726579

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 2816 4362 11462 48207

123109 236461 374570 519660

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 10267 19708 48119 200834

507134 997634 1553050 2179601

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 10394 19135 48811 195166

515733 997347 1578989 2223267

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 8845 18161 44839 182447

481514 918644 1463204 2051034

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 9406 15734 42090 175593

456667 876844 1388026 1960009

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 5292 24000 44324 113004 470128

1210657 2356179 3675431 5120985

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 6813 12420 31493 135519

350802 686980 1080708 1510261

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave +++++ +++++ 13833 58466

151375 300182 492445 654734

+++++ +++++ 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave +++++ +++++ 8872 37503

101953 206593 337483 453433

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1541 6794 12213 33134 131705

338598 643029 1009984 1411923

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 6308 11028 28481 122258

308626 601403 948132 1325238

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 124 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane DFB Ave 2589 4753 11529 48251

122106 239384 375807 522887

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 6884 12765 33178 139566

348406 696059 1090230 1527793

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chloroethyl vinyl ether DFB Ave 1869 3984 10192 41067

100134 208398 313500 436785

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 7564 14930 37294 158135

397656 794708 1248175 1745247

1.00 2.00 5.00 20.0

50.0 100 150 200

Toluene DFB Ave 4017 14904 28786 74548 305710

791155 1558816 2453857 3422834

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 7005 11724 29021 127802

325796 654311 1058276 1459268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane DFB Ave 3579 6500 15804 62968

161526 322360 519398 716065

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 8289 14024 36478 144290

371408 720453 1142505 1570157

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 5569 11637 27497 111881

284612 560890 913572 1263367

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 4064 7418 19500 85045

219735 442108 718959 994298

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 3616 5912 14445 60214

154974 316106 499079 690159

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 17003 31983 82345 327328

831189 1624419 2599260 3554021

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 9223 18665 46324 184447

476816 915102 1474279 2004578

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 5151 10625 25733 108914

286131 568808 929412 1279270

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 2120 9059 17971 45661 183060

484613 948132 1510230 2077566

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 10400 45804 87017 223793 939704

2428374 4783893 7504852 9950024

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 5285 23810 43602 110873 466833

1210753 2416819 3921614 5406441

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 17304 33541 84628 360216

945512 1886331 3080454 4226631

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 2410 4275 10660 49043

129169 263003 446109 613724

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 31324 57244 148746 610310

1601454 3109566 5106365 6881199

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 7072 12892 33053 135512

347188 690763 1135272 1541345

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 125 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 3258 7169 18231 71670

177658 357760 598529 812983

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 2270 5288 12868 53399

135614 264488 444171 613409

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 36750 68894 176823 727359

1949080 3820722 6168362 8171167

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 21017 38120 97903 404326

1086544 2165096 3525867 4776401

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 24843 46048 121204 508814

1350744 2716376 4413867 5925708

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 24693 44629 117536 476349

1285442 2595965 4248167 5706737

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 24197 44012 114646 465442

1231564 2399839 3976419 5408653

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 24293 46692 115053 485753

1323232 2676625 4370483 5915680

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 34897 64452 172232 684971

1845685 3596271 5955880 7919600

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 15196 28192 68974 278836

743079 1492625 2463360 3287950

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 30451 57429 145300 590843

1590983 3156888 5179163 6891004

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 14514 28274 70862 274358

742273 1478508 2403110 3219268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 12130 22897 58683 245994

641352 1265519 2063725 2766492

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 25501 48990 128404 516775

1443162 2864857 4811328 6351852

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 517 1453 2909 11888

30736 61117 103368 138335

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 8084 14950 39749 157753

435120 899145 1475044 1901927

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 7491 13587 35512 128859

367053 682660 1206171 1489923

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 8454 16474 43237 175344

469003 960821 1657420 2236810

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 6507 11786 32167 129572

349729 697002 1171916 1518870

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 107966

264099 555702 857139 1182785

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 108560

264333 538799 854290 1167924

20.0

50.0 100 150 200

FORM VI 8260B Page 126 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 461399

1119518 2322467 3587473 4898132

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 158632

400320 840950 1346757 1814509

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

FORM VI 8260B Page 127 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883 Ave 9.9

0.5798 0.5632 0.5150 0.5364

0.5420 0.0100 15.0

Chloromethane 0.8256 0.7243 0.6267 0.6890 Ave 7.9

0.7182 0.7230 0.6810 0.7012

0.7111 0.1000 15.0

Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130 Ave 8.0

0.6517 0.6618 0.6041 0.6323

0.6381 0.0100 15.0

Bromomethane 0.1659 0.2203 0.1716 0.1726 Ave 13.0

0.2077 0.2258 0.2110 0.2234

0.1998 0.0100 15.0

Chloroethane 0.4113 0.3289 0.3175 0.3315 Ave 10.0

0.3369 0.3333 0.3044 0.3069

0.3338 0.0100 15.0

Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079 Ave 6.3

0.9817 1.0066 0.9437 0.9571

0.9993 0.0100 15.0

Acetone +++++ +++++ 0.0554 0.0635 Ave 7.8

0.0614 0.0672 0.0690 0.0671

0.0639 0.0100 15.0

Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319 Ave 7.9

0.8320 0.8249 0.7635 0.7796

0.8265 0.0100 15.0

Acrolein 0.0331 0.0421 0.0314 0.0388 Ave 13.0

0.0392 0.0429 0.0450 0.0450

0.0397 0.0010 15.0

1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008 Ave 4.7

0.3938 0.3925 0.3935 0.4040

0.4001 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785 Ave 6.7

0.4739 0.4784 0.4696 0.4829

0.4862 0.0100 15.0

Methylene Chloride +++++ 0.4011 0.3629 0.4004 Ave 4.0

0.3719 0.3777 0.3682 0.3859

0.3812 0.0100 15.0

Carbon disulfide 1.5962 1.3713 1.3219 1.4559 Ave 6.5

1.5313 1.5882 1.4767 1.4979

1.4799 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 128 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Acetonitrile 0.0371 0.0333 0.0243 0.0295 Ave 13.0

0.0262 0.0281 0.0299 0.0295

0.0297 0.0010 15.0

Acrylonitrile 0.0750 0.0912 0.0677 0.0823 Ave 9.0

0.0764 0.0821 0.0846 0.0849

0.0805 0.0010 15.0

trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560 Ave 4.4

0.4456 0.4511 0.4430 0.4552

0.4499 0.0100 15.0

2-Butanone (MEK) +++++ +++++ 0.0823 0.0919 Ave 6.1

0.0908 0.0953 0.0973 0.0970

0.0924 0.0100 15.0

Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577 Ave 5.4

0.7230 0.7592 0.7369 0.7564

0.7369 0.0100 15.0

Vinyl acetate +++++ 0.6129 0.5650 0.6423 Ave 5.2

0.6107 0.6494 0.6338 0.6642

0.6255 0.0100 15.0

Tetrahydrofuran +++++ +++++ 0.0538 0.0611 Ave 4.2

0.0583 0.0572 0.0571 0.0595

0.0578 0.0100 15.0

1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189 Ave 6.2

0.8749 0.8925 0.8704 0.9084

0.8857 0.1000 15.0

2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515 Ave 5.5

0.7243 0.7285 0.7200 0.7474

0.7341 0.0100 15.0

cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663 Ave 6.4

0.4508 0.4630 0.4488 0.4652

0.4554 0.0100 15.0

Propionitrile 0.0230 0.0200 0.0163 0.0205 Ave 10.0

0.0191 0.0201 0.0217 0.0219

0.0203 0.0010 15.0

Bromochloromethane 0.2191 0.1652 0.1606 0.1825 Ave 10.0

0.1747 0.1747 0.1737 0.1772

0.1785 0.0100 15.0

Chloroform 0.7988 0.7465 0.6742 0.7604 Ave 4.9

0.7195 0.7370 0.7200 0.7434

0.7375 0.0100 15.0

1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390 Ave 4.7

0.7317 0.7368 0.7320 0.7583

0.7394 0.0100 15.0

Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871 Ave 3.4

0.4883 0.4750 0.4767 0.4948

0.4834 0.0100 15.0

1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649 Ave 6.9

0.6479 0.6478 0.6435 0.6685

0.6488 0.0100 15.0

Benzene 1.2306 1.3508 1.2179 1.1306 1.2550 Ave 4.7

1.2277 1.2183 1.1975 1.2355

1.2293 0.0100 15.0

1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618 Ave 5.6

0.3558 0.3552 0.3521 0.3644

0.3536 0.0100 15.0

4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561 Ave 5.1

0.1535 0.1552 0.1604 0.1580

0.1536 0.0100 15.0

2-Hexanone +++++ +++++ 0.1035 0.1187 Ave 7.3

0.1220 0.1257 0.1256 0.1271

0.1204 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 129 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516 Ave 4.9

0.3434 0.3325 0.3291 0.3406

0.3450 0.0100 15.0

1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264 Ave 6.4

0.3130 0.3110 0.3089 0.3197

0.3152 0.0100 15.0

Dibromomethane 0.1457 0.1306 0.1153 0.1288 Ave 6.9

0.1238 0.1238 0.1224 0.1261

0.1271 0.0100 15.0

Bromodichloromethane 0.3875 0.3507 0.3319 0.3726 Ave 4.6

0.3533 0.3599 0.3552 0.3686

0.3600 0.0100 15.0

2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096 Ave 3.2

0.1015 0.1078 0.1021 0.1054

0.1054 0.0100 15.0

cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222 Ave 4.1

0.4033 0.4109 0.4067 0.4210

0.4091 0.0100 15.0

Toluene 0.9341 0.8388 0.7909 0.7458 0.8161 Ave 6.2

0.8023 0.8060 0.7995 0.8258

0.8177 0.0100 15.0

trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412 Ave 8.6

0.3304 0.3383 0.3448 0.3521

0.3392 0.0100 15.0

1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681 Ave 7.7

0.1638 0.1667 0.1692 0.1728

0.1723 0.0100 15.0

Tetrachloroethene 0.5511 0.4482 0.4255 0.4568 Ave 9.0

0.4446 0.4384 0.4251 0.4400

0.4537 0.0100 15.0

1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542 Ave 4.9

0.3407 0.3413 0.3399 0.3540

0.3491 0.0100 15.0

Dibromochloromethane 0.2702 0.2371 0.2274 0.2693 Ave 6.9

0.2630 0.2690 0.2675 0.2786

0.2603 0.0100 15.0

1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607 Ave 10.0

0.1572 0.1634 0.1626 0.1665

0.1651 0.0100 15.0

Chlorobenzene 1.1305 1.0221 0.9605 1.0363 Ave 5.3

0.9949 0.9884 0.9670 0.9960

1.0120 0.3000 15.0

1-Chlorohexane 0.7176 0.7070 0.6491 0.6984 Ave 3.1

0.6765 0.6760 0.6835 0.6837

0.6865 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448 Ave 5.0

0.3425 0.3461 0.3458 0.3585

0.3400 0.0100 15.0

Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796 Ave 3.4

0.5801 0.5769 0.5619 0.5822

0.5753 0.0100 15.0

m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876 Ave 4.5

1.4534 1.4554 1.3960 1.3942

1.4275 0.0100 15.0

o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780 Ave 5.5

1.4493 1.4706 1.4590 1.5151

1.4564 0.0100 15.0

Styrene 1.1505 1.0719 0.9871 1.1405 Ave 5.6

1.1318 1.1478 1.1460 1.1845

1.1200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 130 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1602 0.1366 0.1243 0.1553 Ave 10.0

0.1546 0.1600 0.1660 0.1720

0.1536 0.1000 15.0

Isopropylbenzene 3.8233 3.3535 3.0653 3.4816 Ave 7.4

3.1927 3.1639 3.1360 3.2790

3.3119 0.0100 15.0

Bromobenzene 0.8632 0.7552 0.6812 0.7730 Ave 8.2

0.6922 0.7028 0.6972 0.7345

0.7374 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089 Ave 6.0

0.3542 0.3640 0.3676 0.3874

0.3844 0.3000 15.0

1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046 Ave 6.1

0.2704 0.2691 0.2728 0.2923

0.2827 0.0100 15.0

N-Propylbenzene 4.4856 4.0360 3.6439 4.1493 Ave 6.5

3.8858 3.8875 3.7881 3.8936

3.9712 0.0100 15.0

4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065 Ave 7.0

2.1662 2.2029 2.1653 2.2760

2.2416 0.0100 15.0

1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026 Ave 5.8

2.6929 2.7638 2.7107 2.8237

2.7652 0.0100 15.0

2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174 Ave 6.4

2.5627 2.6413 2.6089 2.7193

2.6625 0.0100 15.0

tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552 Ave 7.3

2.4553 2.4418 2.4420 2.5773

2.5582 0.0100 15.0

1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710 Ave 6.3

2.6381 2.7234 2.6840 2.8189

2.7134 0.0100 15.0

sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075 Ave 5.8

3.6796 3.6591 3.6577 3.7738

3.7828 0.0100 15.0

1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907 Ave 8.4

1.4814 1.5187 1.5128 1.5667

1.5748 0.0100 15.0

p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705 Ave 6.4

3.1719 3.2121 3.1807 3.2836

3.2868 0.0100 15.0

1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651 Ave 6.9

1.4798 1.5043 1.4758 1.5340

1.5559 0.0100 15.0

1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033 Ave 6.4

1.2786 1.2876 1.2674 1.3183

1.3233 0.0100 15.0

n-Butylbenzene 3.1126 2.8700 2.6461 2.9480 Ave 4.7

2.8772 2.9149 2.9548 3.0267

2.9188 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678 Ave 12.0

0.0613 0.0622 0.0635 0.0659

0.0661 0.0100 15.0

1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999 Ave 5.3

0.8675 0.9149 0.9059 0.9063

0.8970 0.0100 15.0

Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351 Ave 9.3

0.7318 0.6946 0.7407 0.7100

0.7568 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 131 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0319 0.9651 0.8910 1.0003 Ave 5.7

0.9350 0.9776 1.0179 1.0659

0.9856 0.0100 15.0

1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392 Ave 5.4

0.6972 0.7092 0.7197 0.7238

0.7171 0.0100 15.0

Dibromofluoromethane 0.4088 Ave 3.6

0.3747 0.4105 0.3974 0.4034

0.3990 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2898 Ave 2.8

0.2681 0.2786 0.2783 0.2818

0.2793 0.0100 15.0

Toluene-d8 (Surr) 1.2317 Ave 3.0

1.1353 1.2008 1.1689 1.1817

1.1837 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5022 Ave 2.5

0.4792 0.5117 0.5010 0.5085

0.5005 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 132 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 8283 14019 34084 128973

408706 762307 1110898 1572519

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 10611 19121 44725 181982

506217 978702 1468998 2055922

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 2072 9537 16111 40052 161885

459341 895799 1302949 1853836

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2132 5817 12250 45578

146376 305638 455210 654905

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 5286 8684 22657 87550

237436 451232 656528 899737

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 14493 27342 66676 266205

691989 1362610 2035639 2806119

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave +++++ +++++ 3957 16764

43292 90934 148822 196769

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 12483 22039 55227 219705

586466 1116585 1646914 2285626

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 16997 44508 89671 410157

1104663 2325112 3885554 5276134

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 5414 11300 26186 105858

277562 531364 848798 1184587

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 7210 13042 32193 126370

334028 647515 1013020 1415755

1.00 2.00 5.00 20.0

50.0 100 150 200

Methylene Chloride PFB Ave +++++ 10588 25901 105736

262156 511318 794285 1131397

+++++ 2.00 5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 20516 36202 94343 384523

1079379 2149891 3185269 4391617

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3815 7023 13902 62328

147511 304606 515971 692080

8.00 16.0 40.0 160

400 800 1200 1600

FORM VI 8260B Page 133 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7715 19252 38635 173831

430688 889127 1460725 1990459

8.00 16.0 40.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 6143 12190 29175 120435

314119 610637 955652 1334459

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave +++++ +++++ 5877 24272

64002 128968 209900 284336

+++++ +++++ 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 10253 18092 48485 200118

509651 1027632 1589481 2217547

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave +++++ 16181 40320 169641

430488 879019 1367143 1947324

+++++ 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave +++++ +++++ 3843 16127

41123 77379 123251 174315

+++++ +++++ 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 12660 21793 57801 242674

616675 1208102 1877461 2663163

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 10444 18966 47829 198464

510518 986077 1552961 2191135

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 6562 11093 29875 123154

317732 626799 968176 1363967

1.00 2.00 5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 3274 5826 13049 61580

150541 311165 533857 726579

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 2816 4362 11462 48207

123109 236461 374570 519660

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 10267 19708 48119 200834

507134 997634 1553050 2179601

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 10394 19135 48811 195166

515733 997347 1578989 2223267

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 8845 18161 44839 182447

481514 918644 1463204 2051034

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 9406 15734 42090 175593

456667 876844 1388026 1960009

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 5292 24000 44324 113004 470128

1210657 2356179 3675431 5120985

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 6813 12420 31493 135519

350802 686980 1080708 1510261

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave +++++ +++++ 13833 58466

151375 300182 492445 654734

+++++ +++++ 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave +++++ +++++ 8872 37503

101953 206593 337483 453433

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1541 6794 12213 33134 131705

338598 643029 1009984 1411923

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 6308 11028 28481 122258

308626 601403 948132 1325238

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 134 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane DFB Ave 2589 4753 11529 48251

122106 239384 375807 522887

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 6884 12765 33178 139566

348406 696059 1090230 1527793

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chloroethyl vinyl ether DFB Ave 1869 3984 10192 41067

100134 208398 313500 436785

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 7564 14930 37294 158135

397656 794708 1248175 1745247

1.00 2.00 5.00 20.0

50.0 100 150 200

Toluene DFB Ave 4017 14904 28786 74548 305710

791155 1558816 2453857 3422834

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 7005 11724 29021 127802

325796 654311 1058276 1459268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane DFB Ave 3579 6500 15804 62968

161526 322360 519398 716065

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 8289 14024 36478 144290

371408 720453 1142505 1570157

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 5569 11637 27497 111881

284612 560890 913572 1263367

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 4064 7418 19500 85045

219735 442108 718959 994298

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 3616 5912 14445 60214

154974 316106 499079 690159

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 17003 31983 82345 327328

831189 1624419 2599260 3554021

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 9223 18665 46324 184447

476816 915102 1474279 2004578

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 5151 10625 25733 108914

286131 568808 929412 1279270

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 2120 9059 17971 45661 183060

484613 948132 1510230 2077566

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 10400 45804 87017 223793 939704

2428374 4783893 7504852 9950024

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 5285 23810 43602 110873 466833

1210753 2416819 3921614 5406441

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 17304 33541 84628 360216

945512 1886331 3080454 4226631

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 2410 4275 10660 49043

129169 263003 446109 613724

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 31324 57244 148746 610310

1601454 3109566 5106365 6881199

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 7072 12892 33053 135512

347188 690763 1135272 1541345

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 135 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 3258 7169 18231 71670

177658 357760 598529 812983

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 2270 5288 12868 53399

135614 264488 444171 613409

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 36750 68894 176823 727359

1949080 3820722 6168362 8171167

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 21017 38120 97903 404326

1086544 2165096 3525867 4776401

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 24843 46048 121204 508814

1350744 2716376 4413867 5925708

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 24693 44629 117536 476349

1285442 2595965 4248167 5706737

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 24197 44012 114646 465442

1231564 2399839 3976419 5408653

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 24293 46692 115053 485753

1323232 2676625 4370483 5915680

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 34897 64452 172232 684971

1845685 3596271 5955880 7919600

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 15196 28192 68974 278836

743079 1492625 2463360 3287950

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 30451 57429 145300 590843

1590983 3156888 5179163 6891004

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 14514 28274 70862 274358

742273 1478508 2403110 3219268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 12130 22897 58683 245994

641352 1265519 2063725 2766492

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 25501 48990 128404 516775

1443162 2864857 4811328 6351852

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 517 1453 2909 11888

30736 61117 103368 138335

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 8084 14950 39749 157753

435120 899145 1475044 1901927

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 7491 13587 35512 128859

367053 682660 1206171 1489923

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 8454 16474 43237 175344

469003 960821 1657420 2236810

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 6507 11786 32167 129572

349729 697002 1171916 1518870

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 107966

264099 555702 857139 1182785

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 108560

264333 538799 854290 1167924

20.0

50.0 100 150 200

FORM VI 8260B Page 136 of 332 01/04/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 461399

1119518 2322467 3587473 4898132

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 158632

400320 840950 1346757 1814509

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

FORM VI 8260B Page 137 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.4279 0.0100 45.9 50.0 -8.3 25.0

Chloromethane Ave 0.5798 0.5246 0.1000 45.2 50.0 -9.5 25.0

Vinyl chloride Ave 0.5072 0.5248 0.0100 51.7 50.0 3.5 25.0

Bromomethane Lin2 0.1523 0.0100 47.2 50.0 -5.7 25.0

Chloroethane Ave 0.2641 0.2426 0.0100 45.9 50.0 -8.2 25.0

Trichlorofluoromethane Ave 0.5875 0.5702 0.0100 48.5 50.0 -2.9 25.0

Acrolein Lin2 0.0673 0.0010 2080 2000 4.0 25.0

1,1-Dichloroethene Ave 0.3748 0.3758 0.0100 50.1 50.0 0.2 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3311 0.0100 42.5 50.0 -15.1 25.0

Acetone Lin1 0.1027 0.0100 46.9 50.0 -6.2 25.0

Carbon disulfide Ave 1.284 1.296 0.0100 50.4 50.0 0.9 25.0

Acetonitrile Ave 0.0330 0.0367 0.0010 446 400 11.4 25.0

Methylene Chloride Ave 0.4276 0.4290 0.0100 50.2 50.0 0.3 25.0

Acrylonitrile Lin2 0.1268 0.0010 407 400 1.7 25.0

trans-1,2-Dichloroethene Ave 0.4413 0.4669 0.0100 52.9 50.0 5.8 25.0

Methyl tert-butyl ether Ave 1.124 1.023 0.0100 45.5 50.0 -9.0 25.0

1,1-Dichloroethane Ave 0.8704 0.8721 0.1000 50.1 50.0 0.2 25.0

Vinyl acetate Ave 0.8347 0.8804 0.0100 52.7 50.0 5.5 25.0

2,2-Dichloropropane Ave 0.4764 0.4986 0.0100 52.3 50.0 4.7 25.0

cis-1,2-Dichloroethene Ave 0.4787 0.4840 0.0100 50.6 50.0 1.1 25.0

2-Butanone (MEK) Ave 0.1710 0.1524 0.0100 44.6 50.0 -10.9 25.0

Propionitrile Ave 0.0316 0.0316 0.0010 399 400 -0.2 25.0

Bromochloromethane Ave 0.1881 0.1702 0.0100 45.2 50.0 -9.5 25.0

Tetrahydrofuran Lin2 0.1042 0.0100 48.0 50.0 -4.0 25.0

Chloroform Ave 0.7669 0.7748 0.0100 50.5 50.0 1.0 25.0

1,1,1-Trichloroethane Ave 0.6244 0.6555 0.0100 52.5 50.0 5.0 25.0

Carbon tetrachloride Ave 0.3568 0.3724 0.0100 52.2 50.0 4.4 25.0

1,1-Dichloropropene Ave 0.6354 0.6306 0.0100 49.6 50.0 -0.8 25.0

Benzene Ave 1.203 1.216 0.0100 50.5 50.0 1.1 25.0

1,2-Dichloroethane Ave 0.3833 0.3697 0.0100 48.2 50.0 -3.5 25.0

Trichloroethene Ave 0.2856 0.2917 0.0100 51.1 50.0 2.1 25.0

1,2-Dichloropropane Ave 0.2993 0.2959 0.0100 49.4 50.0 -1.1 25.0

Dibromomethane Ave 0.1425 0.1397 0.0100 49.0 50.0 -2.0 25.0

Bromodichloromethane Ave 0.3449 0.3379 0.0100 49.0 50.0 -2.0 25.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1258 0.0100 46.9 50.0 -6.2 25.0

cis-1,3-Dichloropropene Ave 0.4015 0.4011 0.0100 53.7 53.8 -0.1 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2120 0.0100 46.7 50.0 -6.7 25.0

Toluene Ave 0.7155 0.7132 0.0100 49.8 50.0 -0.3 25.0

trans-1,3-Dichloropropene Ave 0.3375 0.3348 0.0100 48.2 48.6 -0.8 25.0

1,1,2-Trichloroethane Ave 0.2749 0.2675 0.0100 48.6 50.0 -2.7 25.0

FORM VII 8260B

Page 138 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.3914 0.0100 52.3 50.0 4.6 25.0

1,3-Dichloropropane Ave 0.4540 0.4541 0.0100 50.0 50.0 0.0 25.0

2-Hexanone Ave 0.1954 0.1831 0.0100 46.9 50.0 -6.3 25.0

Dibromochloromethane Ave 0.2462 0.2483 0.0100 50.4 50.0 0.9 25.0

1,2-Dibromoethane Ave 0.1798 0.1719 0.0100 47.8 50.0 -4.4 25.0

1-Chlorohexane Ave 0.5697 0.5208 0.0100 45.7 50.0 -8.6 25.0

Chlorobenzene Ave 0.9049 0.8647 0.3000 47.8 50.0 -4.4 25.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3084 0.0100 49.9 50.0 -0.2 25.0

Ethylbenzene Ave 0.5284 0.5301 0.0100 50.2 50.0 0.3 25.0

m&p-Xylene Ave 1.285 1.283 0.0100 99.8 100 -0.2 25.0

o-Xylene Ave 1.348 1.295 0.0100 48.0 50.0 -4.0 25.0

Styrene Ave 1.015 1.029 0.0100 50.7 50.0 1.4 25.0

Bromoform Ave 0.1432 0.1401 0.1000 48.9 50.0 -2.2 25.0

Isopropylbenzene Ave 3.252 3.211 0.0100 49.4 50.0 -1.3 25.0

Bromobenzene Ave 0.7222 0.7556 0.0100 52.3 50.0 4.6 25.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.5584 0.3000 50.0 50.0 -0.1 25.0

1,2,3-Trichloropropane Ave 0.1732 0.1680 0.0100 48.5 50.0 -3.0 25.0

N-Propylbenzene Ave 3.879 3.806 0.0100 49.1 50.0 -1.9 25.0

2-Chlorotoluene Ave 2.312 2.300 0.0100 49.7 50.0 -0.6 25.0

1,3,5-Trimethylbenzene Ave 2.676 2.896 0.0100 54.1 50.0 8.2 25.0

4-Chlorotoluene Ave 2.685 2.597 0.0100 48.4 50.0 -3.3 25.0

tert-Butylbenzene Ave 2.285 2.273 0.0100 49.7 50.0 -0.5 25.0

1,2,4-Trimethylbenzene Ave 2.723 2.842 0.0100 52.2 50.0 4.4 25.0

sec-Butylbenzene Ave 3.457 3.410 0.0100 49.3 50.0 -1.4 25.0

1,3-Dichlorobenzene Ave 1.415 1.361 0.0100 48.1 50.0 -3.8 25.0

p-Isopropyltoluene Ave 2.902 2.828 0.0100 48.7 50.0 -2.5 25.0

1,4-Dichlorobenzene Ave 1.398 1.440 0.0100 51.5 50.0 3.0 25.0

n-Butylbenzene Ave 2.831 2.940 0.0100 51.9 50.0 3.8 25.0

1,2-Dichlorobenzene Ave 1.252 1.205 0.0100 48.1 50.0 -3.8 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0784 0.0100 46.7 50.0 -6.6 25.0

1,2,4-Trichlorobenzene Ave 0.8500 0.8024 0.0100 47.2 50.0 -5.6 25.0

Hexachlorobutadiene Qua1 0.5223 0.0100 51.7 50.0 3.4 25.0

Naphthalene Lin2 1.356 0.0100 47.5 50.0 -4.9 25.0

1,2,3-Trichlorobenzene Qua2 0.5963 0.0100 45.8 50.0 -8.3 25.0

Dibromofluoromethane Ave 0.3958 0.3997 0.0100 43.7 43.3 1.0 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3112 0.0100 42.1 43.3 -2.6 25.0

Toluene-d8 (Surr) Ave 1.017 1.099 0.0100 46.8 43.3 8.1 25.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5002 0.0100 44.6 43.3 3.0 25.0

FORM VII 8260B

Page 139 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

11/19/2012 17:14

11/19/2012 14:32

11/19/2012 16:28

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.4262 0.3493 0.0100 41.0 50.0 -18.0 25.0

Iodomethane Ave 0.5737 0.6405 0.0100 55.8 50.0 11.6 25.0

Methyl acetate Ave 0.3675 0.2295 0.0100 31.2 50.0 -37.6* 25.0

Hexane Ave 0.7834 0.6708 0.0100 42.8 50.0 -14.4 25.0

Cyclohexane Lin2 0.8544 0.0100 46.7 50.0 -6.6 25.0

Heptane Ave 0.5932 0.5269 0.0100 44.4 50.0 -11.2 25.0

Methylcyclohexane Ave 0.5531 0.5154 0.0100 46.6 50.0 -6.8 25.0

1,3,5-Trichlorobenzene Ave 1.012 1.063 0.0100 52.5 50.0 5.0 25.0

FORM VII 8260B

Page 140 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

12/20/2012 08:13

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173515/2

DB624

TestAmerica Chicago

Lab File ID: 16C1220.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.3486 0.0100 37.4 50.0 -25.3 50.0

Chloromethane Ave 0.5798 0.4665 0.1000 40.2 50.0 -19.5 50.0

Vinyl chloride Ave 0.5072 0.4435 0.0100 43.7 50.0 -12.6 20.0

Bromomethane Lin2 0.1301 0.0100 40.0 50.0 -20.0 50.0

Chloroethane Ave 0.2641 0.2221 0.0100 42.1 50.0 -15.9 50.0

Trichlorofluoromethane Ave 0.5875 0.5691 0.0100 48.4 50.0 -3.1 50.0

Acrolein Lin2 0.0560 0.0010 1722 2000 -13.9 50.0

1,1-Dichloroethene Ave 0.3748 0.3869 0.0100 51.6 50.0 3.2 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3979 0.0100 51.0 50.0 2.1 50.0

Acetone Lin1 0.1062 0.0100 48.7 50.0 -2.6 50.0

Carbon disulfide Ave 1.284 1.102 0.0100 42.9 50.0 -14.2 50.0

Acetonitrile Ave 0.0330 0.0361 0.0010 438 400 9.5 50.0

Methylene Chloride Ave 0.4276 0.4443 0.0100 51.9 50.0 3.9 50.0

Acrylonitrile Lin2 0.1335 0.0010 429 400 7.2 50.0

Methyl tert-butyl ether Ave 1.124 1.185 0.0100 52.7 50.0 5.4 50.0

trans-1,2-Dichloroethene Ave 0.4413 0.4532 0.0100 51.4 50.0 2.7 50.0

1,1-Dichloroethane Ave 0.8704 0.8926 0.1000 51.3 50.0 2.6 50.0

Vinyl acetate Ave 0.8347 0.8694 0.0100 52.1 50.0 4.2 50.0

2,2-Dichloropropane Ave 0.4764 0.4711 0.0100 49.4 50.0 -1.1 50.0

cis-1,2-Dichloroethene Ave 0.4787 0.4912 0.0100 51.3 50.0 2.6 50.0

2-Butanone (MEK) Ave 0.1710 0.1682 0.0100 49.2 50.0 -1.7 50.0

Propionitrile Ave 0.0316 0.0339 0.0010 429 400 7.1 50.0

Bromochloromethane Ave 0.1881 0.2007 0.0100 53.4 50.0 6.7 50.0

Tetrahydrofuran Lin2 0.1171 0.0100 54.1 50.0 8.2 50.0

Chloroform Ave 0.7669 0.8018 0.0100 52.3 50.0 4.5 20.0

1,1,1-Trichloroethane Ave 0.6244 0.6395 0.0100 51.2 50.0 2.4 50.0

Carbon tetrachloride Ave 0.3568 0.3735 0.0100 52.4 50.0 4.7 50.0

1,1-Dichloropropene Ave 0.6354 0.6705 0.0100 52.8 50.0 5.5 50.0

Benzene Ave 1.203 1.278 0.0100 53.1 50.0 6.2 50.0

1,2-Dichloroethane Ave 0.3833 0.4049 0.0100 52.8 50.0 5.6 50.0

Trichloroethene Ave 0.2856 0.3046 0.0100 53.3 50.0 6.7 50.0

1,2-Dichloropropane Ave 0.2993 0.3180 0.0100 53.1 50.0 6.3 20.0

Dibromomethane Ave 0.1425 0.1520 0.0100 53.3 50.0 6.7 50.0

Bromodichloromethane Ave 0.3449 0.3668 0.0100 53.2 50.0 6.3 50.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1474 0.0100 55.0 50.0 9.9 50.0

cis-1,3-Dichloropropene Ave 0.4015 0.4396 0.0100 54.8 50.0 9.5 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2357 0.0100 51.9 50.0 3.8 50.0

Toluene Ave 0.7155 0.7651 0.0100 53.5 50.0 6.9 20.0

trans-1,3-Dichloropropene Ave 0.3375 0.3738 0.0100 55.4 50.0 10.7 50.0

1,1,2-Trichloroethane Ave 0.2749 0.3071 0.0100 55.9 50.0 11.7 50.0

FORM VII 8260B

Page 141 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

12/20/2012 08:13

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173515/2

DB624

TestAmerica Chicago

Lab File ID: 16C1220.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.3971 0.0100 53.1 50.0 6.2 50.0

1,3-Dichloropropane Ave 0.4540 0.5083 0.0100 56.0 50.0 12.0 50.0

2-Hexanone Ave 0.1954 0.2012 0.0100 51.5 50.0 3.0 50.0

Dibromochloromethane Ave 0.2462 0.2737 0.0100 55.6 50.0 11.2 50.0

1,2-Dibromoethane Ave 0.1798 0.1949 0.0100 54.2 50.0 8.4 50.0

1-Chlorohexane Ave 0.5697 0.6029 0.0100 52.9 50.0 5.8 50.0

Chlorobenzene Ave 0.9049 0.9568 0.3000 52.9 50.0 5.7 50.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3244 0.0100 52.5 50.0 5.0 50.0

Ethylbenzene Ave 0.5284 0.5537 0.0100 52.4 50.0 4.8 20.0

m&p-Xylene Ave 1.285 1.367 0.0100 106 100 6.4 50.0

o-Xylene Ave 1.348 1.392 0.0100 51.6 50.0 3.2 50.0

Styrene Ave 1.015 1.080 0.0100 53.2 50.0 6.4 50.0

Bromoform Ave 0.1432 0.1571 0.1000 54.9 50.0 9.7 50.0

Isopropylbenzene Ave 3.252 3.479 0.0100 53.5 50.0 7.0 50.0

Bromobenzene Ave 0.7222 0.8020 0.0100 55.5 50.0 11.0 50.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.6209 0.3000 55.5 50.0 11.1 50.0

1,2,3-Trichloropropane Ave 0.1732 0.1866 0.0100 53.9 50.0 7.7 50.0

N-Propylbenzene Ave 3.879 4.142 0.0100 53.4 50.0 6.8 50.0

2-Chlorotoluene Ave 2.312 2.443 0.0100 52.8 50.0 5.6 50.0

1,3,5-Trimethylbenzene Ave 2.676 2.829 0.0100 52.9 50.0 5.7 50.0

4-Chlorotoluene Ave 2.685 2.817 0.0100 52.5 50.0 4.9 50.0

tert-Butylbenzene Ave 2.285 2.355 0.0100 51.5 50.0 3.1 50.0

1,2,4-Trimethylbenzene Ave 2.723 2.815 0.0100 51.7 50.0 3.4 50.0

sec-Butylbenzene Ave 3.457 3.590 0.0100 51.9 50.0 3.9 50.0

1,3-Dichlorobenzene Ave 1.415 1.438 0.0100 50.8 50.0 1.7 50.0

p-Isopropyltoluene Ave 2.902 2.997 0.0100 51.7 50.0 3.3 50.0

1,4-Dichlorobenzene Ave 1.398 1.451 0.0100 51.9 50.0 3.7 50.0

n-Butylbenzene Ave 2.831 2.838 0.0100 50.1 50.0 0.2 50.0

1,2-Dichlorobenzene Ave 1.252 1.297 0.0100 51.8 50.0 3.6 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0822 0.0100 49.0 50.0 -2.0 50.0

1,2,4-Trichlorobenzene Ave 0.8500 0.7715 0.0100 45.4 50.0 -9.2 50.0

Hexachlorobutadiene Qua1 0.4734 0.0100 46.2 50.0 -7.5 50.0

Naphthalene Lin2 1.296 0.0100 45.4 50.0 -9.2 50.0

1,2,3-Trichlorobenzene Qua2 0.5295 0.0100 40.3 50.0 -19.4 50.0

Dibromofluoromethane Ave 0.3958 0.4147 0.0100 45.3 43.3 4.8 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3282 0.0100 44.4 43.3 2.7 50.0

Toluene-d8 (Surr) Ave 1.017 1.132 0.0100 48.2 43.3 11.3 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.4940 0.0100 44.0 43.3 1.7 50.0

FORM VII 8260B

Page 142 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

12/20/2012 08:36

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173515/3

DB624

TestAmerica Chicago

Lab File ID: 16D1220.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3958 0.4135 0.0100 45.2 43.3 4.5 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3351 0.0100 45.4 43.3 4.8 50.0

Toluene-d8 (Surr) Ave 1.017 1.102 0.0100 46.9 43.3 8.3 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.4948 0.0100 44.1 43.3 1.9 50.0

FORM VII 8260B

Page 143 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS16

12/20/2012 08:36

11/19/2012 14:32

11/19/2012 16:28

CCV 500-173515/3

DB624

TestAmerica Chicago

Lab File ID: 16D1220.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 0.5997 0.4585 0.0100 38.2 50.0 -23.5 50.0

Ethyl ether Ave 0.4262 0.4190 0.0100 49.2 50.0 -1.7 50.0

Iodomethane Ave 0.5737 0.5439 0.0100 94.8 100 -5.2 50.0

3-Chloropropene Ave 0.2319 0.2242 0.0100 96.7 100 -3.3 50.0

Methyl acetate Ave 0.3675 0.4295 0.0100 58.4 50.0 16.9 50.0

Hexane Ave 0.7834 0.7208 0.0100 46.0 50.0 -8.0 50.0

Isopropyl ether Ave 1.776 1.706 0.0100 48.0 50.0 -3.9 50.0

2-Chloro-1,3-butadiene Ave 0.8947 0.8271 0.0100 46.2 50.0 -7.6 50.0

Ethyl acetate Ave 0.3031 0.3555 0.0100 587 500 17.3 50.0

Methacrylonitrile Ave 0.2264 0.2490 0.0100 110 100 10.0 50.0

Cyclohexane Lin2 0.8487 0.0100 46.4 50.0 -7.3 50.0

Isobutyl alcohol Ave 0.0107 0.0129 0.0010 4851 4000 21.3 50.0

2,2,4-Trimethylpentane Ave 1.405 1.312 0.0100 46.7 50.0 -6.6 50.0

Heptane Ave 0.5932 0.5591 0.0100 47.1 50.0 -5.8 50.0

n-Butyl alcohol Ave 0.0063 0.0077 0.0010 4909 4000 22.7 50.0

Methylcyclohexane Ave 0.5531 0.5201 0.0100 47.0 50.0 -6.0 50.0

Methyl methacrylate Ave 0.2123 0.2461 0.0100 116 100 15.9 50.0

2-Nitropropane Ave 0.0771 0.0913 0.0100 4736 4000 18.4 50.0

Ethyl methacrylate Ave 0.3579 0.4203 0.0100 117 100 17.4 50.0

Cyclohexanone Lin1 0.0584 0.0100 4789 4000 19.7 50.0

trans-1,4-Dichloro-2-butene Ave 0.0868 0.1021 0.0100 118 100 17.6 50.0

Pentachloroethane Ave 0.2111 0.2210 0.0100 105 100 4.7 50.0

1,3,5-Trichlorobenzene Ave 1.012 0.9797 0.0100 48.4 50.0 -3.2 50.0

2-Methylnaphthalene Qua2 0.5865 0.0100 44.6 50.0 -10.9 50.0

FORM VII 8260B

Page 144 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.4239 0.0100 39.1 50.0 -21.8 25.0

Chloromethane Ave 0.7111 0.5561 0.1000 39.1 50.0 -21.8 25.0

Vinyl chloride Ave 0.6381 0.5920 0.0100 46.4 50.0 -7.2 25.0

Bromomethane Ave 0.1998 0.1541 0.0100 38.6 50.0 -22.9 25.0

Chloroethane Ave 0.3338 0.2911 0.0100 43.6 50.0 -12.8 25.0

Dichlorofluoromethane Ave 0.999 0.8378 0.0100 41.9 50.0 -16.2 25.0

Trichlorofluoromethane Ave 0.8265 0.7409 0.0100 44.8 50.0 -10.4 25.0

Acrolein Ave 0.0397 0.0406 0.0010 2044 2000 2.2 25.0

1,1-Dichloroethene Ave 0.4001 0.3815 0.0100 47.7 50.0 -4.7 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4598 0.0100 47.3 50.0 -5.4 25.0

Acetone Ave 0.0639 0.0621 0.0100 48.5 50.0 -2.9 25.0

Carbon disulfide Ave 1.480 1.369 0.0100 46.3 50.0 -7.5 25.0

Acetonitrile Ave 0.0297 0.0292 0.0010 393 400 -1.7 25.0

Methylene Chloride Ave 0.3812 0.3602 0.0100 47.2 50.0 -5.5 25.0

Acrylonitrile Ave 0.0805 0.0797 0.0010 396 400 -1.0 25.0

trans-1,2-Dichloroethene Ave 0.4499 0.4398 0.0100 48.9 50.0 -2.3 25.0

Methyl tert-butyl ether Ave 0.7369 0.6905 0.0100 46.9 50.0 -6.3 25.0

1,1-Dichloroethane Ave 0.8857 0.8456 0.1000 47.7 50.0 -4.5 25.0

Vinyl acetate Ave 0.6255 0.6214 0.0100 49.7 50.0 -0.6 25.0

2,2-Dichloropropane Ave 0.7341 0.6853 0.0100 46.7 50.0 -6.6 25.0

cis-1,2-Dichloroethene Ave 0.4554 0.4436 0.0100 48.7 50.0 -2.6 25.0

2-Butanone (MEK) Ave 0.0924 0.0837 0.0100 45.3 50.0 -9.4 25.0

Propionitrile Ave 0.0203 0.0211 0.0010 414 400 3.5 25.0

Bromochloromethane Ave 0.1785 0.1638 0.0100 45.9 50.0 -8.2 25.0

Tetrahydrofuran Ave 0.0578 0.0548 0.0100 47.3 50.0 -5.3 25.0

Chloroform Ave 0.7375 0.7135 0.0100 48.4 50.0 -3.3 25.0

1,1,1-Trichloroethane Ave 0.7394 0.7299 0.0100 49.4 50.0 -1.3 25.0

Carbon tetrachloride Ave 0.4834 0.4652 0.0100 48.1 50.0 -3.8 25.0

1,1-Dichloropropene Ave 0.6488 0.6138 0.0100 47.3 50.0 -5.4 25.0

Benzene Ave 1.229 1.148 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichloroethane Ave 0.3536 0.3244 0.0100 45.9 50.0 -8.3 25.0

Trichloroethene Ave 0.3450 0.3212 0.0100 46.6 50.0 -6.9 25.0

1,2-Dichloropropane Ave 0.3152 0.2970 0.0100 47.1 50.0 -5.8 25.0

Dibromomethane Ave 0.1271 0.1149 0.0100 45.2 50.0 -9.6 25.0

Bromodichloromethane Ave 0.3600 0.3216 0.0100 44.7 50.0 -10.7 25.0

2-Chloroethyl vinyl ether Ave 0.1054 0.0957 0.0100 45.4 50.0 -9.2 25.0

cis-1,3-Dichloropropene Ave 0.4091 0.3814 0.0100 50.1 53.8 -6.8 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1404 0.0100 45.7 50.0 -8.6 25.0

Toluene Ave 0.8177 0.7569 0.0100 46.3 50.0 -7.4 25.0

trans-1,3-Dichloropropene Ave 0.3392 0.3107 0.0100 44.5 48.6 -8.4 25.0

FORM VII 8260B

Page 145 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1573 0.0100 45.6 50.0 -8.7 25.0

Tetrachloroethene Ave 0.4537 0.4260 0.0100 47.0 50.0 -6.1 25.0

1,3-Dichloropropane Ave 0.3491 0.3223 0.0100 46.2 50.0 -7.7 25.0

2-Hexanone Ave 0.1204 0.1135 0.0100 47.1 50.0 -5.7 25.0

Dibromochloromethane Ave 0.2603 0.2454 0.0100 47.1 50.0 -5.7 25.0

1,2-Dibromoethane Ave 0.1651 0.1486 0.0100 45.0 50.0 -10.0 25.0

Chlorobenzene Ave 1.012 0.9004 0.3000 44.5 50.0 -11.0 25.0

1-Chlorohexane Ave 0.6865 0.6546 0.0100 47.7 50.0 -4.6 25.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3297 0.0100 48.5 50.0 -3.0 25.0

Ethylbenzene Ave 0.5753 0.5498 0.0100 47.8 50.0 -4.4 25.0

m&p-Xylene Ave 1.427 1.339 0.0100 93.8 100 -6.2 25.0

o-Xylene Ave 1.456 1.295 0.0100 44.5 50.0 -11.1 25.0

Styrene Ave 1.120 1.076 0.0100 48.0 50.0 -3.9 25.0

Bromoform Ave 0.1536 0.1521 0.1000 49.5 50.0 -1.0 25.0

Isopropylbenzene Ave 3.312 2.951 0.0100 44.6 50.0 -10.9 25.0

Bromobenzene Ave 0.7374 0.6901 0.0100 46.8 50.0 -6.4 25.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3650 0.3000 47.5 50.0 -5.1 25.0

1,2,3-Trichloropropane Ave 0.2827 0.2697 0.0100 47.7 50.0 -4.6 25.0

N-Propylbenzene Ave 3.971 3.489 0.0100 43.9 50.0 -12.2 25.0

4-Chlorotoluene Ave 2.242 2.042 0.0100 45.5 50.0 -8.9 25.0

1,3,5-Trimethylbenzene Ave 2.765 2.737 0.0100 49.5 50.0 -1.0 25.0

2-Chlorotoluene Ave 2.663 2.355 0.0100 44.2 50.0 -11.6 25.0

tert-Butylbenzene Ave 2.558 2.302 0.0100 45.0 50.0 -10.0 25.0

1,2,4-Trimethylbenzene Ave 2.713 2.637 0.0100 48.6 50.0 -2.8 25.0

sec-Butylbenzene Ave 3.783 3.418 0.0100 45.2 50.0 -9.6 25.0

1,3-Dichlorobenzene Ave 1.575 1.369 0.0100 43.5 50.0 -13.1 25.0

p-Isopropyltoluene Ave 3.287 2.935 0.0100 44.7 50.0 -10.7 25.0

1,4-Dichlorobenzene Ave 1.556 1.454 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichlorobenzene Ave 1.323 1.190 0.0100 45.0 50.0 -10.1 25.0

n-Butylbenzene Ave 2.919 2.736 0.0100 46.9 50.0 -6.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0567 0.0100 42.9 50.0 -14.2 25.0

1,2,4-Trichlorobenzene Ave 0.8970 0.7803 0.0100 43.5 50.0 -13.0 25.0

Hexachlorobutadiene Ave 0.7568 0.6904 0.0100 45.6 50.0 -8.8 25.0

Naphthalene Ave 0.9856 0.8667 0.0100 44.0 50.0 -12.1 25.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6586 0.0100 45.9 50.0 -8.2 25.0

Dibromofluoromethane Ave 0.3990 0.3761 0.0100 47.1 50.0 -5.7 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2556 0.0100 45.8 50.0 -8.5 25.0

Toluene-d8 (Surr) Ave 1.184 1.117 0.0100 47.2 50.0 -5.6 25.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4730 0.0100 47.3 50.0 -5.5 25.0

FORM VII 8260B

Page 146 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.4239 0.0100 39.1 50.0 -21.8 25.0

Chloromethane Ave 0.7111 0.5561 0.1000 39.1 50.0 -21.8 25.0

Vinyl chloride Ave 0.6381 0.5920 0.0100 46.4 50.0 -7.2 25.0

Bromomethane Ave 0.1998 0.1541 0.0100 38.6 50.0 -22.9 25.0

Chloroethane Ave 0.3338 0.2911 0.0100 43.6 50.0 -12.8 25.0

Dichlorofluoromethane Ave 0.999 0.8378 0.0100 41.9 50.0 -16.2 25.0

Trichlorofluoromethane Ave 0.8265 0.7409 0.0100 44.8 50.0 -10.4 25.0

Acrolein Ave 0.0397 0.0406 0.0010 2044 2000 2.2 25.0

1,1-Dichloroethene Ave 0.4001 0.3815 0.0100 47.7 50.0 -4.7 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4598 0.0100 47.3 50.0 -5.4 25.0

Acetone Ave 0.0639 0.0621 0.0100 48.5 50.0 -2.9 25.0

Carbon disulfide Ave 1.480 1.369 0.0100 46.3 50.0 -7.5 25.0

Acetonitrile Ave 0.0297 0.0292 0.0010 393 400 -1.7 25.0

Methylene Chloride Ave 0.3812 0.3602 0.0100 47.2 50.0 -5.5 25.0

Acrylonitrile Ave 0.0805 0.0797 0.0010 396 400 -1.0 25.0

trans-1,2-Dichloroethene Ave 0.4499 0.4398 0.0100 48.9 50.0 -2.3 25.0

Methyl tert-butyl ether Ave 0.7369 0.6905 0.0100 46.9 50.0 -6.3 25.0

1,1-Dichloroethane Ave 0.8857 0.8456 0.1000 47.7 50.0 -4.5 25.0

Vinyl acetate Ave 0.6255 0.6214 0.0100 49.7 50.0 -0.6 25.0

2,2-Dichloropropane Ave 0.7341 0.6853 0.0100 46.7 50.0 -6.6 25.0

cis-1,2-Dichloroethene Ave 0.4554 0.4436 0.0100 48.7 50.0 -2.6 25.0

2-Butanone (MEK) Ave 0.0924 0.0837 0.0100 45.3 50.0 -9.4 25.0

Propionitrile Ave 0.0203 0.0211 0.0010 414 400 3.5 25.0

Bromochloromethane Ave 0.1785 0.1638 0.0100 45.9 50.0 -8.2 25.0

Tetrahydrofuran Ave 0.0578 0.0548 0.0100 47.3 50.0 -5.3 25.0

Chloroform Ave 0.7375 0.7135 0.0100 48.4 50.0 -3.3 25.0

1,1,1-Trichloroethane Ave 0.7394 0.7299 0.0100 49.4 50.0 -1.3 25.0

Carbon tetrachloride Ave 0.4834 0.4652 0.0100 48.1 50.0 -3.8 25.0

1,1-Dichloropropene Ave 0.6488 0.6138 0.0100 47.3 50.0 -5.4 25.0

Benzene Ave 1.229 1.148 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichloroethane Ave 0.3536 0.3244 0.0100 45.9 50.0 -8.3 25.0

Trichloroethene Ave 0.3450 0.3212 0.0100 46.6 50.0 -6.9 25.0

1,2-Dichloropropane Ave 0.3152 0.2970 0.0100 47.1 50.0 -5.8 25.0

Dibromomethane Ave 0.1271 0.1149 0.0100 45.2 50.0 -9.6 25.0

Bromodichloromethane Ave 0.3600 0.3216 0.0100 44.7 50.0 -10.7 25.0

2-Chloroethyl vinyl ether Ave 0.1054 0.0957 0.0100 45.4 50.0 -9.2 25.0

cis-1,3-Dichloropropene Ave 0.4091 0.3814 0.0100 50.1 53.8 -6.8 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1404 0.0100 45.7 50.0 -8.6 25.0

Toluene Ave 0.8177 0.7569 0.0100 46.3 50.0 -7.4 25.0

trans-1,3-Dichloropropene Ave 0.3392 0.3107 0.0100 44.5 48.6 -8.4 25.0

FORM VII 8260B

Page 147 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1573 0.0100 45.6 50.0 -8.7 25.0

Tetrachloroethene Ave 0.4537 0.4260 0.0100 47.0 50.0 -6.1 25.0

1,3-Dichloropropane Ave 0.3491 0.3223 0.0100 46.2 50.0 -7.7 25.0

2-Hexanone Ave 0.1204 0.1135 0.0100 47.1 50.0 -5.7 25.0

Dibromochloromethane Ave 0.2603 0.2454 0.0100 47.1 50.0 -5.7 25.0

1,2-Dibromoethane Ave 0.1651 0.1486 0.0100 45.0 50.0 -10.0 25.0

Chlorobenzene Ave 1.012 0.9004 0.3000 44.5 50.0 -11.0 25.0

1-Chlorohexane Ave 0.6865 0.6546 0.0100 47.7 50.0 -4.6 25.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3297 0.0100 48.5 50.0 -3.0 25.0

Ethylbenzene Ave 0.5753 0.5498 0.0100 47.8 50.0 -4.4 25.0

m&p-Xylene Ave 1.427 1.339 0.0100 93.8 100 -6.2 25.0

o-Xylene Ave 1.456 1.295 0.0100 44.5 50.0 -11.1 25.0

Styrene Ave 1.120 1.076 0.0100 48.0 50.0 -3.9 25.0

Bromoform Ave 0.1536 0.1521 0.1000 49.5 50.0 -1.0 25.0

Isopropylbenzene Ave 3.312 2.951 0.0100 44.6 50.0 -10.9 25.0

Bromobenzene Ave 0.7374 0.6901 0.0100 46.8 50.0 -6.4 25.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3650 0.3000 47.5 50.0 -5.1 25.0

1,2,3-Trichloropropane Ave 0.2827 0.2697 0.0100 47.7 50.0 -4.6 25.0

N-Propylbenzene Ave 3.971 3.489 0.0100 43.9 50.0 -12.2 25.0

4-Chlorotoluene Ave 2.242 2.042 0.0100 45.5 50.0 -8.9 25.0

1,3,5-Trimethylbenzene Ave 2.765 2.737 0.0100 49.5 50.0 -1.0 25.0

2-Chlorotoluene Ave 2.663 2.355 0.0100 44.2 50.0 -11.6 25.0

tert-Butylbenzene Ave 2.558 2.302 0.0100 45.0 50.0 -10.0 25.0

1,2,4-Trimethylbenzene Ave 2.713 2.637 0.0100 48.6 50.0 -2.8 25.0

sec-Butylbenzene Ave 3.783 3.418 0.0100 45.2 50.0 -9.6 25.0

1,3-Dichlorobenzene Ave 1.575 1.369 0.0100 43.5 50.0 -13.1 25.0

p-Isopropyltoluene Ave 3.287 2.935 0.0100 44.7 50.0 -10.7 25.0

1,4-Dichlorobenzene Ave 1.556 1.454 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichlorobenzene Ave 1.323 1.190 0.0100 45.0 50.0 -10.1 25.0

n-Butylbenzene Ave 2.919 2.736 0.0100 46.9 50.0 -6.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0567 0.0100 42.9 50.0 -14.2 25.0

1,2,4-Trichlorobenzene Ave 0.8970 0.7803 0.0100 43.5 50.0 -13.0 25.0

Hexachlorobutadiene Ave 0.7568 0.6904 0.0100 45.6 50.0 -8.8 25.0

Naphthalene Ave 0.9856 0.8667 0.0100 44.0 50.0 -12.1 25.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6586 0.0100 45.9 50.0 -8.2 25.0

Dibromofluoromethane Ave 0.3990 0.3761 0.0100 47.1 50.0 -5.7 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2556 0.0100 45.8 50.0 -8.5 25.0

Toluene-d8 (Surr) Ave 1.184 1.117 0.0100 47.2 50.0 -5.6 25.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4730 0.0100 47.3 50.0 -5.5 25.0

FORM VII 8260B

Page 148 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 19:06

12/11/2012 23:48

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.2603 0.2517 0.0100 48.3 50.0 -3.3 25.0

Iodomethane Lin1 0.6879 0.0100 52.8 50.0 5.6 25.0

Methyl acetate Ave 0.2127 0.1450 0.0100 34.1 50.0 -31.8* 25.0

Hexane Ave 0.8764 0.9019 0.0100 51.5 50.0 2.9 25.0

Cyclohexane Lin1 1.057 0.0100 49.4 50.0 -1.2 25.0

Heptane Ave 0.7351 0.6922 0.0100 47.1 50.0 -5.8 25.0

Methylcyclohexane Ave 0.5969 0.6069 0.0100 50.8 50.0 1.7 25.0

1,3,5-Trichlorobenzene Ave 1.226 1.140 0.0100 46.5 50.0 -7.0 25.0

FORM VII 8260B

Page 149 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/12/2012 00:17

12/11/2012 19:06

12/11/2012 23:48

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.2603 0.2517 0.0100 48.3 50.0 -3.3 25.0

Iodomethane Lin1 0.6879 0.0100 52.8 50.0 5.6 25.0

Methyl acetate Ave 0.2127 0.1450 0.0100 34.1 50.0 -31.8* 25.0

Hexane Ave 0.8764 0.9019 0.0100 51.5 50.0 2.9 25.0

Cyclohexane Lin1 1.057 0.0100 49.4 50.0 -1.2 25.0

Heptane Ave 0.7351 0.6922 0.0100 47.1 50.0 -5.8 25.0

Methylcyclohexane Ave 0.5969 0.6069 0.0100 50.8 50.0 1.7 25.0

1,3,5-Trichlorobenzene Ave 1.226 1.140 0.0100 46.5 50.0 -7.0 25.0

FORM VII 8260B

Page 150 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/21/2012 11:31

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173708/2

DB624

TestAmerica Chicago

Lab File ID: 22C1221.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.5905 0.0100 54.5 50.0 8.9 50.0

Chloromethane Ave 0.7111 0.7033 0.1000 49.5 50.0 -1.1 50.0

Vinyl chloride Ave 0.6381 0.6454 0.0100 50.6 50.0 1.1 20.0

Bromomethane Ave 0.1998 0.2732 0.0100 68.4 50.0 36.8 50.0

Chloroethane Ave 0.3338 0.3927 0.0100 58.8 50.0 17.6 50.0

Dichlorofluoromethane Ave 0.999 0.9860 0.0100 49.3 50.0 -1.3 50.0

Trichlorofluoromethane Ave 0.8265 0.8481 0.0100 51.3 50.0 2.6 50.0

Acrolein Ave 0.0397 0.0143 0.0010 722 2000 -63.9* 50.0

1,1-Dichloroethene Ave 0.4001 0.3985 0.0100 49.8 50.0 -0.4 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4954 0.0100 50.9 50.0 1.9 50.0

Acetone Ave 0.0639 0.0594 0.0100 46.4 50.0 -7.2 50.0

Carbon disulfide Ave 1.480 1.253 0.0100 42.3 50.0 -15.4 50.0

Acetonitrile Ave 0.0297 0.0269 0.0010 362 400 -9.4 50.0

Methylene Chloride Ave 0.3812 0.3836 0.0100 50.3 50.0 0.6 50.0

Acrylonitrile Ave 0.0805 0.0736 0.0010 366 400 -8.6 50.0

trans-1,2-Dichloroethene Ave 0.4499 0.4452 0.0100 49.5 50.0 -1.1 50.0

Methyl tert-butyl ether Ave 0.7369 0.7075 0.0100 48.0 50.0 -4.0 50.0

1,1-Dichloroethane Ave 0.8857 0.8845 0.1000 49.9 50.0 -0.1 50.0

Vinyl acetate Ave 0.6255 0.4185 0.0100 33.5 50.0 -33.1 50.0

2,2-Dichloropropane Ave 0.7341 0.6657 0.0100 45.3 50.0 -9.3 50.0

cis-1,2-Dichloroethene Ave 0.4554 0.4549 0.0100 49.9 50.0 -0.1 50.0

2-Butanone (MEK) Ave 0.0924 0.0863 0.0100 46.7 50.0 -6.6 50.0

Propionitrile Ave 0.0203 0.0182 0.0010 359 400 -10.4 50.0

Bromochloromethane Ave 0.1785 0.1742 0.0100 48.8 50.0 -2.4 50.0

Tetrahydrofuran Ave 0.0578 0.0538 0.0100 46.5 50.0 -7.0 50.0

Chloroform Ave 0.7375 0.7347 0.0100 49.8 50.0 -0.4 20.0

1,1,1-Trichloroethane Ave 0.7394 0.7104 0.0100 48.0 50.0 -3.9 50.0

Carbon tetrachloride Ave 0.4834 0.4401 0.0100 45.5 50.0 -9.0 50.0

1,1-Dichloropropene Ave 0.6488 0.6621 0.0100 51.0 50.0 2.1 50.0

Benzene Ave 1.229 1.232 0.0100 50.1 50.0 0.2 50.0

1,2-Dichloroethane Ave 0.3536 0.3513 0.0100 49.7 50.0 -0.6 50.0

Trichloroethene Ave 0.3450 0.3532 0.0100 51.2 50.0 2.4 50.0

1,2-Dichloropropane Ave 0.3152 0.3160 0.0100 50.1 50.0 0.2 20.0

Dibromomethane Ave 0.1271 0.1218 0.0100 47.9 50.0 -4.2 50.0

Bromodichloromethane Ave 0.3600 0.3468 0.0100 48.2 50.0 -3.7 50.0

2-Chloroethyl vinyl ether Ave 0.1054 0.1098 0.0100 52.1 50.0 4.2 50.0

cis-1,3-Dichloropropene Ave 0.4091 0.3900 0.0100 47.7 50.0 -4.7 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1384 0.0100 45.1 50.0 -9.9 50.0

Toluene Ave 0.8177 0.8220 0.0100 50.3 50.0 0.5 20.0

trans-1,3-Dichloropropene Ave 0.3392 0.3154 0.0100 46.5 50.0 -7.0 50.0

FORM VII 8260B

Page 151 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/21/2012 11:31

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173708/2

DB624

TestAmerica Chicago

Lab File ID: 22C1221.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1703 0.0100 49.4 50.0 -1.2 50.0

Tetrachloroethene Ave 0.4537 0.4746 0.0100 52.3 50.0 4.6 50.0

1,3-Dichloropropane Ave 0.3491 0.3524 0.0100 50.5 50.0 0.9 50.0

2-Hexanone Ave 0.1204 0.1145 0.0100 47.5 50.0 -4.9 50.0

Dibromochloromethane Ave 0.2603 0.2581 0.0100 49.6 50.0 -0.8 50.0

1,2-Dibromoethane Ave 0.1651 0.1597 0.0100 48.4 50.0 -3.3 50.0

Chlorobenzene Ave 1.012 1.064 0.3000 52.6 50.0 5.2 50.0

1-Chlorohexane Ave 0.6865 0.7188 0.0100 52.4 50.0 4.7 50.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3343 0.0100 49.2 50.0 -1.7 50.0

Ethylbenzene Ave 0.5753 0.6209 0.0100 54.0 50.0 7.9 20.0

m&p-Xylene Ave 1.427 1.552 0.0100 109 100 8.7 50.0

o-Xylene Ave 1.456 1.523 0.0100 52.3 50.0 4.5 50.0

Styrene Ave 1.120 1.210 0.0100 54.0 50.0 8.0 50.0

Bromoform Ave 0.1536 0.1544 0.1000 50.3 50.0 0.5 50.0

Isopropylbenzene Ave 3.312 3.283 0.0100 49.6 50.0 -0.9 50.0

Bromobenzene Ave 0.7374 0.7156 0.0100 48.5 50.0 -3.0 50.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3740 0.3000 48.6 50.0 -2.7 50.0

1,2,3-Trichloropropane Ave 0.2827 0.2743 0.0100 48.5 50.0 -3.0 50.0

N-Propylbenzene Ave 3.971 4.083 0.0100 51.4 50.0 2.8 50.0

4-Chlorotoluene Ave 2.242 2.247 0.0100 50.1 50.0 0.2 50.0

1,3,5-Trimethylbenzene Ave 2.765 2.838 0.0100 51.3 50.0 2.6 50.0

2-Chlorotoluene Ave 2.663 2.692 0.0100 50.6 50.0 1.1 50.0

tert-Butylbenzene Ave 2.558 2.551 0.0100 49.9 50.0 -0.3 50.0

1,2,4-Trimethylbenzene Ave 2.713 2.728 0.0100 50.3 50.0 0.5 50.0

sec-Butylbenzene Ave 3.783 3.886 0.0100 51.4 50.0 2.7 50.0

1,3-Dichlorobenzene Ave 1.575 1.595 0.0100 50.6 50.0 1.3 50.0

p-Isopropyltoluene Ave 3.287 3.413 0.0100 51.9 50.0 3.8 50.0

1,4-Dichlorobenzene Ave 1.556 1.566 0.0100 50.3 50.0 0.7 50.0

1,2-Dichlorobenzene Ave 1.323 1.338 0.0100 50.5 50.0 1.1 50.0

n-Butylbenzene Ave 2.919 3.096 0.0100 53.0 50.0 6.1 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0527 0.0100 39.8 50.0 -20.3 50.0

1,2,4-Trichlorobenzene Ave 0.8970 0.9150 0.0100 51.0 50.0 2.0 50.0

Hexachlorobutadiene Ave 0.7568 0.7863 0.0100 52.0 50.0 3.9 50.0

Naphthalene Ave 0.9856 0.9108 0.0100 46.2 50.0 -7.6 50.0

1,2,3-Trichlorobenzene Ave 0.7171 0.7018 0.0100 48.9 50.0 -2.1 50.0

Dibromofluoromethane Ave 0.3990 0.3878 0.0100 48.6 50.0 -2.8 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2625 0.0100 47.0 50.0 -6.0 50.0

Toluene-d8 (Surr) Ave 1.184 1.172 0.0100 49.5 50.0 -1.0 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.5040 0.0100 50.3 50.0 0.7 50.0

FORM VII 8260B

Page 152 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/21/2012 11:57

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173708/3

DB624

TestAmerica Chicago

Lab File ID: 22D1221.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3990 0.3658 0.0100 45.9 50.0 -8.3 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2599 0.0100 46.5 50.0 -7.0 50.0

Toluene-d8 (Surr) Ave 1.184 1.153 0.0100 48.7 50.0 -2.6 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4837 0.0100 48.3 50.0 -3.4 50.0

FORM VII 8260B

Page 153 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/21/2012 11:57

12/11/2012 19:06

12/11/2012 23:48

CCV 500-173708/3

DB624

TestAmerica Chicago

Lab File ID: 22D1221.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Lin1 0.5624 0.0100 34.9 50.0 -30.2 50.0

Ethyl ether Ave 0.2603 0.2460 0.0100 47.3 50.0 -5.5 50.0

Iodomethane Lin1 0.5829 0.0100 88.2 100 -11.8 50.0

3-Chloropropene Ave 0.2462 0.2212 0.0100 89.9 100 -10.1 50.0

Methyl acetate Ave 0.2127 0.2037 0.0100 47.9 50.0 -4.3 50.0

Hexane Ave 0.8764 0.8088 0.0100 46.2 50.0 -7.7 50.0

2-Chloro-1,3-butadiene Ave 0.9423 0.9166 0.0100 48.6 50.0 -2.7 50.0

Isopropyl ether Ave 1.545 1.480 0.0100 47.9 50.0 -4.2 50.0

Ethyl acetate Ave 0.1956 0.1780 0.0100 455 500 -9.0 50.0

Methacrylonitrile Ave 0.1427 0.1395 0.0100 97.8 100 -2.2 50.0

Cyclohexane Lin1 0.996 0.0100 46.5 50.0 -7.0 50.0

Isobutyl alcohol Ave 0.0073 0.0061 0.0010 3362 4000 -16.0 50.0

2,2,4-Trimethylpentane Ave 1.673 1.667 0.0100 49.8 50.0 -0.3 50.0

Heptane Ave 0.7351 0.7336 0.0100 49.9 50.0 -0.2 50.0

n-Butyl alcohol Ave 0.0045 0.0035 0.0010 3086 4000 -22.9 50.0

Methylcyclohexane Ave 0.5969 0.6023 0.0100 50.5 50.0 0.9 50.0

Methyl methacrylate Ave 0.1655 0.1576 0.0100 95.3 100 -4.7 50.0

2-Nitropropane Ave 0.0618 0.0656 0.0100 4251 4000 6.3 50.0

Ethyl methacrylate Ave 0.2528 0.2439 0.0100 96.5 100 -3.5 50.0

Cyclohexanone Ave 0.0256 0.0525 0.0100 8220 4000 105.5* 50.0

trans-1,4-Dichloro-2-butene Ave 0.0710 0.0557 0.0100 78.5 100 -21.5 50.0

Pentachloroethane Ave 0.2758 0.2699 0.0100 97.9 100 -2.1 50.0

1,3,5-Trichlorobenzene Ave 1.226 1.252 0.0100 51.1 50.0 2.1 50.0

2-Methylnaphthalene Ave 0.6831 0.5773 0.0100 42.3 50.0 -15.5 50.0

FORM VII 8260B

Page 154 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/24/2012 11:43

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173827/2

DB624

TestAmerica Chicago

Lab File ID: 22C1224.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.6395 0.0100 59.0 50.0 18.0 50.0

Chloromethane Ave 0.7111 0.7439 0.1000 52.3 50.0 4.6 50.0

Vinyl chloride Ave 0.6381 0.6817 0.0100 53.4 50.0 6.8 20.0

Bromomethane Ave 0.1998 0.2696 0.0100 67.5 50.0 34.9 50.0

Chloroethane Ave 0.3338 0.3932 0.0100 58.9 50.0 17.8 50.0

Dichlorofluoromethane Ave 0.999 1.010 0.0100 50.5 50.0 1.1 50.0

Trichlorofluoromethane Ave 0.8265 0.8689 0.0100 52.6 50.0 5.1 50.0

Acrolein Ave 0.0397 0.0459 0.0010 2312 2000 15.6 50.0

1,1-Dichloroethene Ave 0.4001 0.4293 0.0100 53.6 50.0 7.3 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.5317 0.0100 54.7 50.0 9.4 50.0

Acetone Ave 0.0639 0.0568 0.0100 44.4 50.0 -11.2 50.0

Carbon disulfide Ave 1.480 1.236 0.0100 41.8 50.0 -16.5 50.0

Acetonitrile Ave 0.0297 0.0309 0.0010 415 400 3.7 50.0

Methylene Chloride Ave 0.3812 0.3945 0.0100 51.8 50.0 3.5 50.0

Acrylonitrile Ave 0.0805 0.0858 0.0010 426 400 6.6 50.0

trans-1,2-Dichloroethene Ave 0.4499 0.4722 0.0100 52.5 50.0 5.0 50.0

Methyl tert-butyl ether Ave 0.7369 0.7217 0.0100 49.0 50.0 -2.1 50.0

1,1-Dichloroethane Ave 0.8857 0.9220 0.1000 52.1 50.0 4.1 50.0

Vinyl acetate Ave 0.6255 0.4971 0.0100 39.7 50.0 -20.5 50.0

2,2-Dichloropropane Ave 0.7341 0.7559 0.0100 51.5 50.0 3.0 50.0

cis-1,2-Dichloroethene Ave 0.4554 0.4715 0.0100 51.8 50.0 3.5 50.0

2-Butanone (MEK) Ave 0.0924 0.0892 0.0100 48.3 50.0 -3.5 50.0

Propionitrile Ave 0.0203 0.0220 0.0010 433 400 8.3 50.0

Bromochloromethane Ave 0.1785 0.1859 0.0100 52.1 50.0 4.1 50.0

Tetrahydrofuran Ave 0.0578 0.0555 0.0100 47.9 50.0 -4.1 50.0

Chloroform Ave 0.7375 0.7718 0.0100 52.3 50.0 4.7 20.0

1,1,1-Trichloroethane Ave 0.7394 0.7594 0.0100 51.4 50.0 2.7 50.0

Carbon tetrachloride Ave 0.4834 0.4866 0.0100 50.3 50.0 0.7 50.0

1,1-Dichloropropene Ave 0.6488 0.6934 0.0100 53.4 50.0 6.9 50.0

Benzene Ave 1.229 1.290 0.0100 52.5 50.0 4.9 50.0

1,2-Dichloroethane Ave 0.3536 0.3785 0.0100 53.5 50.0 7.0 50.0

Trichloroethene Ave 0.3450 0.3696 0.0100 53.6 50.0 7.1 50.0

1,2-Dichloropropane Ave 0.3152 0.3333 0.0100 52.9 50.0 5.7 20.0

Dibromomethane Ave 0.1271 0.1334 0.0100 52.5 50.0 5.0 50.0

Bromodichloromethane Ave 0.3600 0.3861 0.0100 53.6 50.0 7.3 50.0

2-Chloroethyl vinyl ether Ave 0.1054 0.1109 0.0100 52.6 50.0 5.2 50.0

cis-1,3-Dichloropropene Ave 0.4091 0.4326 0.0100 52.9 50.0 5.7 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1438 0.0100 46.8 50.0 -6.4 50.0

Toluene Ave 0.8177 0.8913 0.0100 54.5 50.0 9.0 20.0

trans-1,3-Dichloropropene Ave 0.3392 0.3473 0.0100 51.2 50.0 2.4 50.0

FORM VII 8260B

Page 155 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/24/2012 11:43

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173827/2

DB624

TestAmerica Chicago

Lab File ID: 22C1224.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1828 0.0100 53.0 50.0 6.0 50.0

Tetrachloroethene Ave 0.4537 0.4850 0.0100 53.5 50.0 6.9 50.0

1,3-Dichloropropane Ave 0.3491 0.3722 0.0100 53.3 50.0 6.6 50.0

2-Hexanone Ave 0.1204 0.1115 0.0100 46.3 50.0 -7.4 50.0

Dibromochloromethane Ave 0.2603 0.2825 0.0100 54.3 50.0 8.6 50.0

1,2-Dibromoethane Ave 0.1651 0.1723 0.0100 52.2 50.0 4.3 50.0

Chlorobenzene Ave 1.012 1.118 0.3000 55.2 50.0 10.4 50.0

1-Chlorohexane Ave 0.6865 0.7687 0.0100 56.0 50.0 12.0 50.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3650 0.0100 53.7 50.0 7.4 50.0

Ethylbenzene Ave 0.5753 0.6414 0.0100 55.7 50.0 11.5 20.0

m&p-Xylene Ave 1.427 1.647 0.0100 115 100 15.4 50.0

o-Xylene Ave 1.456 1.644 0.0100 56.4 50.0 12.9 50.0

Styrene Ave 1.120 1.290 0.0100 57.6 50.0 15.2 50.0

Bromoform Ave 0.1536 0.1670 0.1000 54.3 50.0 8.7 50.0

Isopropylbenzene Ave 3.312 3.559 0.0100 53.7 50.0 7.5 50.0

Bromobenzene Ave 0.7374 0.7771 0.0100 52.7 50.0 5.4 50.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.4010 0.3000 52.2 50.0 4.3 50.0

1,2,3-Trichloropropane Ave 0.2827 0.2996 0.0100 53.0 50.0 6.0 50.0

N-Propylbenzene Ave 3.971 4.412 0.0100 55.6 50.0 11.1 50.0

4-Chlorotoluene Ave 2.242 2.455 0.0100 54.8 50.0 9.5 50.0

1,3,5-Trimethylbenzene Ave 2.765 3.063 0.0100 55.4 50.0 10.8 50.0

2-Chlorotoluene Ave 2.663 2.919 0.0100 54.8 50.0 9.6 50.0

tert-Butylbenzene Ave 2.558 2.745 0.0100 53.7 50.0 7.3 50.0

1,2,4-Trimethylbenzene Ave 2.713 2.977 0.0100 54.9 50.0 9.7 50.0

sec-Butylbenzene Ave 3.783 4.175 0.0100 55.2 50.0 10.4 50.0

1,3-Dichlorobenzene Ave 1.575 1.689 0.0100 53.6 50.0 7.3 50.0

p-Isopropyltoluene Ave 3.287 3.669 0.0100 55.8 50.0 11.6 50.0

1,4-Dichlorobenzene Ave 1.556 1.684 0.0100 54.1 50.0 8.2 50.0

1,2-Dichlorobenzene Ave 1.323 1.448 0.0100 54.7 50.0 9.4 50.0

n-Butylbenzene Ave 2.919 3.331 0.0100 57.1 50.0 14.1 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0611 0.0100 46.2 50.0 -7.5 50.0

1,2,4-Trichlorobenzene Ave 0.8970 0.9477 0.0100 52.8 50.0 5.7 50.0

Hexachlorobutadiene Ave 0.7568 0.8182 0.0100 54.1 50.0 8.1 50.0

Naphthalene Ave 0.9856 0.9710 0.0100 49.3 50.0 -1.5 50.0

1,2,3-Trichlorobenzene Ave 0.7171 0.7398 0.0100 51.6 50.0 3.2 50.0

Dibromofluoromethane Ave 0.3990 0.3785 0.0100 47.4 50.0 -5.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2537 0.0100 45.4 50.0 -9.2 50.0

Toluene-d8 (Surr) Ave 1.184 1.143 0.0100 48.3 50.0 -3.4 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4700 0.0100 46.9 50.0 -6.1 50.0

FORM VII 8260B

Page 156 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/24/2012 12:09

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173827/3

DB624

TestAmerica Chicago

Lab File ID: 22D1224.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3990 0.3458 0.0100 43.3 50.0 -13.3 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2456 0.0100 44.0 50.0 -12.1 50.0

Toluene-d8 (Surr) Ave 1.184 1.115 0.0100 47.1 50.0 -5.8 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4711 0.0100 47.1 50.0 -5.9 50.0

FORM VII 8260B

Page 157 of 332 01/04/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53342-1

CMS22

12/24/2012 12:09

12/11/2012 19:06

12/11/2012 23:48

CCV 500-173827/3

DB624

TestAmerica Chicago

Lab File ID: 22D1224.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Lin1 0.5251 0.0100 32.6 50.0 -34.7 50.0

Ethyl ether Ave 0.2603 0.2277 0.0100 43.7 50.0 -12.5 50.0

Iodomethane Lin1 0.5570 0.0100 84.4 100 -15.7 50.0

3-Chloropropene Ave 0.2462 0.2214 0.0100 89.9 100 -10.1 50.0

Methyl acetate Ave 0.2127 0.1957 0.0100 46.0 50.0 -8.0 50.0

Hexane Ave 0.8764 0.7801 0.0100 44.5 50.0 -11.0 50.0

2-Chloro-1,3-butadiene Ave 0.9423 0.8618 0.0100 45.7 50.0 -8.6 50.0

Isopropyl ether Ave 1.545 1.375 0.0100 44.5 50.0 -11.0 50.0

Ethyl acetate Ave 0.1956 0.1702 0.0100 435 500 -13.0 50.0

Methacrylonitrile Ave 0.1427 0.1285 0.0100 90.1 100 -9.9 50.0

Cyclohexane Lin1 0.9215 0.0100 42.9 50.0 -14.1 50.0

Isobutyl alcohol Ave 0.0073 0.0063 0.0010 3490 4000 -12.8 50.0

2,2,4-Trimethylpentane Ave 1.673 1.570 0.0100 47.0 50.0 -6.1 50.0

Heptane Ave 0.7351 0.6901 0.0100 46.9 50.0 -6.1 50.0

n-Butyl alcohol Ave 0.0045 0.0036 0.0010 3178 4000 -20.6 50.0

Methylcyclohexane Ave 0.5969 0.5568 0.0100 46.6 50.0 -6.7 50.0

Methyl methacrylate Ave 0.1655 0.1550 0.0100 93.7 100 -6.4 50.0

2-Nitropropane Ave 0.0618 0.0660 0.0100 4275 4000 6.9 50.0

Ethyl methacrylate Ave 0.2528 0.2372 0.0100 93.8 100 -6.2 50.0

Cyclohexanone Ave 0.0256 0.0502 0.0100 7852 4000 96.3* 50.0

trans-1,4-Dichloro-2-butene Ave 0.0710 0.0589 0.0100 82.9 100 -17.1 50.0

Pentachloroethane Ave 0.2758 0.2673 0.0100 96.9 100 -3.1 50.0

1,3,5-Trichlorobenzene Ave 1.226 1.143 0.0100 46.6 50.0 -6.8 50.0

2-Methylnaphthalene Ave 0.6831 0.5262 0.0100 38.5 50.0 -23.0 50.0

FORM VII 8260B

Page 158 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: MB 500-173515/4

Matrix: Lab File ID: 16M1220.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/20/2012 09:00

DB624 ID:

Analysis Batch No.: 173515 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 2.16

78-93-3 2-Butanone (MEK) <5.00 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 106 70-134

2037-26-5 Toluene-d8 (Surr) 113 75-122

460-00-4 4-Bromofluorobenzene (Surr) 107 70-122

1868-53-7 Dibromofluoromethane 103 75-120

FORM I 8260B

Page 159 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: MB 500-173708/6

Matrix: Lab File ID: 22M1221.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5 (mL)

0.2(mm)

Date Analyzed: 12/21/2012 13:16

DB624 ID:

Analysis Batch No.: 173708 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.30

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 90 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 88 75-120

1868-53-7 Dibromofluoromethane 88 75-120

FORM I 8260B

Page 160 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: MB 500-173827/6

Matrix: Lab File ID: 22M1224.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/24/2012 13:33

DB624 ID:

Analysis Batch No.: 173827 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 90 75-125

2037-26-5 Toluene-d8 (Surr) 96 75-120

460-00-4 4-Bromofluorobenzene (Surr) 88 75-120

1868-53-7 Dibromofluoromethane 92 75-120

FORM I 8260B

Page 161 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: LCS 500-173515/5

Matrix: Lab File ID: 16S1220.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/20/2012 09:23

DB624 ID:

Analysis Batch No.: 173515 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 43.68 5.00 2.16

78-93-3 2-Butanone (MEK) 45.67 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 98 70-134

2037-26-5 Toluene-d8 (Surr) 111 75-122

460-00-4 4-Bromofluorobenzene (Surr) 102 70-122

1868-53-7 Dibromofluoromethane 103 75-120

FORM I 8260B

Page 162 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: LCS 500-173708/4

Matrix: Lab File ID: 22S1221.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5 (mL)

0.2(mm)

Date Analyzed: 12/21/2012 12:23

DB624 ID:

Analysis Batch No.: 173708 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 46.74 5.00 1.30

78-93-3 2-Butanone (MEK) 41.90 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 94 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 103 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 163 of 332 01/04/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53342-1

Lab Sample ID: LCS 500-173827/4

Matrix: Lab File ID: 22S1224.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/24/2012 12:35

DB624 ID:

Analysis Batch No.: 173827 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 48.03 5.00 1.29

78-93-3 2-Butanone (MEK) 50.18 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 92 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 94 75-120

1868-53-7 Dibromofluoromethane 92 75-120

FORM I 8260B

Page 164 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS16

170196

Start Date:

End Date: 11/19/2012 17:14

11/19/2012 11:14

BFB 500-170196/5 11/19/2012 11:14 1 16B1119c.D DB624 0.2(mm)

STD1 500-170196/6 IC 11/19/2012 12:14 1 16I1119A.D DB624 0.2(mm)

STD2 500-170196/7 IC 11/19/2012 12:37 1 16I1119B.D DB624 0.2(mm)

STD3 500-170196/8 

ICIS

11/19/2012 13:00 1 16I1119C.D DB624 0.2(mm)

STD4 500-170196/9 IC 11/19/2012 13:23 1 16I1119D.D DB624 0.2(mm)

STD5 500-170196/10 

IC

11/19/2012 13:46 1 16I1119E.D DB624 0.2(mm)

STD6 500-170196/11 

IC

11/19/2012 14:09 1 16I1119F.D DB624 0.2(mm)

STD1AP 500-170196/12 

IC

11/19/2012 14:32 1 DB624 0.2(mm)

STD2AP 500-170196/13 

IC

11/19/2012 14:55 1 DB624 0.2(mm)

STD3AP 500-170196/14 

IC

11/19/2012 15:18 1 DB624 0.2(mm)

STD4AP 500-170196/15 

IC

11/19/2012 15:42 1 DB624 0.2(mm)

STD5AP 500-170196/16 

IC

11/19/2012 16:05 1 DB624 0.2(mm)

STD6AP 500-170196/17 

IC

11/19/2012 16:28 1 DB624 0.2(mm)

ICV 500-170196/19 11/19/2012 17:14 1 16S1119.D DB624 0.2(mm)

8260B

Page 165 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS16

173515

Start Date:

End Date: 12/20/2012 14:38

12/20/2012 07:38

BFB 500-173515/6 12/20/2012 07:38 1 16B1220a.D DB624 0.2(mm)

CCV 500-173515/2 12/20/2012 08:13 1 16C1220.D DB624 0.2(mm)

CCV 500-173515/3 12/20/2012 08:36 1 16D1220.D DB624 0.2(mm)

MB 500-173515/4 12/20/2012 09:00 1 16M1220.D DB624 0.2(mm)

LCS 500-173515/5 12/20/2012 09:23 1 16S1220.D DB624 0.2(mm)

ZZZZZ 12/20/2012 09:59 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 10:23 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 10:46 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 11:09 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 11:32 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 11:55 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 12:19 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 12:42 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 13:05 1 DB624 0.2(mm)

ZZZZZ 12/20/2012 13:28 1 DB624 0.2(mm)

500-53342-2 FC Composite 5 12/20/2012 13:52 1 53342-02.D DB624 0.2(mm)

ZZZZZ 12/20/2012 14:38 1 DB624 0.2(mm)

8260B

Page 166 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS22

172614

Start Date:

End Date: 12/12/2012 00:17

12/11/2012 13:45

BFB 500-172614/1 12/11/2012 13:45 1 22B1211.D DB624 0.2(mm)

STD01 500-172614/2 

IC

12/11/2012 14:23 1 22I1211A.D DB624 0.2(mm)

STD02 500-172614/3 

IC

12/11/2012 14:51 1 22I1211B.D DB624 0.2(mm)

STD03 500-172614/4 

IC

12/11/2012 15:20 1 22I1211C.D DB624 0.2(mm)

STD04 500-172614/5 

IC

12/11/2012 15:48 1 22I1211D.D DB624 0.2(mm)

STD05 500-172614/6 

IC

12/11/2012 16:16 1 22I1211E.D DB624 0.2(mm)

STD06 500-172614/7 

ICIS

12/11/2012 16:44 1 22I1211F.D DB624 0.2(mm)

STD07 500-172614/8 

IC

12/11/2012 17:13 1 22I1211G.D DB624 0.2(mm)

STD08 500-172614/9 

IC

12/11/2012 17:41 1 22I1211H.D DB624 0.2(mm)

STD09 500-172614/10 

IC

12/11/2012 18:09 1 22I1211I.D DB624 0.2(mm)

STD02AP 

500-172614/12 IC

12/11/2012 19:06 1 DB624 0.2(mm)

STD05AP 

500-172614/15 IC

12/11/2012 20:30 1 DB624 0.2(mm)

STD06AP 

500-172614/16 IC

12/11/2012 20:59 1 DB624 0.2(mm)

STD07AP 

500-172614/17 IC

12/11/2012 21:27 1 DB624 0.2(mm)

STD08AP 

500-172614/18 IC

12/11/2012 21:55 1 DB624 0.2(mm)

STD09AP 

500-172614/19 IC

12/11/2012 22:24 1 DB624 0.2(mm)

STD03AP 

500-172614/21 IC

12/11/2012 23:20 1 DB624 0.2(mm)

STD04AP 

500-172614/22 IC

12/11/2012 23:48 1 DB624 0.2(mm)

ICV 500-172614/23 12/12/2012 00:17 1 22S1211.D DB624 0.2(mm)

8260B

Page 167 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS22

172615

Start Date:

End Date: 12/12/2012 00:17

12/11/2012 13:45

BFB 500-172615/1 12/11/2012 13:45 1 22B1211.D DB624 0.2(mm)

STD01 500-172615/2 

IC

12/11/2012 14:23 1 22I1211A.D DB624 0.2(mm)

STD02 500-172615/3 

IC

12/11/2012 14:51 1 22I1211B.D DB624 0.2(mm)

STD03 500-172615/4 

IC

12/11/2012 15:20 1 22I1211C.D DB624 0.2(mm)

STD04 500-172615/5 

IC

12/11/2012 15:48 1 22I1211D.D DB624 0.2(mm)

STD05 500-172615/6 

IC

12/11/2012 16:16 1 22I1211E.D DB624 0.2(mm)

STD06 500-172615/7 

ICIS

12/11/2012 16:44 1 22I1211F.D DB624 0.2(mm)

STD07 500-172615/8 

IC

12/11/2012 17:13 1 22I1211G.D DB624 0.2(mm)

STD08 500-172615/9 

IC

12/11/2012 17:41 1 22I1211H.D DB624 0.2(mm)

STD09 500-172615/10 

IC

12/11/2012 18:09 1 22I1211I.D DB624 0.2(mm)

STD02AP 

500-172615/12 IC

12/11/2012 19:06 1 DB624 0.2(mm)

STD05AP 

500-172615/15 IC

12/11/2012 20:30 1 DB624 0.2(mm)

STD06AP 

500-172615/16 IC

12/11/2012 20:59 1 DB624 0.2(mm)

STD07AP 

500-172615/17 IC

12/11/2012 21:27 1 DB624 0.2(mm)

STD08AP 

500-172615/18 IC

12/11/2012 21:55 1 DB624 0.2(mm)

STD09AP 

500-172615/19 IC

12/11/2012 22:24 1 DB624 0.2(mm)

STD03AP 

500-172615/21 IC

12/11/2012 23:20 1 DB624 0.2(mm)

STD04AP 

500-172615/22 IC

12/11/2012 23:48 1 DB624 0.2(mm)

ICV 500-172615/23 12/12/2012 00:17 1 22S1211.D DB624 0.2(mm)

8260B

Page 168 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS22

173708

Start Date:

End Date: 12/21/2012 22:40

12/21/2012 10:53

BFB 500-173708/1 12/21/2012 10:53 1 22B1221.D DB624 0.2(mm)

CCV 500-173708/2 12/21/2012 11:31 1 22C1221.D DB624 0.2(mm)

CCV 500-173708/3 12/21/2012 11:57 1 22D1221.D DB624 0.2(mm)

LCS 500-173708/4 12/21/2012 12:23 1 22S1221.D DB624 0.2(mm)

MB 500-173708/6 12/21/2012 13:16 1 22M1221.D DB624 0.2(mm)

500-53342-2 DL FC Composite 5 DL 12/21/2012 22:40 50 53342-02.D DB624 0.2(mm)

8260B

Page 169 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53342-1

CMS22

173827

Start Date:

End Date: 12/24/2012 22:42

12/24/2012 11:02

BFB 500-173827/1 12/24/2012 11:02 1 22B1224.D DB624 0.2(mm)

CCV 500-173827/2 12/24/2012 11:43 1 22C1224.D DB624 0.2(mm)

CCV 500-173827/3 12/24/2012 12:09 1 22D1224.D DB624 0.2(mm)

LCS 500-173827/4 12/24/2012 12:35 1 22S1224.D DB624 0.2(mm)

MB 500-173827/6 12/24/2012 13:33 1 22M1224.D DB624 0.2(mm)

500-53342-4 Trip Blank 12/24/2012 13:59 1 53342-04.D DB624 0.2(mm)

500-53342-3 FC EB 5 12/24/2012 14:25 1 53342-03.D DB624 0.2(mm)

ZZZZZ 12/24/2012 14:51 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 15:17 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 15:43 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 16:10 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 16:37 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 17:03 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 17:29 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 17:55 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 18:21 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 18:47 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 19:13 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 19:40 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 20:06 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 20:32 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 20:58 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 21:24 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 21:50 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 22:16 1 DB624 0.2(mm)

ZZZZZ 12/24/2012 22:42 1 DB624 0.2(mm)

8260B

Page 170 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173454 12/19/12 13:00 Estes, William R

Batch Method:

TestAmerica Chicago

5030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount AnalysisComment

FC Composite 5 5 g 5 mL MeOH from soil 

jar

500-53342-A-2 5030B, 8260B T

Batch Notes

Balance ID C-0133

Methanol Lot Number DH247

Pipette ID C-2207

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

8260B Page 1 of 1

Page 171 of 332 01/04/2013


METALS

Page 174 of 332 01/04/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

METALS

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53342-1

FC Composite 5 500-53342-1 

FC EB 5 500-53342-3 

Comments:

Page 175 of 332 01/04/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40

500-53342-1

FC Composite 5

Solid Date Sampled: 12/17/2012 14:50

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 30.0

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 409 3.01 0.358 mg/Kg 1 6010B

7440-50-8 Copper 693 3.01 0.815 mg/Kg 1 6010B

7440-47-3 Chromium 14200 3.01 0.502 mg/Kg 1 6010B

7440-02-0 Nickel 77.4 3.01 0.659 mg/Kg B 1 6010B

7439-92-1 Lead 250 1.50 0.517 mg/Kg B 1 6010B

7440-62-2 Vanadium 238 1.50 0.228 mg/Kg 1 6010B

7440-66-6 Zinc 441 6.02 2.06 mg/Kg 1 6010B

7439-97-6 Mercury 0.321 0.0540 0.0206 mg/Kg 1 7471A

FORM IA-IN Page 176 of 332 01/04/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40

500-53342-1

FC Composite 5

Solid Date Sampled: 12/17/2012 14:50

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.500 0.500 0.0100 mg/L 1 6010B

7440-50-8 Copper <0.0250 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium 0.166 0.0250 0.0100 mg/L 1 6010B

7440-02-0 Nickel 0.531 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium 0.00669 0.0250 0.00500 mg/L J 1 6010B

7440-66-6 Zinc 0.0502 0.100 0.0200 mg/L J 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000020 mg/L

0

1 7470A

FORM IA-IN Page 177 of 332 01/04/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-3

Date Received: 12/18/2012 09:40

500-53342-1

FC EB 5

Water Date Sampled: 12/17/2012 14:30

Reporting Basis: WET

METALS

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.0100 0.0100 0.000440 mg/L 1 6010B

7440-50-8 Copper 0.00616 0.0100 0.00106 mg/L J 1 6010B

7440-47-3 Chromium <0.0100 0.0100 0.000960 mg/L 1 6010B

7440-02-0 Nickel <0.0100 0.0100 0.00190 mg/L 1 6010B

7439-92-1 Lead 0.00245 0.00500 0.00158 mg/L J B 1 6010B

7440-62-2 Vanadium <0.00500 0.00500 0.000620 mg/L 1 6010B

7440-66-6 Zinc 0.00789 0.0200 0.00472 mg/L J 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000071 mg/L

0

1 7470A

FORM IA-IN Page 178 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173517/10

12/19/2012 09:45

Found C True %R

CCV 500-173517/15

12/19/2012 10:20

CCV 500-173517/27

12/19/2012 11:45

Found C True %R Found C True %R

Barium 0.4009 0.400 100 0.4996 0.500 100 0.5050 0.500 101

Chromium 0.4092 0.400 102 0.5119 0.500 102 0.5055 0.500 101

Copper 0.4066 0.400 102 0.5085 0.500 102 0.5117 0.500 102

Lead 0.4102 0.400 103 0.5092 0.500 102 0.5026 0.500 101

Nickel 0.4046 0.400 101 0.5056 0.500 101 0.5011 0.500 100

Vanadium 4.040 4.00 101 5.048 5.00 101 5.027 5.00 101

Zinc 0.4049 0.400 101 0.5067 0.500 101 0.4940 0.500 99

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 179 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173517/39

12/19/2012 13:02

Found C True %R

CCV 500-173517/51

12/19/2012 14:26

CCV 500-173517/63

12/19/2012 15:47

Found C True %R Found C True %R

Barium 0.5058 0.500 101 0.4985 0.500 100 0.5064 0.500 101

Chromium 0.5060 0.500 101 0.5069 0.500 101 0.5161 0.500 103

Copper 0.5141 0.500 103 0.5071 0.500 101 0.5146 0.500 103

Lead 0.5023 0.500 100 0.5049 0.500 101 0.5134 0.500 103

Nickel 0.5009 0.500 100 0.5041 0.500 101 0.5121 0.500 102

Vanadium 5.029 5.00 101 5.027 5.00 101 5.116 5.00 102

Zinc 0.4922 0.500 98 0.5013 0.500 100 0.5102 0.500 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 180 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173518/10

12/19/2012 18:41

Found C True %R

CCV 500-173518/27

12/19/2012 20:32

CCV 500-173518/39

12/19/2012 21:57

Found C True %R Found C True %R

Barium 0.4028 0.400 101 0.5103 0.500 102 0.5135 0.500 103

Chromium 0.4072 0.400 102 0.5110 0.500 102 0.5092 0.500 102

Copper 0.4055 0.400 101 0.5154 0.500 103 0.5149 0.500 103

Lead 0.4072 0.400 102 0.5098 0.500 102 0.5055 0.500 101

Nickel 0.4012 0.400 100 0.5034 0.500 101 0.5014 0.500 100

Vanadium 4.032 4.00 101 5.081 5.00 102 5.067 5.00 101

Zinc 0.4013 0.400 100 0.4996 0.500 100 0.4948 0.500 99

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 181 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173518/51

12/19/2012 23:21

Found C True %R Found C True %R Found C True %R

Barium 0.5130 0.500 103

Chromium 0.5100 0.500 102

Copper 0.5146 0.500 103

Lead 0.5098 0.500 102

Nickel 0.5037 0.500 101

Vanadium 5.078 5.00 102

Zinc 0.4979 0.500 100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 182 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173573/7

12/20/2012 09:11

Found C True %R

CCV 500-173573/20

12/20/2012 09:39

Found C True %R Found C True %R

Mercury 1.930 2.00 97 1.270 1.00 127

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 183 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173574/7

12/20/2012 09:59

Found C True %R

CCV 500-173574/10

12/20/2012 10:05

CCV 500-173574/22

12/20/2012 10:28

Found C True %R Found C True %R

Mercury 1.990 2.00 100 0.9540 1.00 95 0.9780 1.00 98

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 184 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173572/7

12/20/2012 08:24

Found C True %R

CCV 500-173572/31

12/20/2012 09:12

CCV 500-173572/43

12/20/2012 09:34

Found C True %R Found C True %R

Mercury 2.086 2.00 104 1.022 J 1.00 102 1.082 J 1.00 108

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 185 of 332 01/04/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53342-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-173572/55

12/20/2012 09:57

Found C True %R

CCV 500-173572/67

12/20/2012 10:19

CCV 500-173572/75

12/20/2012 10:34

Found C True %R Found C True %R

Mercury <2.00 1.00 93 1.017 1.00 102 1.016 1.00 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 186 of 332 01/04/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173517/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.01990 100 50-150

Copper 0.0200 0.01955 98 50-150

Chromium 0.0200 0.02070 104 50-150

Nickel 0.0200 0.02010 101 50-150

Lead 0.0100 0.01229 123 50-150

Vanadium 0.0100 0.01023 102 50-150

Zinc 0.0400 0.04138 103 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173517/75

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02015 101 50-150

Copper 0.0200 0.01926 96 50-150

Chromium 0.0200 0.02135 107 50-150

Nickel 0.0200 0.02068 103 50-150

Lead 0.0100 0.01158 116 50-150

Vanadium 0.0100 0.01071 107 50-150

Zinc 0.0400 0.04222 106 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173518/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02016 101 50-150

Copper 0.0200 0.01972 99 50-150

Chromium 0.0200 0.02105 105 50-150

Nickel 0.0200 0.01981 99 50-150

Lead 0.0100 0.01011 101 50-150

Vanadium 0.0100 0.01023 102 50-150

Zinc 0.0400 0.04064 102 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 187 of 332 01/04/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

CRQL CHECK STANDARD

METALS

Method: 7470A Instrument ID: HG6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173572/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 <2.00 96 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 188 of 332 01/04/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

CRQL CHECK STANDARD

METALS

Method: 7471A Instrument ID: HG5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173573/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.1280 J ^ 64 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173574/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.1810 J 91 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 189 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173517/11 CCB 500-173517/16 CCB 500-173517/28 CCB 500-173517/40

12/19/2012 09:53 12/19/2012 10:26 12/19/2012 11:51 12/19/2012 13:08

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 190 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

mg/L

Analyte RL Found C Found C Found C Found C

CCB 500-173517/52 CCB 500-173517/64

12/19/2012 14:32 12/19/2012 15:53

3-IN

Barium 0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 191 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173518/11 CCB 500-173518/28 CCB 500-173518/40 CCB 500-173518/52

12/19/2012 18:48 12/19/2012 20:38 12/19/2012 22:04 12/19/2012 23:27

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 192 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173573/8 CCB 500-173573/21

12/20/2012 09:12 12/20/2012 09:41

3-IN

Mercury 0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 193 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173574/8 CCB 500-173574/11 CCB 500-173574/23

12/20/2012 10:01 12/20/2012 10:07 12/20/2012 10:30

3-IN

Mercury 0.200 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 194 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173572/8 CCB 500-173572/32 CCB 500-173572/44 CCB 500-173572/56

12/20/2012 08:26 12/20/2012 09:13 12/20/2012 09:36 12/20/2012 09:59

3-IN

Mercury 2.00 <2.00 <2.00 <2.00 <2.00

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 195 of 332 01/04/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53342-1

ug/L

Analyte RL Found C Found C Found C Found C

CCB 500-173572/68 CCB 500-173572/76

12/20/2012 10:21 12/20/2012 10:36

3-IN

Mercury 2.00 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 196 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173339/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: ICP5

METHOD BLANK

METALS

 173517

TestAmerica Chicago

7440-39-3 Barium <1.00 6010B

7440-50-8 Copper <1.00 6010B

7440-47-3 Chromium <1.00 6010B

7440-02-0 Nickel 0.3300 J 6010B

7439-92-1 Lead 0.2580 J 6010B

7440-62-2 Vanadium <0.500 6010B

7440-66-6 Zinc <2.00 6010B

FORM III-IN

Page 197 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173349/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: ICP5

METHOD BLANK

METALS

 173517

TestAmerica Chicago

7440-39-3 Barium 0.002710 J 6010B

7440-50-8 Copper <0.0100 6010B

7440-47-3 Chromium 0.001210 J 6010B

7440-02-0 Nickel <0.0100 6010B

7439-92-1 Lead 0.002720 J 6010B

7440-62-2 Vanadium <0.00500 6010B

7440-66-6 Zinc <0.0200 6010B

FORM III-IN

Page 198 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-173323/1-B

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: ICP5

METHOD BLANK

METALS - TCLP

 173518

TestAmerica Chicago

7440-39-3 Barium <0.500 6010B

7440-50-8 Copper <0.0250 6010B

7440-47-3 Chromium <0.0250 6010B

7440-02-0 Nickel <0.0250 6010B

7439-92-1 Lead <0.0500 6010B

7440-62-2 Vanadium <0.0250 6010B

7440-66-6 Zinc <0.100 6010B

FORM III-IN

Page 199 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173428/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: HG6

METHOD BLANK

METALS

 173572

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 200 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-173323/1-C

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: HG6

METHOD BLANK

METALS - TCLP

 173572

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 201 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173393/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53342-1

Instrument Code: HG5

METHOD BLANK

METALS

 173573

TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN

Page 202 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSA 500-173517/13

P51219A

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0020

Copper -0.0022

Lead 0.0054

Nickel 0.0008

Vanadium 0.0041

Zinc 0.0081

Aluminum 500 509 102

Antimony -0.0017

Arsenic -0.0012

Beryllium 0.0000

Boron 0.0004

Cadmium 0.0040

Calcium 500 479 96

Cobalt 0.0001

Iron 200 189 95

Magnesium 500 517 103

Manganese 0.0035

Molybdenum 0.0125

Potassium -0.0053

Selenium 0.0002

Silicon 0.0151

Silver 0.0000

Sodium 0.0079

Strontium 0.0023

Thallium 0.0073

Tin 0.0014

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 203 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSAB 500-173517/14

P51219A

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.518 104

Chromium 0.500 0.482 96

Copper 0.500 0.560 112

Lead 0.0500 0.0528 106

Nickel 1.00 0.948 95

Vanadium 0.500 0.508 102

Zinc 1.00 0.902 90

Aluminum 500 511 102

Antimony 0.600 0.617 103

Arsenic 0.100 0.104 104

Beryllium 0.500 0.481 96

Boron 0.0011

Cadmium 1.00 0.941 94

Calcium 500 479 96

Cobalt 0.500 0.472 94

Iron 200 191 95

Magnesium 500 519 104

Manganese 0.500 0.501 100

Molybdenum 0.0124

Potassium -0.0129

Selenium 0.0500 0.0472 94

Silicon 0.0159

Silver 0.200 0.223 111

Sodium 0.0129

Strontium 0.0023

Thallium 0.100 0.104 104

Tin 0.0020

Titanium 0.0009

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 204 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSA 500-173517/76

P51219A

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0003

Chromium 0.0021

Copper -0.0025

Lead 0.0038

Nickel 0.0004

Vanadium 0.0041

Zinc 0.0080

Aluminum 500 507 101

Antimony 0.0003

Arsenic -0.0005

Beryllium -0.0001

Boron 0.0010

Cadmium 0.0035

Calcium 500 488 98

Cobalt 0.0000

Iron 200 193 97

Magnesium 500 522 104

Manganese 0.0045

Molybdenum 0.0127

Potassium -0.0103

Selenium -0.0026

Silicon 0.0155

Silver 0.0002

Sodium 0.0106

Strontium 0.0022

Thallium 0.0042

Tin -0.0011

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 205 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSAB 500-173517/77

P51219A

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.508 102

Chromium 0.500 0.490 98

Copper 0.500 0.553 111

Lead 0.0500 0.0533 107

Nickel 1.00 0.965 97

Vanadium 0.500 0.513 103

Zinc 1.00 0.935 93

Aluminum 500 509 102

Antimony 0.600 0.623 104

Arsenic 0.100 0.104 104

Beryllium 0.500 0.490 98

Boron 0.0012

Cadmium 1.00 0.965 96

Calcium 500 488 98

Cobalt 0.500 0.479 96

Iron 200 194 97

Magnesium 500 523 105

Manganese 0.500 0.508 102

Molybdenum 0.0145

Potassium -0.0103

Selenium 0.0500 0.0481 96

Silicon 0.0146

Silver 0.200 0.223 111

Sodium 0.0169

Strontium 0.0022

Thallium 0.100 0.108 108

Tin -0.0003

Titanium 0.0009

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 206 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSA 500-173518/13

P51219B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0019

Copper -0.0021

Lead 0.0018

Nickel 0.0005

Vanadium 0.0039

Zinc 0.0075

Aluminum 500 509 102

Antimony -0.0009

Arsenic 0.0002

Beryllium -0.0001

Boron 0.0007

Cadmium 0.0025

Calcium 500 478 96

Cobalt 0.0000

Iron 200 189 94

Magnesium 500 519 104

Manganese 0.0048

Molybdenum 0.0125

Potassium -0.0137

Selenium -0.0021

Silicon 0.0145

Silver 0.0002

Sodium 0.0138

Strontium 0.0022

Thallium 0.0058

Tin -0.0017

Titanium 0.0008

Total Heavy Metals 0.0025

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 207 of 332 01/04/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53342-1

ICSAB 500-173518/14

P51219B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.518 104

Chromium 0.500 0.483 97

Copper 0.500 0.556 111

Lead 0.0500 0.0504 101

Nickel 1.00 0.943 94

Vanadium 0.500 0.508 102

Zinc 1.00 0.902 90

Aluminum 500 510 102

Antimony 0.600 0.613 102

Arsenic 0.100 0.107 107

Beryllium 0.500 0.480 96

Boron 0.0009

Cadmium 1.00 0.935 93

Calcium 500 481 96

Cobalt 0.500 0.470 94

Iron 200 190 95

Magnesium 500 522 104

Manganese 0.500 0.501 100

Molybdenum 0.0115

Potassium -0.0099

Selenium 0.0500 0.0483 97

Silicon 0.0130

Silver 0.200 0.222 111

Sodium 0.0206

Strontium 0.0022

Thallium 0.100 0.104 104

Tin 0.0005

Titanium 0.0008

Total Heavy Metals 4.05 3.87 96

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 208 of 332 01/04/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173339/2-A 

Lab Name: Job No.: 500-53342-1

Sample Matrix: Solid LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Barium 200 199.5 100 80 120 6010B

Copper 25.0 25.15 101 80 120 6010B

Chromium 20.0 20.20 101 80 120 6010B

Nickel 50.0 49.95 100 80 120 6010B

Lead 10.0 10.14 101 80 120 6010B

Vanadium 50.0 50.42 101 80 120 6010B

Zinc 50.0 49.15 98 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 209 of 332 01/04/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173349/2-A 

Lab Name: Job No.: 500-53342-1

Sample Matrix: Water LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.955 98 80 120 6010B

Copper 0.250 0.2524 101 80 120 6010B

Chromium 0.200 0.1989 99 80 120 6010B

Nickel 0.500 0.4934 99 80 120 6010B

Lead 0.100 0.1010 101 80 120 6010B

Vanadium 0.500 0.4993 100 80 120 6010B

Zinc 0.500 0.4858 97 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 210 of 332 01/04/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173406/3-A 

Lab Name: Job No.: 500-53342-1

Sample Matrix: Water LCS Source: M12KSPKIC_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.975 99 80 120 6010B

Copper 0.250 0.2464 99 80 120 6010B

Chromium 0.200 0.1969 98 80 120 6010B

Nickel 0.500 0.4873 97 80 120 6010B

Lead 0.100 0.09785 98 80 120 6010B

Vanadium 0.500 0.4959 99 80 120 6010B

Zinc 0.500 0.4782 96 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 211 of 332 01/04/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173428/8-A 

Lab Name: Job No.: 500-53342-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002086 104 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 212 of 332 01/04/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173393/8-A 

Lab Name: Job No.: 500-53342-1

Sample Matrix: Solid LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Mercury 0.167 0.1467 88 80 120 ^ 7471A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 213 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:03

Prep Method: 3010A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.01 0.00044

Chromium 0.01 0.00096

Copper 0.01 0.00106

Lead 0.005 0.00158

Nickel 0.01 0.0019

Vanadium 0.005 0.00062

Zinc 0.02 0.00472

FORM IX - IN

Page 214 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:07

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 215 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:20

Prep Method: 3050B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Barium 1 0.119

Chromium 1 0.167

Copper 1 0.271

Lead 0.5 0.172

Nickel 1 0.219

Vanadium 0.5 0.0759

Zinc 2 0.686

FORM IX - IN

Page 216 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:03

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 217 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 11/01/2005 15:36

Prep Method: 3010A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.5 0.01

Chromium 0.025 0.01

Copper 0.025 0.01

Lead 0.05 0.005

Nickel 0.025 0.01

Vanadium 0.025 0.005

Zinc 0.1 0.02

FORM IX - IN

Page 218 of 332 01/04/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 01/28/2008 10:37

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.01

Chromium 0.01 0.01

Copper 0.01 0.01

Lead 0.005 0.005

Nickel 0.01 0.01

Vanadium 0.005 0.005

Zinc 0.02 0.02

FORM IX - IN

Page 219 of 332 01/04/2013
9-IN

Instrument ID: HG6

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 08/31/2012 10:08

Prep Method: 7470A

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 220 of 332 01/04/2013
9-IN

Instrument ID: HG6

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 08/31/2012 10:08

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 221 of 332 01/04/2013
9-IN

Instrument ID: HG6

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 11/01/2005 11:39

Prep Method: 7470A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 2 0.2

FORM IX - IN

Page 222 of 332 01/04/2013
9-IN

Instrument ID: HG6

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 09/16/2006 08:48

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 2 1

FORM IX - IN

Page 223 of 332 01/04/2013
9-IN

Instrument ID: HG5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7471A MDL Date: 08/31/2012 10:15

Prep Method: 7471A

Analyte Wavelength/

Mass

RL MDL

(ug/Kg) (ug/Kg)

Mercury 16.7 6.37

FORM IX - IN

Page 224 of 332 01/04/2013
9-IN

Instrument ID: HG5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7471A XMDL Date: 08/31/2012 10:16

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 225 of 332 01/04/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53342-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP5

SDG No.:

(mg/L)

11/19/2012 14:31

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 50 6010B

Nickel 50 6010B

Lead 50 6010B

Vanadium 100 6010B

Zinc 20 6010B

FORM XI - IN

Page 226 of 332 01/04/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53342-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG5

SDG No.:

(ug/L)

03/01/2008 11:18

METALS

Mercury 5.0 7471A

FORM XI - IN

Page 227 of 332 01/04/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53342-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG6

SDG No.:

(ug/L)

11/01/2010 11:39

METALS

Mercury 5.0 7470A

FORM XI - IN

Page 228 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

METALS

TestAmerica Chicago

Prep Method: 3050B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173339/1-A 12/18/2012 16:00 173339 1 100

LCS 500-173339/2-A 12/18/2012 16:00 173339 1 100

500-53342-1 12/18/2012 16:00 173339 1.1079 100

FORM XII-IN

Page 229 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173349/1-A 12/18/2012 15:30 173349 50 50

LCS 500-173349/2-A 12/18/2012 15:30 173349 50 50

500-53342-3 12/18/2012 15:30 173349 50 50

FORM XII-IN

Page 230 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

LB2 500-173323/1-B 12/19/2012 08:20 173406 50 50

LCS 500-173406/3-A 12/19/2012 08:20 173406 50 50

500-53342-1 12/19/2012 08:20 173406 50 50

FORM XII-IN

Page 231 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

METALS

TestAmerica Chicago

Prep Method: 7471A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173393/7-A 12/19/2012 14:45 173393 0.6 50

LCS 500-173393/8-A 12/19/2012 14:45 173393 0.6 50

500-53342-1 12/19/2012 14:45 173393 0.6182 50

FORM XII-IN

Page 232 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173428/7-A 12/19/2012 14:00 173428 25 25

LCS 500-173428/8-A 12/19/2012 14:00 173428 25 25

LB2 500-173323/1-C 12/19/2012 14:00 173428 25 25

500-53342-1 12/19/2012 14:00 173428 25 25

500-53342-3 12/19/2012 14:00 173428 25 25

FORM XII-IN

Page 233 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

ICP5

12/19/2012 08:45 12/19/2012 17:31

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 08:45

ZZZZZZ 08:51

ZZZZZZ 08:57

ZZZZZZ 09:04

ZZZZZZ 09:10

ZZZZZZ 09:15

ZZZZZZ 09:20

ZZZZZZ 09:28

ZZZZZZ 09:36

ICV 500-173517/10 1 09:45 X X X X X X X

ICB 500-173517/11 1 09:53 X X X X X X X

CRI 500-173517/12 1 09:59 X X X X X X X

ICSA 500-173517/13 1 10:05 X X X X X X X

ICSAB 500-173517/14 1 10:12 X X X X X X X

CCV 500-173517/15 1 10:20 X X X X X X X

CCB 500-173517/16 1 10:26 X X X X X X X

MB 500-173339/1-A 1 T 10:33 X X X X X X X

LCS 500-173339/2-A 1 T 10:39 X X X X X X X

ZZZZZZ 10:45

ZZZZZZ 10:52

ZZZZZZ 10:58

ZZZZZZ 11:04

ZZZZZZ 11:11

ZZZZZZ 11:17

ZZZZZZ 11:30

ZZZZZZ 11:37

CCV 500-173517/27 1 11:45 X X X X X X X

CCB 500-173517/28 1 11:51 X X X X X X X

ZZZZZZ 11:57

ZZZZZZ 12:04

ZZZZZZ 12:10

ZZZZZZ 12:16

ZZZZZZ 12:22

ZZZZZZ 12:28

ZZZZZZ 12:35

ZZZZZZ 12:41

ZZZZZZ 12:47

ZZZZZZ 12:53

CCV 500-173517/39 1 13:02 X X X X X X X

CCB 500-173517/40 1 13:08 X X X X X X X

ZZZZZZ 13:14

ZZZZZZ 13:21

FORM XIII-IN Page 234 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

ICP5

12/19/2012 08:45 12/19/2012 17:31

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 13:27

ZZZZZZ 13:33

500-53342-1 1 T 13:39 X X X X X X X

MB 500-173349/1-A 1 T 13:52 X X X X X X X

LCS 500-173349/2-A 1 T 13:58 X X X X X X X

ZZZZZZ 14:04

ZZZZZZ 14:11

ZZZZZZ 14:18

CCV 500-173517/51 1 14:26 X X X X X X X

CCB 500-173517/52 1 14:32 X X X X X X X

ZZZZZZ 14:38

ZZZZZZ 14:45

ZZZZZZ 14:51

ZZZZZZ 14:57

500-53342-3 1 T 15:03 X X X X X X X

ZZZZZZ 15:14

ZZZZZZ 15:20

ZZZZZZ 15:26

ZZZZZZ 15:33

ZZZZZZ 15:39

CCV 500-173517/63 1 15:47 X X X X X X X

CCB 500-173517/64 1 15:53 X X X X X X X

ZZZZZZ 16:00

ZZZZZZ 16:06

ZZZZZZ 16:12

ZZZZZZ 16:18

ZZZZZZ 16:25

ZZZZZZ 16:31

ZZZZZZ 16:37

ZZZZZZ 16:43

CCV 500-173517/73 16:52

CCB 500-173517/74 16:58

CRI 500-173517/75 1 17:04 X X X X X X X

ICSA 500-173517/76 1 17:10 X X X X X X X

ICSAB 500-173517/77 1 17:16 X X X X X X X

CCV 500-173517/78 17:25

CCB 500-173517/79 17:31

Prep Types

T = Total/NA

FORM XIII-IN Page 235 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

ICP5

12/19/2012 17:42 12/20/2012 00:26

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 17:42

ZZZZZZ 17:48

ZZZZZZ 17:54

ZZZZZZ 18:01

ZZZZZZ 18:07

ZZZZZZ 18:12

ZZZZZZ 18:17

ZZZZZZ 18:24

ZZZZZZ 18:33

ICV 500-173518/10 1 18:41 X X X X X X X

ICB 500-173518/11 1 18:48 X X X X X X X

CRI 500-173518/12 1 18:54 X X X X X X X

ICSA 500-173518/13 1 19:00 X X X X X X X

ICSAB 500-173518/14 1 19:06 X X X X X X X

CCV 500-173518/15 19:15

CCB 500-173518/16 19:21

ZZZZZZ 19:27

ZZZZZZ 19:33

ZZZZZZ 19:40

ZZZZZZ 19:46

ZZZZZZ 19:52

ZZZZZZ 19:58

ZZZZZZ 20:04

ZZZZZZ 20:11

ZZZZZZ 20:17

ZZZZZZ 20:23

CCV 500-173518/27 1 20:32 X X X X X X X

CCB 500-173518/28 1 20:38 X X X X X X X

ZZZZZZ 20:44

ZZZZZZ 20:50

ZZZZZZ 20:56

ZZZZZZ 21:07

LB2 500-173323/1-B 1 P 21:13 X X X X X X X

LCS 500-173406/3-A 1 T 21:20 X X X X X X X

ZZZZZZ 21:26

ZZZZZZ 21:32

ZZZZZZ 21:43

ZZZZZZ 21:49

CCV 500-173518/39 1 21:57 X X X X X X X

CCB 500-173518/40 1 22:04 X X X X X X X

ZZZZZZ 22:10

ZZZZZZ 22:16

FORM XIII-IN Page 236 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

ICP5

12/19/2012 17:42 12/20/2012 00:26

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 22:22

ZZZZZZ 22:29

ZZZZZZ 22:35

500-53342-1 1 P 22:41 X X X X X X X

ZZZZZZ 22:54

ZZZZZZ 23:00

ZZZZZZ 23:06

ZZZZZZ 23:13

CCV 500-173518/51 1 23:21 X X X X X X X

CCB 500-173518/52 1 23:27 X X X X X X X

ZZZZZZ 23:34

ZZZZZZ 23:40

ZZZZZZ 23:46

ZZZZZZ 23:52

ZZZZZZ 23:59

ZZZZZZ 00:05

ZZZZZZ 00:11

CCV 500-173518/60 00:19

CCB 500-173518/61 00:26

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 237 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

HG6

12/20/2012 08:12 12/20/2012 10:48

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 08:12

ZZZZZZ 08:14

ZZZZZZ 08:16

ZZZZZZ 08:18

ZZZZZZ 08:20

ZZZZZZ 08:22

ICV 500-173572/7 1 08:24 X

ICB 500-173572/8 1 08:26 X

CRA 500-173572/9 1 08:28 X

ZZZZZZ 08:30

ZZZZZZ 08:32

ZZZZZZ 08:34

ZZZZZZ 08:36

ZZZZZZ 08:39

ZZZZZZ 08:41

ZZZZZZ 08:43

ZZZZZZ 08:45

ZZZZZZ 08:46

CCV 500-173572/19 08:49

CCB 500-173572/20 08:51

ZZZZZZ 08:52

ZZZZZZ 08:54

ZZZZZZ 08:56

ZZZZZZ 08:58

ZZZZZZ 09:00

ZZZZZZ 09:02

ZZZZZZ 09:04

ZZZZZZ 09:06

ZZZZZZ 09:08

ZZZZZZ 09:10

CCV 500-173572/31 1 09:12 X

CCB 500-173572/32 1 09:13 X

ZZZZZZ 09:15

ZZZZZZ 09:17

ZZZZZZ 09:19

ZZZZZZ 09:21

ZZZZZZ 09:23

ZZZZZZ 09:25

ZZZZZZ 09:26

ZZZZZZ 09:28

ZZZZZZ 09:30

MB 500-173428/7-A 1 T 09:32 X FORM XIII-IN Page 238 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

HG6

12/20/2012 08:12 12/20/2012 10:48

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

CCV 500-173572/43 1 09:34 X

CCB 500-173572/44 1 09:36 X

LCS 500-173428/8-A 1 T 09:38 X

LB2 500-173323/1-C 1 P 09:40 X

500-53342-1 1 P 09:42 X

ZZZZZZ 09:44

ZZZZZZ 09:45

ZZZZZZ 09:47

ZZZZZZ 09:49

ZZZZZZ 09:51

ZZZZZZ 09:53

ZZZZZZ 09:55

CCV 500-173572/55 1 09:57 X

CCB 500-173572/56 1 09:59 X

ZZZZZZ 10:01

ZZZZZZ 10:03

ZZZZZZ 10:05

ZZZZZZ 10:06

ZZZZZZ 10:08

ZZZZZZ 10:10

ZZZZZZ 10:12

ZZZZZZ 10:14

ZZZZZZ 10:16

ZZZZZZ 10:18

CCV 500-173572/67 1 10:19 X

CCB 500-173572/68 1 10:21 X

ZZZZZZ 10:23

ZZZZZZ 10:25

ZZZZZZ 10:27

500-53342-3 1 T 10:29 X

ZZZZZZ 10:31

ZZZZZZ 10:32

CCV 500-173572/75 1 10:34 X

CCB 500-173572/76 1 10:36 X

ZZZZZZ 10:38

ZZZZZZ 10:40

ZZZZZZ 10:42

ZZZZZZ 10:44

CCV 500-173572/81 10:46

CCB 500-173572/82 10:48

FORM XIII-IN Page 239 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

HG6

12/20/2012 08:12 12/20/2012 10:48

7470A

METALS

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 240 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

HG5

12/20/2012 08:58 12/20/2012 09:41

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

STD01REP1 08:58 X

500-173573/1 IC 

STD02REP1 09:00 X

500-173573/2 IC 

STD03REP1 09:01 X

500-173573/3 IC 

STD04REP1 09:03 X

500-173573/4 IC 

STD05REP1 09:06 X

500-173573/5 IC 

STD06REP1 09:07 X

500-173573/6 IC 

ICV 500-173573/7 1 09:11 X

ICB 500-173573/8 1 09:12 X

CRA 500-173573/9 1 09:14 X

MB 500-173393/7-A 1 T 09:16 X

LCS 500-173393/8-A 1 T 09:18 X

ZZZZZZ 09:20

ZZZZZZ 09:22

ZZZZZZ 09:24

ZZZZZZ 09:26

ZZZZZZ 09:28

ZZZZZZ 09:29

ZZZZZZ 09:31

ZZZZZZ 09:34

CCV 500-173573/20 1 09:39 X

CCB 500-173573/21 1 09:41 X

Prep Types

T = Total/NA

FORM XIII-IN Page 241 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

HG5

12/20/2012 09:45 12/20/2012 10:44

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

STD01REP1 09:45 X

500-173574/1 IC 

STD02REP1 09:46 X

500-173574/2 IC 

STD03REP1 09:48 X

500-173574/3 IC 

STD04REP1 09:50 X

500-173574/4 IC 

STD05REP1 09:52 X

500-173574/5 IC 

STD06REP1 09:54 X

500-173574/6 IC 

ICV 500-173574/7 1 09:59 X

ICB 500-173574/8 1 10:01 X

CRA 500-173574/9 1 10:03 X

CCV 500-173574/10 1 10:05 X

CCB 500-173574/11 1 10:07 X

ZZZZZZ 10:09

ZZZZZZ 10:10

ZZZZZZ 10:12

ZZZZZZ 10:14

ZZZZZZ 10:17

ZZZZZZ 10:19

500-53342-1 1 T 10:21 X

ZZZZZZ 10:23

ZZZZZZ 10:24

ZZZZZZ 10:26

CCV 500-173574/22 1 10:28 X

CCB 500-173574/23 1 10:30 X

ZZZZZZ 10:32

ZZZZZZ 10:34

ZZZZZZ 10:36

ZZZZZZ 10:38

ZZZZZZ 10:40

CCV 500-173574/29 10:42

CCB 500-173574/30 10:44

Prep Types

T = Total/NA

FORM XIII-IN Page 242 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/18/12 16:30

173339 12/18/12 16:00

Batch Method:

TestAmerica Chicago

3050B

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg InitialAmount FinalAmount M12JSPKIC 00002

CALC NOT SET TO 

RUN

MB 500-173339/1 3050B, 6010B 1 g 100 mL

CALC NOT SET TO 

RUN

LCS 1 g 100 mL 1 mL

500-173339/2

3050B, 6010B

FC Composite 5 CALC NOT SET TO 

RUN

500-53342-A-1 3050B, 6010B T 1.1079 g 100 mL

Batch Notes

Analyst BL

Balance ID C-1966

First End time 1630

Hydrogen peroxide lot number L08A06

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hood ID or number 3

Hot Block ID number 8

Oven, Bath or Block Temperature 1 90 Degrees C

Oven, Bath or Block Temperature 2 90 Degrees C

Pipette ID 1628

First Start time 1600

ID number of the thermometer J59717

Digestion Tube/Cup Lot # MF06LKK01

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 243 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/18/12 16:00

173349 12/18/12 15:30

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12JSPKIC 00002

MB 500-173349/1 3010A, 6010B 50 mL 50 mL

LCS 50 mL 50 mL 0.5 mL

500-173349/2

3010A, 6010B

500-53342-E-3 FC EB 5 3010A, 6010B T 50 mL 50 mL

Batch Notes

First End time 1600

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hot Block ID number 4

Pipette ID 1627

First Start time 1530

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 244 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Hudson, Lawrence A

12/19/12 08:50

173406 12/19/12 08:20

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment

LB2 50 mL 50 mL T-748

500-173323/1-A

3010A, 6010B

LCS 50 mL 50 mL 0.5 mL

500-173406/3

3010A, 6010B

500-53342-A-1-C FC Composite 5 3010A, 6010B P 50 mL 50 mL LB2 T-748

Batch Notes

Batch Comment T-744, T-748

First End time 0850

Lot # of hydrochloric acid 0000013500

Lot # of Nitric Acid L10022

Hot Block ID number 4

Pipette ID 1627

First Start time 0820

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

P TCLP

6010B Page 1 of 1

Page 245 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/19/12 16:00

173428 12/19/12 14:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173428/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-173428/8

7470A, 7470A

LB2 25 mL 25 mL

500-173323/1-A

7470A, 7470A

500-53342-A-1-C FC Composite 5 7470A, 7470A P 25 mL 25 mL

500-53342-E-3 FC EB 5 7470A, 7470A T 25 mL 25 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK 7470A Page 1 of 2

Page 246 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/19/12 16:00

173428 12/19/12 14:00

Batch Method:

TestAmerica Chicago

7470A

Basis Basis Description

T Total/NA

P TCLP

7470A Page 2 of 2

Page 247 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/19/12 15:15

173393 12/19/12 14:45

Batch Method:

TestAmerica Chicago

7471A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173393/7 7471A, 7471A 0.6 g 50 mL

LCS 0.6 g 50 mL 0.0001 mL

500-173393/8

7471A, 7471A

500-53342-A-1 FC Composite 5 7471A, 7471A T 0.6182 g 50 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Balance ID c0975

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Blank Soil Lot Number teflon strip_00001

Filter Lot # 21782182

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 2

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 90

Oven, Bath or Block Temperature 2 90

Pipette ID 1631

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Syringe Lot # 1292669

ID number of the thermometer j60025

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

T Total/NA

7471A Page 1 of 1

Page 248 of 332 01/04/2013
GENERAL CHEMISTRY

Page 249 of 332 01/04/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

GENERAL CHEMISTRY

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53342-1

FC Composite 5 500-53342-1 

FC Composite 5 500-53342-2 

FC EB 5 500-53342-3 

Comments:

Page 250 of 332 01/04/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40

500-53342-1

FC Composite 5

Solid Date Sampled: 12/17/2012 14:50

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 30.0

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <3.33 3.33 1.30 mg/Kg 1 7196A

57-12-5 Cyanide, Total 0.905 1.59 0.524 mg/Kg J 1 9014

18496-25-8 Sulfide 798 82.8 13.2 mg/Kg 1 9034

HEM (Oil & Grease) 13200 1650 732 mg/Kg 1 9071B

FORM IB-IN Page 251 of 332 01/04/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40

500-53342-1

FC Composite 5

Solid Date Sampled: 12/17/2012 14:50

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <48.7 48.7 3.80 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.59 0.200 0.200 SU 1 9045C

% Moisture 70.0 0.100 0.100 % 1 SM 2540G

Total Solids 30.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 252 of 332 01/04/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53342-3

Date Received: 12/18/2012 09:40

500-53342-1

FC EB 5

Water Date Sampled: 12/17/2012 14:30

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 1 7196A

57-12-5 Cyanide, Total <0.0100 0.0100 0.00331 mg/L 1 9014

Sulfide, Reactive <1.00 1.00 1.00 mg/L 1 9034

HEM (Oil & Grease) <5.36 5.36 1.55 mg/L 1 1664A

18496-25-8 Sulfide <1.00 1.00 0.230 mg/L 1 9034

FORM IB-IN Page 253 of 332 01/04/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

Analyst: KD Batch Start Date: 12/18/2012

Reporting Units: mg/L Analytical Batch No.: 173293

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 11:20 Chromium, hexavalent 0.2602 0.250 104 90-110 WSTCR2_00008

 2 ICB 11:20 Chromium, hexavalent <0.0100

 8 CCV 11:23 Chromium, hexavalent 0.4934 0.500 99 90-110 WSTCR1_00008

 9 CCB 11:24 Chromium, hexavalent <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 254 of 332 01/04/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

Analyst: APW Batch Start Date: 12/27/2012

Reporting Units: mg/L Analytical Batch No.: 174027

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 12:40 Chromium, hexavalent 0.2548 0.250 102 90-110 WSTCR2_00008

 2 ICB 12:40 Chromium, hexavalent <0.0200

 10 CCV 12:46 Chromium, hexavalent 0.5130 0.500 103 90-110 WSTCR1_00008

 11 CCB 12:46 Chromium, hexavalent <0.0200

 18 CCV 12:51 Chromium, hexavalent 0.5138 0.500 103 90-110 WSTCR1_00008

 19 CCB 12:52 Chromium, hexavalent <0.0200

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 255 of 332 01/04/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

Analyst: EAT Batch Start Date: 12/27/2012

Reporting Units: mg/L Analytical Batch No.: 174042

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 14:40 Cyanide, Total 0.1006 0.100 101 90-110 WSTINCN2_00563

 2 ICB 14:40 Cyanide, Total <0.0100

 13 CCV 14:43 Cyanide, Total 0.1942 0.200 97 90-110 WSTINCN1_00571

 14 CCB 14:43 Cyanide, Total <0.0100

 25 CCV 14:47 Cyanide, Total 0.1938 0.200 97 90-110 WSTINCN1_00571

 26 CCB 14:47 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 256 of 332 01/04/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53342-1

Analyst: EAT Batch Start Date: 12/28/2012

Reporting Units: mg/L Analytical Batch No.: 174173

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 15:25 Cyanide, Total 0.1017 0.100 102 90-110 WSTINCN2_00564

 2 ICB 15:25 Cyanide, Total <0.0100

 13 CCV 15:29 Cyanide, Total 0.1954 0.200 98 90-110 WSTINCN1_00572

 14 CCB 15:29 Cyanide, Total <0.0100

 25 CCV 15:33 Cyanide, Total 0.1951 0.200 98 90-110 WSTINCN1_00572

 26 CCB 15:33 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 257 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Method Analyte Result Qual Dil

3-IN

500-53342-1

Lab Sample ID Units

TestAmerica Chicago

METHOD BLANK

GENERAL CHEMISTRY

RL

Batch ID: 173459 Date: 12/21/2012 09:55 Prep Batch: 173450 Date: 12/21/2012 05:05

1664A MB 500-173450/1-A HEM (Oil & Grease) <5.00 mg/L 5.00 1

Batch ID: 173293 Date: 12/18/2012 11:21

7196A MB 500-173293/3 Chromium, hexavalent <0.0100 mg/L 0.0100 1

Batch ID: 174027 Date: 12/27/2012 12:41 Prep Batch: 173790 Date: 12/22/2012 12:00

7196A MB 500-173790/1-A Chromium, hexavalent <1.00 mg/Kg 1.00 1

Batch ID: 174042 Date: 12/27/2012 14:40 Prep Batch: 173980 Date: 12/27/2012 09:50

9014 MB 500-173980/1-A Cyanide, Total <0.0100 mg/L 0.0100 1

Batch ID: 174173 Date: 12/28/2012 15:30 Prep Batch: 174096 Date: 12/28/2012 11:20

MB <0.500

500-174096/12-A

9014 Cyanide, Total mg/Kg 0.500 1

Batch ID: 173472 Date: 12/19/2012 12:15 Prep Batch: 173290 Date: 12/19/2012 10:05

9034 MB 500-173290/1-A Sulfide, Reactive <50.0 mg/Kg 50.0 1

Batch ID: 173474 Date: 12/19/2012 13:35 Prep Batch: 173291 Date: 12/19/2012 11:25

9034 MB 500-173291/1-A Sulfide <25.0 mg/Kg 25.0 1

Batch ID: 173845 Date: 12/24/2012 13:19 Prep Batch: 173844 Date: 12/24/2012 08:00

9034 MB 500-173844/1-A Sulfide, Reactive <1.00 mg/L 1.00 1

Batch ID: 173846 Date: 12/24/2012 13:19

9034 MB 500-173846/1 Sulfide <1.00 mg/L 1.00 1

Batch ID: 173330 Date: 12/19/2012 09:20 Prep Batch: 173324 Date: 12/19/2012 05:10

9071B MB 500-173324/1-A HEM (Oil & Grease) <500 mg/Kg 500 1

FORM III-IN

Page 258 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53342-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173293 Date: 12/18/2012 11:22

7196A 500-53342-3 Chromium, hexavalent <0.0100 mg/L

7196A 500-53342-3 

MS 

Chromium, hexavalent 0.2502 mg/L 0.250 100 85-115

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 259 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53342-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173293 Date: 12/18/2012 11:23

7196A 500-53342-3 

MSD 

Chromium, hexavalent 0.2555 mg/L 0.250 102 85-115 2 20

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 260 of 332 01/04/2013
7A-IN

Job No.: 500-53342-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Solid

TestAmerica Chicago

Batch ID: 174027 Date: 12/27/2012 12:42 Prep Batch: 173790 Date: 12/22/2012 12:00

LCS Source: WSTCR2_00008

7196A LCS 10.0 92

500-173790/2-

A

Chromium, hexavalent 9.188 mg/Kg 80-120

Batch ID: 174027 Date: 12/27/2012 12:42 Prep Batch: 173790 Date: 12/22/2012 12:00

LCS Source: WSTCR13_00629

7196A LCS 676 99

500-173790/3-

A

Chromium, hexavalent 669.0 mg/Kg 80-120

Batch ID: 174173 Date: 12/28/2012 15:30 Prep Batch: 174096 Date: 12/28/2012 11:20

LCS Source: WSTINCN2_00564

9014 LCS 5.00 107

500-174096/13

-A

Cyanide, Total 5.325 mg/Kg 80-120

Batch ID: 173472 Date: 12/19/2012 12:15 Prep Batch: 173290 Date: 12/19/2012 10:10

LCS Source: WSTSF1_00036

9034 LCS 180 94

500-173290/2-

A

Sulfide, Reactive 168.6 mg/Kg 80-120

Batch ID: 173474 Date: 12/19/2012 13:35 Prep Batch: 173291 Date: 12/19/2012 11:25

LCS Source: WSTSF1_00036

9034 LCS 180 93

500-173291/2-

A

Sulfide 168.3 mg/Kg 80-120

Batch ID: 173330 Date: 12/19/2012 09:31 Prep Batch: 173324 Date: 12/19/2012 05:10

LCS Source: 1664 HEM_00060

9071B LCS 4000 102

500-173324/2-

A

HEM (Oil & Grease) 4090 mg/Kg 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 261 of 332 01/04/2013
7A-IN

Job No.: 500-53342-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Water

TestAmerica Chicago

Batch ID: 173459 Date: 12/21/2012 09:58 Prep Batch: 173450 Date: 12/21/2012 05:16

LCS Source: 1664 HEM_00060

1664A LCS 40.0 92

500-173450/2-

A

HEM (Oil & Grease) 36.70 mg/L 78-114

Batch ID: 173293 Date: 12/18/2012 11:21

LCS Source: WSTCR2_00008

7196A LCS 0.250 106

500-173293/4

Chromium, hexavalent 0.2652 mg/L 85-115

Batch ID: 174042 Date: 12/27/2012 14:40 Prep Batch: 173980 Date: 12/27/2012 09:50

LCS Source: WSTINCN2_00563

9014 LCS 0.100 107

500-173980/2-

A

Cyanide, Total 0.1066 mg/L 80-120

Batch ID: 173846 Date: 12/24/2012 13:20

LCS Source: WSTSF1_00036

9034 LCS 3.60 104

500-173846/2

Sulfide 3.760 mg/L 80-120

Batch ID: 173845 Date: 12/24/2012 13:29 Prep Batch: 173844 Date: 12/24/2012 08:15

LCS Source: WSTSF1_00036

9034 LCS 3.60 105

500-173844/2-

A

Sulfide, Reactive 3.767 mg/L 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 262 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 10:43

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 263 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:44

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 264 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 14:44

Prep Method: 3060A

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Chromium, hexavalent 1 0.389

FORM IX - IN

Page 265 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:45

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.02 0.00325

FORM IX - IN

Page 266 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:18

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Cyanide, Total 0.5 0.165

FORM IX - IN

Page 267 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:19

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 268 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:22

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 269 of 332 01/04/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:22

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 270 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 16:25

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide, Reactive 50 3.9

FORM IX - IN

Page 271 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 01/02/2006 09:18

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide, Reactive 1 1

FORM IX - IN

Page 272 of 332 01/04/2013
9-IN

Instrument ID: FP4

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1010 MDL Date: 11/11/2005 10:25

Analyte Wavelength/

Mass

RL MDL

(Degrees (Degrees F)

Flashpoint 40 40

FORM IX - IN

Page 273 of 332 01/04/2013
9-IN

Instrument ID: NoEquip

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1664A MDL Date: 05/29/2012 15:22

Prep Method: 1664A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

HEM (Oil & Grease) 5 1.45

FORM IX - IN

Page 274 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:57

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide 1 0.23

FORM IX - IN

Page 275 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:59

Prep Method: 9030B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide 25 4

FORM IX - IN

Page 276 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9045C MDL Date: 11/01/2005 06:06

Analyte Wavelength/

Mass

RL MDL

(SU) (SU)

pH 0.2 0.2

FORM IX - IN

Page 277 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9071B MDL Date: 05/29/2012 15:24

Prep Method: 9071B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

HEM (Oil & Grease) 500 222

FORM IX - IN

Page 278 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: Moisture MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

Percent Moisture 0.1 0.1

Percent Solids 0.1 0.1

FORM IX - IN

Page 279 of 332 01/04/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53342-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: SM 2540G MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

% Moisture 0.1 0.1

Total Solids 0.1 0.1

FORM IX - IN

Page 280 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173290/1-A 12/19/2012 10:05 173290 10.0000 10

LCS 500-173290/2-A 12/19/2012 10:10 173290 10.0000 10

500-53342-1 12/19/2012 10:50 173290 10.2666 10

FORM XII-IN

Page 281 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 3060A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173790/1-A 12/22/2012 12:00 173790 2.5 100

LCS 500-173790/2-A 12/22/2012 12:00 173790 2.5 100

LCS 500-173790/3-A 12/22/2012 12:00 173790 2.5 100

500-53342-1 12/22/2012 12:00 173790 2.5007 100

FORM XII-IN

Page 282 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173844/1-A 12/24/2012 08:00 173844 250 250

LCS 500-173844/2-A 12/24/2012 08:15 173844 250 250

500-53342-3 12/24/2012 08:30 173844 250 250

FORM XII-IN

Page 283 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173980/1-A 12/27/2012 09:50 173980 50 50

LCS 500-173980/2-A 12/27/2012 09:50 173980 50 50

500-53342-3 12/27/2012 09:50 173980 50 50

FORM XII-IN

Page 284 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-174096/12-A 12/28/2012 11:20 174096 1.0000 50

LCS 500-174096/13-A 12/28/2012 11:20 174096 1.0000 50

500-53342-1 12/28/2012 11:20 174096 1.0495 50

FORM XII-IN

Page 285 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9030B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173291/1-A 12/19/2012 11:25 173291 10.0000 10

LCS 500-173291/2-A 12/19/2012 11:25 173291 10.0000 10

500-53342-1 12/19/2012 11:25 173291 10.0683 10

FORM XII-IN

Page 286 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9071B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173324/1-A 12/19/2012 05:10 173324 10 10

LCS 500-173324/2-A 12/19/2012 05:10 173324 10 10

500-53342-1 12/19/2012 05:10 173324 10.1047 10

FORM XII-IN

Page 287 of 332 01/04/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53342-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 1664A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173450/1-A 12/21/2012 05:05 173450 1000 1000

LCS 500-173450/2-A 12/21/2012 05:16 173450 1000 1000

500-53342-3 12/21/2012 07:09 173450 933 1000

FORM XII-IN

Page 288 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

SPEC5

12/18/2012 11:20 12/18/2012 11:24

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-173293/1 1 11:20 X

ICB 500-173293/2 1 11:20 X

MB 500-173293/3 1 T 11:21 X

LCS 500-173293/4 1 T 11:21 X

500-53342-3 1 T 11:22 X

500-53342-3 MS 1 T 11:22 X

500-53342-3 MSD 1 T 11:23 X

CCV 500-173293/8 1 11:23 X

CCB 500-173293/9 1 11:24 X

Prep Types

T = Total/NA

FORM XIII-IN Page 289 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

SPEC5

12/27/2012 12:40 12/27/2012 12:59

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-174027/1 1 12:40 X

ICB 500-174027/2 1 12:40 X

MB 500-173790/1-A 1 T 12:41 X

LCS 500-173790/2-A 1 T 12:42 X

LCS 500-173790/3-A 50 T 12:42 X

ZZZZZZ 12:43

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:45

CCV 500-174027/10 1 12:46 X

CCB 500-174027/11 1 12:46 X

ZZZZZZ 12:47

ZZZZZZ 12:48

ZZZZZZ 12:48

ZZZZZZ 12:49

500-53342-1 1 T 12:50 X

ZZZZZZ 12:51

CCV 500-174027/18 1 12:51 X

CCB 500-174027/19 1 12:52 X

ZZZZZZ 12:53

ZZZZZZ 12:53

ZZZZZZ 12:54

ZZZZZZ 12:55

ZZZZZZ 12:55

ZZZZZZ 12:56

ZZZZZZ 12:57

CCV 500-174027/27 12:57

CCB 500-174027/28 12:58

ZZZZZZ 12:59

Prep Types

T = Total/NA

FORM XIII-IN Page 290 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

SPEC5

12/27/2012 14:40 12/27/2012 14:49

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-174042/1 1 14:40 X

ICB 500-174042/2 1 14:40 X

MB 500-173980/1-A 1 T 14:40 X

LCS 500-173980/2-A 1 T 14:40 X

ZZZZZZ 14:41

ZZZZZZ 14:41

ZZZZZZ 14:41

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:43

CCV 500-174042/13 1 14:43 X

CCB 500-174042/14 1 14:43 X

ZZZZZZ 14:44

500-53342-3 1 T 14:44 X

ZZZZZZ 14:44

ZZZZZZ 14:44

ZZZZZZ 14:45

ZZZZZZ 14:45

ZZZZZZ 14:45

ZZZZZZ 14:46

ZZZZZZ 14:46

ZZZZZZ 14:46

CCV 500-174042/25 1 14:47 X

CCB 500-174042/26 1 14:47 X

ZZZZZZ 14:47

ZZZZZZ 14:47

ZZZZZZ 14:48

ZZZZZZ 14:48

ZZZZZZ 14:48

ZZZZZZ 14:49

CCV 500-174042/33 14:49

CCB 500-174042/34 14:49

Prep Types

T = Total/NA

FORM XIII-IN Page 291 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

SPEC5

12/28/2012 15:25 12/28/2012 15:34

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-174173/1 1 15:25 X

ICB 500-174173/2 1 15:25 X

ZZZZZZ 15:25

ZZZZZZ 15:26

ZZZZZZ 15:26

ZZZZZZ 15:26

ZZZZZZ 15:27

ZZZZZZ 15:27

ZZZZZZ 15:27

ZZZZZZ 15:28

ZZZZZZ 15:28

ZZZZZZ 15:28

CCV 500-174173/13 1 15:29 X

CCB 500-174173/14 1 15:29 X

ZZZZZZ 15:29

MB 500-174096/12-A 1 T 15:30 X

LCS 500-174096/13-A 1 T 15:30 X

ZZZZZZ 15:30

500-53342-1 1 T 15:31 X

ZZZZZZ 15:31

ZZZZZZ 15:31

ZZZZZZ 15:32

ZZZZZZ 15:32

ZZZZZZ 15:32

CCV 500-174173/25 1 15:33 X

CCB 500-174173/26 1 15:33 X

ZZZZZZ 15:33

ZZZZZZ 15:34

ZZZZZZ 15:34

ZZZZZZ 15:34

Prep Types

T = Total/NA

FORM XIII-IN Page 292 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 12:15 12/19/2012 12:24

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-173290/1-A 1 T 12:15 X

LCS 500-173290/2-A 1 T 12:15 X

ZZZZZZ 12:16

ZZZZZZ 12:17

ZZZZZZ 12:17

ZZZZZZ 12:18

ZZZZZZ 12:19

500-53342-1 1 T 12:19 X

ZZZZZZ 12:20

ZZZZZZ 12:21

ZZZZZZ 12:22

ZZZZZZ 12:22

ZZZZZZ 12:23

ZZZZZZ 12:24

Prep Types

T = Total/NA

FORM XIII-IN Page 293 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/24/2012 13:19 12/24/2012 13:51

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-173844/1-A 1 T 13:19 X

LCS 500-173844/2-A 1 T 13:29 X

500-53342-3 1 T 13:40 X

ZZZZZZ 13:51

Prep Types

T = Total/NA

FORM XIII-IN Page 294 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

FP4

12/20/2012 10:00 12/20/2012 13:53

1010

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

F

P

T

y

p

e

ZZZZZZ 10:00

500-53342-1 1 T 11:00 X

ZZZZZZ 13:53

Prep Types

T = Total/NA

FORM XIII-IN Page 295 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NoEquip

12/21/2012 09:55 12/21/2012 11:16

1664A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-173450/1-A 1 T 09:55 X

LCS 500-173450/2-A 1 T 09:58 X

ZZZZZZ 10:02

ZZZZZZ 10:06

ZZZZZZ 10:09

ZZZZZZ 10:13

ZZZZZZ 10:17

ZZZZZZ 10:20

ZZZZZZ 10:24

ZZZZZZ 10:28

ZZZZZZ 10:31

500-53342-3 1 T 10:35 X

ZZZZZZ 10:39

ZZZZZZ 10:43

ZZZZZZ 10:46

ZZZZZZ 10:50

ZZZZZZ 10:54

ZZZZZZ 10:57

ZZZZZZ 11:01

ZZZZZZ 11:05

ZZZZZZ 11:08

ZZZZZZ 11:12

ZZZZZZ 11:16

Prep Types

T = Total/NA

FORM XIII-IN Page 296 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 13:35 12/19/2012 13:39

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-173291/1-A 1 T 13:35 X

LCS 500-173291/2-A 1 T 13:35 X

ZZZZZZ 13:36

ZZZZZZ 13:36

ZZZZZZ 13:37

500-53342-1 1 T 13:38 X

ZZZZZZ 13:38

ZZZZZZ 13:39

Prep Types

T = Total/NA

FORM XIII-IN Page 297 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/24/2012 13:19 12/24/2012 14:00

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-173846/1 1 T 13:19 X

LCS 500-173846/2 1 T 13:20 X

ZZZZZZ 13:22

ZZZZZZ 13:24

ZZZZZZ 13:26

ZZZZZZ 13:28

ZZZZZZ 13:30

ZZZZZZ 13:32

ZZZZZZ 13:33

ZZZZZZ 13:35

ZZZZZZ 13:37

ZZZZZZ 13:39

ZZZZZZ 13:41

ZZZZZZ 13:43

ZZZZZZ 13:45

ZZZZZZ 13:47

ZZZZZZ 13:48

ZZZZZZ 13:50

ZZZZZZ 13:52

ZZZZZZ 13:54

ZZZZZZ 13:56

500-53342-3 1 T 13:58 X

ZZZZZZ 14:00

Prep Types

T = Total/NA

FORM XIII-IN Page 298 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 13:35 12/20/2012 17:10

9045C

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

p

H

T

y

p

e

ZZZZZZ 13:35

ZZZZZZ 13:41

ZZZZZZ 13:47

ZZZZZZ 13:53

ZZZZZZ 13:59

ZZZZZZ 18:30

ZZZZZZ 19:29

ZZZZZZ 20:28

ZZZZZZ 21:28

ZZZZZZ 22:27

ZZZZZZ 23:26

ZZZZZZ 00:25

ZZZZZZ 01:24

ZZZZZZ 02:23

ZZZZZZ 03:22

ZZZZZZ 04:22

ZZZZZZ 05:21

ZZZZZZ 06:20

ZZZZZZ 07:19

ZZZZZZ 08:18

ZZZZZZ 09:17

ZZZZZZ 10:16

ZZZZZZ 11:16

ZZZZZZ 12:15

ZZZZZZ 13:14

ZZZZZZ 14:13

ZZZZZZ 15:12

ZZZZZZ 16:11

500-53342-1 1 T 17:10 X

Prep Types

T = Total/NA

FORM XIII-IN Page 299 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 09:20 12/19/2012 11:23

9071B

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-173324/1-A 1 T 09:20 X

LCS 500-173324/2-A 1 T 09:31 X

ZZZZZZ 09:42

ZZZZZZ 09:53

ZZZZZZ 10:05

ZZZZZZ 10:16

ZZZZZZ 10:27

ZZZZZZ 10:38

ZZZZZZ 10:50

ZZZZZZ 11:01

ZZZZZZ 11:12

500-53342-1 1 T 11:23 X

Prep Types

T = Total/NA

FORM XIII-IN Page 300 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 08:40 12/19/2012 08:40

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

500-53342-1 1 T 08:40 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 301 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/21/2012 07:08 12/21/2012 13:07

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 07:08

ZZZZZZ 07:08

ZZZZZZ 07:08

ZZZZZZ 07:08

ZZZZZZ 07:08

ZZZZZZ 07:08

ZZZZZZ 07:08

500-53342-2 1 T 07:20 X X

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 08:54

ZZZZZZ 13:01

ZZZZZZ 13:01

ZZZZZZ 13:07

Prep Types

T = Total/NA

FORM XIII-IN Page 302 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/18/2012 07:13 12/18/2012 11:45

SM 2540G

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

M

o

i

s

t

T

y

p

e

ZZZZZZ 07:13

ZZZZZZ 07:13

ZZZZZZ 07:13

ZZZZZZ 07:13

ZZZZZZ 07:13

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

ZZZZZZ 08:04

500-53342-1 1 T 09:57 X

ZZZZZZ 09:57

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

ZZZZZZ 11:45

Prep Types

T = Total/NA

FORM XIII-IN Page 303 of 332 01/04/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53342-1

NOEQUIP

12/19/2012 07:31 12/19/2012 07:31

SM 2540G

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

T

S

T

y

p

e

500-53342-1 1 T 07:31 X

Prep Types

T = Total/NA

FORM XIII-IN Page 304 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Deb, Khona

12/18/12 11:25

173293 12/18/12 11:20

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL 100 mL Color Resp. is 

Blank

ICV 25 uL

500-173293/1

7196A

100 mL 100 mL Color Resp. is 

Blank

ICB 

500-173293/2

7196A

100 mL 100 mL Color Resp. is 

Blank

MB 500-173293/3 7196A

100 mL 100 mL Color Resp. is 

Blank

LCS 25 uL

500-173293/4

7196A

FC EB 5 100 mL 100 mL Color Resp. is 

Blank

500-53342-F-3 7196A T

FC EB 5 100 mL 100 mL Color Resp. is 

Blank

500-53342-F-3 25 uL

MS

7196A T

FC EB 5 100 mL 100 mL Color Resp. is 

Blank

500-53342-F-3 25 uL

MSD

7196A T

100 mL 100 mL Color Resp. is 

Blank

CCV 50 uL

500-173293/8

7196A

100 mL 100 mL Color Resp. is 

Blank

CCB 

500-173293/9

7196A

Batch Notes

Batch Comment filter paper lot# 100232

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number Hexa Chrome Color Reagent-00007

First End time See Start Date/Time

First Start time See Start Date/Time

Sulfuric Acid Reagent ID Number H2SO4 00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 305 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/27/12 13:00

173790 12/22/12 12:00

Batch Method:

TestAmerica Chicago

3060A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTCR13 00629 WSTCR2 00008 AnalysisComment

MB 500-173790/1 3060A, 7196A 2.5 g 100 mL

LCS 2.5 g 100 mL 25 uL soluble

500-173790/2

3060A, 7196A

LCS 2.5 g 100 mL 100 mL soluble 0.0105

500-173790/3

3060A, 7196A

500-53342-A-1 FC Composite 5 3060A, 7196A T 2.5007 g 100 mL

Batch Notes

Alkaline Digestion Solution Reagent ID CR6digestion_00028

Batch Comment Filter Paper Lot # 100727

First End time see above

Potassium Chromate Lot # K00741

Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002

Lead Chromate Lot # 15813PE

Lead Chromate Vendor ID Lead(II)Chrom_00001

Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002)

Magnesium Chloride Vendor JT Baker

First Start time see above

Ending Temperature 90 Celsius

Starting Temperature 90 Celsius

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 306 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/27/12 13:00

174027 12/27/12 12:40

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL Color Resp. is 

Blank

ICV 25 uL

500-174027/1

7196A

Color Resp. is 

Blank

ICB 

500-174027/2

7196A

Color Resp. is 

Blank

MB 

500-173790/1-A

7196A

Color Resp. is 

Blank

LCS 

500-173790/2-A

7196A

Color Resp. is 

Blank

LCS 

500-173790/3-A

7196A

100 mL Color Resp. is 

Blank

CCV 50 uL

500-174027/10

7196A

Color Resp. is 

Blank

CCB 

500-174027/11

7196A

FC Composite 5 Color Resp. is 

Blank

500-53342-A-1-I 7196A T

100 mL Color Resp. is 

Blank

CCV 50 uL

500-174027/18

7196A

Color Resp. is 

Blank

CCB 

500-174027/19

7196A

Batch Notes

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number CR+6 ColorRGT_00007

Sulfuric Acid Reagent ID Number H2SO4_00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 307 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

01/03/13 11:20

173980 12/27/12 09:50

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00563

MB 500-173980/1 9010B, 9014 50 mL 50 mL y

LCS 50 mL 50 mL y 500 uL

500-173980/2

9010B, 9014

500-53342-D-3 FC EB 5 9010B, 9014 T 50 mL 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00018

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 308 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/27/12 14:50

174042 12/27/12 14:40

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00571 WSTINCN2 00563

ICV 25 mL 25 mL 250 uL

500-174042/1

9014

CCV 25 mL 25 mL 500 uL

500-174042/13

9014

CCV 25 mL 25 mL 500 uL

500-174042/25

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 309 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/28/12 12:50

174096 12/28/12 11:20

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00564

MB 1.0000 g 50 mL y

500-174096/12

9010B, 9014

LCS 1.0000 g 50 mL y 500 uL

500-174096/13

9010B, 9014

500-53342-A-1 FC Composite 5 9010B, 9014 T 1.0495 g 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00018

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 310 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/28/12 15:35

174173 12/28/12 15:25

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00572 WSTINCN2 00564

ICV 25 mL 25 mL 250 uL

500-174173/1

9014

CCV 25 mL 25 mL 500 uL

500-174173/13

9014

CCV 25 mL 25 mL 500 uL

500-174173/25

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 311 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 11:15

173290 12/19/12 10:05

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-173290/1 7.3.4, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-173290/2

7.3.4, 9034

500-53342-A-1 FC Composite 5 7.3.4, 9034 T 10.2666 g 10 mL

Batch Notes

Batch Comment Balance ID # 2489

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 312 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 12:25

173472 12/19/12 12:15

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount

MB 10 mL 5 mL 4.86 mL OK 10 mL

500-173290/1-A

9034

LCS 10 mL 5 mL 0.44 mL OK 10 mL

500-173290/2-A

9034

500-53342-A-1-A FC Composite 5 9034 T 10 mL 5 mL 4.82 mL OK 10 mL

Batch Notes

Normality of Iodine Solution 0.0232 N

Nominal Amount Used 10 g

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 313 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 09:00

173844 12/24/12 08:00

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount

MB 500-173844/1 7.3.4, 9034 250 mL 250 mL

LCS 250 mL 250 mL

500-173844/2

7.3.4, 9034

500-53342-G-3 FC EB 5 7.3.4, 9034 T 250 mL 250 mL

Batch Notes

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 314 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 14:02

173845 12/24/12 13:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036

MB 250 mL 5 mL 4.91 mL OK 250 mL

500-173844/1-A

9034

LCS 250 mL 5 mL 2.49 mL OK 250 mL 5 mL

500-173844/2-A

9034

500-53342-G-3-A FC EB 5 9034 T 250 mL 5 mL 5.10 mL OK 250 mL

Batch Notes

Normality of Iodine Solution 0.0240 N

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 315 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/20/12 15:50

173625 12/20/12 10:00

Batch Method:

TestAmerica Chicago

1010

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

500-53342-A-1 FC Composite 5 1010 T gray clay

Batch Notes

Equipment ID HFP 339

Basis Basis Description

T Total/NA

1010 Page 1 of 1

Page 316 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/21/12 09:25

173450 12/21/12 05:05

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis GrossWeight TareWeight InitialAmount FinalAmount

MB 500-173450/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL

LCS 1390 g 390 g 1000 mL 1000 mL

500-173450/2

1664A, 1664A

500-53342-H-3 FC EB 5 1664A, 1664A T 1320 g 387 g 933 mL 1000 mL

Batch Notes

Batch Comment phase separating filter lot # 6711653

Concentration End Time See end date/time

Concentration Start Time See start date/time

Person's name who did the concentration See analyst name

Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, 

pf-70610210

Evaporator Temperature 50 DEG. Degrees C

Extraction Analyst see analyst name

Sulfuric Acid Lot Number MALG35029

Hexane Lot# HEXANES_00012

Manifold ID 1851

Methanol Lot Number Methanol_00007

Na2SO4 Lot Number Na2SO4_00006

Nominal Amount Used 1000 mL

Sufficient volume for MS/MSD? NO

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 317 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/21/12 11:20

173459 12/21/12 09:55

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 1000 mL 1000 mL 76 2.3144 g 2.3152 g 2.3154 g

500-173450/1-A

1664A

LCS 1000 mL 1000 mL 77 6.2848 g 6.3214 g 6.3215 g

500-173450/2-A

1664A

500-53342-H-3-A FC EB 5 1664A T 1000 mL 1000 mL 87 2.3495 g 2.3500 g 2.3501 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2 1664 HEM 00060

Pass_0.0005g 0.0007999999999

99912 g

0.0009999999999

9989 g

MB 

500-173450/1-A

1664A

Pass_0.0005g 0.0366 g 0.0367000000000

006 g

LCS 5 mL

500-173450/2-A

1664A

FC EB 5 Pass_0.0005g 0.0005000000000

00167 g

0.0005999999999

99934 g

500-53342-H-3-A 1664A T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0020 / 0.9999 g

Calibration Check Before 1st Weighing 0.0020 / 0.1002 g

Person's name who did the concentration see analyst name

Evaporator Temperature 50 Degrees C

Hexane Lot# Hexanes_00012

Methanol Lot Number Methanol_00006

Na2SO4 Lot Number Na2SO4_00006

Silica Gel Lot Number Silica gel_00003 (checked in batch 157954, 

7/31/12

Speedvap ID# 1564

Weight Set ID 1144 / 2495

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 318 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 12:55

173291 12/19/12 11:25

Batch Method:

TestAmerica Chicago

9030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-173291/1 9030B, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-173291/2

9030B, 9034

500-53342-A-1 FC Composite 5 9030B, 9034 T 10.0683 g 10 mL

Batch Notes

Batch Comment BAlance ID #2489

Distillation Temperature 70 Degrees C

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014

Sulfuric Acid Reagent ID Number 20% H2SO4_00003

Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 319 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 13:40

173474 12/19/12 13:35

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount IodineAmount TitrantVolume1 CalcMsg

MB 10 mL 5 mL 4.65 mL OK

500-173291/1-A

9034

LCS 10 mL 5 mL 0.44 mL OK

500-173291/2-A

9034

500-53342-A-1-B FC Composite 5 9034 T 10 mL 10 mL 3.31 mL OK

Batch Notes

HCl Concentration 6N

Lot # of hydrochloric acid 6NHCL00006

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0232 N

Sodium Thiosulfate Reagent ID Number NO2S2O300008

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

Normality of first Titrant 0.0246 N

Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 320 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 14:02

173846 12/24/12 13:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036

MB 500-173846/1 9034 4.91 mL 5 mL 250 mL 250 mL OK

LCS 2.49 mL 5 mL 250 mL 250 mL OK 5 mL

500-173846/2

9034

500-53342-G-3 FC EB 5 9034 T 5.10 mL 5 mL 250 mL 250 mL OK

Batch Notes

First End time 14:02

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0240 N

Sodium Thiosulfate Lot Number NO2S2O300008

Sodium Thiosulfate Vendor INHOUSE

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

First Start time 13:19

Sulfuric Acid Reagent ID Number 6NHCL00006

Normality of first Titrant 0.0246 N

Titrant Standardization Date 11/21/12

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 321 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 07:35

173324 12/19/12 05:10

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount 1664 HEM 00060

MB 500-173324/1 9071B, 9071B 10 g 10 mL

LCS 10 g 10 mL 5 mL

500-173324/2

9071B, 9071B

500-53342-A-1 FC Composite 5 9071B, 9071B T 10.1047 g 10 mL

Batch Notes

Acid used for pH adjust Lot # J23A13

Balance ID 1634

Concentration End Time See end date / time

Concentration Start Time See start date / time

Evaporator Temperature 50 DEG. C

Filter Paper Lot Number 6711653

Hexane Lot# HEXANES_00012

Na2SO4 Lot Number Na2SO4_00006

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 322 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 11:35

173330 12/19/12 09:20

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 10 mL 10 mL 24 2.3781 g 2.3790 g 2.3791 g

500-173324/1-A

9071B

LCS 10 mL 10 mL 25 2.3332 g 2.3745 g 2.3741 g

500-173324/2-A

9071B

500-53342-A-1-D FC Composite 5 9071B T 10 mL 10 mL 35 2.3177 g 2.3577 g 2.3576 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2

Pass_0.0005g 0.0009000000000

00123 g

0.0010000000000

0033 g

MB 

500-173324/1-A

9071B

Pass_0.0005g 0.0412999999999

997 g

0.0408999999999

997 g

LCS 

500-173324/2-A

9071B

FC Composite 5 Pass_0.0005g 0.04 g 0.0399000000000

003 g

500-53342-A-1-D 9071B T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0019 / 0.9999

Calibration Check Before 1st Weighing 0.0019 / 0.9999

Evaporator Temperature 50 Celsius

Filter Paper Lot # 6711653

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 323 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173667 12/21/12 07:08 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53342-A-2 FC Composite 5 Moisture T 8 1.27 g 11.33 g 3.98 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/21/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 0715

Date samples were removed from oven 12/22/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0800

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

Moisture Page 1 of 1

Page 324 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173229 12/18/12 07:13 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

SM 2540G

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53342-A-1 FC Composite 5 SM 2540G T 17 1.28 g 11.68 g 4.40 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/18/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 0720

Date samples were removed from oven 12/19/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0700

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

SM 2540G Page 1 of 1

Page 325 of 332 01/04/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173385 12/19/12 07:31 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

SM 2540G

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg

FC Composite 5 Not Calculated. 

RunCalculation 

is NULL

500-53342-A-1 SM 2540G T

Batch Notes

Basis Basis Description

T Total/NA

SM 2540G Page 1 of 1

Page 326 of 332 01/04/2013





Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53342-1

Login Number: 53342

Question Answer Comment

Creator: Scott, Sherri L

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 2.4

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

TestAmerica Chicago Page 332 of 332 01/04/2013
ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Chicago

2417 Bond Street

University Park, IL 60484

Tel: (708)534-5200

TestAmerica Job ID: 500-53342-1

Client Project/Site: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, South Carolina 29651

Attn: Mr. Robert Stevens

Authorized for release by:

1/4/2013 2:18:19 PM

Donna Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited

parameters, exceptions are noted in this report. This report may not be reproduced except in full,

and with written approval from the laboratory. For questions please contact the Project Manager

at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is

intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Project Integration, Inc

Project/Site: John Deere Des Moines Works (JDDMW)

TestAmerica Job ID: 500-53342-1

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

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Case Narrative

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Job ID: 500-53342-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-53342-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/18/2012 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 2.4o C.

GC/MS VOA 

Method(s) 8260B: One internal standard response was outside of acceptance limits for the following sample:FC Composite 5 

(500-53342-2). The sample was re-analyzed at a dilution for Acetone with all internal standard areas within limits. Both sets of data have 

been provided.

No other analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-1

Barium ☼

RL

3.01 mg/Kg

MDL

0.358

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

409 1 6010B Total/NA

Copper 693 3.01 0.815 mg/Kg 1 ☼ 6010B Total/NA

Chromium 14200 3.01 0.502 mg/Kg 1 ☼ 6010B Total/NA

Nickel 77.4 B 3.01 0.659 mg/Kg 1 ☼ 6010B Total/NA

Lead 250 B 1.50 0.517 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 238 1.50 0.228 mg/Kg 1 ☼ 6010B Total/NA

Zinc 441 6.02 2.06 mg/Kg 1 ☼ 6010B Total/NA

Chromium 0.166 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.531 0.0250 0.0100 mg/L 1 6010B TCLP

Vanadium 0.00669 J 0.0250 0.00500 mg/L 1 6010B TCLP

Zinc 0.0502 J 0.100 0.0200 mg/L 1 6010B TCLP

Mercury 0.321 0.0540 0.0206 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Cyanide, Total 0.905 J 1.59 0.524 mg/Kg 1 ☼ 9014 Total/NA

Sulfide 798 82.8 13.2 mg/Kg 1 ☼ 9034 Total/NA

pH 9.59 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 13200 1650 732 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 30.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-2

2-Butanone (MEK) ☼

RL

18.6 ug/Kg

MDL

6.72

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

28.2 1 8260B Total/NA

Acetone - DL 3200 928 241 ug/Kg 50 ☼ 8260B Total/NA

Client Sample ID: FC EB 5 Lab Sample ID: 500-53342-3

Copper

RL

0.0100 mg/L

MDL

0.00106

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

0.00616 J 1 6010B Total/NA

Lead 0.00245 J B 0.00500 0.00158 mg/L 1 6010B Total/NA

Zinc 0.00789 J 0.0200 0.00472 mg/L 1 6010B Total/NA

Client Sample ID: Trip Blank Lab Sample ID: 500-53342-4

 No Detections

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Method Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method Method Description Protocol Laboratory

8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI

6010B Metals (ICP) SW846 TAL CHI

7470A Mercury (CVAA) SW846 TAL CHI

7471A Mercury (CVAA) SW846 TAL CHI

1010 Ignitability, Pensky-Martens Closed-Cup Method SW846 TAL CHI

1664A HEM and SGT-HEM 1664A TAL CHI

7196A Chromium, Hexavalent SW846 TAL CHI

9014 Cyanide SW846 TAL CHI

9034 Sulfide, Reactive SW846 TAL CHI

9034 Sulfide, Acid soluble and Insoluble (Titrimetric) SW846 TAL CHI

9045C pH SW846 TAL CHI

9071B HEM and SGT-HEM SW846 TAL CHI

Moisture Percent Moisture EPA TAL CHI

SM 2540G Total, Fixed, and Volatile Solids SM TAL CHI

Protocol References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

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Sample Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Lab Sample ID Client Sample ID Matrix Collected Received

500-53342-1 FC Composite 5 Solid 12/17/12 14:50 12/18/12 09:40

500-53342-2 FC Composite 5 Solid 12/17/12 14:40 12/18/12 09:40

500-53342-3 FC EB 5 Water 12/17/12 14:30 12/18/12 09:40

500-53342-4 Trip Blank Water 12/17/12 00:00 12/18/12 09:40

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-1

Date Collected: 12/17/12 14:50 Matrix: Solid

Date Received: 12/18/12 09:40 Percent Solids: 30.0

Method: 6010B - Metals (ICP)

RL MDL

Barium 409 3.01 0.358 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 693 3.01 0.815 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Chromium 14200 3.01 0.502 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Nickel 77.4 B 3.01 0.659 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Lead 250 B 1.50 0.517 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Vanadium 238 1.50 0.228 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Zinc 441 6.02 2.06 mg/Kg ☼ 12/18/12 16:00 12/19/12 13:39 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/19/12 08:20 12/19/12 22:41 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:41 1

Chromium 0.166 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:41 1

Nickel 0.531 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:41 1

Lead <0.0500 0.0500 0.00500 mg/L 12/19/12 08:20 12/19/12 22:41 1

Vanadium 0.00669 J 0.0250 0.00500 mg/L 12/19/12 08:20 12/19/12 22:41 1

Zinc 0.0502 J 0.100 0.0200 mg/L 12/19/12 08:20 12/19/12 22:41 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/19/12 14:00 12/20/12 09:42 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.321 0.0540 0.0206 mg/Kg ☼ 12/19/12 14:45 12/20/12 10:21 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 12/20/12 11:00 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <3.33 3.33 1.30 mg/Kg ☼ 12/22/12 12:00 12/27/12 12:50 1

Cyanide, Total 0.905 J 1.59 0.524 mg/Kg ☼ 12/28/12 11:20 12/28/12 15:31 1

Sulfide 798 82.8 13.2 mg/Kg ☼ 12/19/12 11:25 12/19/12 13:38 1

Sulfide, Reactive <48.7 48.7 3.80 mg/Kg 12/19/12 10:50 12/19/12 12:19 1

pH 9.59 0.200 0.200 SU 12/20/12 17:10 1

HEM (Oil & Grease) 13200 1650 732 mg/Kg ☼ 12/19/12 05:10 12/19/12 11:23 1

Total Solids 30.0 0.100 0.100 % 12/19/12 07:31 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-2

Date Collected: 12/17/12 14:40 Matrix: Solid

Date Received: 12/18/12 09:40 Percent Solids: 26.9

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 28.2 18.6 6.72 ug/Kg ☼ 12/20/12 13:52 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 112 70 - 134 12/20/12 13:52 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 100 75 - 122 12/20/12 13:52 1

4-Bromofluorobenzene (Surr) 83 70 - 122 12/20/12 13:52 1

Dibromofluoromethane 111 75 - 120 12/20/12 13:52 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 3200 928 241 ug/Kg ☼ 12/19/12 13:00 12/21/12 22:40 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 94 75 - 125 12/19/12 13:00 12/21/12 22:40 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 96 75 - 120 12/19/12 13:00 12/21/12 22:40 50

4-Bromofluorobenzene (Surr) 86 75 - 120 12/19/12 13:00 12/21/12 22:40 50

Dibromofluoromethane 95 75 - 120 12/19/12 13:00 12/21/12 22:40 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 5 Lab Sample ID: 500-53342-3

Date Collected: 12/17/12 14:30 Matrix: Water

Date Received: 12/18/12 09:40

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/24/12 14:25 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/24/12 14:25 1

1,2-Dichloroethane-d4 (Surr) 94 75 - 125 12/24/12 14:25 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 100 75 - 120 12/24/12 14:25 1

4-Bromofluorobenzene (Surr) 90 75 - 120 12/24/12 14:25 1

Dibromofluoromethane 96 75 - 120 12/24/12 14:25 1

Method: 6010B - Metals (ICP)

RL MDL

Barium <0.0100 0.0100 0.000440 mg/L 12/18/12 15:30 12/19/12 15:03 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.00616 J 0.0100 0.00106 mg/L 12/18/12 15:30 12/19/12 15:03 1

Chromium <0.0100 0.0100 0.000960 mg/L 12/18/12 15:30 12/19/12 15:03 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/18/12 15:30 12/19/12 15:03 1

Lead 0.00245 J B 0.00500 0.00158 mg/L 12/18/12 15:30 12/19/12 15:03 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/18/12 15:30 12/19/12 15:03 1

Zinc 0.00789 J 0.0200 0.00472 mg/L 12/18/12 15:30 12/19/12 15:03 1

Method: 7470A - Mercury (CVAA)

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/19/12 14:00 12/20/12 10:29 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

HEM (Oil & Grease) <5.36 5.36 1.55 mg/L 12/21/12 07:09 12/21/12 10:35 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/18/12 11:22 1

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/27/12 09:50 12/27/12 14:44 1

Sulfide <1.00 1.00 0.230 mg/L 12/24/12 13:58 1

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/24/12 08:30 12/24/12 13:40 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: Trip Blank Lab Sample ID: 500-53342-4

Date Collected: 12/17/12 00:00 Matrix: Water

Date Received: 12/18/12 09:40

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/24/12 13:59 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/24/12 13:59 1

1,2-Dichloroethane-d4 (Surr) 95 75 - 125 12/24/12 13:59 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 99 75 - 120 12/24/12 13:59 1

4-Bromofluorobenzene (Surr) 92 75 - 120 12/24/12 13:59 1

Dibromofluoromethane 96 75 - 120 12/24/12 13:59 1

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Definitions/Glossary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Qualifiers

Metals

Qualifier Description

B Compound was found in the blank and sample.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

General Chemistry

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

EDL Estimated Detection Limit

EPA United States Environmental Protection Agency

MDA Minimum detectable activity

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

GC/MS VOA

Prep Batch: 173454

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-2 - DL FC Composite 5 Total/NA Solid 5030B

Analysis Batch: 173515

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-2 FC Composite 5 Total/NA Solid 8260B

LCS 500-173515/5 Lab Control Sample Total/NA Solid 8260B

MB 500-173515/4 Method Blank Total/NA Solid 8260B

Analysis Batch: 173708

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-2 - DL FC Composite 5 Total/NA Solid 8260B 173454

LCS 500-173708/4 Lab Control Sample Total/NA Solid 8260B

MB 500-173708/6 Method Blank Total/NA Solid 8260B

Analysis Batch: 173827

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 8260B

500-53342-4 Trip Blank Total/NA Water 8260B

LCS 500-173827/4 Lab Control Sample Total/NA Water 8260B

MB 500-173827/6 Method Blank Total/NA Water 8260B

Metals

Leach Batch: 173323

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 TCLP Solid 1311

LB2 500-173323/1-B LB2 Method Blank TCLP Solid 1311

LB2 500-173323/1-C LB2 Method Blank TCLP Solid 1311

Prep Batch: 173339

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 3050B

LCS 500-173339/2-A Lab Control Sample Total/NA Solid 3050B

MB 500-173339/1-A Method Blank Total/NA Solid 3050B

Prep Batch: 173349

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 3010A

LCS 500-173349/2-A Lab Control Sample Total/NA Water 3010A

MB 500-173349/1-A Method Blank Total/NA Water 3010A

Prep Batch: 173393

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 7471A

LCS 500-173393/8-A Lab Control Sample Total/NA Solid 7471A

MB 500-173393/7-A Method Blank Total/NA Solid 7471A

Prep Batch: 173406

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 TCLP Solid 3010A 173323

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Prep Batch: 173406 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LB2 500-173323/1-B LB2 Method Blank TCLP Solid 3010A 173323

LCS 500-173406/3-A Lab Control Sample Total/NA Solid 3010A

Prep Batch: 173428

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 TCLP Solid 7470A 173323

500-53342-3 FC EB 5 Total/NA Water 7470A

LB2 500-173323/1-C LB2 Method Blank TCLP Solid 7470A 173323

LCS 500-173428/8-A Lab Control Sample Total/NA Water 7470A

MB 500-173428/7-A Method Blank Total/NA Water 7470A

Analysis Batch: 173517

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 6010B 173339

500-53342-3 FC EB 5 Total/NA Water 6010B 173349

LCS 500-173339/2-A Lab Control Sample Total/NA Solid 6010B 173339

LCS 500-173349/2-A Lab Control Sample Total/NA Water 6010B 173349

MB 500-173339/1-A Method Blank Total/NA Solid 6010B 173339

MB 500-173349/1-A Method Blank Total/NA Water 6010B 173349

Analysis Batch: 173518

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 TCLP Solid 6010B 173406

LB2 500-173323/1-B LB2 Method Blank TCLP Solid 6010B 173406

LCS 500-173406/3-A Lab Control Sample Total/NA Solid 6010B 173406

Analysis Batch: 173572

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 TCLP Solid 7470A 173428

500-53342-3 FC EB 5 Total/NA Water 7470A 173428

LB2 500-173323/1-C LB2 Method Blank TCLP Solid 7470A 173428

LCS 500-173428/8-A Lab Control Sample Total/NA Water 7470A 173428

MB 500-173428/7-A Method Blank Total/NA Water 7470A 173428

Analysis Batch: 173573

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173393/8-A Lab Control Sample Total/NA Solid 7471A 173393

MB 500-173393/7-A Method Blank Total/NA Solid 7471A 173393

Analysis Batch: 173574

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 7471A 173393

General Chemistry

Analysis Batch: 173229

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid SM 2540G

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 173290

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 7.3.4

LCS 500-173290/2-A Lab Control Sample Total/NA Solid 7.3.4

MB 500-173290/1-A Method Blank Total/NA Solid 7.3.4

Prep Batch: 173291

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9030B

LCS 500-173291/2-A Lab Control Sample Total/NA Solid 9030B

MB 500-173291/1-A Method Blank Total/NA Solid 9030B

Analysis Batch: 173293

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 7196A

500-53342-3 MS FC EB 5 Total/NA Water 7196A

500-53342-3 MSD FC EB 5 Total/NA Water 7196A

LCS 500-173293/4 Lab Control Sample Total/NA Water 7196A

MB 500-173293/3 Method Blank Total/NA Water 7196A

Prep Batch: 173324

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9071B

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B

MB 500-173324/1-A Method Blank Total/NA Solid 9071B

Analysis Batch: 173330

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9071B 173324

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B 173324

MB 500-173324/1-A Method Blank Total/NA Solid 9071B 173324

Analysis Batch: 173385

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid SM 2540G

Analysis Batch: 173404

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid Moisture

Prep Batch: 173450

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 1664A

LCS 500-173450/2-A Lab Control Sample Total/NA Water 1664A

MB 500-173450/1-A Method Blank Total/NA Water 1664A

Analysis Batch: 173459

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 1664A 173450

LCS 500-173450/2-A Lab Control Sample Total/NA Water 1664A 173450

MB 500-173450/1-A Method Blank Total/NA Water 1664A 173450

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Analysis Batch: 173472

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9034 173290

LCS 500-173290/2-A Lab Control Sample Total/NA Solid 9034 173290

MB 500-173290/1-A Method Blank Total/NA Solid 9034 173290

Analysis Batch: 173474

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9034 173291

LCS 500-173291/2-A Lab Control Sample Total/NA Solid 9034 173291

MB 500-173291/1-A Method Blank Total/NA Solid 9034 173291

Analysis Batch: 173479

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9045C

Analysis Batch: 173625

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 1010

Analysis Batch: 173667

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-2 FC Composite 5 Total/NA Solid Moisture

Prep Batch: 173790

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 3060A

LCS 500-173790/2-A Lab Control Sample Total/NA Solid 3060A

LCS 500-173790/3-A Lab Control Sample Total/NA Solid 3060A

MB 500-173790/1-A Method Blank Total/NA Solid 3060A

Prep Batch: 173844

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 7.3.4

LCS 500-173844/2-A Lab Control Sample Total/NA Water 7.3.4

MB 500-173844/1-A Method Blank Total/NA Water 7.3.4

Analysis Batch: 173845

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 9034 173844

LCS 500-173844/2-A Lab Control Sample Total/NA Water 9034 173844

MB 500-173844/1-A Method Blank Total/NA Water 9034 173844

Analysis Batch: 173846

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 9034

LCS 500-173846/2 Lab Control Sample Total/NA Water 9034

MB 500-173846/1 Method Blank Total/NA Water 9034

Prep Batch: 173980

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 9010B

LCS 500-173980/2-A Lab Control Sample Total/NA Water 9010B

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 173980 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

MB 500-173980/1-A Method Blank Total/NA Water 9010B

Analysis Batch: 174027

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 7196A 173790

LCS 500-173790/2-A Lab Control Sample Total/NA Solid 7196A 173790

LCS 500-173790/3-A Lab Control Sample Total/NA Solid 7196A 173790

MB 500-173790/1-A Method Blank Total/NA Solid 7196A 173790

Analysis Batch: 174042

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-3 FC EB 5 Total/NA Water 9014 173980

LCS 500-173980/2-A Lab Control Sample Total/NA Water 9014 173980

MB 500-173980/1-A Method Blank Total/NA Water 9014 173980

Prep Batch: 174096

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9010B

LCS 500-174096/13-A Lab Control Sample Total/NA Solid 9010B

MB 500-174096/12-A Method Blank Total/NA Solid 9010B

Analysis Batch: 174173

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53342-1 FC Composite 5 Total/NA Solid 9014 174096

LCS 500-174096/13-A Lab Control Sample Total/NA Solid 9014 174096

MB 500-174096/12-A Method Blank Total/NA Solid 9014 174096

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Surrogate Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (70-134) (75-122) (70-122) (75-120)

12DCE TOL BFB DBFM

500-53342-2 112 100 83 111

Percent Surrogate Recovery (Acceptance Limits)

FC Composite 5

LCS 500-173515/5 Lab Control Sample 98 111 102 103

MB 500-173515/4 Method Blank 106 113 107 103

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE DBFM TOL BFB

500-53342-2 - DL 94 95 96 86

Percent Surrogate Recovery (Acceptance Limits)

FC Composite 5

LCS 500-173708/4 Lab Control Sample 94 96 97 103

MB 500-173708/6 Method Blank 90 88 97 88

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Water Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE TOL BFB DBFM

500-53342-3 94 100 90 96

Percent Surrogate Recovery (Acceptance Limits)

FC EB 5

500-53342-4 Trip Blank 95 99 92 96

LCS 500-173827/4 Lab Control Sample 92 97 94 92

MB 500-173827/6 Method Blank 90 96 88 92

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: MB 500-173515/4 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173515

RL MDL

Acetone <5.00 5.00 2.16 ug/Kg 12/20/12 09:00 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.81 ug/Kg 12/20/12 09:00 1

1,2-Dichloroethane-d4 (Surr) 106 70 - 134 12/20/12 09:00 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 113 75 - 122 12/20/12 09:00 1

4-Bromofluorobenzene (Surr) 107 70 - 122 12/20/12 09:00 1

Dibromofluoromethane 103 75 - 120 12/20/12 09:00 1

Lab Sample ID: LCS 500-173515/5 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173515

Acetone 50.0 43.68 ug/Kg 87 50 - 138

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 45.67 ug/Kg 91 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

98

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 111 75 - 122

4-Bromofluorobenzene (Surr) 102 70 - 122

Dibromofluoromethane 103 75 - 120

Lab Sample ID: MB 500-173708/6 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173708

RL MDL

Acetone <5.00 5.00 1.30 ug/Kg 12/21/12 13:16 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/Kg 12/21/12 13:16 1

1,2-Dichloroethane-d4 (Surr) 90 75 - 125 12/21/12 13:16 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 97 75 - 120 12/21/12 13:16 1

4-Bromofluorobenzene (Surr) 88 75 - 120 12/21/12 13:16 1

Dibromofluoromethane 88 75 - 120 12/21/12 13:16 1

Lab Sample ID: LCS 500-173708/4 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173708

Acetone 50.0 46.74 ug/Kg 93 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 41.90 ug/Kg 84 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

94

LCS LCS

%Recovery Qualifier Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 500-173708/4 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173708

Toluene-d8 (Surr) 75 - 120

Surrogate

97

LCS LCS

%Recovery Qualifier Limits

4-Bromofluorobenzene (Surr) 103 75 - 120

Dibromofluoromethane 96 75 - 120

Lab Sample ID: MB 500-173827/6 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173827

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/24/12 13:33 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/24/12 13:33 1

1,2-Dichloroethane-d4 (Surr) 90 75 - 125 12/24/12 13:33 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 96 75 - 120 12/24/12 13:33 1

4-Bromofluorobenzene (Surr) 88 75 - 120 12/24/12 13:33 1

Dibromofluoromethane 92 75 - 120 12/24/12 13:33 1

Lab Sample ID: LCS 500-173827/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173827

Acetone 50.0 48.03 ug/L 96 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 50.18 ug/L 100 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

92

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 92 75 - 120

Method: 6010B - Metals (ICP)

Lab Sample ID: MB 500-173339/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173339

RL MDL

Barium <1.00 1.00 0.119 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <1.00 1.00 0.271 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

Chromium <1.00 1.00 0.167 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

Nickel 0.3300 J 1.00 0.219 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

Lead 0.2580 J 0.500 0.172 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

Vanadium <0.500 0.500 0.0759 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

Zinc <2.00 2.00 0.686 mg/Kg 12/18/12 16:00 12/19/12 10:33 1

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: LCS 500-173339/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173339

Barium 200 199.5 mg/Kg 100 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 25.0 25.15 mg/Kg 101 80 - 120

Chromium 20.0 20.20 mg/Kg 101 80 - 120

Nickel 50.0 49.95 mg/Kg 100 80 - 120

Lead 10.0 10.14 mg/Kg 101 80 - 120

Vanadium 50.0 50.42 mg/Kg 101 80 - 120

Zinc 50.0 49.15 mg/Kg 98 80 - 120

Lab Sample ID: MB 500-173349/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173349

RL MDL

Barium 0.002710 J 0.0100 0.000440 mg/L 12/18/12 15:30 12/19/12 13:52 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0100 0.0100 0.00106 mg/L 12/18/12 15:30 12/19/12 13:52 1

Chromium 0.001210 J 0.0100 0.000960 mg/L 12/18/12 15:30 12/19/12 13:52 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/18/12 15:30 12/19/12 13:52 1

Lead 0.002720 J 0.00500 0.00158 mg/L 12/18/12 15:30 12/19/12 13:52 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/18/12 15:30 12/19/12 13:52 1

Zinc <0.0200 0.0200 0.00472 mg/L 12/18/12 15:30 12/19/12 13:52 1

Lab Sample ID: LCS 500-173349/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173349

Barium 2.00 1.955 mg/L 98 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2524 mg/L 101 80 - 120

Chromium 0.200 0.1989 mg/L 99 80 - 120

Nickel 0.500 0.4934 mg/L 99 80 - 120

Lead 0.100 0.1010 mg/L 101 80 - 120

Vanadium 0.500 0.4993 mg/L 100 80 - 120

Zinc 0.500 0.4858 mg/L 97 80 - 120

Lab Sample ID: LCS 500-173406/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173518 Prep Batch: 173406

Barium 2.00 1.975 mg/L 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2464 mg/L 99 80 - 120

Chromium 0.200 0.1969 mg/L 98 80 - 120

Nickel 0.500 0.4873 mg/L 97 80 - 120

Lead 0.100 0.09785 mg/L 98 80 - 120

Vanadium 0.500 0.4959 mg/L 99 80 - 120

Zinc 0.500 0.4782 mg/L 96 80 - 120

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: LB2 500-173323/1-B LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173518 Prep Batch: 173406

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/19/12 08:20 12/19/12 21:13 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:13 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:13 1

Nickel <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:13 1

Lead <0.0500 0.0500 0.00500 mg/L 12/19/12 08:20 12/19/12 21:13 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/19/12 08:20 12/19/12 21:13 1

Zinc <0.100 0.100 0.0200 mg/L 12/19/12 08:20 12/19/12 21:13 1

Method: 7470A - Mercury (CVAA)

Lab Sample ID: MB 500-173428/7-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173572 Prep Batch: 173428

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/19/12 14:00 12/20/12 09:32 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173428/8-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173572 Prep Batch: 173428

Mercury 0.00200 0.002086 mg/L 104 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LB2 500-173323/1-C LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173572 Prep Batch: 173428

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/19/12 14:00 12/20/12 09:40 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

Lab Sample ID: MB 500-173393/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173573 Prep Batch: 173393

RL MDL

Mercury <0.0167 0.0167 0.00637 mg/Kg 12/19/12 14:45 12/20/12 09:16 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173393/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173573 Prep Batch: 173393

Mercury 0.167 0.1467 mg/Kg 88 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 1664A - HEM and SGT-HEM

Lab Sample ID: MB 500-173450/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173459 Prep Batch: 173450

RL MDL

HEM (Oil & Grease) <5.00 5.00 1.45 mg/L 12/21/12 05:05 12/21/12 09:55 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173450/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173459 Prep Batch: 173450

HEM (Oil & Grease) 40.0 36.70 mg/L 92 78 - 114

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 7196A - Chromium, Hexavalent

Lab Sample ID: MB 500-173293/3 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173293

RL MDL

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/18/12 11:21 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173293/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173293

Chromium, hexavalent 0.250 0.2652 mg/L 106 85 - 115

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53342-3 MS Client Sample ID: FC EB 5

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173293

Chromium, hexavalent <0.0100 0.250 0.2502 mg/L 100 85 - 115

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53342-3 MSD Client Sample ID: FC EB 5

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173293

Chromium, hexavalent <0.0100 0.250 0.2555 mg/L 102 85 - 115 2 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Lab Sample ID: MB 500-173790/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

RL MDL

Chromium, hexavalent <1.00 1.00 0.389 mg/Kg 12/22/12 12:00 12/27/12 12:41 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7196A - Chromium, Hexavalent (Continued)

Lab Sample ID: LCS 500-173790/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

Chromium, hexavalent 10.0 9.188 mg/Kg 92 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LCS 500-173790/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

Chromium, hexavalent 676 669.0 mg/Kg 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9014 - Cyanide

Lab Sample ID: MB 500-173980/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174042 Prep Batch: 173980

RL MDL

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/27/12 09:50 12/27/12 14:40 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173980/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174042 Prep Batch: 173980

Cyanide, Total 0.100 0.1066 mg/L 107 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-174096/12-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

RL MDL

Cyanide, Total <0.500 0.500 0.165 mg/Kg 12/28/12 11:20 12/28/12 15:30 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174096/13-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

Cyanide, Total 5.00 5.325 mg/Kg 107 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Reactive

Lab Sample ID: MB 500-173290/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173472 Prep Batch: 173290

RL MDL

Sulfide, Reactive <50.0 50.0 3.90 mg/Kg 12/19/12 10:05 12/19/12 12:15 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9034 - Sulfide, Reactive (Continued)

Lab Sample ID: LCS 500-173290/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173472 Prep Batch: 173290

Sulfide, Reactive 180 168.6 mg/Kg 94 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173844/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173845 Prep Batch: 173844

RL MDL

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/24/12 08:00 12/24/12 13:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173844/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173845 Prep Batch: 173844

Sulfide, Reactive 3.60 3.767 mg/L 105 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)

Lab Sample ID: MB 500-173291/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173474 Prep Batch: 173291

RL MDL

Sulfide <25.0 25.0 4.00 mg/Kg 12/19/12 11:25 12/19/12 13:35 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173291/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173474 Prep Batch: 173291

Sulfide 180 168.3 mg/Kg 93 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173846/1 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173846

RL MDL

Sulfide <1.00 1.00 0.230 mg/L 12/24/12 13:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173846/2 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173846

Sulfide 3.60 3.760 mg/L 104 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

TestAmerica Chicago

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9071B - HEM and SGT-HEM

Lab Sample ID: MB 500-173324/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

RL MDL

HEM (Oil & Grease) <500 500 222 mg/Kg 12/19/12 05:10 12/19/12 09:20 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173324/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

HEM (Oil & Grease) 4000 4090 mg/Kg 102 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

TestAmerica Chicago

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-1

Date Collected: 12/17/12 14:50 Matrix: Solid

Date Received: 12/18/12 09:40 Percent Solids: 30.0

Prep 3050B 173339 12/18/12 16:00 RL TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Analysis 6010B 1 173517 12/19/12 13:39 TDS TAL CHI

TCLP Leach 1311 173323 12/18/12 14:00 DB TAL CHI

TCLP Prep 3010A 173406 12/19/12 08:20 LAH TAL CHI

TCLP Analysis 6010B 1 173518 12/19/12 22:41 TDS TAL CHI

TCLP Prep 7470A 173428 12/19/12 14:00 BJB TAL CHI

TCLP Analysis 7470A 1 173572 12/20/12 09:42 BJB TAL CHI

Total/NA Prep 7471A 173393 12/19/12 14:45 BJB TAL CHI

Total/NA Analysis 7471A 1 173574 12/20/12 10:21 BJB TAL CHI

Total/NA Analysis SM 2540G 1 173229 12/18/12 09:57 CMV TAL CHI

Total/NA Prep 9071B 173324 12/19/12 05:10 MTB TAL CHI

Total/NA Analysis 9071B 1 173330 12/19/12 11:23 MTB TAL CHI

Total/NA Analysis SM 2540G 1 173385 12/19/12 07:31 CMV TAL CHI

Total/NA Analysis Moisture 1 173404 12/19/12 08:40 CMV TAL CHI

Total/NA Prep 7.3.4 173290 12/19/12 10:50 CLM TAL CHI

Total/NA Analysis 9034 1 173472 12/19/12 12:19 CLM TAL CHI

Total/NA Prep 9030B 173291 12/19/12 11:25 CLM TAL CHI

Total/NA Analysis 9034 1 173474 12/19/12 13:38 CLM TAL CHI

Total/NA Analysis 9045C 1 173479 CLM TAL CHI

12/20/12 17:10

12/20/12 18:10

(Start)

(End)

Total/NA Analysis 1010 1 173625 APW TAL CHI

12/20/12 11:00

12/20/12 12:00

(Start)

(End)

Total/NA Prep 3060A 173790 12/22/12 12:00 APW TAL CHI

Total/NA Analysis 7196A 1 174027 APW TAL CHI

12/27/12 12:50

12/27/12 12:51

(Start)

(End)

Total/NA Prep 9010B 174096 12/28/12 11:20 EAT TAL CHI

Total/NA Analysis 9014 1 174173 EAT TAL CHI

12/28/12 15:31

12/28/12 15:31

(Start)

(End)

Client Sample ID: FC Composite 5 Lab Sample ID: 500-53342-2

Date Collected: 12/17/12 14:40 Matrix: Solid

Date Received: 12/18/12 09:40 Percent Solids: 26.9

Analysis 8260B 1 173515 12/20/12 13:52 BDW TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 173454 12/19/12 13:00 WRE TAL CHI

Total/NA Analysis 8260B DL 50 173708 12/21/12 22:40 EA TAL CHI

Total/NA Analysis Moisture 1 173667 12/21/12 07:20 CMV TAL CHI

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 5 Lab Sample ID: 500-53342-3

Date Collected: 12/17/12 14:30 Matrix: Water

Date Received: 12/18/12 09:40

Analysis 8260B 1 173827 12/24/12 14:25 EA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 3010A 173349 12/18/12 15:30 RL TAL CHI

Total/NA Analysis 6010B 1 173517 12/19/12 15:03 TDS TAL CHI

Total/NA Prep 7470A 173428 12/19/12 14:00 BJB TAL CHI

Total/NA Analysis 7470A 1 173572 12/20/12 10:29 BJB TAL CHI

Total/NA Analysis 7196A 1 173293 KD TAL CHI

12/18/12 11:22

12/18/12 11:22

(Start)

(End)

Total/NA Prep 1664A 173450 12/21/12 07:09 MTB TAL CHI

Total/NA Analysis 1664A 1 173459 12/21/12 10:35 MTB TAL CHI

Total/NA Prep 7.3.4 173844 12/24/12 08:30 CLB TAL CHI

Total/NA Analysis 9034 1 173845 12/24/12 13:40 CLB TAL CHI

Total/NA Analysis 9034 1 173846 CLB TAL CHI

12/24/12 13:58

12/24/12 14:00

(Start)

(End)

Total/NA Prep 9010B 173980 12/27/12 09:50 EAT TAL CHI

Total/NA Analysis 9014 1 174042 EAT TAL CHI

12/27/12 14:44

12/27/12 14:44

(Start)

(End)

Client Sample ID: Trip Blank Lab Sample ID: 500-53342-4

Date Collected: 12/17/12 00:00 Matrix: Water

Date Received: 12/18/12 09:40

Analysis 8260B 1 173827 12/24/12 13:59 EA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

TestAmerica Chicago

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Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory: TestAmerica Chicago

All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alabama State Program 4 40461 04-30-13

California NELAP 9 01132CA 04-30-13

Georgia State Program 4 N/A 04-30-13

Georgia State Program 4 939 04-30-13

Hawaii State Program 9 N/A 04-30-13

Illinois NELAP 5 100201 04-30-13

Indiana State Program 5 C-IL-02 04-30-13

Iowa State Program 7 82 05-01-14

Kansas NELAP 7 E-10161 10-31-13

Kentucky State Program 4 90023 12-31-12

Kentucky (UST) State Program 4 66 04-11-13

L-A-B DoD ELAP L2304 01-06-13

L-A-B ISO/IEC 17025 L2304 01-06-13

Louisiana NELAP 6 30720 06-30-13

Massachusetts State Program 1 M-IL035 06-30-13

Mississippi State Program 4 N/A 04-30-13

North Carolina DENR State Program 4 291 12-31-13

North Dakota State Program 8 R-194 04-30-13

Oklahoma State Program 6 8908 08-31-13

South Carolina State Program 4 77001 04-30-13

Texas NELAP 6 T104704252-09-TX 02-28-13

USDA Federal P330-12-00038 02-06-15

Virginia NELAP 3 460142 06-14-13

Wisconsin State Program 5 999580010 08-31-13

Wyoming State Program 8 8TMS-Q 04-30-13

TestAmerica Chicago

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Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53342-1

Login Number: 53342

Question Answer Comment

Creator: Scott, Sherri L

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 2.4

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

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