Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received Higher Heating Value 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Moisture 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Ash 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 As Received % Sulfur 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Higher Heating Value 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis % Ash 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis % Sulfur 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Antimony 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Arsenic 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Beryllium 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Cadmium 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Chlorine 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Chromium 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Cobalt 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Fluorine 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Lead 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Manganese 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Mercury 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis Nickel 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dry

basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174/D5142 ASTM D4239 Method B ASTM D5865 ASTM D3174/D5142 ASTM D4239 Method B ASTM D3683 ASTM D3683 ASTM D3683 ASTM D3683 ASTM D6721 ASTM D3683 ASTM D3683 ASTM D3761 ASTM D3683 ASTM D3683 ASTM D6722 ASTM D3683 ASTM D3683EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 19 6/20/2010 6/20/2010 12271.00 Btu/lb 20 6/20/2010 6/20/2010 12454.00 Btu/lb 21 6/20/2010 6/20/2010 12408.00 Btu/lb 22 6/20/2010 6/20/2010 12286.00 Btu/lb 28 6/29/2010 6/29/2010 12841.00 Btu/lb 29 6/29/2010 6/29/2010 12611.00 Btu/lb 30 6/30/2010 6/30/2010 12943.00 Btu/lb 31 6/30/2010 6/30/2010 12992.00 Btu/lb 32 7/1/2010 7/1/2010 12924.00 Btu/lb 33 7/1/2010 7/1/2010 12839.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 5.03 12.65 0.81 12922 Btu/lb 13.32 0.85 4.61 12.1 0.81 13056 Btu/lb 12.69 0.85 4.32 12.39 0.81 12968 Btu/lb 12.95 0.84 4.69 12.88 0.84 12890 Btu/lb 13.51 0.88 5.03 9.39 1.3 13521 Btu/lb 9.89 1.37 5.14 10.77 1.27 13293 Btu/lb 11.35 1.34 4.88 8.92 1.14 13607 Btu/lb 9.38 1.2 4.57 9.05 1.32 13615 Btu/lb 9.48 1.38 4.76 9.59 1.23 13570 Btu/lb 10.07 1.29 4.87 9.46 1.19 13497 Btu/lb 9.84 1.25Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 790 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 3 840 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 3 860 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 3 770 ppm 0.1 μg/g <2.0 μg/g <2.0 μg/g 4 1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 1000 ppm 0.07 μg/g <2.0 μg/g 6 μg/g 4 1000 ppm 0.09 μg/g <2.0 μg/g 11 μg/g 4 1100 ppm 0.09 μg/g <2.0 μg/g 6 μg/g 4 1100 ppm 0.08 μg/g <2.0 μg/g 7 μg/g 4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g <2.0 μg/g 28 μg/g 13 μg/g 11 μg/g μg/g <2.0 μg/g 28 μg/g 20 μg/g 11 μg/g μg/g <2.0 μg/g 25 μg/g 13 μg/g 63 μg/g μg/g <2.0 μg/g 28 μg/g 14 μg/g 12 μg/g μg/g <2.0 μg/g 15 μg/g 11 μg/g 12 μg/g μg/g <2.0 μg/g 15 μg/g 12 μg/g 14 μg/g μg/g <2.0 μg/g 15 μg/g 10 μg/g 11 μg/g μg/g <2.0 μg/g 14 μg/g 11 μg/g 9 μg/g μg/g <2.0 μg/g 17 μg/g 12 μg/g 11 μg/g μg/g <2.0 μg/g 16 μg/g 11 μg/g 12 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 15 μg/g <2.0 μg/g 70 ppm 12 μg/g 16 μg/g <2.0 μg/g 63 ppm 13 μg/g 14 μg/g <2.0 μg/g 62 ppm 12 μg/g 14 μg/g <2.0 μg/g 68 ppm 13 μg/g 12 μg/g <2.0 μg/g 82 ppm 10 μg/g 12 μg/g <2.0 μg/g 63 ppm 10 μg/g 11 μg/g <2.0 μg/g 91 ppm 9 μg/g 10 μg/g <2.0 μg/g 62 ppm 9 μg/g 13 μg/g <2.0 μg/g 74 ppm 10 μg/g 11 μg/g <2.0 μg/g 69 ppm 9 μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygenEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 28 6/29/2010 6/29/2010 12841.00 Btu/lb 29 6/29/2010 6/29/2010 12611.00 Btu/lb 30 6/30/2010 6/30/2010 12943.00 Btu/lb 31 6/30/2010 6/30/2010 12992.00 Btu/lb 32 7/1/2010 7/1/2010 12924.00 Btu/lb 33 7/1/2010 7/1/2010 12839.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 5.03 9.39 1.3 13521 Btu/lb 9.89 1.37 5.14 10.77 1.27 13293 Btu/lb 11.35 1.34 4.88 8.92 1.14 13607 Btu/lb 9.38 1.2 4.57 9.05 1.32 13615 Btu/lb 9.48 1.38 4.76 9.59 1.23 13570 Btu/lb 10.07 1.29 4.87 9.46 1.19 13497 Btu/lb 9.84 1.25Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 1100 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 1000 ppm 0.07 μg/g <2.0 μg/g 6 μg/g 4 1000 ppm 0.09 μg/g <2.0 μg/g 11 μg/g 4 1100 ppm 0.09 μg/g <2.0 μg/g 6 μg/g 4 1100 ppm 0.08 μg/g <2.0 μg/g 7 μg/g 4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g <2.0 μg/g 15 μg/g 11 μg/g 12 μg/g μg/g <2.0 μg/g 15 μg/g 12 μg/g 14 μg/g μg/g <2.0 μg/g 15 μg/g 10 μg/g 11 μg/g μg/g <2.0 μg/g 14 μg/g 11 μg/g 9 μg/g μg/g <2.0 μg/g 17 μg/g 12 μg/g 11 μg/g μg/g <2.0 μg/g 16 μg/g 11 μg/g 12 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 12 μg/g <2.0 μg/g 82 ppm 10 μg/g 12 μg/g <2.0 μg/g 63 ppm 10 μg/g 11 μg/g <2.0 μg/g 91 ppm 9 μg/g 10 μg/g <2.0 μg/g 62 ppm 9 μg/g 13 μg/g <2.0 μg/g 74 ppm 10 μg/g 11 μg/g <2.0 μg/g 69 ppm 9 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

OxygenEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 23 6/28/2010 6/28/2010 12513.00 Btu/lb 24 6/28/2010 6/28/2010 12558.00 Btu/lb 25 6/28/2010 6/28/2010 12386.00 Btu/lb 26 6/28/2010 6/28/2010 12320.00 Btu/lb 27 6/28/2010 6/28/2010 12583.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 4.9 11.29 0.96 13158 Btu/lb 11.87 1.01 4.43 11.45 1.03 13141 Btu/lb 11.98 1.08 4.67 12.24 0.98 12993 Btu/lb 12.84 1.03 4.76 12.67 0.97 12935 Btu/lb 13.3 1.02 4.37 11.42 0.96 13158 Btu/lb 11.94 1.01Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 910 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 3 900 ppm 0.11 μg/g <2.0 μg/g <2.0 μg/g 4 970 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 860 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4 910 ppm 0.08 μg/g <2.0 μg/g <2.0 μg/g 4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g <2.0 μg/g 24 μg/g 15 μg/g 10 μg/g μg/g <2.0 μg/g 25 μg/g 14 μg/g 10 μg/g μg/g <2.0 μg/g 23 μg/g 13 μg/g 11 μg/g μg/g <2.0 μg/g 25 μg/g 14 μg/g 11 μg/g μg/g <2.0 μg/g 24 μg/g 13 μg/g 21 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 14 μg/g <2.0 μg/g 85 ppm 14 μg/g 14 μg/g <2.0 μg/g 121 ppm 13 μg/g 15 μg/g <2.0 μg/g 71 ppm 13 μg/g 14 μg/g <2.0 μg/g 90 ppm 13 μg/g 15 μg/g <2.0 μg/g 69 ppm 13 μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 54755 Westmoreland Partners Roanoke Valley Energy Authority Boiler 2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm