# ANALYTICAL REPORT Job Number: 500-53342-1 Job Description: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, SC 29651 Attention: Mr. Robert Stevens

_____________________________________________Approved for release. Donna L Ingersoll Project Manager II 1/4/2013 2:22 PM 

# Donna L Ingersoll Project Manager II donna.ingersoll@testamericainc.com

01/04/2013

cc:Mr. David Kirby Mr. Robert Malcomson 

## These test results meet all the requirements of NELAC for accredited parameters. The Lab Certification ID# is 100201.
All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be reproduced only in its entirety.
Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street, University Park, IL 60484 Tel (708) 534-5200 Fax (708) 534-5211www.testamericainc.com 

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# Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 5 Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 6 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 9 Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 10 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 11 Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 13 Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 14 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 24 QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 27 Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 46 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 47 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 53 Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 57 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 81 Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82 GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 82 Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 82 Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 83 Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 104 Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 108 Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 108 Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 138 Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 159 Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 159

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# Table of Contents
Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 162 Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 165 Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 171 Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .174 Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 174 Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 175 Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 176 Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 179 Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 179 Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 187 Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 190 Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 203 Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 209 Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 214 Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 226 Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 229 Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 234 Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 243 General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 249 Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 250 Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 251 Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 254 Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 254 Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 258 Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 259 Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 261

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# Table of Contents Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 263 Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 281 Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 289 Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 305 Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . .327 Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 330 Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 332

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### Job Narrative 500-53342-1 Comments 

### No additional comments. Receipt 

### The samples were received on 12/18/2012 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.4o C. GC/MS VOA 

### Method(s) 8260B: One internal standard response was outside of acceptance limits for the following sample:FC Composite 5 (500-53342-2). The sample was re- analyzed at a dilution for Acetone with all internal standard areas within limits . Both sets of data have been provided. No other analytical or quality issues were noted. Metals 

### No analytical or quality issues were noted. General Chemistry 

### No analytical or quality issues were noted.



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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53342-1

Instrument ID: Analysis Batch Number: CMS16 170196 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD1 500-170196/6 IC 16I1119A.D 11/19/12 12:14 GC Column:DB624 ID:0.2(mm)

Acetone Poor chromatography wernerb 11/19/12 13:19 1.91

8260B 

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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53342-1

Instrument ID: Analysis Batch Number: CMS22 172614 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD01 500-172614/2 IC 22I1211A.D 12/11/12 14:23 GC Column:DB624 ID:0.2(mm)

Trichloroethene Baseline alikpalae 12/11/12 19:50 7.55 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD02 500-172614/3 IC 22I1211B.D 12/11/12 14:51 GC Column:DB624 ID:0.2(mm)

Bromomethane Baseline alikpalae 12/11/12 19:54 2.01 Acetonitrile Split Peak alikpalae 12/11/12 19:54 3.59 Tetrachloroethene Split Peak alikpalae 12/11/12 19:54 9.75

8260B 

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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53342-1

Instrument ID: Analysis Batch Number: CMS22 172615 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD01 500-172615/2 IC 22I1211A.D 12/11/12 14:23 GC Column:DB624 ID:0.2(mm)

Trichloroethene Baseline alikpalae 12/11/12 19:50 7.55 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD02 500-172615/3 IC 22I1211B.D 12/11/12 14:51 GC Column:DB624 ID:0.2(mm)

Bromomethane Baseline alikpalae 12/11/12 19:54 2.01 Acetonitrile Split Peak alikpalae 12/11/12 19:54 3.59 Tetrachloroethene Split Peak alikpalae 12/11/12 19:54 9.75

8260B 

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## SAMPLE SUMMARY Client: Project Integration, Inc Job Number: 500-53342-1
Client Sample ID Lab Sample ID Client Matrix Sampled Received Date/Time Date/Time
500-53342-1 FC Composite 5 Solid 12/17/2012 1450 12/18/2012 0940 500-53342-2 FC Composite 5 Solid 12/17/2012 1440 12/18/2012 0940 500-53342-3 FC EB 5 Water 12/17/2012 1430 12/18/2012 0940 500-53342-4 Trip Blank Water 12/17/2012 0000 12/18/2012 0940

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53342-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier

500-53342-1 FC COMPOSITE 5 

### 3.01 mg/Kg 6010B 409 Barium 3.01 mg/Kg 6010B 693 Copper 3.01 mg/Kg 6010B 14200 Chromium 3.01 mg/Kg 6010B 77.4 B Nickel 1.50 mg/Kg 6010B 250 B Lead 1.50 mg/Kg 6010B 238 Vanadium 6.02 mg/Kg 6010B 441 Zinc 0.0540 mg/Kg 7471A 0.321 Mercury 40.0 Degrees F 1010 >176 Flashpoint 1.59 mg/Kg 9014 0.905 J Cyanide,Total 82.8 mg/Kg 9034 798 Sulfide 0.200 SU 9045C 9.59 pH 1650 mg/Kg 9071B 13200 HEM (Oil & Grease) 0.10 % Moisture 70 Percent Moisture 0.10 % Moisture 30 Percent Solids 0.100 % SM 2540G 70.0 % Moisture 0.100 % SM 2540G 30.0 Total Solids 

### TCLP 0.0250 mg/L 6010B 0.166 Chromium 0.0250 mg/L 6010B 0.531 Nickel 0.0250 mg/L 6010B 0.00669 J Vanadium 0.100 mg/L 6010B 0.0502 J Zinc

500-53342-2 FC COMPOSITE 5 

### 928 ug/Kg 8260B 3200 Acetone 18.6 ug/Kg 8260B 28.2 2-Butanone (MEK) 0.10 % Moisture 73 Percent Moisture 0.10 % Moisture 27 Percent Solids

500-53342-3 FC EB 5 

### 0.0100 mg/L 6010B 0.00616 J Copper 0.00500 mg/L 6010B 0.00245 J B Lead 0.0200 mg/L 6010B 0.00789 J Zinc

TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53342-1 Preparation Method Method Lab Location Description Matrix:Solid 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation, Metals TAL CHI SW846 3050B Metals (ICP) TAL CHI SW846 6010B TCLP Extraction TAL CHI SW846 1311 Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A TCLP Extraction TAL CHI SW846 1311 Preparation, Mercury TAL CHI SW846 7470A Mercury (CVAA) TAL CHI SW846 7471A Preparation, Mercury TAL CHI SW846 7471A Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010 Chromium, Hexavalent TAL CHI SW846 7196A Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 pH TAL CHI SW846 9045C HEM and SGT-HEM TAL CHI SW846 9071B Preparation, HEM and SGT-HEM TAL CHI SW846 9071B Percent Moisture TAL CHI EPA Moisture Total, Fixed,andVolatile Solids TAL CHI SM SM 2540G Matrix:Water 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A Preparation, Mercury TAL CHI SW846 7470A HEM and SGT-HEM TAL CHI 1664A1664A HEM and SGT-HEM (SPE) TAL CHI 1664A1664A Chromium, Hexavalent TAL CHI SW846 7196A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53342-1 Preparation Method Method Lab Location Description Lab References: TAL CHI=TestAmerica Chicago 

### Method References: 1664A=EPA-821-98-002 EPA=US Environmental ProtectionAgency SM = "Standard Methods For The Examination Of Water And Wastewater " SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago 

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## METHOD /ANALYST SUMMARY Client: Project Integration, Inc Job Number: 500-53342-1

Method Analyst Analyst ID Alikpala, Elaine EA SW846 8260B Werner, Brian D BDW SW846 8260B Smith,Todd D TDS SW846 6010B Bills, Brandon J BJB SW846 7470A Bills, Brandon J BJB SW846 7471A Wasowicz, Andrew P APW SW846 1010 Brogan,MaryT MTB 1664A1664A Deb, Khona KD SW846 7196A Wasowicz, Andrew P APW SW846 7196A Treadwell,ElianeA EAT SW846 9014 Boyd, Cheryl L CLB SW846 9034 Moore, Colleen L CLM SW846 9034 Moore, Colleen L CLM SW846 9045C Brogan,MaryT MTB SW846 9071B Veldhuizen, Chris M CMV EPA Moisture Veldhuizen, Chris M CMV SM SM 2540G

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: % Moisture: 73.1 500-53342-2 Solid Date Sampled: 12/17/2012 1440 Date Received: 12/18/2012 0940 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/20/2012 1352 12/20/2012 1352 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53342-02.D 5 g 5 mL 5030B CMS16
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173515 N/A Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 28.2 18.6 6.72 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 112 70 - 134 1,2-Dichloroethane-d4 (Surr) 100 75 - 122 Toluene-d8 (Surr) 83 70 - 122 4-Bromofluorobenzene (Surr) 111 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: % Moisture: 73.1 500-53342-2 Solid Date Sampled: 12/17/2012 1440 Date Received: 12/18/2012 0940 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/19/2012 1300 12/21/2012 2240 50 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53342-02.D 5 g 5 mL RunType: DL 5030B CMS22
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173708 500-173454 Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 3200 928 241 Acetone Surrogate %Rec Acceptance Limits Qualifier 94 75 - 125 1,2-Dichloroethane-d4 (Surr) 96 75 - 120 Toluene-d8 (Surr) 86 75 - 120 4-Bromofluorobenzene (Surr) 95 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC EB 5


### Client Matrix: 500-53342-3 Water Date Sampled: 12/17/2012 1430 Date Received: 12/18/2012 0940 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/24/2012 1425 12/24/2012 1425 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53342-03.D 5 mL 5 mL 5030B CMS22
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173827 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 94 75 - 125 1,2-Dichloroethane-d4 (Surr) 100 75 - 120 Toluene-d8 (Surr) 90 75 - 120 4-Bromofluorobenzene (Surr) 96 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: Trip Blank


### Client Matrix: 500-53342-4 Water Date Sampled: 12/17/2012 0000 Date Received: 12/18/2012 0940 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/24/2012 1359 12/24/2012 1359 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53342-04.D 5 mL 5 mL 5030B CMS22
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173827 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 95 75 - 125 1,2-Dichloroethane-d4 (Surr) 99 75 - 120 Toluene-d8 (Surr) 92 75 - 120 4-Bromofluorobenzene (Surr) 96 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: % Moisture: 70.0 500-53342-1 Solid Date Sampled: 12/17/2012 1450 Date Received: 12/18/2012 0940 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51219A Dilution: 1.0 InitialWeight /Volume: 1.1079 g 12/19/2012 1339 FinalWeight /Volume: 100 mL 12/18/2012 1600 3050B ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173517 500-173339 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 409 3.01 0.358 Barium 693 3.01 0.815 Copper 14200 3.01 0.502 Chromium 77.4 B 3.01 0.659 Nickel 250 B 1.50 0.517 Lead 238 1.50 0.228 Vanadium 441 6.02 2.06 Zinc
6010B Metals (ICP)-TCLP 

### 6010B Instrument ID: Lab File ID: P51219B Dilution: 1.0 InitialWeight /Volume: 50 mL 12/19/2012 2241 FinalWeight /Volume: 50 mL 12/19/2012 0820 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173518 500-173406 500-173323 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/18/2012 1400 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.500 0.500 0.0100 Barium <0.0250 0.0250 0.0100 Copper 0.166 0.0250 0.0100 Chromium 0.531 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead 0.00669 J 0.0250 0.00500 Vanadium 0.0502 J 0.100 0.0200 Zinc

7470A Mercury(CVAA)-TCLP 

### 7470A Instrument ID: Lab File ID: 122012R.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/20/2012 0942 FinalWeight /Volume: 25 mL 12/19/2012 1400 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173572 500-173428 500-173323 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/18/2012 1400 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000200 Mercury

7471A Mercury(CVAA)

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: % Moisture: 70.0 500-53342-1 Solid Date Sampled: 12/17/2012 1450 Date Received: 12/18/2012 0940 7471A Mercury(CVAA) 

### 7471A Instrument ID: Lab File ID: 122012B.PRN Dilution: 1.0 InitialWeight /Volume: 0.6182 g 12/20/2012 1021 FinalWeight /Volume: 50 mL 12/19/2012 1445 7471A HG5
Analysis Date: Prep Date: Analysis Batch: 500-173574 500-173393 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 0.321 0.0540 0.0206 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1 Client Sample ID: 

### Lab Sample ID: FC EB 5


### Client Matrix: 500-53342-3 Water Date Sampled: 12/17/2012 1430 Date Received: 12/18/2012 0940 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51219A Dilution: 1.0 InitialWeight /Volume: 50 mL 12/19/2012 1503 FinalWeight /Volume: 50 mL 12/18/2012 1530 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173517 500-173349 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL <0.0100 0.0100 0.000440 Barium 0.00616 J 0.0100 0.00106 Copper <0.0100 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel 0.00245 J B 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium 0.00789 J 0.0200 0.00472 Zinc

7470A Mercury(CVAA) 

### 7470A Instrument ID: Lab File ID: 122012R.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/20/2012 1029 FinalWeight /Volume: 25 mL 12/19/2012 1400 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173572 500-173428 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000710 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: 500-53342-1 Solid Date Sampled: 12/17/2012 1450 Date Received: 12/18/2012 0940 Analyte Result QualUnits MDL RL Dil Method Flashpoint >176 Degrees F 40.0 40.0 1.0 1010 DryWt Corrected: N Analysis Date (Start): 12/20/ 20121100(End) 12/20/2012 1200 

### Analysis Batch: 500-173625 Chromium, hexavalent <3.33 mg/Kg 1.30 3.33 1.0 7196A DryWt Corrected: Y Analysis Date (Start): 12/27/2012 1250 (End) 12/27/2012 1251 

### Analysis Batch: 500-174027 Prep Batch: 500-173790 Prep Date: 12/22/2012 1200 Cyanide,Total 0.905 J mg/Kg 0.524 1.59 1.0 9014 DryWt Corrected: Y Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1531 

### Analysis Batch: 500-174173 Prep Batch: 500-174096 Prep Date: 12/28/20121120 Sulfide 798 mg/Kg 13.2 82.8 1.0 9034 DryWt Corrected: Y Analysis Date: 12/19/2012 1338 Analysis Batch: 500-173474 Prep Batch: 500-173291 Prep Date: 12/19/20121125 Sulfide, Reactive <48.7 mg/Kg 3.80 48.7 1.0 9034 DryWt Corrected: N Analysis Date: 12/19/2012 1219 Analysis Batch: 500-173472 Prep Batch: 500-173290 Prep Date: 12/19/2012 1050 pH 9.59 SU 0.200 0.200 1.0 9045C DryWt Corrected: N Analysis Date (Start): 12/20/2012 1710 (End) 12/20/2012 1810 

### Analysis Batch: 500-173479 HEM (Oil & Grease) 13200 mg/Kg 732 1650 1.0 9071B DryWt Corrected: Y Analysis Date: 12/19/20121123 Analysis Batch: 500-173330 Prep Batch: 500-173324 Prep Date: 12/19/2012 0510 Percent Moisture 70 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/19/2012 0840 Analysis Batch: 500-173404 Percent Solids 30 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/19/2012 0840 Analysis Batch: 500-173404 % Moisture 70.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/18/2012 0957 Analysis Batch: 500-173229 Total Solids 30.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/19/2012 0731 Analysis Batch: 500-173385

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC Composite 5


### Client Matrix: 500-53342-2 Solid Date Sampled: 12/17/2012 1440 Date Received: 12/18/2012 0940 Analyte Result QualUnits MDL RL Dil Method Percent Moisture 73 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/21/2012 0720 Analysis Batch: 500-173667 Percent Solids 27 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/21/2012 0720 Analysis Batch: 500-173667

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53342-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC EB 5


### Client Matrix: 500-53342-3 Water Date Sampled: 12/17/2012 1430 Date Received: 12/18/2012 0940 Analyte Result QualUnits MDL RL Dil Method HEM (Oil & Grease) <5.36 mg/L 1.55 5.36 1.0 1664A Analysis Date: 12/21/2012 1035 Analysis Batch: 500-173459 Prep Batch: 500-173450 Prep Date: 12/21/2012 0709 Chromium, hexavalent <0.0100 mg/L 0.00325 0.0100 1.0 7196A Analysis Date (Start): 12/18/ 20121122(End) 12/18/20121122 

### Analysis Batch: 500-173293 Cyanide,Total <0.0100 mg/L 0.00331 0.0100 1.0 9014 Analysis Date (Start): 12/27/2012 1444 (End) 12/27/2012 1444 

### Analysis Batch: 500-174042 Prep Batch: 500-173980 Prep Date: 12/27/2012 0950 Sulfide <1.00 mg/L 0.230 1.00 1.0 9034 Analysis Date (Start): 12/24/2012 1358 (End) 12/24/2012 1400 

### Analysis Batch: 500-173846 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034 Analysis Date: 12/24/2012 1340 Analysis Batch: 500-173845 Prep Batch: 500-173844 Prep Date: 12/24/2012 0830

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## Quality Control Results Job Number: 500-53342-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53342-2 FC Composite 5 111 112 100 83 MB 500-173515/4 103 106 113 107 LCS 500-173515/5 103 98 111 102

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 70-134 TOL=Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

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## Quality Control Results Job Number: 500-53342-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53342-2 DL FC Composite 5 DL 95 94 96 86 MB 500-173708/6 88 90 97 88 LCS 500-173708/4 96 94 97 103

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## Quality Control Results Job Number: 500-53342-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix:Water 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53342-3 FC EB 5 96 94 100 90 500-53342-4 Trip Blank 96 95 99 92 MB 500-173827/6 92 90 96 88 LCS 500-173827/4 92 92 97 94

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173515

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 16M1220.D 5 g 5 mL Units: ug/Kg 

### Method: 8260B Preparation: 5030B
CMS16 MB 500-173515/4
Analysis Date: 12/20/2012 0900 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173515

Prep Date: Leach Date: 12/20/2012 0900 N/A Analyte RL MDL Qual Result <5.00 5.00 2.16 Acetone <5.00 5.00 1.81 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 106 70 - 134 Toluene-d8 (Surr) 113 75 - 122 4-Bromofluorobenzene (Surr) 107 70 - 122 Dibromofluoromethane 103 75 - 120

Solid 1.0 

### Lab Control Sample - Batch: 500-173515

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 16S1220.D 5 g 5 mL Units: ug/Kg 

### Method: 8260B Preparation: 5030B
CMS16 LCS 500-173515/5
Analysis Date: 12/20/2012 0923 Analysis Batch: Prep Batch: Leach Batch: 500-173515 N/A N/A Prep Date: Leach Date: 12/20/2012 0923 N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 43.68 87 50 - 138 Acetone 50.0 45.67 91 58 - 133 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 98 70 - 134 Toluene-d8 (Surr) 111 75 - 122 4-Bromofluorobenzene (Surr) 102 70 - 122 Dibromofluoromethane 103 75 - 120

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## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173708

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22M1221.D Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS22 MB 500-173708/6
Analysis Date: 12/21/2012 1316 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173708

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <5.00 5.00 1.30 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 90 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 88 75 - 120 Dibromofluoromethane 88 75 - 120

Solid 1.0 

### Lab Control Sample - Batch: 500-173708

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22S1221.D Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS22 LCS 500-173708/4
Analysis Date: 12/21/2012 1223 Analysis Batch: Prep Batch: Leach Batch: 500-173708 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 46.74 93 46 - 153 Acetone 50.0 41.90 84 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 94 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 103 75 - 120 Dibromofluoromethane 96 75 - 120

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## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173827

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22M1224.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS22 MB 500-173827/6
Analysis Date: 12/24/2012 1333 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173827

Prep Date: Leach Date: 12/24/2012 1333 N/A Analyte RL MDL Qual Result <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 90 75 - 125 Toluene-d8 (Surr) 96 75 - 120 4-Bromofluorobenzene (Surr) 88 75 - 120 Dibromofluoromethane 92 75 - 120

Water 1.0 

### Lab Control Sample - Batch: 500-173827

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22S1224.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS22 LCS 500-173827/4
Analysis Date: 12/24/2012 1235 Analysis Batch: Prep Batch: Leach Batch: 500-173827 N/A N/A Prep Date: Leach Date: 12/24/2012 1235 N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 48.03 96 46 - 153 Acetone 50.0 50.18 100 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 92 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 94 75 - 120 Dibromofluoromethane 92 75 - 120

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## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173339

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 MB 500-173339/1-A
Analysis Date: 12/19/2012 1033 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173517 500-173339
Prep Date: Leach Date: 12/18/2012 1600 N/A Analyte RL MDL Qual Result <1.00 1.00 0.119 Barium <1.00 1.00 0.271 Copper <1.00 1.00 0.167 Chromium 0.3300 J 1.00 0.219 Nickel 0.2580 J 0.500 0.172 Lead <0.500 0.500 0.0759 Vanadium <2.00 2.00 0.686 Zinc

Solid 1.0 

### Lab Control Sample - Batch: 500-173339

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 LCS 500-173339/2-A
Analysis Date: 12/19/2012 1039 Analysis Batch: Prep Batch: Leach Batch: 500-173517 500-173339 N/A Prep Date: Leach Date: 12/18/2012 1600 N/A Analyte Qual Limit % Rec. Result SpikeAmount 200 199.5 100 80 - 120 Barium 25.0 25.15 101 80 - 120 Copper 20.0 20.20 101 80 - 120 Chromium 50.0 49.95 100 80 - 120 Nickel 10.0 10.14 101 80 - 120 Lead 50.0 50.42 101 80 - 120 Vanadium 50.0 49.15 98 80 - 120 Zinc

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## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173349

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 MB 500-173349/1-A
Analysis Date: 12/19/2012 1352 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173517 500-173349
Prep Date: Leach Date: 12/18/2012 1530 N/A Analyte RL MDL Qual Result 0.002710 J 0.0100 0.000440 Barium <0.0100 0.0100 0.00106 Copper 0.001210 J 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel 0.002720 J 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium <0.0200 0.0200 0.00472 Zinc

Water 1.0 

### Lab Control Sample - Batch: 500-173349

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 LCS 500-173349/2-A
Analysis Date: 12/19/2012 1358 Analysis Batch: Prep Batch: Leach Batch: 500-173517 500-173349 N/A Prep Date: Leach Date: 12/18/2012 1530 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.955 98 80 - 120 Barium 0.250 0.2524 101 80 - 120 Copper 0.200 0.1989 99 80 - 120 Chromium 0.500 0.4934 99 80 - 120 Nickel 0.100 0.1010 101 80 - 120 Lead 0.500 0.4993 100 80 - 120 Vanadium 0.500 0.4858 97 80 - 120 Zinc

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## 01/04/2013 Page 31 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPW Leachate Blank- Batch: 500-173406

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A TCLP ICP5 LB2 500-173323/1-B
Analysis Date: 12/19/2012 2113 Analysis Batch: Prep Batch: Leach Batch: 500-173323 500-173518 500-173406
Prep Date: Leach Date: 12/19/2012 0820 12/18/2012 1400 Analyte RL MDL Qual Result <0.500 0.500 0.0100 Barium <0.0250 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium <0.0250 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

Water 1.0 

### Lab Control Sample - Batch: 500-173406

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 LCS 500-173406/3-A
Analysis Date: 12/19/2012 2120 Analysis Batch: Prep Batch: Leach Batch: 500-173518 500-173406 N/A Prep Date: Leach Date: 12/19/2012 0820 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.975 99 80 - 120 Barium 0.250 0.2464 99 80 - 120 Copper 0.200 0.1969 98 80 - 120 Chromium 0.500 0.4873 97 80 - 120 Nickel 0.100 0.09785 98 80 - 120 Lead 0.500 0.4959 99 80 - 120 Vanadium 0.500 0.4782 96 80 - 120 Zinc

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## 01/04/2013 Page 32 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173428

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122012R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 MB 500-173428/7-A
Analysis Date: 12/20/2012 0932 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173572 500-173428
Prep Date: Leach Date: 12/19/2012 1400 N/A Analyte RL MDL Qual Result <0.000200 0.000200 0.0000200 Mercury

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPW Leachate Blank- Batch: 500-173428

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122012R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A TCLP HG6 LB2 500-173323/1-C
Analysis Date: 12/20/2012 0940 Analysis Batch: Prep Batch: Leach Batch: 500-173323 500-173572 500-173428
Prep Date: Leach Date: 12/19/2012 1400 12/18/2012 1400 Analyte RL MDL Qual Result <0.000200 0.000200 0.0000200 Mercury

Water 1.0 

### Lab Control Sample - Batch: 500-173428

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122012R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 LCS 500-173428/8-A
Analysis Date: 12/20/2012 0938 Analysis Batch: Prep Batch: Leach Batch: 500-173572 500-173428 N/A Prep Date: Leach Date: 12/19/2012 1400 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.00200 0.002086 104 80 - 120 Mercury

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## 01/04/2013 Page 33 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173393

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122012A.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 MB 500-173393/7-A
Analysis Date: 12/20/2012 0916 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173573 500-173393
Prep Date: Leach Date: 12/19/2012 1445 N/A Analyte RL MDL Qual Result <0.0167 0.0167 0.00637 Mercury

Solid 1.0 

### Lab Control Sample - Batch: 500-173393

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122012A.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 LCS 500-173393/8-A
Analysis Date: 12/20/2012 0918 Analysis Batch: Prep Batch: Leach Batch: 500-173573 500-173393 N/A Prep Date: Leach Date: 12/19/2012 1445 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.167 0.1467 88 80 - 120 Mercury

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## 01/04/2013 Page 34 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173450

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment MB 500-173450/1-A
Analysis Date: 12/21/2012 0955 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173459 500-173450
Prep Date: Leach Date: 12/21/2012 0505 N/A Analyte RL MDL Qual Result <5.00 5.00 1.45 HEM (Oil & Grease)

Water 1.0 

### Lab Control Sample - Batch: 500-173450

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment LCS 500-173450/2-A
Analysis Date: 12/21/2012 0958 Analysis Batch: Prep Batch: Leach Batch: 500-173459 500-173450 N/A Prep Date: Leach Date: 12/21/2012 0516 N/A Analyte Qual Limit % Rec. Result SpikeAmount 40.0 36.70 92 78 -114 HEM (Oil & Grease)

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## 01/04/2013 Page 35 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173293

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 MB 500-173293/3
Analysis Date: 12/18/20121121 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173293

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00325 Chromium, hexavalent

Water 1.0 

### Lab Control Sample - Batch: 500-173293

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 LCS 500-173293/4
Analysis Date: 12/18/20121121 Analysis Batch: Prep Batch: Leach Batch: 500-173293 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.250 0.2652 106 85 -115 Chromium, hexavalent

Dilution: Dilution: Water 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Water 

### Method: 7196A Preparation: N/A

N/A

N/A SPEC5

SPEC5 500-53342-3

500-53342-3 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173293

12/18/20121122 N/A N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173293 N/A N/A

Analysis Date: Prep Date: Leach Date: 12/18/20121123 N/A N/A Analysis Batch: Prep Batch: Leach Batch: 500-173293 N/A N/A

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 100 102 85 -115 2 20 Chromium, hexavalent

TestAmerica Chicago 

## 01/04/2013 Page 36 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water 12/18/20121122 12/18/20121123 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Water 

### Method: 7196A Preparation: N/A

Units:mg/L 500-53342-3 500-53342-3 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173293

Analysis Date: Prep Date: Leach Date: N/A N/A Analysis Date: Prep Date: Leach Date: N/A N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
<0.0100 0.250 0.250 0.2502 0.2555 Chromium, hexavalent

TestAmerica Chicago 

## 01/04/2013 Page 37 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173790

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 MB 500-173790/1-A
Analysis Date: 12/27/2012 1241 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174027 500-173790
Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte RL MDL Qual Result <1.00 1.00 0.389 Chromium, hexavalent

Solid 1.0 

### Lab Control Sample - Batch: 500-173790

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173790/2-A
Analysis Date: 12/27/2012 1242 Analysis Batch: Prep Batch: Leach Batch: 500-174027 500-173790 N/A Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte Qual Limit % Rec. Result SpikeAmount 10.0 9.188 92 80 - 120 Chromium, hexavalent

Solid 50 

### Lab Control Sample - Batch: 500-173790

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173790/3-A
Analysis Date: 12/27/2012 1242 Analysis Batch: Prep Batch: Leach Batch: 500-174027 500-173790 N/A Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte Qual Limit % Rec. Result SpikeAmount 676 669.0 99 80 - 120 Chromium, hexavalent

TestAmerica Chicago 

## 01/04/2013 Page 38 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173980

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-173980/1-A
Analysis Date: 12/27/2012 1440 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174042 500-173980
Prep Date: Leach Date: 12/27/2012 0950 N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00331 Cyanide,Total

Water 1.0 

### Lab Control Sample - Batch: 500-173980

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-173980/2-A
Analysis Date: 12/27/2012 1440 Analysis Batch: Prep Batch: Leach Batch: 500-174042 500-173980 N/A Prep Date: Leach Date: 12/27/2012 0950 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.100 0.1066 107 80 - 120 Cyanide,Total

TestAmerica Chicago 

## 01/04/2013 Page 39 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174096

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-174096/12-A
Analysis Date: 12/28/2012 1530 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174173 500-174096
Prep Date: Leach Date: 12/28/20121120 N/A Analyte RL MDL Qual Result <0.500 0.500 0.165 Cyanide,Total

Solid 1.0 

### Lab Control Sample - Batch: 500-174096

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-174096/13-A
Analysis Date: 12/28/2012 1530 Analysis Batch: Prep Batch: Leach Batch: 500-174173 500-174096 N/A Prep Date: Leach Date: 12/28/20121120 N/A Analyte Qual Limit % Rec. Result SpikeAmount 5.00 5.325 107 80 - 120 Cyanide,Total

TestAmerica Chicago 

## 01/04/2013 Page 40 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173290

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-173290/1-A
Analysis Date: 12/19/2012 1215 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173472 500-173290
Prep Date: Leach Date: 12/19/2012 1005 N/A Analyte RL MDL Qual Result <50.0 50.0 3.90 Sulfide, Reactive

Solid 1.0 

### Lab Control Sample - Batch: 500-173290

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-173290/2-A
Analysis Date: 12/19/2012 1215 Analysis Batch: Prep Batch: Leach Batch: 500-173472 500-173290 N/A Prep Date: Leach Date: 12/19/2012 1010 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 168.6 94 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/04/2013 Page 41 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173291

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment MB 500-173291/1-A
Analysis Date: 12/19/2012 1335 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173474 500-173291
Prep Date: Leach Date: 12/19/20121125 N/A Analyte RL MDL Qual Result <25.0 25.0 4.00 Sulfide

Solid 1.0 

### Lab Control Sample - Batch: 500-173291

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment LCS 500-173291/2-A
Analysis Date: 12/19/2012 1335 Analysis Batch: Prep Batch: Leach Batch: 500-173474 500-173291 N/A Prep Date: Leach Date: 12/19/20121125 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 168.3 93 80 - 120 Sulfide

TestAmerica Chicago 

## 01/04/2013 Page 42 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173844

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-173844/1-A
Analysis Date: 12/24/2012 1319 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173845 500-173844
Prep Date: Leach Date: 12/24/2012 0800 N/A Analyte RL MDL Qual Result <1.00 1.00 1.00 Sulfide, Reactive

Water 1.0 

### Lab Control Sample - Batch: 500-173844

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-173844/2-A
Analysis Date: 12/24/2012 1329 Analysis Batch: Prep Batch: Leach Batch: 500-173845 500-173844 N/A Prep Date: Leach Date: 12/24/2012 0815 N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.767 105 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/04/2013 Page 43 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173846

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment MB 500-173846/1
Analysis Date: 12/24/2012 1319 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173846

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <1.00 1.00 0.230 Sulfide

Water 1.0 

### Lab Control Sample - Batch: 500-173846

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment LCS 500-173846/2
Analysis Date: 12/24/2012 1320 Analysis Batch: Prep Batch: Leach Batch: 500-173846 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.760 104 80 - 120 Sulfide

TestAmerica Chicago 

## 01/04/2013 Page 44 of 332

## Quality Control Results
Job Number: 500-53342-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173324

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment MB 500-173324/1-A
Analysis Date: 12/19/2012 0920 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173330 500-173324
Prep Date: Leach Date: 12/19/2012 0510 N/A Analyte RL MDL Qual Result <500 500 222 HEM (Oil & Grease)

Solid 1.0 

### Lab Control Sample - Batch: 500-173324

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment LCS 500-173324/2-A
Analysis Date: 12/19/2012 0931 Analysis Batch: Prep Batch: Leach Batch: 500-173330 500-173324 N/A Prep Date: Leach Date: 12/19/2012 0510 N/A Analyte Qual Limit % Rec. Result SpikeAmount 4000 4090 102 80 - 120 HEM (Oil & Grease)

TestAmerica Chicago 

## 01/04/2013 Page 45 of 332

## DATA REPORTING QUALIFIERS Client: Project Integration, Inc Job Number: 500-53342-1

Lab Section Qualifier Description 

### Metals Compound was found in the blank and sample. B ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA,DLCK or MRL standard: Instrument related QC exceeds the control limits. ^
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J
General Chemistry Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J

TestAmerica Chicago 

## 01/04/2013 Page 46 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS VOA Prep Batch: 500-173454 

### Solid FC Composite 5 5030B 500-53342-2DL T Analysis Batch:500-173515 

### Lab Control Sample Solid 8260B LCS 500-173515/5 T Method Blank Solid 8260B MB 500-173515/4 T Solid FC Composite 5 8260B 500-53342-2 T Analysis Batch:500-173708 

### Lab Control Sample Solid 8260B LCS 500-173708/4 T Method Blank Solid 8260B MB 500-173708/6 T Solid 500-173454 FC Composite 5 8260B 500-53342-2DL T Analysis Batch:500-173827 

### Lab Control Sample Water 8260B LCS 500-173827/4 T Method Blank Water 8260B MB 500-173827/6 T Water FC EB 5 8260B 500-53342-3 T Water Trip Blank 8260B 500-53342-4 T
Report Basis T=Total



### TestAmerica Chicago 

## 01/04/2013 Page 47 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 500-173323 

### TCLP SPLPW Leachate Blank Solid 1311 LB2 500-173323/1-B P TCLP SPLPW Leachate Blank Solid 1311 LB2 500-173323/1-C P Solid FC Composite 5 1311 500-53342-1 P Prep Batch: 500-173339 

### Lab Control Sample Solid 3050B LCS 500-173339/2-A T Method Blank Solid 3050B MB 500-173339/1-A T Solid FC Composite 5 3050B 500-53342-1 T Prep Batch: 500-173349 

### Lab Control Sample Water 3010A LCS 500-173349/2-A T Method Blank Water 3010A MB 500-173349/1-A T Water FC EB 5 3010A 500-53342-3 T Prep Batch: 500-173393 

### Lab Control Sample Solid 7471A LCS 500-173393/8-A T Method Blank Solid 7471A MB 500-173393/7-A T Solid FC Composite 5 7471A 500-53342-1 T Prep Batch: 500-173406 

### Lab Control Sample Water 3010A LCS 500-173406/3-A T TCLP SPLPW Leachate Blank Solid 500-173323 3010A LB2 500-173323/1-B P Solid 500-173323 FC Composite 5 3010A 500-53342-1 P Prep Batch: 500-173428 

### Lab Control Sample Water 7470A LCS 500-173428/8-A T Method Blank Water 7470A MB 500-173428/7-A T TCLP SPLPW Leachate Blank Solid 500-173323 7470A LB2 500-173323/1-C P Solid 500-173323 FC Composite 5 7470A 500-53342-1 P Water FC EB 5 7470A 500-53342-3 T Analysis Batch:500-173517 

### Lab Control Sample Solid 500-173339 6010B LCS 500-173339/2-A T Method Blank Solid 500-173339 6010B MB 500-173339/1-A T Lab Control Sample Water 500-173349 6010B LCS 500-173349/2-A T Method Blank Water 500-173349 6010B MB 500-173349/1-A T Solid 500-173339 FC Composite 5 6010B 500-53342-1 T Water 500-173349 FC EB 5 6010B 500-53342-3 T Analysis Batch:500-173518 

### TCLP SPLPW Leachate Blank Solid 500-173406 6010B LB2 500-173323/1-B P Lab Control Sample Water 500-173406 6010B LCS 500-173406/3-A T Solid 500-173406 FC Composite 5 6010B 500-53342-1 P

TestAmerica Chicago 

## 01/04/2013 Page 48 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Analysis Batch:500-173572 

### TCLP SPLPW Leachate Blank Solid 500-173428 7470A LB2 500-173323/1-C P Lab Control Sample Water 500-173428 7470A LCS 500-173428/8-A T Method Blank Water 500-173428 7470A MB 500-173428/7-A T Solid 500-173428 FC Composite 5 7470A 500-53342-1 P Water 500-173428 FC EB 5 7470A 500-53342-3 T Analysis Batch:500-173573 

### Lab Control Sample Solid 500-173393 7471A LCS 500-173393/8-A T Method Blank Solid 500-173393 7471A MB 500-173393/7-A T Analysis Batch:500-173574 

### Solid 500-173393 FC Composite 5 7471A 500-53342-1 T
Report Basis P= TCLP T=Total



### TestAmerica Chicago 

## 01/04/2013 Page 49 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-173229 

### Solid FC Composite 5 SM 2540G 500-53342-1 T Prep Batch: 500-173290 

### Lab Control Sample Solid 7.3.4 LCS 500-173290/2-A T Method Blank Solid 7.3.4 MB 500-173290/1-A T Solid FC Composite 5 7.3.4 500-53342-1 T Prep Batch: 500-173291 

### Lab Control Sample Solid 9030B LCS 500-173291/2-A T Method Blank Solid 9030B MB 500-173291/1-A T Solid FC Composite 5 9030B 500-53342-1 T Analysis Batch:500-173293 

### Lab Control Sample Water 7196A LCS 500-173293/4 T Method Blank Water 7196A MB 500-173293/3 T Water FC EB 5 7196A 500-53342-3 T Matrix Spike Water 7196A 500-53342-3MS T Matrix Spike Duplicate Water 7196A 500-53342-3MSD T Prep Batch: 500-173324 

### Lab Control Sample Solid 9071B LCS 500-173324/2-A T Method Blank Solid 9071B MB 500-173324/1-A T Solid FC Composite 5 9071B 500-53342-1 T Analysis Batch:500-173330 

### Lab Control Sample Solid 500-173324 9071B LCS 500-173324/2-A T Method Blank Solid 500-173324 9071B MB 500-173324/1-A T Solid 500-173324 FC Composite 5 9071B 500-53342-1 T Analysis Batch:500-173385 

### Solid FC Composite 5 SM 2540G 500-53342-1 T Analysis Batch:500-173404 

### Solid FC Composite 5 Moisture 500-53342-1 T Prep Batch: 500-173450 

### Lab Control Sample Water 1664A LCS 500-173450/2-A T Method Blank Water 1664A MB 500-173450/1-A T Water FC EB 5 1664A 500-53342-3 T Analysis Batch:500-173459 

### Lab Control Sample Water 500-173450 1664A LCS 500-173450/2-A T Method Blank Water 500-173450 1664A MB 500-173450/1-A T Water 500-173450 FC EB 5 1664A 500-53342-3 T

TestAmerica Chicago 

## 01/04/2013 Page 50 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-173472 

### Lab Control Sample Solid 500-173290 9034 LCS 500-173290/2-A T Method Blank Solid 500-173290 9034 MB 500-173290/1-A T Solid 500-173290 FC Composite 5 9034 500-53342-1 T Analysis Batch:500-173474 

### Lab Control Sample Solid 500-173291 9034 LCS 500-173291/2-A T Method Blank Solid 500-173291 9034 MB 500-173291/1-A T Solid 500-173291 FC Composite 5 9034 500-53342-1 T Analysis Batch:500-173479 

### Solid FC Composite 5 9045C 500-53342-1 T Analysis Batch:500-173625 

### Solid FC Composite 5 1010 500-53342-1 T Analysis Batch:500-173667 

### Solid FC Composite 5 Moisture 500-53342-2 T Prep Batch: 500-173790 

### Lab Control Sample Solid 3060A LCS 500-173790/2-A T Lab Control Sample Solid 3060A LCS 500-173790/3-A T Method Blank Solid 3060A MB 500-173790/1-A T Solid FC Composite 5 3060A 500-53342-1 T Prep Batch: 500-173844 

### Lab Control Sample Water 7.3.4 LCS 500-173844/2-A T Method Blank Water 7.3.4 MB 500-173844/1-A T Water FC EB 5 7.3.4 500-53342-3 T Analysis Batch:500-173845 

### Lab Control Sample Water 500-173844 9034 LCS 500-173844/2-A T Method Blank Water 500-173844 9034 MB 500-173844/1-A T Water 500-173844 FC EB 5 9034 500-53342-3 T Analysis Batch:500-173846 

### Lab Control Sample Water 9034 LCS 500-173846/2 T Method Blank Water 9034 MB 500-173846/1 T Water FC EB 5 9034 500-53342-3 T Prep Batch: 500-173980 

### Lab Control Sample Water 9010B LCS 500-173980/2-A T Method Blank Water 9010B MB 500-173980/1-A T Water FC EB 5 9010B 500-53342-3 T

TestAmerica Chicago 

## 01/04/2013 Page 51 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-174027 

### Lab Control Sample Solid 500-173790 7196A LCS 500-173790/2-A T Lab Control Sample Solid 500-173790 7196A LCS 500-173790/3-A T Method Blank Solid 500-173790 7196A MB 500-173790/1-A T Solid 500-173790 FC Composite 5 7196A 500-53342-1 T Analysis Batch:500-174042 

### Lab Control Sample Water 500-173980 9014 LCS 500-173980/2-A T Method Blank Water 500-173980 9014 MB 500-173980/1-A T Water 500-173980 FC EB 5 9014 500-53342-3 T Prep Batch: 500-174096 

### Lab Control Sample Solid 9010B LCS 500-174096/13-A T Method Blank Solid 9010B MB 500-174096/12-A T Solid FC Composite 5 9010B 500-53342-1 T Analysis Batch:500-174173 

### Lab Control Sample Solid 500-174096 9014 LCS 500-174096/13-A T Method Blank Solid 500-174096 9014 MB 500-174096/12-A T Solid 500-174096 FC Composite 5 9014 500-53342-1 T
Report Basis T=Total



### TestAmerica Chicago 

## 01/04/2013 Page 52 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1 

## Laboratory Chronicle

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 14:50 500-53342-1 FC Composite 5



### P:3050B 500-53342-A-1-E 500-173517 500-173339 12/18/2012 16:00 RL TAL CHI 1 A:6010B 500-53342-A-1-E 500-173517 500-173339 12/19/2012 13:39 TDS TAL CHI 1 P:3010A 500-53342-A-1-F 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B 500-53342-A-1-F 500-173518 500-173406 12/19/2012 22:41 TDS TAL CHI 1 P:7470A 500-53342-A-1-H 500-173572 500-173428 12/19/2012 14:00 BJB TAL CHI 1 A:7470A 500-53342-A-1-H 500-173572 500-173428 12/20/2012 09:42 BJB TAL CHI 1 P:7471A 500-53342-A-1-G 500-173574 500-173393 12/19/2012 14:45 BJB TAL CHI 1 A:7471A 500-53342-A-1-G 500-173574 500-173393 12/20/2012 10:21 BJB TAL CHI 1 A:1010 500-53342-A-1 500-173625 12/20/201211:00 APW TAL CHI 1 P:3060A 500-53342-A-1-I 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A 500-53342-A-1-I 500-174027 500-173790 12/27/2012 12:50 APW TAL CHI 1 P:9010B 500-53342-A-1-J 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 500-53342-A-1-J 500-174173 500-174096 12/28/2012 15:31 EAT TAL CHI 1 P:7.3.4 500-53342-A-1-A 500-173472 500-173290 12/19/2012 10:50 CLM TAL CHI 1 A:9034 500-53342-A-1-A 500-173472 500-173290 12/19/2012 12:19 CLM TAL CHI 1 P:9030B 500-53342-A-1-B 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 500-53342-A-1-B 500-173474 500-173291 12/19/2012 13:38 CLM TAL CHI 1 A:9045C 500-53342-A-1 500-173479 12/20/2012 17:10 CLM TAL CHI 1 P:9071B 500-53342-A-1-D 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B 500-53342-A-1-D 500-173330 500-173324 12/19/201211:23 MTB TAL CHI 1 A:Moisture 500-53342-A-1 500-173404 12/19/2012 08:40 CMV TAL CHI 1 A:SM 2540G 500-53342-A-1 500-173229 12/18/2012 09:57 CMV TAL CHI 1 A:SM 2540G 500-53342-A-1 500-173385 12/19/2012 07:31 CMV TAL CHI 1

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 14:40 500-53342-2 FC Composite 5



### P:5030B 500-53342-A-2 500-173515 12/20/2012 13:52 BDW TAL CHI 1 A:8260B 500-53342-A-2 500-173515 12/20/2012 13:52 BDW TAL CHI 1 P:5030B 500-53342-A-2-A 500-173708 500-173454 12/19/2012 13:00 WRE TAL CHI DL 50 A:8260B 500-53342-A-2-A 500-173708 500-173454 12/21/2012 22:40 EA TAL CHI DL 50 A:Moisture 500-53342-A-2 500-173667 12/21/2012 07:20 CMV TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/04/2013 Page 53 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1 

## Laboratory Chronicle

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 14:30 500-53342-3 FC EB 5



### P:5030B 500-53342-A-3 500-173827 12/24/2012 14:25 EA TAL CHI 1 A:8260B 500-53342-A-3 500-173827 12/24/2012 14:25 EA TAL CHI 1 P:3010A 500-53342-E-3-A 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B 500-53342-E-3-A 500-173517 500-173349 12/19/2012 15:03 TDS TAL CHI 1 P:7470A 500-53342-E-3-B 500-173572 500-173428 12/19/2012 14:00 BJB TAL CHI 1 A:7470A 500-53342-E-3-B 500-173572 500-173428 12/20/2012 10:29 BJB TAL CHI 1 P:1664A 500-53342-H-3-A 500-173459 500-173450 12/21/2012 07:09 MTB TAL CHI 1 A:1664A 500-53342-H-3-A 500-173459 500-173450 12/21/2012 10:35 MTB TAL CHI 1 A:7196A 500-53342-F-3 500-173293 12/18/201211:22 KD TAL CHI 1 P:9010B 500-53342-D-3-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 500-53342-D-3-A 500-174042 500-173980 12/27/2012 14:44 EAT TAL CHI 1 P:7.3.4 500-53342-G-3-A 500-173845 500-173844 12/24/2012 08:30 CLB TAL CHI 1 A:9034 500-53342-G-3-A 500-173845 500-173844 12/24/2012 13:40 CLB TAL CHI 1 A:9034 500-53342-G-3 500-173846 12/24/2012 13:58 CLB TAL CHI 1

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 14:30 500-53342-3 MS FC EB 5



### A:7196A 500-53342-F-3 MS 500-173293 12/18/201211:22 KD TAL CHI 1

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 14:30 500-53342-3 MSD FC EB 5



### A:7196A 500-53342-F-3 MSD 500-173293 12/18/201211:23 KD TAL CHI 1

12/18/2012 09:40 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/17/2012 00:00 500-53342-4 Trip Blank



### P:5030B 500-53342-A-4 500-173827 12/24/2012 13:59 EA TAL CHI 1 A:8260B 500-53342-A-4 500-173827 12/24/2012 13:59 EA TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/04/2013 Page 54 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A MB N/A



### P:5030B MB 500-173515/4 500-173515 12/20/2012 09:00 BDW TAL CHI 1 A:8260B MB 500-173515/4 500-173515 12/20/2012 09:00 BDW TAL CHI 1 A:8260B MB 500-173708/6 500-173708 12/21/2012 13:16 EA TAL CHI 1 P:5030B MB 500-173827/6 500-173827 12/24/2012 13:33 EA TAL CHI 1 A:8260B MB 500-173827/6 500-173827 12/24/2012 13:33 EA TAL CHI 1 P:3050B MB 500-173339/1-A 500-173517 500-173339 12/18/2012 16:00 RL TAL CHI 1 A:6010B MB 500-173339/1-A 500-173517 500-173339 12/19/2012 10:33 TDS TAL CHI 1 P:3010A MB 500-173349/1-A 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B MB 500-173349/1-A 500-173517 500-173349 12/19/2012 13:52 TDS TAL CHI 1 P:7470A MB 500-173428/7-A 500-173572 500-173428 12/19/2012 14:00 BJB TAL CHI 1 A:7470A MB 500-173428/7-A 500-173572 500-173428 12/20/2012 09:32 BJB TAL CHI 1 P:7471A MB 500-173393/7-A 500-173573 500-173393 12/19/2012 14:45 BJB TAL CHI 1 A:7471A MB 500-173393/7-A 500-173573 500-173393 12/20/2012 09:16 BJB TAL CHI 1 P:1664A MB 500-173450/1-A 500-173459 500-173450 12/21/2012 05:05 MTB TAL CHI 1 A:1664A MB 500-173450/1-A 500-173459 500-173450 12/21/2012 09:55 MTB TAL CHI 1 A:7196A MB 500-173293/3 500-173293 12/18/201211:21 KD TAL CHI 1 P:3060A MB 500-173790/1-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A MB 500-173790/1-A 500-174027 500-173790 12/27/2012 12:41 APW TAL CHI 1 P:9010B MB 500-173980/1-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 MB 500-173980/1-A 500-174042 500-173980 12/27/2012 14:40 EAT TAL CHI 1 P:9010B MB 500-174096/12-A 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 MB 500-174096/12-A 500-174173 500-174096 12/28/2012 15:30 EAT TAL CHI 1 P:7.3.4 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 10:05 CLM TAL CHI 1 A:9034 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 12:15 CLM TAL CHI 1 P:9030B MB 500-173291/1-A 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 MB 500-173291/1-A 500-173474 500-173291 12/19/2012 13:35 CLM TAL CHI 1 P:7.3.4 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 08:00 CLB TAL CHI 1 A:9034 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 13:19 CLB TAL CHI 1 A:9034 MB 500-173846/1 500-173846 12/24/2012 13:19 CLB TAL CHI 1 P:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 09:20 MTB TAL CHI 1
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LB2 N/A



### P:3010A LB2 500-173323/1-B 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B LB2 500-173323/1-B 500-173518 500-173406 12/19/2012 21:13 TDS TAL CHI 1 P:7470A LB2 500-173323/1-C 500-173572 500-173428 12/19/2012 14:00 BJB TAL CHI 1 A:7470A LB2 500-173323/1-C 500-173572 500-173428 12/20/2012 09:40 BJB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/04/2013 Page 55 of 332

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53342-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LCS N/A



### P:5030B LCS 500-173515/5 500-173515 12/20/2012 09:23 BDW TAL CHI 1 A:8260B LCS 500-173515/5 500-173515 12/20/2012 09:23 BDW TAL CHI 1 A:8260B LCS 500-173708/4 500-173708 12/21/2012 12:23 EA TAL CHI 1 P:5030B LCS 500-173827/4 500-173827 12/24/2012 12:35 EA TAL CHI 1 A:8260B LCS 500-173827/4 500-173827 12/24/2012 12:35 EA TAL CHI 1 P:3050B LCS 500-173339/2-A 500-173517 500-173339 12/18/2012 16:00 RL TAL CHI 1 A:6010B LCS 500-173339/2-A 500-173517 500-173339 12/19/2012 10:39 TDS TAL CHI 1 P:3010A LCS 500-173349/2-A 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B LCS 500-173349/2-A 500-173517 500-173349 12/19/2012 13:58 TDS TAL CHI 1 P:3010A LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 21:20 TDS TAL CHI 1 P:7470A LCS 500-173428/8-A 500-173572 500-173428 12/19/2012 14:00 BJB TAL CHI 1 A:7470A LCS 500-173428/8-A 500-173572 500-173428 12/20/2012 09:38 BJB TAL CHI 1 P:7471A LCS 500-173393/8-A 500-173573 500-173393 12/19/2012 14:45 BJB TAL CHI 1 A:7471A LCS 500-173393/8-A 500-173573 500-173393 12/20/2012 09:18 BJB TAL CHI 1 P:1664A LCS 500-173450/2-A 500-173459 500-173450 12/21/2012 05:16 MTB TAL CHI 1 A:1664A LCS 500-173450/2-A 500-173459 500-173450 12/21/2012 09:58 MTB TAL CHI 1 A:7196A LCS 500-173293/4 500-173293 12/18/201211:21 KD TAL CHI 1 P:3060A LCS 500-173790/2-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A LCS 500-173790/2-A 500-174027 500-173790 12/27/2012 12:42 APW TAL CHI 1 P:3060A LCS 500-173790/3-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 50 A:7196A LCS 500-173790/3-A 500-174027 500-173790 12/27/2012 12:42 APW TAL CHI 50 P:9010B LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 14:40 EAT TAL CHI 1 P:9010B LCS 500-174096/13-A 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 15:30 EAT TAL CHI 1 P:7.3.4 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 10:10 CLM TAL CHI 1 A:9034 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 12:15 CLM TAL CHI 1 P:9030B LCS 500-173291/2-A 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 13:35 CLM TAL CHI 1 A:9034 LCS 500-173846/2 500-173846 12/24/2012 13:20 CLB TAL CHI 1 P:7.3.4 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 08:15 CLB TAL CHI 1 A:9034 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 13:29 CLB TAL CHI 1 P:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 09:31 MTB TAL CHI 1 

### Lab References: TAL CHI=TestAmerica Chicago

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/04/2013 Page 56 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 04/26/13 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L Mallin / JTBaker, Lot E50600 / K19H00 1664 HEM_00060 SGT-HEM 4000 mg/L 8260 IS SK_00026 1,4-Dichlorobenzene-d4 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 8260 IS WK_00381 1, Lot NA 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00026 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 IS SK_00027 1,4-Dichlorobenzene-d4 50 ug/mL 20 mL 4000 uL 12/14/1211/30/12 8260 LOW IS_00104 MEOH, Lot DA946 1,4-Difluorobenzene 50 ug/mL Chlorobenzene-d5 50 ug/mL Pentafluorobenzene 50 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00027 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/14/1211/30/12 8260 LOW SS_00106 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/27/1212/13/12 8260 LOW SS_00107 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 8260 SS WK_00378 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 

## 01/04/2013 Page 57 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL 

## 01/04/2013 Page 58 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL 

## 01/04/2013 Page 59 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 8260 STD WK_00216 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL 

## 01/04/2013 Page 60 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 

## 01/04/2013 Page 61 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 .ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACRNITSTDSK_00034 Acetonitrile 800 ug/mL 2 mL 2 mL 12/18/1212/11/12 ACR/NITRSTDWK_00212 METHANOL, Lot NA Acrolein 4000 ug/mL 

## 01/04/2013 Page 62 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 02/28/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091858 .ACRNITSTDSK_00034 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/26/1211/19/12 GAS STD WK RE_00244 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/18/1212/11/12 GAS STD WK RE_00254 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 8260 SS WK_00385 1,2-Dichloroethane-d4 (Surr) 43.28 ug/L 5 mL 0.8656 uL 01/01/1312/18/12 INST16 IS/SS_00223 1, Lot NA 4-Bromofluorobenzene (Surr) 43.28 ug/L Dibromofluoromethane 43.28 ug/L Toluene-d8 (Surr) 43.28 ug/L 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 01/01/1312/18/12 .8260 SS WK_00385 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 

## 01/04/2013 Page 63 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 KET/CS2 STDWK_00184 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00014 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL level1std5ppm_00006 Benzene 0.5 ug/mL 1 mL 100 uL 12/31/1603/20/12 level 1_00011 1, Lot CY647 Ethylbenzene 0.5 ug/mL m-Xylene & p-Xylene 1 ug/mL o-Xylene 0.5 ug/mL Toluene 0.5 ug/mL Trichloroethene 0.5 ug/mL Vinyl chloride 0.5 ug/mL level18260wk_00006 Benzene 5 ug/mL 2 mL 100 uL 02/28/1203/22/11 .level1std5ppm_00006 1, Lot CY647 Ethylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL o-Xylene 5 ug/mL Toluene 5 ug/mL Trichloroethene 5 ug/mL level1gaswk_00006 100 uLVinyl chloride 5 ug/mL level18260sk_00001 Benzene 100 ug/mL 1 mL 1 mL 06/30/1203/22/11 ..level18260wk_00006 1, Lot NA Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL Trichloroethene 100 ug/mL 06/30/12 (Purchased Reagent) Benzene 100 ug/mL Restek, Lot AO67921 ...level18260sk_00001 Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL Trichloroethene 100 ug/mL 02/28/1203/22/11 2 mLlevel1gaspt_00005 100 uLVinyl chloride 100 ug/mL ..level1gaswk_00006 1, Lot CY647 02/28/1203/22/11 1 mLlevel1gassk_00001 1 mLVinyl chloride 2000 ug/mL ...level1gaspt_00005 MEOH, Lot NA 02/28/12 (Purchased Reagent) Vinyl chloride 2000 ug/mL SUPELCO, Lot LB65254 ....level1gassk_00001 

## 01/04/2013 Page 64 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 8260 SS WK_00378 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 1 mL 200 uL 12/03/1211/19/12 LOW8260SS WK_00042 1, Lot DA057 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 .8260 SS WK_00378 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD WK_00212 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 11/26/1211/19/12 LOW8260STD WK_00209 1, Lot DG596 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL 

## 01/04/2013 Page 65 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00244 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00180 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00175 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 

## 01/04/2013 Page 66 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 

## 01/04/2013 Page 67 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL 

## 01/04/2013 Page 68 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/26/1211/19/12 .GAS STD WK RE_00244 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 .VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 8260 STD WK_00216 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 12/18/1212/11/12 LOW8260STD WK_00215 1, Lot DG860 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 

## 01/04/2013 Page 69 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00254 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL 

## 01/04/2013 Page 70 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Dichlorodifluoromethane 5 ug/mL Dichlorofluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00184 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00179 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 .8260 STD WK_00216 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL 

## 01/04/2013 Page 71 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL 

## 01/04/2013 Page 72 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/18/1212/11/12 .GAS STD WK RE_00254 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 .KET/CS2 STDWK_00184 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL 

## 01/04/2013 Page 73 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00014 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/25/1212/11/12 .VA/2CEVESTDWK_00179 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 ACR/NITRSTDWK_00205 Acetonitrile 80 ug/mL 1 mL 100 uL 11/26/1211/19/12 LOWACRSTD WK_00189 MEOH, Lot DG596 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 .ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 ..ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACR/NITRSTDWK_00212 Acetonitrile 80 ug/mL 1 mL 100 uL 12/18/1212/11/12 LOWACRSTD WK_00193 MEOH, Lot DG860 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00034 Acetonitrile 800 ug/mL 2 mL 2 mL 12/18/1212/11/12 .ACR/NITRSTDWK_00212 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 02/28/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091858 ..ACRNITSTDSK_00034 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 05/31/17 (Purchased Reagent) Mercury 1000 ug/mL ULTRA, Lot L00365 M11FSTKHG_00001 01/01/13 (Purchased Reagent) Mercury 1000 ug/mL Inorganic Ventures, Lot E2-HG02091 M12ASTKHG_00001 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1310/04/12 M12JSPKIC_00002 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mLTl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL K 1000 ug/mL 

## 01/04/2013 Page 74 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL Mn 500 ug/mL 

## 01/04/2013 Page 75 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1311/20/12 M12KSPKIC_00001 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mLTl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL K 1000 ug/mL Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 

## 01/04/2013 Page 76 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL Mn 500 ug/mL Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12GSTKIC_00002 Barium 0.5 ug/mL 1000 mL 10 mL 07/10/1312/10/12 M12LCCVIC_00001 1, Lot N/A Chromium 0.5 ug/mL Copper 0.5 ug/mL Lead 0.5 ug/mL Nickel 0.5 ug/mL Vanadium 5 ug/mL Zinc 0.5 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL 

## 01/04/2013 Page 77 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Zinc 50 ug/mL M12ESTKIC_00002 Barium 20 ug/L 1000 mL 2 mL 06/01/1312/03/12 M12LCRIIC_00001 1, Lot NA Chromium 20 ug/L Copper 20 ug/L Lead 10 ug/L Nickel 20 ug/L Vanadium 10 ug/L Zinc 40 ug/L 06/01/13 (Purchased Reagent) Barium 10 ug/mL IV, Lot F2-MEB423074 .M12ESTKIC_00002 Chromium 10 ug/mL Copper 10 ug/mL Lead 5 ug/mL Nickel 10 ug/mL Vanadium 5 ug/mL Zinc 20 ug/mL M12GSTKIC_00002 Barium 0.4 ug/mL 1000 mL 8 mL 07/10/1312/06/12 M12LICVIC_00001 1, Lot N/A Chromium 0.4 ug/mL Copper 0.4 ug/mL Lead 0.4 ug/mL Nickel 0.4 ug/mL Vanadium 4 ug/mL Zinc 0.4 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL Zinc 50 ug/mL M12KSTKIC_00003 Al 500 ug/mL 1000 mL 100 mL 12/01/1312/03/12 M12LISAIC_00001 1, Lot na Ca 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL M12ISTKIC_00003 Ag 0.2 ug/mL 1000 mL 10 mL 09/01/1312/03/12 M12LISBIC_00001 1, Lot B51037 As 0.1 ug/mL Barium 0.5 ug/mL Be 0.5 ug/mL Cd 1 ug/mL Chromium 0.5 ug/mL Co 0.5 ug/mL Copper 0.5 ug/mL Lead 0.05 ug/mL 

## 01/04/2013 Page 78 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Mn 0.5 ug/mL Nickel 1 ug/mL Sb 0.6 ug/mL Se 0.05 ug/mL Tl 0.1 ug/mL Vanadium 0.5 ug/mL Zinc 1 ug/mL Al 500 ug/mL M12KSTKIC_00003 100 mLCa 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 09/01/13 (Purchased Reagent) Ag 20 ug/mL IV, Lot E2-MEB399019 .M12ISTKIC_00003 As 10 ug/mL Barium 50 ug/mL Be 50 ug/mL Cd 100 ug/mL Chromium 50 ug/mL Co 50 ug/mL Copper 50 ug/mL Lead 5 ug/mL Mn 50 ug/mL Nickel 100 ug/mL Sb 60 ug/mL Se 5 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 100 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/25/1212/11/12 VA/2CEVESTDWK_00179 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/03/1211/19/12 VOC/THF SPK_00124 1, Lot DG596 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 

## 01/04/2013 Page 79 of 332

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/25/1212/11/12 VOC/THF SPK_00127 1, Lot DG860 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 04/30/15 (Purchased Reagent) Chromium, hexavalent 1000 mg/L ERA, Lot 160412 WSTCR1_00008 12/29/12 (Purchased Reagent) Chromium, hexavalent 16.9 mg/L STL, Lot Lead(II)Chrom_00001 WSTCR13_00629 05/31/17 (Purchased Reagent) Chromium, hexavalent 1000 mg/L Ultra Scientific, Lot L00439 WSTCR2_00008 12/27/1212/27/12 100 mLWSTCN1_00011 1 mLCyanide, Total 10 mg/L WSTINCN1_00571 DI WATER, Lot NA 01/31/14 (Purchased Reagent) Cyanide, Total 1000 mg/L ERA, Lot 060112 .WSTCN1_00011 12/28/1212/28/12 100 mLWSTCN1_00011 1 mLCyanide, Total 10 mg/L WSTINCN1_00572 DI WATER, Lot NA 01/31/14 (Purchased Reagent) Cyanide, Total 1000 mg/L ERA, Lot 060112 .WSTCN1_00011 WSTCN2_00028 Cyanide, Amenable 10 mg/L 100 mL 1 mL 12/27/1212/27/12 WSTINCN2_00563 DI WATER, Lot NA Cyanide, Free 10 mg/L Cyanide, Reactive 10 mg/L Cyanide, Total 10 mg/L Cyanide, Weak Acid Dissociable 10 mg/L 03/31/13 (Purchased Reagent) Cyanide, Amenable 1000 mg/L RICCA, Lot 4204518 .WSTCN2_00028 Cyanide, Free 1000 mg/L Cyanide, Reactive 1000 mg/L Cyanide, Total 1000 mg/L Cyanide, Weak Acid Dissociable 1000 mg/L WSTCN2_00028 Cyanide, Amenable 10 mg/L 100 mL 1 mL 12/28/1212/28/12 WSTINCN2_00564 DI WATER, Lot NA Cyanide, Free 10 mg/L Cyanide, Reactive 10 mg/L Cyanide, Total 10 mg/L Cyanide, Weak Acid Dissociable 10 mg/L 03/31/13 (Purchased Reagent) Cyanide, Amenable 1000 mg/L RICCA, Lot 4204518 .WSTCN2_00028 Cyanide, Free 1000 mg/L Cyanide, Reactive 1000 mg/L Cyanide, Total 1000 mg/L Cyanide, Weak Acid Dissociable 1000 mg/L 11/15/13 (Purchased Reagent) Sulfide 180 mg/L NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL WSTSF1_00036 Sulfide as H2S 209.1 mg/L Sulfide, Reactive 180 mg/L



## 01/04/2013 Page 80 of 332

# Certification Summary Client: Project Integration, Inc TestAmerica Job ID: 500-53342-1 Project/Site:John Deere Des MoinesWorks(JDDMW)

Laboratory Authority Program EPA Region Certification ID TestAmerica Chicago 40461 State Program Alabama 4 TestAmerica Chicago 01132CA NELAP California 9 TestAmerica Chicago 939 State Program Georgia 4 TestAmerica Chicago N/A State Program Georgia 4 TestAmerica Chicago N/A State Program Hawaii 9 TestAmerica Chicago 100201 NELAP Illinois 5 TestAmerica Chicago C-IL-02 State Program Indiana 5 TestAmerica Chicago 82 State Program Iowa 7 TestAmerica Chicago E-10161 NELAP Kansas 7 TestAmerica Chicago 90023 State Program Kentucky 4 TestAmerica Chicago 66 State Program Kentucky (UST) 4 TestAmerica Chicago L2304 DoD ELAP L-A-B TestAmerica Chicago L2304 ISO/IEC 17025 L-A-B TestAmerica Chicago 30720 NELAP Louisiana 6 TestAmerica Chicago M-IL035 State Program Massachusetts 1 TestAmerica Chicago N/A State Program Mississippi 4 TestAmerica Chicago 291 State Program North Carolina DENR 4 TestAmerica Chicago R-194 State Program North Dakota 8 TestAmerica Chicago 8908 State Program Oklahoma 6 TestAmerica Chicago 77001 State Program South Carolina 4 TestAmerica Chicago T104704252-09-TX NELAP Texas 6 TestAmerica Chicago P330-12-00038 Federal USDA TestAmerica Chicago 460142 NELAP Virginia 3 TestAmerica Chicago 999580010 State Program Wisconsin 5 TestAmerica Chicago 8TMS-Q State Program Wyoming 8 Accreditation may not be offered or required for all methods and analytes reported in this package

.Please contact your project manager for the laboratory’s current list of certified methods and analytes.



### TestAmerica Chicago 

## 01/04/2013 Page 81 of 332

# Method 8260B Volatile Organic Compounds (GC/MS) by Method 8260B

01/04/2013

Page 82 of 332

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53342-1 SDG No.: Matrix:Solid Level:Low TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53342-2 FC Composite 5 111 112 100 83 MB 500-173515/4 103 106 113 107 LCS 500-173515/5 103 98 111 102



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 70-134 TOL = Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B # Column to be used to flag recovery values


## 01/04/2013 Page 83 of 332

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53342-1 SDG No.: Matrix:Solid Level:Medium TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53342-2 DL FC Composite 5 DL 95 94 96 86 MB 500-173708/6 88 90 97 88 LCS 500-173708/4 96 94 97 103



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/04/2013 Page 84 of 332

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53342-1 SDG No.: Matrix:Water Level:Low TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53342-3 FC EB 5 96 94 100 90 500-53342-4 Trip Blank 96 95 99 92 MB 500-173827/6 92 90 96 88 LCS 500-173827/4 92 92 97 94



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/04/2013 Page 85 of 332

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53342-1

Lab File ID:16S1220.D Solid Lab ID:LCS 500-173515/5 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 43.68 50-138 87 2-Butanone (MEK) 50.0 45.67 58-133 91

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/04/2013 Page 86 of 332

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Medium 500-53342-1

Lab File ID:22S1221.D Solid Lab ID:LCS 500-173708/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 46.74 46-153 93 2-Butanone (MEK) 50.0 41.90 54-138 84

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/04/2013 Page 87 of 332

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53342-1

Lab File ID:22S1224.D Water Lab ID:LCS 500-173827/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/L) SPIKE ADDED (ug/L) # LCS LCS COMPOUND Acetone 50.0 48.03 46-153 96 2-Butanone (MEK) 50.0 50.18 54-138 100

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/04/2013 Page 88 of 332

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/21/2012 13:16 DB624 N Heated Purge:(Y/N) CMS22 22M1221.D Lab File ID: Lab Sample ID:MB 500-173708/6 Solid Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/21/2012 12:23 22S1221.D LCS 500-173708/4 12/21/2012 22:40 53342-02.D 500-53342-2 DL FC Composite 5 DL

FORM IV 8260B 

## 01/04/2013 Page 89 of 332

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/20/2012 09:00 DB624 Y Heated Purge:(Y/N) CMS16 16M1220.D Lab File ID: Lab Sample ID:MB 500-173515/4 Solid Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/20/2012 09:23 16S1220.D LCS 500-173515/5 12/20/2012 13:52 53342-02.D 500-53342-2 FC Composite 5

FORM IV 8260B 

## 01/04/2013 Page 90 of 332

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53342-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/24/2012 13:33 DB624 N Heated Purge:(Y/N) CMS22 22M1224.D Lab File ID: Lab Sample ID:MB 500-173827/6 Water Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/24/2012 12:35 22S1224.D LCS 500-173827/4 12/24/2012 13:59 53342-04.D 500-53342-4 Trip Blank 12/24/2012 14:25 53342-03.D 500-53342-3 FC EB 5

FORM IV 8260B 

## 01/04/2013 Page 91 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:16B1119c.D CMS16 11/19/2012 11:14 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 170196

5015.0 - 40.0 % of mass 95 19.7 7530.0 - 60.0 % of mass 95 53.5 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.5 173Less than 2.0 % of mass 174 0.7 (1.0)1 17450.0 - 120.00 % of mass 95 75.9 1755.0 - 9.0 % of mass 174 5.3 (6.9)1 17695.0 - 101.0 % of mass 174 74.4 (98.0)1 1775.0 - 9.0 % of mass 176 5.8 (7.8)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 16I1119A.D 11/19/2012 12:14 STD1 500-170196/6 16I1119B.D 11/19/2012 12:37 STD2 500-170196/7 16I1119C.D 11/19/2012 13:00 STD3 500-170196/8 16I1119D.D 11/19/2012 13:23 STD4 500-170196/9 16I1119E.D 11/19/2012 13:46 STD5 500-170196/10 16I1119F.D 11/19/2012 14:09 STD6 500-170196/11 16S1119.D 11/19/2012 17:14 ICV 500-170196/19

FORM V 8260B 

## 01/04/2013 Page 92 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:16B1220a.D CMS16 12/20/2012 07:38 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173515

5015.0 - 40.0 % of mass 95 21.7 7530.0 - 60.0 % of mass 95 47.1 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 8.2 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 79.5 1755.0 - 9.0 % of mass 174 5.2 (6.5)1 17695.0 - 101.0 % of mass 174 77.5 (97.5)1 1775.0 - 9.0 % of mass 176 5.2 (6.7)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 16C1220.D 12/20/2012 08:13 CCV 500-173515/2 16D1220.D 12/20/2012 08:36 CCV 500-173515/3 16M1220.D 12/20/2012 09:00 MB 500-173515/4 16S1220.D 12/20/2012 09:23 LCS 500-173515/5 FC Composite 5 53342-02.D 12/20/2012 13:52 500-53342-2

FORM V 8260B 

## 01/04/2013 Page 93 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:22B1211.D CMS22 12/11/2012 13:45 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 172614

5015.0 - 40.0 % of mass 95 22.6 7530.0 - 60.0 % of mass 95 45.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.5 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 86.2 1755.0 - 9.0 % of mass 174 5.9 (6.8)1 17695.0 - 101.0 % of mass 174 86.4 (100.2)1 1775.0 - 9.0 % of mass 176 4.9 (5.7)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22I1211A.D 12/11/2012 14:23 STD01 500-172614/2 22I1211B.D 12/11/2012 14:51 STD02 500-172614/3 22I1211C.D 12/11/2012 15:20 STD03 500-172614/4 22I1211D.D 12/11/2012 15:48 STD04 500-172614/5 22I1211E.D 12/11/2012 16:16 STD05 500-172614/6 22I1211F.D 12/11/2012 16:44 STD06 500-172614/7 22I1211G.D 12/11/2012 17:13 STD07 500-172614/8 22I1211H.D 12/11/2012 17:41 STD08 500-172614/9 22I1211I.D 12/11/2012 18:09 STD09 500-172614/10 22S1211.D 12/12/2012 00:17 ICV 500-172614/23

FORM V 8260B 

## 01/04/2013 Page 94 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:22B1211.D CMS22 12/11/2012 13:45 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 172615

5015.0 - 40.0 % of mass 95 22.6 7530.0 - 60.0 % of mass 95 45.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.5 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 86.2 1755.0 - 9.0 % of mass 174 5.9 (6.8)1 17695.0 - 101.0 % of mass 174 86.4 (100.2)1 1775.0 - 9.0 % of mass 176 4.9 (5.7)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22I1211A.D 12/11/2012 14:23 STD01 500-172615/2 22I1211B.D 12/11/2012 14:51 STD02 500-172615/3 22I1211C.D 12/11/2012 15:20 STD03 500-172615/4 22I1211D.D 12/11/2012 15:48 STD04 500-172615/5 22I1211E.D 12/11/2012 16:16 STD05 500-172615/6 22I1211F.D 12/11/2012 16:44 STD06 500-172615/7 22I1211G.D 12/11/2012 17:13 STD07 500-172615/8 22I1211H.D 12/11/2012 17:41 STD08 500-172615/9 22I1211I.D 12/11/2012 18:09 STD09 500-172615/10 22S1211.D 12/12/2012 00:17 ICV 500-172615/23

FORM V 8260B 

## 01/04/2013 Page 95 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:22B1221.D CMS22 12/21/2012 10:53 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173708

5015.0 - 40.0 % of mass 95 27.5 7530.0 - 60.0 % of mass 95 49.0 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 8.2 173Less than 2.0 % of mass 174 0.4 (0.4)1 17450.0 - 120.00 % of mass 95 92.1 1755.0 - 9.0 % of mass 174 6.7 (7.3)1 17695.0 - 101.0 % of mass 174 92.3 (100.3)1 1775.0 - 9.0 % of mass 176 6.0 (6.5)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22C1221.D 12/21/2012 11:31 CCV 500-173708/2 22D1221.D 12/21/2012 11:57 CCV 500-173708/3 22S1221.D 12/21/2012 12:23 LCS 500-173708/4 22M1221.D 12/21/2012 13:16 MB 500-173708/6 FC Composite 5 DL 53342-02.D 12/21/2012 22:40 500-53342-2 DL

FORM V 8260B 

## 01/04/2013 Page 96 of 332

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53342-1

Lab File ID: Instrument ID:22B1224.D CMS22 12/24/2012 11:02 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173827

5015.0 - 40.0 % of mass 95 24.4 7530.0 - 60.0 % of mass 95 44.1 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.8 173Less than 2.0 % of mass 174 1.9 (1.9)1 17450.0 - 120.00 % of mass 95 101.2 1755.0 - 9.0 % of mass 174 9.0 (8.9)1 17695.0 - 101.0 % of mass 174 97.2 (96.0)1 1775.0 - 9.0 % of mass 176 5.2 (5.3)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22C1224.D 12/24/2012 11:43 CCV 500-173827/2 22D1224.D 12/24/2012 12:09 CCV 500-173827/3 22S1224.D 12/24/2012 12:35 LCS 500-173827/4 22M1224.D 12/24/2012 13:33 MB 500-173827/6 Trip Blank 53342-04.D 12/24/2012 13:59 500-53342-4 FC EB 5 53342-03.D 12/24/2012 14:25 500-53342-3

FORM V 8260B 

## 01/04/2013 Page 97 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD3 500-170196/8 Date Analyzed:11/19/2012 13:00
Lab File ID (Standard): 16I1119C.D Instrument ID:CMS16 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10620

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 464716 116179 170040 680160 134826 539304 3.42 3.99 6.38 INITIAL CALIBRATION MID-POINT 3.92 2.92 4.49 3.49 6.88 5.88 232358 340080 269652

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170196/19 258949 378895 285510 3.42 3.99 6.38 CCV 500-173515/2 306031 446450 343252 3.42 3.99 6.38 CCV 500-173515/3 299433 436791 334061 3.42 3.99 6.38 MB 500-173515/4 281103 405415 311525 3.42 3.99 6.38 LCS 500-173515/5 299125 434722 333232 3.42 3.99 6.38 500-53342-2 FC Composite 5 241093 359760 232539 3.42 3.99 6.38



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 98 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD3 500-170196/8 Date Analyzed:11/19/2012 13:00
Lab File ID (Standard): 16I1119C.D Instrument ID:CMS16 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10620

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 283260 70815 8.21 INITIAL CALIBRATION MID-POINT 8.71 7.71 141630

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170196/19 139276 8.21 CCV 500-173515/2 162988 8.21 CCV 500-173515/3 161510 8.22 MB 500-173515/4 157163 8.21 LCS 500-173515/5 157933 8.21 500-53342-2 FC Composite 5 58638* 8.22



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 99 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD06 500-172614/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N)N Calibration ID:10829

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 1409738 352435 493044 1972176 417716 1670864 6.27 7.24 10.64 INITIAL CALIBRATION MID-POINT 6.77 5.77 7.74 6.74 11.14 10.14 704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172614/23 772269 1099840 931671 6.26 7.24 10.64 CCV 500-173708/2 687278 977657 817789 6.26 7.24 10.64 CCV 500-173708/3 687212 935438 801033 6.26 7.24 10.64 LCS 500-173708/4 680014 968230 803959 6.26 7.24 10.64 MB 500-173708/6 675524 913201 797068 6.26 7.24 10.64 500-53342-2 DL FC Composite 5 DL 553196 775796 655962 6.26 7.24 10.64



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 100 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD06 500-172614/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N)N Calibration ID:10829

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 1003186 250797 13.08 INITIAL CALIBRATION MID-POINT 13.58 12.58 501593

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172614/23 542063 13.08 CCV 500-173708/2 512733 13.08 CCV 500-173708/3 451000 13.07 LCS 500-173708/4 489137 13.08 MB 500-173708/6 423190 13.08 500-53342-2 DL FC Composite 5 DL 344276 13.07



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 101 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD06 500-172615/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N)N Calibration ID:10830

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 1409738 352435 493044 1972176 417716 1670864 6.27 7.24 10.64 INITIAL CALIBRATION MID-POINT 6.77 5.77 7.74 6.74 11.14 10.14 704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172615/23 772269 1099840 931671 6.26 7.24 10.64 CCV 500-173827/2 690066 966119 829756 6.26 7.24 10.64 CCV 500-173827/3 718212 976330 827808 6.26 7.24 10.64 LCS 500-173827/4 678203 926614 799281 6.26 7.24 10.64 MB 500-173827/6 646307 901906 766183 6.26 7.24 10.64 500-53342-4 Trip Blank 670114 929055 794089 6.26 7.24 10.64 500-53342-3 FC EB 5 629756 877752 760147 6.27 7.24 10.64



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 102 of 332

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53342-1
Sample No.:STD06 500-172615/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N)N Calibration ID:10830

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 1003186 250797 13.08 INITIAL CALIBRATION MID-POINT 13.58 12.58 501593

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172615/23 542063 13.08 CCV 500-173827/2 505828 13.07 CCV 500-173827/3 467889 13.08 LCS 500-173827/4 489029 13.08 MB 500-173827/6 424583 13.08 500-53342-4 Trip Blank 435535 13.08 500-53342-3 FC EB 5 410915 13.08



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/04/2013 Page 103 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:
FC Composite 5 SDG No.: 500-53342-1
Lab Sample ID:500-53342-2 Matrix: 53342-02.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/17/2012 14:40 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

73.1 1
Level: (low/med)Low 5(g)
0.2(mm) Date Analyzed:12/20/2012 13:52

ID: DB624
Analysis Batch No.: 173515 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL18.6 6.72 78-93-3 2-Butanone (MEK) 28.2


### %REC CAS NO. LIMITS Q SURROGATE 112 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 100 75-122 2037-26-5 Toluene-d8 (Surr) 83 70-122 460-00-4 4-Bromofluorobenzene (Surr) 111 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 104 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:
FC Composite 5 DL SDG No.: 500-53342-1
Lab Sample ID:500-53342-2 DL Matrix: 53342-02.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/17/2012 14:40 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

73.1 50
Level: (low/med)Medium 5(g) 5 (mL) 5(mL) 0.2(mm) Date Analyzed:12/21/2012 22:40

ID: DB624
Analysis Batch No.: 173708 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL928 241 67-64-1 Acetone 3200


### %REC CAS NO. LIMITS Q SURROGATE 94 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-120 2037-26-5 Toluene-d8 (Surr) 86 75-120 460-00-4 4-Bromofluorobenzene (Surr) 95 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 105 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC EB 5 SDG No.: 500-53342-1
Lab Sample ID:500-53342-3 Matrix: 53342-03.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/17/2012 14:30 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(mL)
0.2(mm) Date Analyzed:12/24/2012 14:25

ID: DB624
Analysis Batch No.: 173827 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 94 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 100 75-120 2037-26-5 Toluene-d8 (Surr) 90 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 106 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:
Trip Blank SDG No.: 500-53342-1
Lab Sample ID:500-53342-4 Matrix: 53342-04.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/17/2012 00:00 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(mL)
0.2(mm) Date Analyzed:12/24/2012 13:59

ID: DB624
Analysis Batch No.: 173827 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 95 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 99 75-120 2037-26-5 Toluene-d8 (Surr) 92 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 107 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-170196/6 16I1119A.D 2 Level STD2 500-170196/7 16I1119B.D 3 Level STD3 500-170196/8 16I1119C.D 4 Level STD4 500-170196/9 16I1119D.D 5 Level STD5 500-170196/10 16I1119E.D 6 Level STD6 500-170196/11 16I1119F.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Dichlorodifluoromethane 0.5101 0.4328 0.4745 0.4472 0.4791Ave 5.9 0.4553 0.0100 15.0 0.4665 Chloromethane 0.6409 0.5486 0.6042 0.5514 0.5726Ave 6.2 0.5611 0.1000 15.0 0.5798 Vinyl chloride 0.5489 0.4879 0.5232 0.4889 0.5055Ave 4.9 0.4889 0.0100 15.0 0.5072 Bromomethane 0.2173 0.1622 0.1619 0.1577 0.1599Lin2 0.9990 0.1594 0.0100 0.9900 0.30230.1550 Chloroethane 0.2848 0.2512 0.2658 0.2550 0.2653Ave 4.4 0.2627 0.0100 15.0 0.2641 Trichlorofluoromethane 0.6410 0.5479 0.5898 0.5813 0.5855Ave 5.1 0.5792 0.0100 15.0 0.5875 Acrolein 0.0833 0.0649 0.0739 0.0632 0.0635Lin2 0.9920 0.0576 0.0010 0.9900 4.11290.0627 1,1-Dichloroethene 0.3883 0.3810 0.3940 0.3681 0.3657Ave 4.2 0.3520 0.0100 15.0 0.3748 1,1,2-Trichloro-1,2,2-trifluoroethane 0.4271 0.3940 0.4076 0.3784 0.3788Ave 6.6 0.3531 0.0100 15.0 0.3898 Acetone 0.2177 0.1065 0.1169 0.1078 0.1047Lin1 0.9950 0.0952 0.0100 0.9900 0.55990.0976 Carbon disulfide 1.2281 1.2015 1.3462 1.3937 1.2778Ave 5.7 1.2592 0.0100 15.0 1.2844 Acetonitrile 0.0349 0.0327 0.0349 0.0328 0.0329Ave 6.1 0.0294 0.0010 15.0 0.0330 Methylene Chloride 0.4402 0.4262 0.4539 0.4254 0.4228Ave 4.4 0.3973 0.0100 15.0 0.4276 Acrylonitrile 0.1608 0.1223 0.1370 0.1213 0.1263Lin2 0.9950 0.1142 0.0010 0.9900 1.55620.1209 trans-1,2-Dichloroethene 0.4687 0.4410 0.4603 0.4325 0.4314Ave 4.6 0.4139 0.0100 15.0 0.4413



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 108 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Methyl tert-butyl ether 1.2409 1.0967 1.2053 1.0887 1.1030Ave 7.6 1.0084 0.0100 15.0 1.1238 1,1-Dichloroethane 0.9158 0.8754 0.8985 0.8573 0.8580Ave 4.0 0.8171 0.1000 15.0 0.8704 Vinyl acetate 0.7794 0.7899 0.8439 0.8848 0.9027Ave 6.1 0.8075 0.0100 15.0 0.8347 2,2-Dichloropropane 0.5123 0.4762 0.4910 0.4760 0.4692Ave 5.5 0.4333 0.0100 15.0 0.4764 cis-1,2-Dichloroethene 0.5178 0.4752 0.4900 0.4699 0.4727Ave 4.9 0.4468 0.0100 15.0 0.4787 2-Butanone (MEK) 0.1907 0.1661 0.1744 0.1666 0.1738Ave 7.0 0.1547 0.0100 15.0 0.1710 Propionitrile 0.0377 0.0303 0.0325 0.0300 0.0310Ave 10.0 0.0283 0.0010 15.0 0.0316 Bromochloromethane 0.2134 0.1810 0.1955 0.1835 0.1826Ave 7.7 0.1724 0.0100 15.0 0.1881 Tetrahydrofuran 0.1362 0.1110 0.1157 0.1060 0.1101Lin2 0.9970 0.0981 0.0100 0.9900 0.15500.1053 Chloroform 0.8071 0.7676 0.7909 0.7569 0.7592Ave 3.9 0.7200 0.0100 15.0 0.7669 1,1,1-Trichloroethane 0.6379 0.6227 0.6514 0.6248 0.6266Ave 3.7 0.5828 0.0100 15.0 0.6244 Carbon tetrachloride 0.3601 0.3514 0.3626 0.3590 0.3620Ave 1.9 0.3457 0.0100 15.0 0.3568 1,1-Dichloropropene 0.6628 0.6440 0.6397 0.6320 0.6326Ave 3.2 0.6014 0.0100 15.0 0.6354 Benzene 1.2960 1.2332 1.2212 1.1893 1.1679Ave 5.2 1.1124 0.0100 15.0 1.2033 1,2-Dichloroethane 0.4036 0.3828 0.3925 0.3773 0.3822Ave 3.7 0.3615 0.0100 15.0 0.3833 Trichloroethene 0.3071 0.2871 0.2880 0.2787 0.2819Ave 4.3 0.2706 0.0100 15.0 0.2856 1,2-Dichloropropane 0.2945 0.3110 0.2983 0.3002 0.3013Ave 2.3 0.2903 0.0100 15.0 0.2993 Dibromomethane 0.1499 0.1401 0.1448 0.1410 0.1445Ave 3.6 0.1346 0.0100 15.0 0.1425 Bromodichloromethane 0.3131 0.3276 0.3492 0.3570 0.3677Ave 5.9 0.3548 0.0100 15.0 0.3449 2-Chloroethyl vinyl ether 0.1275 0.1289 0.1333 0.1400 0.1446Ave 5.1 0.1302 0.0100 15.0 0.1341



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 109 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 cis-1,3-Dichloropropene 0.3823 0.3878 0.3955 0.4081 0.4277Ave 4.1 0.4075 0.0100 15.0 0.4015 4-Methyl-2-pentanone (MIBK) 0.2134 0.2212 0.2438 0.2360 0.2310Ave 5.2 0.2176 0.0100 15.0 0.2272 Toluene 0.7563 0.7457 0.7103 0.7065 0.7016Ave 4.3 0.6724 0.0100 15.0 0.7155 trans-1,3-Dichloropropene 0.3019 0.3263 0.3366 0.3455 0.3644Ave 6.4 0.3505 0.0100 15.0 0.3375 1,1,2-Trichloroethane 0.2720 0.2647 0.2830 0.2757 0.2832Ave 2.6 0.2710 0.0100 15.0 0.2749 Tetrachloroethene 0.3877 0.3857 0.3641 0.3770 0.3714Ave 3.1 0.3585 0.0100 15.0 0.3741 1,3-Dichloropropane 0.4386 0.4678 0.4537 0.4585 0.4651Ave 2.7 0.4404 0.0100 15.0 0.4540 2-Hexanone 0.1953 0.1931 0.1955 0.2045 0.1961Ave 2.7 0.1880 0.0100 15.0 0.1954 Dibromochloromethane 0.2040 0.2329 0.2507 0.2602 0.2677Ave 9.7 0.2616 0.0100 15.0 0.2462 1,2-Dibromoethane 0.1811 0.1775 0.1848 0.1786 0.1848Ave 2.7 0.1720 0.0100 15.0 0.1798 1-Chlorohexane 0.6093 0.5831 0.5505 0.5582 0.5737Ave 4.3 0.5435 0.0100 15.0 0.5697 Chlorobenzene 0.9184 0.9225 0.9033 0.9116 0.9054Ave 2.2 0.8681 0.3000 15.0 0.9049 1,1,1,2-Tetrachloroethane 0.2930 0.2979 0.3101 0.3188 0.3208Ave 3.6 0.3132 0.0100 15.0 0.3090 Ethylbenzene 0.5544 0.5503 0.5126 0.5352 0.5171Ave 4.1 0.5009 0.0100 15.0 0.5284 m&p-Xylene 1.3686 1.3827 1.3012 1.2861 1.2289Ave 6.9 1.1453 0.0100 15.0 1.2855 o-Xylene 1.3495 1.4372 1.3698 1.3557 1.3252Ave 4.5 1.2528 0.0100 15.0 1.3484 Styrene 0.9608 1.0612 1.0145 1.0388 1.0303Ave 3.6 0.9843 0.0100 15.0 1.0150 Bromoform 0.1125 0.1362 0.1408 0.1514 0.1643Ave 13.0 0.1539 0.1000 15.0 0.1432 Isopropylbenzene 3.1539 3.6540 3.1572 3.3315 3.1688Ave 6.7 3.0455 0.0100 15.0 3.2518 Bromobenzene 0.6695 0.7563 0.7093 0.7420 0.7361Ave 4.2 0.7199 0.0100 15.0 0.7222



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 110 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 1,1,2,2-Tetrachloroethane 0.5452 0.5696 0.5597 0.5706 0.5758Ave 3.0 0.5328 0.3000 15.0 0.5589 1,2,3-Trichloropropane 0.1912 0.1794 0.1660 0.1701 0.1701Ave 6.1 0.1622 0.0100 15.0 0.1732 N-Propylbenzene 3.9287 4.2993 3.7879 3.9367 3.7362Ave 6.3 3.5832 0.0100 15.0 3.8787 2-Chlorotoluene 2.3554 2.5038 2.2305 2.3361 2.2656Ave 4.9 2.1830 0.0100 15.0 2.3124 1,3,5-Trimethylbenzene 2.6219 2.9360 2.6333 2.7109 2.6361Ave 5.3 2.5201 0.0100 15.0 2.6764 4-Chlorotoluene 2.6491 2.9401 2.6216 2.7188 2.6440Ave 5.1 2.5353 0.0100 15.0 2.6848 tert-Butylbenzene 2.2801 2.5455 2.2199 2.2982 2.2247Ave 6.1 2.1418 0.0100 15.0 2.2850 1,2,4-Trimethylbenzene 2.7631 3.0061 2.6438 2.7255 2.6458Ave 5.8 2.5511 0.0100 15.0 2.7226 sec-Butylbenzene 3.5331 3.8935 3.3623 3.4462 3.3180Ave 7.1 3.1870 0.0100 15.0 3.4567 1,3-Dichlorobenzene 1.4471 1.5053 1.3813 1.4255 1.3778Ave 4.0 1.3501 0.0100 15.0 1.4145 p-Isopropyltoluene 2.9586 3.2474 2.8310 2.8845 2.8017Ave 6.6 2.6869 0.0100 15.0 2.9017 1,4-Dichlorobenzene 1.3977 1.4878 1.3669 1.4117 1.3954Ave 3.8 1.3295 0.0100 15.0 1.3982 n-Butylbenzene 2.8602 3.1543 2.7994 2.7899 2.7599Ave 6.2 2.6239 0.0100 15.0 2.8313 1,2-Dichlorobenzene 1.2797 1.3306 1.2155 1.2573 1.2376Ave 3.9 1.1916 0.0100 15.0 1.2521 1,2-Dibromo-3-Chloropropane 0.0873 0.0832 0.0794 0.0812 0.0900Ave 4.7 0.0826 0.0100 15.0 0.0839 1,2,4-Trichlorobenzene 0.9789 0.9823 0.8678 0.7520 0.7794Ave 13.0 0.7396 0.0100 15.0 0.8500 Hexachlorobutadiene 0.6292 0.6291 0.5100 0.4198 0.4138Qua1 0.9940 +++++ 0.0100 0.9900 0.74170.5403-0.001 Naphthalene 1.6968 1.5945 1.4268 1.3407 1.4423Lin2 0.9970 1.3291 0.0100 0.9900 1.66281.3908 1,2,3-Trichlorobenzene 0.7531 0.7667 0.6080 0.5315 0.5708Qua2 0.9900 0.5407 0.0100 0.9900 0.46540.6784-0.001 Dibromofluoromethane 0.4012 0.4120 0.3878 0.4079Ave 4.3 0.3703 0.0100 15.0 0.3958



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 111 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 1,2-Dichloroethane-d4 (Surr) 0.3252 0.3396 0.3092 0.3325Ave 6.0 0.2918 0.0100 15.0 0.3196 Toluene-d8 (Surr) 1.0538 1.0512 0.9999 1.0425Ave 4.8 0.9393 0.0100 15.0 1.0174 4-Bromofluorobenzene (Surr) 0.5024 0.5042 0.4741 0.5018Ave 5.3 0.4456 0.0100 15.0 0.4856



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 112 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-170196/6 16I1119A.D Level2 STD2 500-170196/7 16I1119B.D Level3 STD3 500-170196/8 16I1119C.D Level4 STD4 500-170196/9 16I1119D.D Level5 STD5 500-170196/10 16I1119E.D Level6 STD6 500-170196/11 16I1119F.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Dichlorodifluoromethane Ave PFB 12902 50070 127370 264568 422626 553924 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 16213 63463 162200 326211 505093 682571 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 13885 56436 140448 289222 445896 594740 5.00 20.0 50.0 100 150 200 Bromomethane Lin2 PFB 5496 18758 43458 93314 141095 193922 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 7205 29060 71345 150837 234006 319655 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 16215 63387 158331 343881 516513 704692 5.00 20.0 50.0 100 150 200 Acrolein Lin2 PFB 84258 300252 793200 1494545 2240120 2801943 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 9821 44072 105755 217759 322621 428198 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 10804 45578 109401 223828 334178 429549 5.00 20.0 50.0 100 150 200 Acetone Lin1 PFB 5507 12315 31383 63749 92368 115814 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 31066 138989 361364 824494 1127201 1531938 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 7059 30299 75012 155141 232468 286410 40.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 11136 49301 121856 251650 373003 483310 5.00 20.0 50.0 100 150 200 Acrylonitrile Lin2 PFB 32531 113188 294241 574185 891617 1111839 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 11855 51013 123566 255847 380526 503496 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 31388 126868 323557 644017 972967 1226790 5.00 20.0 50.0 100 150 200


### FORM VI 8260B 

## 01/04/2013 Page 113 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 1,1-Dichloroethane Ave PFB 23166 101272 241193 507139 756847 994036 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 19714 91380 226543 523396 796266 982422 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 12960 55088 131791 281610 413914 527180 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 13099 54969 131526 277962 416945 543539 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 4823 19213 46819 98580 153328 188153 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 11092 40835 102296 208849 323908 406897 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 5399 20944 52481 108571 161097 209785 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Lin2 PFB 3446 12837 31053 62700 97150 119315 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 20416 88794 212306 447767 669705 875928 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 16137 72040 174862 369627 552754 709015 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 13245 59272 142459 312633 472055 620557 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 16767 74498 171713 373900 558058 731603 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 47671 208006 479794 1035802 1523052 1996925 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 14847 64572 154226 328584 498369 649012 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 11297 48428 113149 242684 367651 485784 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 10834 52448 117184 261424 392941 521104 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 5515 23635 56895 122814 188390 241667 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 11517 55249 137199 310916 479512 636972 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 4691 21736 52381 121903 188565 233764 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 14063 65411 155392 355410 557705 731626 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB 7850 37307 95785 205560 301187 390574 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 114 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Toluene Ave DFB 27820 125770 279057 615277 914875 1207131 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 11105 55044 132225 300866 475199 629293 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 6881 30616 75972 163072 249804 329645 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 11739 49681 113412 247302 371178 488872 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 13281 60253 141339 300730 464793 600568 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 5913 24867 60900 134127 195945 256358 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 6176 29991 78104 170673 267577 356811 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 6662 29944 72598 155572 240952 308703 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 15413 67451 147771 330227 506094 661180 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 27808 118815 281396 597934 904889 1183858 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 8870 38367 96602 209122 320615 427140 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 16785 70876 159684 351002 516773 683074 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 82877 356156 810673 1687130 2456378 3123829 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 40858 185102 426723 889192 1324449 1708514 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 29090 136679 316041 681314 1029721 1342275 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 3407 17540 43862 99282 164184 209852 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 51019 228406 516591 1065124 1575324 2017775 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 10830 47272 116055 237235 365963 476962 5.00 20.0 50.0 100 150 200 1,1,2,2-Tetrachloroethane Ave DCB 8819 35605 91578 182439 286268 352978 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 3093 11214 27159 54392 84576 107459 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 63553 268743 619776 1258627 1857403 2373990 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 115 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 2-Chlorotoluene Ave DCB 38102 156509 364951 746878 1126306 1446295 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 42413 183522 430864 866728 1310538 1669636 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 42853 183778 428943 869237 1314457 1679760 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 36885 159113 363220 734777 1106000 1419051 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 44697 187908 432579 871394 1315353 1690213 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 57153 243374 550146 1101803 1649521 2111505 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 23410 94092 226011 455769 684977 894523 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 47861 202992 463212 922211 1392838 1780196 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 22610 92998 223660 451341 693731 880833 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 46268 197168 458033 891981 1372078 1738419 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 20701 83175 198883 401981 615248 789503 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 1412 5199 12985 25946 44755 54754 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 15835 61405 141991 240412 387497 490028 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Qua1 DCB 10179 39324 83450 134222 205730 +++++ 5.00 20.0 50.0 100 150 +++++ Naphthalene Lin2 DCB 27448 99668 233455 428628 717029 880550 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Qua2 DCB 12182 47927 99479 169921 283755 358235 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 46408 110602 229403 359839 450525 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 54848 133405 269262 433613 523883 20.0 50.0 100 150 200 Toluene-d8 (Surr) Ave DFB 177743 413010 870860 1359449 1686334 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 64705 157084 310979 501486 607718 20.0 50.0 100 150 200



### FORM VI 8260B 

## 01/04/2013 Page 116 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend: Ave = Average ISTD Lin1 = Linear 1/conc ISTD Lin2 = Linear 1/conc^2 ISTD Qua1 = Quadratic 1/conc ISTD Qua2 = Quadratic 1/conc^2 ISTD



### FORM VI 8260B 

## 01/04/2013 Page 117 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD01 500-172614/2 22I1211A.D 2 Level STD02 500-172614/3 22I1211B.D 3 Level STD03 500-172614/4 22I1211C.D 4 Level STD04 500-172614/5 22I1211D.D 5 Level STD05 500-172614/6 22I1211E.D 6 Level STD06 500-172614/7 22I1211F.D 7 Level STD07 500-172614/8 22I1211G.D 8 Level STD08 500-172614/9 22I1211H.D 9 Level STD09 500-172614/10 22I1211I.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883Ave 9.9 0.5798 0.5632 0.5150 0.5364 0.0100 15.0 0.5420 Chloromethane 0.8256 0.7243 0.6267 0.6890Ave 7.9 0.7182 0.7230 0.6810 0.7012 0.1000 15.0 0.7111 Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130Ave 8.0 0.6517 0.6618 0.6041 0.6323 0.0100 15.0 0.6381 Bromomethane 0.1659 0.2203 0.1716 0.1726Ave 13.0 0.2077 0.2258 0.2110 0.2234 0.0100 15.0 0.1998 Chloroethane 0.4113 0.3289 0.3175 0.3315Ave 10.0 0.3369 0.3333 0.3044 0.3069 0.0100 15.0 0.3338 Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079Ave 6.3 0.9817 1.0066 0.9437 0.9571 0.0100 15.0 0.9993 Acetone +++++ +++++ 0.0554 0.0635Ave 7.8 0.0614 0.0672 0.0690 0.0671 0.0100 15.0 0.0639 Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319Ave 7.9 0.8320 0.8249 0.7635 0.7796 0.0100 15.0 0.8265 Acrolein 0.0331 0.0421 0.0314 0.0388Ave 13.0 0.0392 0.0429 0.0450 0.0450 0.0010 15.0 0.0397 1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008Ave 4.7 0.3938 0.3925 0.3935 0.4040 0.0100 15.0 0.4001 1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785Ave 6.7 0.4739 0.4784 0.4696 0.4829 0.0100 15.0 0.4862 Methylene Chloride +++++ 0.4011 0.3629 0.4004Ave 4.0 0.3719 0.3777 0.3682 0.3859 0.0100 15.0 0.3812 Carbon disulfide 1.5962 1.3713 1.3219 1.4559Ave 6.5 1.5313 1.5882 1.4767 1.4979 0.0100 15.0 1.4799



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 118 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Acetonitrile 0.0371 0.0333 0.0243 0.0295Ave 13.0 0.0262 0.0281 0.0299 0.0295 0.0010 15.0 0.0297 Acrylonitrile 0.0750 0.0912 0.0677 0.0823Ave 9.0 0.0764 0.0821 0.0846 0.0849 0.0010 15.0 0.0805 trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560Ave 4.4 0.4456 0.4511 0.4430 0.4552 0.0100 15.0 0.4499 2-Butanone (MEK) +++++ +++++ 0.0823 0.0919Ave 6.1 0.0908 0.0953 0.0973 0.0970 0.0100 15.0 0.0924 Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577Ave 5.4 0.7230 0.7592 0.7369 0.7564 0.0100 15.0 0.7369 Vinyl acetate +++++ 0.6129 0.5650 0.6423Ave 5.2 0.6107 0.6494 0.6338 0.6642 0.0100 15.0 0.6255 Tetrahydrofuran +++++ +++++ 0.0538 0.0611Ave 4.2 0.0583 0.0572 0.0571 0.0595 0.0100 15.0 0.0578 1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189Ave 6.2 0.8749 0.8925 0.8704 0.9084 0.1000 15.0 0.8857 2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515Ave 5.5 0.7243 0.7285 0.7200 0.7474 0.0100 15.0 0.7341 cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663Ave 6.4 0.4508 0.4630 0.4488 0.4652 0.0100 15.0 0.4554 Propionitrile 0.0230 0.0200 0.0163 0.0205Ave 10.0 0.0191 0.0201 0.0217 0.0219 0.0010 15.0 0.0203 Bromochloromethane 0.2191 0.1652 0.1606 0.1825Ave 10.0 0.1747 0.1747 0.1737 0.1772 0.0100 15.0 0.1785 Chloroform 0.7988 0.7465 0.6742 0.7604Ave 4.9 0.7195 0.7370 0.7200 0.7434 0.0100 15.0 0.7375 1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390Ave 4.7 0.7317 0.7368 0.7320 0.7583 0.0100 15.0 0.7394 Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871Ave 3.4 0.4883 0.4750 0.4767 0.4948 0.0100 15.0 0.4834 1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649Ave 6.9 0.6479 0.6478 0.6435 0.6685 0.0100 15.0 0.6488 Benzene 1.2306 1.3508 1.2179 1.1306 1.2550Ave 4.7 1.2277 1.2183 1.1975 1.2355 0.0100 15.0 1.2293 1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618Ave 5.6 0.3558 0.3552 0.3521 0.3644 0.0100 15.0 0.3536 4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561Ave 5.1 0.1535 0.1552 0.1604 0.1580 0.0100 15.0 0.1536 2-Hexanone +++++ +++++ 0.1035 0.1187Ave 7.3 0.1220 0.1257 0.1256 0.1271 0.0100 15.0 0.1204



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 119 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516Ave 4.9 0.3434 0.3325 0.3291 0.3406 0.0100 15.0 0.3450 1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264Ave 6.4 0.3130 0.3110 0.3089 0.3197 0.0100 15.0 0.3152 Dibromomethane 0.1457 0.1306 0.1153 0.1288Ave 6.9 0.1238 0.1238 0.1224 0.1261 0.0100 15.0 0.1271 Bromodichloromethane 0.3875 0.3507 0.3319 0.3726Ave 4.6 0.3533 0.3599 0.3552 0.3686 0.0100 15.0 0.3600 2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096Ave 3.2 0.1015 0.1078 0.1021 0.1054 0.0100 15.0 0.1054 cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222Ave 4.1 0.4033 0.4109 0.4067 0.4210 0.0100 15.0 0.4091 Toluene 0.9341 0.8388 0.7909 0.7458 0.8161Ave 6.2 0.8023 0.8060 0.7995 0.8258 0.0100 15.0 0.8177 trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412Ave 8.6 0.3304 0.3383 0.3448 0.3521 0.0100 15.0 0.3392 1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681Ave 7.7 0.1638 0.1667 0.1692 0.1728 0.0100 15.0 0.1723 Tetrachloroethene 0.5511 0.4482 0.4255 0.4568Ave 9.0 0.4446 0.4384 0.4251 0.4400 0.0100 15.0 0.4537 1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542Ave 4.9 0.3407 0.3413 0.3399 0.3540 0.0100 15.0 0.3491 Dibromochloromethane 0.2702 0.2371 0.2274 0.2693Ave 6.9 0.2630 0.2690 0.2675 0.2786 0.0100 15.0 0.2603 1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607Ave 10.0 0.1572 0.1634 0.1626 0.1665 0.0100 15.0 0.1651 Chlorobenzene 1.1305 1.0221 0.9605 1.0363Ave 5.3 0.9949 0.9884 0.9670 0.9960 0.3000 15.0 1.0120 1-Chlorohexane 0.7176 0.7070 0.6491 0.6984Ave 3.1 0.6765 0.6760 0.6835 0.6837 0.0100 15.0 0.6865 1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448Ave 5.0 0.3425 0.3461 0.3458 0.3585 0.0100 15.0 0.3400 Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796Ave 3.4 0.5801 0.5769 0.5619 0.5822 0.0100 15.0 0.5753 m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876Ave 4.5 1.4534 1.4554 1.3960 1.3942 0.0100 15.0 1.4275 o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780Ave 5.5 1.4493 1.4706 1.4590 1.5151 0.0100 15.0 1.4564 Styrene 1.1505 1.0719 0.9871 1.1405Ave 5.6 1.1318 1.1478 1.1460 1.1845 0.0100 15.0 1.1200



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 120 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1602 0.1366 0.1243 0.1553Ave 10.0 0.1546 0.1600 0.1660 0.1720 0.1000 15.0 0.1536 Isopropylbenzene 3.8233 3.3535 3.0653 3.4816Ave 7.4 3.1927 3.1639 3.1360 3.2790 0.0100 15.0 3.3119 Bromobenzene 0.8632 0.7552 0.6812 0.7730Ave 8.2 0.6922 0.7028 0.6972 0.7345 0.0100 15.0 0.7374 1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089Ave 6.0 0.3542 0.3640 0.3676 0.3874 0.3000 15.0 0.3844 1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046Ave 6.1 0.2704 0.2691 0.2728 0.2923 0.0100 15.0 0.2827 N-Propylbenzene 4.4856 4.0360 3.6439 4.1493Ave 6.5 3.8858 3.8875 3.7881 3.8936 0.0100 15.0 3.9712 4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065Ave 7.0 2.1662 2.2029 2.1653 2.2760 0.0100 15.0 2.2416 1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026Ave 5.8 2.6929 2.7638 2.7107 2.8237 0.0100 15.0 2.7652 2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174Ave 6.4 2.5627 2.6413 2.6089 2.7193 0.0100 15.0 2.6625 tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552Ave 7.3 2.4553 2.4418 2.4420 2.5773 0.0100 15.0 2.5582 1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710Ave 6.3 2.6381 2.7234 2.6840 2.8189 0.0100 15.0 2.7134 sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075Ave 5.8 3.6796 3.6591 3.6577 3.7738 0.0100 15.0 3.7828 1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907Ave 8.4 1.4814 1.5187 1.5128 1.5667 0.0100 15.0 1.5748 p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705Ave 6.4 3.1719 3.2121 3.1807 3.2836 0.0100 15.0 3.2868 1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651Ave 6.9 1.4798 1.5043 1.4758 1.5340 0.0100 15.0 1.5559 1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033Ave 6.4 1.2786 1.2876 1.2674 1.3183 0.0100 15.0 1.3233 n-Butylbenzene 3.1126 2.8700 2.6461 2.9480Ave 4.7 2.8772 2.9149 2.9548 3.0267 0.0100 15.0 2.9188 1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678Ave 12.0 0.0613 0.0622 0.0635 0.0659 0.0100 15.0 0.0661 1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999Ave 5.3 0.8675 0.9149 0.9059 0.9063 0.0100 15.0 0.8970 Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351Ave 9.3 0.7318 0.6946 0.7407 0.7100 0.0100 15.0 0.7568



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 121 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.0319 0.9651 0.8910 1.0003Ave 5.7 0.9350 0.9776 1.0179 1.0659 0.0100 15.0 0.9856 1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392Ave 5.4 0.6972 0.7092 0.7197 0.7238 0.0100 15.0 0.7171 Dibromofluoromethane 0.4088Ave 3.6 0.3747 0.4105 0.3974 0.4034 0.0100 15.0 0.3990 1,2-Dichloroethane-d4 (Surr) 0.2898Ave 2.8 0.2681 0.2786 0.2783 0.2818 0.0100 15.0 0.2793 Toluene-d8 (Surr) 1.2317Ave 3.0 1.1353 1.2008 1.1689 1.1817 0.0100 15.0 1.1837 4-Bromofluorobenzene (Surr) 0.5022Ave 2.5 0.4792 0.5117 0.5010 0.5085 0.0100 15.0 0.5005



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 122 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD01 500-172614/2 22I1211A.D Level2 STD02 500-172614/3 22I1211B.D Level3 STD03 500-172614/4 22I1211C.D Level4 STD04 500-172614/5 22I1211D.D Level5 STD05 500-172614/6 22I1211E.D Level6 STD06 500-172614/7 22I1211F.D Level7 STD07 500-172614/8 22I1211G.D Level8 STD08 500-172614/9 22I1211H.D Level9 STD09 500-172614/10 22I1211I.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 8283 14019 34084 128973 408706 762307 1110898 1572519 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 10611 19121 44725 181982 506217 978702 1468998 2055922 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 2072 9537 16111 40052 161885 459341 895799 1302949 1853836 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Ave PFB 2132 5817 12250 45578 146376 305638 455210 654905 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 5286 8684 22657 87550 237436 451232 656528 899737 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 14493 27342 66676 266205 691989 1362610 2035639 2806119 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Ave PFB +++++ +++++ 3957 16764 43292 90934 148822 196769 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 12483 22039 55227 219705 586466 1116585 1646914 2285626 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 16997 44508 89671 410157 1104663 2325112 3885554 5276134 40.0 80.0 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 5414 11300 26186 105858 277562 531364 848798 1184587 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 7210 13042 32193 126370 334028 647515 1013020 1415755 1.00 2.00 5.00 20.0 50.0 100 150 200 Methylene Chloride Ave PFB +++++ 10588 25901 105736 262156 511318 794285 1131397 +++++ 2.00 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 20516 36202 94343 384523 1079379 2149891 3185269 4391617 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 3815 7023 13902 62328 147511 304606 515971 692080 8.00 16.0 40.0 160 400 800 1200 1600



### FORM VI 8260B 

## 01/04/2013 Page 123 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Acrylonitrile Ave PFB 7715 19252 38635 173831 430688 889127 1460725 1990459 8.00 16.0 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 6143 12190 29175 120435 314119 610637 955652 1334459 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB +++++ +++++ 5877 24272 64002 128968 209900 284336 +++++ +++++ 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 10253 18092 48485 200118 509651 1027632 1589481 2217547 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB +++++ 16181 40320 169641 430488 879019 1367143 1947324 +++++ 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB +++++ +++++ 3843 16127 41123 77379 123251 174315 +++++ +++++ 5.00 20.0 50.0 100 150 200 1,1-Dichloroethane Ave PFB 12660 21793 57801 242674 616675 1208102 1877461 2663163 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 10444 18966 47829 198464 510518 986077 1552961 2191135 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 6562 11093 29875 123154 317732 626799 968176 1363967 1.00 2.00 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 3274 5826 13049 61580 150541 311165 533857 726579 8.00 16.0 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 2816 4362 11462 48207 123109 236461 374570 519660 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 10267 19708 48119 200834 507134 997634 1553050 2179601 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 10394 19135 48811 195166 515733 997347 1578989 2223267 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 8845 18161 44839 182447 481514 918644 1463204 2051034 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 9406 15734 42090 175593 456667 876844 1388026 1960009 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 5292 24000 44324 113004 470128 1210657 2356179 3675431 5120985 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 6813 12420 31493 135519 350802 686980 1080708 1510261 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB +++++ +++++ 13833 58466 151375 300182 492445 654734 +++++ +++++ 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ +++++ +++++ 8872 37503 101953 206593 337483 453433 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 1541 6794 12213 33134 131705 338598 643029 1009984 1411923 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 6308 11028 28481 122258 308626 601403 948132 1325238 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 124 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane Ave DFB 2589 4753 11529 48251 122106 239384 375807 522887 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 6884 12765 33178 139566 348406 696059 1090230 1527793 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 1869 3984 10192 41067 100134 208398 313500 436785 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 7564 14930 37294 158135 397656 794708 1248175 1745247 1.00 2.00 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 4017 14904 28786 74548 305710 791155 1558816 2453857 3422834 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 7005 11724 29021 127802 325796 654311 1058276 1459268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave DFB 3579 6500 15804 62968 161526 322360 519398 716065 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 8289 14024 36478 144290 371408 720453 1142505 1570157 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 5569 11637 27497 111881 284612 560890 913572 1263367 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 4064 7418 19500 85045 219735 442108 718959 994298 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 3616 5912 14445 60214 154974 316106 499079 690159 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 17003 31983 82345 327328 831189 1624419 2599260 3554021 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 9223 18665 46324 184447 476816 915102 1474279 2004578 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 5151 10625 25733 108914 286131 568808 929412 1279270 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 2120 9059 17971 45661 183060 484613 948132 1510230 2077566 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 10400 45804 87017 223793 939704 2428374 4783893 7504852 9950024 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 5285 23810 43602 110873 466833 1210753 2416819 3921614 5406441 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 17304 33541 84628 360216 945512 1886331 3080454 4226631 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 2410 4275 10660 49043 129169 263003 446109 613724 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 31324 57244 148746 610310 1601454 3109566 5106365 6881199 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 7072 12892 33053 135512 347188 690763 1135272 1541345 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 125 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 1,1,2,2-Tetrachloroethane Ave DCB 3258 7169 18231 71670 177658 357760 598529 812983 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 2270 5288 12868 53399 135614 264488 444171 613409 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 36750 68894 176823 727359 1949080 3820722 6168362 8171167 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 21017 38120 97903 404326 1086544 2165096 3525867 4776401 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 24843 46048 121204 508814 1350744 2716376 4413867 5925708 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 24693 44629 117536 476349 1285442 2595965 4248167 5706737 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 24197 44012 114646 465442 1231564 2399839 3976419 5408653 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 24293 46692 115053 485753 1323232 2676625 4370483 5915680 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 34897 64452 172232 684971 1845685 3596271 5955880 7919600 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 15196 28192 68974 278836 743079 1492625 2463360 3287950 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 30451 57429 145300 590843 1590983 3156888 5179163 6891004 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 14514 28274 70862 274358 742273 1478508 2403110 3219268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 12130 22897 58683 245994 641352 1265519 2063725 2766492 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 25501 48990 128404 516775 1443162 2864857 4811328 6351852 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 517 1453 2909 11888 30736 61117 103368 138335 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 8084 14950 39749 157753 435120 899145 1475044 1901927 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Ave DCB 7491 13587 35512 128859 367053 682660 1206171 1489923 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 8454 16474 43237 175344 469003 960821 1657420 2236810 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 6507 11786 32167 129572 349729 697002 1171916 1518870 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 107966 264099 555702 857139 1182785 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 108560 264333 538799 854290 1167924 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 126 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172614

10829 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 461399 1119518 2322467 3587473 4898132 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 158632 400320 840950 1346757 1814509 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD



### FORM VI 8260B 

## 01/04/2013 Page 127 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD01 500-172615/2 22I1211A.D 2 Level STD02 500-172615/3 22I1211B.D 3 Level STD03 500-172615/4 22I1211C.D 4 Level STD04 500-172615/5 22I1211D.D 5 Level STD05 500-172615/6 22I1211E.D 6 Level STD06 500-172615/7 22I1211F.D 7 Level STD07 500-172615/8 22I1211G.D 8 Level STD08 500-172615/9 22I1211H.D 9 Level STD09 500-172615/10 22I1211I.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883Ave 9.9 0.5798 0.5632 0.5150 0.5364 0.0100 15.0 0.5420 Chloromethane 0.8256 0.7243 0.6267 0.6890Ave 7.9 0.7182 0.7230 0.6810 0.7012 0.1000 15.0 0.7111 Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130Ave 8.0 0.6517 0.6618 0.6041 0.6323 0.0100 15.0 0.6381 Bromomethane 0.1659 0.2203 0.1716 0.1726Ave 13.0 0.2077 0.2258 0.2110 0.2234 0.0100 15.0 0.1998 Chloroethane 0.4113 0.3289 0.3175 0.3315Ave 10.0 0.3369 0.3333 0.3044 0.3069 0.0100 15.0 0.3338 Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079Ave 6.3 0.9817 1.0066 0.9437 0.9571 0.0100 15.0 0.9993 Acetone +++++ +++++ 0.0554 0.0635Ave 7.8 0.0614 0.0672 0.0690 0.0671 0.0100 15.0 0.0639 Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319Ave 7.9 0.8320 0.8249 0.7635 0.7796 0.0100 15.0 0.8265 Acrolein 0.0331 0.0421 0.0314 0.0388Ave 13.0 0.0392 0.0429 0.0450 0.0450 0.0010 15.0 0.0397 1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008Ave 4.7 0.3938 0.3925 0.3935 0.4040 0.0100 15.0 0.4001 1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785Ave 6.7 0.4739 0.4784 0.4696 0.4829 0.0100 15.0 0.4862 Methylene Chloride +++++ 0.4011 0.3629 0.4004Ave 4.0 0.3719 0.3777 0.3682 0.3859 0.0100 15.0 0.3812 Carbon disulfide 1.5962 1.3713 1.3219 1.4559Ave 6.5 1.5313 1.5882 1.4767 1.4979 0.0100 15.0 1.4799



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 128 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Acetonitrile 0.0371 0.0333 0.0243 0.0295Ave 13.0 0.0262 0.0281 0.0299 0.0295 0.0010 15.0 0.0297 Acrylonitrile 0.0750 0.0912 0.0677 0.0823Ave 9.0 0.0764 0.0821 0.0846 0.0849 0.0010 15.0 0.0805 trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560Ave 4.4 0.4456 0.4511 0.4430 0.4552 0.0100 15.0 0.4499 2-Butanone (MEK) +++++ +++++ 0.0823 0.0919Ave 6.1 0.0908 0.0953 0.0973 0.0970 0.0100 15.0 0.0924 Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577Ave 5.4 0.7230 0.7592 0.7369 0.7564 0.0100 15.0 0.7369 Vinyl acetate +++++ 0.6129 0.5650 0.6423Ave 5.2 0.6107 0.6494 0.6338 0.6642 0.0100 15.0 0.6255 Tetrahydrofuran +++++ +++++ 0.0538 0.0611Ave 4.2 0.0583 0.0572 0.0571 0.0595 0.0100 15.0 0.0578 1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189Ave 6.2 0.8749 0.8925 0.8704 0.9084 0.1000 15.0 0.8857 2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515Ave 5.5 0.7243 0.7285 0.7200 0.7474 0.0100 15.0 0.7341 cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663Ave 6.4 0.4508 0.4630 0.4488 0.4652 0.0100 15.0 0.4554 Propionitrile 0.0230 0.0200 0.0163 0.0205Ave 10.0 0.0191 0.0201 0.0217 0.0219 0.0010 15.0 0.0203 Bromochloromethane 0.2191 0.1652 0.1606 0.1825Ave 10.0 0.1747 0.1747 0.1737 0.1772 0.0100 15.0 0.1785 Chloroform 0.7988 0.7465 0.6742 0.7604Ave 4.9 0.7195 0.7370 0.7200 0.7434 0.0100 15.0 0.7375 1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390Ave 4.7 0.7317 0.7368 0.7320 0.7583 0.0100 15.0 0.7394 Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871Ave 3.4 0.4883 0.4750 0.4767 0.4948 0.0100 15.0 0.4834 1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649Ave 6.9 0.6479 0.6478 0.6435 0.6685 0.0100 15.0 0.6488 Benzene 1.2306 1.3508 1.2179 1.1306 1.2550Ave 4.7 1.2277 1.2183 1.1975 1.2355 0.0100 15.0 1.2293 1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618Ave 5.6 0.3558 0.3552 0.3521 0.3644 0.0100 15.0 0.3536 4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561Ave 5.1 0.1535 0.1552 0.1604 0.1580 0.0100 15.0 0.1536 2-Hexanone +++++ +++++ 0.1035 0.1187Ave 7.3 0.1220 0.1257 0.1256 0.1271 0.0100 15.0 0.1204



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 129 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516Ave 4.9 0.3434 0.3325 0.3291 0.3406 0.0100 15.0 0.3450 1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264Ave 6.4 0.3130 0.3110 0.3089 0.3197 0.0100 15.0 0.3152 Dibromomethane 0.1457 0.1306 0.1153 0.1288Ave 6.9 0.1238 0.1238 0.1224 0.1261 0.0100 15.0 0.1271 Bromodichloromethane 0.3875 0.3507 0.3319 0.3726Ave 4.6 0.3533 0.3599 0.3552 0.3686 0.0100 15.0 0.3600 2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096Ave 3.2 0.1015 0.1078 0.1021 0.1054 0.0100 15.0 0.1054 cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222Ave 4.1 0.4033 0.4109 0.4067 0.4210 0.0100 15.0 0.4091 Toluene 0.9341 0.8388 0.7909 0.7458 0.8161Ave 6.2 0.8023 0.8060 0.7995 0.8258 0.0100 15.0 0.8177 trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412Ave 8.6 0.3304 0.3383 0.3448 0.3521 0.0100 15.0 0.3392 1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681Ave 7.7 0.1638 0.1667 0.1692 0.1728 0.0100 15.0 0.1723 Tetrachloroethene 0.5511 0.4482 0.4255 0.4568Ave 9.0 0.4446 0.4384 0.4251 0.4400 0.0100 15.0 0.4537 1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542Ave 4.9 0.3407 0.3413 0.3399 0.3540 0.0100 15.0 0.3491 Dibromochloromethane 0.2702 0.2371 0.2274 0.2693Ave 6.9 0.2630 0.2690 0.2675 0.2786 0.0100 15.0 0.2603 1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607Ave 10.0 0.1572 0.1634 0.1626 0.1665 0.0100 15.0 0.1651 Chlorobenzene 1.1305 1.0221 0.9605 1.0363Ave 5.3 0.9949 0.9884 0.9670 0.9960 0.3000 15.0 1.0120 1-Chlorohexane 0.7176 0.7070 0.6491 0.6984Ave 3.1 0.6765 0.6760 0.6835 0.6837 0.0100 15.0 0.6865 1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448Ave 5.0 0.3425 0.3461 0.3458 0.3585 0.0100 15.0 0.3400 Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796Ave 3.4 0.5801 0.5769 0.5619 0.5822 0.0100 15.0 0.5753 m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876Ave 4.5 1.4534 1.4554 1.3960 1.3942 0.0100 15.0 1.4275 o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780Ave 5.5 1.4493 1.4706 1.4590 1.5151 0.0100 15.0 1.4564 Styrene 1.1505 1.0719 0.9871 1.1405Ave 5.6 1.1318 1.1478 1.1460 1.1845 0.0100 15.0 1.1200



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 130 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1602 0.1366 0.1243 0.1553Ave 10.0 0.1546 0.1600 0.1660 0.1720 0.1000 15.0 0.1536 Isopropylbenzene 3.8233 3.3535 3.0653 3.4816Ave 7.4 3.1927 3.1639 3.1360 3.2790 0.0100 15.0 3.3119 Bromobenzene 0.8632 0.7552 0.6812 0.7730Ave 8.2 0.6922 0.7028 0.6972 0.7345 0.0100 15.0 0.7374 1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089Ave 6.0 0.3542 0.3640 0.3676 0.3874 0.3000 15.0 0.3844 1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046Ave 6.1 0.2704 0.2691 0.2728 0.2923 0.0100 15.0 0.2827 N-Propylbenzene 4.4856 4.0360 3.6439 4.1493Ave 6.5 3.8858 3.8875 3.7881 3.8936 0.0100 15.0 3.9712 4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065Ave 7.0 2.1662 2.2029 2.1653 2.2760 0.0100 15.0 2.2416 1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026Ave 5.8 2.6929 2.7638 2.7107 2.8237 0.0100 15.0 2.7652 2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174Ave 6.4 2.5627 2.6413 2.6089 2.7193 0.0100 15.0 2.6625 tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552Ave 7.3 2.4553 2.4418 2.4420 2.5773 0.0100 15.0 2.5582 1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710Ave 6.3 2.6381 2.7234 2.6840 2.8189 0.0100 15.0 2.7134 sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075Ave 5.8 3.6796 3.6591 3.6577 3.7738 0.0100 15.0 3.7828 1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907Ave 8.4 1.4814 1.5187 1.5128 1.5667 0.0100 15.0 1.5748 p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705Ave 6.4 3.1719 3.2121 3.1807 3.2836 0.0100 15.0 3.2868 1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651Ave 6.9 1.4798 1.5043 1.4758 1.5340 0.0100 15.0 1.5559 1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033Ave 6.4 1.2786 1.2876 1.2674 1.3183 0.0100 15.0 1.3233 n-Butylbenzene 3.1126 2.8700 2.6461 2.9480Ave 4.7 2.8772 2.9149 2.9548 3.0267 0.0100 15.0 2.9188 1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678Ave 12.0 0.0613 0.0622 0.0635 0.0659 0.0100 15.0 0.0661 1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999Ave 5.3 0.8675 0.9149 0.9059 0.9063 0.0100 15.0 0.8970 Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351Ave 9.3 0.7318 0.6946 0.7407 0.7100 0.0100 15.0 0.7568



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 131 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.0319 0.9651 0.8910 1.0003Ave 5.7 0.9350 0.9776 1.0179 1.0659 0.0100 15.0 0.9856 1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392Ave 5.4 0.6972 0.7092 0.7197 0.7238 0.0100 15.0 0.7171 Dibromofluoromethane 0.4088Ave 3.6 0.3747 0.4105 0.3974 0.4034 0.0100 15.0 0.3990 1,2-Dichloroethane-d4 (Surr) 0.2898Ave 2.8 0.2681 0.2786 0.2783 0.2818 0.0100 15.0 0.2793 Toluene-d8 (Surr) 1.2317Ave 3.0 1.1353 1.2008 1.1689 1.1817 0.0100 15.0 1.1837 4-Bromofluorobenzene (Surr) 0.5022Ave 2.5 0.4792 0.5117 0.5010 0.5085 0.0100 15.0 0.5005



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/04/2013 Page 132 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD01 500-172615/2 22I1211A.D Level2 STD02 500-172615/3 22I1211B.D Level3 STD03 500-172615/4 22I1211C.D Level4 STD04 500-172615/5 22I1211D.D Level5 STD05 500-172615/6 22I1211E.D Level6 STD06 500-172615/7 22I1211F.D Level7 STD07 500-172615/8 22I1211G.D Level8 STD08 500-172615/9 22I1211H.D Level9 STD09 500-172615/10 22I1211I.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 8283 14019 34084 128973 408706 762307 1110898 1572519 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 10611 19121 44725 181982 506217 978702 1468998 2055922 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 2072 9537 16111 40052 161885 459341 895799 1302949 1853836 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Ave PFB 2132 5817 12250 45578 146376 305638 455210 654905 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 5286 8684 22657 87550 237436 451232 656528 899737 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 14493 27342 66676 266205 691989 1362610 2035639 2806119 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Ave PFB +++++ +++++ 3957 16764 43292 90934 148822 196769 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 12483 22039 55227 219705 586466 1116585 1646914 2285626 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 16997 44508 89671 410157 1104663 2325112 3885554 5276134 40.0 80.0 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 5414 11300 26186 105858 277562 531364 848798 1184587 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 7210 13042 32193 126370 334028 647515 1013020 1415755 1.00 2.00 5.00 20.0 50.0 100 150 200 Methylene Chloride Ave PFB +++++ 10588 25901 105736 262156 511318 794285 1131397 +++++ 2.00 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 20516 36202 94343 384523 1079379 2149891 3185269 4391617 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 3815 7023 13902 62328 147511 304606 515971 692080 8.00 16.0 40.0 160 400 800 1200 1600



### FORM VI 8260B 

## 01/04/2013 Page 133 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Acrylonitrile Ave PFB 7715 19252 38635 173831 430688 889127 1460725 1990459 8.00 16.0 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 6143 12190 29175 120435 314119 610637 955652 1334459 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB +++++ +++++ 5877 24272 64002 128968 209900 284336 +++++ +++++ 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 10253 18092 48485 200118 509651 1027632 1589481 2217547 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB +++++ 16181 40320 169641 430488 879019 1367143 1947324 +++++ 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB +++++ +++++ 3843 16127 41123 77379 123251 174315 +++++ +++++ 5.00 20.0 50.0 100 150 200 1,1-Dichloroethane Ave PFB 12660 21793 57801 242674 616675 1208102 1877461 2663163 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 10444 18966 47829 198464 510518 986077 1552961 2191135 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 6562 11093 29875 123154 317732 626799 968176 1363967 1.00 2.00 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 3274 5826 13049 61580 150541 311165 533857 726579 8.00 16.0 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 2816 4362 11462 48207 123109 236461 374570 519660 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 10267 19708 48119 200834 507134 997634 1553050 2179601 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 10394 19135 48811 195166 515733 997347 1578989 2223267 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 8845 18161 44839 182447 481514 918644 1463204 2051034 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 9406 15734 42090 175593 456667 876844 1388026 1960009 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 5292 24000 44324 113004 470128 1210657 2356179 3675431 5120985 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 6813 12420 31493 135519 350802 686980 1080708 1510261 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB +++++ +++++ 13833 58466 151375 300182 492445 654734 +++++ +++++ 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ +++++ +++++ 8872 37503 101953 206593 337483 453433 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 1541 6794 12213 33134 131705 338598 643029 1009984 1411923 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 6308 11028 28481 122258 308626 601403 948132 1325238 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 134 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane Ave DFB 2589 4753 11529 48251 122106 239384 375807 522887 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 6884 12765 33178 139566 348406 696059 1090230 1527793 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 1869 3984 10192 41067 100134 208398 313500 436785 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 7564 14930 37294 158135 397656 794708 1248175 1745247 1.00 2.00 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 4017 14904 28786 74548 305710 791155 1558816 2453857 3422834 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 7005 11724 29021 127802 325796 654311 1058276 1459268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave DFB 3579 6500 15804 62968 161526 322360 519398 716065 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 8289 14024 36478 144290 371408 720453 1142505 1570157 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 5569 11637 27497 111881 284612 560890 913572 1263367 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 4064 7418 19500 85045 219735 442108 718959 994298 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 3616 5912 14445 60214 154974 316106 499079 690159 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 17003 31983 82345 327328 831189 1624419 2599260 3554021 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 9223 18665 46324 184447 476816 915102 1474279 2004578 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 5151 10625 25733 108914 286131 568808 929412 1279270 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 2120 9059 17971 45661 183060 484613 948132 1510230 2077566 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 10400 45804 87017 223793 939704 2428374 4783893 7504852 9950024 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 5285 23810 43602 110873 466833 1210753 2416819 3921614 5406441 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 17304 33541 84628 360216 945512 1886331 3080454 4226631 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 2410 4275 10660 49043 129169 263003 446109 613724 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 31324 57244 148746 610310 1601454 3109566 5106365 6881199 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 7072 12892 33053 135512 347188 690763 1135272 1541345 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 135 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 1,1,2,2-Tetrachloroethane Ave DCB 3258 7169 18231 71670 177658 357760 598529 812983 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 2270 5288 12868 53399 135614 264488 444171 613409 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 36750 68894 176823 727359 1949080 3820722 6168362 8171167 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 21017 38120 97903 404326 1086544 2165096 3525867 4776401 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 24843 46048 121204 508814 1350744 2716376 4413867 5925708 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 24693 44629 117536 476349 1285442 2595965 4248167 5706737 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 24197 44012 114646 465442 1231564 2399839 3976419 5408653 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 24293 46692 115053 485753 1323232 2676625 4370483 5915680 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 34897 64452 172232 684971 1845685 3596271 5955880 7919600 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 15196 28192 68974 278836 743079 1492625 2463360 3287950 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 30451 57429 145300 590843 1590983 3156888 5179163 6891004 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 14514 28274 70862 274358 742273 1478508 2403110 3219268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 12130 22897 58683 245994 641352 1265519 2063725 2766492 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 25501 48990 128404 516775 1443162 2864857 4811328 6351852 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 517 1453 2909 11888 30736 61117 103368 138335 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 8084 14950 39749 157753 435120 899145 1475044 1901927 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Ave DCB 7491 13587 35512 128859 367053 682660 1206171 1489923 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 8454 16474 43237 175344 469003 960821 1657420 2236810 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 6507 11786 32167 129572 349729 697002 1171916 1518870 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 107966 264099 555702 857139 1182785 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 108560 264333 538799 854290 1167924 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/04/2013 Page 136 of 332

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53342-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 461399 1119518 2322467 3587473 4898132 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 158632 400320 840950 1346757 1814509 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD



### FORM VI 8260B 

## 01/04/2013 Page 137 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 11/19/2012 17:14 11/19/2012 12:14 11/19/2012 14:09 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4279 0.4665 0.0100 45.9 50.0 -8.3 25.0 Ave Chloromethane 0.5246 0.5798 0.1000 45.2 50.0 -9.5 25.0 Ave Vinyl chloride 0.5248 0.5072 0.0100 51.7 50.0 3.5 25.0 Ave Bromomethane 0.1523 0.0100 47.2 50.0 -5.7 25.0 Lin2 Chloroethane 0.2426 0.2641 0.0100 45.9 50.0 -8.2 25.0 Ave Trichlorofluoromethane 0.5702 0.5875 0.0100 48.5 50.0 -2.9 25.0 Ave Acrolein 0.0673 0.0010 2080 2000 4.0 25.0 Lin2 1,1-Dichloroethene 0.3758 0.3748 0.0100 50.1 50.0 0.2 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.3311 0.3898 0.0100 42.5 50.0 -15.1 25.0 Ave Acetone 0.1027 0.0100 46.9 50.0 -6.2 25.0 Lin1 Carbon disulfide 1.296 1.284 0.0100 50.4 50.0 0.9 25.0 Ave Acetonitrile 0.0367 0.0330 0.0010 446 400 11.4 25.0 Ave Methylene Chloride 0.4290 0.4276 0.0100 50.2 50.0 0.3 25.0 Ave Acrylonitrile 0.1268 0.0010 407 400 1.7 25.0 Lin2 trans-1,2-Dichloroethene 0.4669 0.4413 0.0100 52.9 50.0 5.8 25.0 Ave Methyl tert-butyl ether 1.023 1.124 0.0100 45.5 50.0 -9.0 25.0 Ave 1,1-Dichloroethane 0.8721 0.8704 0.1000 50.1 50.0 0.2 25.0 Ave Vinyl acetate 0.8804 0.8347 0.0100 52.7 50.0 5.5 25.0 Ave 2,2-Dichloropropane 0.4986 0.4764 0.0100 52.3 50.0 4.7 25.0 Ave cis-1,2-Dichloroethene 0.4840 0.4787 0.0100 50.6 50.0 1.1 25.0 Ave 2-Butanone (MEK) 0.1524 0.1710 0.0100 44.6 50.0 -10.9 25.0 Ave Propionitrile 0.0316 0.0316 0.0010 399 400 -0.2 25.0 Ave Bromochloromethane 0.1702 0.1881 0.0100 45.2 50.0 -9.5 25.0 Ave Tetrahydrofuran 0.1042 0.0100 48.0 50.0 -4.0 25.0 Lin2 Chloroform 0.7748 0.7669 0.0100 50.5 50.0 1.0 25.0 Ave 1,1,1-Trichloroethane 0.6555 0.6244 0.0100 52.5 50.0 5.0 25.0 Ave Carbon tetrachloride 0.3724 0.3568 0.0100 52.2 50.0 4.4 25.0 Ave 1,1-Dichloropropene 0.6306 0.6354 0.0100 49.6 50.0 -0.8 25.0 Ave Benzene 1.216 1.203 0.0100 50.5 50.0 1.1 25.0 Ave 1,2-Dichloroethane 0.3697 0.3833 0.0100 48.2 50.0 -3.5 25.0 Ave Trichloroethene 0.2917 0.2856 0.0100 51.1 50.0 2.1 25.0 Ave 1,2-Dichloropropane 0.2959 0.2993 0.0100 49.4 50.0 -1.1 25.0 Ave Dibromomethane 0.1397 0.1425 0.0100 49.0 50.0 -2.0 25.0 Ave Bromodichloromethane 0.3379 0.3449 0.0100 49.0 50.0 -2.0 25.0 Ave 2-Chloroethyl vinyl ether 0.1258 0.1341 0.0100 46.9 50.0 -6.2 25.0 Ave cis-1,3-Dichloropropene 0.4011 0.4015 0.0100 53.7 53.8 -0.1 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2120 0.2272 0.0100 46.7 50.0 -6.7 25.0 Ave Toluene 0.7132 0.7155 0.0100 49.8 50.0 -0.3 25.0 Ave trans-1,3-Dichloropropene 0.3348 0.3375 0.0100 48.2 48.6 -0.8 25.0 Ave 1,1,2-Trichloroethane 0.2675 0.2749 0.0100 48.6 50.0 -2.7 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 138 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 11/19/2012 17:14 11/19/2012 12:14 11/19/2012 14:09 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Tetrachloroethene 0.3914 0.3741 0.0100 52.3 50.0 4.6 25.0 Ave 1,3-Dichloropropane 0.4541 0.4540 0.0100 50.0 50.0 0.0 25.0 Ave 2-Hexanone 0.1831 0.1954 0.0100 46.9 50.0 -6.3 25.0 Ave Dibromochloromethane 0.2483 0.2462 0.0100 50.4 50.0 0.9 25.0 Ave 1,2-Dibromoethane 0.1719 0.1798 0.0100 47.8 50.0 -4.4 25.0 Ave 1-Chlorohexane 0.5208 0.5697 0.0100 45.7 50.0 -8.6 25.0 Ave Chlorobenzene 0.8647 0.9049 0.3000 47.8 50.0 -4.4 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3084 0.3090 0.0100 49.9 50.0 -0.2 25.0 Ave Ethylbenzene 0.5301 0.5284 0.0100 50.2 50.0 0.3 25.0 Ave m&p-Xylene 1.283 1.285 0.0100 99.8 100 -0.2 25.0 Ave o-Xylene 1.295 1.348 0.0100 48.0 50.0 -4.0 25.0 Ave Styrene 1.029 1.015 0.0100 50.7 50.0 1.4 25.0 Ave Bromoform 0.1401 0.1432 0.1000 48.9 50.0 -2.2 25.0 Ave Isopropylbenzene 3.211 3.252 0.0100 49.4 50.0 -1.3 25.0 Ave Bromobenzene 0.7556 0.7222 0.0100 52.3 50.0 4.6 25.0 Ave 1,1,2,2-Tetrachloroethane 0.5584 0.5589 0.3000 50.0 50.0 -0.1 25.0 Ave 1,2,3-Trichloropropane 0.1680 0.1732 0.0100 48.5 50.0 -3.0 25.0 Ave N-Propylbenzene 3.806 3.879 0.0100 49.1 50.0 -1.9 25.0 Ave 2-Chlorotoluene 2.300 2.312 0.0100 49.7 50.0 -0.6 25.0 Ave 1,3,5-Trimethylbenzene 2.896 2.676 0.0100 54.1 50.0 8.2 25.0 Ave 4-Chlorotoluene 2.597 2.685 0.0100 48.4 50.0 -3.3 25.0 Ave tert-Butylbenzene 2.273 2.285 0.0100 49.7 50.0 -0.5 25.0 Ave 1,2,4-Trimethylbenzene 2.842 2.723 0.0100 52.2 50.0 4.4 25.0 Ave sec-Butylbenzene 3.410 3.457 0.0100 49.3 50.0 -1.4 25.0 Ave 1,3-Dichlorobenzene 1.361 1.415 0.0100 48.1 50.0 -3.8 25.0 Ave p-Isopropyltoluene 2.828 2.902 0.0100 48.7 50.0 -2.5 25.0 Ave 1,4-Dichlorobenzene 1.440 1.398 0.0100 51.5 50.0 3.0 25.0 Ave n-Butylbenzene 2.940 2.831 0.0100 51.9 50.0 3.8 25.0 Ave 1,2-Dichlorobenzene 1.205 1.252 0.0100 48.1 50.0 -3.8 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0784 0.0839 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2,4-Trichlorobenzene 0.8024 0.8500 0.0100 47.2 50.0 -5.6 25.0 Ave Hexachlorobutadiene 0.5223 0.0100 51.7 50.0 3.4 25.0 Qua1 Naphthalene 1.356 0.0100 47.5 50.0 -4.9 25.0 Lin2 1,2,3-Trichlorobenzene 0.5963 0.0100 45.8 50.0 -8.3 25.0 Qua2 Dibromofluoromethane 0.3997 0.3958 0.0100 43.7 43.3 1.0 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3112 0.3196 0.0100 42.1 43.3 -2.6 25.0 Ave Toluene-d8 (Surr) 1.099 1.017 0.0100 46.8 43.3 8.1 25.0 Ave 4-Bromofluorobenzene (Surr) 0.5002 0.4856 0.0100 44.6 43.3 3.0 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 139 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 11/19/2012 17:14 11/19/2012 14:32 11/19/2012 16:28 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3493 0.4262 0.0100 41.0 50.0 -18.0 25.0 Ave Iodomethane 0.6405 0.5737 0.0100 55.8 50.0 11.6 25.0 Ave Methyl acetate 0.2295 0.3675 0.0100 31.2 50.0 -37.6* 25.0 Ave Hexane 0.6708 0.7834 0.0100 42.8 50.0 -14.4 25.0 Ave Cyclohexane 0.8544 0.0100 46.7 50.0 -6.6 25.0 Lin2 Heptane 0.5269 0.5932 0.0100 44.4 50.0 -11.2 25.0 Ave Methylcyclohexane 0.5154 0.5531 0.0100 46.6 50.0 -6.8 25.0 Ave 1,3,5-Trichlorobenzene 1.063 1.012 0.0100 52.5 50.0 5.0 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 140 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 12/20/2012 08:13 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173515/2

DB624 TestAmerica Chicago

Lab File ID:16C1220.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.3486 0.4665 0.0100 37.4 50.0 -25.3 50.0 Ave Chloromethane 0.4665 0.5798 0.1000 40.2 50.0 -19.5 50.0 Ave Vinyl chloride 0.4435 0.5072 0.0100 43.7 50.0 -12.6 20.0 Ave Bromomethane 0.1301 0.0100 40.0 50.0 -20.0 50.0 Lin2 Chloroethane 0.2221 0.2641 0.0100 42.1 50.0 -15.9 50.0 Ave Trichlorofluoromethane 0.5691 0.5875 0.0100 48.4 50.0 -3.1 50.0 Ave Acrolein 0.0560 0.0010 1722 2000 -13.9 50.0 Lin2 1,1-Dichloroethene 0.3869 0.3748 0.0100 51.6 50.0 3.2 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.3979 0.3898 0.0100 51.0 50.0 2.1 50.0 Ave Acetone 0.1062 0.0100 48.7 50.0 -2.6 50.0 Lin1 Carbon disulfide 1.102 1.284 0.0100 42.9 50.0 -14.2 50.0 Ave Acetonitrile 0.0361 0.0330 0.0010 438 400 9.5 50.0 Ave Methylene Chloride 0.4443 0.4276 0.0100 51.9 50.0 3.9 50.0 Ave Acrylonitrile 0.1335 0.0010 429 400 7.2 50.0 Lin2 Methyl tert-butyl ether 1.185 1.124 0.0100 52.7 50.0 5.4 50.0 Ave trans-1,2-Dichloroethene 0.4532 0.4413 0.0100 51.4 50.0 2.7 50.0 Ave 1,1-Dichloroethane 0.8926 0.8704 0.1000 51.3 50.0 2.6 50.0 Ave Vinyl acetate 0.8694 0.8347 0.0100 52.1 50.0 4.2 50.0 Ave 2,2-Dichloropropane 0.4711 0.4764 0.0100 49.4 50.0 -1.1 50.0 Ave cis-1,2-Dichloroethene 0.4912 0.4787 0.0100 51.3 50.0 2.6 50.0 Ave 2-Butanone (MEK) 0.1682 0.1710 0.0100 49.2 50.0 -1.7 50.0 Ave Propionitrile 0.0339 0.0316 0.0010 429 400 7.1 50.0 Ave Bromochloromethane 0.2007 0.1881 0.0100 53.4 50.0 6.7 50.0 Ave Tetrahydrofuran 0.1171 0.0100 54.1 50.0 8.2 50.0 Lin2 Chloroform 0.8018 0.7669 0.0100 52.3 50.0 4.5 20.0 Ave 1,1,1-Trichloroethane 0.6395 0.6244 0.0100 51.2 50.0 2.4 50.0 Ave Carbon tetrachloride 0.3735 0.3568 0.0100 52.4 50.0 4.7 50.0 Ave 1,1-Dichloropropene 0.6705 0.6354 0.0100 52.8 50.0 5.5 50.0 Ave Benzene 1.278 1.203 0.0100 53.1 50.0 6.2 50.0 Ave 1,2-Dichloroethane 0.4049 0.3833 0.0100 52.8 50.0 5.6 50.0 Ave Trichloroethene 0.3046 0.2856 0.0100 53.3 50.0 6.7 50.0 Ave 1,2-Dichloropropane 0.3180 0.2993 0.0100 53.1 50.0 6.3 20.0 Ave Dibromomethane 0.1520 0.1425 0.0100 53.3 50.0 6.7 50.0 Ave Bromodichloromethane 0.3668 0.3449 0.0100 53.2 50.0 6.3 50.0 Ave 2-Chloroethyl vinyl ether 0.1474 0.1341 0.0100 55.0 50.0 9.9 50.0 Ave cis-1,3-Dichloropropene 0.4396 0.4015 0.0100 54.8 50.0 9.5 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2357 0.2272 0.0100 51.9 50.0 3.8 50.0 Ave Toluene 0.7651 0.7155 0.0100 53.5 50.0 6.9 20.0 Ave trans-1,3-Dichloropropene 0.3738 0.3375 0.0100 55.4 50.0 10.7 50.0 Ave 1,1,2-Trichloroethane 0.3071 0.2749 0.0100 55.9 50.0 11.7 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 141 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 12/20/2012 08:13 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173515/2

DB624 TestAmerica Chicago

Lab File ID:16C1220.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Tetrachloroethene 0.3971 0.3741 0.0100 53.1 50.0 6.2 50.0 Ave 1,3-Dichloropropane 0.5083 0.4540 0.0100 56.0 50.0 12.0 50.0 Ave 2-Hexanone 0.2012 0.1954 0.0100 51.5 50.0 3.0 50.0 Ave Dibromochloromethane 0.2737 0.2462 0.0100 55.6 50.0 11.2 50.0 Ave 1,2-Dibromoethane 0.1949 0.1798 0.0100 54.2 50.0 8.4 50.0 Ave 1-Chlorohexane 0.6029 0.5697 0.0100 52.9 50.0 5.8 50.0 Ave Chlorobenzene 0.9568 0.9049 0.3000 52.9 50.0 5.7 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3244 0.3090 0.0100 52.5 50.0 5.0 50.0 Ave Ethylbenzene 0.5537 0.5284 0.0100 52.4 50.0 4.8 20.0 Ave m&p-Xylene 1.367 1.285 0.0100 106 100 6.4 50.0 Ave o-Xylene 1.392 1.348 0.0100 51.6 50.0 3.2 50.0 Ave Styrene 1.080 1.015 0.0100 53.2 50.0 6.4 50.0 Ave Bromoform 0.1571 0.1432 0.1000 54.9 50.0 9.7 50.0 Ave Isopropylbenzene 3.479 3.252 0.0100 53.5 50.0 7.0 50.0 Ave Bromobenzene 0.8020 0.7222 0.0100 55.5 50.0 11.0 50.0 Ave 1,1,2,2-Tetrachloroethane 0.6209 0.5589 0.3000 55.5 50.0 11.1 50.0 Ave 1,2,3-Trichloropropane 0.1866 0.1732 0.0100 53.9 50.0 7.7 50.0 Ave N-Propylbenzene 4.142 3.879 0.0100 53.4 50.0 6.8 50.0 Ave 2-Chlorotoluene 2.443 2.312 0.0100 52.8 50.0 5.6 50.0 Ave 1,3,5-Trimethylbenzene 2.829 2.676 0.0100 52.9 50.0 5.7 50.0 Ave 4-Chlorotoluene 2.817 2.685 0.0100 52.5 50.0 4.9 50.0 Ave tert-Butylbenzene 2.355 2.285 0.0100 51.5 50.0 3.1 50.0 Ave 1,2,4-Trimethylbenzene 2.815 2.723 0.0100 51.7 50.0 3.4 50.0 Ave sec-Butylbenzene 3.590 3.457 0.0100 51.9 50.0 3.9 50.0 Ave 1,3-Dichlorobenzene 1.438 1.415 0.0100 50.8 50.0 1.7 50.0 Ave p-Isopropyltoluene 2.997 2.902 0.0100 51.7 50.0 3.3 50.0 Ave 1,4-Dichlorobenzene 1.451 1.398 0.0100 51.9 50.0 3.7 50.0 Ave n-Butylbenzene 2.838 2.831 0.0100 50.1 50.0 0.2 50.0 Ave 1,2-Dichlorobenzene 1.297 1.252 0.0100 51.8 50.0 3.6 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0822 0.0839 0.0100 49.0 50.0 -2.0 50.0 Ave 1,2,4-Trichlorobenzene 0.7715 0.8500 0.0100 45.4 50.0 -9.2 50.0 Ave Hexachlorobutadiene 0.4734 0.0100 46.2 50.0 -7.5 50.0 Qua1 Naphthalene 1.296 0.0100 45.4 50.0 -9.2 50.0 Lin2 1,2,3-Trichlorobenzene 0.5295 0.0100 40.3 50.0 -19.4 50.0 Qua2 Dibromofluoromethane 0.4147 0.3958 0.0100 45.3 43.3 4.8 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3282 0.3196 0.0100 44.4 43.3 2.7 50.0 Ave Toluene-d8 (Surr) 1.132 1.017 0.0100 48.2 43.3 11.3 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4940 0.4856 0.0100 44.0 43.3 1.7 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 142 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 12/20/2012 08:36 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173515/3

DB624 TestAmerica Chicago

Lab File ID:16D1220.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.4135 0.3958 0.0100 45.2 43.3 4.5 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3351 0.3196 0.0100 45.4 43.3 4.8 50.0 Ave Toluene-d8 (Surr) 1.102 1.017 0.0100 46.9 43.3 8.3 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4948 0.4856 0.0100 44.1 43.3 1.9 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 143 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS16 12/20/2012 08:36 11/19/2012 14:32 11/19/2012 16:28 CCV 500-173515/3

DB624 TestAmerica Chicago

Lab File ID:16D1220.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.4585 0.5997 0.0100 38.2 50.0 -23.5 50.0 Ave Ethyl ether 0.4190 0.4262 0.0100 49.2 50.0 -1.7 50.0 Ave Iodomethane 0.5439 0.5737 0.0100 94.8 100 -5.2 50.0 Ave 3-Chloropropene 0.2242 0.2319 0.0100 96.7 100 -3.3 50.0 Ave Methyl acetate 0.4295 0.3675 0.0100 58.4 50.0 16.9 50.0 Ave Hexane 0.7208 0.7834 0.0100 46.0 50.0 -8.0 50.0 Ave Isopropyl ether 1.706 1.776 0.0100 48.0 50.0 -3.9 50.0 Ave 2-Chloro-1,3-butadiene 0.8271 0.8947 0.0100 46.2 50.0 -7.6 50.0 Ave Ethyl acetate 0.3555 0.3031 0.0100 587 500 17.3 50.0 Ave Methacrylonitrile 0.2490 0.2264 0.0100 110 100 10.0 50.0 Ave Cyclohexane 0.8487 0.0100 46.4 50.0 -7.3 50.0 Lin2 Isobutyl alcohol 0.0129 0.0107 0.0010 4851 4000 21.3 50.0 Ave 2,2,4-Trimethylpentane 1.312 1.405 0.0100 46.7 50.0 -6.6 50.0 Ave Heptane 0.5591 0.5932 0.0100 47.1 50.0 -5.8 50.0 Ave n-Butyl alcohol 0.0077 0.0063 0.0010 4909 4000 22.7 50.0 Ave Methylcyclohexane 0.5201 0.5531 0.0100 47.0 50.0 -6.0 50.0 Ave Methyl methacrylate 0.2461 0.2123 0.0100 116 100 15.9 50.0 Ave 2-Nitropropane 0.0913 0.0771 0.0100 4736 4000 18.4 50.0 Ave Ethyl methacrylate 0.4203 0.3579 0.0100 117 100 17.4 50.0 Ave Cyclohexanone 0.0584 0.0100 4789 4000 19.7 50.0 Lin1 trans-1,4-Dichloro-2-butene 0.1021 0.0868 0.0100 118 100 17.6 50.0 Ave Pentachloroethane 0.2210 0.2111 0.0100 105 100 4.7 50.0 Ave 1,3,5-Trichlorobenzene 0.9797 1.012 0.0100 48.4 50.0 -3.2 50.0 Ave 2-Methylnaphthalene 0.5865 0.0100 44.6 50.0 -10.9 50.0 Qua2



### FORM VII 8260B 

## 01/04/2013 Page 144 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172614/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4239 0.5420 0.0100 39.1 50.0 -21.8 25.0 Ave Chloromethane 0.5561 0.7111 0.1000 39.1 50.0 -21.8 25.0 Ave Vinyl chloride 0.5920 0.6381 0.0100 46.4 50.0 -7.2 25.0 Ave Bromomethane 0.1541 0.1998 0.0100 38.6 50.0 -22.9 25.0 Ave Chloroethane 0.2911 0.3338 0.0100 43.6 50.0 -12.8 25.0 Ave Dichlorofluoromethane 0.8378 0.999 0.0100 41.9 50.0 -16.2 25.0 Ave Trichlorofluoromethane 0.7409 0.8265 0.0100 44.8 50.0 -10.4 25.0 Ave Acrolein 0.0406 0.0397 0.0010 2044 2000 2.2 25.0 Ave 1,1-Dichloroethene 0.3815 0.4001 0.0100 47.7 50.0 -4.7 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.4598 0.4862 0.0100 47.3 50.0 -5.4 25.0 Ave Acetone 0.0621 0.0639 0.0100 48.5 50.0 -2.9 25.0 Ave Carbon disulfide 1.369 1.480 0.0100 46.3 50.0 -7.5 25.0 Ave Acetonitrile 0.0292 0.0297 0.0010 393 400 -1.7 25.0 Ave Methylene Chloride 0.3602 0.3812 0.0100 47.2 50.0 -5.5 25.0 Ave Acrylonitrile 0.0797 0.0805 0.0010 396 400 -1.0 25.0 Ave trans-1,2-Dichloroethene 0.4398 0.4499 0.0100 48.9 50.0 -2.3 25.0 Ave Methyl tert-butyl ether 0.6905 0.7369 0.0100 46.9 50.0 -6.3 25.0 Ave 1,1-Dichloroethane 0.8456 0.8857 0.1000 47.7 50.0 -4.5 25.0 Ave Vinyl acetate 0.6214 0.6255 0.0100 49.7 50.0 -0.6 25.0 Ave 2,2-Dichloropropane 0.6853 0.7341 0.0100 46.7 50.0 -6.6 25.0 Ave cis-1,2-Dichloroethene 0.4436 0.4554 0.0100 48.7 50.0 -2.6 25.0 Ave 2-Butanone (MEK) 0.0837 0.0924 0.0100 45.3 50.0 -9.4 25.0 Ave Propionitrile 0.0211 0.0203 0.0010 414 400 3.5 25.0 Ave Bromochloromethane 0.1638 0.1785 0.0100 45.9 50.0 -8.2 25.0 Ave Tetrahydrofuran 0.0548 0.0578 0.0100 47.3 50.0 -5.3 25.0 Ave Chloroform 0.7135 0.7375 0.0100 48.4 50.0 -3.3 25.0 Ave 1,1,1-Trichloroethane 0.7299 0.7394 0.0100 49.4 50.0 -1.3 25.0 Ave Carbon tetrachloride 0.4652 0.4834 0.0100 48.1 50.0 -3.8 25.0 Ave 1,1-Dichloropropene 0.6138 0.6488 0.0100 47.3 50.0 -5.4 25.0 Ave Benzene 1.148 1.229 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichloroethane 0.3244 0.3536 0.0100 45.9 50.0 -8.3 25.0 Ave Trichloroethene 0.3212 0.3450 0.0100 46.6 50.0 -6.9 25.0 Ave 1,2-Dichloropropane 0.2970 0.3152 0.0100 47.1 50.0 -5.8 25.0 Ave Dibromomethane 0.1149 0.1271 0.0100 45.2 50.0 -9.6 25.0 Ave Bromodichloromethane 0.3216 0.3600 0.0100 44.7 50.0 -10.7 25.0 Ave 2-Chloroethyl vinyl ether 0.0957 0.1054 0.0100 45.4 50.0 -9.2 25.0 Ave cis-1,3-Dichloropropene 0.3814 0.4091 0.0100 50.1 53.8 -6.8 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1404 0.1536 0.0100 45.7 50.0 -8.6 25.0 Ave Toluene 0.7569 0.8177 0.0100 46.3 50.0 -7.4 25.0 Ave trans-1,3-Dichloropropene 0.3107 0.3392 0.0100 44.5 48.6 -8.4 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 145 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172614/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1573 0.1723 0.0100 45.6 50.0 -8.7 25.0 Ave Tetrachloroethene 0.4260 0.4537 0.0100 47.0 50.0 -6.1 25.0 Ave 1,3-Dichloropropane 0.3223 0.3491 0.0100 46.2 50.0 -7.7 25.0 Ave 2-Hexanone 0.1135 0.1204 0.0100 47.1 50.0 -5.7 25.0 Ave Dibromochloromethane 0.2454 0.2603 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dibromoethane 0.1486 0.1651 0.0100 45.0 50.0 -10.0 25.0 Ave Chlorobenzene 0.9004 1.012 0.3000 44.5 50.0 -11.0 25.0 Ave 1-Chlorohexane 0.6546 0.6865 0.0100 47.7 50.0 -4.6 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3297 0.3400 0.0100 48.5 50.0 -3.0 25.0 Ave Ethylbenzene 0.5498 0.5753 0.0100 47.8 50.0 -4.4 25.0 Ave m&p-Xylene 1.339 1.427 0.0100 93.8 100 -6.2 25.0 Ave o-Xylene 1.295 1.456 0.0100 44.5 50.0 -11.1 25.0 Ave Styrene 1.076 1.120 0.0100 48.0 50.0 -3.9 25.0 Ave Bromoform 0.1521 0.1536 0.1000 49.5 50.0 -1.0 25.0 Ave Isopropylbenzene 2.951 3.312 0.0100 44.6 50.0 -10.9 25.0 Ave Bromobenzene 0.6901 0.7374 0.0100 46.8 50.0 -6.4 25.0 Ave 1,1,2,2-Tetrachloroethane 0.3650 0.3844 0.3000 47.5 50.0 -5.1 25.0 Ave 1,2,3-Trichloropropane 0.2697 0.2827 0.0100 47.7 50.0 -4.6 25.0 Ave N-Propylbenzene 3.489 3.971 0.0100 43.9 50.0 -12.2 25.0 Ave 4-Chlorotoluene 2.042 2.242 0.0100 45.5 50.0 -8.9 25.0 Ave 1,3,5-Trimethylbenzene 2.737 2.765 0.0100 49.5 50.0 -1.0 25.0 Ave 2-Chlorotoluene 2.355 2.663 0.0100 44.2 50.0 -11.6 25.0 Ave tert-Butylbenzene 2.302 2.558 0.0100 45.0 50.0 -10.0 25.0 Ave 1,2,4-Trimethylbenzene 2.637 2.713 0.0100 48.6 50.0 -2.8 25.0 Ave sec-Butylbenzene 3.418 3.783 0.0100 45.2 50.0 -9.6 25.0 Ave 1,3-Dichlorobenzene 1.369 1.575 0.0100 43.5 50.0 -13.1 25.0 Ave p-Isopropyltoluene 2.935 3.287 0.0100 44.7 50.0 -10.7 25.0 Ave 1,4-Dichlorobenzene 1.454 1.556 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichlorobenzene 1.190 1.323 0.0100 45.0 50.0 -10.1 25.0 Ave n-Butylbenzene 2.736 2.919 0.0100 46.9 50.0 -6.3 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0567 0.0661 0.0100 42.9 50.0 -14.2 25.0 Ave 1,2,4-Trichlorobenzene 0.7803 0.8970 0.0100 43.5 50.0 -13.0 25.0 Ave Hexachlorobutadiene 0.6904 0.7568 0.0100 45.6 50.0 -8.8 25.0 Ave Naphthalene 0.8667 0.9856 0.0100 44.0 50.0 -12.1 25.0 Ave 1,2,3-Trichlorobenzene 0.6586 0.7171 0.0100 45.9 50.0 -8.2 25.0 Ave Dibromofluoromethane 0.3761 0.3990 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2556 0.2793 0.0100 45.8 50.0 -8.5 25.0 Ave Toluene-d8 (Surr) 1.117 1.184 0.0100 47.2 50.0 -5.6 25.0 Ave 4-Bromofluorobenzene (Surr) 0.4730 0.5005 0.0100 47.3 50.0 -5.5 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 146 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4239 0.5420 0.0100 39.1 50.0 -21.8 25.0 Ave Chloromethane 0.5561 0.7111 0.1000 39.1 50.0 -21.8 25.0 Ave Vinyl chloride 0.5920 0.6381 0.0100 46.4 50.0 -7.2 25.0 Ave Bromomethane 0.1541 0.1998 0.0100 38.6 50.0 -22.9 25.0 Ave Chloroethane 0.2911 0.3338 0.0100 43.6 50.0 -12.8 25.0 Ave Dichlorofluoromethane 0.8378 0.999 0.0100 41.9 50.0 -16.2 25.0 Ave Trichlorofluoromethane 0.7409 0.8265 0.0100 44.8 50.0 -10.4 25.0 Ave Acrolein 0.0406 0.0397 0.0010 2044 2000 2.2 25.0 Ave 1,1-Dichloroethene 0.3815 0.4001 0.0100 47.7 50.0 -4.7 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.4598 0.4862 0.0100 47.3 50.0 -5.4 25.0 Ave Acetone 0.0621 0.0639 0.0100 48.5 50.0 -2.9 25.0 Ave Carbon disulfide 1.369 1.480 0.0100 46.3 50.0 -7.5 25.0 Ave Acetonitrile 0.0292 0.0297 0.0010 393 400 -1.7 25.0 Ave Methylene Chloride 0.3602 0.3812 0.0100 47.2 50.0 -5.5 25.0 Ave Acrylonitrile 0.0797 0.0805 0.0010 396 400 -1.0 25.0 Ave trans-1,2-Dichloroethene 0.4398 0.4499 0.0100 48.9 50.0 -2.3 25.0 Ave Methyl tert-butyl ether 0.6905 0.7369 0.0100 46.9 50.0 -6.3 25.0 Ave 1,1-Dichloroethane 0.8456 0.8857 0.1000 47.7 50.0 -4.5 25.0 Ave Vinyl acetate 0.6214 0.6255 0.0100 49.7 50.0 -0.6 25.0 Ave 2,2-Dichloropropane 0.6853 0.7341 0.0100 46.7 50.0 -6.6 25.0 Ave cis-1,2-Dichloroethene 0.4436 0.4554 0.0100 48.7 50.0 -2.6 25.0 Ave 2-Butanone (MEK) 0.0837 0.0924 0.0100 45.3 50.0 -9.4 25.0 Ave Propionitrile 0.0211 0.0203 0.0010 414 400 3.5 25.0 Ave Bromochloromethane 0.1638 0.1785 0.0100 45.9 50.0 -8.2 25.0 Ave Tetrahydrofuran 0.0548 0.0578 0.0100 47.3 50.0 -5.3 25.0 Ave Chloroform 0.7135 0.7375 0.0100 48.4 50.0 -3.3 25.0 Ave 1,1,1-Trichloroethane 0.7299 0.7394 0.0100 49.4 50.0 -1.3 25.0 Ave Carbon tetrachloride 0.4652 0.4834 0.0100 48.1 50.0 -3.8 25.0 Ave 1,1-Dichloropropene 0.6138 0.6488 0.0100 47.3 50.0 -5.4 25.0 Ave Benzene 1.148 1.229 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichloroethane 0.3244 0.3536 0.0100 45.9 50.0 -8.3 25.0 Ave Trichloroethene 0.3212 0.3450 0.0100 46.6 50.0 -6.9 25.0 Ave 1,2-Dichloropropane 0.2970 0.3152 0.0100 47.1 50.0 -5.8 25.0 Ave Dibromomethane 0.1149 0.1271 0.0100 45.2 50.0 -9.6 25.0 Ave Bromodichloromethane 0.3216 0.3600 0.0100 44.7 50.0 -10.7 25.0 Ave 2-Chloroethyl vinyl ether 0.0957 0.1054 0.0100 45.4 50.0 -9.2 25.0 Ave cis-1,3-Dichloropropene 0.3814 0.4091 0.0100 50.1 53.8 -6.8 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1404 0.1536 0.0100 45.7 50.0 -8.6 25.0 Ave Toluene 0.7569 0.8177 0.0100 46.3 50.0 -7.4 25.0 Ave trans-1,3-Dichloropropene 0.3107 0.3392 0.0100 44.5 48.6 -8.4 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 147 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1573 0.1723 0.0100 45.6 50.0 -8.7 25.0 Ave Tetrachloroethene 0.4260 0.4537 0.0100 47.0 50.0 -6.1 25.0 Ave 1,3-Dichloropropane 0.3223 0.3491 0.0100 46.2 50.0 -7.7 25.0 Ave 2-Hexanone 0.1135 0.1204 0.0100 47.1 50.0 -5.7 25.0 Ave Dibromochloromethane 0.2454 0.2603 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dibromoethane 0.1486 0.1651 0.0100 45.0 50.0 -10.0 25.0 Ave Chlorobenzene 0.9004 1.012 0.3000 44.5 50.0 -11.0 25.0 Ave 1-Chlorohexane 0.6546 0.6865 0.0100 47.7 50.0 -4.6 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3297 0.3400 0.0100 48.5 50.0 -3.0 25.0 Ave Ethylbenzene 0.5498 0.5753 0.0100 47.8 50.0 -4.4 25.0 Ave m&p-Xylene 1.339 1.427 0.0100 93.8 100 -6.2 25.0 Ave o-Xylene 1.295 1.456 0.0100 44.5 50.0 -11.1 25.0 Ave Styrene 1.076 1.120 0.0100 48.0 50.0 -3.9 25.0 Ave Bromoform 0.1521 0.1536 0.1000 49.5 50.0 -1.0 25.0 Ave Isopropylbenzene 2.951 3.312 0.0100 44.6 50.0 -10.9 25.0 Ave Bromobenzene 0.6901 0.7374 0.0100 46.8 50.0 -6.4 25.0 Ave 1,1,2,2-Tetrachloroethane 0.3650 0.3844 0.3000 47.5 50.0 -5.1 25.0 Ave 1,2,3-Trichloropropane 0.2697 0.2827 0.0100 47.7 50.0 -4.6 25.0 Ave N-Propylbenzene 3.489 3.971 0.0100 43.9 50.0 -12.2 25.0 Ave 4-Chlorotoluene 2.042 2.242 0.0100 45.5 50.0 -8.9 25.0 Ave 1,3,5-Trimethylbenzene 2.737 2.765 0.0100 49.5 50.0 -1.0 25.0 Ave 2-Chlorotoluene 2.355 2.663 0.0100 44.2 50.0 -11.6 25.0 Ave tert-Butylbenzene 2.302 2.558 0.0100 45.0 50.0 -10.0 25.0 Ave 1,2,4-Trimethylbenzene 2.637 2.713 0.0100 48.6 50.0 -2.8 25.0 Ave sec-Butylbenzene 3.418 3.783 0.0100 45.2 50.0 -9.6 25.0 Ave 1,3-Dichlorobenzene 1.369 1.575 0.0100 43.5 50.0 -13.1 25.0 Ave p-Isopropyltoluene 2.935 3.287 0.0100 44.7 50.0 -10.7 25.0 Ave 1,4-Dichlorobenzene 1.454 1.556 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichlorobenzene 1.190 1.323 0.0100 45.0 50.0 -10.1 25.0 Ave n-Butylbenzene 2.736 2.919 0.0100 46.9 50.0 -6.3 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0567 0.0661 0.0100 42.9 50.0 -14.2 25.0 Ave 1,2,4-Trichlorobenzene 0.7803 0.8970 0.0100 43.5 50.0 -13.0 25.0 Ave Hexachlorobutadiene 0.6904 0.7568 0.0100 45.6 50.0 -8.8 25.0 Ave Naphthalene 0.8667 0.9856 0.0100 44.0 50.0 -12.1 25.0 Ave 1,2,3-Trichlorobenzene 0.6586 0.7171 0.0100 45.9 50.0 -8.2 25.0 Ave Dibromofluoromethane 0.3761 0.3990 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2556 0.2793 0.0100 45.8 50.0 -8.5 25.0 Ave Toluene-d8 (Surr) 1.117 1.184 0.0100 47.2 50.0 -5.6 25.0 Ave 4-Bromofluorobenzene (Surr) 0.4730 0.5005 0.0100 47.3 50.0 -5.5 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 148 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 19:06 12/11/2012 23:48 ICV 500-172614/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.2517 0.2603 0.0100 48.3 50.0 -3.3 25.0 Ave Iodomethane 0.6879 0.0100 52.8 50.0 5.6 25.0 Lin1 Methyl acetate 0.1450 0.2127 0.0100 34.1 50.0 -31.8* 25.0 Ave Hexane 0.9019 0.8764 0.0100 51.5 50.0 2.9 25.0 Ave Cyclohexane 1.057 0.0100 49.4 50.0 -1.2 25.0 Lin1 Heptane 0.6922 0.7351 0.0100 47.1 50.0 -5.8 25.0 Ave Methylcyclohexane 0.6069 0.5969 0.0100 50.8 50.0 1.7 25.0 Ave 1,3,5-Trichlorobenzene 1.140 1.226 0.0100 46.5 50.0 -7.0 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 149 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/12/2012 00:17 12/11/2012 19:06 12/11/2012 23:48 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.2517 0.2603 0.0100 48.3 50.0 -3.3 25.0 Ave Iodomethane 0.6879 0.0100 52.8 50.0 5.6 25.0 Lin1 Methyl acetate 0.1450 0.2127 0.0100 34.1 50.0 -31.8* 25.0 Ave Hexane 0.9019 0.8764 0.0100 51.5 50.0 2.9 25.0 Ave Cyclohexane 1.057 0.0100 49.4 50.0 -1.2 25.0 Lin1 Heptane 0.6922 0.7351 0.0100 47.1 50.0 -5.8 25.0 Ave Methylcyclohexane 0.6069 0.5969 0.0100 50.8 50.0 1.7 25.0 Ave 1,3,5-Trichlorobenzene 1.140 1.226 0.0100 46.5 50.0 -7.0 25.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 150 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/21/2012 11:31 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173708/2

DB624 TestAmerica Chicago

Lab File ID:22C1221.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.5905 0.5420 0.0100 54.5 50.0 8.9 50.0 Ave Chloromethane 0.7033 0.7111 0.1000 49.5 50.0 -1.1 50.0 Ave Vinyl chloride 0.6454 0.6381 0.0100 50.6 50.0 1.1 20.0 Ave Bromomethane 0.2732 0.1998 0.0100 68.4 50.0 36.8 50.0 Ave Chloroethane 0.3927 0.3338 0.0100 58.8 50.0 17.6 50.0 Ave Dichlorofluoromethane 0.9860 0.999 0.0100 49.3 50.0 -1.3 50.0 Ave Trichlorofluoromethane 0.8481 0.8265 0.0100 51.3 50.0 2.6 50.0 Ave Acrolein 0.0143 0.0397 0.0010 722 2000 -63.9* 50.0 Ave 1,1-Dichloroethene 0.3985 0.4001 0.0100 49.8 50.0 -0.4 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.4954 0.4862 0.0100 50.9 50.0 1.9 50.0 Ave Acetone 0.0594 0.0639 0.0100 46.4 50.0 -7.2 50.0 Ave Carbon disulfide 1.253 1.480 0.0100 42.3 50.0 -15.4 50.0 Ave Acetonitrile 0.0269 0.0297 0.0010 362 400 -9.4 50.0 Ave Methylene Chloride 0.3836 0.3812 0.0100 50.3 50.0 0.6 50.0 Ave Acrylonitrile 0.0736 0.0805 0.0010 366 400 -8.6 50.0 Ave trans-1,2-Dichloroethene 0.4452 0.4499 0.0100 49.5 50.0 -1.1 50.0 Ave Methyl tert-butyl ether 0.7075 0.7369 0.0100 48.0 50.0 -4.0 50.0 Ave 1,1-Dichloroethane 0.8845 0.8857 0.1000 49.9 50.0 -0.1 50.0 Ave Vinyl acetate 0.4185 0.6255 0.0100 33.5 50.0 -33.1 50.0 Ave 2,2-Dichloropropane 0.6657 0.7341 0.0100 45.3 50.0 -9.3 50.0 Ave cis-1,2-Dichloroethene 0.4549 0.4554 0.0100 49.9 50.0 -0.1 50.0 Ave 2-Butanone (MEK) 0.0863 0.0924 0.0100 46.7 50.0 -6.6 50.0 Ave Propionitrile 0.0182 0.0203 0.0010 359 400 -10.4 50.0 Ave Bromochloromethane 0.1742 0.1785 0.0100 48.8 50.0 -2.4 50.0 Ave Tetrahydrofuran 0.0538 0.0578 0.0100 46.5 50.0 -7.0 50.0 Ave Chloroform 0.7347 0.7375 0.0100 49.8 50.0 -0.4 20.0 Ave 1,1,1-Trichloroethane 0.7104 0.7394 0.0100 48.0 50.0 -3.9 50.0 Ave Carbon tetrachloride 0.4401 0.4834 0.0100 45.5 50.0 -9.0 50.0 Ave 1,1-Dichloropropene 0.6621 0.6488 0.0100 51.0 50.0 2.1 50.0 Ave Benzene 1.232 1.229 0.0100 50.1 50.0 0.2 50.0 Ave 1,2-Dichloroethane 0.3513 0.3536 0.0100 49.7 50.0 -0.6 50.0 Ave Trichloroethene 0.3532 0.3450 0.0100 51.2 50.0 2.4 50.0 Ave 1,2-Dichloropropane 0.3160 0.3152 0.0100 50.1 50.0 0.2 20.0 Ave Dibromomethane 0.1218 0.1271 0.0100 47.9 50.0 -4.2 50.0 Ave Bromodichloromethane 0.3468 0.3600 0.0100 48.2 50.0 -3.7 50.0 Ave 2-Chloroethyl vinyl ether 0.1098 0.1054 0.0100 52.1 50.0 4.2 50.0 Ave cis-1,3-Dichloropropene 0.3900 0.4091 0.0100 47.7 50.0 -4.7 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1384 0.1536 0.0100 45.1 50.0 -9.9 50.0 Ave Toluene 0.8220 0.8177 0.0100 50.3 50.0 0.5 20.0 Ave trans-1,3-Dichloropropene 0.3154 0.3392 0.0100 46.5 50.0 -7.0 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 151 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/21/2012 11:31 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173708/2

DB624 TestAmerica Chicago

Lab File ID:22C1221.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1703 0.1723 0.0100 49.4 50.0 -1.2 50.0 Ave Tetrachloroethene 0.4746 0.4537 0.0100 52.3 50.0 4.6 50.0 Ave 1,3-Dichloropropane 0.3524 0.3491 0.0100 50.5 50.0 0.9 50.0 Ave 2-Hexanone 0.1145 0.1204 0.0100 47.5 50.0 -4.9 50.0 Ave Dibromochloromethane 0.2581 0.2603 0.0100 49.6 50.0 -0.8 50.0 Ave 1,2-Dibromoethane 0.1597 0.1651 0.0100 48.4 50.0 -3.3 50.0 Ave Chlorobenzene 1.064 1.012 0.3000 52.6 50.0 5.2 50.0 Ave 1-Chlorohexane 0.7188 0.6865 0.0100 52.4 50.0 4.7 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3343 0.3400 0.0100 49.2 50.0 -1.7 50.0 Ave Ethylbenzene 0.6209 0.5753 0.0100 54.0 50.0 7.9 20.0 Ave m&p-Xylene 1.552 1.427 0.0100 109 100 8.7 50.0 Ave o-Xylene 1.523 1.456 0.0100 52.3 50.0 4.5 50.0 Ave Styrene 1.210 1.120 0.0100 54.0 50.0 8.0 50.0 Ave Bromoform 0.1544 0.1536 0.1000 50.3 50.0 0.5 50.0 Ave Isopropylbenzene 3.283 3.312 0.0100 49.6 50.0 -0.9 50.0 Ave Bromobenzene 0.7156 0.7374 0.0100 48.5 50.0 -3.0 50.0 Ave 1,1,2,2-Tetrachloroethane 0.3740 0.3844 0.3000 48.6 50.0 -2.7 50.0 Ave 1,2,3-Trichloropropane 0.2743 0.2827 0.0100 48.5 50.0 -3.0 50.0 Ave N-Propylbenzene 4.083 3.971 0.0100 51.4 50.0 2.8 50.0 Ave 4-Chlorotoluene 2.247 2.242 0.0100 50.1 50.0 0.2 50.0 Ave 1,3,5-Trimethylbenzene 2.838 2.765 0.0100 51.3 50.0 2.6 50.0 Ave 2-Chlorotoluene 2.692 2.663 0.0100 50.6 50.0 1.1 50.0 Ave tert-Butylbenzene 2.551 2.558 0.0100 49.9 50.0 -0.3 50.0 Ave 1,2,4-Trimethylbenzene 2.728 2.713 0.0100 50.3 50.0 0.5 50.0 Ave sec-Butylbenzene 3.886 3.783 0.0100 51.4 50.0 2.7 50.0 Ave 1,3-Dichlorobenzene 1.595 1.575 0.0100 50.6 50.0 1.3 50.0 Ave p-Isopropyltoluene 3.413 3.287 0.0100 51.9 50.0 3.8 50.0 Ave 1,4-Dichlorobenzene 1.566 1.556 0.0100 50.3 50.0 0.7 50.0 Ave 1,2-Dichlorobenzene 1.338 1.323 0.0100 50.5 50.0 1.1 50.0 Ave n-Butylbenzene 3.096 2.919 0.0100 53.0 50.0 6.1 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0527 0.0661 0.0100 39.8 50.0 -20.3 50.0 Ave 1,2,4-Trichlorobenzene 0.9150 0.8970 0.0100 51.0 50.0 2.0 50.0 Ave Hexachlorobutadiene 0.7863 0.7568 0.0100 52.0 50.0 3.9 50.0 Ave Naphthalene 0.9108 0.9856 0.0100 46.2 50.0 -7.6 50.0 Ave 1,2,3-Trichlorobenzene 0.7018 0.7171 0.0100 48.9 50.0 -2.1 50.0 Ave Dibromofluoromethane 0.3878 0.3990 0.0100 48.6 50.0 -2.8 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2625 0.2793 0.0100 47.0 50.0 -6.0 50.0 Ave Toluene-d8 (Surr) 1.172 1.184 0.0100 49.5 50.0 -1.0 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5040 0.5005 0.0100 50.3 50.0 0.7 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 152 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/21/2012 11:57 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173708/3

DB624 TestAmerica Chicago

Lab File ID:22D1221.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3658 0.3990 0.0100 45.9 50.0 -8.3 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2599 0.2793 0.0100 46.5 50.0 -7.0 50.0 Ave Toluene-d8 (Surr) 1.153 1.184 0.0100 48.7 50.0 -2.6 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4837 0.5005 0.0100 48.3 50.0 -3.4 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 153 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/21/2012 11:57 12/11/2012 19:06 12/11/2012 23:48 CCV 500-173708/3

DB624 TestAmerica Chicago

Lab File ID:22D1221.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.5624 0.0100 34.9 50.0 -30.2 50.0 Lin1 Ethyl ether 0.2460 0.2603 0.0100 47.3 50.0 -5.5 50.0 Ave Iodomethane 0.5829 0.0100 88.2 100 -11.8 50.0 Lin1 3-Chloropropene 0.2212 0.2462 0.0100 89.9 100 -10.1 50.0 Ave Methyl acetate 0.2037 0.2127 0.0100 47.9 50.0 -4.3 50.0 Ave Hexane 0.8088 0.8764 0.0100 46.2 50.0 -7.7 50.0 Ave 2-Chloro-1,3-butadiene 0.9166 0.9423 0.0100 48.6 50.0 -2.7 50.0 Ave Isopropyl ether 1.480 1.545 0.0100 47.9 50.0 -4.2 50.0 Ave Ethyl acetate 0.1780 0.1956 0.0100 455 500 -9.0 50.0 Ave Methacrylonitrile 0.1395 0.1427 0.0100 97.8 100 -2.2 50.0 Ave Cyclohexane 0.996 0.0100 46.5 50.0 -7.0 50.0 Lin1 Isobutyl alcohol 0.0061 0.0073 0.0010 3362 4000 -16.0 50.0 Ave 2,2,4-Trimethylpentane 1.667 1.673 0.0100 49.8 50.0 -0.3 50.0 Ave Heptane 0.7336 0.7351 0.0100 49.9 50.0 -0.2 50.0 Ave n-Butyl alcohol 0.0035 0.0045 0.0010 3086 4000 -22.9 50.0 Ave Methylcyclohexane 0.6023 0.5969 0.0100 50.5 50.0 0.9 50.0 Ave Methyl methacrylate 0.1576 0.1655 0.0100 95.3 100 -4.7 50.0 Ave 2-Nitropropane 0.0656 0.0618 0.0100 4251 4000 6.3 50.0 Ave Ethyl methacrylate 0.2439 0.2528 0.0100 96.5 100 -3.5 50.0 Ave Cyclohexanone 0.0525 0.0256 0.0100 8220 4000 105.5* 50.0 Ave trans-1,4-Dichloro-2-butene 0.0557 0.0710 0.0100 78.5 100 -21.5 50.0 Ave Pentachloroethane 0.2699 0.2758 0.0100 97.9 100 -2.1 50.0 Ave 1,3,5-Trichlorobenzene 1.252 1.226 0.0100 51.1 50.0 2.1 50.0 Ave 2-Methylnaphthalene 0.5773 0.6831 0.0100 42.3 50.0 -15.5 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 154 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/24/2012 11:43 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173827/2

DB624 TestAmerica Chicago

Lab File ID:22C1224.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.6395 0.5420 0.0100 59.0 50.0 18.0 50.0 Ave Chloromethane 0.7439 0.7111 0.1000 52.3 50.0 4.6 50.0 Ave Vinyl chloride 0.6817 0.6381 0.0100 53.4 50.0 6.8 20.0 Ave Bromomethane 0.2696 0.1998 0.0100 67.5 50.0 34.9 50.0 Ave Chloroethane 0.3932 0.3338 0.0100 58.9 50.0 17.8 50.0 Ave Dichlorofluoromethane 1.010 0.999 0.0100 50.5 50.0 1.1 50.0 Ave Trichlorofluoromethane 0.8689 0.8265 0.0100 52.6 50.0 5.1 50.0 Ave Acrolein 0.0459 0.0397 0.0010 2312 2000 15.6 50.0 Ave 1,1-Dichloroethene 0.4293 0.4001 0.0100 53.6 50.0 7.3 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5317 0.4862 0.0100 54.7 50.0 9.4 50.0 Ave Acetone 0.0568 0.0639 0.0100 44.4 50.0 -11.2 50.0 Ave Carbon disulfide 1.236 1.480 0.0100 41.8 50.0 -16.5 50.0 Ave Acetonitrile 0.0309 0.0297 0.0010 415 400 3.7 50.0 Ave Methylene Chloride 0.3945 0.3812 0.0100 51.8 50.0 3.5 50.0 Ave Acrylonitrile 0.0858 0.0805 0.0010 426 400 6.6 50.0 Ave trans-1,2-Dichloroethene 0.4722 0.4499 0.0100 52.5 50.0 5.0 50.0 Ave Methyl tert-butyl ether 0.7217 0.7369 0.0100 49.0 50.0 -2.1 50.0 Ave 1,1-Dichloroethane 0.9220 0.8857 0.1000 52.1 50.0 4.1 50.0 Ave Vinyl acetate 0.4971 0.6255 0.0100 39.7 50.0 -20.5 50.0 Ave 2,2-Dichloropropane 0.7559 0.7341 0.0100 51.5 50.0 3.0 50.0 Ave cis-1,2-Dichloroethene 0.4715 0.4554 0.0100 51.8 50.0 3.5 50.0 Ave 2-Butanone (MEK) 0.0892 0.0924 0.0100 48.3 50.0 -3.5 50.0 Ave Propionitrile 0.0220 0.0203 0.0010 433 400 8.3 50.0 Ave Bromochloromethane 0.1859 0.1785 0.0100 52.1 50.0 4.1 50.0 Ave Tetrahydrofuran 0.0555 0.0578 0.0100 47.9 50.0 -4.1 50.0 Ave Chloroform 0.7718 0.7375 0.0100 52.3 50.0 4.7 20.0 Ave 1,1,1-Trichloroethane 0.7594 0.7394 0.0100 51.4 50.0 2.7 50.0 Ave Carbon tetrachloride 0.4866 0.4834 0.0100 50.3 50.0 0.7 50.0 Ave 1,1-Dichloropropene 0.6934 0.6488 0.0100 53.4 50.0 6.9 50.0 Ave Benzene 1.290 1.229 0.0100 52.5 50.0 4.9 50.0 Ave 1,2-Dichloroethane 0.3785 0.3536 0.0100 53.5 50.0 7.0 50.0 Ave Trichloroethene 0.3696 0.3450 0.0100 53.6 50.0 7.1 50.0 Ave 1,2-Dichloropropane 0.3333 0.3152 0.0100 52.9 50.0 5.7 20.0 Ave Dibromomethane 0.1334 0.1271 0.0100 52.5 50.0 5.0 50.0 Ave Bromodichloromethane 0.3861 0.3600 0.0100 53.6 50.0 7.3 50.0 Ave 2-Chloroethyl vinyl ether 0.1109 0.1054 0.0100 52.6 50.0 5.2 50.0 Ave cis-1,3-Dichloropropene 0.4326 0.4091 0.0100 52.9 50.0 5.7 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1438 0.1536 0.0100 46.8 50.0 -6.4 50.0 Ave Toluene 0.8913 0.8177 0.0100 54.5 50.0 9.0 20.0 Ave trans-1,3-Dichloropropene 0.3473 0.3392 0.0100 51.2 50.0 2.4 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 155 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/24/2012 11:43 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173827/2

DB624 TestAmerica Chicago

Lab File ID:22C1224.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1828 0.1723 0.0100 53.0 50.0 6.0 50.0 Ave Tetrachloroethene 0.4850 0.4537 0.0100 53.5 50.0 6.9 50.0 Ave 1,3-Dichloropropane 0.3722 0.3491 0.0100 53.3 50.0 6.6 50.0 Ave 2-Hexanone 0.1115 0.1204 0.0100 46.3 50.0 -7.4 50.0 Ave Dibromochloromethane 0.2825 0.2603 0.0100 54.3 50.0 8.6 50.0 Ave 1,2-Dibromoethane 0.1723 0.1651 0.0100 52.2 50.0 4.3 50.0 Ave Chlorobenzene 1.118 1.012 0.3000 55.2 50.0 10.4 50.0 Ave 1-Chlorohexane 0.7687 0.6865 0.0100 56.0 50.0 12.0 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3650 0.3400 0.0100 53.7 50.0 7.4 50.0 Ave Ethylbenzene 0.6414 0.5753 0.0100 55.7 50.0 11.5 20.0 Ave m&p-Xylene 1.647 1.427 0.0100 115 100 15.4 50.0 Ave o-Xylene 1.644 1.456 0.0100 56.4 50.0 12.9 50.0 Ave Styrene 1.290 1.120 0.0100 57.6 50.0 15.2 50.0 Ave Bromoform 0.1670 0.1536 0.1000 54.3 50.0 8.7 50.0 Ave Isopropylbenzene 3.559 3.312 0.0100 53.7 50.0 7.5 50.0 Ave Bromobenzene 0.7771 0.7374 0.0100 52.7 50.0 5.4 50.0 Ave 1,1,2,2-Tetrachloroethane 0.4010 0.3844 0.3000 52.2 50.0 4.3 50.0 Ave 1,2,3-Trichloropropane 0.2996 0.2827 0.0100 53.0 50.0 6.0 50.0 Ave N-Propylbenzene 4.412 3.971 0.0100 55.6 50.0 11.1 50.0 Ave 4-Chlorotoluene 2.455 2.242 0.0100 54.8 50.0 9.5 50.0 Ave 1,3,5-Trimethylbenzene 3.063 2.765 0.0100 55.4 50.0 10.8 50.0 Ave 2-Chlorotoluene 2.919 2.663 0.0100 54.8 50.0 9.6 50.0 Ave tert-Butylbenzene 2.745 2.558 0.0100 53.7 50.0 7.3 50.0 Ave 1,2,4-Trimethylbenzene 2.977 2.713 0.0100 54.9 50.0 9.7 50.0 Ave sec-Butylbenzene 4.175 3.783 0.0100 55.2 50.0 10.4 50.0 Ave 1,3-Dichlorobenzene 1.689 1.575 0.0100 53.6 50.0 7.3 50.0 Ave p-Isopropyltoluene 3.669 3.287 0.0100 55.8 50.0 11.6 50.0 Ave 1,4-Dichlorobenzene 1.684 1.556 0.0100 54.1 50.0 8.2 50.0 Ave 1,2-Dichlorobenzene 1.448 1.323 0.0100 54.7 50.0 9.4 50.0 Ave n-Butylbenzene 3.331 2.919 0.0100 57.1 50.0 14.1 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0611 0.0661 0.0100 46.2 50.0 -7.5 50.0 Ave 1,2,4-Trichlorobenzene 0.9477 0.8970 0.0100 52.8 50.0 5.7 50.0 Ave Hexachlorobutadiene 0.8182 0.7568 0.0100 54.1 50.0 8.1 50.0 Ave Naphthalene 0.9710 0.9856 0.0100 49.3 50.0 -1.5 50.0 Ave 1,2,3-Trichlorobenzene 0.7398 0.7171 0.0100 51.6 50.0 3.2 50.0 Ave Dibromofluoromethane 0.3785 0.3990 0.0100 47.4 50.0 -5.1 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2537 0.2793 0.0100 45.4 50.0 -9.2 50.0 Ave Toluene-d8 (Surr) 1.143 1.184 0.0100 48.3 50.0 -3.4 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4700 0.5005 0.0100 46.9 50.0 -6.1 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 156 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/24/2012 12:09 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173827/3

DB624 TestAmerica Chicago

Lab File ID:22D1224.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3458 0.3990 0.0100 43.3 50.0 -13.3 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2456 0.2793 0.0100 44.0 50.0 -12.1 50.0 Ave Toluene-d8 (Surr) 1.115 1.184 0.0100 47.1 50.0 -5.8 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4711 0.5005 0.0100 47.1 50.0 -5.9 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 157 of 332

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53342-1

CMS22 12/24/2012 12:09 12/11/2012 19:06 12/11/2012 23:48 CCV 500-173827/3

DB624 TestAmerica Chicago

Lab File ID:22D1224.D Heated Purge: (Y/N)N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.5251 0.0100 32.6 50.0 -34.7 50.0 Lin1 Ethyl ether 0.2277 0.2603 0.0100 43.7 50.0 -12.5 50.0 Ave Iodomethane 0.5570 0.0100 84.4 100 -15.7 50.0 Lin1 3-Chloropropene 0.2214 0.2462 0.0100 89.9 100 -10.1 50.0 Ave Methyl acetate 0.1957 0.2127 0.0100 46.0 50.0 -8.0 50.0 Ave Hexane 0.7801 0.8764 0.0100 44.5 50.0 -11.0 50.0 Ave 2-Chloro-1,3-butadiene 0.8618 0.9423 0.0100 45.7 50.0 -8.6 50.0 Ave Isopropyl ether 1.375 1.545 0.0100 44.5 50.0 -11.0 50.0 Ave Ethyl acetate 0.1702 0.1956 0.0100 435 500 -13.0 50.0 Ave Methacrylonitrile 0.1285 0.1427 0.0100 90.1 100 -9.9 50.0 Ave Cyclohexane 0.9215 0.0100 42.9 50.0 -14.1 50.0 Lin1 Isobutyl alcohol 0.0063 0.0073 0.0010 3490 4000 -12.8 50.0 Ave 2,2,4-Trimethylpentane 1.570 1.673 0.0100 47.0 50.0 -6.1 50.0 Ave Heptane 0.6901 0.7351 0.0100 46.9 50.0 -6.1 50.0 Ave n-Butyl alcohol 0.0036 0.0045 0.0010 3178 4000 -20.6 50.0 Ave Methylcyclohexane 0.5568 0.5969 0.0100 46.6 50.0 -6.7 50.0 Ave Methyl methacrylate 0.1550 0.1655 0.0100 93.7 100 -6.4 50.0 Ave 2-Nitropropane 0.0660 0.0618 0.0100 4275 4000 6.9 50.0 Ave Ethyl methacrylate 0.2372 0.2528 0.0100 93.8 100 -6.2 50.0 Ave Cyclohexanone 0.0502 0.0256 0.0100 7852 4000 96.3* 50.0 Ave trans-1,4-Dichloro-2-butene 0.0589 0.0710 0.0100 82.9 100 -17.1 50.0 Ave Pentachloroethane 0.2673 0.2758 0.0100 96.9 100 -3.1 50.0 Ave 1,3,5-Trichlorobenzene 1.143 1.226 0.0100 46.6 50.0 -6.8 50.0 Ave 2-Methylnaphthalene 0.5262 0.6831 0.0100 38.5 50.0 -23.0 50.0 Ave



### FORM VII 8260B 

## 01/04/2013 Page 158 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:MB 500-173515/4 Matrix: 16M1220.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(g)
0.2(mm) Date Analyzed:12/20/2012 09:00

ID: DB624
Analysis Batch No.: 173515 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone <5.00 5.00 1.81 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 106 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 113 75-122 2037-26-5 Toluene-d8 (Surr) 107 70-122 460-00-4 4-Bromofluorobenzene (Surr) 103 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 159 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:MB 500-173708/6 Matrix: 22M1221.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5 (mL) 0.2(mm) Date Analyzed:12/21/2012 13:16

ID: DB624
Analysis Batch No.: 173708 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 90 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 88 75-120 460-00-4 4-Bromofluorobenzene (Surr) 88 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 160 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:MB 500-173827/6 Matrix: 22M1224.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(mL)
0.2(mm) Date Analyzed:12/24/2012 13:33

ID: DB624
Analysis Batch No.: 173827 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 90 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-120 2037-26-5 Toluene-d8 (Surr) 88 75-120 460-00-4 4-Bromofluorobenzene (Surr) 92 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 161 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:LCS 500-173515/5 Matrix: 16S1220.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(g)
0.2(mm) Date Analyzed:12/20/2012 09:23

ID: DB624
Analysis Batch No.: 173515 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone 43.68 5.00 1.81 78-93-3 2-Butanone (MEK) 45.67


### %REC CAS NO. LIMITS Q SURROGATE 98 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 111 75-122 2037-26-5 Toluene-d8 (Surr) 102 70-122 460-00-4 4-Bromofluorobenzene (Surr) 103 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 162 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:LCS 500-173708/4 Matrix: 22S1221.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5 (mL) 0.2(mm) Date Analyzed:12/21/2012 12:23

ID: DB624
Analysis Batch No.: 173708 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone 46.74 5.00 1.47 78-93-3 2-Butanone (MEK) 41.90


### %REC CAS NO. LIMITS Q SURROGATE 94 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 103 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 163 of 332

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53342-1
Lab Sample ID:LCS 500-173827/4 Matrix: 22S1224.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Low 5(mL)
0.2(mm) Date Analyzed:12/24/2012 12:35

ID: DB624
Analysis Batch No.: 173827 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone 48.03 5.00 1.47 78-93-3 2-Butanone (MEK) 50.18


### %REC CAS NO. LIMITS Q SURROGATE 92 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 94 75-120 460-00-4 4-Bromofluorobenzene (Surr) 92 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/04/2013 Page 164 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS16 170196 Start Date: End Date:11/19/2012 17:14 11/19/2012 11:14

BFB 500-170196/5 DB624 0.2(mm) 1 11/19/2012 11:14 16B1119c.D STD1 500-170196/6 IC DB624 0.2(mm) 1 11/19/2012 12:14 16I1119A.D STD2 500-170196/7 IC DB624 0.2(mm) 1 11/19/2012 12:37 16I1119B.D STD3 500-170196/8 ICIS DB624 0.2(mm) 1 11/19/2012 13:00 16I1119C.D STD4 500-170196/9 IC DB624 0.2(mm) 1 11/19/2012 13:23 16I1119D.D STD5 500-170196/10 IC DB624 0.2(mm) 1 11/19/2012 13:46 16I1119E.D STD6 500-170196/11 IC DB624 0.2(mm) 1 11/19/2012 14:09 16I1119F.D STD1AP 500-170196/12 IC DB624 0.2(mm) 1 11/19/2012 14:32 STD2AP 500-170196/13 IC DB624 0.2(mm) 1 11/19/2012 14:55 STD3AP 500-170196/14 IC DB624 0.2(mm) 1 11/19/2012 15:18 STD4AP 500-170196/15 IC DB624 0.2(mm) 1 11/19/2012 15:42 STD5AP 500-170196/16 IC DB624 0.2(mm) 1 11/19/2012 16:05 STD6AP 500-170196/17 IC DB624 0.2(mm) 1 11/19/2012 16:28 ICV 500-170196/19 DB624 0.2(mm) 1 11/19/2012 17:14 16S1119.D



### 8260B 

## 01/04/2013 Page 165 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS16 173515 Start Date: End Date:12/20/2012 14:38 12/20/2012 07:38

BFB 500-173515/6 DB624 0.2(mm) 1 12/20/2012 07:38 16B1220a.D CCV 500-173515/2 DB624 0.2(mm) 1 12/20/2012 08:13 16C1220.D CCV 500-173515/3 DB624 0.2(mm) 1 12/20/2012 08:36 16D1220.D MB 500-173515/4 DB624 0.2(mm) 1 12/20/2012 09:00 16M1220.D LCS 500-173515/5 DB624 0.2(mm) 1 12/20/2012 09:23 16S1220.D ZZZZZ DB624 0.2(mm) 1 12/20/2012 09:59 ZZZZZ DB624 0.2(mm) 1 12/20/2012 10:23 ZZZZZ DB624 0.2(mm) 1 12/20/2012 10:46 ZZZZZ DB624 0.2(mm) 1 12/20/2012 11:09 ZZZZZ DB624 0.2(mm) 1 12/20/2012 11:32 ZZZZZ DB624 0.2(mm) 1 12/20/2012 11:55 ZZZZZ DB624 0.2(mm) 1 12/20/2012 12:19 ZZZZZ DB624 0.2(mm) 1 12/20/2012 12:42 ZZZZZ DB624 0.2(mm) 1 12/20/2012 13:05 ZZZZZ DB624 0.2(mm) 1 12/20/2012 13:28 500-53342-2 FC Composite 5 DB624 0.2(mm) 1 12/20/2012 13:52 53342-02.D ZZZZZ DB624 0.2(mm) 1 12/20/2012 14:38



### 8260B 

## 01/04/2013 Page 166 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS22 172614 Start Date: End Date:12/12/2012 00:17 12/11/2012 13:45

BFB 500-172614/1 DB624 0.2(mm) 1 12/11/2012 13:45 22B1211.D STD01 500-172614/2 IC DB624 0.2(mm) 1 12/11/2012 14:23 22I1211A.D STD02 500-172614/3 IC DB624 0.2(mm) 1 12/11/2012 14:51 22I1211B.D STD03 500-172614/4 IC DB624 0.2(mm) 1 12/11/2012 15:20 22I1211C.D STD04 500-172614/5 IC DB624 0.2(mm) 1 12/11/2012 15:48 22I1211D.D STD05 500-172614/6 IC DB624 0.2(mm) 1 12/11/2012 16:16 22I1211E.D STD06 500-172614/7 ICIS DB624 0.2(mm) 1 12/11/2012 16:44 22I1211F.D STD07 500-172614/8 IC DB624 0.2(mm) 1 12/11/2012 17:13 22I1211G.D STD08 500-172614/9 IC DB624 0.2(mm) 1 12/11/2012 17:41 22I1211H.D STD09 500-172614/10 IC DB624 0.2(mm) 1 12/11/2012 18:09 22I1211I.D STD02AP 500-172614/12 IC DB624 0.2(mm) 1 12/11/2012 19:06 STD05AP 500-172614/15 IC DB624 0.2(mm) 1 12/11/2012 20:30 STD06AP 500-172614/16 IC DB624 0.2(mm) 1 12/11/2012 20:59 STD07AP 500-172614/17 IC DB624 0.2(mm) 1 12/11/2012 21:27 STD08AP 500-172614/18 IC DB624 0.2(mm) 1 12/11/2012 21:55 STD09AP 500-172614/19 IC DB624 0.2(mm) 1 12/11/2012 22:24 STD03AP 500-172614/21 IC DB624 0.2(mm) 1 12/11/2012 23:20 STD04AP 500-172614/22 IC DB624 0.2(mm) 1 12/11/2012 23:48 ICV 500-172614/23 DB624 0.2(mm) 1 12/12/2012 00:17 22S1211.D



### 8260B 

## 01/04/2013 Page 167 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS22 172615 Start Date: End Date:12/12/2012 00:17 12/11/2012 13:45

BFB 500-172615/1 DB624 0.2(mm) 1 12/11/2012 13:45 22B1211.D STD01 500-172615/2 IC DB624 0.2(mm) 1 12/11/2012 14:23 22I1211A.D STD02 500-172615/3 IC DB624 0.2(mm) 1 12/11/2012 14:51 22I1211B.D STD03 500-172615/4 IC DB624 0.2(mm) 1 12/11/2012 15:20 22I1211C.D STD04 500-172615/5 IC DB624 0.2(mm) 1 12/11/2012 15:48 22I1211D.D STD05 500-172615/6 IC DB624 0.2(mm) 1 12/11/2012 16:16 22I1211E.D STD06 500-172615/7 ICIS DB624 0.2(mm) 1 12/11/2012 16:44 22I1211F.D STD07 500-172615/8 IC DB624 0.2(mm) 1 12/11/2012 17:13 22I1211G.D STD08 500-172615/9 IC DB624 0.2(mm) 1 12/11/2012 17:41 22I1211H.D STD09 500-172615/10 IC DB624 0.2(mm) 1 12/11/2012 18:09 22I1211I.D STD02AP 500-172615/12 IC DB624 0.2(mm) 1 12/11/2012 19:06 STD05AP 500-172615/15 IC DB624 0.2(mm) 1 12/11/2012 20:30 STD06AP 500-172615/16 IC DB624 0.2(mm) 1 12/11/2012 20:59 STD07AP 500-172615/17 IC DB624 0.2(mm) 1 12/11/2012 21:27 STD08AP 500-172615/18 IC DB624 0.2(mm) 1 12/11/2012 21:55 STD09AP 500-172615/19 IC DB624 0.2(mm) 1 12/11/2012 22:24 STD03AP 500-172615/21 IC DB624 0.2(mm) 1 12/11/2012 23:20 STD04AP 500-172615/22 IC DB624 0.2(mm) 1 12/11/2012 23:48 ICV 500-172615/23 DB624 0.2(mm) 1 12/12/2012 00:17 22S1211.D



### 8260B 

## 01/04/2013 Page 168 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS22 173708 Start Date: End Date:12/21/2012 22:40 12/21/2012 10:53

BFB 500-173708/1 DB624 0.2(mm) 1 12/21/2012 10:53 22B1221.D CCV 500-173708/2 DB624 0.2(mm) 1 12/21/2012 11:31 22C1221.D CCV 500-173708/3 DB624 0.2(mm) 1 12/21/2012 11:57 22D1221.D LCS 500-173708/4 DB624 0.2(mm) 1 12/21/2012 12:23 22S1221.D MB 500-173708/6 DB624 0.2(mm) 1 12/21/2012 13:16 22M1221.D 500-53342-2 DL FC Composite 5 DL DB624 0.2(mm) 50 12/21/2012 22:40 53342-02.D



### 8260B 

## 01/04/2013 Page 169 of 332

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53342-1

CMS22 173827 Start Date: End Date:12/24/2012 22:42 12/24/2012 11:02

BFB 500-173827/1 DB624 0.2(mm) 1 12/24/2012 11:02 22B1224.D CCV 500-173827/2 DB624 0.2(mm) 1 12/24/2012 11:43 22C1224.D CCV 500-173827/3 DB624 0.2(mm) 1 12/24/2012 12:09 22D1224.D LCS 500-173827/4 DB624 0.2(mm) 1 12/24/2012 12:35 22S1224.D MB 500-173827/6 DB624 0.2(mm) 1 12/24/2012 13:33 22M1224.D 500-53342-4 Trip Blank DB624 0.2(mm) 1 12/24/2012 13:59 53342-04.D 500-53342-3 FC EB 5 DB624 0.2(mm) 1 12/24/2012 14:25 53342-03.D ZZZZZ DB624 0.2(mm) 1 12/24/2012 14:51 ZZZZZ DB624 0.2(mm) 1 12/24/2012 15:17 ZZZZZ DB624 0.2(mm) 1 12/24/2012 15:43 ZZZZZ DB624 0.2(mm) 1 12/24/2012 16:10 ZZZZZ DB624 0.2(mm) 1 12/24/2012 16:37 ZZZZZ DB624 0.2(mm) 1 12/24/2012 17:03 ZZZZZ DB624 0.2(mm) 1 12/24/2012 17:29 ZZZZZ DB624 0.2(mm) 1 12/24/2012 17:55 ZZZZZ DB624 0.2(mm) 1 12/24/2012 18:21 ZZZZZ DB624 0.2(mm) 1 12/24/2012 18:47 ZZZZZ DB624 0.2(mm) 1 12/24/2012 19:13 ZZZZZ DB624 0.2(mm) 1 12/24/2012 19:40 ZZZZZ DB624 0.2(mm) 1 12/24/2012 20:06 ZZZZZ DB624 0.2(mm) 1 12/24/2012 20:32 ZZZZZ DB624 0.2(mm) 1 12/24/2012 20:58 ZZZZZ DB624 0.2(mm) 1 12/24/2012 21:24 ZZZZZ DB624 0.2(mm) 1 12/24/2012 21:50 ZZZZZ DB624 0.2(mm) 1 12/24/2012 22:16 ZZZZZ DB624 0.2(mm) 1 12/24/2012 22:42



### 8260B 

## 01/04/2013 Page 170 of 332

### Lab Name: Job No.: SDG No.: GC/MS VOA BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Estes, William R 12/19/12 13:00 173454 Batch Method: TestAmerica Chicago

5030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount AnalysisComment FC Composite 5 5 g 5 mL MeOH from soil jar 500-53342-A-2 5030B, 8260B T

Batch Notes Balance ID C-0133 Methanol Lot Number DH247 Pipette ID C-2207
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 8260B 

## 01/04/2013 Page 171 of 332

# 01/04/2013 Page 172 of 332

# 01/04/2013 Page 173 of 332

# METALS

01/04/2013 Page 174 of 332

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID METALS

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53342-1 TestAmerica Chicago

500-53342-1 FC Composite 5 500-53342-3 FC EB 5

Comments:



## 01/04/2013 Page 175 of 332

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40 500-53342-1 FC Composite 5

Solid 12/17/2012 14:50 Date Sampled: Reporting Basis: DRY 

### METALS

TestAmerica Chicago

% Solids: 30.0

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 409 mg/Kg 3.01 0.358 1 6010B 7440-50-8 Copper 693 mg/Kg 3.01 0.815 1 6010B 7440-47-3 Chromium 14200 mg/Kg 3.01 0.502 1 6010B 7440-02-0 Nickel 77.4 mg/Kg B 3.01 0.659 1 6010B 7439-92-1 Lead 250 mg/Kg B 1.50 0.517 1 6010B 7440-62-2 Vanadium 238 mg/Kg 1.50 0.228 1 6010B 7440-66-6 Zinc 441 mg/Kg 6.02 2.06 1 6010B 7439-97-6 Mercury 0.321 mg/Kg 0.0540 0.0206 1 7471A



### FORM IA-IN 

## 01/04/2013 Page 176 of 332

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40 500-53342-1 FC Composite 5

Solid 12/17/2012 14:50 Date Sampled: Reporting Basis: WET 

### METALS - TCLP

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium <0.500 mg/L 0.500 0.0100 1 6010B 7440-50-8 Copper <0.0250 mg/L 0.0250 0.0100 1 6010B 7440-47-3 Chromium 0.166 mg/L 0.0250 0.0100 1 6010B 7440-02-0 Nickel 0.531 mg/L 0.0250 0.0100 1 6010B 7439-92-1 Lead <0.0500 mg/L 0.0500 0.00500 1 6010B 7440-62-2 Vanadium 0.00669 J mg/L 0.0250 0.00500 1 6010B 7440-66-6 Zinc 0.0502 J mg/L 0.100 0.0200 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000020 0 1 7470A



### FORM IA-IN 

## 01/04/2013 Page 177 of 332

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-3

Date Received: 12/18/2012 09:40 500-53342-1 FC EB 5

Water 12/17/2012 14:30 Date Sampled: Reporting Basis: WET 

### METALS

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium <0.0100 mg/L 0.0100 0.000440 1 6010B 7440-50-8 Copper 0.00616 J mg/L 0.0100 0.00106 1 6010B 7440-47-3 Chromium <0.0100 mg/L 0.0100 0.000960 1 6010B 7440-02-0 Nickel <0.0100 mg/L 0.0100 0.00190 1 6010B 7439-92-1 Lead 0.00245 J mg/L B 0.00500 0.00158 1 6010B 7440-62-2 Vanadium <0.00500 mg/L 0.00500 0.000620 1 6010B 7440-66-6 Zinc 0.00789 J mg/L 0.0200 0.00472 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000071 0 1 7470A



### FORM IA-IN 

## 01/04/2013 Page 178 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173517/10 12/19/2012 09:45
Found C True %R 

### CCV 500-173517/15 12/19/2012 10:20 CCV 500-173517/27 12/19/2012 11:45
Found Found C C True %R True %R 

### Barium 

### 0.4009 0.4996 0.5050 0.400 0.500 0.500 100 100 101 Chromium 

### 0.4092 0.5119 0.5055 0.400 0.500 0.500 102 102 101 Copper 

### 0.4066 0.5085 0.5117 0.400 0.500 0.500 102 102 102 Lead 

### 0.4102 0.5092 0.5026 0.400 0.500 0.500 103 102 101 Nickel 

### 0.4046 0.5056 0.5011 0.400 0.500 0.500 101 101 100 Vanadium 

### 4.040 5.048 5.027 4.00 5.00 5.00 101 101 101 Zinc 

### 0.4049 0.5067 0.4940 0.400 0.500 0.500 101 101 99

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 179 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173517/39 12/19/2012 13:02
Found C True %R 

### CCV 500-173517/51 12/19/2012 14:26 CCV 500-173517/63 12/19/2012 15:47
Found Found C C True %R True %R 

### Barium 

### 0.5058 0.4985 0.5064 0.500 0.500 0.500 101 100 101 Chromium 

### 0.5060 0.5069 0.5161 0.500 0.500 0.500 101 101 103 Copper 

### 0.5141 0.5071 0.5146 0.500 0.500 0.500 103 101 103 Lead 

### 0.5023 0.5049 0.5134 0.500 0.500 0.500 100 101 103 Nickel 

### 0.5009 0.5041 0.5121 0.500 0.500 0.500 100 101 102 Vanadium 

### 5.029 5.027 5.116 5.00 5.00 5.00 101 101 102 Zinc 

### 0.4922 0.5013 0.5102 0.500 0.500 0.500 98 100 102

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 180 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173518/10 12/19/2012 18:41
Found C True %R 

### CCV 500-173518/27 12/19/2012 20:32 CCV 500-173518/39 12/19/2012 21:57
Found Found C C True %R True %R 

### Barium 

### 0.4028 0.5103 0.5135 0.400 0.500 0.500 101 102 103 Chromium 

### 0.4072 0.5110 0.5092 0.400 0.500 0.500 102 102 102 Copper 

### 0.4055 0.5154 0.5149 0.400 0.500 0.500 101 103 103 Lead 

### 0.4072 0.5098 0.5055 0.400 0.500 0.500 102 102 101 Nickel 

### 0.4012 0.5034 0.5014 0.400 0.500 0.500 100 101 100 Vanadium 

### 4.032 5.081 5.067 4.00 5.00 5.00 101 102 101 Zinc 

### 0.4013 0.4996 0.4948 0.400 0.500 0.500 100 100 99

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 181 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173518/51 12/19/2012 23:21
Found C True %R Found Found C C True %R True %R 

### Barium 

### 0.5130 0.500103 Chromium 

### 0.5100 0.500102 Copper 

### 0.5146 0.500103 Lead 

### 0.5098 0.500102 Nickel 

### 0.5037 0.500101 Vanadium 

### 5.078 5.00102 Zinc 

### 0.4979 0.500100

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 182 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173573/7 12/20/2012 09:11
Found C True %R 

### CCV 500-173573/20 12/20/2012 09:39
Found Found C C True %R True %R 

### Mercury 

### 1.930 1.270 2.00 1.00 97 127

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 183 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173574/7 12/20/2012 09:59
Found C True %R 

### CCV 500-173574/10 12/20/2012 10:05 CCV 500-173574/22 12/20/2012 10:28
Found Found C C True %R True %R 

### Mercury 

### 1.990 0.9540 0.9780 2.00 1.00 1.00 100 95 98

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 184 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173572/7 12/20/2012 08:24
Found C True %R 

### CCV 500-173572/31 12/20/2012 09:12 CCV 500-173572/43 12/20/2012 09:34
Found Found C C True %R True %R 

### Mercury 

### 2.086 1.022 1.082 2.00 1.00 1.00 104 102 108 J J

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 185 of 332

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53342-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte CCV 500-173572/55 12/20/2012 09:57
Found C True %R 

### CCV 500-173572/67 12/20/2012 10:19 CCV 500-173572/75 12/20/2012 10:34
Found Found C C True %R True %R 

### Mercury 

### <2.00 1.017 1.016 1.00 1.00 1.00 93 102 102

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 186 of 332

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53342-1 CRQL CHECK STANDARD METALS

Method:6010B Instrument ID:ICP5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173517/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units:mg/L

50-150 Barium 0.0200 0.01990 100 50-150 Copper 0.0200 0.01955 98 50-150 Chromium 0.0200 0.02070 104 50-150 Nickel 0.0200 0.02010 101 50-150 Lead 0.0100 0.01229 123 50-150 Vanadium 0.0100 0.01023 102 50-150 Zinc 0.0400 0.04138 103 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173517/75

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units:mg/L

50-150 Barium 0.0200 0.02015 101 50-150 Copper 0.0200 0.01926 96 50-150 Chromium 0.0200 0.02135 107 50-150 Nickel 0.0200 0.02068 103 50-150 Lead 0.0100 0.01158 116 50-150 Vanadium 0.0100 0.01071 107 50-150 Zinc 0.0400 0.04222 106 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173518/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units:mg/L

50-150 Barium 0.0200 0.02016 101 50-150 Copper 0.0200 0.01972 99 50-150 Chromium 0.0200 0.02105 105 50-150 Nickel 0.0200 0.01981 99 50-150 Lead 0.0100 0.01011 101 50-150 Vanadium 0.0100 0.01023 102 50-150 Zinc 0.0400 0.04064 102

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 187 of 332

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53342-1 CRQL CHECK STANDARD METALS

Method:7470A Instrument ID:HG6 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173572/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units:ug/L

50-150 Mercury 0.200 <2.00 96

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 188 of 332

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53342-1 CRQL CHECK STANDARD METALS

Method:7471A Instrument ID:HG5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173573/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units:ug/L

50-150 Mercury 0.200 0.1280 J ^ 64 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173574/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units:ug/L

50-150 Mercury 0.200 0.1810 J 91

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 189 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173517/11 CCB 500-173517/16 CCB 500-173517/28 CCB 500-173517/40 12/19/2012 09:53 12/19/2012 10:26 12/19/2012 11:51 12/19/2012 13:08 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 190 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 mg/L

C Found C Found C Found C Found RL 

### Analyte CCB 500-173517/52 CCB 500-173517/64 12/19/2012 14:32 12/19/2012 15:53 

### 3-IN

Barium 

### <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 191 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173518/11 CCB 500-173518/28 CCB 500-173518/40 CCB 500-173518/52 12/19/2012 18:48 12/19/2012 20:38 12/19/2012 22:04 12/19/2012 23:27 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 192 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173573/8 CCB 500-173573/21 12/20/2012 09:12 12/20/2012 09:41 

### 3-IN

Mercury 

### <0.200 <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 193 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173574/8 CCB 500-173574/11 CCB 500-173574/23 12/20/2012 10:01 12/20/2012 10:07 12/20/2012 10:30 

### 3-IN

Mercury 

### <0.200 <0.200 <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 194 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173572/8 CCB 500-173572/32 CCB 500-173572/44 CCB 500-173572/56 12/20/2012 08:26 12/20/2012 09:13 12/20/2012 09:36 12/20/2012 09:59 

### 3-IN

Mercury 

### <2.00 <2.00 <2.00 <2.00 2.00

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 195 of 332

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53342-1 ug/L

C Found C Found C Found C Found RL 

### Analyte CCB 500-173572/68 CCB 500-173572/76 12/20/2012 10:21 12/20/2012 10:36 

### 3-IN

Mercury 

### <0.200 <0.200 2.00

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/04/2013 Page 196 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173339/1-A Concentration Units:mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:ICP5 METHOD BLANK METALS

173517 TestAmerica Chicago

7440-39-3 Barium <1.00 6010B 7440-50-8 Copper <1.00 6010B 7440-47-3 Chromium <1.00 6010B 7440-02-0 Nickel 0.3300 J 6010B 7439-92-1 Lead 0.2580 J 6010B 7440-62-2 Vanadium <0.500 6010B 7440-66-6 Zinc <2.00 6010B

FORM III-IN 

## 01/04/2013 Page 197 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173349/1-A Concentration Units:mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:ICP5 METHOD BLANK METALS

173517 TestAmerica Chicago

7440-39-3 Barium 0.002710 J 6010B 7440-50-8 Copper <0.0100 6010B 7440-47-3 Chromium 0.001210 J 6010B 7440-02-0 Nickel <0.0100 6010B 7439-92-1 Lead 0.002720 J 6010B 7440-62-2 Vanadium <0.00500 6010B 7440-66-6 Zinc <0.0200 6010B

FORM III-IN 

## 01/04/2013 Page 198 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB2 500-173323/1-B Concentration Units:mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:ICP5 METHOD BLANK METALS - TCLP

173518 TestAmerica Chicago

7440-39-3 Barium <0.500 6010B 7440-50-8 Copper <0.0250 6010B 7440-47-3 Chromium <0.0250 6010B 7440-02-0 Nickel <0.0250 6010B 7439-92-1 Lead <0.0500 6010B 7440-62-2 Vanadium <0.0250 6010B 7440-66-6 Zinc <0.100 6010B

FORM III-IN 

## 01/04/2013 Page 199 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173428/7-A Concentration Units:mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:HG6 METHOD BLANK METALS

173572 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/04/2013 Page 200 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB2 500-173323/1-C Concentration Units:mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:HG6 METHOD BLANK METALS - TCLP

173572 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/04/2013 Page 201 of 332

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173393/7-A Concentration Units:mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53342-1

Instrument Code:HG5 METHOD BLANK METALS

173573 TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN 

## 01/04/2013 Page 202 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSA 500-173517/13 P51219Amg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0020 Chromium -0.0022 Copper 0.0054 Lead 0.0008 Nickel 0.0041 Vanadium 0.0081 Zinc 

### 509 Aluminum 500 102 -0.0017 Antimony -0.0012 Arsenic 0.0000 Beryllium 0.0004 Boron 0.0040 Cadmium 479 Calcium 500 96 0.0001 Cobalt 189 Iron 200 95 517 Magnesium 500 103 0.0035 Manganese 0.0125 Molybdenum -0.0053 Potassium 0.0002 Selenium 0.0151 Silicon 0.0000 Silver 0.0079 Sodium 0.0023 Strontium 0.0073 Thallium 0.0014 Tin 0.0008 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 203 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSAB 500-173517/14 P51219Amg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.518 Barium 0.500 104 0.482 Chromium 0.500 96 0.560 Copper 0.500 112 0.0528 Lead 0.0500 106 0.948 Nickel 1.00 95 0.508 Vanadium 0.500 102 0.902 Zinc 1.00 90 

### 511 Aluminum 500 102 0.617 Antimony 0.600 103 0.104 Arsenic 0.100 104 0.481 Beryllium 0.500 96 0.0011 Boron 0.941 Cadmium 1.00 94 479 Calcium 500 96 0.472 Cobalt 0.500 94 191 Iron 200 95 519 Magnesium 500 104 0.501 Manganese 0.500 100 0.0124 Molybdenum -0.0129 Potassium 0.0472 Selenium 0.0500 94 0.0159 Silicon 0.223 Silver 0.200 111 0.0129 Sodium 0.0023 Strontium 0.104 Thallium 0.100 104 0.0020 Tin 0.0009 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 204 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSA 500-173517/76 P51219Amg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0003 Barium 0.0021 Chromium -0.0025 Copper 0.0038 Lead 0.0004 Nickel 0.0041 Vanadium 0.0080 Zinc 

### 507 Aluminum 500 101 0.0003 Antimony -0.0005 Arsenic -0.0001 Beryllium 0.0010 Boron 0.0035 Cadmium 488 Calcium 500 98 0.0000 Cobalt 193 Iron 200 97 522 Magnesium 500 104 0.0045 Manganese 0.0127 Molybdenum -0.0103 Potassium -0.0026 Selenium 0.0155 Silicon 0.0002 Silver 0.0106 Sodium 0.0022 Strontium 0.0042 Thallium -0.0011 Tin 0.0008 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 205 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSAB 500-173517/77 P51219Amg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.508 Barium 0.500 102 0.490 Chromium 0.500 98 0.553 Copper 0.500 111 0.0533 Lead 0.0500 107 0.965 Nickel 1.00 97 0.513 Vanadium 0.500 103 0.935 Zinc 1.00 93 

### 509 Aluminum 500 102 0.623 Antimony 0.600 104 0.104 Arsenic 0.100 104 0.490 Beryllium 0.500 98 0.0012 Boron 0.965 Cadmium 1.00 96 488 Calcium 500 98 0.479 Cobalt 0.500 96 194 Iron 200 97 523 Magnesium 500 105 0.508 Manganese 0.500 102 0.0145 Molybdenum -0.0103 Potassium 0.0481 Selenium 0.0500 96 0.0146 Silicon 0.223 Silver 0.200 111 0.0169 Sodium 0.0022 Strontium 0.108 Thallium 0.100 108 -0.0003 Tin 0.0009 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 206 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSA 500-173518/13 P51219Bmg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0019 Chromium -0.0021 Copper 0.0018 Lead 0.0005 Nickel 0.0039 Vanadium 0.0075 Zinc 

### 509 Aluminum 500 102 -0.0009 Antimony 0.0002 Arsenic -0.0001 Beryllium 0.0007 Boron 0.0025 Cadmium 478 Calcium 500 96 0.0000 Cobalt 189 Iron 200 94 519 Magnesium 500 104 0.0048 Manganese 0.0125 Molybdenum -0.0137 Potassium -0.0021 Selenium 0.0145 Silicon 0.0002 Silver 0.0138 Sodium 0.0022 Strontium 0.0058 Thallium -0.0017 Tin 0.0008 Titanium 0.0025 Total Heavy Metals



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 207 of 332

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53342-1
ICSAB 500-173518/14 P51219Bmg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.518 Barium 0.500 104 0.483 Chromium 0.500 97 0.556 Copper 0.500 111 0.0504 Lead 0.0500 101 0.943 Nickel 1.00 94 0.508 Vanadium 0.500 102 0.902 Zinc 1.00 90 

### 510 Aluminum 500 102 0.613 Antimony 0.600 102 0.107 Arsenic 0.100 107 0.480 Beryllium 0.500 96 0.0009 Boron 0.935 Cadmium 1.00 93 481 Calcium 500 96 0.470 Cobalt 0.500 94 190 Iron 200 95 522 Magnesium 500 104 0.501 Manganese 0.500 100 0.0115 Molybdenum -0.0099 Potassium 0.0483 Selenium 0.0500 97 0.0130 Silicon 0.222 Silver 0.200 111 0.0206 Sodium 0.0022 Strontium 0.104 Thallium 0.100 104 0.0005 Tin 0.0008 Titanium 3.87 Total Heavy Metals 4.05 96



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 208 of 332

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173339/2-A Lab Name: Job No.:500-53342-1 Sample Matrix:Solid LCS Source:M12JSPKIC_00002 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Barium 200 199.5 100 6010B 80 120 Copper 25.0 25.15 101 6010B 80 120 Chromium 20.0 20.20 101 6010B 80 120 Nickel 50.0 49.95 100 6010B 80 120 Lead 10.0 10.14 101 6010B 80 120 Vanadium 50.0 50.42 101 6010B 80 120 Zinc 50.0 49.15 98 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/04/2013 Page 209 of 332

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173349/2-A Lab Name: Job No.:500-53342-1 Sample Matrix:Water LCS Source:M12JSPKIC_00002 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.955 98 6010B 80 120 Copper 0.250 0.2524 101 6010B 80 120 Chromium 0.200 0.1989 99 6010B 80 120 Nickel 0.500 0.4934 99 6010B 80 120 Lead 0.100 0.1010 101 6010B 80 120 Vanadium 0.500 0.4993 100 6010B 80 120 Zinc 0.500 0.4858 97 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/04/2013 Page 210 of 332

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173406/3-A Lab Name: Job No.:500-53342-1 Sample Matrix:Water LCS Source:M12KSPKIC_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.975 99 6010B 80 120 Copper 0.250 0.2464 99 6010B 80 120 Chromium 0.200 0.1969 98 6010B 80 120 Nickel 0.500 0.4873 97 6010B 80 120 Lead 0.100 0.09785 98 6010B 80 120 Vanadium 0.500 0.4959 99 6010B 80 120 Zinc 0.500 0.4782 96 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/04/2013 Page 211 of 332

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173428/8-A Lab Name: Job No.:500-53342-1 Sample Matrix:Water LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Mercury 0.00200 0.002086 104 7470A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/04/2013 Page 212 of 332

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173393/8-A Lab Name: Job No.:500-53342-1 Sample Matrix:Solid LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Mercury 0.167 0.1467 88 ^ 7471A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/04/2013 Page 213 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:03 Method: 3010A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.00044 0.01 Chromium 0.00096 0.01 Copper 0.00106 0.01 Lead 0.00158 0.005 Nickel 0.0019 0.01 Vanadium 0.00062 0.005 Zinc 0.00472 0.02

FORM IX - IN 

## 01/04/2013 Page 214 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:07 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/04/2013 Page 215 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:20 Method: 3050B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Barium 0.119 1 Chromium 0.167 1 Copper 0.271 1 Lead 0.172 0.5 Nickel 0.219 1 Vanadium 0.0759 0.5 Zinc 0.686 2

FORM IX - IN 

## 01/04/2013 Page 216 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:03 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/04/2013 Page 217 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 11/01/2005 15:36 Method: 3010A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.01 0.5 Chromium 0.01 0.025 Copper 0.01 0.025 Lead 0.005 0.05 Nickel 0.01 0.025 Vanadium 0.005 0.025 Zinc 0.02 0.1

FORM IX - IN 

## 01/04/2013 Page 218 of 332

### 9-IN

Instrument ID:ICP5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 01/28/2008 10:37 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.01 0.01 Chromium 0.01 0.01 Copper 0.01 0.01 Lead 0.005 0.005 Nickel 0.01 0.01 Vanadium 0.005 0.005 Zinc 0.02 0.02

FORM IX - IN 

## 01/04/2013 Page 219 of 332

### 9-IN

Instrument ID:HG6 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 08/31/2012 10:08 Method: 7470A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/04/2013 Page 220 of 332

### 9-IN

Instrument ID:HG6 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 08/31/2012 10:08 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/04/2013 Page 221 of 332

### 9-IN

Instrument ID:HG6 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 11/01/2005 11:39 Method: 7470A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.2 2

FORM IX - IN 

## 01/04/2013 Page 222 of 332

### 9-IN

Instrument ID:HG6 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 09/16/2006 08:48 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 1 2

FORM IX - IN 

## 01/04/2013 Page 223 of 332

### 9-IN

Instrument ID:HG5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7471A MDL Date: 08/31/2012 10:15 Method: 7471A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/Kg) (ug/Kg) Mercury 6.37 16.7

FORM IX - IN 

## 01/04/2013 Page 224 of 332

### 9-IN

Instrument ID:HG5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7471A XMDL Date: 08/31/2012 10:16 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/04/2013 Page 225 of 332

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53342-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

ICP5 SDG No.:

(mg/L) 11/19/2012 14:31 METALS

Barium 206010B Copper 206010B Chromium 506010B Nickel 506010B Lead 506010B Vanadium 1006010B Zinc 206010B

FORM XI - IN 

## 01/04/2013 Page 226 of 332

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53342-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG5 SDG No.:

(ug/L) 03/01/2008 11:18 METALS

Mercury 5.07471A

FORM XI - IN 

## 01/04/2013 Page 227 of 332

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53342-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG6 SDG No.:

(ug/L) 11/01/2010 11:39 METALS

Mercury 5.07470A

FORM XI - IN 

## 01/04/2013 Page 228 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 METALS
TestAmerica Chicago
Prep Method:3050B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/18/2012 16:00 173339 MB 500-173339/1-A 100 1 12/18/2012 16:00 173339 LCS 500-173339/2-A 100 1 12/18/2012 16:00 173339 500-53342-1 100 1.1079

FORM XII-IN 

## 01/04/2013 Page 229 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/18/2012 15:30 173349 MB 500-173349/1-A 50 50 12/18/2012 15:30 173349 LCS 500-173349/2-A 50 50 12/18/2012 15:30 173349 500-53342-3 50 50

FORM XII-IN 

## 01/04/2013 Page 230 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/19/2012 08:20 173406 LB2 500-173323/1-B 50 50 12/19/2012 08:20 173406 LCS 500-173406/3-A 50 50 12/19/2012 08:20 173406 500-53342-1 50 50

FORM XII-IN 

## 01/04/2013 Page 231 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 METALS
TestAmerica Chicago
Prep Method:7471A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 14:45 173393 MB 500-173393/7-A 50 0.6 12/19/2012 14:45 173393 LCS 500-173393/8-A 50 0.6 12/19/2012 14:45 173393 500-53342-1 50 0.6182

FORM XII-IN 

## 01/04/2013 Page 232 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 METALS
TestAmerica Chicago
Prep Method:7470A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/19/2012 14:00 173428 MB 500-173428/7-A 25 25 12/19/2012 14:00 173428 LCS 500-173428/8-A 25 25 12/19/2012 14:00 173428 LB2 500-173323/1-C 25 25 12/19/2012 14:00 173428 500-53342-1 25 25 12/19/2012 14:00 173428 500-53342-3 25 25

FORM XII-IN 

## 01/04/2013 Page 233 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

ICP5 12/19/2012 08:45 12/19/2012 17:31 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 08:45 ZZZZZZ 08:51 ZZZZZZ 08:57 ZZZZZZ 09:04 ZZZZZZ 09:10 ZZZZZZ 09:15 ZZZZZZ 09:20 ZZZZZZ 09:28 ZZZZZZ 09:36 ZZZZZZ 1 09:45 XXXXXXX ICV 500-173517/10 1 09:53 XXXXXXX ICB 500-173517/11 1 09:59 XXXXXXX CRI 500-173517/12 1 10:05 XXXXXXX ICSA 500-173517/13 1 10:12 XXXXXXX ICSAB 500-173517/14 1 10:20 XXXXXXX CCV 500-173517/15 1 10:26 XXXXXXX CCB 500-173517/16 1 10:33 XXXXXXX MB 500-173339/1-A T 1 10:39 XXXXXXX LCS 500-173339/2-A T 10:45 ZZZZZZ 10:52 ZZZZZZ 10:58 ZZZZZZ 11:04 ZZZZZZ 11:11 ZZZZZZ 11:17 ZZZZZZ 11:30 ZZZZZZ 11:37 ZZZZZZ 1 11:45 XXXXXXX CCV 500-173517/27 1 11:51 XXXXXXX CCB 500-173517/28 11:57 ZZZZZZ 12:04 ZZZZZZ 12:10 ZZZZZZ 12:16 ZZZZZZ 12:22 ZZZZZZ 12:28 ZZZZZZ 12:35 ZZZZZZ 12:41 ZZZZZZ 12:47 ZZZZZZ 12:53 ZZZZZZ 1 13:02 XXXXXXX CCV 500-173517/39 1 13:08 XXXXXXX CCB 500-173517/40 13:14 ZZZZZZ 13:21 ZZZZZZ



### FORM XIII-IN 

## 01/04/2013 Page 234 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

ICP5 12/19/2012 08:45 12/19/2012 17:31 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 13:27 ZZZZZZ 13:33 ZZZZZZ 1 13:39 XXXXXXX 500-53342-1 T 1 13:52 XXXXXXX MB 500-173349/1-A T 1 13:58 XXXXXXX LCS 500-173349/2-A T 14:04 ZZZZZZ 14:11 ZZZZZZ 14:18 ZZZZZZ 1 14:26 XXXXXXX CCV 500-173517/51 1 14:32 XXXXXXX CCB 500-173517/52 14:38 ZZZZZZ 14:45 ZZZZZZ 14:51 ZZZZZZ 14:57 ZZZZZZ 1 15:03 XXXXXXX 500-53342-3 T 15:14 ZZZZZZ 15:20 ZZZZZZ 15:26 ZZZZZZ 15:33 ZZZZZZ 15:39 ZZZZZZ 1 15:47 XXXXXXX CCV 500-173517/63 1 15:53 XXXXXXX CCB 500-173517/64 16:00 ZZZZZZ 16:06 ZZZZZZ 16:12 ZZZZZZ 16:18 ZZZZZZ 16:25 ZZZZZZ 16:31 ZZZZZZ 16:37 ZZZZZZ 16:43 ZZZZZZ 16:52 CCV 500-173517/73 16:58 CCB 500-173517/74 1 17:04 XXXXXXX CRI 500-173517/75 1 17:10 XXXXXXX ICSA 500-173517/76 1 17:16 XXXXXXX ICSAB 500-173517/77 17:25 CCV 500-173517/78 17:31 CCB 500-173517/79 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 235 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

ICP5 12/19/2012 17:42 12/20/2012 00:26 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 17:42 ZZZZZZ 17:48 ZZZZZZ 17:54 ZZZZZZ 18:01 ZZZZZZ 18:07 ZZZZZZ 18:12 ZZZZZZ 18:17 ZZZZZZ 18:24 ZZZZZZ 18:33 ZZZZZZ 1 18:41 XXXXXXX ICV 500-173518/10 1 18:48 XXXXXXX ICB 500-173518/11 1 18:54 XXXXXXX CRI 500-173518/12 1 19:00 XXXXXXX ICSA 500-173518/13 1 19:06 XXXXXXX ICSAB 500-173518/14 19:15 CCV 500-173518/15 19:21 CCB 500-173518/16 19:27 ZZZZZZ 19:33 ZZZZZZ 19:40 ZZZZZZ 19:46 ZZZZZZ 19:52 ZZZZZZ 19:58 ZZZZZZ 20:04 ZZZZZZ 20:11 ZZZZZZ 20:17 ZZZZZZ 20:23 ZZZZZZ 1 20:32 XXXXXXX CCV 500-173518/27 1 20:38 XXXXXXX CCB 500-173518/28 20:44 ZZZZZZ 20:50 ZZZZZZ 20:56 ZZZZZZ 21:07 ZZZZZZ 1 21:13 XXXXXXX LB2 500-173323/1-B P 1 21:20 XXXXXXX LCS 500-173406/3-A T 21:26 ZZZZZZ 21:32 ZZZZZZ 21:43 ZZZZZZ 21:49 ZZZZZZ 1 21:57 XXXXXXX CCV 500-173518/39 1 22:04 XXXXXXX CCB 500-173518/40 22:10 ZZZZZZ 22:16 ZZZZZZ



### FORM XIII-IN 

## 01/04/2013 Page 236 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

ICP5 12/19/2012 17:42 12/20/2012 00:26 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 22:22 ZZZZZZ 22:29 ZZZZZZ 22:35 ZZZZZZ 1 22:41 XXXXXXX 500-53342-1 P 22:54 ZZZZZZ 23:00 ZZZZZZ 23:06 ZZZZZZ 23:13 ZZZZZZ 1 23:21 XXXXXXX CCV 500-173518/51 1 23:27 XXXXXXX CCB 500-173518/52 23:34 ZZZZZZ 23:40 ZZZZZZ 23:46 ZZZZZZ 23:52 ZZZZZZ 23:59 ZZZZZZ 00:05 ZZZZZZ 00:11 ZZZZZZ 00:19 CCV 500-173518/60 00:26 CCB 500-173518/61 Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 237 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

HG6 12/20/2012 08:12 12/20/2012 10:48 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 08:12 ZZZZZZ 08:14 ZZZZZZ 08:16 ZZZZZZ 08:18 ZZZZZZ 08:20 ZZZZZZ 08:22 ZZZZZZ 1 08:24 X ICV 500-173572/7 1 08:26 X ICB 500-173572/8 1 08:28 X CRA 500-173572/9 08:30 ZZZZZZ 08:32 ZZZZZZ 08:34 ZZZZZZ 08:36 ZZZZZZ 08:39 ZZZZZZ 08:41 ZZZZZZ 08:43 ZZZZZZ 08:45 ZZZZZZ 08:46 ZZZZZZ 08:49 CCV 500-173572/19 08:51 CCB 500-173572/20 08:52 ZZZZZZ 08:54 ZZZZZZ 08:56 ZZZZZZ 08:58 ZZZZZZ 09:00 ZZZZZZ 09:02 ZZZZZZ 09:04 ZZZZZZ 09:06 ZZZZZZ 09:08 ZZZZZZ 09:10 ZZZZZZ 1 09:12 X CCV 500-173572/31 1 09:13 X CCB 500-173572/32 09:15 ZZZZZZ 09:17 ZZZZZZ 09:19 ZZZZZZ 09:21 ZZZZZZ 09:23 ZZZZZZ 09:25 ZZZZZZ 09:26 ZZZZZZ 09:28 ZZZZZZ 09:30 ZZZZZZ 1 09:32 X MB 500-173428/7-A T



### FORM XIII-IN 

## 01/04/2013 Page 238 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

HG6 12/20/2012 08:12 12/20/2012 10:48 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 1 09:34 X CCV 500-173572/43 1 09:36 X CCB 500-173572/44 1 09:38 X LCS 500-173428/8-A T 1 09:40 X LB2 500-173323/1-C P 1 09:42 X 500-53342-1 P 09:44 ZZZZZZ 09:45 ZZZZZZ 09:47 ZZZZZZ 09:49 ZZZZZZ 09:51 ZZZZZZ 09:53 ZZZZZZ 09:55 ZZZZZZ 1 09:57 X CCV 500-173572/55 1 09:59 X CCB 500-173572/56 10:01 ZZZZZZ 10:03 ZZZZZZ 10:05 ZZZZZZ 10:06 ZZZZZZ 10:08 ZZZZZZ 10:10 ZZZZZZ 10:12 ZZZZZZ 10:14 ZZZZZZ 10:16 ZZZZZZ 10:18 ZZZZZZ 1 10:19 X CCV 500-173572/67 1 10:21 X CCB 500-173572/68 10:23 ZZZZZZ 10:25 ZZZZZZ 10:27 ZZZZZZ 1 10:29 X 500-53342-3 T 10:31 ZZZZZZ 10:32 ZZZZZZ 1 10:34 X CCV 500-173572/75 1 10:36 X CCB 500-173572/76 10:38 ZZZZZZ 10:40 ZZZZZZ 10:42 ZZZZZZ 10:44 ZZZZZZ 10:46 CCV 500-173572/81 10:48 CCB 500-173572/82



### FORM XIII-IN 

## 01/04/2013 Page 239 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

HG6 12/20/2012 08:12 12/20/2012 10:48 7470A METALS

Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 240 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

HG5 12/20/2012 08:58 12/20/2012 09:41 7471A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 08:58 X STD01REP1 500-173573/1 IC 09:00 X STD02REP1 500-173573/2 IC 09:01 X STD03REP1 500-173573/3 IC 09:03 X STD04REP1 500-173573/4 IC 09:06 X STD05REP1 500-173573/5 IC 09:07 X STD06REP1 500-173573/6 IC 1 09:11 X ICV 500-173573/7 1 09:12 X ICB 500-173573/8 1 09:14 X CRA 500-173573/9 1 09:16 X MB 500-173393/7-A T 1 09:18 X LCS 500-173393/8-A T 09:20 ZZZZZZ 09:22 ZZZZZZ 09:24 ZZZZZZ 09:26 ZZZZZZ 09:28 ZZZZZZ 09:29 ZZZZZZ 09:31 ZZZZZZ 09:34 ZZZZZZ 1 09:39 X CCV 500-173573/20 1 09:41 X CCB 500-173573/21 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 241 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

HG5 12/20/2012 09:45 12/20/2012 10:44 7471A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 09:45 X STD01REP1 500-173574/1 IC 09:46 X STD02REP1 500-173574/2 IC 09:48 X STD03REP1 500-173574/3 IC 09:50 X STD04REP1 500-173574/4 IC 09:52 X STD05REP1 500-173574/5 IC 09:54 X STD06REP1 500-173574/6 IC 1 09:59 X ICV 500-173574/7 1 10:01 X ICB 500-173574/8 1 10:03 X CRA 500-173574/9 1 10:05 X CCV 500-173574/10 1 10:07 X CCB 500-173574/11 10:09 ZZZZZZ 10:10 ZZZZZZ 10:12 ZZZZZZ 10:14 ZZZZZZ 10:17 ZZZZZZ 10:19 ZZZZZZ 1 10:21 X 500-53342-1 T 10:23 ZZZZZZ 10:24 ZZZZZZ 10:26 ZZZZZZ 1 10:28 X CCV 500-173574/22 1 10:30 X CCB 500-173574/23 10:32 ZZZZZZ 10:34 ZZZZZZ 10:36 ZZZZZZ 10:38 ZZZZZZ 10:40 ZZZZZZ 10:42 CCV 500-173574/29 10:44 CCB 500-173574/30 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 242 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Laird, Rebecca 12/18/12 16:30 12/18/12 16:00 173339 Batch Method: TestAmerica Chicago

3050B Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg InitialAmount FinalAmount M12JSPKIC 00002 CALC NOT SET TO RUN 1 g 100 mL MB 500-173339/1 3050B, 6010B CALC NOT SET TO RUN 1 g 100 mL 1 mL LCS 500-173339/2 3050B, 6010B FC Composite 5 CALC NOT SET TO RUN 1.1079 g 100 mL 500-53342-A-1 3050B, 6010B T

Batch Notes Analyst BL Balance ID C-1966 First End time 1630 Hydrogen peroxide lot number L08A06 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L08022 Hood ID or number 3 Hot Block ID number 8 Oven, Bath or Block Temperature 1 90 Degrees C Oven, Bath or Block Temperature 2 90 Degrees C Pipette ID 1628 First Start time 1600 ID number of the thermometer J59717 Digestion Tube/Cup Lot # MF06LKK01
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

## 01/04/2013 Page 243 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Laird, Rebecca 12/18/12 16:00 12/18/12 15:30 173349 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12JSPKIC 00002 50 mL 50 mL MB 500-173349/1 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173349/2 3010A, 6010B FC EB 5 50 mL 50 mL 500-53342-E-3 3010A, 6010B T
Batch Notes First End time 1600 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L08022 Hot Block ID number 4 Pipette ID 1627 First Start time 1530 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

## 01/04/2013 Page 244 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Hudson, Lawrence A 12/19/12 08:50 12/19/12 08:20 173406 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment 50 mL 50 mL T-748 LB2 500-173323/1-A 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173406/3 3010A, 6010B FC Composite 5 50 mL 50 mL LB2 T-748 500-53342-A-1-C 3010A, 6010B P
Batch Notes Batch Comment T-744, T-748 First End time 0850 Lot # of hydrochloric acid 0000013500 Lot # of Nitric Acid L10022 Hot Block ID number 4 Pipette ID 1627 First Start time 0820 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description P TCLP



### Page 1 of 1 6010B 

## 01/04/2013 Page 245 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/19/12 16:00 12/19/12 14:00 173428 Batch Method: TestAmerica Chicago

7470A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 25 mL 25 mL MB 500-173428/7 7470A, 7470A 25 mL 25 mL 0.00005 mL LCS 500-173428/8 7470A, 7470A 25 mL 25 mL LB2 500-173323/1-A 7470A, 7470A FC Composite 5 25 mL 25 mL 500-53342-A-1-C 7470A, 7470A P FC EB 5 25 mL 25 mL 500-53342-E-3 7470A, 7470A T
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 6 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 88 Oven, Bath or Block Temperature 2 88 Pipette ID 2240 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Temperature 88 Celsius ID number of the thermometer hb305412 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Visual ck - digestate F.V. consistency OK



### Page 1 of 2 7470A 

## 01/04/2013 Page 246 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/19/12 16:00 12/19/12 14:00 173428 Batch Method: TestAmerica Chicago

7470A
Basis Basis Description T Total/NA P TCLP



### Page 2 of 2 7470A 

## 01/04/2013 Page 247 of 332

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/19/12 15:15 12/19/12 14:45 173393 Batch Method: TestAmerica Chicago

7471A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 0.6 g 50 mL MB 500-173393/7 7471A, 7471A 0.6 g 50 mL 0.0001 mL LCS 500-173393/8 7471A, 7471A FC Composite 5 0.6182 g 50 mL 500-53342-A-1 7471A, 7471A T
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Balance ID c0975 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Blank Soil Lot Number teflon strip_00001 Filter Lot # 21782182 Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 2 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 90 Oven, Bath or Block Temperature 2 90 Pipette ID 1631 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Syringe Lot # 1292669 ID number of the thermometer j60025 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description T Total/NA 

### Page 1 of 1 7471A 

## 01/04/2013 Page 248 of 332

# GENERAL CHEMISTRY

01/04/2013 Page 249 of 332

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID GENERAL CHEMISTRY

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53342-1 TestAmerica Chicago

500-53342-1 FC Composite 5 500-53342-2 FC Composite 5 500-53342-3 FC EB 5

Comments:



## 01/04/2013 Page 250 of 332

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40 500-53342-1 FC Composite 5

Solid 12/17/2012 14:50 Date Sampled: Reporting Basis: DRY 

### GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 30.0

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <3.33 mg/Kg 3.33 1.30 1 7196A 57-12-5 Cyanide, Total 0.905 J mg/Kg 1.59 0.524 1 9014 18496-25-8 Sulfide 798 mg/Kg 82.8 13.2 1 9034 HEM (Oil & Grease) 13200 mg/Kg 1650 732 1 9071B



### FORM IB-IN 

## 01/04/2013 Page 251 of 332

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-1

Date Received: 12/18/2012 09:40 500-53342-1 FC Composite 5

Solid 12/17/2012 14:50 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result Sulfide, Reactive <48.7 mg/Kg 48.7 3.80 1 9034 Flashpoint >176 Degrees F 40.0 40.0 1 1010 pH 9.59 SU 0.200 0.200 1 9045C % Moisture 70.0 % 0.100 0.100 1 SM 2540G Total Solids 30.0 % 0.100 0.100 1 SM 2540G



### FORM IB-IN 

## 01/04/2013 Page 252 of 332

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53342-3

Date Received: 12/18/2012 09:40 500-53342-1 FC EB 5

Water 12/17/2012 14:30 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <0.0100 mg/L 0.0100 0.00325 1 7196A 57-12-5 Cyanide, Total <0.0100 mg/L 0.0100 0.00331 1 9014 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1 9034 HEM (Oil & Grease) <5.36 mg/L 5.36 1.55 1 1664A 18496-25-8 Sulfide <1.00 mg/L 1.00 0.230 1 9034



### FORM IB-IN 

## 01/04/2013 Page 253 of 332

### 2-IN

Lab Name: Job No.: SDG No.: 500-53342-1
Analyst:KD Batch Start Date:12/18/2012 Reporting Units:mg/L Analytical Batch No.: 173293 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) RecoveryLimits QualReagent 

### TestAmerica Chicago

ICV 11:20 Chromium, hexavalent 0.2602 0.250 104 90-110 WSTCR2_00008 1ICB 11:20 Chromium, hexavalent <0.0100 2CCV 11:23 Chromium, hexavalent 0.4934 0.500 99 90-110 WSTCR1_00008 8CCB 11:24 Chromium, hexavalent <0.0100 9



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 254 of 332

### 2-IN

Lab Name: Job No.: SDG No.: 500-53342-1
Analyst:APW Batch Start Date:12/27/2012 Reporting Units:mg/L Analytical Batch No.: 174027 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) RecoveryLimits QualReagent 

### TestAmerica Chicago

ICV 12:40 Chromium, hexavalent 0.2548 0.250 102 90-110 WSTCR2_00008 1ICB 12:40 Chromium, hexavalent <0.0200 2CCV 12:46 Chromium, hexavalent 0.5130 0.500 103 90-110 WSTCR1_00008 10CCB 12:46 Chromium, hexavalent <0.0200 11CCV 12:51 Chromium, hexavalent 0.5138 0.500 103 90-110 WSTCR1_00008 18CCB 12:52 Chromium, hexavalent <0.0200 19



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 255 of 332

### 2-IN

Lab Name: Job No.: SDG No.: 500-53342-1
Analyst:EAT Batch Start Date:12/27/2012 Reporting Units:mg/L Analytical Batch No.: 174042 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) RecoveryLimits QualReagent 

### TestAmerica Chicago

ICV 14:40 Cyanide, Total 0.1006 0.100 101 90-110 WSTINCN2_00563 1ICB 14:40 Cyanide, Total <0.0100 2CCV 14:43 Cyanide, Total 0.1942 0.200 97 90-110 WSTINCN1_00571 13CCB 14:43 Cyanide, Total <0.0100 14CCV 14:47 Cyanide, Total 0.1938 0.200 97 90-110 WSTINCN1_00571 25CCB 14:47 Cyanide, Total <0.0100 26



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 256 of 332

### 2-IN

Lab Name: Job No.: SDG No.: 500-53342-1
Analyst:EAT Batch Start Date:12/28/2012 Reporting Units:mg/L Analytical Batch No.: 174173 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) RecoveryLimits QualReagent 

### TestAmerica Chicago

ICV 15:25 Cyanide, Total 0.1017 0.100 102 90-110 WSTINCN2_00564 1ICB 15:25 Cyanide, Total <0.0100 2CCV 15:29 Cyanide, Total 0.1954 0.200 98 90-110 WSTINCN1_00572 13CCB 15:29 Cyanide, Total <0.0100 14CCV 15:33 Cyanide, Total 0.1951 0.200 98 90-110 WSTINCN1_00572 25CCB 15:33 Cyanide, Total <0.0100 26



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 257 of 332

### Lab Name: Job No.: SDG No.:

Method Analyte ResultQual Dil 

### 3-IN

500-53342-1

Lab Sample ID Units 

### TestAmerica Chicago METHOD BLANK GENERAL CHEMISTRY

RL
Batch ID:173459 Date:12/21/2012 09:55 173450 Date:12/21/2012 05:05 Prep Batch: <5.00 MB 500-173450/1-A 1 5.00 mg/L HEM (Oil & Grease) 1664A Batch ID:173293 Date:12/18/2012 11:21 <0.0100 MB 500-173293/3 1 0.0100 mg/L Chromium, hexavalent 7196A Batch ID:174027 Date:12/27/2012 12:41 173790 Date:12/22/2012 12:00 Prep Batch: <1.00 MB 500-173790/1-A 1 1.00 mg/Kg Chromium, hexavalent 7196A Batch ID:174042 Date:12/27/2012 14:40 173980 Date:12/27/2012 09:50 Prep Batch:<0.0100 MB 500-173980/1-A 1 0.0100 mg/L Cyanide, Total 9014 Batch ID:174173 Date:12/28/2012 15:30 174096 Date:12/28/2012 11:20 Prep Batch:<0.500 MB 500-174096/12-A 1 0.500 mg/Kg Cyanide, Total 9014 Batch ID:173472 Date:12/19/2012 12:15 173290 Date:12/19/2012 10:05 Prep Batch: <50.0 MB 500-173290/1-A 1 50.0 mg/Kg Sulfide, Reactive 9034 Batch ID:173474 Date:12/19/2012 13:35 173291 Date:12/19/2012 11:25 Prep Batch: <25.0 MB 500-173291/1-A 1 25.0 mg/Kg Sulfide 9034 Batch ID:173845 Date:12/24/2012 13:19 173844 Date:12/24/2012 08:00 Prep Batch: <1.00 MB 500-173844/1-A 1 1.00 mg/L Sulfide, Reactive 9034 Batch ID:173846 Date:12/24/2012 13:19 <1.00 MB 500-173846/1 1 1.00 mg/L Sulfide 9034 Batch ID:173330 Date:12/19/2012 09:20 173324 Date:12/19/2012 05:10 Prep Batch: <500 MB 500-173324/1-A 1 500 mg/Kg HEM (Oil & Grease) 9071B



### FORM III-IN 

## 01/04/2013 Page 258 of 332

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53342-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173293 Date:12/18/2012 11:22 Chromium, hexavalent 7196A mg/L <0.0100 500-53342-3 7196A 500-53342-3 MS Chromium, hexavalent 0.2502 mg/L 0.250 85-115 100



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/04/2013 Page 259 of 332

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53342-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE DUPLICATE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173293 Date:12/18/2012 11:23 7196A 500-53342-3 MSD Chromium, hexavalent 0.2555 mg/L 0.250 102 85-115 2 20



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/04/2013 Page 260 of 332

### 7A-IN

Job No.:500-53342-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Solid TestAmerica Chicago

Batch ID:174027 Date:12/27/2012 12:42 173790 Date:12/22/2012 12:00 Prep Batch: LCS Source: WSTCR2_00008 10.0 92 7196A LCS 500-173790/2- A Chromium, hexavalent 9.188 mg/Kg 80-120

Batch ID:174027 Date:12/27/2012 12:42 173790 Date:12/22/2012 12:00 Prep Batch: LCS Source: WSTCR13_00629 676 99 7196A LCS 500-173790/3- A Chromium, hexavalent 669.0 mg/Kg 80-120

Batch ID:174173 Date:12/28/2012 15:30 174096 Date:12/28/2012 11:20 Prep Batch: LCS Source: WSTINCN2_00564 5.00 107 9014 LCS 500-174096/13 -A Cyanide, Total 5.325 mg/Kg 80-120

Batch ID:173472 Date:12/19/2012 12:15 173290 Date:12/19/2012 10:10 Prep Batch: LCS Source: WSTSF1_00036 180 94 9034 LCS 500-173290/2- A Sulfide, Reactive 168.6 mg/Kg 80-120

Batch ID:173474 Date:12/19/2012 13:35 173291 Date:12/19/2012 11:25 Prep Batch: LCS Source: WSTSF1_00036 180 93 9034 LCS 500-173291/2- A Sulfide 168.3 mg/Kg 80-120

Batch ID:173330 Date:12/19/2012 09:31 173324 Date:12/19/2012 05:10 Prep Batch: LCS Source: 1664 HEM_00060 4000 102 9071B LCS 500-173324/2- A HEM (Oil & Grease) 4090 mg/Kg 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 261 of 332

### 7A-IN

Job No.:500-53342-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Water TestAmerica Chicago

Batch ID:173459 Date:12/21/2012 09:58 173450 Date:12/21/2012 05:16 Prep Batch: LCS Source: 1664 HEM_00060 40.0 92 1664A LCS 500-173450/2- A HEM (Oil & Grease) 36.70 mg/L 78-114

Batch ID:173293 Date:12/18/2012 11:21 LCS Source: WSTCR2_00008 0.250 106 7196A LCS 500-173293/4 Chromium, hexavalent 0.2652 mg/L 85-115 Batch ID:174042 Date:12/27/2012 14:40 173980 Date:12/27/2012 09:50 Prep Batch: LCS Source: WSTINCN2_00563 0.100 107 9014 LCS 500-173980/2- A Cyanide, Total 0.1066 mg/L 80-120

Batch ID:173846 Date:12/24/2012 13:20 LCS Source: WSTSF1_00036 3.60 104 9034 LCS 500-173846/2 Sulfide 3.760 mg/L 80-120 Batch ID:173845 Date:12/24/2012 13:29 173844 Date:12/24/2012 08:15 Prep Batch: LCS Source: WSTSF1_00036 3.60 105 9034 LCS 500-173844/2- A Sulfide, Reactive 3.767 mg/L 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/04/2013 Page 262 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 10:43 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/04/2013 Page 263 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:44 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/04/2013 Page 264 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 14:44 Method: 3060A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Chromium, hexavalent 0.389 1

FORM IX - IN 

## 01/04/2013 Page 265 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:45 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.02

FORM IX - IN 

## 01/04/2013 Page 266 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:18 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Cyanide, Total 0.165 0.5

FORM IX - IN 

## 01/04/2013 Page 267 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:19 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/04/2013 Page 268 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:22 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/04/2013 Page 269 of 332

### 9-IN

Instrument ID:SPEC5 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:22 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/04/2013 Page 270 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 16:25 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide, Reactive 3.9 50

FORM IX - IN 

## 01/04/2013 Page 271 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 01/02/2006 09:18 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide, Reactive 1 1

FORM IX - IN 

## 01/04/2013 Page 272 of 332

### 9-IN

Instrument ID:FP4 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1010 MDL Date: 11/11/2005 10:25 Method: Analyte Wavelength/ Mass RL MDL (Degrees (Degrees F) Flashpoint 40 40

FORM IX - IN 

## 01/04/2013 Page 273 of 332

### 9-IN

Instrument ID:NoEquip 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1664A MDL Date: 05/29/2012 15:22 Method: 1664A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) HEM (Oil & Grease) 1.45 5

FORM IX - IN 

## 01/04/2013 Page 274 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:57 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide 0.23 1

FORM IX - IN 

## 01/04/2013 Page 275 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:59 Method: 9030B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide 4 25

FORM IX - IN 

## 01/04/2013 Page 276 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9045C MDL Date: 11/01/2005 06:06 Method: Analyte Wavelength/ Mass RL MDL (SU) (SU) pH 0.2 0.2

FORM IX - IN 

## 01/04/2013 Page 277 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9071B MDL Date: 05/29/2012 15:24 Method: 9071B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) HEM (Oil & Grease) 222 500

FORM IX - IN 

## 01/04/2013 Page 278 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

Moisture MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) Percent Moisture 0.1 0.1 Percent Solids 0.1 0.1

FORM IX - IN 

## 01/04/2013 Page 279 of 332

### 9-IN

Instrument ID:NOEQUIP 500-53342-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

SM 2540G MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) % Moisture 0.1 0.1 Total Solids 0.1 0.1

FORM IX - IN 

## 01/04/2013 Page 280 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 10:05 173290 MB 500-173290/1-A 10 10.0000 12/19/2012 10:10 173290 LCS 500-173290/2-A 10 10.0000 12/19/2012 10:50 173290 500-53342-1 10 10.2666

FORM XII-IN 

## 01/04/2013 Page 281 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:3060A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/22/2012 12:00 173790 MB 500-173790/1-A 100 2.5 12/22/2012 12:00 173790 LCS 500-173790/2-A 100 2.5 12/22/2012 12:00 173790 LCS 500-173790/3-A 100 2.5 12/22/2012 12:00 173790 500-53342-1 100 2.5007

FORM XII-IN 

## 01/04/2013 Page 282 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/24/2012 08:00 173844 MB 500-173844/1-A 250 250 12/24/2012 08:15 173844 LCS 500-173844/2-A 250 250 12/24/2012 08:30 173844 500-53342-3 250 250

FORM XII-IN 

## 01/04/2013 Page 283 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/27/2012 09:50 173980 MB 500-173980/1-A 50 50 12/27/2012 09:50 173980 LCS 500-173980/2-A 50 50 12/27/2012 09:50 173980 500-53342-3 50 50

FORM XII-IN 

## 01/04/2013 Page 284 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/28/2012 11:20 174096 MB 500-174096/12-A 50 1.0000 12/28/2012 11:20 174096 LCS 500-174096/13-A 50 1.0000 12/28/2012 11:20 174096 500-53342-1 50 1.0495

FORM XII-IN 

## 01/04/2013 Page 285 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9030B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 11:25 173291 MB 500-173291/1-A 10 10.0000 12/19/2012 11:25 173291 LCS 500-173291/2-A 10 10.0000 12/19/2012 11:25 173291 500-53342-1 10 10.0683

FORM XII-IN 

## 01/04/2013 Page 286 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9071B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 05:10 173324 MB 500-173324/1-A 10 10 12/19/2012 05:10 173324 LCS 500-173324/2-A 10 10 12/19/2012 05:10 173324 500-53342-1 10 10.1047

FORM XII-IN 

## 01/04/2013 Page 287 of 332

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53342-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:1664A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/21/2012 05:05 173450 MB 500-173450/1-A 1000 1000 12/21/2012 05:16 173450 LCS 500-173450/2-A 1000 1000 12/21/2012 07:09 173450 500-53342-3 1000 933

FORM XII-IN 

## 01/04/2013 Page 288 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

SPEC5 12/18/2012 11:20 12/18/2012 11:24 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 11:20 X ICV 500-173293/1 1 11:20 X ICB 500-173293/2 1 11:21 X MB 500-173293/3 T 1 11:21 X LCS 500-173293/4 T 1 11:22 X 500-53342-3 T 1 11:22 X 500-53342-3 MS T 1 11:23 X 500-53342-3 MSD T 1 11:23 X CCV 500-173293/8 1 11:24 X CCB 500-173293/9 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 289 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

SPEC5 12/27/2012 12:40 12/27/2012 12:59 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 12:40 X ICV 500-174027/1 1 12:40 X ICB 500-174027/2 1 12:41 X MB 500-173790/1-A T 1 12:42 X LCS 500-173790/2-A T 50 12:42 X LCS 500-173790/3-A T 12:43 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:45 ZZZZZZ 1 12:46 X CCV 500-174027/10 1 12:46 X CCB 500-174027/11 12:47 ZZZZZZ 12:48 ZZZZZZ 12:48 ZZZZZZ 12:49 ZZZZZZ 1 12:50 X 500-53342-1 T 12:51 ZZZZZZ 1 12:51 X CCV 500-174027/18 1 12:52 X CCB 500-174027/19 12:53 ZZZZZZ 12:53 ZZZZZZ 12:54 ZZZZZZ 12:55 ZZZZZZ 12:55 ZZZZZZ 12:56 ZZZZZZ 12:57 ZZZZZZ 12:57 CCV 500-174027/27 12:58 CCB 500-174027/28 12:59 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 290 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

SPEC5 12/27/2012 14:40 12/27/2012 14:49 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 14:40 X ICV 500-174042/1 1 14:40 X ICB 500-174042/2 1 14:40 X MB 500-173980/1-A T 1 14:40 X LCS 500-173980/2-A T 14:41 ZZZZZZ 14:41 ZZZZZZ 14:41 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:43 ZZZZZZ 1 14:43 X CCV 500-174042/13 1 14:43 X CCB 500-174042/14 14:44 ZZZZZZ 1 14:44 X 500-53342-3 T 14:44 ZZZZZZ 14:44 ZZZZZZ 14:45 ZZZZZZ 14:45 ZZZZZZ 14:45 ZZZZZZ 14:46 ZZZZZZ 14:46 ZZZZZZ 14:46 ZZZZZZ 1 14:47 X CCV 500-174042/25 1 14:47 X CCB 500-174042/26 14:47 ZZZZZZ 14:47 ZZZZZZ 14:48 ZZZZZZ 14:48 ZZZZZZ 14:48 ZZZZZZ 14:49 ZZZZZZ 14:49 CCV 500-174042/33 14:49 CCB 500-174042/34 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 291 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

SPEC5 12/28/2012 15:25 12/28/2012 15:34 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 15:25 X ICV 500-174173/1 1 15:25 X ICB 500-174173/2 15:25 ZZZZZZ 15:26 ZZZZZZ 15:26 ZZZZZZ 15:26 ZZZZZZ 15:27 ZZZZZZ 15:27 ZZZZZZ 15:27 ZZZZZZ 15:28 ZZZZZZ 15:28 ZZZZZZ 15:28 ZZZZZZ 1 15:29 X CCV 500-174173/13 1 15:29 X CCB 500-174173/14 15:29 ZZZZZZ 1 15:30 X MB 500-174096/12-A T 1 15:30 X LCS 500-174096/13-A T 15:30 ZZZZZZ 1 15:31 X 500-53342-1 T 15:31 ZZZZZZ 15:31 ZZZZZZ 15:32 ZZZZZZ 15:32 ZZZZZZ 15:32 ZZZZZZ 1 15:33 X CCV 500-174173/25 1 15:33 X CCB 500-174173/26 15:33 ZZZZZZ 15:34 ZZZZZZ 15:34 ZZZZZZ 15:34 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 292 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 12:15 12/19/2012 12:24 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 12:15 X MB 500-173290/1-A T 1 12:15 X LCS 500-173290/2-A T 12:16 ZZZZZZ 12:17 ZZZZZZ 12:17 ZZZZZZ 12:18 ZZZZZZ 12:19 ZZZZZZ 1 12:19 X 500-53342-1 T 12:20 ZZZZZZ 12:21 ZZZZZZ 12:22 ZZZZZZ 12:22 ZZZZZZ 12:23 ZZZZZZ 12:24 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 293 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/24/2012 13:19 12/24/2012 13:51 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 13:19 X MB 500-173844/1-A T 1 13:29 X LCS 500-173844/2-A T 1 13:40 X 500-53342-3 T 13:51 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 294 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

FP4 12/20/2012 10:00 12/20/2012 13:53 1010 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes F P T y p e 10:00 ZZZZZZ 1 11:00 X 500-53342-1 T 13:53 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 295 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1
NoEquip 12/21/2012 09:55 12/21/2012 11:16 1664A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 09:55 X MB 500-173450/1-A T 1 09:58 X LCS 500-173450/2-A T 10:02 ZZZZZZ 10:06 ZZZZZZ 10:09 ZZZZZZ 10:13 ZZZZZZ 10:17 ZZZZZZ 10:20 ZZZZZZ 10:24 ZZZZZZ 10:28 ZZZZZZ 10:31 ZZZZZZ 1 10:35 X 500-53342-3 T 10:39 ZZZZZZ 10:43 ZZZZZZ 10:46 ZZZZZZ 10:50 ZZZZZZ 10:54 ZZZZZZ 10:57 ZZZZZZ 11:01 ZZZZZZ 11:05 ZZZZZZ 11:08 ZZZZZZ 11:12 ZZZZZZ 11:16 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 296 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 13:35 12/19/2012 13:39 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 13:35 X MB 500-173291/1-A T 1 13:35 X LCS 500-173291/2-A T 13:36 ZZZZZZ 13:36 ZZZZZZ 13:37 ZZZZZZ 1 13:38 X 500-53342-1 T 13:38 ZZZZZZ 13:39 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 297 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/24/2012 13:19 12/24/2012 14:00 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 13:19 X MB 500-173846/1 T 1 13:20 X LCS 500-173846/2 T 13:22 ZZZZZZ 13:24 ZZZZZZ 13:26 ZZZZZZ 13:28 ZZZZZZ 13:30 ZZZZZZ 13:32 ZZZZZZ 13:33 ZZZZZZ 13:35 ZZZZZZ 13:37 ZZZZZZ 13:39 ZZZZZZ 13:41 ZZZZZZ 13:43 ZZZZZZ 13:45 ZZZZZZ 13:47 ZZZZZZ 13:48 ZZZZZZ 13:50 ZZZZZZ 13:52 ZZZZZZ 13:54 ZZZZZZ 13:56 ZZZZZZ 1 13:58 X 500-53342-3 T 14:00 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 13:35 12/20/2012 17:10 9045C GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes p H T y p e 13:35 ZZZZZZ 13:41 ZZZZZZ 13:47 ZZZZZZ 13:53 ZZZZZZ 13:59 ZZZZZZ 18:30 ZZZZZZ 19:29 ZZZZZZ 20:28 ZZZZZZ 21:28 ZZZZZZ 22:27 ZZZZZZ 23:26 ZZZZZZ 00:25 ZZZZZZ 01:24 ZZZZZZ 02:23 ZZZZZZ 03:22 ZZZZZZ 04:22 ZZZZZZ 05:21 ZZZZZZ 06:20 ZZZZZZ 07:19 ZZZZZZ 08:18 ZZZZZZ 09:17 ZZZZZZ 10:16 ZZZZZZ 11:16 ZZZZZZ 12:15 ZZZZZZ 13:14 ZZZZZZ 14:13 ZZZZZZ 15:12 ZZZZZZ 16:11 ZZZZZZ 1 17:10 X 500-53342-1 T Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 09:20 12/19/2012 11:23 9071B GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 09:20 X MB 500-173324/1-A T 1 09:31 X LCS 500-173324/2-A T 09:42 ZZZZZZ 09:53 ZZZZZZ 10:05 ZZZZZZ 10:16 ZZZZZZ 10:27 ZZZZZZ 10:38 ZZZZZZ 10:50 ZZZZZZ 11:01 ZZZZZZ 11:12 ZZZZZZ 1 11:23 X 500-53342-1 T Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 08:40 12/19/2012 08:40 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 1 08:40 XX 500-53342-1 T Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/21/2012 07:08 12/21/2012 13:07 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 07:08 ZZZZZZ 07:08 ZZZZZZ 07:08 ZZZZZZ 07:08 ZZZZZZ 07:08 ZZZZZZ 07:08 ZZZZZZ 07:08 ZZZZZZ 1 07:20 XX 500-53342-2 T 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 08:54 ZZZZZZ 13:01 ZZZZZZ 13:01 ZZZZZZ 13:07 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/18/2012 07:13 12/18/2012 11:45 SM 2540G GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes M o i s t T y p e 07:13 ZZZZZZ 07:13 ZZZZZZ 07:13 ZZZZZZ 07:13 ZZZZZZ 07:13 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 08:04 ZZZZZZ 1 09:57 X 500-53342-1 T 09:57 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ 11:45 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/04/2013 Page 303 of 332

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53342-1

NOEQUIP 12/19/2012 07:31 12/19/2012 07:31 SM 2540G GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes T S T y p e 1 07:31 X 500-53342-1 T Prep Types T = Total/NA



### FORM XIII-IN 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Deb, Khona 12/18/12 11:25 12/18/12 11:20 173293 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL 100 mL Color Resp. is Blank 25 uL ICV 500-173293/1 7196A 100 mL 100 mL Color Resp. is Blank ICB 500-173293/2 7196A 100 mL 100 mL Color Resp. is Blank MB 500-173293/3 7196A 100 mL 100 mL Color Resp. is Blank 25 uL LCS 500-173293/4 7196A FC EB 5 100 mL 100 mL Color Resp. is Blank 500-53342-F-3 7196A T FC EB 5 100 mL 100 mL Color Resp. is Blank 25 uL 500-53342-F-3 MS 7196A T FC EB 5 100 mL 100 mL Color Resp. is Blank 25 uL 500-53342-F-3 MSD 7196A T 100 mL 100 mL Color Resp. is Blank 50 uL CCV 500-173293/8 7196A 100 mL 100 mL Color Resp. is Blank CCB 500-173293/9 7196A

Batch Notes Batch Comment filter paper lot# 100232 Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number Hexa Chrome Color Reagent-00007 First End time See Start Date/Time First Start time See Start Date/Time Sulfuric Acid Reagent ID Number H2SO4 00007
Basis Basis Description T Total/NA



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500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/27/12 13:00 12/22/12 12:00 173790 Batch Method: TestAmerica Chicago

3060A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTCR13 00629 WSTCR2 00008 AnalysisComment 2.5 g 100 mL MB 500-173790/1 3060A, 7196A 2.5 g 100 mL 25 uL soluble LCS 500-173790/2 3060A, 7196A 2.5 g 100 mL 100 mL soluble 0.0105 LCS 500-173790/3 3060A, 7196A FC Composite 5 2.5007 g 100 mL 500-53342-A-1 3060A, 7196A T
Batch Notes Alkaline Digestion Solution Reagent ID CR6digestion_00028 Batch Comment Filter Paper Lot # 100727 First End time see above Potassium Chromate Lot # K00741 Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002 Lead Chromate Lot # 15813PE Lead Chromate Vendor ID Lead(II)Chrom_00001 Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002) Magnesium Chloride Vendor JT Baker First Start time see above Ending Temperature 90 Celsius Starting Temperature 90 Celsius
Basis Basis Description T Total/NA



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500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/27/12 13:00 12/27/12 12:40 174027 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL Color Resp. is Blank 25 uL ICV 500-174027/1 7196A Color Resp. is Blank ICB 500-174027/2 7196A Color Resp. is Blank MB 500-173790/1-A 7196A Color Resp. is Blank LCS 500-173790/2-A 7196A Color Resp. is Blank LCS 500-173790/3-A 7196A 100 mL Color Resp. is Blank 50 uL CCV 500-174027/10 7196A Color Resp. is Blank CCB 500-174027/11 7196A FC Composite 5 Color Resp. is Blank 500-53342-A-1-I 7196A T 100 mL Color Resp. is Blank 50 uL CCV 500-174027/18 7196A Color Resp. is Blank CCB 500-174027/19 7196A

Batch Notes Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number CR+6 ColorRGT_00007 Sulfuric Acid Reagent ID Number H2SO4_00007
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 01/03/13 11:20 12/27/12 09:50 173980 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00563 50 mL 50 mL y MB 500-173980/1 9010B, 9014 50 mL 50 mL y 500 uL LCS 500-173980/2 9010B, 9014 FC EB 5 50 mL 50 mL y 500-53342-D-3 9010B, 9014 T
Batch Notes Bismuth Nitrate Lot # BismuthNO3_00018 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA



### Page 1 of 1 9014 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/27/12 14:50 12/27/12 14:40 174042 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00571 WSTINCN2 00563 25 mL 25 mL 250 uL ICV 500-174042/1 9014 25 mL 25 mL 500 uL CCV 500-174042/13 9014 25 mL 25 mL 500 uL CCV 500-174042/25 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/28/12 12:50 12/28/12 11:20 174096 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00564 1.0000 g 50 mL y MB 500-174096/12 9010B, 9014 1.0000 g 50 mL y 500 uL LCS 500-174096/13 9010B, 9014 FC Composite 5 1.0495 g 50 mL y 500-53342-A-1 9010B, 9014 T
Batch Notes Bismuth Nitrate Lot # BismuthNO3_00018 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA



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500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/28/12 15:35 12/28/12 15:25 174173 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00572 WSTINCN2 00564 25 mL 25 mL 250 uL ICV 500-174173/1 9014 25 mL 25 mL 500 uL CCV 500-174173/13 9014 25 mL 25 mL 500 uL CCV 500-174173/25 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 11:15 12/19/12 10:05 173290 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-173290/1 7.3.4, 9034 10.0000 g 10 mL 10 mL LCS 500-173290/2 7.3.4, 9034 FC Composite 5 10.2666 g 10 mL 500-53342-A-1 7.3.4, 9034 T
Batch Notes Batch Comment Balance ID # 2489
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 12:25 12/19/12 12:15 173472 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount 10 mL 5 mL 4.86 mL OK 10 mL MB 500-173290/1-A 9034 10 mL 5 mL 0.44 mL OK 10 mL LCS 500-173290/2-A 9034 FC Composite 5 10 mL 5 mL 4.82 mL OK 10 mL 500-53342-A-1-A 9034 T
Batch Notes Normality of Iodine Solution 0.0232 N Nominal Amount Used 10 g Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 09:00 12/24/12 08:00 173844 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 250 mL 250 mL MB 500-173844/1 7.3.4, 9034 250 mL 250 mL LCS 500-173844/2 7.3.4, 9034 FC EB 5 250 mL 250 mL 500-53342-G-3 7.3.4, 9034 T
Batch Notes

Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 14:02 12/24/12 13:19 173845 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036 250 mL 5 mL 4.91 mL OK 250 mL MB 500-173844/1-A 9034 250 mL 5 mL 2.49 mL OK 250 mL 5 mL LCS 500-173844/2-A 9034 FC EB 5 250 mL 5 mL 5.10 mL OK 250 mL 500-53342-G-3-A 9034 T
Batch Notes Normality of Iodine Solution 0.0240 N Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/20/12 15:50 12/20/12 10:00 173625 Batch Method: TestAmerica Chicago

1010 Lab Sample ID Client Sample IDMethod ChainBasisAnalysisComment FC Composite 5 gray clay 500-53342-A-1 1010 T
Batch Notes Equipment ID HFP 339
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/21/12 09:25 12/21/12 05:05 173450 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis GrossWeight TareWeight InitialAmount FinalAmount 1390 g 390 g 1000 mL 1000 mL MB 500-173450/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL LCS 500-173450/2 1664A, 1664A FC EB 5 1320 g 387 g 933 mL 1000 mL 500-53342-H-3 1664A, 1664A T
Batch Notes Batch Comment phase separating filter lot # 6711653 Concentration End Time See end date/time Concentration Start Time See start date/time Person's name who did the concentration See analyst name Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, pf-70610210 Evaporator Temperature 50 DEG. Degrees C Extraction Analyst see analyst name Sulfuric Acid Lot Number MALG35029 Hexane Lot# HEXANES_00012 Manifold ID 1851 Methanol Lot Number Methanol_00007 Na2SO4 Lot Number Na2SO4_00006 Nominal Amount Used 1000 mL Sufficient volume for MS/MSD? NO
Basis Basis Description T Total/NA



### Page 1 of 1 1664A 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/21/12 11:20 12/21/12 09:55 173459 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 1000 mL 1000 mL 76 2.3144 g 2.3152 g 2.3154 g MB 500-173450/1-A 1664A 1000 mL 1000 mL 77 6.2848 g 6.3214 g 6.3215 g LCS 500-173450/2-A 1664A FC EB 5 1000 mL 1000 mL 87 2.3495 g 2.3500 g 2.3501 g 500-53342-H-3-A 1664A T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 1664 HEM 00060 Pass_0.0005g 0.0007999999999 99912 g 0.0009999999999 9989 g MB 500-173450/1-A 1664A Pass_0.0005g 0.0366 g 0.0367000000000 006 g 5 mL LCS 500-173450/2-A 1664A FC EB 5 Pass_0.0005g 0.0005000000000 00167 g 0.0005999999999 99934 g 500-53342-H-3-A 1664A T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0020 / 0.9999 g Calibration Check Before 1st Weighing 0.0020 / 0.1002 g Person's name who did the concentration see analyst name Evaporator Temperature 50 Degrees C Hexane Lot# Hexanes_00012 Methanol Lot Number Methanol_00006 Na2SO4 Lot Number Na2SO4_00006 Silica Gel Lot Number Silica gel_00003 (checked in batch 157954, 7/31/12 Speedvap ID# 1564 Weight Set ID 1144 / 2495
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 12:55 12/19/12 11:25 173291 Batch Method: TestAmerica Chicago

9030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-173291/1 9030B, 9034 10.0000 g 10 mL 10 mL LCS 500-173291/2 9030B, 9034 FC Composite 5 10.0683 g 10 mL 500-53342-A-1 9030B, 9034 T
Batch Notes Batch Comment BAlance ID #2489 Distillation Temperature 70 Degrees C Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014 Sulfuric Acid Reagent ID Number 20% H2SO4_00003 Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 13:40 12/19/12 13:35 173474 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount IodineAmount TitrantVolume1 CalcMsg 10 mL 5 mL 4.65 mL OK MB 500-173291/1-A 9034 10 mL 5 mL 0.44 mL OK LCS 500-173291/2-A 9034 FC Composite 5 10 mL 10 mL 3.31 mL OK 500-53342-A-1-B 9034 T
Batch Notes HCl Concentration 6N Lot # of hydrochloric acid 6NHCL00006 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0232 N Sodium Thiosulfate Reagent ID Number NO2S2O300008 Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR Normality of first Titrant 0.0246 N Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 14:02 12/24/12 13:19 173846 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036 4.91 mL 5 mL 250 mL 250 mL OK MB 500-173846/1 9034 2.49 mL 5 mL 250 mL 250 mL OK 5 mL LCS 500-173846/2 9034 FC EB 5 5.10 mL 5 mL 250 mL 250 mL OK 500-53342-G-3 9034 T
Batch Notes First End time 14:02 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0240 N Sodium Thiosulfate Lot Number NO2S2O300008 Sodium Thiosulfate Vendor INHOUSE Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR First Start time 13:19 Sulfuric Acid Reagent ID Number 6NHCL00006 Normality of first Titrant 0.0246 N Titrant Standardization Date 11/21/12
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/19/12 07:35 12/19/12 05:10 173324 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 1664 HEM 00060 10 g 10 mL MB 500-173324/1 9071B, 9071B 10 g 10 mL 5 mL LCS 500-173324/2 9071B, 9071B FC Composite 5 10.1047 g 10 mL 500-53342-A-1 9071B, 9071B T
Batch Notes Acid used for pH adjust Lot # J23A13 Balance ID 1634 Concentration End Time See end date / time Concentration Start Time See start date / time Evaporator Temperature 50 DEG. C Filter Paper Lot Number 6711653 Hexane Lot# HEXANES_00012 Na2SO4 Lot Number Na2SO4_00006
Basis Basis Description T Total/NA



### Page 1 of 1 9071B 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/19/12 11:35 12/19/12 09:20 173330 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 10 mL 10 mL 24 2.3781 g 2.3790 g 2.3791 g MB 500-173324/1-A 9071B 10 mL 10 mL 25 2.3332 g 2.3745 g 2.3741 g LCS 500-173324/2-A 9071B FC Composite 5 10 mL 10 mL 35 2.3177 g 2.3577 g 2.3576 g 500-53342-A-1-D 9071B T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 Pass_0.0005g 0.0009000000000 00123 g 0.0010000000000 0033 g MB 500-173324/1-A 9071B Pass_0.0005g 0.0412999999999 997 g 0.0408999999999 997 g LCS 500-173324/2-A 9071B FC Composite 5 Pass_0.0005g 0.04 g 0.0399000000000 003 g 500-53342-A-1-D 9071B T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0019 / 0.9999 Calibration Check Before 1st Weighing 0.0019 / 0.9999 Evaporator Temperature 50 Celsius Filter Paper Lot # 6711653
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/21/12 07:08 173667 Batch Method: TestAmerica Chicago

Moisture Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC Composite 5 8 1.27 g 11.33 g 3.98 g 500-53342-A-2 Moisture T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/21/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 0715 Date samples were removed from oven 12/22/12 Oven Temp when samples removed from oven 105 Degrees C Time Samples were removed from oven 0800 Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA



### Page 1 of 1 Moisture 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/18/12 07:13 173229 Batch Method: TestAmerica Chicago

SM 2540G Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC Composite 5 17 1.28 g 11.68 g 4.40 g 500-53342-A-1 SM 2540G T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/18/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 0720 Date samples were removed from oven 12/19/12 Oven Temp when samples removed from oven 105 Degrees C Time Samples were removed from oven 0700 Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA



### Page 1 of 1 SM 2540G 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53342-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/19/12 07:31 173385 Batch Method: TestAmerica Chicago

SM 2540G Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg FC Composite 5 Not Calculated. RunCalculation is NULL 500-53342-A-1 SM 2540G T

Batch Notes

Basis Basis Description T Total/NA



### Page 1 of 1 SM 2540G 

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## Login Sample Receipt Checklist
Client: Project Integration, Inc Job Number: 500-53342-1 Login Number: 53342

Question Answer Comment Creator: Scott, Sherri L List Source:TestAmerica Chicago List Number: 1



### True Radioactivity wasn't checked or is </= background as measured by a survey meter. True The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or tampered with. True Samples were received on ice. True Cooler Temperature is acceptable

. True Cooler Temperature is recorded

. 2.4 True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within HoldingTime

. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample PreservationVerified

. True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). True Multiphasic samples are not present. True Samples do not require splitting or compositing. N/A Residual Chlorine Checked.

TestAmerica Chicago 

## 01/04/2013 Page 332 of 332

# ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel:(708)534-5200 TestAmerica Job ID: 500-53342-1 Client Project/Site: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, South Carolina 29651 Attn: Mr. Robert Stevens
Authorized for release by: 1/4/2013 2:18:19 PM Donna Ingersoll Project Manager II donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 

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# Table of Contents Client: Project Integration, Inc Project/Site: John Deere Des Moines Works (JDDMW) TestAmerica Job ID: 500-53342-1



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## 1/4/2013 

# Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 

# Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 

# Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 

# Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 

# Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 

# Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 

# Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 

# Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11 

# QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12 

# Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 

# QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 

# Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26 

# Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28 

# Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29 

# Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 

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