### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10678 AES W arrior Run 1 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 10678 AES Warrior Run 1 As Received Higher Heating Value 

### 10678 AES Warrior Run 1 As Received % Moisture 

### 10678 AES Warrior Run 1 As Received % Ash 

### 10678 AES Warrior Run 1 As Received % Sulfur 

### 10678 AES Warrior Run 1 Dry basis Higher Heating Value 

### 10678 AES Warrior Run 1 Dry basis % Ash 

### 10678 AES Warrior Run 1 Dry basis % Sulfur 

### 10678 AES Warrior Run 1 Dry basis Antim ony 

### 10678 AES Warrior Run 1 Dry basis Arsenic 

### 10678 AES Warrior Run 1 Dry basis Bery llium 

### 10678 AES Warrior Run 1 Dry basis Cadmium 

### 10678 AES Warrior Run 1 Dry basis Chlorine 

### 10678 AES Warrior Run 1 Dry basis Chromium 

### 10678 AES Warrior Run 1 Dry basis Cobalt 

### 10678 AES Warrior Run 1 Dry basis Fluorine 

### 10678 AES Warrior Run 1 Dry basis Lead 

### 10678 AES Warrior Run 1 Dry basis Manganese 

### 10678 AES Warrior Run 1 Dry basis Mercury 

### 10678 AES Warrior Run 1 Dry basis Nickel 

### 10678 AES Warrior Run 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### D4809 D3173 D482 D1552 / D4239 D5865 D3174 D4239 6010B 6010B 6010B 6010B 9056 6010B 6010B 9056 6010B 6010B 7471A 6010B 6010BEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10678 AES Warrior Run 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units AG 1 

### 3/24/2010 3/24/2010 12336.00 Btu/lb AG 2 3/25/2010 3/25/2010 11601.00 Btu/lb AG 3 3/26/2010 3/26/2010 11808.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 4.1 16.15 12864 Btu/lb 16.84 2.012 5.8 18.18 12315 Btu/lb 19.3 1.869 6.4 17.37 12615 Btu/lb 18.57 1.573Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 280 ppm 280 ppm 240 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 69 ppm 4.1 92 ppm 5.8 87 ppm 6.4 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 16.97 16.84 66.21 75.04 4.53 1.9 2.012 16.67 19.3 64.04 74.22 3.71 1.17 1.869 16.58 18.57 64.85 74.44 4.25 1.39 1.573 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 4.34 4.62 4.16EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10678 AES Warrior Run 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units PM/Met 1 

### 7/21/2010 7/21/2010 12129.00 Btu/lb PM/Met 2 7/22/2010 7/22/2010 12091.00 Btu/lb PM/Met 3 7/23/2010 7/23/2010 11835.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 4.3 15.41 1.719 12674 Btu/lb 16.11 1.719 3 17 2.388 12465 Btu/lb 17.53 2.388 3.6 18.42 1.93 12277 Btu/lb 19.11 1.93Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 252 ppm 0.275 mg/Kg [<0.3] mg/Kg 11 mg/Kg 0.82 220 ppm 0.285 mg/Kg [<0.3] mg/Kg 12 mg/Kg 1.5 256 ppm 0.239 mg/Kg [<0.3] mg/Kg 6.4 mg/Kg 0.94Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg [<0.15] mg/Kg 11 mg/Kg 9.7 mg/Kg 51 mg/Kg mg/Kg [<0.15] mg/Kg 13 mg/Kg 9.1 mg/Kg 35 mg/Kg mg/Kg [<0.15] mg/Kg 13 mg/Kg 9.3 mg/Kg 28 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 20 mg/Kg 4.5 mg/Kg 5 mg/Kg 16 mg/Kg 3.7 mg/Kg 6.1 mg/Kg 26 mg/Kg 3.8 mg/Kg 5.1 mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 4.3 18.72 16.11 65.18 72.93 4.09 1.41 1.719 3 18.59 17.53 63.88 73.13 3.87 1.48 2.388 3.6 17.69 19.11 63.2 70.03 3.91 1.39 1.93 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 4.71 3.49 3.55EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10678 AES Warrior Run 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units ORG 1 

### 3/27/2010 3/27/2010 11488.00 Btu/lb ORG 2 3/27/2010 3/27/2010 11330.00 Btu/lb ORG 3 3/27/2010 3/27/2010 11355.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 5.6 18.41 12167 Btu/lb 19.5 2.432 7.9 16.66 12302 Btu/lb 18.09 0.99 6.5 18.31 12145 Btu/lb 19.59 1.576Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 5.6 7.9 6.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 17.69 19.5 62.81 70.73 3.47 1.31 2.432 3.69 18.27 18.09 63.65 72.62 3.55 1.47 0.99 6.18 18.19 19.59 62.22 70.84 4.03 1.4 1.576 1.74 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10678 AES Warrior Run 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units PM/Met 1 

### 3/24/2010 3/24/2010 11677.00 Btu/lb PM/Met 2 3/25/2010 3/25/2010 11788.00 Btu/lb PM/Met 3 3/26/2010 3/26/2010 11740.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.2 19 12449 Btu/lb 20.26 1.447 5 17.18 12409 Btu/lb 18.09 2.015 7.3 13.58 12664 Btu/lb 14.65 1.576Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 240 ppm 0.291 mg/Kg [<0.3] mg/Kg 9.9 mg/Kg 0.7 230 ppm 0.249 mg/Kg [<0.3] mg/Kg 15 mg/Kg 0.71 270 ppm 0.254 mg/Kg [<0.3] mg/Kg 9.4 mg/Kg 0.69Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg [<0.15] mg/Kg 8.2 mg/Kg 8.5 mg/Kg 33 mg/Kg mg/Kg [<0.15] mg/Kg 9.4 mg/Kg 11 mg/Kg 43 mg/Kg mg/Kg [<0.15] mg/Kg 7.7 mg/Kg 7.9 mg/Kg 45 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 4 mg/Kg 4.3 mg/Kg 6.2 5.6 mg/Kg 5.3 mg/Kg 5 4.3 mg/Kg 4.7 mg/Kg 7.3 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 16.49 20.26 63.25 75.2 3.61 0.8 1.447 3.78 19.94 18.09 61.97 72.14 2.59 0.82 2.015 4.64 17.63 14.65 67.71 73.21 3.64 0.99 1.576 3.54 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm