# TI-D-130

LETTER OF TRANSMITTAL Trigon Engineering Consultants, Inc. 700 Blue Ridge Road, Suite 101 Raleigh, North Carolina 27606 (919) 755-5011 

### To: Mr. 

### Bruce 

### C Jordan, Director Attn: Bill Neuffer Date: Project No. July 29, 1998 046-97-048 US EPA - Emission Standards Division NC Mutual Life Building Project Name Lee Brick & 

### Tile 411 W. Chapel Hill Street Sanford, North Carolina Durham, North Carolina 27701 WE ARE SENDING YOU**~** Attached 

### 0 Under separate cover via ______ the follo\Ning items COPIES DESCRIPTION I Letter - Information Request for Brick and Structural Clav Products Manufacturing I Stationarv Source Samoling Reoort- Stack Test Results for Kiln No. 2

THESE ARE TRA..'\iSMITIED AS CHECKED BELOWo 

## 0 For Approval 

## 121 For Your Use 

## 121 As Requested 

## 0 For Review and Comment
REMARKSo COPIES TO: Mr. J.R. Holton, Lee Brick & Tile, Inc. (letter only) Mr. Dale Overcash, Harding Lawson Associates



### SIGNED 

# IENGINEERING CONSULTANTS, INC. 700 Blue Ridge Road, Suite 101 • Raleigh, NC 27606 • (919) 755·5011 • FAX (919) 755·1414 

### July 29, 1998 Bruce C. Jordan, Director Attn: Bill Neuffer U S Environmental Protection Agency Emission Standards Division (MD-13) Office ofAir Quality Planning and Standards NC Mutual Life Building 411 W Chapel Hill Street Durham, NC 27701 Phone: (919) 541-5435 Reference: Information Request for Brick and Structural Clay Products Manufacturing Operations- Lee Brick and Tile, Sanford, NC Dear Mr. Neuffer Please find enclosed a copy ofthe stack test results performed for Kiln 2 

### at the Sanford, North Carolina facility. Ifyou have any questions, please contact Kirk Rife ofTrigon at (336) 668-0093 or Mr. J.R. Holton ofLee Brick at (919) 774-4800.

KLR\meg F:\CLIE:lT3601prvjects.98\0368022\EPA2.doc 

### Attachments Yours Truly, 

### TRIGON ENGINEERING CONSULTANTS, INC. 

## --.....



# K;,~,~\\ Vice President, Environmental Affairs

CC: Dale Overcash, Harding Lawson Associates J.R. Holton, Lee Brick and Tile

### LeeBrick&

### TileCompanY 

### Kiln2PC-1

### Stack 

### Kiln2PC-2

### Stack 

### sanford,Northcarolina Trig onProject#046-9'7-043 Apri1l99'7 

# 3

### Stationary Source Sampling Report LeeBrick& 

### Tile Company 

### Kiln 2PC-I Stack 

### Kiln 2PC-2 Stack Sanford, North Carolina TrigonProject

### # 046-97-048 April1997

# STATIONARY SOURCE SAMPLING REPORT FOR LEE BRICK & TILE COMPANY SANFORD, NORTH CAROLINA Kiln 2 PC-1 Stack Kiln 2 PC-2 Stack

Performed by: TrigonEngineering Consultants, Inc. Environmental, Health & Safety Division 6200 Harris Technology Blvd. Charlotte, North Carolina 28269 704/598-1049 TrigonProject 

### # 046-97-048 April 1997

### REPORT CERTIFICATION 

### This report, all testing details, and final results have been performed under the supervision and reviewed by the persons named below. Date._________Signature.____________________ _ RobertF. Callahan ProjectManager Environmental, Health & 

### SafetyDivision TrigonEngineering Consultants, Inc. Date._________Signature.____________________ _ Paul

### R Jenkins, Jr. QualityAssurance Manager Environmental, Health & 

### SafetyDivision TrigonEngineering Consultants, Inc. Date._________Signature,____________________ _

u 

### J.A "Tony" Blanton Manager StackTesting Department Environmental, Health & 

### SafetyDivision TrigonEngineering Consultants, Inc.

### TABLE OF CONTE:'{TS 1.0 INTRODUCTION................ .................................................................................. 1 1.1 Purpose......................................................................................................................... 1 1.2 Outline ofTest Program ............................................................................................... 1 1.3 Test Participants ...........................................................................................................2 2.0 

### PROCESS DESCRIPTION................. ...................................................................3 

### 2. 1 Discussion............... . ............ ............ .................................................................3 Figure 1- Process 

### AirFlow Schematic -No. 2 Kiln......................................................4 3.0 

### SAl'\-lPLINGMETHODS........................................................................................................5 

### 3.1 Sampling Strategy..........................................................................................................5 3.2 Sampling and Analytical Procedures.........•....................................................................5 3.2.1 SamplingPorts, Traverse Points and Cyclonic FlowDetermination..................................................................5 3.2.2 Stack Gas 

### Velocity and Volumetric FlowRateDetennination......................6 3.2.3 DryMolecularWeight Determination............................................................7 3.2.4 Moisture Detennination.................................................................................8 3.2.

### 5 TotalFluoride Sampling and Analysis............................................................9 3.2.6 HydrogenFluoride Sampling and Analysis .................................................. 10 3.2.7 Sampling Ports and Points ........................................................................... 11 Location ofSampling Ports and Points Figure 2 - PC-1 Stack.................................................................................. 12 Figure 3 - PC-2 Stack.................................................................................. 13 3.3 Quality Assurance and Quality ControL..................................................................... 14 4.0 

### RESULTS............................................................................................................................... 15 4.1 Summary ofResults..................................................................................................... 15 4.2 Discussion...............................................................:.................................................... 15 4.3 Detailed Stack Sampiing Results ................................................................................. 15 SummaryofResults Table 1 - PC-1 Stack, TotalFluoride Sampling........................................................... 16 Table 2- PC-1 Stack, HydrogenFluoride Sampling.................................................... 17 Table 3 - PC-2 Stack, TotalFluoride Sampling ........................................................... 18 Table 4- PC-2 Stack, HydrogenFluoride Sampling.................................................... 19 

### 5.0 APPENDICES........................................................................................................................20 A SummaryofResults andExample Calculations B. 

### Field Data Sheets C. 

### LaboratoryData D. ProductionDocumentation 

### E. Calibration Data
Ill 

# 1

### 1.0 L'IITRODUCTION This section describes the purpose, a briefoutline including the sampling and analytical strategy, and the personnel involved in the test program. 

### 1.1 Purpose The purpose of this sampling project was to determine concentrations and emission rates of total fluoride and hydrogen fluoride from two emission points associated with the No. 2 

### Kiln located at the Lee Brick and Tile Company facility in Sanford, North Carolina. The results ofthe sampling and the documentation provided in this report

### will be used byLee.Brick for emissioninventorypurposes. 1.2 OutlineofTestProgram Stationary source sampling was performed April 18, 1997 by the Environmental, Health & 

### Safety Division ofTrigonEngineering Consultants, Inc. on the No. 2 

### Kiln which is used to dry bricks. Three !-hour sampling runs were conducted simultaneously for total fluoride and hydrogen fluoride at the two exhaust stacks (PC-! and PC-2) which serve No. 2 

### Kiln. United States Environmental Protection Agency (US EPA) Methods 1 through 4 and Method 13B were used for the determination oftotal fluoride concentrations and emission rates. Method 26Awas used for the determination ofhydrogen fluoride concentrations and emission rates. All sampling and analytical procedures used were those established by the US EPA in standard reference test methods and appropriate state-of-the-art analytical procedures. The test runs were conducted during normal operating conditions.

11.3 TestParticipants 

### ·A

### list ofthe project participants, titles, affiliation and telephone numbers canbefound below. Participant Robert F. Callahan Paul R Jenkins, Jr.

Chris B. Brooks LoganE. Butler Jason J. Tagliaferri

JohnD. Archer David C. Stoll BobbyMcCoy Title Project !vfanager QualityAssurance Manager Senior Environmental Scientist Environmental Scientist Environmental Scientist Environmental Scientist Environmental Scientist ManagerPlant

Engineering AITLliation TrigonEngineering

Consultants, Inc. Trigon Engineering

Consultants, Inc. TrigonEngineering

Consultants, Inc. TrigonEngineering

Consultants, Inc. TrigonEngineering

Consultants, Inc. TrigonEngineering

Consultants, Inc. Trigon Engineering

Consultants, Inc. Lee Brickand Tile



### 2 Contact Telephone: (704) 598-1049 Facsimile: (704) 598-1050
•··........•.......·. ......... ···············•·/·•••••·•·••> 

# r

i••• 

## i ·································································· ·················· ........

·······i····················································}............·.)······· ···••• }············ 

## .<T <• · .····•· •·• 2 

### c:<···•••···•__; 

# r \hi .......... ·····•: 

# r

Telephone: (919) 774-4800 Facsimile: (919) 774-7557

### 2.0 PROCESS DESCRIPTION This section contains abriefdescription ofthe No. 2 

### Kiln and an 

### air flow schematic. 2.1 Discussion The No. 2 

### Kiln at Lee Brick and Tile Company dries standard 10-hole red brick for its brick manufacturing facility in Sanford, North Carolina. The pollutant sampling was conducted during normal production hours. The 

### kiln produced brick at the optimum operating level and was fired with natural gas. The flue gases passed from the 

### kiln to an induced draft 

### (LD.) fan, 2 stacks (PC-I and PC-2) and to the atmosphere. The 

### kiln emissions are exhausted uncontrolled to the atmosphere. Figure 1 

### details the 

### air flow schematic of

### the No.2 

### Kiln.

3 

# !D

## No.2 Kiln
Atmosphere Atmosphere 

# t t Sampling



# Location~ 

# IStack



# ~

**~** Stack

# I

**~Sampling**Location 

# t t ID. Fan 

# t 

# I Kiln 

# I Figure 1 ProcessAirFlowSchematic

4 

# II

### 3.0 SA.c'\-IPLING 

### METHODS This section describes the sampling strategy, sampling and analytical methods, and quality assurance/quality control procedures implemented during this project. 

### 3.1 Sampling Strategy The sampling and analytical procedures used during this test program were those established by the US EPA and NC DEHNR Sampling runs were conducted in triplicate to validate the sampling. Tests were conducted during normal operating conditions. There were no unusual conditions noted during the sampling. 

### 3.2 Sampling and Analytical Procedures The US EPAmethods used in this sampling programwereMethod 1for the iocation ofsampling ports and polll.ts, and determlll.ation of cyclonic flow, Method 2 for volumetric flow rate determlll.ation, Method 3 for the determlll.ation of dry molecular weight of the stack gas, and Method 4 for the determlll.ation ofmoisture in the stack gas. Method l3B was used to determlll.e concentrations and emission rates oftotal fluoride. Method 26A was used for determlll.ation ofhydrogen fluoride. A sampling and analysis synopsis is discussed briefly in the followlll.g subsection. These test methods are available in the Code ofFederalRegulations Volume 40, Part 60 orby request from Trigon. 

### 3.2.1 Sampling Ports, Traverse Points and Cyclonic Flow Determination ThePC-1 and PC-2 stacksampling locations were prepared according to the criteria inMethod 1. 

### The duct diameters upstreamand downstream from the sampling ports were determlll.ed prior to sampling. The number oftraverse points were chosen with respect to sampling port location. For isokinetic traverses Method 1 specifies a minimum of 8 traverse points for sampling ports located >8/>2 downstream/upstream stack diameters from flow disturbances and 24 traverse points when located >21>0.5. The amount ofcyclonic flow was determlll.ed accordingto the criteria detailed inMethod 1.



### 5

### 3.2.2 StackGas Velocity and Volumetric FlowRateDetermination Method 2 is used for determining the average gas velocity in a stack from measurements ofgas density and the average velocityhead with a Type S (Stausscheibe orreverse type) pitot tube. This method is applicable for quantifying gasflows which meet the criteria ofMethod I. Method 2 cannot be used for direct measurement ofgas streams which exhibit cyclonic flow conditions as determined by Method I, 

### Section 2.4. 

### In principle measurements of velocity head and temperature are performed at the traverse points specified by Method I. 

### A properly scaled differential pressure gauge was selected for the range oft.p values encountered during the traverse. A 0 - I

### 0 inches ofwater inclined manometer was used as the differential pressure gauge. During this project, the sampling location met all ofthe criteria detailed in Method I. 

### Gas stream density was determined by Method 3. Moisture determination was performed by Method 4. The principal components ofthe gasvelocity measurement system were sequentially:



## * A calibrated stainless steel Type S pitot tube and TypeK thermocouple; 

## * * * Leak-free interface tubing betweenpitot tube and differential pressure gauge; A 0 to I

### 0 inch inclined manometer and; AnNISItraceable pyrometer. The apparatus was set-up according to manufacturer and reference method recommendations. Pretest and posttest leak checks were conducted using procedures outlined in Method 2, Section 3

### .I. Velocity head and temperature measurements were performed at the traverse points specified by Method I. 

### The atmospheric and static pressure ofthe stack 

### was also determined for each set ofvelocity head readings. The volumetric flow rate calculations used were those specified in Method 2, Section 5. A more comprehensive explanation of the reference method is detailed in the Quality Assurance Handbookfor 

### AirPollutionMeasurement Systems: VolumeIII 

### (EPA/600/R-94/038c).

6 

# ;3

### 3.2.3 Dry MolecularWeightDetennination Method 3 is applicable for detennining carbon dioxide and oxygen concentrations and 

### dry molecular weight ofa sample from a gas stream ofa fossil-fuel combustion process. This method may also be applicable to otherprocesses where it has been detennined that compounds other than carbon dioxide, oxygen, carbon monoxide, and 

### nitrogen are not present in concentrations sufficient to affect the results. In

### principle a gas sample was withdrawn from the emission source by multi-point, integrated sampling. The collected samples were then analyzed for percent carbon dioxide, percent oxygen, and percent carbon monoxide. The dry molecularweight detennination was performedby an Orsat analyzer. During this project, the gaseous components were collected using a Method 3 sampling system following the Analytical Procedures outlined in the reference method. The principal components ofthe sampling system were sequentially:

• A stainless steel probe; 

# • A one-way squeezebulb, to transport the sample to the Tedlarbag; 

# • A saturatortubeto remove particulate matter and excess moisture and; 

# • A leak-free Tedlarbag equipped with a double-end shut-offquick connect. The analysis was performed with an Orsat type combustion gas analyzer within 8 hours of sample collection. The dry molecular weight was calculated using Equation 3-1, Section 7 ofMethod 3. The analyzer was maintained and operated according to the instructions recommended by the manufacturer and in accordance with Method 3 criteria. The analyzer was leak-checked according to Section 6 of Method 3. The oxygen reagent was validated by analyzing a sample ofambient 

### air which must meet the specifications of20.9%

## ±0.3%.

7

### 3.2.4 Moisture Detennination Method 4 involves the detennination ofstack gas moisture. The moisture content is used to correct the emission concentration or mass emission rate to a dry basis. EPA Method 4, Section 3.3 ofthe EPA's Quality Assurance Handbook, Volume 

### ill,EPA-600/4-77-027b, was used to measure stackgas moisture content. Section 3.3 of the Quality Assurance Handbook, Volume 

### ill, provides detailed information on the application ofMethod4. Preliminary flue gas moisture content (for purposes ofsetting the isokinetic flow rate) was detennined using wet bulb/dry bulb thermometers and partial pressure, vapor and saturated vapor pressure equations. This technique is described in Method4 and is summarized below:



# • • • • Moistenthe wet bulb thermometerwickwithdeionized water; Insert boththermometers into the flue gas stream and monitorthe wet bulb temperature; When the wet bulb temperature 

### has stabilized, record both the wet bulb and dry bulb thermometertemperatures; Calculate the flue gas moisture content (PMV) using the equations below. SVP = VaporPressure ofWaterat Saturation, inches ofMercury

SVP = IaxY(6.69ll- (3144/(Wet Bulb+ 390.86))) PMV=PercentMoistureby Volume PMV

### =(SVP · (0.000367(P,)(DryBulb- Wet Bulb)(!+((Wet Bulb- 32)/1571))))/(P..,.) x 100 P.o. = Absolute Pressure ofStack 

### Gas P"" =(BarometricPressure+ (Static Pressure/13.6)) The moisture content for emission rate calculations was detennined in conjunction with the Method 13B and 26Aisokinetic sampling trains. The reference method involves the withdrawal ofgaseous and particulatepollutants from the emission source at an isokinetic rate using anisokinetic sampling system. The sampling and analytical procedure for reference Method 4 

### will be discussed in detail in Section 3.2.5 withtheisokinetic sampling procedures.


### 8

### 3.2.5 Total Fluoride SamplingandAnalysis Testing for total fluoride was perfonned according to US EPA Method 13B. Emissions containing fluoride and particulate matter were withdrawn isokinetically from the emission source and collected in a multi component sampling train. The emission source gas stream was bubbled through a measured volume of deionized water in order to quantitatively separate and capture fluoride emissions. According to Section 7.1 ofMethod 13B an unheated glass filter was inserted between the third and fourth impingers to collect fluoride particulate matter from the gas stream. The principal components ofthe sampling system were sequentially:



## * * * * A stainless steel sample nozzle and borosilicate probe liner; A heated (248°F ±25°F) probe and filter bypass assembly; An 

### irnpinger train consisting offour sequential impingers. The first two impingers containing 100 

### mJ ofdeionized water followed by an empty impinger, and an unheated filter assembly. The fourth and final impinger contained 200 grams ofindicating silica gel and; A metering system capable of maintaining an isokinetic sampling rate and accurately determining the sample volume according to those specifications in APTD-0581. The fluoride samples were recovered by measuring the liquid in 

### the first three impingers to the nearest milliliter and recordingthe data on the moisture detennination fonn. This solution was transferred to a high density polyethylene storage container. The filter was then removed and added to same storage container. The back half of the sampling 

### train, filter assembly, and connecting glassware was quantitatively rinsed with deionized water and added to the sample storage container. The resulting solution was diluted to 500 

### mJ with deionized water. All volumetric data was recorded on the sample recovery forms. All sample containers were sealed and the liquid level marked. Chain of custody documentation commenced at this time. Blanks ofthe absorbing solution and rinsing reagent were submitted and analyzed with the samples. Samples were blank corrected for any background analyte concentrations. The samples and appropriate blanks were analyzed in-house by Trigon Engineering Consultants, Inc. Sample analysis was perfonned using the ion selective electrode procedure detailed in Method 13B. 

### 9 

# ;h

### 3.2.6 Hydrogen Fluoride SamplingandAnalysis Testing for hydrogen fluoride was performed according to EPAMethod 26A Gaseous and particulate pollutants were withdrawn isokinetically from the emission source and collected in a multi component sampling train. In principle, particulate matter includes any material that was condensed at or above the filtration temperature ofapproximately 250 degrees Fahrenheit and 

### was collected on a quartz filter.

The gaseous components were then bubbled through a measured volume of0 IN sulfuric acid and O.!N sodium hydroxide to determine the moisture, and hydrogen fluoride content of the emission source. The principal components ofthe sampling system were sequentially:



### * A borosilicateglass sample nozzle and probe linet;; 

## * A heated (248°F ±250f) probe and filter assembly with quartz filter; 

## *
* An 

### impinger train consisting offour sequential impingers. Impingers one and two containing 100 

### ml each ofan absorbing solution consisting ofdilute sulfuric acid (O.!NH 2

### S04). 

### Impinger three contained 100 

### ml of dilute sodium hydroxide (O.!N NaOH) followed by an impinger containing 200 grams ofsilica gel; and A metering system capable of maintaining an isokinetic sampling rate and accurately determining the sample volume accordingto those specifications in APID-0581. Sample clean up began immediately after each test run. Hydrogen fluoride was collected in the O.!N sulfuric acid solution in impingers one and two. The liquid in these impingers 

### was measured to the nearest milliliter. The collected sample was placed in a glass storage container alongwith the deionized water rinse ofimpingers one and two and connecting glassware. The container 

### was sealed and the liquid level was marked. The O.!N sodiumhydroxide solutionin impingerthree

### was used as a scrubber to protect the sampling console. The liquid in this impinger was measured to determine the moisture content and later discarded. The hydrogen fluoride sample container 

### was sealed and the liquid level marked. The samples were then shipped to Enthalpy Analytical, Inc., Raleigh, North Carolina with chain of custody documentation where they were analyzed by ion chromatography. The moisture collected by the silica gel in the fourth impinger was determined to the nearest 0.1 

### gram. All collected condensate measurements were recorded on the moisture determination and sample analysis data recoveryform. The particulate matter sample was also discarded.
10 

# 17

### 3.2.7 Sampling Ports and Points The dimensions ofeach stack and the location ofthe sampling ports and points are detailed in Figures 

### 2 and 3. Method 1 sampling criteria was maintained. The stack cross sections were divided into the appropriate number ofequal 

### areas. The ports were labeled A and B. During the runs each point was sampled for a specified period oftime, which yielded a total test time of60 minutes perrun.

11

## No.2 Kiln PC-1 Stack

Not to Scale 

## Figure2 Location ofSamplingPorts andPoints 12

## No. 2 Kiln PC-2 Stack

Notto Scale 

## Figure3 Location ofSamplingPorts and Points 13

## ;)_(

### 3.3 Quality Assurance and Quality Control 

### Trigon Engineering Consultants, Inc., has established quality assurance and quality control (QA/QC) guidelines for providing the highest quality sampling and analytical data from source tests. These 

### QAJQC procedures were implemented to ensure the acceptability and reliability ofthe data generated. In summary, a high degree ofdata quality 

### was maintained throughout this project. All leak checks 

### and isokinetic QAcriteria were met. Each sampling train was leak checked prior to and immediately after sampling. Leakrates for 

### all ofthe isokinetic sampling trains were less 

### than the maximum criterion of 0.02 cubic feet per minute. All sampling rates were also within the 100% ±10% criterion established for isokinetic sampling. Quality control procedures for Methods 13B and 26A have included the analysis ofreagent blank, spikes and laboratory control samples. The quality assurance samples are reported in Appendix Cwith the laboratory data. Field data and final laboratory results were entered into Trigon's 

### Air Quality Data System by an environmental scientist, independently audited by the Project Manager, and reviewed by the Quality Assurance Manager for verification ofdata. After QC review by the QA Manager, the Department Manager verified the 

### final report for completeness and reasonableness of data. The report was returned to the Project Manager for review and preparation ofthe final draft. The report requires the signature ofthe Project Manager, QA Manager, and the Department Manager before release to the client. Data and final reports are archived in a secured area for a minimum period ofthree years. Trigon's field and laboratory test equipment has been maintained and calibrated in accordance with quality assurance procedures established by the US EPA in the Quality Assurance Handbook for 

### Air Pollution Measurement Systems: Volume III. Equipment calibrations including pre-test and post-test calibration data are presented inAppendixE.

14

### 4.0 RESULTS This section presents the mean total fluoride and hydrogen fluoride sampling results. Tabular results are also provided to present data from individual sampling runs collected during this project. Detailed sampling results and example calculations for the test program can be found in Appendix A Field data sheets and sample recovery documentation are presented in AppendixB. 4.1 Summary ofResults The table belowis a synopsis ofthe total fluoride and hydrogen fluoride sampling conducted at the No. 2 

### Kiln, PC-1 and PC-2 Stacks. Pollutant, lbslhr PC-1 Stack PC-2 Stack Total Fluoride 

### !.09 2.85 HydrogenFluoride 

### 0.99 2.56 4.2 Discussion The results from this sampling project 

### will be used by Lee Brick & Tile Company for emission inventory purposes. 4.3 Detailed StackSampling Results Tables 1, 2, 

### 3 and 

### 4 present the data from individual sampling runs 

### atPC-1 and PC-2 Stacks. Included in these tables are gas velocity and volumetric flow rates, exhaust gas temperatures, and total fluoride and hydrogen fluoride catch, concentrations, and emissionrates.

15

## TABLE! Summary ofResults, Total Fluoride Sampling PC-1 Stack RunNumber 1 2 Date 04/18/97 04/18/97 Sample Identification 7048-01 7048-02 RunDuration, Minutes 60 60 Sample Time, 24-hour clock 0933-1115 1220-1324 Percent Isokinetic 99.5 101.8 Volume of

### Gas Sampled, 53.09 39 04

dry standard cubic feet*(DSCF) Average Stack Temperature, °F 301.3 306.2 Stack 

### Gas Velocity, feet/second 22.3 20.8 Stack

### Gas FlowRate, 6440 5922

dry standard cubic feet/minute*(DSCFM) Stack

### Gas Flow Rate, 9877 9201

actual cubic feet/minute(ACFM) Total Fluoride:

Catch, mg 66.4 60.5 Concentration, grains/dscf* 0.0193 0.0239 Emission Rate, lbslhr 1.06 1.21

* 68°F, 29.92 Inches Hg
16 3 Avg. 04/18/97 7048-03 60 1432-1537 101.6 101.0 51.56 47.90 286.5 298.0 21.0 21.4 6125 6162 9274 9451 63.8 63.6 0.0191 0.0207 1.00 1.09

### TABLE2 Summary ofResults, HydrogenFluoride Sampling PC-1 Stack RunNumber 1 2 

### 3 Date 04/18/97 04/18/97 04/18/97 Sample Identification 7048-08 7048-09 7048-10 

### RunDuration, :Minutes 60 60 60 Sample Time, 24-hour clock 0933-1115 1220-1324 1432-1537 Percent Isokinetic 102.0 98.0 96.2 Volume of

### Gas Sampled, 48.38 47.81 46.19

dry standard cubic feet*(DSCF) Average StackTemperature, °F 295.6 298.5 282.6 Stack

### Gas Velocity, feet/second 19.8 20.1 19.2 Stack

### Gas FlowRate, 5621 5783 5691



### dry standard cubic feet/minute*(DSCFM) Stack

### Gas FlowRate, 8731 8871 8492

actual cubic feet/minute(ACFM) HydrogenFluoride:

Catch, mg 68.159 68.170 52.208 Concentration, grains/dscf* 0.022 0.022 0.017 EmissionRate, lbslhr 1.05 1.09 0.85



## * 68°F, 29.92 Inches Hg 17 Avg.

98.7 47.46 292.2 19.7 5698 8698 62.846 0.020 0.99

### TABLE3 Summary ofResults, TotalFluoride Sampling PC-2 Stack RunNumber 1 2 Date 04/18/97 04118/97 Sample Identification 7048-04 7048-05 RunDuration, Minutes 60 60 Sample Time, 24-hour clock 0933-1114 1220-1325 PercentIsokinetic 100.4 104.8 Volume of

### Gas Sampled, 54.88 38.61

dry standard cubic feet*(DSCF) Average StackTemperature, °F 404.9 395.7 Stack 

### Gas Velocity, feet/second 51.7 50.8 Stack 

### Gas FlowRate, 12901 12770

dry standard cubic feet/minute*(DSCFM) Stack 

### Gas FlowRate, 22853 22433

actual cubic feet/minute(ACFM) TotalFluoride:

Catch, mg 89.6 66.7 Concentration, grains/dscf* 0.0251 0.0266 EmissionRate, lbs/hr 2.78 2.91

* 68°F, 29.92 Inches Hg
18 3 Avg. 04/18/97 7048-06 60 1432-1537 1039 103.0 52.74 48.74 416.8 405.8 49.3 50.6 11974 12548 21782 22356 94.9 83.7 0.0277 0.0265 2.84 2.85

### TABLE4 Summary ofResults, HydrogenFluoride Sampling PC-2 Stack RunNumber 1 2 3 Date 04/18/97 04/18/97 04/18/97 Sample Identification 7048-11 7048-12 7048-13 RunDuration, .Minutes 60 60 60 Sample Time, 24-hour clock 0936-1116 1220-1325 1432-1537 Percent Isokinetic 99.5 99.7 103.0 Volume ofGas 

### Sampled, 54.00 53.34 51.76

dry 

### standard cubic feet*(DSCF) Average StackTemperature, °F 398.8 391.4 411.8 Stack Gas 

### Velocity, feet/second 50.4 49.0 47.9 Stack Gas 

### FlowRate, 12642 12458 11705

dry standard cubic feet/minute*(DSCFM) Stack Gas 

### FlowRate, 22281 21661 21155

actual cubic feet/minute(ACFM) Hydrogen Fluoride:

Catch, mg 87.497 75.711 88.263 Concentration, grains/

### dscf* 0.025 0.022 0.026 EmissionRate, lbslhr 2.70 2.33 2.63

* 68°F, 29.92 Inches Hg 19 Avg.

100.7 53.03 400.7 49.1 12268 21699 83.824 0.024 2.56

### 5.0 

### APPENDICES This section contains detailed supportive documentation that encompasses all 

### aspects ofthe emission test program. Its contents serve as the foundation for the test report. The emission test report presents a summary ofthe informationgathered during the sampling activities. The information contained 

### in the appendices is necessary to facilitate the review of the emission test report and determine whether proper procedures were used to accomplish the test plan objectives. Defensible data and the subsequent pollutant concentrations and emission rates is one ofthe primary objectives ofany emission test program. To this end, all 

### r.esults, example calculations, field data sheets, sample recovery, laboratory results, chain ofcustody documentation, and equipment calibrations have beenprovided to support these objectives.

20

### APPENDIX A
SUMMARY OFRESULTSAND LX&'HPLE CALCULATIONS •'·}

'• 

### A-I

### SUM[\1ARY OFRESlJL.TS EPAMETHOD 13B Determination ofTotal Fluoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2 PC-1 Run Number 1 2 3 Avg Date: 04/18/97 04/18/97 04/18/97 

### TT Net Time ofTest, minutes 60 60 60 PB BarometricPressure, in. Hg 29.41 29.38 29.35 29.38 SP Static Pressure, in. Hg -0.008 -0.008 -0.008 -0.008 PS Stack Pressure, Absolute, in. Hg 29.402 29.372 29.342 29.372 VM Actual Meter Volume Sampled, cu. ft. 52.89 39.44 52.40 48.24 DH Avg. DeltaH, in. H20 2.7 1.4 2.5 2.2 

### TM Avg. Gas MeterTemp., Deg. F 60.7 65.7 69.8 65.4 VSTD Volume Sampled at Stand. Cond., cu. ft. 53.09 39.04 51.56 47.90 

# vw Volume ofWater Collected, m1 

### 51.1 42.4 55.1 49.5 VMV Volume ofWaterVapor at Std. Cond., SCF 2.41 2.00 2.59 2.33 Bws Moisture Content ofGas Stream 0.043 0.049 0.048 0.047 PMV Percent Moisture in Stack 4.3 4.9 4.8 4.7 MFD Mole FractionofDry Gas 0.957 0.951 0.952 0.953 P02 Percent Oxygen, Dry 19.0 18.5 18.8 18.8 PC02 Percent Carbon Dioxide, Dry 1.4 1.9 1.5 1.6 PCO Percent CarbonMonoxide, Dry 0.0 0.0 0.0 0.0 

### MD Mole. Wt. StackGas, Dry Basis, lb/lb mole 28.984 29.044 28.992 29.007 MW Mole. Wt. StackGas, Wet Basis, lb/lb mole 28.508 28.507 28.466 28.493 CP 

### Pitot Tube Constant 0.84 0.84 0.84 0.84 DPS Avg. Sqrt. DeltaP, in. H20 0.33 0.30 0.31 0.31 TS Avg. StackTemp., Deg. F 301.3 306.2 286.5 298.0 

# vs Avg. Stack Velocity, ft/sec 22.3 20.8 21.0 21.4 AS 

### Area Stack, ft2 7.37 7.37 7.37 7 A-2 

# 30

### SillvfMARY OFRESULTS EPAMETHOD 13B Determination ofTotal Fluoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina Kiln 

### 2 PC-1 QS Gas Volume Flow, Dry Std. Cond. CFM 6440 5922 6125 6162 QA Actual Gas Volume Flow, CFM 9877 9201 9274 9451 QSW Gas Volume Flow, Wet Std. Cond., CFM 6732 6225 6433 6463 DN Sample Nozzle Diameter, inches 0.432 0.382 0.432 0.415**At~** 

### Area ofNozzle, ft2 0.00102 0.00080 0.00102 0.00094 PERI Percent Isokinetic 99.5 101.8 101.6 101.0

Fluoride Concentrations and Emission Rates 

### FMF Catch,mg 66.4 60.5 63.8 63.6 CAN Concentration, gr/dscf 0.0193 0.0239 0.0191 0.0207 CAT Concentration, gr/acf 0.0126 0.0154 0.0126 0.0135 CAW Emission Rate, lbs/hr 1.06 1.21 1.00 1.09

•. A-3 

# .3/

### SUMMARY OFRESULTS EPAMETHOD 26A Determination ofHydrogen Halide and HalogenEmissions Lee Brick & 

### Tile Company Sanford, North Carolina Kiln 2 PC-1 Run Number 1 2 3 Avg Date: 04/18/97 04/18/97 04/18/97 

### TT NetTime ofTest, minutes 60 60 60 PB JarometricPressure, in. 

### Hg 29.41 29.38 29.35 29.38 SP Static Pressure, in. 

### Hg -0.008 -0.008 -0.008 -0.008 PS StackPressure, Absolute, in. 

### Hg 29.402 29.372 29.342 29.372 

### VM ActualMeterVolume Sampled, cu. ft. 48.56 48.46 47.15 48.06 DH Avg. DeltaH, in. 

### H20 2.4 2.3 2.2 2.3 

### TM Avg. Gas MeterTemp., Deg. F 64.1 68.7 71.7 68.2 VSTD Volume Sampled at Stand. Cond., cu. ft. 48.38 47.81 46.19 47.46 

# vw Volume ofWater Collected, mi 

### 68.5 49.0 39.7 52.4 VMV Volume ofWaterVapor at Std. Cond., SCF 3.22 2.31 1.87 2.47 Bws Moisture Content of Gas Stream 0.062 0.046 0.039 0.049 PMV Percent Moisture in 

### Stack 6.2 4.6 3.9 4.9 

### MFD Mole Fraction ofDry Gas 0.938 0.954 0.961 0.951 P02 Percent Oxygen, Dry 19.0 18.5 18.8 18.8 PC02 Percent Carbon Dioxide, Dry 1.4 1.9 1.5 1.6 PCO Percent Carbon Monoxide, Dry 0.0 0.0 0.0 0.0 

### MD Mole. Wt. Stack Gas, DryBasis, lb/lb mole 28.984 29.044 28.992 29.007 

### MW Mole. Wt. Stack Gas, Wet Basis, lb/lb mole 28.298 28.536 28.565 28.466 CP PitotTube Constant 0.84 0.84 0.84 0.84 DPS Avg. Sqrt. DeltaP, in. 

### H20 0.29 0.29 0.28 0.29 TS Avg. StackTemp., Deg. F 295.6 298.5 282.6 292.2 

# vs Avg. StackVelocity, ft/sec 19.8 20.1 19.2 19.7 AS AreaStack, ft2 7.37 7.37 7.37 7.37 A-4

### 3~

### SUMMARYOFRESULTS EPAMETI-IOD 26A Determination ofHydrogen Halide and Halogen Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2PC-1 QS Gas Volume Flow, DryStd. Cond. CFM 5621 5783 5691 5698 QA Actual Gas Volume Flow, CFM 8731 8871 8492 8698 QSW Gas Volume Flow, Wet Std. Cond., CFM 5995 6062 5921 5993 DN Sample Nozzle Diameter, inches 0.436 0.436 0.436 0.436 AN 

### Area ofNozzle, ft2 0.00104 0.00104 0.00104 0.00104 PERI PercentIsokinetic 102.0 98.0 96.2 98.7

Hydrogen FluorideAnalysis 

### FMF Hydrogen Fluoride Catch, mg 68.159 68.170 52.208 62.846 CAI"\1 Hydrogen Fluoride Concentration, gr/dscf 0.022 0.022 0.017 0.020 CAT Hydrogen Fluoride Concentration, gr/acf 0.014 0.014 0.012 0.013 CAW Hydrogen Fluoride EmissionRate, lbs/hr 1.05 1.09 0.85 0.99

'• 

### A-5

### SUMMARYOFRESu'LTS EPAMETHOD 13B Determination ofTotal F1uoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2 PC-2 Run Number 1 2 3 Avg Date: 04/18/97 04/18/97 04/18/97 TT 

### NetTime ofTest, minutes 60 60 60 PB Barometric Pressure, in. Hg 29.41 29.38 29.35 29.38 SP Static Pressure, in. Hg -0.028 -0.028 -0.028 -0.028 PS StackPressure, Absolute, in. Hg 29.382 29.352 29.322 29.352 

### VM ActualMeterVolume Sampled, cu. ft. 55.10 39.32 54.17 49.53 DH Avg. DeltaH, in. H20 2.9 1.5 2.8 2.4 

### TM Avg. Gas MeterTemp., Deg. F 64.9 70.0 75.8 70.2 VSTD Volume Sampled at Stand. Cond., cu. ft. 54.88 38.61 52.74 48.74 

# vw Volume ofWater Collected, 

### m1 72.3 52.0 82.4 68.9 VMV Volume ofWaterVapor at Std. Cond., SCF 3.40 2.45 3.88 3.24 Bws Moisture Content ofGas Stream 0.058 0.060 0.069 0.062 PMV Percent Moisture in Stack 5.8 6.0 6.9 6.2 MFD Mole Fraction ofDryGas 0.942 0.940 0.931 0.938 P02 Percent Oxygen, Dry 17.9 18.0 17.7 17.9 PC02 Percent Carbon Dioxide, Dry 2.3 2.0 2.5 2.3 PCO Percent Carbon Monoxide, Dry 0.0 0.0 0.0 0.0 MD Mole. Wt. Stack Gas, DryBasis, lb/lb mole 29.084 29.040 29.108 29.077 MW Mole. Wt. StackGas, Wet Basis, lb/lb mole 28.437 28.382 28.347 28.389 CP PitotTube Constant 0.84 0.84 0.84 0.84 DPS Avg. Sqrt. Delta P, in. H20 0.71 0.70 0.67 0.69 TS Avg. StackTemp., Deg. F 404.9 395.7 416.8 405.8 

# vs Avg. StackVelocity, ft/sec 51.7 50.8 49.3 50.6 AS Area Stack, ft2 7.37 7.37 7.37 7.37
A-6

### SUMi\1A.RY OFRESULTS EPAMETHOD 13B Determination ofTotal Fluoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2PC-2 QS Gas Volume Flow, Dry Std. Cond. CFM 12901 12770 11974 12548 QA Actual Gas VolumeFlow, CFM 22853 22433 21782 22356 QSW Gas Volume Flow, Wet Std. Cond., CFM 13700 13579 12855 13378 DN Sample Nozzle Diameter, inches 0.309 0.255 0.309 0.291 AN Area ofNozzle, ft2 0.00052 0.00035 0.00052 0.00047 PERl Percent Isokinetic 100.4 104.8 103.9 103.0

Fluoride Concentrations and Emission Rates 

### FMF Catch, mg 89.6 66.7 94.9 83.7 CAN Concentration, gr/dscf 0.0251 0.0266 0.0277 0.0265 CAT Concentration, gr/acf 0.0142 0.0151 0.0152 0.0149 CAW Emission Rate, lbs/hr 2.78 2.91 2.84 2.85

A-i

### SUMMARY OFRESliL TS EPAMETHOD 13B Determination ofTotal Fluoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2 PC-2 Example Calculations Run 1 StackPressure, Absolute, 

### in. Hg PS 

# =PB 

## + SP 

# = Volume Sampled at Stand. Cond., cu. ft. 

### 17.647 • VM • (PB 

## + DH/13.6) VSTD = ------------------------------ = Thf 

## + 460 Volume ofWater Vapor at Std. Cond., SCF VMV = 

### 0.04709 • VW = 

### Moisture Content ofGas Stream VMV Bvvs = --------------------------------- = 

### VSTD+VMV Percent Moisture 

### in Stack lOO*VMV PMV 

### == -------------------- = 

### VSTD+VMV MoleFraction ofDryGas 100-PMV

**~** 

### == ------------------ = 

### 100 Mole. WL StackGas, Dry Basis, lbllb mole 

### MD 

### == 0.44 • %C02 

## + 0.32 • %02 

## + 0.28 • (100- %C02- %02) = 

### Mole. Wt. StackGas, Wet Basis, lbllb mole 

### MW

## = MD • (1 - Bvvs) 

## + 18.0 • Bvvs 

## = Avg. StackVelocity, ft/sec (TS 

## + 460) 

### VS == 

### 85.49 • CP • DPS • SQRT ---------- == 

### (PS • MW)

A-8 

### 29.382 54.88

3.40 0.058
5.8
0.942 29.084 28.437 51.7**SL~IMARY** 

### OFRESl:L.TS EPAMETHOD 13B DeterminationofTotal Fluoride Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2 PC-2 Gas Volume Flow, Dry Std. Cond. CFM 1058.82 *VS *AS* PS * (1- Bws) QS = 

# -------= TS 

## + 460 Actual Gas Volume Flow, CFM QA=VS*AS*60= Gas Volume Flow, WetStd. Cond., CFM QSW = QS • (1/(1-Bws)] = Area ofNozzle, ft2 AN= ((ON/2)"'2 *3.14159)/144 = Percent Isokinetic 0.0945 *(TS 

## + 460) • VSTD PERI=------------= 

### TT *VS • PS * (1 - Bws) • AN Concentration, 

### gr/dscf (AtStandard Conditions) CAl"! 

## = 0.0154 *FMF 

### IVSTD 

## = Emission Rate, lbs!hr (AtStandard Conditions) CAW = 

### 0.00857 • CAN • QS = 

### Standard Conditions 68 Deg. F, 29.92 in. 

### Hg

A·9 

### 12901 22853 13700 0.00052 100.4
0.0251 278



# 37

### SUMMARY OFRESULTS EPA N!ETI!OD 26A Determination of Hydrogen Halide and Halogen Emissions Lee Brick & 

### Tile Company Sanford, North Carolina 

### Kiln 2 PC-2 Run Number 1 2 3 Avg Date: 04/18/97 04/18/97 04/18/97 

### TT NetTime ofTest, minutes 60 60 60 PB Barometric Pressure, in. Hg 29.41 29.38 29.35 29.38 SP Static Pressure, in. Hg -0.028 -0.028 -0.028 -0.028 PS StackPressure,Absolute,in. Hg 29.382 29.352 29.322 29.352 VM Actual MeterVolume Sampled, cu. ft. 54.00 54.03 52.84 53.62 DH Avg. Delta H, in. H20 2.9 2.8 2.6 27 

### TM Avg. Gas MeterTemp., Deg. F 62.8 68.9 72.3 68.0 VSTD Volume Sampled at Stand. Cond., cu. ft. 54.00 53.34 51.76 53.03 

## vw Volume ofWater Collected, ml 

### 73.6 65.5 80.0 73.0 VMV Volume ofWaterVapor atStd. Cond., SCF 3.46 3.08 3.77 3.44 Bws Moisture ContentofGas Stream 0.060 0.055 0.068 0.061 PMV Percent Moisture inStack 6.0 5.5 6.8 6.1 MFD 

### Mole Fraction ofDry Gas 0.940 0.945 0.932 0.939 P02 Percent Oxygen, 

### Dry 17.9 18.0 17.7 17.9 PC02 Percent Carbon Dioxide, Dry 2.3 2.0 2.5 2.3 PCO Percent CarbonMonoxide, Dry 0.0 0.0 0.0 0.0 

### MD Mole. Wt. Stack Gas, DryBasis, lb/lb mole 29.084 29.040 29.108 29.077 MW Mole. Wt. StackGas, WetBasis, lb/lb mole 28.416 28.437 28.355 28.402 CP PitotTube Constant 0.84 0.84 0.84 0.84 DPS Avg. Sqrt. DeltaP, in. H20 0.69 0.68 0.65 0.67 TS Avg. StackTemp., Deg. F 398.8 391.4 411.8 400.7 

# vs Avg. Stack Velocity, ft/sec 50.4 49.0 47.9 49.1 AS AreaStack, ft2 7.37 7.37 7.37 7.37 A-10

### SUMMARYOFRESl..JLTS EPAMETHOD 26A Determination ofHydrogen Halide and Halogen Emissions Lee Brick & 

### Tile Company Sanford, North Carolina Kiln 

### 2PC-2 QS Gas Volume Flow, DryStd. Cond. CFM 12642 12458 11705 12268 QA Actual Gas Volume Flow, CFM 22281 21661 21155 21699 QSW Gas VolumeFlow, Wet Std. Cond., CFM 13453 13178 12556 13062 DN Sample Nozzle Diameter, inches 0.311 0.311 0.311 0.311 AN Area ofNozzle, ft2 0.00053 0.00053 0.00053 0.00053 PERI PercentIsokinetic 99.5 99.7 103.0 100.7

Hydrogen Fluoride Analysis 

### FMF 

### HydrogenFluoride Catch, mg 87.497 75.711 88.263 83.824 CAN Hydrogen Fluoride Concentration, gr/dscf 0.025 0.022 0.026 0.024 CAT Hydrogen Fluoride Concentration, gr/acf 0.014 0.013 O.D15 0.014 CAW Hydrogen Fluoride Emission Rate, lbs/hr 2.70 2.33 2.63 2.56

A-ll 

# 37**SL~llv1ARY** 

### OF

### RESuLTS EPAMETHOD 26A Determination ofHydrogenHalide and Halogen Emissions Lee Brick & 

### Tile Company Sanford,North Carolina 

### Kiln 2 PC-2 Example Calculations Run 1 StackPressure, Absolute, 

### in. Hg PS 

### == PB + SP 

### == Volume



### sam~lf.g,f7 **s~-*c(IJW.+clJrh** 13
_ 6) VSID 

### == -------------------------------------------------- == TM+460
Moisture

**Conte~as** 

### Stream Bvvs 

### == ---------------------------------- ==

**VSID+~** 

### Percent

**Mo%W~' ~~ck** 

**p~** 

### == --------------------------- ==

**VSID+~** 

### Mole FractionofDryGas

**100-P~**



### ~ 

### == ----------------------- == 100 Mole. Wt. StackGas, DryBasis, lb/lb mole MD 

### == 0.44 

### * %C02 + 0.32 

### * %02 + 0.28 

### * (100 - %C02- %02) 

### == Avg. StackVelocity, ft/sec (TS + 460) VS 

### == 85 49 

### * CP 

### * DPS 

### * SQRT -------------------- 

### ==
. (PS 

## * MW)

A-12 

### 29.382 54.00



### 3.46 0.060
6.0
0.940 29.084 28.416 50.4

### SUMMARYOFRESULTS EPAMETHOD 26A Determination ofHydrogen Halide and Halogen Emissions Lee Brick & 

### Tile Company Sanford, North Carolina Kiln 

### 2PC-2 Gas Volume Flow, DryStd. Cond. CFM 1058.82 *VS *AS* PS * (1- Bws) QS 

## = ----------------------------------------------- = TS 

## + 460 Actual Gas Volume Flow, 

### CFM QA=VS*AS*60= Gas Volume Flow, Wet Std. Cond., 

### CFM QSW = QS * [1/(1-Bws)] = AreaofNozzle, ft2 AN= ((DN/2) A 

### 2 *3.14159)/144 = Percent !sokinetic 0.0945 *(TS 

## + 460) *VSTD PEFti = ------------------------------------------ = TT 

### *VS *PS *(1- Bws) *AN Hvdrogen

**Fluo.ride.Con~entration,** 

### gr/dscf (At ::stanoarocondltJonsJ 

### CAN = 0.0154 *FMF

## IVSTD = Hydrogen Fluoride Emission Ftate, lbs/hr (At Standard Conditions) CAW = 0.00857 * CAN *QS = Standard Conditions 68 Deg. F, 29.92 in. 

### Hg

A-13 

### 12642 22281 13453 0.00053 99.5 0.0250 2.70

### APPE.'iDIX B
FIELD DATA SHEETS

B-l

### EPA Method I Detennination of Sampling Ports and Points Oieot 

# L?t G .. s.k c-0 

# :t\P Sampling LDcatioo 

### (.I., 

### ?.. PC..-.; \ Sampling Location Dimensions: From Far Wall to Outside of Port 

### 51.J· 

### 7S Nipple Length 0 Depth ofDuct 

### 31.1. 

### "15 ,. Width (Rectangular Duct) _ _;r_J_f.__ Equivalent Diameter Calculation (DE): Zx Leo•tbx W'odtb 2 ( / ) ( / City/State 

## Sc,,,f; c

## 2 Date G" < 'i l 

# \ I

. I

**D!Si1.1RBANCZ~** !- 1 I I
SAMPUNC _ LOCArloN I 

# I ' • II

**'~** 

# ,o 

# i-

**~** 

# LJ_ 

# ill , DE = ----- = ------ 

### =_,_/',..:/f..;_,_ K 

# II !

**_Q~** · 

# I DIS'I'URBANC!:



# \~ Distance to Ports From Nearest F1ow Disturbance! Upstream · A Downstream · B 

## .,

**~"** 

## '=---'•

**·~?:''** 

### .n Dimensions in Inches {.:J -r.;u ..-r-" 1 ,(..-'· 1 Duct Diameter> ,)D



### ~-~ 3.

### .,-j Stack Area. in Square Feet 

### 7. 

### 3 7 Calculations By _:£!.:::._•'?:::..______ _ ScMnuzlic ofSampling Location

Poinr .Nippl• DIS&aicrFrom

**~**

# .. St.dc:.ID m Leoom Outsid ..oC Port I 

### 21 3(,.1S" 6.77-+/ 00 0 

### I. OC> 

## 2. 

## 0.1 1,\o 

### .lS" 2.L{(o 

# " 2 . "{(., 

## J II 

### & ')G 1\ 

### 'iT D 

### '1.3'-i 

## '1 tl.l j (,. .11"" 

### C:... )o 

### D 

# v. <;U 

# s- 1).o I

### "i 0 

## 1 

# t'i (, 3(".<., 

### 13.08 0 

## 13.08 I 

## Vi. 3r..ls 23. 

### I 0 

### 2.3 (p

### l 

## 6 1S".o 1t..

# 7s )I. 

### ')<,. 0 

### :tl.((.. 

## 'i 

## B.L

# > "'k· 7\ 

### ?:.c. 1. ,.- p 

### ?,c. 

### 2,(' (u 

### 1(-e L :3<,.75

**~2....'1{ ~**  

### )2-.

**~** 

### ( f3.3 .7\' 

### )i . 2 

## 'i 0 

### 1i.'2-'7 ll- 

## 'P "i

**,~.,,7)'** )f.'iA..; 

### ;o; ?(' 0 ";;', 

## ,( 

# @ I

# • .Cr.-...

**.~J.dllUU** - 

### Determination ofStack Gas Velocity, Volumetric Flow Rate and Cyclonic Flow Gient C,.""€ BIZtct<= ·' {;u,£' Sampling Lcc>LJOn 

### ;!,<.A 2 f'c - I Run D>ee <I-/e -17 Barometric

**Pressu~.** in. Hg _ _.:;::2.;;..1_ ....;.'1_1 ______ _ S<><ic Pressure. in. H,O _-...;.o:...:...·':..:'--------- S<atic Pressure. in. Hg _-_o_._oc...;..:;S ________ _ Stack Pressure. in. Hg -.,-.....="2...;.'.;..·<1'-'o'-'z."------=--- Stack

**Dimension~** in.• di:uneter/side 1 3(..?S City. StJ.te

**5.-...J~oiZb** Ale. Oper:nors G"L§ , JoA Tune o o Pitot Tube I.D. No. -.:;2.:..:•.::."'-;·..:o:,:z:..:S"-------- Date Cllibr:ned 

### --="':..;;,t-/..:•-'J,t-/.:...1.;..7-:::--:------- Pitot Tube Coefficient ___ c...;.. B::....;,</,---.,.-:---- Leak Cleek.

## in. H,O <0.1 @ 8.7 

## .> </. I Side 2. 

## in.--------------- Field Data Tr:t.nrse Vdodtr Head .1p fnd'ies. Sladt Cvdonlc Flow Ofienninaelon

**P~nt** u,o TempenJureT ."lumber

**~-** at o- R.t'f'ft'ftlC8 Antle wtlldl Yldds a. Sun .1D·

( o.o/8 

## o.oe "2 <lfc "253 0. /C., 

### o.es l't 

## z.e, 

## z o.o'l 

### C!.o'l '2.

### '18 

### 2-!>i. 0 ,(.,. 

### o. II I I 

### !'I 

### 3' C./0 0. /7. 

### z.'/7 

### r.5s0. '" 

### o.o' fu /1... y o./o 0./2 "2.$b 

### "255 0 .I/ ll.oS 0 

## 5 

# I s 0.10 C .12. '2.</(. 

### 2.54 {)./0 0.07 tO 0 

# " 0./<.) ().(/ '2-t/7 'Z.5"I 

### o.oo

**{),a~** 

### ,5 17 

## 7. 0.1

### I (J./0 

### v(1 '253 o.oS 0 .0"" /7 "2.2.

**~** 

# I CJ./I 0.10 "2

### 5

### S'"" 2.5!

**o.a~** a

### .o1 

## z.c.. !>/ 'I 0 .1{

**().C~** 7. 

### 57 2. !:i5

**~** !0

**~-IZ** 33 7."2. (Q 

### o.<t.'T l!.cS 

### "2.5'7 2.5! 0.// ().!] 7.1 '2.!) II 

### o.og 

## c.c'-

**""Z'!i~** 

### :2..$5" ". (0 f) .f

### <I :z.G. 

## z.:; 17.- 0-07

**~-clo** 

# ZS"< 2..5'1 t) .10 

## D.!'/ if! 

# s.J 

# I

**o.cfl~** 

# z.5z.. . /9.5° Ann... Stack Temper:lture, Dry. "F (A) 

### l 

## '7 "2.- Difference (A· B) 

### 1.-z... Stack Temper:nure. Wet "F (B) __ ,:_1.:.,1..:;o __ _ Preliminary Pereent 

### Moisture-----=·(.,~---
**Commen~-------------------------------------------------------------**



# ®~J'k Dale: 

### 'f I Z.l I '!7 B-3

## EPA ,}[ethod 3 - Molecular Weight Determination - Data Analysis Client :-lame 

# 6 I r 

### J( Project :-lumber Ci-t(r'-(7-o-{ 

### 8 City;State 

### < 

### £..v) N(_ Sample Date Cij 1/'<ijl Sampling Location V:::J. .:> ., PC.- I Operator LA6 Sample Type '"-Tedlar Bag aLMultipoint o Single Pomt Fuel Type---""'/U'"'·'-;-!v-c-"7 1----:;C,:-- 4,----- Analyzer Type Orsat Serial # 

## 8'1-

**~**c I lir Oxygen Calibration Check Must Be 20.9 :!: 0.1% Analyzer Leak Checks o Pipet and Bubbler Levels Leakfree? j1q_ Buret 

### ff. l - I

### '1, 1 

## = <0.2 mJ? Run # and/or Sample ID Sampling Time (04 Hour Oock) c9H 111 

# - - 

## - 5> Gas Replicate 1 Replicate 2 Replicate 3 Average Multiplie.- MolecularWeir,ht Percent Dry lbilb moe Actual Net Actual Net Actual Net 

## co, I,(' 

# r.s /, L{ j, '-( I . '-( 

### I. 

## 'i I. 

## '1

## J

## Ji!" 0.44 

## o.

**~3i** 

## o, 

# zo.( {'I 0 

## 16 f i'i I 

### 2o. '-\ 

## 1'1 0 

### l'i.

**u;!>~** 0.32 

# G. 69 I 

## co 

## 2.JJ .§ a.o Z- 0.\ 

### !).o 

### -z._o .

**~(** 

### a 

### c - 6. 

## ou 0.28 

## o. (; 0 c N, 100 

## ·7'1.)"' 100

**1~.** Sb 100 l'i. (, 

### l"i.)'!>J'

# ".- o.28 . 

### <l- 

### 1Vi Total 

### 28. '1'11 Run# and/or Sample ID



### -~--------- Sampling Time (24 ·Hour Oock) /1-ZC: • 15"2.-/ Gas Replicate 1 Replicate 2 Replicate 3 Average Multiplier MolecularWeifoht Perce 1 

## 'jL Dry lb/lb mo e Actual Net Actual Net Actual Net

**~**

# ..· 

## co. ' I .

# "t 

# '" I. 'l I.

# 9 /. t I 

# e,

**~~~~**

**~1** 0.44 

### 0. '62.1 

## o, 

# zo .4 

## 1B.)" Zo 

## '1 JQ,( Zo .3 ig,(' 

## IB.S"o0fl 0.32 

## '>. '!20 

## co 

# zo. '1 l).o 

## Zo -{ (),Q 

### ?.o. 

### 3 O.D 

### ~o,;.;•S, 0.28. 0, 6cc N, 100 

### l'i- (p 100 l'j. (, 100 <'i .., l'i ,(r

### >I>¥ 0;28 

### l'L. Z'i/ Total 

### 2"1. 038 Run # and/or Sample ID """---------- Sampling Time (24- Hour Oock) ;</Jz 

### -;S;/ Gas . I Renlicate 2 Reolicate3 Average· Multiplier MolecularWeight Renlical<> 1 Percent Dry lbllb mole Actual Net Actual Net Actual Net . 

## co,

**1.~** 

## LS ,_,... (,)""

**1.~** 

### 1.\ 

# 1.s-o 0.44 . **().f,~o** 0 ·•

1 

# -z.o. .3 tS.

# e. 2o.:. 

# ,e,.e. --zo';

**l8{~** 

### /3.\Xl 0.32: ·.· 

## c,. o10 

## co 

## Zv.J O.o 

### "lo. :> 

## o.o 

## u ... o-o o.o0 0;28 O-ooa N, .. 100 ·. 

### l'i 1 100

**~.1** 100 l'i. I <'i.lo 0.28 . 22.. 31\- Total 

### '2. $' '1'1 2.. Note: Calculate the F, before evacuating any bag samples. Compare the F, to the expected fuel values. If a discrepancy exits, reanalyze the sample. The F, calculation is as follows: F = 20.9% - %02



## • %co, F.,. Ranges For Common Fuels Anthracite Coal and t.ianite L016 · l.l30 Wood 1.000. 1.120 Bituminous Coal t.083 . 1.230 Wood Bark: 1.003 . 1.130 Distillate Oil 1.260 · Ul3 Satural Gas 1.600 · U36 Residual 01l 1.210. LJ10 ?rooane 1AJ-l · 1.586 13--1 Date: 

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# ·.:a Nozzle .'io.

**--"J~c:;_v'.::.O..!.q.::.5_** Orsat System 

### 0 r .:'<t 1-- End Time \

# l'77

ll-l2 LEAK CHECKS Pre-Test 

### 0 .t...'C.I @ 

### i ,- In. Hg. Post-Test 0 . . --, @

**~-~** In. Hg.



### Pre·T~st Pitot <0.1@



### :.._'9~tr In. H::O 

### _q_t Post-Test Pitot <0.1@

**~** :.1 In. H!O Tedlar Bag :'-lo.

**-~?:__**

### ____ _ Bag Look Check



### _::.C'.!.v_,(~----­ Observer (_[,._ .../{er, C}l .,:;..:Cl,d/,,



# :)3

### EPA J!ethod I Determination of Sampling Ports and Points
Sampling Location Dimensions: 

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### 5L.. 7

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## V ) City;St.lte __ 

### :S::c:.:.··"':.:.';.:•:.:.·r~cl~:.:.~::._J:_~------ Date __ _:C::...'"::...,:...I

**:._'~:.:.1.::.>:.:."**________ _ 

# \ I DISTVREANCSil' . SA,lJPUNC LOCATION{- 

# l I K 

## ·---- =----- =_..!,.;1!...:.!)/-_ DE= Distance to Ports From Nearest Flow Disturbance: Upstream· A 

### IS''

**~-·/~.~** Dimensions in Inches 1..;"' Lt-.....

**~** Duct Diameters ,{1.0

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### 2>.o ')').(., (/1. '{ 

### 1\.o 02..3> 

## Bs. 2. 

## '1J.j 'j/.q s I

### 2."'"

SciwmalU: ofSampling Loetzlion

Slade Dbtance- F'rom

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# I 11. Z."i >.

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### 71' 

## {.- !,Cl)"'

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# J

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## _.;.s;,_.

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## I> 1 Preliminary Percent Moisture __ 4"-'"'-----

**Commen~--------------------------------------------** 13- I4 

# e;.'l

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# 1 I

## zz . '7

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### L PC - ? Operator_..::"-::;1'3:.:.'.:.,•(_---,.----- Sample Type lil._Tedlar Bag

**~Multipoint** c Single Point Fuel Type t0

## -.+. 0 ( G-s Analyzer Type Orsat Serial# 

## t"- '>co-/ (li__O:<ygen Calibration Check Must Be 20.9 

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### - 

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## co, J.] 

## 2 3 2 3 

### 2 3 

### J -( 

## '2.'{ 2. 

## "'>31 tK-

**0.~** 

### I . 62\ 

## o, 

## 2o. )._ !1 

## 4 2<-> .

### 2. /7 

## 1 Zr;.J- 

### 11 

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### '>· Iii 

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# o.o 0.

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### 1'1 

# 8 100 

# ...., g 100 

### 11.& {C., 'i)D 0.28 

## 22 3'-·1'-/ Total 

## 2'7 

## c 8 (, Run# and/or Sample 

### ID

# _2.=---------- 1!2<0 • IJZ--1 Sampling Time (24 ·Hour Oock) o>f3'5' ' '5'[



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## 1'1 2.o 2.o 

## Z -=-o¢'

### t



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## 0. 986 

## o, zo.?- !&., 

## 1'1

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### Oo Q.

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### N, 100 

## 11 

# e, 100 

### So-1 100

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## 1'1 'i

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### ID ..:3:::._ ________ _ 1'132- 15?? Sampling Time (24 · Hour Oock) I;;2 e >



### ]~ d 

## LVI) Gas Replicate 1 Replicate 2 Replicate3 Average Multiplier MolecularWeight Perceot Dry lb/lb mole Actual Net Actual Net Actual Net

. . 

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## 2( 

# 2s 

# - Z.) 

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# l-'lii12

# i1

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### 6

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### '1<1 "1 .··. 100 

# '71 '7 100 

### l<i.B

**l~ ~~=~-**  0.28 

## '2 2. ' JC,. 

# :> '77.61 Total 

## 2't {t-• ( Note: Calculate tbe F. before evacuating any bag samples. Compan: tbe F. to tbe expected fuel values. If a discrepancy exits, reanalyze the sample. The F. calculation is as follows: 20.9%-%0, F = **--;;;--;::;:~.o..**



### • %co, F., Ranges For Common Fuels Anthracilc Coal and L1tnite 1.016 . 1.130 Wood Bituminous Coal 1.083 . 1.230 Wood Baric. Distillate Oil 1.:60 · }A13 Suural Gas Residual OU 1..210. 1.370 Prooaae 

### ' Date: 

# I (21 I

# r 7 1.000.

**1.1~** 1.003. 1.130 1.600 . 1.836 U34 ·

**1..~86**

## ;313 

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______ 

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### 7) Chain of Custody: Date Received OJ

# ;;c, /c., 7 

### Received By PI< j 

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# - Run :-lumber /.- 

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## - '..:.' -:..c, Final Volume. ml

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### ::...... .::.- ::..oa ::..

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# ,., i-/o 

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**EP.~** Jfethod _-=-.:::'-' __ C:ienr __ 

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### ='t:..''~:~_J_:_f'J_C. ____________ Date _ 

### __;G,_''-f!..i/~I~:::..'"..J.'~-7 ___ _ Sampling Locaricn _ _c::'--'-''



### \~,·--7...=--_-_.c_P..:::;C::_- .=2..=------------ Oper:Hors _ 

### ___;:_70::_-~;_- ___ _ 

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### Z'<.

## Y!/1

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### L·o cv eter emp. _ _;_::___ Stack Temp. 

# '-!\ C

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## -~i!~'-'-!-**!,r~-**_::::L:__-__:_P-'r_c.:?_=------------ Operators

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# :-1ENGINEERING CONSULTANTS, INC. 6200 Harris Technology Blvd. • Charlotte, NC 28269 • {704) 598·1049 • FAX {704) 598·1050 April 22. l997 

### REPORT OF LABORATORY**Al~AL**

### YSIS Mr. Rad Holton Lee Brick & Tile Company Post Office Box I027 Sanford, North Carolina 27330 Trigon Project !1/o.: 046-97-048 Trigon Project Name: Compliance StackTest April1997 Trigon Sample Number. Date Collected: Description:**ln~u:gaoi~: aoilb:~i~**  Date Analyzed EPA Method ofAnalysis 

### !.!nils Fluoride as FVolume ofSolution Fluoride as FTrigon Sample Number. Date Collected: Description:**Io2rgaoi~:** 

## Aoilb:sis Date Analyzed EPA Method ofAnalysis Fluoride as FVolume ofSolution Fluoride as Fmg/1 I mg



### !.!nils mg:l l mg 7048-0! 04/l8/97 RWll K2PC-l 04/22197 340.2 102.2 0.650 66.4
7048-04 04/!8197 RWl l K2PC-2 04/22197 340.2 !37.8 0.650 89.6 Comments: All ofthe above data has been blankcorrected. C-2 7048-02 04/!8/97 RW12 K2PC-l 04/22/97 340.2 93.! 0.650 60.5
7048-05 04/18/97 Run2 K2PC-2 04/22197 340.2 102.6 0.650 66.7 7048-03 041! 8/97 Rwt3 K2PC-! 04/22/97 340.2 98.1 0.650 63.8
7048-06 04/18197 RW13 K2PC-2 04122197 3402 !46.0 0.650 94.9 7048-07 041!8/97 Field Blank 04/22197 340.2 <!.0 0.650 <0.65Mr. Rad Holton Page 2 Apnl22. 1997 Trigon Project "'o.: Trigon Project Name: 046-97-1148 Compliance StackTest April 1997 The data contained in this report were obtained using U.S. EPA approved methodologies. These data have been reviewed and are approved for release.

Paul R. Jenkins, Jr. Laboratory Director 

### QUALITYASSL'RANCE DATA Analyses were performed using Orion Model 720A Ion Selective Meter. Serial Number 001390 and Fluoride potentiometric electrode Model 96-119 BN, Serial Number XZl 01736. Reagents used in performing these analyses were logged in the Trigon Laboratory Analysis book as follows: Fluoride Standard Number 3173-16 Lot NumberF:2 11 1,000 ppm as FFluoride TISAB Number7-34021 Lot Number02276LL Fluoride Electrode Filling Solution Number90000I Lot NumberYZ1 The slope for the fluoride electrode was -57.9 millivolts. The acceptable slope for the fluoride electrode must be in the range of-54 to -60 millivolts. The following matrix interference checks. calibration performance checks and precision checks were performed: Trigon Sample Number: 7048-112 7048-113 QCl-710 Date Collected: 04/18197 04/18/97 07/15/96 Description: Run2 Run 3 Laboratory K2PC-I K2PC-1 Control Duplicate Spike Code 64669 ID!l[gliDi!:

**~Dllb:5ia** Date Analyzed 04f22197 04f22J97 04f22J97 EPA Method ofAnalysis 340.2 340.2 340.2 

### J.!n.il.:i Fluoride as F- mg/1 91.8 87.9 9.89 Volume ofSolution I 0.650 0.650 0.100 Fluoride as F· True mg 59.7 8.91 9.73 mg/1 Percent Recovery o/o 1.4% RPD 98.7% 10!.6% Sample No. 7048-113 spiked with 4.0 mg/100 ml ofFluoride as FRPD = Relative Percent Difference

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# Trigon Engineering Consultants, Inc. Lee Brick (046-97-048) 

# Analytical Report (0497-24) 

# EPA Method26 Hydrogen Fluoride


# EnthalpyAnalytical, Inc. 32 I I Bramer Drive Raleigh, NC 27604 919/850-4392

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**~•** ENTHALPYanalyt1cal, 1nc C6Comp4Dy: TneorvLee Bnck Cliem ff: 046 4 97-048 i ' Analyst: BGH Enthalpy#' 0497-24 ParaJl)l:ten: Hvdroacn Fluoride. PO#' Verbal

**lfS~es:** 7 Reoort Date: 05112/97 Compound 

# I Sample 1D & Catch We1ght tug) 7048..08 7048..09 7048-10 7048-11 7048-13 Hydrogen Fluoride 68,159 68,170 52,208 87.497 75,711 88,263

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Client#: 046-97-048 Anal_yst: BGH PO# Verbal Custody Analysis

Labeling Reproducibility Quality ofData Reporting Notes Parameters HF Samples were received on .!./23/97 by Steve Eckard afterbeing relinquished by Paul Jenkins ofTrigon. Samples were cold upon arrival and kept cold during storage. Prior to and during analysis thev were kept under lock with access only to authorized personnel ofEnthalpy Analytical, lnc. The samples were analyzed for hydrogen fluoride according to the procedures outlined m the EPA Method 26. Quanntauon was performed a Hewleu Packard series 1100 High Performance Liquid Chromatograph. Detection occurred by indirect UV at 280nm. Separation was accomplished by a Hamilton PRP-XlOO 150 mmx 4.6 mmanion exchange column using 2 mMpotassium hydrogen phthalate pH6.1 as the eluent at 1.2 mL per minute. Standards were prepared in 0.1 N H2S04. A four point calibration curve was run before and after the samples. Data from all calibration runs were used for the calibration curve. The linearity coefficient ofthe curve was 0.9999 OK OK- The lower (first) standard calculated values were between 66% and 147% ofthe tag value although the peaks were well above the noise level. The samples did not have similar variability in the reproducibility. All samples were significantly greater than the lower standard. OK MDL --Minimum Detection Limit. LOQ --LimitofQuantitation.

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# ~ ENTHALPYanalyt1cal. 1nc.'(j0"'('-,._.,,_,_.,.,.TrigonEngineeringConsultants,Inc.Company:L..b•..lt.r'•Address>:..·t.-r"'1.()ChainofCu11ti>dy·Sampler'sSignatureContact:f.,1J:,lo....ProjectNo.o¥/·1.,-t:J..,,PurchaseOrderNo.NumberofContainers:7-IJ..p,,/'·/'tj.//'""SamplingMethods:rYJ.-II..c1.,(t1HF()SampleIDIDateITimeISampleDispositionRemarks'I1.............""'/).·r.q1>..,ll/........,Q.·l.'·,t'.·1,I,/,._JcI.c".I.•;..,;.,"""Ic/:.•.IL..JLj-.l.ic.,J"--·tf,_.....(.,L'f..p,,'..-1.•L.-1((.,.._;,)l"tY.u/c:-'t?:•,:;'/Jv<,-S-/oCIf,J...,?...,11/(j.tor;J··7,.III-/o._,,.-It111&IIl'l7•:IclA/fl.""'/(/·1•Jfl<,il'lL.tJ·f,vC·l...,f.',.>tJ,,'0·I1'-tf.z)v•).zPt•'I'<-1J:.'!..Pt•I"·',..._"-J:...z...P<..::./'\'-IIVi7-•7c-·£...,,..,._/,-lL.(,••'<,C•._,'-'·''1&'..../..f-/<C.],17\'-"''J,1-o./L//).·/.-:.(c;,_...'f,hA,.\//'By:/),-(jI../.1/.flLReceivedforLaboratoryBy:Date(fimeIIIr;,{J_Date(fime___I______I___/I',\<·-.f,,'·'j..;.).2l/It...,,.k./1n.F-..A(,';By:'Comments:Date/TimeI'"'$6·4f.7I--4-n,;,IDate/Time"'{J/1"11tx;n

# Sample Chromatograms**,..-~**

# :::~ 

# 1 C-14 

### .......:

# "~ ENTHALPYanalytical, inc**=~:** es:::...:;r.. ::·a::e Sa1:1.p:..e Name 

### Ace.

**Ooe::-a~or** S
**~1.:::.....,",:...:::.** ';:;'.:lo

**e~**

### ..... --...'--- . --- 

### _o,.cq. Method .4l: ..a2.ys :..s Me-:hod 

### Las:: changed 08 -Nay- 97, 20::6:4: Seq. Line '7048-08

**~,,** Via: !3GH

**In~ F:\H?CE~M'\2'.SEQU~~CE\0497-24A.S**  

### A.NIONS.M

**F:\H?CHEM\2\ME~HODS\0497-24A.M** 5 

### I 9 

### I 9 7 9 : 3 7 : 2 9 .Z\.!"1 

### by BG2 Ar ...a:..ys:..s

**c~** a:-- ..:..or:s Ion by V-;a:.e::::-s

**~:;c:.** :::·: - PRP-x2-0C 150x4 .l :::o:u:nr: WJD1 A. Wave!engtn-280 nm **(0497-24A\054-C50~** .Q) mAU



### ~ 175- 150- 125-

**~** N 100- 

### .,. .,. N 75- 50- 25- /

0 0 2 4 6 8

**Ex::e~~al S::anda~d**  

### Report **=====~===============================================================** 

### Sorted By Calib. Data Modified Multiplier Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area AmtiArea Amount Grp Name

**[mi~]** mAU 

### *s [ng

### lull 

# -------l------l----------l----------l----------l--l------------------ 2.442 VB 

### 888.68726 1.49852e-2 13.31719 HF Totals 13.31719 

## =====================================================================

**~~~ E~d**  

### of 

### Repor: 

## ••• G::-cuc::o 5/9/97 9:4:3:16 AM BG!-: C-15 

### ?age 1 

### :c:: -

# ,-

.- .....

**~** ::: ,_,, ____ _ _,.:.. .. - I:-:j ec::.i::)r_ Da-ce 

### Samp:..e Name 

### _:;:::c;. Ope::-a:.or Seq'.J.enc<::: F:.le 

### Acq.

**Me~hod** A.::a:..ys:..s 

### Me:.hod. Las= 

### cha:1ged. 02-May-97, 

### 2C:2S:35 Sec. Li:1e 

### 7048-08 *ll

**V~a:** BG!-:

**~-** 

### F:\E?CHEM\2\SEQVENCE\0497-24A.S AlCONS .M ? :

### \H?C:iEM\2\ME':':lODS\. 04 9-:- 2

**4-~-.** 

### M 5

### I 9/97 9 : 3 7 : 2 9 A."l 

### :Jy 3G:i: 54 2


### ;..r.a::..ys:..s o: a::ions l:::)n by 

### Wa':ers 430 IC - PR?-xlOO 2.S0x4.: c:;.:..'.liT'C.

**mA~** 175- 150-

, 25 -= 100

**~**

75- 50- 25- 0 0WJS1 A, Wavelength=280 nm (0497-24A\054-C502.D) 

## "' "' "'

2 4 € 8 

## ===================================================================== External Standard Report 

## ===================================================================== Soo:-ted By Calib. Daca Modified Multiplieo:- Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not reported Signal 1: VWD1 A,

**Res~lts** 

### obtained Wavelength=280 nm with enhanced integrator' RetTime Type Area Amt/Ao:-ea Amount Grp Name [min] rnAU *s [ng/ul] 

# -------l------l----------l----------l----------1--l------------------ 2.441 VB 871.13208 1.49818e-2 13.05115 HF 

### Totals 13.05115 

## ===================================================================== *** End of

**Repc~t ~~** * 

### G:-ouc:;.o 5/9,/:::; 9:43:34

**-~'V!** 3GE C-16 ""= -

### - --- = .--:__::-

**~.-** ...:...·.

**Sarr.~~e** 

### Na:ne Ace;. Ope::-a::or

**Se~-.1e::ce** 

### F:.2.e Ace;:

**Me:::~oc**

**~.:..a:.ys.:..s** Me':.hod I..as<:: cha::ged **~** '_.,.-.- ·'- 

## ----- -·-- 

### 08-May-97, 20:42:2l Seq.

**~~~e** 

### 7048-09

**~1: V~a**  

### BGH ·-" F:\H?CSEM\2 1

### \SEQUENCE\0497-24A.S 

### ANIONS.M F:\HPCHEM\2\METHOCS\0497-24A.M 5/9/97 9:37:29 AM by BGH

**?R~-x:·JG** :.sex.;.:. ::::l'...lrn:". VVVD1 A. Wavelength=280 nm (0497-24A\055-0601.D} mAU



### ~ 175- 150- 125- 100- 75- 50- 25-

0 0 2 4 6 8

**ExteY~al** 

### Standa=d

**Repo~t** 

## ;;===============;=================================================== Sorted By Calib. Data Modified Multiplier Dilutior.. Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime 

### Type Area Amt/Area Amount Grp 

### Name [min] mAU *S 

### [ng/ul] 

# -------1------1 ----------l----------l----------l--l------------------ 2.445 

### vo 952.83130 1.49966e-2 14.28927 HF Totals 14.28927 

## *** End of Reporc 

## *** G:-oucho 5/9 9:43:51 AM BGn C-17 

### :?age l 

## c: ::.. 

# ,Y/

### ( \ 

### Sa::cp:..e Nane Acq. Cpe::-at.cr Seque!:ce 

## ?:..:..'= A::q.

**Me~hod** A....."'lalys :..s Met.!lod

**Las~** 

### cha::ged **08-May-9~,** 

### 2C:55:04 Sec;:. 7048-09 

### *::.: SGn 

### ?:\E?CHEM',2\SEQUENCE\0497-24A.S ANIONS.M F:\E?CHEM\2\METEODS\0497-24A.M 5/9/97 9:37:29 AM by BGn 

### Line Via::.. 6 2
F

.... "'la::..ys:.s cf anions Ion by Wa-cers 430 IC - PR:?-x:oo ::..sOx4 .l ::::J:;.u:n::

mAU 175...:: 150- 125- 100- 75- 50- 25-

0-

0 W./01 A, Wave!ength-280 nm (0497-24A\055-0602.0)



### ~

"- <0 

# .. .. N (• 

## ,, '

2 4 6 I I 8

**==========================~==========================================**

**Exte~nal Standa~d**  

### Report 

## ===================================================================== Screed By 

### Calib. Data Modified Multiplier 

### Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42

**&~** l.

### 000 0 1.0000 not reported Signal 1: VWD1 A,

Results obtained 

### Wavelength=280 nm with enhanced integrator! RetTime Type

**A~ea** 

### Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------1------1----------1----------1----------1--1------------------ 2.446 va 917.41705 1.49905e-2 13.75258 EF Totals 13.75258 

## ===================================================================== *** End of Report *•* G!:'oucho 5/9/97 9:44:08 P-..1'1 BGH C-18 Page _ 

## c: _ 

# ..

m:

### Sample Name Ace;. Operat.or OS-May-97,

**2:.:c-.~,** 7048-10 *ll 

### BGH Sequ.e:1::e File F: **\EPC.HEM\2\S:SQt:-"ENCE\0497-24.~** .. S 

### Ace;. Met.hod

**~FIONS.M** 

### Ana:..ysis Met.hod F:\HPC2:EM\2\ME'::"HODS\0497-24A.M Last changed 5/9/97 9 : 3 7 : 2 9 AM by BGH Seq. L2.:1e 

### Via:. 

### 56 _.. **~.:** - 

### --

**.~"lalys:.s** 

### of ar_i.ons Ion by wa-:ers 43J ::::c - PEF-xl:JO 2..5·Jx4. 2.. ·:::J2.'..lrrw
mAU 175- 150- 125- 100-' 75- 50- 25-

0 VWD1 A. Wavelength-280 nm **(0497-24A\056-070~** .:J) 

## "' 155_,

2 6 

## ===================================================================== Exte=nal

**S~anda=d Repo~:**  

## ===================================================================== Sor::ed By Calib. Dat.a Modified Mult.iplier Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not. reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------1----------l----------l----------l --1------------------ 2.430 VB 767.52802 1.49585e-2 11.48107 HF Totals 11.48107 

## =====================================================================

****~ E~d**  

### of Report *** C·l9 

### Groucho 5/9/97 9:44:25 AM BGH Page l 

## c:: _ 

# S3 mrr

## ===================================================================== :::::jecc:_:Jn

**:Ja~e** 08-May-?'7, 21:28·:47 Seq. L:..:;.e 

### Sam:t:=le Name 7048-10 •:.1 Vial 56 .:..cc.

**O:Je~at.or** 3GH

**I~j** 2 

### Seque!lce ?ile F: \ H:!?CHEM\ 2\S2Ql'ENC2\049

**~-** 

### 24A. S Ace.

**Met~cd ~~:ONS.M**  

### J:._li2.ysis

**Met.~** ...od F: \HPCE3M\2\ME':'EODS\0491-24.:;..M 

### Las:: cha?::ged 5/9/97 9:37:29 A.M 

### by BGH _r..._'"la2.ysls o:: ar.;.ions Ion by Wacers 43C IC - ?i(.?-x:..oo 2.50x4 .l 

### cclurn ... "": mAL: 175- 150- 125- 100- 75- 50- 25-

0 0VVV01 A.

**Wa~Je!ength-280** nm (04S7-24A\056-0702.D)

2 

## "' N 

### " N

4 6 8 

## =====================================================================

**Ex::er~al** 

### Standard Report 

## ===================================================================== Sorted By Calib. Data Modified Multiplier 

### DiL.ttion Uncalibrated Peaks Signa2. 

### Friday, May 09, 1997 9:36:42

**-~** 

### 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator' RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------!----------!----------l----------l--l------------------ 2.428

**v~** 

### 765.29181 1.49579e-2 11.44718 HF Totals 11.44718

**~**** 

### End of Report 

### *•• 9:44:42

**;.1~** 

### BG:O C-20 

### ?age

**.-.~** 

## , 

## - .....,_ 

### - 

# ..

m1:

### ::; :=-- J 5: :._.:: Sa..:n:;::..e

**~Ja:r.:=:**

**Ir~j** 

### ec':.ior-_ Sa:.e Samp=..e Name 08-May-97, 2::33:4: 7048-ll 

### "A":.: Seq. L:..:1.e 

## v:..a:..

**Ac~. Ope~a:o=**  

### BGH Inj l 

### Sec:::-.le::;.ce File F: \:,CPCH3M\2\SEQu""ENCE\0497-24A. S Ace.

**Me~~oc ~-~=ONS.M** 

**~-'a::.ys** 

### is Me::hod F: \H?C:n3M\2\ME':'HODS\ 04? 7- 

### 24A. M

**Las~** 

### changed 5/9/97 9:37:29 AM by BGr.

**.~J.al.ysis** o.: 

### an:..ons :on by Wa-:.e::-s 43C :::c - **P~:?-xlOO** 3..50x4 

### .1

**co~'..l:nr.** \fl./l/01 A Wavelength-280 nm (049i-24A\057-0801.!J) mAU

**~iS** 150- 125- "- :I: 

## "' 100- 

## "' .,. N 75- 50- 25-

0 0 2 4 6 8 

## ===================================================================== Ex-:.ernal Scanda::-d Report 

## ===================================================================== Sor::ed By Calib. Data Modified 

### Mul':.iplie:::- 

### Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 

### not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.455 BB 1134.99304 1.50220e-2 17.04985 HF Totals 17.04985 

## ===================================================================== **"ll" 

### End of Report 

### ***

**Grouc~o** 

### 5/9/97 9:44:59

**k~** 

### BG:,C C-21 

### Page C; 1 c -**::1~2c':i:Jr:** Da:.= 08-May-91, 2::46:30 

### Seq. 

### Samp2..e Name 7048-l::... .,..::..l

**~v·ia2..** • C BG·_,.;_ 

### n.::c;.

**pe:-:~?=-** 

## s - ·· "" "'

**\""DC'-~M\·' -~~'-"'NC-'**  **0'-~** 2'' •

eqJe::..co:::

**.:'-~- ~:**  n-

**::.~** .::.\;::.C:.'>c!i..,' ..... !!.\ --::;:::,-

**~.'""l...,:,** I'"'-i --" 

### A:::: a. 

### Me::hoC. JI.NIONS. M lL'"1i=._ys is Me::hod F: \B:?CHEM\ 2\METHODS\ 049'7- 2

**4;.~.** M 

### Las':

**cha~9ed** 

### 5/9/97 9:37:29

**~~** 

### bv BG2

**.;....:-~a::..ys:..s** ::.: ar:ions Ion 

### by Wa:..e=s 430 IC - 

### ?;.::-x::.oo

**~5Cx4.2.** mAU17:S15C125- 100- 75- 50- VVVC1 A._ WaveJength-280 nm (0497-24A\057-0802.:J) 

### 8 

## '"

"' "' v N 

## s

25-


# ------~~~----------------_L------~--

0 

### c 2 4 5 8 

## ===================================================================== External Standa=d Report 

## ===================================================================== Sorted By Calib. Daca Moci=ied !VIu:. ciplie:::- Dilutior. Ur.calibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not repo:::-:ed Signal l: VWD1 A,

Resulcs obcained Wavelength=280 nm with enhanced inceg:::-acor' RecTime Type Area Arne/Area Amount Grp Name [min] mAU •s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.459 B3 

### 1127.93579 1.50212e-2 16.94290 Hr Totals 16.94290 

## ====================================================================;

**~~T** 

### End of

**Repor~** ***~T** C-22

**G~~u.c~** ...o 5/9/97 9:45:17 F-..\1 BGH 

### :=:age _;_ c: ::::::-1;ec=:..on Da::e 02-May-97, 2:.:::?:2l Seq. Line 9 Sar.1p:.e Name 7048-:2 "'l: Via2. 52

**-~-** Aca. Onerato= BGH I::j 1 • - F 'l F \'"""cu-"\21

**--r;·•-N~-'** 0"-a- 

### 24' " Seque:::ce :. e : n_ .r:..t:.1·:

**\~.::.;,.:C.!:..!.,_.:::.\** _.., 1-

**r~** .... 

### Acq.

**Me~hod** 

### AN:ONS.M '· ' . M . d F \··or'-1-M' 2·

**M-~--oDS\0"-9-** 

### 24A M

**.'"u-:la~ys:..s** 

### etno : rL

**~·-"-** \ \ ...::..:cl • !· .. 

### • -

**~** 

### d "/9/97 9 3- •• 'M

**~** 

### -G·- .:...;aS ._ C_..ange ::: : I : L. '7 .-u . ...;y b n 

### Ar.alysis of anions Ion by Wat:e:cs 430 IC - PRP-x100 150x4 .1 ·column
mAU 175- 150- 125- 100- 75- 50-

0 VVV01 A. Wavelength-280 nm
**(0497-24A\C58-0901.~)** 

## "' "' '"

2 4 

### Exte:cnal Standard Report Sorted By Signal 6

Calib. Data Modified 

### Multiplier F:ciday, May 09, 1997 9:36:42 AM 

### 1.0000 Dilution Uncalibrated Peaks Signal 1: VWD1 A,



### Results obtained 1.0000 not reported Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount [ng/ul] [min] mAU *s 

### Grp Name 8



# -------1------1----------1----------1 1--1------------------ 2.463 Vb 

### 1154.25696 1.50242e-2 17.34179 HF Totals 17.34179 

## ===================================================================== "'"'* End of Repcrt C-23

**G!'8t.;.C~'10** 5/9/97 9:45:34 AM BGH 

### Pa·;e l o: r .(" 

### ', :r..jec:.:..or: Da::e 03-May-97,

**..::;.:..:~..::;:_.:..**

**Sam~~e** Name 704S-l2 *ll 

### Ace.

**Ooeca~~c** 

### BGE sec:rJ.enCe File F: **\H?C:-12M\2\SEQGENCE\0497-2~.~.** S 

### Acq.

**Me~h~d ?~IONS.M**  F

.... ·.1.alys:..s Method F: \H?CH:::M\2\ME:T30:JS\049/-24;.._.M

**~as~ cha~ged**  

### 5/9/97 9:37:29

**-~by** 

### BGE Sec. -:l:_a:-_ I::j c 

## ss

**?-~alys~s** 

# o:

**a~i~~s I~n**  

### by

**Wa~ecs** 

### 430 IC - **?~?-xlOO** l50x4.l colurrc. mAU 175- 150- 125

**~** 100- 75-

### so25-

0 0 VWD1 A, Wavelength-280 nm (0497-24A\058-0902.'J)



### "' 

## "' " N



# •

**Ex~ernal Sta~dard**  Report € 

## =====================================================================

**S~rted** 

### By 

### Calib.

**Da~a** MoCified 

### Multiplier

**Diluti~n**

**U~calibrated** 

### Peaks Signal FriCay, May 09, l997 9:36:42 Pd"v'! 

### 1.0000 1.0000

**n~t rep~rted**  

### Signal 1: VWD1 A, Wavelength;280 nm

Results obtained with enhanced integrator' RetTime Type Area

**Am~/Area** 

### Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.459 V3 1081.10022 1.50154e-2 16.23313 

## H= Totals 16.23313 

## ===================================================================== *** End of Report

***~*** 

### Gcou:::ho 5/9/97 9:45:51 A."'l 

### BGE ?age _ c; ,.r--- 

## ' 

# = --2 - **-,--~---** _:;:; _,_-__

# .. _ 

### - -=--- 

## ===================================================================== Injec:io:: Da:9 Samp::..e

**Na~e** 

### A:::q. Ope::::-a:::::::::- 

### Seq-J.e:lce 

## ?:..:e Acq.

**Met~od** 

### 08-May-9"7, 22:.25

**7G42-~3** 

### ""l::. 

### BGE cc : '-''' 

### ..: F: \Z:PC::3M\ 2\

**S:C~U=:)JCE\** 04

## 9-:-:

**4:.~** _S 

### ANIGNS.M ·A.."l.alysis 

### Method F:
**\H?C:!EM\2\ME:':'E~2S\0497-24J:-** __ M Last 

### changed 5/9/97 9:37:29 P..M by BG:! 

### Seq. Li::1e 

## v:.al

Ir ..j 53 1 ll..nalysis of ar .

### .:..ons Ion by 

### Wac.e::-s .:;30 IC - PRP-xlOO 150x4 .1 

### column
mAU 175- 150-

**~** 125- T 

## "

**~** 

### .,. 100- N 75- 50- 25- 0 0 2 6 8 

## ===================================================================== Sor::ed By 

### Calib. Data

**Mod~=ied** 

### Multiplier Dilution Un:::alibrated Peaks **Ex~ernal Standa~d**  

### Report Signa: F::-iday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 

### not repo:::-ted Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhan:::ed integrator! RetTime Type Area Amt/Area Amount Grp Name [min] rnAU 

### *s [ng/ul]



## -- - - - - - I-- -- - - I-- -- - - - -- - I-- - --- - - -- I-- - - -- -- - - I-- I---- ---- - -- -- --- - - 2.472 VB 

### 1255.28821 1.50347e-2 18.87288 HF Totals 

### 18.87288 

## ===================================================================== ""*.,.. 

### End o: Report 

# .....

**~:::-oucho** 5/9/97 9:46:09 J:l..J.'1 

### BG!: Pag-e _ o: - ;-rw:::jec:.:..c·:-1 I:a':e 08-May-9'7, 22:37:48

**Seq.~:.:;.:=** .:..'.,· Sa:-r.p:..e Name 7C45-13 7:"11 Via:.. 59 r- P._cc. Ooe::-a:or BGE Ir:j 2 

### Seq,.le:'.ce File F: \ E?CHEM\2\SEQUENCE\0497- 24.'<. S

**Ac~. Me~~od**  **.~V:ONS.M**

**.~_-,alys** 

### is Mec:!lod F: \E?CHEM\2\METHODS\0497- 24A. M Las': c!-.a:'.ged 5/9

### I 9 7 9: 37: 2 9 Jl.M 

### by BGE A:la2.y·sis c: 

### ar.ior:..s Ion 

### by

**Wa:e~s** 430 

### :c - PR?-x:.oo l50x4 .1 

### co_'Jrr-::

**VW'::~** A Wave!engtn-280 nm (0497-24A\059-1002.0) mAU :1l 

### ""

150- 125- 100- 75- 50- 25-

0 

# :---~

___ ___,o'----------"2 _________ •=---------'6'---------"a _______ _.crr-,· 

## =====================================================================

**Exce~nal** 

### Standard

**Repo~t** 

## ===================================================================== Sorted By Calib.

**Da~a** 

### Modified Mul:i.p2..ier 

### Dilucion Signal Friday, May 09, 1997 9:36:42 A.t'VJ 

### 1.0000 1.0000 Uncalibrated Peaks noc reported Signal 1: VWD1 A, Wavelength:280 nm

Results obtained with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------1------1----------1----------1----------1--1------------------ 2.477

**v~** 

### 1250.34436 1.50342e-2 18.79795 HF Totals 18.79795 

### *** End of Reporc C-26 

### Page 1 cf 1 Gr-:Jucl:o 5 .' 9.· 97 9 : 4 6 : 2 6 ;.Jv'! BGH 

# 90/ -..,.:

- - - 

### Ir:jec::.i:J:: Date 

### 08-May-97, 22:5:036 Seq. L:.ne

**Samf~e** 

### Name

**7048-:~** 

### *ll 

### Ace.

**Ooe=ato~** BG2 S - • p·· F

**'--.,"--~"'· -~s~Qc--"c~\0'97**  

### 2"-A s

eqJ.ence 1...:..e : \n- -_r_.:...L·: \...::: \ .::. · !:...;." ..::. -:r. - _ • 

### !r:j ....

**Ac~ Me~~od**  **~~:ONS.M** .1\...-,a:..

### ys

**~** s Me

### :.hod F : \ :C:?CSEM\ 2

### \ME:T:l:J'JS\ 04 9 7- 2 4." .. M

- - 1-, • 5 

### I 9 '9- 0 3 7 2 c 'M b B"'-' 

### .!....las_ c..a::1gea. 1 1 _, : : _, r-..!. 

### y

**~...:r**...

**A.."1a2.ys~s** of 

### ar.ions Ion by Wa::e=s 430 IC - 

### PR?-xlOO

**150x~.l** colaiTL-: WV01 A. Wavelength=280 nm

**(0467-24A\06C-110~.D)** mAU



### ~
150- 125- 100- 75- 50- 25- /

0 0 2 6 8 

## ==============================================:====================== Exte=nal Standard

**Repo~c** 

## ========================================:============================

**so~:.ed** 

### By

**Cal~b.** 

### Data Modified Multiplie!:" 

### Di2.ution Uncalibrated Peaks Signal Fr:.day, May 09, 1997 9:36:42 A.t"l 

### 1.0000 1.0000 not: 

### reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integ=ator! RecTime Type Area Amt/A=ea Amount 

### Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.387 HF Totals 0.00000 1

**War~i~gs** 

### or Errors Warr.:.ng Calibrated compound(s) not found Groucho 5/9/97 

### 9:46:44 AM 3G2 C-27

# r·- '

## ' **=--~** 

# - ,::.=_::...::....·; .- --'·-·-·-· -/.t"". ---. 

## ... -:.-.

**========================================~=========================---**

**::::~:::::l::::: ::a::~**  08-May-97, 23:03:25

**Samp~e ~ame**  

### 7C4S-:4

**~::** rlca.

**Ooe~a~o~** 

### BGH

**secru.e:1~e** File F: \H?CHEM\2\SEQUENCE\049'7-24?.. S

**.:;.c~·. Me::~-::;d**  1-..N::JNS. M

**~-"lalys.:.** s 

### Method F: \!-::?C?.EM\2\ME:'rtCI::·S\04 97- 24A. M 

### Last c!"' ...a::ged 5 /9/97 9 : 3 7 : 2 9 .Z:U'\1 by

**3G~** 

### Seq. Li.::e 

### Vial

**T-,~** 

## -·· . 

### .: 6C 2

**?~a~ys~s** 

### of ar.ior.s Ion by

**Wa::~~s** 

### 430 IC - PRP-xlOO 15Cx4. l coluw.!"' ..

**\/V'v'lJ~** .;., Wavelength-280 nm

**(C497·24A\060·~** 102.0) mAL' lll 

## ,.,. 17=.-

**~50-** 125- 100- 75- 50- 25- 0 0 2 4 6 8

**Exte~r.al** 

### Standa=d Repo=t 

## =====================================================================

**So:-::~d** 

### 3y

**Signa~**

**ca:~~.** 

### 0ata Modified

**Mul::ipl~er** 

### Dilu:ion

**Unca~ibratad** 

### Peaks E'ricay, May 09, 1997 9:36:42 AM 1.0000 1.0000 not repo:-ted Signal 1: VWD1 A, Wavelength=280 nm

Results obtained with enhanced integrator! 

### Ret':'ime [min] 

# -------: 2.387 

### Tota:s **~tpe** 

### Area Amt/Area Amount Grp Name mAU 

### *s [ng/ul] 

# ------1----------1----------1----------1--l ------------------ HF 0.00000 Calibrated compound(s) not four.d

**G~cuc:hc** 5/9. 97 9:47:05 .Al'V!

**~Gr:** C-28 

### Page _ o: .:..

# Curve(s)/QA Point(s) Chromatograms**,-~**

# :::~ 

# 1 . C-29 

### ........:

# ~ ENTHALPYanalyt1cal. 1nc.**~a:.2.** :njec:.:..on Date 08-May-97, l8:34:C5 Samp::..e Name 5.162

**ug/rr~** Hr 

### Ace.

**One~ator** 

### BGE Se(iue:J.Ce 

### File F: \EPCEiEM\2\SEQUENCZ\0437 

### -24A. S Acq.

**Me~hod** ANIONS.M 

### ;:._,a'..ys:..s Method F: \H?CHEM\2\ME':'H:JuS\0437-24A.M T - • ""d 

## -/a I 9- , · 07 • 7 

### AM b 

### BG"

**~as_** 

### cna:1g-

**~ ~-**  

### ' _.:.: :.:. . y

**-~** Seq.

**L~r:e** 

## v:..a:

Ir:" l 1

**fl~alysis** 

## c: anions Ion by

**Wat:e~s** 

### 430 IC - ?R?-x'..OO l50x-±.l 

### cclurr.n
mAU 175- 150- 125- 100- 75- 50-

0-

0 VVV01 A, Wavelength=280 nm (0497-24A\051-0101 .D) '""' 

## "' '""'

\

2 4 6 8 

## ===================================================================== External Standard Report 

## =====================================================================

**So~t:ed** 

### By Calib. Data Modified Mult.iplier 

### D:.lut.ion

**Uncalib~ated** 

### Peaks Signal

**F~iday,** 

### May 09, 1997 9:36:42 AM 1.0000 1.0000 not reported Signal 1: VWD1 A, Wavelength=280 nm

Results obtained with enhanced

**integ~ator!** 

### RetTime Type Area

**Amt/A~ea** 

### Amount Grp Name [min] mAU *s [ng/ul]



## --- -- -- I- - ---- I-- -- -- - - -- I-- - --- ---- I-- - -- ----- I-- I---------- ----- -- - 2.398 PBA 513.70020 1.48616e-2 7.63441 HF Totals 7.63441 

## =====================================================================

***~~** 

### End of Report 

### *** Groucho 5/9..-97 11:18:31 AM BGH C-30 

### ?age 1 cf ::. 

# 9Y**:::~ec:.:.·::Jr-_** :0a:.e
**08-Ma::··-~7,** 18:46:53 Seq. 

### L:..::e Sam:;:le Name 5.162 ug/mL :S:F Vial :o-2.. 

### Acq. Ope=a:o= BGE Inj 2 Seq"-.1e:1ce Fi.l.e 

### F: \H?CEZM\2\SEQu-;;:NCE\0497- 24A. S

**A~~. Me~~od**  **~~:ONS.M** 

### _n,_,a:..ys ;_s Me':hod F: \H?CE:OM\ 2\ME':':iCDS\0497- 24A. M Last cl::a:1g-ed 5/9/97 :'..:!.:07:17 k"! 

### by BGH .n..na:ysis of a:::..or:s lor .. by Wat.ers 430

**~C** - PRP-xlOO 150x4 .1 cc:i..um.!1 WJD1 A. Wavelength-280 nm {0497-24A\051-01C2..D) mAU 175- 150- 125- 100- 75- 50- 25-

**~** 0-

0 2 6 

### a 

## ====================================================================: Sor-ceC. By 

### Calib. Data Modified Mul-ciplieo:- Diluti::Jn 

### Uncalibrated Peaks **Ex~ernal S~a~Card**  Report 

### Signal Friday, May 09, 1997 9:36:42

**k~** 

### 1.0000 1.0000 not repc:.-t:ed 

### Signal 1: VWDl A,

Results obtained Wavelength=280 nm with

**er~anced** 

### intego:-ator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul]


## ------ - I---- -- I------ --- - I---- ------ I---------- I-- I--------- --------- 2.392 PEA 411.50070 1.47888e-2 6.08562 HF Totals 6.08562 

## =====================================================================

****~** 

### End of Report G=oucl'w 

### 5/9/97 1:!.::.9:18 AM BG!': *** Page _ cf 

## o--' 

## /J

## - ( 

### =--2 -. - ,-r--.-- .

**~** -c:..-. '.

**~::-** - -:; - - . - 

## ===================================================================== Ir.j e:::..:.cr. Da:e 

### Samp2.e Name 

### _:;.cq. Ope:r-a::o.:- Seque:-tce F:.le

**_.;.::~.** 

### Me::I:od



### . **Jl~-:a.:..ys** :i.s 

### Me::hod

:..as:.

**c!-'.~.anged** 

### 09-Ma.y-97, 00:58:4'- Seq. 5. :..62 ugl:n.L H? 

### BGH F: \HPCHEM\2

**\SEQL~NCE\** 049--;- 24.:. .. S 

### AN:CONS.M

**F:\HPCHEM\2\ME~30DS\049--2~A.M** 

### 5

### I 9

### I 9

### 7 

### :2. :0

### 7 : 17 .l'J1 

### by BG2 **Li~e** V::..a2.

I :;.j 

### .1'-.r,a.lys:..s o: a.:c.ions Ion by Wate::-s 430 IC - PR?-x:..oo l50x4.::. cc:.·J.rrc:: mAU **VVVD~** A, Wavelength:280 nm (0497-24A\051-1601.D) 

### ,., 1': 175- 150 _.: 125- 100- 75-

**~** 50-

**~** 

### .,. 

### "' "' 25- 

## "' 

# -

"-. 0 0 2 **------'"-----------=------------'4"------------'5'----------'8'--------.....!!"~** 

## ===================================================================== Sorted By Calib. Data Modified Multiplier Dilution Uncalibrated Peaks Excernal

**S~anda=d** 

### Repo=t 

### Signal Friday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced

**integrator~** 

### RetTime Type Area AmtiArea Amount 

### Grp Name [min] mAU 

## *s [nglull



## - --- -- - I--- --- I-- - -- --- - - I-- -- - - - --- I-- - --- ---- I-- I---- --- - - -- -- -- --- 2.384 PBA 234.06892 1.45116e-2 3.39672 H? 

### Totals 3.39672 

## ===================================================================== *** 

### End of

**Repo~: ~~** * Groucl;.o 5/9/97 1::11:05 .A.M 3G2 

### of :..

### :..c..:.s.. **~ -~--~~~**  _:;::;- . **..../.!""----~**

**:!'.~ec:ci.8:-.** 

### Da:.e 09-Mc.y-S7, 02-:1::28 

### Samp2.e Name 5.162 

### ug/m:... E? 

### Aca.

**0De=~co= BG~**  

### Sec::Je::cce

**Fi~**

### e F: \E?CHEM\2\SEQl.i3NCE\ 04 9

### 7- 24A. 

### S

**A::~. Me::~oc**  **~~cONS.M** .2\...'l.a:':.ys:_s Me:.hod F: **\HPC:1EM\2\M=:~:-:ODS\0497-24F** .. M 

### Las:: cha:1gec 5/9/97 l1:07:l7 AM by BGE Seq. L:..:1e 

## v:.a:

:::j • r .l..o 5:.

2

**A..-.a~ys:;.s** o:: ar_ior.s :lor.. by Wa:.ers 430 IC - **PR?-x~OO** l5Cx4.l colu:-r.:1 VWD1 A. Wave!ength=280 nm (0497-24A\051-16C2. J,l mAU 175- 150- 125- 100- 75- 50- 25-

0 2 4 6 6

**Ex:erna~** 

### sca:1dard Repo=c **~==~===~===============~============~====~===========================** 

### Sor:ed By Calib Da:a Modified

**Mul~iplier** 

### Dilu::ion Uncalibra:ed Peaks Sigr.a.l 

### Friday, May 09, 1997 9:36:42

**~.M** 

### 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced **i~tegrator!** 

### RetTime Type Area Amt/A=ea Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------1--l------------------ 2.387 PBA 241.46312 1.45313e-2 3.50877 HF Tota:!.s 3.50877 **=~===================================================================** 

### *** End of 

### Reporc G:r-oucho 5/9/91 1l.: 2.::.: 23 Al"'1 BGH C-33 ?age _ 

## o: - m::,.·· I:--.j e..::.2.::n:

**~a::e** 

### SaiT.F:..e Naiile Ace_. Ope::a::o:: 

### Seque:1ce Fi:!..e Acq. 

### Method .:.

... 1a:l.ys:.s Met:.

### hod

...

**~~-** ......

**-..,~** .... ,-...=.;:l LIO..::. '-

**\,..J.J.C..-.~** _.._... 08-May-97, 18:59:42 Sec;:. 10.13 

### ug/mL EF 

### BGE F:\HPCHEM\2\SEQUENCE\0497-24A.S JI.NIONS. M " \··oc··"M' 21

**M-~·Jor-\04~-** 

### 24A M

- : n_ :i.... . \ \ !!. ....

**~** .....:;:; • _, l - - .• 5/9/97 l:..:C.... :::.""! AM by 3GE L:.:1e 

## v:.a::.. 2
J...na2.ysis of anions Ion 

### by Waters 430 :::::: - PR:?-x100 150x4 .1 colurrc:. VWD1 A, Wavetength=280 nm (0497-24A\052-D201.D) mAU 17:::- 150- 125- !; 

### ,. N 100- 

### ,. N 75- 50- 25-



# ·---------- 0- 

## " i 0 2 4 6 

### Ex::ernal Scandard Reporc Sorted By Signal Cali=. 

### Data Modified Multiplie:: Friday, May 09, 1997 9:36:42 JI.M 1.0000 

### D:...lu:ion Uncalibrated Peaks Signal l: VWD1 A,

Results obtained 1.0000 not reporced Wavelength=280 nm with

**er~anced** 

### integrator!

**Re::T~me** 

### Type Area Arnt/Area Arnoun:: 

### Grp Name [min] rnAU 

### *s [ng/ul] 8



# -------l------l----------l----------l----------l--l------------------ 2.424 PBA 833.04645 1.49739e-2 12.47398 HF Totals 12.47398

**~~~==~===============================================================** 

### *** End of Report 

### *** Grouc::-- ..o 5/9/97 1.:..:19:42 Jl.Jvl 3GH C-3-l 

### Page _ c: :./ 

### - - - = 

## ---= _::....:..'. - ._._-..____ '..;..;:':::: ---------

**'~** 

## -- ... c:.-. 

### Samp:.e Name _:;.cc. Ooera:.or 

### secru.enCe ?:.le 

### Ace. Mec!"10d

. A ..**ncl~ys** 

### :.s 

### Me:.hod 

### 08-May-97, 19:12:34 

## :.o. 13 ug/rr.L E? 

### BGH F: \H?CHEM\2\S2QlJENCE\0497-24.Z\.. S ANIONS.M

- \H:oc··-M·.

**2\M-,..:.r~"-'** 

### 04°- -" M .t' : ·- !"' • .:.•• \ .!:.. - ••UJ.....;:::, \ • _, ! - L. '%i-l... Las-: cl-.a:1ged 5/9/97 1:.. : 0"7 : l '7 k'V! by BG:E 

### Sec;:. L:..ne 2 'Ji 

## a:

Inl 2

**-~-::.a2.ysis** of 

### anior.s Ion by

**Wa~e::-s** 43C IC - PR?-x::.oo l50x4.l 

### c:::lumr. VWDi A, Wavelengtn=280 nm (0497-24A\C52-C202.Q) mAU 

## iii 175- 150- 

## "' 125- "- 100- :I: 

### "'

**~** 75- N 50- 25-

0 

# ........----

0 2 4 6 8

**Externa~** 

### Scanda=d Report 

## ===================================================================== So!:ted By Calib. Data Modified Mult.iplie::- 

### Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42

**k~** 

### 1.0000 l.

### 0000 not repo!:ted Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------1------1----------1 ----------l-·--------l--l------------------ 2.419 PBA 766.99170 l.49584e-2 11.47294 HF Totals 11.47294 

## =====================================================================

***~*** 

### End of 

### Report

 ~**  

### Groucho 5/9/97 11:20:06 JI.M 

### BGE C-35 

### Page 1 

### o: :. rrw

### I:--.jec::2..or: :)a-=e 09-May··-97 I 0::24: 

## :s Sample Name 10.13 us/mL EF 

### Acq.

**Cpe~ato~** 

### BGE Sequence Fi:!.e F: \Hl?C!':i::M\2\SEQUENC:0:\0497-24i' .. S Acq. Methoc ANIONS.M ALa:ysis Method
**F:\HPCHEM\2\M:O:~HODS\0497-24A.M** Las:. cha:1ged 5/9/91 ll:07:l7 &"1 by 3G2 

### Seq. I..::.:1e 

### V:.a...:...

Ir:J

**i'~calysis** 

### o: anions Ion by

**Wate~s** 

### 430

**~C** 

### - PRP-x:oo 150x4 .1 colum."":. mAU 175- 150- 125- 100- 75- 50- 25 -

D 0 **VWO~** A_ Waveiengtli-280 nm (0497-24A\052-i 701.0) 

## "' l'l

"- I :g 

### .,. N

2 4 6 8 

## ===================================================================== Ex=ernal

**Standa~d** 

### Repo=t 

## =====================================================================

**Sor~ed** By 

### Ca:ib. Data Modified 

### Mul:.ipli.er Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 not reported Signal 1: VWD1 A, Wavelength=280 nm

Results obtained with enhanced

**integ~ator!** 

### RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.406

**v~A** 

### 589.25447 1.48992e-2 8.77956 HF Totals 8.77956

**~*~** End of Report 

### *** G::-oucjo 5/9/97 12.:11:41 P..L'\1 BG;.{ 

### C-36 ?age - cf

**~** 

# /1/Z)**:1:.:--.~ec:::.:Jn** 0ace 09-May-97, 01:3/:C:.

**Sam;:~e** Name 

### :.c .13 uc/m:..

**H~** 

### Acq.

**Oper~~o~** 

### BGE 

### Seque::1ce File F: \HPCHEM\2\SEQl.JENCE\ 0497- 24_2:._. S Acq. Method ANIONS.M

**~alysis** 

### Me:chod F:\E:?CHEM,2\METHODS\049"7-24A.M Last: cha::ged 5/9/97 11:07::.7

**-~by** BGr. 

### Seq. L:..::.e

**·~J.:.a::.**

Ir.J **~-** 52

2 

### Analysis cf

**a~io~s** 

### Ion by Waters 430 IC - PR:?-x100 lSOx4 .1 eelurn_.,..,.
mAU 175

**~** 150- 125- 100- 75- 50- 25-VWOi A, Wavelength-280 nm (049/.24A\052-i702.0) ill 

### '"'

0 v N


### o-:-----

0 2 4 5 

# '" 0 

## "'

8 

## ===================================================================== External Standa=d

**Repo=~** 

## ===================================================================== Sort:ed By Calib. Dat:a Modified Mult:iplier Dilution 

### Uncalibrated Peaks Signal 

### Friday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 not reported Signal 1: VWD1 A, Wavelength=280 nm

Results obtained with enhanced integrator! RetTime Type Area Amt/Area Amount 

### Grp Name [min] mAU

**~s** 

### [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.401 VBA 585.75067 1.48977e-2 8.72631 HF Totals 8.72631 

## ===================================================================== ***

**E~d** 

### of Report

***~~**

**G!""O'-.J.C~O** 5/ 9; 

### 11:11:59 AM BGE C-37 

### Page 1 

## c: :_ 

# /Ol,- 

### Ir.j ec:.:.::r.:. Da::e 

### Sample Name 

### .::..cq. Ope::-a:.or

**Se~.J.ence** 

### F:!..2.e

**-~cq** ·. Met:.hoC. 

### .::: ...alys:.s Me:.hod 

### Las:: c::.ar..ged ..__,___

## ---- - --- . '..!::: __;; - ·,_. .;)

**·~** - -- 02-Mav-SI, 19:25:25 Seq.

**~i::-.e** l9. 50.. 

## ug 1m.I. HF 

## v:.a.: BGE

**~~j** 

### F:

**\H?CH~M\** 

### 2

**\S2Q\JENC~\**

### 0497- 

### 24A. S ANIONS.M

-
**\~cor---M'** 2·· M--"'00" 1 

### 0'

**c~** 2'' M t' : n

_ _ ::..::.. \ \ L •.::. • ;J. ...., ·, ""= _., i - -:r- .• . 

### 5/9/97 1:!.:07:17 AM 

### jy BG2 53 1 

### A..:.:..a::..ys:.s c: a!" ..:.:Jr:s .=on by 

### wa:e:rs 43C :c - P?.?-x:oo 

### 2.50x4.:

**c:::l~rr.r.** mAU 175- 150- 125- iOC-

?S50- 25- 0 0 VVVDi .A.. Wavelength-280 nm
**(0497-24A\053-030~** .D) 0>• 0> n_;

2 4 

### Ex:.ernal Standard Report 6 8 

## ===================================================================== Sor::ed By Calib. Data

**Mod~fied** 

### Mul::ipl:'..er !J i l ',.l':.

### ion Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 

### 1.0000 1.0000 not reported Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integra:or! RetTime Type Area Amt/Area Amount Grp Name [min] mAU 

### *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.464 VBA 1325.48840 1.50410e-2 19.93673 HF Totals 19.93673 

## ===================================================================== *** End of Report

 ~**  Groucho 5 '='' 97 11: C9: 23 AJ-1 3GZ.: C-38 ?age 

## c: ' 

## /0;)..·. 

## .. =--'== - **::~r-~:;~.r ~**  

### '--- 

## ----·.

**'~** 

## =====================================================================

**:r...je::-:.:..~n** 

### Da:.e Samp=..e Name

**Ac~. Ope~a..~c::­**  

### Seque!lce Fi::.e Acq.

**Me~hod** Analysis Method

**~as':** 

### changed OE-May-97, 13:38:::.6 Seq. l9. 50 

### ug/mL F.F 

### BGE F: \HPCEEM\2\SEQlJENCE\0497-24A. S AN:ONS.M F: \EPCHEM\2\ME':':"'!ODS\0497- 24."'-. M 5/9/97 11:07:17 A.M. by BG2 L:.::e 

### v:..a::..

I:::j 3 53

2

**.~** 

### ..a:ys:.s c: ar:ions Ion by

**Wate~s** 43C 

### IC - PF.P-x:.OC l5Cx4 .l c::;. .l·.J.rnr: \fiNO; A. Wavelength-280 nm (0497-24A\053-03C2.D) mAU



### ~ 175- 150- "- r 

### "' 

## "' 125- 

### .,. N 

# I 100- I •' 75- 50- 25-

0 0 2 4 6 8 

### .., 

## "' .,. 

## "'



## ===================================================================== Excernal

**sc~~dard** 

### Report 

## ===================================================================== Sorced 

### By Calib. Data Modified Multiplie:::.- Dilution 

### Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 

### not reported Signal 1: VWDl A,

Results obtained Wavelength=280 nm with enhanced integrator' RetTime Type Area Amt/Area Amount 

### Grp Name [min] m.ZI.U *s [ng/ul]

**-------l------l----------l----------l~---------1--l** 

# ------------------ 2.458 VBA 1321.37598 1.50407e-2 19.87441 HF 

### Totals 19.87441 

## ===================================================================== *** 

### End of Report **T 

### G:::-cu::;,.o 5/9/97 11:C9:41 Al<l BGH C-39 

### Page 1 or · 

# /0.3I" **!n:ec~io~** Dace 09-May-97, 01:49:52 Seq. 

### Line 

### Sample Name :'.9.50 u;/mL H?

**-~Jia.::..** 

### Ace.

**Opera~or** 

### BGH Sequence File F:\HPCHEM\2\S3QuENCE\0497-24A.S **I!".~** 

### Acq.

**Me~hod** 

### ANIONS.M A.""lalysis Method F:\HPCHEM\2\METH0DS\0497-24A.M Las: changed 5/9/97 11:07:17

**A.~** 

### by BGH .A.n.a.::..ysis 

### of anions Ion by Wace!:"s 430 IC - 

### PRP-x:oo 15Ox4. 2. 

### eelurnn mAU 175- 150- 125- 100- 75-

**50~** 25-**\fiNO~** A Waveiength-260 nm
**(0497-24A\053-180~** _Q) 

## "'' "' "'
!!: 

## "' 

# .. .. N

0 ·,!i I 

### >---~~------~----------------~/~--------~------ 0 2 4 6 8 

## ===================================================================== External Standard Report 

## ===================================================================== Sorted By ca:ib. Data Modified Multiplier Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AI-1 1.0000 1.0000 not reported Signal 1: VWDl A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------1--l------------------ 2.449 VBA 1261.49463 1.50353e-2 18.96693 HF Totals 18.96693 

## =====================================================================

***~*** 

### End of Report

 ~**  

### Grouc:w 5/9/97 11:12:17 AN BGE C-40 Page l c: 

# /cYl

### =--e: - ,.., ' 

## --

**~** ' 

### - ' 

### ·- "": :: 

## - ..:. -:::..... _ ,--,--

**--~-**

**~::...:--~** ..... .:. ·-'

**:::::r.~ec-.:2.:)::** Da::e 09-May-97, 02:C2:39 

### Seq. 18 Sam:;:le Na.:ne l9. 50 ug/mL H? 

### v:..al 53 

### Acq.

**Ope~a~or** 

### BGH 2 

### Seq-..1ence File F:\HPCHEM\2\SEQU2NC3\0497-24A.S Acq.

**Me~hod** 

### ANIONS.M A.:l.alysis

**Me~hod** 

### F: \HPClEM\2\METHODS\ 0497-24.:. ..M

**Las~** 

### cha::1ged 5/9/97 11:07: l7 AM by BGE Analysis o: anions Ion by

**Wa~e~s** 

### 430 IC - PR?-xlOO 150x4.1

**co:u~'** mAU

, 75- 

### : 150- 125- 100- 75 _: 50- 25-

0 0**VVV'J~** A. Wavelength 280 nm {0497-24A\053-1802.0)

'Ic' 0 

### .,.

2 "- :I: 

## "' "' .,. N

4 6 8 c a. 

### .,. 

## "'



## ===================================================================== Sor:.ed By 

### Calib. Data Modified Multiplie!."" 

### Dilution Uncalibrated Peaks **Ex~ernal** 

### Standard

**Repo=~** 

### Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not repon:ed Signal 1: VWD1 A,

Results obtained Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amount Grp Name [min] mAU *s [ng/ul] 

# -------1------1----------1----------1----------1--1------------------ 2.453

**v~A** 

### 1272.74597 1.50363e-2 19.13744 HF Totals 19.13744 

## =:=================================================================== *** End o: Report *** 3:coucho 5/9/97 11:12:35 AM BGH C-41 

### Page 1 

# o= 1( 2::-:jec=:i.or: Da:.e 08-May-9'7, 19:5::06 Sarrr;:=.e Name 34.34 ug/mL HF 

### Ace.

**Ooe~~to~** 

### BGH

**Seque~ce** 

### 2ile F:\H?CH3M\2\SEQUENCE\0497-24A.S Acq. Method ANIONS.M Analysis Met!:lod F:\H?CH3M\2\ME'CHODS\0497-24A.M Last changed 5/9/97 l1:07:17 AM by BGH ,:,eq.

**v:..a~** -

**~** . 

## - - 63

l

**?~alysis** 

### of anions Ion by

**Wate~s** 

### 430

**~C** 

### - PRP-xlOO l50x4.l col:unr. mAU 175- 150-


### - 125

**~**



# - 100- 75- 50- 25-



### o0W..JD1 A. Wavelength-280 nm

**(0497-24A\06~401.0)** 

# "'

**~**

' ';

/ \ 2 4 6 6 

## =====================================================================

**Exte~nal** 

### Standa=d Repo=t 

## ===================================================================== Sorted By Calib. Data Modified Multiplier Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42 AM 1.0000 1.0000 not reported Signal 1: VWD1 A, wavelength=280 nm

Results obtained with enhanced integrator! RetTime Type Area

**Amt/A~ea** 

### Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------1--l------------------ 2.525 BBA 2360.42920 1.50908e-2 35.62084 HF Totals 35.62084 

## ===================================================================== *** End of Report *** -



### Groucho 5/9/97 11:10:00 Al'J! BGH C-42 

### Page - cf :.. 

# ;ob=:__e --

**:::~e:::.:..c.:--~** ::a::e 08-Mav-97, 20:C3:52

**Sam~:e** Name 34.34-ug/mL HF Acq.

**Ope~a~o~** BGE Sequence F:.le F: \HPCHEM\2\SE:Ql.J"ENCE\ 0497-24JI .. S Acq.

**Me~hod** AN:ONS.M .1\.nalys:.s Met.hod F: \HPCHEM\2\M2'C'HODS\0497-24.:0,..M Last changed 5/9/97 .l.l:07:17 AM by BGE 

### Sea. Line V "' -l

-"-- l!lJ 4 55

2 

### A.:.-::.a2.ysis o: a::ions Ion by 

### Wate:::-s 430 IC - PRP-xlOO l50x4 _ 1 colu!'n.i..J.
mAU VVVD1 A. Vvavelength-280 nm (049i·24A\065-04C2.0) 

## "' 175- 150- 125- 100- 75-5C25-

0-'--.----

0

Sor:ed By ;;:



### "' N 

## "'
2 Ext.ernal Standard Report Signal 6

Cal:.b. Data Modi:ied 

### Multiplier Friday, May 09, .l997 9:36:42

**Jl~** 1.0000 Dilut.ion Uncalibra=ed Peaks 1.0000 not repo:::-ted Signal 1: VWD1 A, Wavelength;280 nm

Results obtained wit.h enhanced int.egrator! Ret.Time Type Area Amt/Area Amount Grp Name [min] mAU 

### *s [ng/ul] 8 ·a> ·a>



## "'



# -------l------l----------l----------l----------1--l------------------ 2.529 VBA 2318.62378 1.5089/e-2 34.98729 HF Tota::.s 34.98729 

## ===================================================================== *** End of Report 

### ***

**Groc:::~-:o** 5/9:97 11:::.0:17

**-~~** 3GH C--13 Page 

# /07/ ?:....:.e ?:

**:::j9ct2.~~** Da-:e 09-May-9"7, 02:2.5:25

**~c.** r..:..::.e :..9 

### Sample Name 34.34 ug/mL HF v::.a:. 6S Ace.

**Ooe~ato~** 

### BGE Inj 1 

### Seciuence FEe F: \EPCHE:M\2\SEQuENCE\0497-24.Z1 .. S Acq. Method ANIONS.M

**A!".~.al**vsi.s Met.hod F: \li?CHEM\2\ME':'SODS\0497-24A. M 

### Las::· changed 5/9/97 11:07:17 AM by BGH Ana'-ys:'..s of anions Ion by Wate:r-s 430 IC - PR?-x:.oo 150x4.1 ca:.'-'ITL": \1\NOi A. WaiJelength-280 nm
**(0497-24A\065-~** 901.0) mAU



### ~ 175--= !j: ' 150 _: N N 

## "' N 125- ,\ II 100

**~** 75- 50- 25 _;

0 0 2 4 6 8 

### Extecnal Standard Repor:: **====================================================================~** 

### Sorted By Calib. Data Modified Multiplier Dilution Uncalibrated Peaks Signal Friday, May 09, 1997 9:36:42

**k~** 

### 1.0000 1.0000 

### not reported 

### Signal 1: VWD1 A, Wavelength;280 nm

Results obtained with enhanced integrator! RetTime Type Area Amt/A:r-ea Amount Grp Name [min] mAU *s [ng/ul] 

# -------l------l----------l----------l----------l--l------------------ 2.522 VBA 2200.03882 1.50862e-2 33.19019 HF Totals 33.19019
**==~=========================================================~========** 

## *** End of Report 

### *** Gco'-Ocho 5/9/97 '-'-: l2: 53 Al'-1 

### BGH C--1-l 

### Page _ 

## c:: :.. 

# ;oY-..."' ,--,....- \.._..,4-- ---- 

### -

**-.~---.--** .,;,.-;:'':;! _,_____ -. '-,.:.: -L-_

**I~~ec~io~ ~a:e**  09-May-97, 02:22:13 Sample Name 34.34 ug/mL HF 

### Acq. Oneracor BGE Sequ.ence F:'..le F: \H:?C5EM\2\SEQuENCE\0497-24A. S Acq. Method AN=ONS.M ·A..'lalys:._s Method F: \HPCHEM\2\ME':'HODS\0497-24A.M

Lase= changed 5/9/97 ll: 07:17 .1'.1'1 

### by BGE **Se~.** 

### V:._a:. :Cnj 1'0' 65

2

**-~.alys~s** of

**a~ions** Icn 

### by

**Wate~s** 430 IC - PR?-xlOO 

### 150x4.l co2_uiTL-: mAU **VWD~** A. Wavelength-280 nm (049i-24A\065-1902.:J) 0 ;;

, 15- 150- 125- 100- 75- 50- 25-



### o-

____ _ 0


### Sorced Ey 2 

## "' N 

## "' N 

# '

4 

### External Standard Report Signal 6



### Calib. Data Modified Multiplier Friday, May 09, 1997 9:36:42 AM 1.0000 Dilution Uncalibrated Peaks Signal 1: VWD1 A,

Results obtained 1.0000 not reported Wavelength=280 nm with enhanced integrator! RetTime Type Area Amt/Area Amounc Grp Name [min] mAU Ts [ng/ul] **--~--** 

### e



# -------1------1----------1 ----------l----------l--l------------------ 2.526 VBA 2209.78418 1.50865e-2 33.33787 HF Totals 33.33787
**;;;;:==~=======;==============================;================;=====** 

### *** End of 

### Report T** Groucho 5/9/97 ll: :3: ll fu"'1 BGH C--15 

### Page _ ,__APPE:"iDIX D
PRODUCTION DATA

D-1

### P.O. Box 1027 • Sanford, North Carolina 27331-1027 TOLL FREE (NC, SC, VA) 1-800-672-7559 • 

### April 25, 1997 Trigon Engineering Attn: Mr. Robert F. Callahan 6200 Harris Technology Blvd. Charlotte, N.C. 28269 Re: Your Letter April 23, 1997 Stack Testing. Dear Sir; FRANK G. PERRY, SR. Pres1dent J.R. HOLTON Secretary/Treasurer CJ 

### • Telephone: (919) 774-4800

Facsimile: 919-774-7557



### As you requested the production for kiln 2 on the day of stack test and all other times is as follows: Green Brick (unfired) 89,136 x 5 lbs. 

## = 445,680 lb- 2,000 

## = 222.84 tons. Fired bric% 89,136 x 4 lbs 

## = 356,544 lbs - 2,000 

## = 187.27 tons. If any other documentation is required please advise either myself or Bobby McCoy.



# y~ Holton S cr tary and Treasure JRH: 

### jn



# r



# s

**6it5~-o** 

# C>J A

# 2

# i !leo.-e 

# If, -/J{)

# o

D-2 

# Ill**APPE~DIXE** 

### CALIBRATION DATA

E-1



# .jlb ..

### QUALITY ASSURANCE AND EQUIPMENT CALIBRATION PROCEDURES 

### General. Each item offield or laboratory test equipmentpurchased or fabricated by Trigon EngineeringConsultantsis assigneda unique, permanentidentificationnumber. New items for which calibration is required are calibrated before initial field use. Equipment whose calibration status may change with use or with time is inspected in the field before testing begins, and again upon return from each field use. When an item of equipment is found to be out of calibration, it is adjusted and recalibrated or retired from service. All equipment is periodically recalibrated in full, regardless of the outcome of these regular inspections. Calibrations are conducted in accordance with United States Environmental Protection Agency (US EPA) specifications. Trigonfollows thecalibrationproceduresoutlinedin EPA Reference Methods found in the Code of Federal Regulations (Volume 40, Part 60) and those recommended in the Quality Assurance Handbook for Air Pollution Measurement Systems: Volume III (EPN600/R-94/038c). When the Reference Methods do not detail procedures, Trigon uses methods such as those prescribed by the American Society for Testing and Materials (ASTM). Data obtained during calibrations are recorded on standardized forms, which are verified for completeness and accuracy by the Quality Assurance Manager. Data reduction and subsequentcalculationsare performedusingTrigon'sAir QualityData System. Calibration calculations are performed by an environmental scientist, independently audited by the Project Manager, and reviewed by the Quality Assurance Managerfor verification ofdata. Copies of calibration data are included in each test or project report. Inspection and Maintenance. An 

### effective preventative maintenance program is necessary to ensure equipment performance quality prior to, during, and following every test. Each item of equipment returning from the field is inspected before it is returned to storage. During the course of these inspections, items are cleaned, repaired, reconditioned, and recalibrated when necessary. Each item of equipment transported to the field for a test project 

### is inspected again prior to being packed. Trigon performs these quality assurance checks prior to departure for the project site to detect equipment problems which may occur during periods of storage. Trigon transports adequate back-up equipment to each project so as to avoid any unforeseen circumstances. Calibration. Source sampling equipment that require calibration include nozzles, pitot tubes, thermometers, flow meters, dry gas meters, and barometers. The following sections detail the calibration procedures followed by Trigon for each item.

E-2

### Nozzles. Each probe nozzle is uniquely andpermanently identified at the time ofpurchase or fabrication, and it is calibrated before initial field use and prior to each test. The inside diameter of the nozzle is measured to the nearest 

### 0.001 inch using a digital micrometer. Three measurements are made using different diameters each time. If 

### the difference between the high and the low measurements do not exceed 

### 0.004 inch, the average of the three measurements is used. If 

### the difference exceeds this amount, or when the nozzle becomes nicked, dented, or corroded, the nozzle is reshaped, sharpened, and recalibrated. Regardless of usage, all nozzles are inspected and recalibrated on a yearly basis. Pitot Tubes. All Type Spitot tubes are constructed and calibrated in strict accordance with the procedures contained in EPA Reference Method 

### 2. A Type S pitot tube will have a coefficient of

### 0.84 ::!::0.02. A standardpitot tube will have a coefficient of

### 0.99. Each pitot tube is visually inspected prior to any field use. If 

### the inspection indicates damage, it is recalibrated. Regardless ofusage, all pitot tubes are inspected and recalibrated on a yearly basis. Drv Gas Meter and Orifice. Each metering system receives a full calibration at the time ofpurchase and annually, thereafter. Post-testcalibrations are performed aftereach source test. If

### the calibration factor, y 

### (gamma), deviates by less than five percent from the initial value, the·test data are acceptable. Ify 

### deviates by more than five percent, the meter is 

### recalibrated and the meter coefficient (initial or recalibrated) thatyields the lowest sample volume for the test runs is used. Standard practice at Trigon is to recalibrate the dry gas meter anytime y 

### is found to be outside the range of 

### 0.98

**~** 

### y 

### < 

### 1.02. Barometer. Each field barometer is calibrated to agree within 

## ± 0.1 inches Hg of a reference mercury barometer. The barometric pressure is corrected for pressure and temperature. Prior to and following each field test the field barometer is verified. Thermometers. Each new thermometer, pyrometer and thermocouple purchased or fabricated by Trigon is calibrated in strict accordance with US EPA Protocol. Calibration tolerance limits are as follow: Impinger Temperature Gauge Dry Gas Meter Temperature Gauge Stack Thermocouples 

### ::!:l°C or 

### 2°F ::!:3°C or 

### 5.4°F 

### ::!:: 1.5% of absolute temperature All thermometers and thermocouples are inspected and calibrated prior to and following each field test. Regardlessofusage, all thermometersand thermocouples are inspected and recalibrated on a yearly basis. Laboratorv Equipment. Trigon Engineering Consultants has a written quality assurance document that covers calibration and maintenance oflaboratory equipment. This includes calibration ofeach analytical balance againstClass Sweights. Calibration ofthermometers, barometers, and wet test meters are traceable to NIST. A copy of our quality assurance document may be obtained by written request.
E-3

### PRETEST - POSTEST C.-\LIBR.-\TION OAT.-\ FOR.\!

**Client_~·~·-~~r_-~>-~~·------------** 

### City;State __ _;_(.;:-::-:-'.

**~:o....::,.;,.;:; -~';;:.'** ----;.___:_''v.:::..c 1 _:C::______ _ 

### Pretest Date '-' 1 ·' 1' ' 

### Calibrator

**--"'0;..:(:...-~<**__ 

### Postest Date



### o~ 

## (2-1/,; 7 

### Calibrator .-;;;-- -:;·I' 

### Referenee Thermometer ____ .._10"'0"'."'0"'2"'2'----- Reference Barometer ____ **6!£0"-!0cL·!L00~3L..**

### ___ _ Pretest Postest Temoernture. "F Ret: Temn. "F Temoernture. "F Ret: Temn. "F Omega Red Team DB!WB #100.025 

### I Omeoa Green Team DB/WB #100.031 Omega Blue Team DB!WB #100.017 c.<;-

## It- 7 6"'; /tc; 

### ! 

# c;r, //<i ,; (,

**~(';** Omega Gold Team DB!WB #100.032 

### '"f·h 7

**;,:~!/~** 

### 0! /:,;, /_,3/ ',: _3 Omega Grev Team DB!WB #100.033 Omeoa CEM DBM'B #100.026 Drv Gas Meter Inlet/Outlet #300.035 0 3 /< 3 {: lt!:i. t.;. 

### 1/_, I 

## G3 Drv Gas Meter Inlet/Outlet #300.045 

## I I Drv Gas \leter Inlet/Outlet #300.067 Drv Gas Meter Inlet/Outlet #300.100 t;l/(,1 

## c; )../{). i 

### . '/'I l,) I \.J , 

### (,3 Drv Gas Meter Inlet/Outlet #300.200

**/.)/~l** 1- J. /£}. 

### I l,oZ./ul 

### 1-3 

### I Drv Gas \leter Inlet/Outlet #300.2I4

**~I** /£I t. 1 /.:. -2. 

### I I,Z./·cZ- (, 1 

### I Drv Gas \leter Inlet/Outlet #300.241 Drv Gas Meter Inlet/Outlet #300.248

**t.~l/5 ~**  l

**/~** l 

### I v31G3 

### &3 Drv Gas Meter Inlet/Outlet #300. 

## I Drv Gas Meter Inlet/Outlet #300. Umbilical Adaotor # f #300. Ci..Jr.J ( l !'?. 

### l,l- 

### G3 Umbilical Adanror # 7 #300. I ZJ 

### ' ) I.- 

### /) iJZ.. 

## 03 Umbilical Adaoror # "' #300. I 

### 5

**~-** (,). 

### tJ. t,

**~ ~]'**  Umbilical Adaotor #

**~** #300.

**~** c I 

### (, J 

### t. ' '· 3 

### {,< Umbilical Adaotor # 1C#300. (4 

## ,:;;, G,7., (. '3 Umbilical Adantor # !\ #300. ). I I.

**t;~** I 

### 5 

# - (;I. 

### 1..3 

## I Probe #200. Co7 

### "' 3 /_ <:' 

### &I f., j Probe #200. ("<")

**~** 

## o. I 

### < &1 (;) Probe #200. OO'i 

### (.. 3 

### .: 3 

### 1.:2-- 

## &3 Probe #200. 0 'l :;l &. 

### i

**~3** t 1 ::?- 

### (.;'3 Probe #200. 

# ,., .\ '{ 

### t ' ,;. 

### 3 

### &7 VI Probe #200. Pitot #200.

**"~** 

### e <C: G l 

### {,<

**c.;~** 

### fo 3 Pitot #200. f') ,. 1./ 

## (,. 3 

## (. 3 (..."). 

### (,3
Field Baro in. HI> Ref. Baro ln. H• Field Baro in.Ho· Ref.Baro in. H2 Barometer Red Team #600.00\ Barometer Green Team #600.0!4 Barometer Blue Team #600.010



# '~·"' ).

**~** 

### .. v·

**z.~.** 50 Z..i.J5 Barometer Gold Team #600.02](0\ l s. 3 '.. , I .!'1' 

### ::;,z

**;;.~'.** 

### :: . ) 

## . Barometer CEM #600.02010) 

### Were all postest calibrations within the specified EPA Quality Assurance criteria? z'Yes D 

### No
E-4 

# !15'

### PRETEST- POSTEST C.-\LIBRATIOC'i DATA FOR.\!
/ . \ 

### Cll 

### .ent ' - ·-' .'-"

**.~** .ir - **--~~-~~-~-~~---~-~-~-·~·~-~·---------------** 

### Pretest Date '"'-"' /' ' ' Calibrator .J

## J!

**-~--** 

### Postest Date C't/J1 

## /'ti Calibrator JJ I

**-J~·'** 

### Reference Thermometer _______ _.1-'"0-'"0'-'. 0"'2"'2'------- Reference Barometer ________ **6~0"-!0"-.'"00~3._**

### ____ _ Pretest Postest 

### I Temoerature "F Ref. Temn_ "F Temperature. "F Ref. Temn. "F Omeoa Red Team DB/WB #100.025 I Omega Green Team DB/WB #100.031 

### I I Omeoa Blue Team DB!WB #100.0!i Ome.a Gold Team DB!WB #100.032 Omega Grev Team DB!WB #100.033 

## I Ome•a CEM DB!WB #100.026 Drv Gas \feter Inlet/Outlet #300.035 

### I Drv Gas Meter Inlet/Outlet #300.045 Drv Gas Meter Inlet/Outlet #300.0/ii 

### ! 

### I Drv Gas Meter Inlet/Outlet #300.100 

## I I I Drv Gas Meter Inlet/Outlet #300.200 

### I I Drv Gas Meter lnlet/Outlet #300.214 

## I Drv Gas \!eter lnlet/Outlet #300.241 

## I Drv Gas Meter Inlet/Outlet #300.248 

### I 

### I Drv Gas Meter Inlet/Outlet #300. 

### I Drv Gas Meter Inlet/Outlet #300. 

### I Umbilical Adaptor# 1). #300. -"111

**~.,**

**~ ~-**  

### {,;i., 

## h

**~** Umbilical Adaptor # 1 3 #300. :)..{.. 4 ') (, 5

## - 63 c; 5 Umbilical Adaotor # #300. Umbilical Adaotor # #300. Umbilical Adaptor # #300. L:mbilical Adantor # #300. 

### I I Probe #200. =')

**~~**

**~""** 

### &1 (,) Probe #200. 

### c ' r, 

# n (.

**~** 

### l/1 L.· 3 Probe #200. (') ' 7 (,4

**~** 3 !;L 

### v3 Probe #200. Probe #200. Probe #200. Pitot #200. Pitot #200.
Field Baro in. H.,. Ref. Baro in. Ho Field Baro in.Ho Ref. Baro in• Ho Barometer Red Team #600.001 Barometer Green Team #600.014 Barometer Blue Team #600.010 Barometer Gold Team #600.0211 D\ Barometer CEM #600.020(0) ( 

### Were all postest calibrations within the specified EPA Quality Assurance criteria? 1<1 

### Yes a No
E-5

### ISOKINETIC CON'TROL CONSOLE CALIBRATION FOR..\1 Console Number: 300.100 Calibrator: BLS Calibration Date: 12/24i96 

### Dry Gas Meter .'iumber: 1557648 Expiration Date: 12/24/97 Barometric Pressure, in. Hg: 29.070 Console Gas Volume 1'rfeter Temperatures Time Console 

# I

Orifice Wet Test Dry Gas Wet Test Dry Gas Meter DGM DGM Orifice Setting Meter Meter Meter Avg. 

### B Factor Yferer



### -il.H 

## vw



# ~~ t,. Inlet Outlet td Minutes y 

### :.IH@ in. 

### H,O 

## tt3 •F tdj tao 

### •F in. 

### H,O 

### •F •F 0.50 

# I 5 5.11 69.2 

# I 79.0 77.0 78.0 

# I 12.45 0.993 

# I 1.760 

# I 1.00 

### 5 5.11 69.3 83.5 78.0 

# I 80.8 8.96 0.997 1.814 

# I 1.50 10 10.22 69.3 86.5 78.5 82.5 14.71 0.999 

# I 1.828 2.00 10 10.22 69.2 86.5 79.0 82.8 

# I 12.97 0.998 1.893 

# I 3.00 10 10.24 69.4 90.5 80.0 85.3 10.59 0.998 1.886 

## I 4.00 10 10.23 69.3 93.0 81.0 87.0 9.21 1.000 1.895 

# I Average 1.00 

### 1.85 

## y t.H@ Tolerances: 1.00 1.84 ::!:0.02 =0.15 

## Y and

**D.~** 

### are calculated as follows: 

### Vw 

## * P, 

## * (t0 

## + 460) 

## y = ·------------------------------------------- = 

### 1.00 

# v" • (P, 

## + t.H/13.6) • 

### (t.. 

## + 460) 0.0317 

### * t.H 

### (t,. 

## + 460) * 

### B 

## t.H@ = --------------------- • (----------------------)2 

### = 1.85 P, 

### * 

### (t0 

## + 460) 

### Vw
E-6 

# //7.:::::. "\; ISOKINETIC CONSOLE CALIIHtATION DATA SHEET

Client L:ee fsf'lcJ\ City/State **~N.-fcwd** tJ.r. Project No. 046-97- ottr EmissionSource Nit,) f'(-)

r:n

__, Date ()lf- fJ 5 !9 2 Darometric Pressure, Pb '2<1. 3 3 in. Hg Wet Test Meter Number 600.002 Calibrator's lniliiiiS fr S
>

lsokinetic Console ldentirication Number 100. Z?IJS-- Dry Gas Meter Identirication Number / 5 S 7 6 lf 9: Pretest Y 1.00

Or lOco M<l<t (All) ln. 11 1 0 I:J :2:> **))~** ) **]~** 317>- 100 JYV

; 'C;. · ·.· i .' .. · ··.

I nlllal Settings; V11hnne$ 1111d Tecnper11lures

. . . .· ,. Wet Test Meter

. Isoklnetlc Consoli! ··.• .... ,. .. ···

Dry Gal **M~~·~ V~clluni,**  **Y~h111it** •nil **Ten•peralur~** · .. •. **~·** Vacuuaa Voluoie ...... ()IJIIel A•<rac•

ln. llu (V .> rt' .· "F "ff (I.J "F 70 Cl. Ln 1'1._5_ 7'l 0 co 3. 7_S
7.o cFi7 Cf)_ 0 'lO .0 ?rG o

--, ) i.C /0()\f- C() 5 '?Jo ?:7 75

V., = Gas volume of wet test meter, ft 1

V • = Gas volume of dry gas meter, re

lw = Tempera lure of wet test meier, oF Meier Volume (V.) rc• 10.0 10.0 10.0

t• = Average Temperature of dry gas meter, or

All = Pressure differential across orifice, in. 11 2 0 . . **M<le~** Tenip, (C.l . "ff· 67 0 (C] (J (?.o 1'hue (6) 1nln. 1', 0.3 II. O):J jl ? **~** ,J I ;lJ'I IJ 3 I.O]r;
r = /.CQC

Yi = Ratio of accuracy of wet test meter to dry gas meter for each replicate •.. . v.I\ (1, + 460)
v, (I'• + (AII/B.6)(1. + 460)

.·· IO • 2'L >) ( Sj' j -x + 460)

' I '

< '2'i. n + ( 7 ) **~** /13.6)( ('). ( + 460)

10. 2'\ '7 3

. > < **~i'3.** 7S + 460!

( )'(. -z,-, + ( ? ) ) /13.6)( r'i ( + 460) IOxl•(?) **~** ' ' < '? , 7 s· + 460)

. ) '

< 'J'l. 5 ·,, + < '2 n ti3.6H Or· + 460) !

Y = Average ratio of accurncy of wet lesl meier lo dry gas meter for all replicates; tolerance = pretest Y ± 0.05 }'

Pb = Darometric Pressure, in. Jig

0 = Time of calibration run, minutes

### ISOKINETIC CONTROL CONSOLE CALffiRATION FOR.'-1 Console Number: 300.200 

### Calibrator: PRJ Calibration Date: 04/01/97 

### Dry Gas Meter Number: 1523437 

### E-qJiration Date: 04/01/98 

### Barometric Pressure, in. Hg: 29.261 Console Gas Volume Meter Temperatures Time Console

Orifice Wet Test Dty Gas Wet Test Dry Gas Meter DGM DGM Setting Meter Meter Meter Avg. 

# e Factor

<l.H 

## vw



# ~ t.. Inlet Outlet td Minutes y in. H,O 

### rr' 'F tdi [do 'F 'F 'F 

### 0.50 

### 5 5.21 70.1 92.0 86.0 89.0 12.67 0.993 1.00 

### 5 5.21 70.2 95.0 86.0 90.5 9.15 0.994 1.50 10 10.41 70.0 97.0 87.0 92.0 15.28 0.997 2.00 10 10.42 70.0 99.0 87.0 93.0 13.29 0.996 3.00 10 10.43 70.0 102.0 88.0 95.0 10.88 0.996 4.00 10 10.43 69.7 103.5 88.5 96.0 9.51 0.996 Average 1.00 

### y 

### Tolerances: 1.00 ±0.02 

### Y and llH@ are calculated as follows: 

### Vw * 

### P. * 

### (td 

## + 460) y 

### = -------------------------------------------- = 

### 1.00 

## vd • (P. 

## + t.R'l3.6) • 

### (t.. 

## + 460) o.0317 • t.H 

### (t.. 

## + 460) • e t.H® 

### = --------------------- • (----------------------)2 

### = 1.91 

### P• * 

### (td 

## + 460) 

### Vw

E·8 Orifice Meter <l.H@ in. H,O 

### 1.780 1.853 1.931 1.944 1.947 1.978 1.91

ll}i@ 

### 1.84 ±0.15



# II10ISOKINETICCONSOLECALillRATIONDATASHEETClientLj'eRr:ckv-T:(e,City/StateS4rd../'/('ProjectNo.046-97_{'yi{)EmissionSourceK:-InZ-[lr7Date01/IZ'l!97BarometricPressure,Pb211in.HgWetTestMeterNuml>erIsokineticConsoleIdentificationNumber300.ZGODryGasMeterIdentificationNuml>erInitialSeUtrigs,and..•······TestMeterOryGuV•(!!PIJI;•11clMeterMeterTelt\peral111"1!.(.111)...•..•..(V.)(1.)ln.110Voi:uumVolumelnlel··OullelAverageft'•r1In,llg(V.,)ft'"F"F.(1,.)"F_,'10.0(ok(8),..,.._Y,600.002Calibrator'sInitialsTti:/5Z3L/37PretestY1.00v.T\(1,+460)v,u•.+(.Ut/tJ.6HI.+460)lOx(71J+460)z.311o.z.._n1?ss111o1n3J,J/2.05IoYl\,>fOLO(+ (231/13.6)((.,[,'i+460)1o.zqIns171o1?o.3'<)237r..)10.017.10)0X( +460)0.r-('{S10.Z1/(Z'i\1+ (z.-s?/13.6)(lrG.'1+460)--10.0)0X+460)Z.37I3.5liOlqIS\U171/.5I8/.Sl.t.....<"jlliZ-ILI0.9'<3,a.z'l(z+ (237/13.6)(1,4.'1+460)Vw=Gasvolumeofwettestmeter,feVd=Gasvolumeofdrygasmeter,fet,.=Temperatureofwettestmeter,optd=AverageTemperatureofdrygasmeter,opaH=Pressuredifferentialacrossorifice,in.H20y=0.qq5Yi=RatioofaccuracyofwettestmetertodrygasmeterforeachreplicateY=Averageratioofaccuracy•ofwettestmetertodrygasmeterforallreplicates;tolerance=pretestY±0.05Y1\=BarometricPressure,in.1-Ig0=Timeofcalibrationrun,minutes

### ISOKJNETIC CONTROL CONSOLE CALIBRATION FOR.t'\-1 Console Number: 300.214 Calibrator: DAC Calibration Date: 07/25/96 Dry Gas Meter Number: 2547128 Expiration Date: 07!25/97 Barometric Pressure, 

### in. Hg: 29.234 Console

Orifice Setting

AH in.Hp 

### 0.50 1.00 1.50 2.00 3.00 4.00 Gas Volume Meter Temperatures Time Console WetTest Dry Gas Wet Test Dry Gas Meter DGM DGM

Meter Meter Meter Avg. I} Factor



## vw

# ~~ tN Inlet Outlet !d Minutes y 

### -rtl •F tdi !do 

### •F •F "F 

### 5 5.08 80.7 89.0 85.5 87.3 12.62 0.995 5 5.09 80.9 94.5 87.0 90.8 9.15 0.998 10 10.20 81.1 96.5 88.0 92.3 14.82 0.997 10 10.23 81.2 99.0 89.5 94.3 12.98 0.996 10 10.24 81.2 101.5 90.5 96.0 10.54 0.996 10 10.24 81.3 104.0 91.0 97.5 9.17 0.996 

### Average 1.00 y Tolerances: 1.00 ::::0.02 

### Y and D.H@ are calculated as follows: 

# v

w • 

### pb .. (td 

## + 460) 

## y = -------------------------------------------- = 

### 1.00 

### vd • (Pb 

## + D.H/13.6) •**(~** 

## + 460) 0.0317 • D.H**(~** 

## + 460) • 9 

### D.H@ = -----:-------------- • (----------------------/ = 

### 1.90 

### pb (td 

## + 460) 

# vw

E-10 Orifice Meter llH@ in. H,O



### 1.845 1.929 1.894 1.931 1.904 1.917 

### 1.90 D.H@ 1.84 ::::0.15



# ld-1**~** ISOKINETIC CONSOLE CALIBRATION DATA SHEET

Client Ler **ISr~rk ~---n**  I"--

City/State SaV\-furrl

/VC Project No. 046

- 9 7- \)lit Emission Smuce I{(., 7

- P( l

Date nlj I z.<; !9 7 Darometric Pressure, P b Z. <? • Z- ( in. llg Wet Test Meter Number 600.002 Calibrator's Initials cY!Y1

lsokinetic Console Identification Number 300. L/ 1 ( Dry Gas Meter Identification Number 2 ",i((/7 5

P1etest }' 1.00

Orlnce Mcltr (4.11) ln. 11

1 0 Initial Seltlngs,

**Volu1ne~** ll'll! Temperahn·es lsoklnellc Consoli) no- Gu M(l•r

**V•~•!ulll, Va!~tQit**  **~'"' T~mperiilur~** 

· · V•cuna• I Volua•• I lnleJ ·1 Ollllel I Averos•

ln.

IlK (V J fl' "F "F (IJ "F

5. 3 I 0.17 I i)Lj S n.D

1 o<.>.3
**~.3** tn.L7 ln.5 **lz~.D** 1:?3.'6

(" '

) ,_) to.3Z-I03.o lgo.s **lcot...~**

V w = Gas volume of wet test meter, ft 1

Vd =Gas volume of dry gas meter, fe

**~** = Temperature of wet test meter, °F Wet Test Meter Meter Mtler **Volu1n~** T••IP• (V.) (t.) fl' "F 10.0 **(,~.0** 10.0 lo'l.q 10.0 **iD~** 0

td = Average Temperature of dry gas meter, or

**~II** = Pressure differential across orifice, in. 11

2 0 1'illlt (8) ....... 1', ((.27. II

0(0 I
II. zZ I**o_qq~.** I
11. 3s lo.tWII Y= i. 00(

Yi = natio of accuracy of wet test meter to dry gas meter for each replicate v.

,., u, + 460)
V, u>, + (Ati!lMl (1. + 460)
10. l'l Z-1 ( l,'(, 3 + 460) iD.(I ( 29.? I + ( 2?<; /13.6)( 1-l 0 + 460)

10 x z-'i **.z~** ( D3

**~** + 460)

iD. 2 7 ( Z'l.ll + (

**Z.?~** /B.6)( <. 7 'i + 460)

10 x zq a ( g(, 1 + 460)

10. **~** 1- ( Z'l.Z I + ( z 'IS /ll.6)( bZ. 0 + 460)

Y = Average ratio of accuracy of wet test meter to dry gas meter for all replicates; tolerance

= pretest Y ± 0.05 Y

Pb = Barometric Pressure, in. llg

0 = Time of calibration n111, minutes

### ISOKlNETIC CONTROL CONSOLE CALIBRATION FOR.'>! 

### Console Number: 300.248 Calibrator: RID Calibration Date: 08/15/96 Dry Gas Meter Number: 008761 Expiration Date: 08/15/97 Barometric Pressure, in. 

### Hg: 

### 29.304 Console Gas Volume Meter Temperatures Time Console

Orifice WetTest Dry Gas WetTest Dry Gas Meter DGM Setting Meter Meter Meter Avg. (}

M1 

## vw



# ~~ 1w Inlet Outlet td Minutes in. H,O 

### ttl 'F tdi 

# "0 'F 'F 'F 

### 0.50 5 5.06 76.0 84.5 81.0 82.8 12.45 1.00 5 5.09 76.0 89.8 83.8 86.8 9.32 1.50 10 10.15 76.5 92.0 85.3 88.7 15.40 2.00 10 10.18 77.0 96.0 87.5 91.8 13.25 3.00 10 10.19 77.0 98.8 89.8 94.3 10.94 4.00 10 10.15 77.0 97.0 89.0 93.0 9.45 Average Tolerances: 

### Y and

**~H@** 

### are calculated as follows: 

# vw. pb. (td 

## + 460) y = -------------------------------------------- 

# = 1.00 

## vd • (Pb 

## +

**~H/13.6)** 

### • 

### (lw 

## + 460) 0.0317 •

**~H** 

### (lw 

## + 460) * 

### IJ



### ~H® = -----:--------------- • (----------------------/ 

# = 1.96 pb (td 

## + 460) 

# vw

E-12 DGM Factor y 

### 0.999 1.000 1.004 1.004 1.005 1.004 1.00 

### y 

### 1.00 Orifice Meter 

### Mi@ in. H,O



### 1.775 1.975 2.019 1.985 2.021 2.015

1.96
±0.02 ±0.15



## /~3" \jj **~** ISOKINETIC CONSOLE CALIBRATION OATA SHEET

Client Ur fSrirlr .r-}; k

City/State Su'fl£d

!IG Project No. 046- 97- 0 1 \

**~** Emission Source /0

!11 ? /J( I

I

z v Date ll'/ I 21( /9 1 naromehic Pressure, 1\ 2f/f3 in. Ilg Wet Test Meter Number 600.002 Calibrator's Initials ...J1..!.Q

lsokinetic Console Identification Number 300. 2_li '6

Dry Gas Meter Identification Number (Xl/j 7 c, \

Pretest Y 1.00

Orifice Meier (<111) ln. 11

1 0 210 ?_2'1 z. 7-<f lnlllal SelllilllSjVoluule$ lllld Telilperah•re!!

. lsoklne!lc

**CQ!l~o!~** >

. .·

.. ·. ······· Wet Test Meier

llry (;u Meier

**V~oulllll, V~tiuu~**  **•~d** ·.·· **Teniperalut~** ... Vacuna1 Votunoe Intel outlet Averoge

ln. llg (V .J n• "F "(I (I.J "I'
(Q.O tO.IL fi.O 17.0 ?3.0

(,. 0 I() .t S I{ 0 ') 71')0 ¥11. **~**
1.,,0 (0.11 qz.O '?/.0 S'£. s

V w = Gas volume of wet test meter, ft 1

V d = Gas volume of dry gas meter, ft 1

**~** = Temperature of wei lest meter, •r Meter Vohuue (V,) ft' 10.0 10.0 10.0

td = Average Temperature of dry gas meter, •r

6.11 = Pressure differential across orifice, ln. liP Meter Te••P• (I.) "F (p '{I) l91 (( **{.,~.o 11~··**  (9) n•ln.

1',

I 2-.

**~)** j.OIO

I z_,_<; o (. D ( \ rz. so (011-
Y = /.01\

Yi = Ratio of accuracy of wet test meter to dry gas meter for each replicate V" I\

**(I~** + 460)
V, (1'. + (L\ll/13.6)(1, + 460)

IO x Z'l 't3 ( &' 3. D + 460) to.tl- < :a 'fl + ( 2.7q JIJ.6)( L>gu + 460)

10. l y 'i3 ( 1ij.g + 460) JO.f5 ( U.'t] + ( z l'l /13.6)( t,'/ 'I + 460)

10. z y q3 ( 61,

. s + 460) /0.1'7 ( 21i3 +(Z.l''t/13.6)( &f.D + 460)

Y = Average ratio of accuracy of wet test meter to dry gas meter for all replicates; tolerance

= pretest Y :t 0.05 Y

Pb = Barometric Pressure, in. Jig

0 = Time of calibration run, minutes

### TYPE "S" PITOT TCBE CALIBRATION FOR:\1 Date: 01/03/97 

### Calibrator: 

### JJT Specifications: A.) Pilot tube assembly must be level. B.) If pitot tube is damaged explain under co=ents section. C.) Z = A Sin 1 (<0.125) and W = A Sin 9 (<0.03125) D.) a .::_10" and

### /3 .::_5' I.D. Lengtb a1° aZO /310 /320 

# ,. go A, in. 

### Z. in. W, in. P. .\, in. PB, in. Individual PitotTubes 200.057 l' 1.0 1.0 0.5 1.0 0.0 0.0 0.630 0.000 0.00000 0.315 0.315 200.019 2' 1.0 1.0 0.0 0.0 1.0 1.0 0.936 0.016 0.01634 0.468 0.468 200.058 30" 0.0 1.0 2.0 4.0 3.0 0.0 0.918 0.048 0.00000 0.459 0.-+59 200.049 3' 3.0 0.0 1.0 1.0 1.0 1.5 0.949 0.017**O.D2~** 0.474 0.-+75 200.028 3' 2.0 7.0 1.0 1.0 3.0 1.0 0.977 0.051 0.01705 0.488 0.489 200.025** 5' 1.0 2.0 2.0 2.0 1.0 1.5 0.931 0.016 0.02437 0.466 0.465 200.054 5' 2.0 1.0 0.5 0.5 1.0 

### 1.5 0.784 0.01-+ 0.02052 0.392 0.392 200.044 

### tr 2.0 1.0 1.0 1.0 3.0 1.0 0.984 0.051 0.01717 0.492 0.492 200.038 7' 3.0 0.0 0.0 0.0 0.0 

### 1.5 0.951 0.000 0.02489 0.476 0.475 200.030 7' 6.0 7.0 1.0 1.0 2.0 1.0 0.978 0.034 0.01707 0.489 0.489 200.055 7' 1.0 1.0 0.0 1.0 0.0 1.0 0.841 0.000 0.01468 0.421 0.420 200.031 10' 4.0 8.0 1.0 0.0 1.0 1.5 0.943 0.016 0.02468 0.471 0.472 300.164 And. 3.0 3.0 1.0 3.0 3.0 1.0 1.113 0.058 0.01942 0.556 0.557

Co=ents: Pitol Tubes Required Only Minor Maintenance · Further Calibration Not Required •• Inconel 300.164 =Anderson Pitol Tube Extension E-14 Dt. in. 0.2-+7 0.377 0.377 0.375 0.375 0.379 0.377 0.376 0.376 0.374 0.375 0.372 0.374

### TYPE "S"' PITOT TL"BE CALIBR.HION FOR:\! Date: 01;03/97 Calibrator: JJT Spec1fications: A.) Pitot tube assembly must be level. B.) If pitot tube is damaged explain under comments section. C) Z = A Sin i' (.:;:0.125) and W = A Sin 9 (.:;:0.03125) D.) a _:s!O' and

### /3 .:;:5' I.D. Length go

**~** in. Z. in. W, in.

**P.~** in. PB, in. Dt, in. P!totTubes Attached to Probes 200.020 2' 2.0 2.0 0.0 200.021 2' 0.0 0.0 0.0 200.036 2' 200.037 2' 200.004 3' 200.005 3' 200.006 3' 200.015 3' 200.016 3' 200.017 3' 200.007 5' 200.008 5' 200.009 5' 200.022 5' 200.027 5' 200.034 5' 200.056 5' 200.061 5' 200.024. 6' 200.010 7' 200.011 7' 200.012 7' 200.039 7' 200.040 7' 200.059 7' 200.060 7' 200.041 8' 200.045 8' 200.013 10' 200.014 10' 200.050 12' 200.051 12' 200.052 12' 200.053 12' 0.0 1.0 0.0 0.0 1.0 1.0 0.0 1.0 0.0 1.0 4.0 0.0 2.0 2.0 2.0 3.0 6.0 1.0 1.0 2.0 1.0 0.0 0.0 0.0 2.0 2.0 1.0 2.0 2.0 0.5 0.0 2.0 2.0 5.0 5.0 3.0 0.0 1.0 2.0 2.0 2.0 3.0 0.0 1.0 0.0 0.0 0.0 0.0 4.0 5.0 2.0 0.0 1.0 0.0 0.0 0.0 0.0 0.0 1.0 0.0 2.0 2.0 1.0 2.0 0.0 2.0 0.0 1.0 1.0 0.0 0.0 

## o.o 0.0 0.0 2.0 2.0 0.0 0.0 3.0 0.0 0.0 1.0 2.0 2.0 0.0 0.0 2.0 0.0 0.0 1.0 2.0 1.0 0.0 0.0 1.0 0.0 1.0 0.0 2.0 1.0 1.0 1.0 2.0 0.0 2.0 0.0 2.0 0.0 1.0 3.0 3.0 4.0 1.0 1.0 3.0 1.0 0.0 0.0 0.0 2.0 1.0 1.0 1.0 2.0 3.0 1.0 0.0 0.0 1.0 1.0 0.0 3.0 0.0 3.0 1.0 1.0 3.0 1.0 2.0 1.0 2.0 1.0 2.0 2.0 1.0 5.0 0.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 0.0 1.0 !.0 2.0 1.0 1.0 0.0 0.0 0.0 1.0 0.0 1.5 0.0 1.0 1.0 1.0 1.0 0.5 1.0 1.0 1.5 1.5 0.0 1.0 1.0 1.5 1.5 0.0 2.0 1.0 1.0 1.0 0.5 1.0 1.0 0.0 1.0 1.0 1.0 1.0 0.0 2.0 1.0 0.0 1.063 1.054 0.990 0.969 0.936 0.948 0.934 0.943 0.946 0.939 0.948 0.950 0.938 0.949 0.940 0.934 0.935 0.597 0.580 0.938 0.942 0.943 0.955 0.944 0.598 0.604 0.931 0.937 0.937 0.955 0.964 0.917 0.907 0.961 0.000 0.055 0.000 0.051 0.016 0.017 0.049 0.016 0.033 0.016 0.033 0.017 0.033 0.033 0.016 0.081 0.000 0.010 0.010 0.016 0.016 0.016 0.017 0.033 0.000 0.011 0.016 0.033 0.016 0.017 0.000 0.000 0.000 0.017 0.00000 0.02759 0.00000 0.01691 0.01634 0.01654 0.01630 0.00823 0.01651 0.01639 0.02482 0.02487 0.00000 0.01656 0.01641 0.02445 0.02448 0.00000 0.02024 0.01637 0.01644 0.01646 0.00833 0.01648 0.01044 0.00000 0.01625 0.01635 0.01635 0.01667 0.00000 0.03200 0.01583 0.00000 0.531 0.527 0.495 0.485 0.468 0.474 0.467 0.471 0.473 0.469 0.474 0.475 0.469 0.474 0.470 0.467 0.467 0.299 0.290 0.469 0.471 0.471 0.477 0.472 0.299 0.302 0.465 0.468 0.468 0.478 0.482 0.458 0.454 0.480

Comments: Pitot Tubes Required Only Minor Maintenance . Further Cllibration Not Required • Water Cooled E-15 0.532 0.527 0.495 0.484 0.468 0.474 0.467 0.472 0.473 0.470 0.474 0.475 0.469 0.475 0.470 0.467 0.468 0.298 0.290 0.469 0.471 0.472 0.478 0.472 O.Z99 0.302 0.466 0.469 0.469 0.477 0.482 0.459 0.453 0.481 0.371 0.373 0.375 0.372 0.377 0.378 0.374 0.378 0.374 0.374 0.375 0.378 0.375 0.376 0.374 0.373 0.374 0.252 0.251 0.375 0.375 0.375 0.375 0.373 0.253 0.251 0.376 0.375 0.374 0.375 0.375 0.376 0.376 0.376

## STAINLESS STEEL NOZZLE CALIBRATION DATA SETTHREE Date Calibrated: 

### 01/03/97 Calibrated By: ELB Nozzle Diameter (a) Nozzle Davg(c) Dl 02 03 Diff. Number (in.) (in.) (in.) (in.) (b) 5/8" Nozzle 300.118 0.684 

### 0.685 0.684 0.683 0.002 

### 1/2" Nozzles 300.115(1) 0.494 

### 0.495 0.493 0.494 0.002 300.116(2) 0.495 

### 0.495 0.495 0.494 0.001 300.117(3) 0.495 

### 0.494 0.494 0.497 0.003 7/lll' Nozzles 300.131(1) 0.439 

### 0.438 0.439 0.440 0.002 300.132(2) 0.425 

### 0.424 0.424 0.427 0.003 300.133(3) 0.426 

### 0.426 0.425 0.427 0.002 3/8" Nozzles 300.125(1) 0.372 

### 0.371 0.373 0.371 0.002 300.126(2) 0.370 

### 0.372 0.369 0.369 0.003 300.127(3) 0.371 

### 0.370 0.371 0.372 0.002 5/16" Nozzles 300.109(1) 0.300 

### 0.300 0.300 0.301 0.001 300.110(2) 0.300 

### 0.299 0.300 0.300 0.001 300.111(3) 0.299 

### 0.300 0.299 0.298 0.002 1/4" Nozzles 300.112(1) 0.249 

### 0.248 0.250 0.250 0.002 300.113(2) 0.246 

### 0.246 0.246 0.246 0.000 300.114(3) 0.250 

### 0.250 0.250 0.249 0.001 3/11l' Nozzles 300.128(1) 0.174 

### 0.176 0.173**0.17'~** 

### 0.003 300.129(2) 0.174 

### 0.173 0.175 0.174 0.002 300.130(3) 0.171 

### 0.170 0.171 0.173 0.003

where: (a) 01, 02 and 03 = three differ.,t noz::l• inskie diameters, measured to neatest 0.001 in. (b) 0 = maximum difference between arry two diameters, (in.) 0 < 0.004 in. (c) Oavg .:a av«age of 01, 02, and 03 E·I6 

## /:?7

## STAJNLESS STEEL NOZZLE CALIBRUION DATA SET FOUR 

## Date Calibrated: 01/03/97 

## Calibrated By: ELB Nozzle Diameter (a) Nozzle Davg(c) D1 D2 D3 Diff. Number (in.) (in.) (in.) (in.) 

### (b) 3/4" Nozzle 300.236(1) 0.758 0.759 0.758 0.758 0.001 

### 5!8" Nozzle 300.235(1) 0.618 0.617 0.618 0.618 0.001 1/2" Nozzles 300.189(1) 0.488 0.488 0.489 0.487 0.002 300.190(2) 0.493 0.492 0.494 0.494 0.002 300.251(3) 0.494 0.492 0.494 0.495 0.003 7/16" Nozzles 300.234(1) 0.430 0.429 0.430 0.430 0.001 300.233(2) 0.430 0.428 0.430 0.431 0.003 3/8" Nozzles 300.187(1) 0.375 0.374 0.375 0.376 0.002 300.188(2) 0.372 0.373 0.373 0.371 0.002 300.252(3) 0.367 0.368 0.368 0.365 0.003 

### 5!16" Nozzles 300.193(1) 0.308 0.308 0.309 0.307 0.002 300.194(2) 0.307 0.307 0.307 0.307 0.000 300.195(3) 0.313 0.313 0.315 0.312 0.003 114" Nozzles 300.191(1) 0.239 0.239 0.239 0.238 0.001 300.192(2) 0.235 0.235 0.235 0.236 0.001 300.253(3) 0.234 0.234 0.234 0.235 0.001 7

/32" Nozzle 300.255(1) 

### 0.222 0.221 0.221 0.223 0.002 3/16" Nozzles 300.232(1) 0.174 0.173 0.173 0.176 0.003 300.231(2) 0.177 0.176 0.177 0.177 0.001 300.254(3) 0.183 0.184 0.183 0.181 0.003 

### 5!32" Nozzle 300.256(1) 0.149 0.149 0.149 0.148 0.001 where: (a) 01, 02 and 03 "" thr" different noz:te inside diameters, measuntd to nearest 0.001 in. (b) 0 a maximum difference between any two dlameters. (in.) 0 < 0.004 in. (c)

**Oav~** "" av•aQe of 01, 02, and 03 E-17 

## I

### P'\ 7

### REX NOZZLE CALIBRATION DATA 5/8"

**S~'iK** Date Caliorated: 01/03/97 Caliorated 

### By: PRJ Nozzle Diameter (a) Nozzle Davg(c) Dl D2 D3 Diff. Number (in.) (in.) (in.) (in.) (b) 1.25"

**~ozzles** 300.283 1.225 1.224 1.226 1.226 0.002 300.284 1.228

**1.~28** 1.227 1.229 0.002 1" Nozzles 300.218 0.999 0.999 0.998 0.999 0.001 300.219 0.995 0.995 0.995 0.996 0.001 5/8" Nozzles 300.101 0.623 0.623 0.625 0.622 0.003 300.102 0.623 0.623 0.622 0.623 0.001 300.186 0.622 0.621 0.622 0.622 0.001 112" Nozzles 300.103 0.497 0.496 0.497 0.498 0.002 300.104 0.502 0.502 0.502 0.503 0.001 300.270 0.496 0.495 0.496 0.497 0.002 7/16" Nozzles 300.078 0.432 0.431 0.432 0.432 0.001 300.095 0.442 0.443 0.441 0.441 0.002 300.096 0.436 0.436 0.434 0.437 0.003 3/8" Nozzles 300.077 0.382 0.381 0.382 0.383 0.002 300.093 0.378 0.378 0.379 0.376 0.003 300.094 0.381 0.382 0.381 0.381 0.001 5/16" Nozzles 300.088 0.311 0.312 0.311 0.311 0.001 300.089 0.309 0.308 0.310 0.310 0.002 300.092 0.311 0.310 0.310 0.313 0.003 1/4" Nozzles 300.075 0.255 0.255 0.255 0.254 0.001 300.121 0.253 0.252 0.253 0.253 0.001 300.122 0.241 0.241 0.241 0.241 0.000 3/16" Nozzles 300.183 0.192 0.192 0.192 0.191 0.001 300.184 0.191 0.191 0.190 0.191 0.001 300.185 0.190 0.190 0.191 0.190 0.001 1/8" Nozzles 300.239 0.128 0.126 0.128 0.130 0.004 300.240 0.133 0.134 0.132 0.133 0.002 

### """'"' (a) 01. 02 and D3 • ttl,... dltf...,t ncz:i• 1nS1da

**diamM~** mee.sured to nMtast 0.001 1n. (r;)) D • I"NJUmum diff...n<:a r;,_......, any twa

**diamlll:~.** (in.) D < 0.004 1n. (c) Davg • averaga at 01, 02. and D3 E-lS 

# /2 '/

### PYREX NOZZLE CALIBR.\TION DATA 5/8"

**SHA..t~X** 

### Date Calibrated: 01/03/97 

### Calibrated By: PRJ 

### Nozzle Diameter (a) Nozzle Number 300.282 300.272 300.280 300.271 300.274 300.275 300.279
300.273 300.278

300.091 300.276

300.281 where: 

### Davg(c) (in.) 

### 0.995 0.622 0.627 0.496 0.497 0.500 0.435 0.375 0.376

0.242 0.245

0.125 01 02 03 Diff. (in.) (in.) (in.) 

### (b) 1" Nozzles 0.995 0.995 0.996 0.001 5/8" Nozzles 0.623 0.623 0.621 0.002 0.627 0.627 0.627 0.000 1/2" Nozzles 0.496 0.496 0.497 0.001 0.496 0.497 0.499 0.003 0.499 0.501 0.500 0.002 7/16" Nozzles 0.434 0.435 0.435 0.001 3/8" Nozzles 0.373 0.376 0.376 0.003 0.376 0.377 0.375 0.002 5/16" Nozzles
1/4" Nozzles 0.242 0.242 0.242 0.000 0.243 0.245 0.246 0.003 3/16" Nozzles
1/8" Nozzles 0.124 0.124 0.126 0.002 (a) 01, 02 and 03 ,. three different nozzle inside diameters. me.asured to nurest 0.001 in. (b) D '"' max1mum difference between any two diameters, (in.) 0 < 0.004 in. (c) Oavg == average of 01, 02, and 03
E-19 

# !30

### TEMPERATURE SENSOR CALIBRATION FORM NIST REFERENCE THERMOMETERTRANSFER CALIBRATION Tolerance:

**+/~** 1.5% of Absolute Temperature Date: 01!03/97 Barometric Pressure, In. Hg: Ambient Temperature. Deg. F: 76 Reference Thermometer No.: Cllibrated By: PRJ Reference Thermometer No.: NIST Reference Transfer Thermocouple lD No. Reference Thermometer Temperature

Degrees F ·30 to 120 Deg. FThermometer Serial Number 97133 Source Point Instrument Temperature

Degrees F 100.022 1 Water Bath 46 2 WaterBath 74 3 Water Bath 120 ·5 to 400 Deg. C Thermometer Serial Number U38717 46 74 120 100.024 1 Water Bath 74 23 Deg. C 2 Water Bath 120 49 Deg. C 3 Oil Bath 274 134 Deg. C ·120 to 2000 Deg. F Omega HH25 KF Pyrometer Serial Number T·124997 Red Team 100.025 1 Water Bath 47 4 7 2 Water Bath 72 72 3 Water Bath 181 181 ·120 to 2000 Deg. F Omega Hll25 KFPyrometer Serial Number T-151625 Green Team 100.031 1 Water Bath 46 46 2 **~~&ili** 

### u

**~** 3 Water Bath 208 207 ·120 to 2000 Deg. F Omega Hll25 KF Pyrometer Serial Number T·98180 Blue Team 100.017 1 Water Bath 46 46 2 Water Bath 74 74 3 Water Bath 186 187 -120 to 2000 Deg. FOmega HH25 KF Pyrometer Serial Number T·l56311 Gold Team 100.032 1 Water Bath 46 46 2 3 Water Bath Water Bath 74 186 74 186 ·120 to 2000 Deg. FOmega HH2S KF Pyrometer Serial Number T·156877 Grey Team 100.033 1 Water &th 4 7 4 7 2 Water Bath 76 76 3 Water Bath 193 193 ·120 to 2000 Deg. FOmega HII25 KFPyrometer Serial Number T-148889 CEM 100.026 1 Water Bath 46 46 2 **%~r&ili** 74 U 3 Water Bath 186 186

Source =Type ofcalibration system used. Temper:1ture Difference Cllculation; (Ref. Temp. Deg. F 

### + 460) ·(TestTemp. Deg. F 

### + 460) X 100 = <1.5% Ref. Temp. Deg. F 

### + 460 E-20 29..l55 100.02.1 100.028 Temperature

Difference Calculation Percent.% 0.00 0.00 0.00 0.11 -0.03 0.11 0.00 0.00 0.00 0.00 .0.19 0.15 0.00 0.00 .0.15 

## o.oo 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00



# ;3!

### TE:\'1PERATURE SENSOR CALIBRATION FORM THER:VlOCOUPLES Tolerance: +/- 1.5% of Absolute Temperature Date: 01/03/97 Barometric Pressure. In. Hg: Ambient Temperature. Deg. F: 76 Reference Thermometer No.: C.11ibrated By: PRJ Reference Thermometer No.: Reference Ther-mocouple Thermocouple Reference Thermometer Potentiometer ID No. Point Source Temperature Temperature Degrees F Degrees F Omega HH-25 KF Dry Bulb· Red Team 100.o25 1 Water Bath 72 72 2 Water Bath 181 181 3 Oil Bath 290 289 Omega HH-25 KF Wet Bulb • Red Team 100.o2S 1 Water Bath 72 72 2 Water Bath 135 135 3 Water Bath 173 173 Omega HH-25 KF Dr-y Bulb· Green Team 100.031 1 Water Bath 76 75 2 Water Bath 175 175 3 Oil Bath 295 296 Omega HH-25 KF Wet Bulb· Green Team 100.031 l Water Bath 76 75 2 Water Bath 138 137 3 Water Bath lii 177 Omega HH-25 KF Dry Bulb· Blue Team 100.017 l Water Bath 76 76 2 Water Bath 175 !75 3 Oil Bath 295 296 Omega HH-25 KF Wet Bulb· Blue Team 100.017 l Water Bath 76 76 2 Water Bath 138 137 3 Water Bath 177 177 Omega HH-25 KF Dry Bulb· Gold Team 100.032 l Water Bath 76 76 2 Water Bath 175 175 3 Oil Bath 295 295 Omega HH-25 KF Wet Bulb· Gold Team 100.032 1 Water Bath 76 76 2 Water Bath 138 138 3 Water Bath !77 177

Source = Type of calibration system used. Temperature Difference C.llculation: (Rei. Temp. Deg. F 

### + 460) ·(Test Temp. Oeg. F + 460) ···········-·····---------·····--·-··-·-········ X 100 = < 1.5% Ref. Temp. Deg. F 

### +

**~60** E-21 29.455 !00.024 !00.028 Temperature

Difference CaJculation Pereent,% 0.00 0.00 0.13 0.00 0.00 0.00 0.19 0.00 -0.13 0.19 0.17 0.00 0.00 0.00 -0.13 0.00 0.17 0.00 0.00 0.00 0.00 0.00 0.00 0.00



# !32

### TEMPER.\.TURE SENSOR CALIBRATION FOR-"1 THERMOCOUPLES Toler:mce: ?/- 1.5% of Absolute TemperJ.ture Date; 01/03/97 Barometric Pressure. In. Hg: AmbientTempenture, Deg. F: 76 Reference Thermometer No.: Calibrated By: PRJ Reference Thermometer No.: Reference Thermocouple Thermocouple ReCerence Thermometer Potentiometer IDNo. Point Source Tempernture Temperature Degrees F Degrees F r PitotTube 200.019 1 Water Bath 73 73 2 Water Bath 190 190 3 Oil Bath 393 391

**30~** Pitot Tube 200.058 1 Water Bath 55 55 2 Water Bath 187 186 3 Oil Bath 376 375 3' PitotTube 200.049 1 Water Bath 73 73 2 Water Bath 190 190 3 Oil Bath 392 390 3' PitotTube 200.028 1 Water Bath 74 74 2 Water Bath 188 188 3 Oil Bath 391 392 S' PitotTube- lnC"oneJ 200.025 1 Water Bath 73 73 2 Water Bath 188 188 3 Oil Bath 389 387 4 Muffle Furnace 520 5" 

# .. 5 Muffle Furnace 857 855 6 Muffle Furnace 1ll5 1ll6 5' PitotTube 200.054 1 Water Bath 75 75 2 Water Bath 188 188 3 Oil Bath 388 387 6' PitotTube 200.044 1 Water Bath 73 73 2 Water Bath 186 185 3 Oil Bath 386 385 7' PitotTube 200.038 1 Water Bath 73 73 2 Water Bath 186 186 3 Oil Bath 383 382 7' PItot Tube 200.030 1 Water Bath 73 73 2 Water Bath 184 184 3 Oil Bath 391 391 7'PltotTube 200.055 1 Water Bath 73 73 2 Water Bath 184 183 3 Oil Bath 386 385 10' PitotTube 200.031 1 Water Bath 73 73 2 Water Bath 183 183 3 Oil Bath 388 388 Source ,. Type ofc:liibratiou system used. Temperature Difference CaiC"uiation: _(Ref. Temp. Deg. F + 460) ·(festTemp. Deg. F +

**~60)** X 100 =- <1.5% Ref. Temp. Deg. F + 460 29A55 100.023

**100.02~** Tempen1ure

Difference C.J.icul.:llion Percen4% 0.00 0.00 0.:3 0.00 0.15 0.12 0.00 0.00 0.23 0.00 0.00 -{).12 0.00 0.00 0.24 

### -o.:o 0.15 ·0.06 0.00 0.00 0.1: 0.00 0.15 0.12 0.00 0.00 0.11 0.00 0.00 0.00 0.00 0.16 0.11 0.00 0.00 0.00



## 133

### TE:VIPERATURE SENSOR CALIBRATION FORM THERMOCOUPLES Toler:1nce: +/- 1.5% of Absolute Ternper:lture Date: 01!03/97 Barometric Pressure, In. Hg: 29.455 Ambient Temperature. Deg. F: 76 Reference Thermometer No.: 100.024 C>librated By: ELB Reference Thermometer No.: 100.023 Reference Thermocouple Temper::tture Thermocouple Reference Thermometer Potentiometer Difference ID No. Point Source Temperature Temperature Calculation Degrees F Degrees F Percent,% 3' Probe (l) 200.004 Water Bath 70 71 -0.19 2 Water Bath 191 192 ·0.15 3 Oil Bath 384 385 -0.12 3' Probe (2) 200.005 1 Water Bath 77 78 ·0.19 2 Water Bach 133 183 0.00 3 Oil Bath 385 387 ·0.24 3' Probe (3) 200.006 1 Water Bath 74 75 -0.19 2 Water Bath 175 176 ·0.16 3 Oil Bath 385 387 -0.24 3' Probe (4) 200.015 1 Water Bath 69 69 0.00 2 Water Bath 173 175 -0.32 3 Oil Bath 387 387 0.00 3' Probe (5) 200.016 1 Water Bath 65 65 0.00 2 Water Bath 165 165 0.00 3 Oil Bath 385 385 0.00 3' Probe (6) 200.017 1 Water Bath 71 71 0.00 2 Water Bath 167 167 0.00 3 Oil Bath 384 384 0.00

Source = Type of c.1libration system used. Temper:uure Difference Cllculation: (Ref. Temp. Deg. F 

### + 460) . (Test Temp. Deg. F 

### + 460) X 100 = <1.5% Ref. Temp. Deg. F 

### + 460 E-23 

# /3t/

### TE.lVIPERATURE SENSOR CALIBRATION FOR:Yl THER:YIOCOUPLES TolerJ.nce: +/· 1.5% of Absolute Tempenture Date: 01/03/97 Barometric Pressure. In. Hg: 29.455 Ambient Temper:J.ture. Deg. F: 76 Reference Thermometer No.; 100.024 Calibrated By: PRJ Reference Thermometer No.: 100.023 Reference Thermocouple Temperature Thermocouple Reference Thermometer Potentiometer Difference ID No. Point Source Temperature Temperature Calculation Degrees F Degrees F Percent,% 5' Probe (1) 200.007 1 Water Bath 78 78 0.00 2 Water Bath 203 204 ·0.15 3 Oil Bath 385 384 0.12 5' Probe (2) 200.008 1 Water Bath 76 76 0.00 2 Water Bath 195 196 ·0.15 3 Oil Bath 388 388 0.00 5' Probe (3) 200.009 1 Water Bath 80 80 0.00 2 Water Bath 171 173 -0.32 3 Oil Bath 386 384 0.24 5' Probe (4) 200.022 1 Water Bath 81 82 -0.18 2 Water Bath 193 191 0.31 3 Oil Bath 384 383 0.12 5' Probe (5) 200.027 1 Water Bath 79 78 0.19 2 Water Bath 191 192 -0.15 3 Oil Bath 385 384 0.12 5' Probe (6) 200.034 1 Water Bath 75 75 

## o.oo 2 Water Bath 186 188 -0.31 3 Oil Bath 387 385 0.24 5' Probe (7) 200.056 1 Water Bath 67 66 0.19 2 Water Bath 177 177 0.00 3 Oil Bath 383 382 0.12

Source = Type of Qlibration system used. Temperature Difference Calculation: (Rei. Temp. Deg. F + 460)- (TestTemp. Deg. F + 460) 

# ----------------------· X 100 = <1.5% Rei. Temp. Deg. F 

### + 460 E-24

## TEl\'lPERATURE SENSOR CALIBRATION FORM THERMOCOUPLES Tolerance: +/· 1.5% of Absolute Temperature DJ.te: 01/03/97 BJ.rometric Pressure. In. Hg: 29.455 Ambient Temperature. Deg. F: 76 Reference Thermometer No.: 100.G23 Calibr3ted By: JJT Reference Thermometer No.: 100.G23 Reference Thermocouple Temperature Thermocouple Reference Thermometer Potentiometer Difference ID No. Point Source Temperature

**Temper<:~ture** C:llculutlon Degrees F Degrees F Percent.% 300.035 DGM Inlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 182 182 0.00 300.035 DGM Outlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 184 183 0.16 300.045 DGM Inlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 182 182 0.00 300.045 DGM Outlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 186 186 0.00 300.067 DGM Inlet 1 Water Bath 33 34 .0.20 2 Water Bath 72 72 0.00 3 Water Bath 149 148 0.16 300.067 DGM Outlet 1 Water Bath 33 33 0.00 2 Water Bath 72 72 0.00 3 WJ.ter Bath 150 150 0.00 300.100 DGM Inlet 1 Water Bath 33 35 ·0.41 2 Water Bath 71 71 0.00 3 W:lter Bath 198 197 0.15 300.100 DGM Outlet 1 Water B:lth 33 34 ·0.20 2 Water Bath 71 71 0.00 3 Water Both 196 194 0.30

Source = Type of

**~iibr:Hion** system used. TernperJ.ture Difference C.liculation: (Ref. Temp. Deg. F 

### + 460) ·(TestTemp. Deg. F 

### + 460) X 100 = <1.5% Ref. Temp. Deg. F 

### + 460 E-25

### TEMPERATURE SENSOR CALIBRATION FORM THERMOCOUPLES Toler:mce: +i- 1.5% of Absolute Temperature Date: 01103/97 Barometric Pressure. In. Hg: 19A55 Ambient Temperature. Deg. F: 76 Reference Thermometer No.: 100.023 Calibrated By: JJT Reference Thermometer No.; 100.028 Reference Thermocouple Temperature Thermocouple Reference Thermometer Potentiometer Difference ID 

### :-<o. Point Source Temperature Temperature Calculation Degrees F**Degr~s** F Percent,% 300.ZOO DGM Inlet 1 Water Bath 33 34 ·0.20 2 Water Bath 73 73 0.00 3 Water Bath 182 182 0.00 300.ZOO DGM Outlet 1 Water Bath 33 34 -0.20 2 Water Bath 73 73 0.00 3 Water Bath 184 184 0.00 300.214 DGM Inlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 182 183 ·0.16 300..::14 DGM Outlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 186 186 0.00 300.241 DGM Inlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 184 184 0.00 300.241 DGM Outlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 182 182 0.00 300.248 DGM Inlet 1 Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath !82 182 0.00 300.248 DGM Outlet l Water Bath 33 33 0.00 2 Water Bath 73 73 0.00 3 Water Bath 185 !85 0.00

Source =Type of**~libr:~.tion** system used. Temperature Difference Calculation: (Ref. Temp. Deg. F 

### + -160) ·(Test Temp. Deg. F 

### + 460) X 100 = < !.5% Ref. Temp. Deg. F 

### + 460 E-26 

# /37

### TE;\-lPERATURE SENSOR CALIBRATION FORM

**THER~IOCOUPLES** Tolerance: +I- 1.5% of Absolute Temperature Date: 01/03/97 Barometric Pressure. In. Hg: 29.455 Ambient Temperature. Deg. F: 76 Reference Thermometer No.: 100.023 Glibroted By: PRJ Reference Thermometer No.: 100.028 Reference Thermocouple Temperature Thermocouple Reference Thermometer Potentiometer Difference ID No. Point Source Temperature Temperature Calculation

**Degr~s** F Degrees F Percent,% Umblllcal Adaptor #1 300.030 1 Water Bath 32 33 -0.20 2 Water Bath 74 74 0.00 3 Water Bath 124 124 0.00 Umbilical Adaptor #2 300.031 1 Water Bath 32 33 -0.20 2 Water Bath 74 74 0.00 3 Water Bath 124 124 0.00 Umblllcal Adaptor #3 300.032 1 Water Bath 33 34 -0.20 2 Water Bath 74 74 0.00 3 Water Bath 127 127 0.00 Umbilical Adaptor #4 300.042 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 127 127 0.00 Umbilical Adaptor #5 300.043 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 127 127 0.00 Umbilical Adaptor #6 300.044 1 Water Bath 33 34 -0.20 2 Water Bath 74 74 0.00 3 Water '"; 1th 127 127 0.00 Umbilical Adaptor #7 300.134 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 126 126 0.00 Umblllcal Adaptor #8 300.135 1 Water Bath 33 34 -0.20 2 Water Bath 74 74 0.00 3 Water Bath 126 126 0.00
Source = Type of

**~libration** system used. Temper:lture Difference Clicub.tion: ·. (Ref. Temp. Deg. F + 460) ·(TestTemp. Deg. F + 460) X 100 = <1.5% Ref. Temp. Deg. F + -!60 [-27

### TE:\'1PERATURE SENSOR CALIBRATION FORM THER:\'lOCOUPLES Tolero.nce: +:'· 1.5% of Absolute Ternpero.ture Date: 01/03/97 Barometric Pressure. In. Hg: l9.-155 Ambient Temperature. Deg. F: 76 Reference Thermometer No.: !OO.Q23 C.:llibrated By: PRJ Reference Thermometer**~a.:** 100.D28 Reference Thermocouple Tcmpcr:lture Thermocouple Reference Thermometer Potentiometer Difference ID No. Point Source Temperature Temperature C;JJcuJatlon Degrees F Degrees F**Percent~%** Umblllcal Adaptor #9 300.207 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 126 126 0.00 Umbilical Adaptor # 10 300.208 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 126 126 0.00 Umbilical Adaptor #11 300.216 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 125 125 0.00 Umbilical Adaptor #12 300.217 1 Water Bath 33 33 0.00 2 Water Bath 74 74 0.00 3 Water Bath 125 125 0.00 Umblllcal Adaptor #13 300.264 1 Water Bath 33 34 -0.20 

## , Water Bath 74 74 0.00 

### • 3 Water 83th 125 124 0.17 Umbilical Adaptor M26 300.079 1 Water Bath 32 31 0.20 2 Water Bath 74 74 0.00 3 Water Bath 125 124 0.17 Umbilical Adaptor M26 300.166 1 Water Bath 32 32 0.00 2 Water Bath 74 74 0.00 3 Water Bath 125 123 0.34

Source =Type of calibration system used. Temperature Difference Calculation:

. (Ref. Temp. Deg. F 

### + 460) ·(TestTemp. Deg. F 

### + 460)



# -------------------------------------------------------- X 100 

### = <1.5% Ref. Temp. Deg. F 

### +**~60**E'l"2:?, RE_;o_:;·f T!-iE?.MCME':'E?. C:J. , I::-JC. 

### 2 2 3 LAC:<AW.f:..NNA A VS"'w=:**WES~ ?AT~ERSON** **1 ~J**  07424 

### (20:.) 812-7474 

### R E ? 

### 0 R T 0 F C A L I 3 R A T I 0 N**L:QUID-IN-GLASS-L~E~~CMETER** 

### C..1\..LI3R.Z\.':'SD BY SVER READY THE?.MCMETER CO. FOR: TRIGON ENGINEERING MARKED: ERTCO CAT 1002-3FC S/N-2890**R.~~GE:** 

### +30 TO +:24 DEGREES F IN 0.2 DEGREE GR.;DGATIONS. THER."!OME'!ER READING 32.00 F 40.00 60.00 100.00 120.00 CORRECTION (ITS-90) 

## ** 0.00 F -0.06 -0.06

0.00 -0.06 

## ** ALL TEMPERATURES IN THIS REPORT**~~** 

### BASED ON THE INTERNATIONAL TZMPERATJ?E SCALE OF 1990 (ITS-90) PUoLISHED IN**T.~E** 

### METROLGIA 27, NO.1, 3/10/90. THIS**T.~ZRMOMETER** 

### WAS C..l\..L:BRATZD AGAINST A**S~~~ARD** 

### CALIBRATED AT TdE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY (NIST) FORMERLY THE NATIONAL BL'REAU OF**ST.'lliD~'illS** 

### (NBS) IN ACCORDANCE WITH ASTM METHOD E 77,**&~NBS** 

### MONOGRAPH 174. FOR A DISCUSSION OF ACCURACIES ATTAINABLE WITH SUCH THERMOMETERS SEE NBS MONOGRAPH 250-23. IF NO SIGN IS GIVEN ON THE**COR.~ECTION, T.~E**  

### TRUE TEMPERATJRE IS HIGHER T.-iAN**T.~E** 

### INDICATED TEMPERATURE; IF THE SIGN GIVEN IS NEGATIVE, THE TRUE TEMPERATURE IS LOWER T:-iAN THE INDIC..Z\.TED TEMPER.Z\.TURE. TO USE THE**COR.~EC** 

### TIONS PROPERLY, REFERENCE SHOULD BE MADE TO THE NOTES GIVEN BELOW. THE THERMOMETER WAS TESTED IN A LARGE, CLOSED-TOP, ELECTRICALLY HEATED, LIQUID BATH, BEING "IMMERSED" 76MM. THE TZMPERATURE OF THE ROOM WAS ABOUT 25 DEGREES C (77 DEGREES F). IF THE THERMOMETER IS USED UNDER CONDITIONS WHICH WOULD CAUSE THE AVERAGE TEMPERATURE OF THE EMERGENT LIQUID COLUMN TO DIFFER MARKEDLY F?.OM THAT PREVAILING IN THE TEST, APPRECIABLE DIFFERENCES IN THE INDICATIONS OF THE THERMOMETER WOULD RESULT.

TEST**NL~BER:** 

### 154161 DATE: .11/26/96 STANDARD SERIAL NO. 128239 NIST IDENTIFICATION NO. 88024 E-29 

### CONTINUED


# lt/o

### ?AG2 2 OF - 

### R E P 0 R T 0 2 C A L I 3 R A 

### T I 0 N

**LIQUID-IN-GLASS-TH~~~OME~~R** 

### THE

**TABu~TED** 

### CORRECTIONS APPLY

**PROVI~ED TH~**  

### ICE-POINT

**RE~~ING, TAK~N**  

### AFTER EX?OSURE FOR NOT LESS

**THlu~** 

### 3 DAYS TO A TEMPERAruKE OF ABOUT 20 

### DEGREES C (70 

### DEGREES F) IS 32.00 

### DEGREES F. IF THE ICE-POINT READING IS FOUND TO BE HIGHER (OR LOWER) TFJlli STATED, ALL OTHER READINGS WILL BE

**HIGH~R** 

### (OR LOWER) TO THE SA."'E EXTENT. I2 THE rdERMOMETER IS USED AT A GIVEN TEMPERATURE SHORTLY AFTER BEING F£ATED TO A HIGHER

**TEMPERA~E.**

**A.~** 

### ERROR OF 0.01 

### DEGREES OR LESS, FOR EACH 10 

### DEGREE DIFFERENCE

**BE~NEEN** 

### THE TWO TEMPERATURES, MAY BE INTRODUCED. THE TABULATED CORB.ECTIONS A?PLY IF THE

**THER~OMETER** 

### IS USED IN THE UPRIGHT POSITION; IF USED IN A

**HORIZONT~** 

### POSITION, THE INDICATIONS MAY BE A FEW HUriDREDTHS OF A DEGREE HIGHER.

TEST NUMBER: 154151 

### DATE: 11/26/95 STANDARD SERIAL NO. 128239 

### NIST IDENTIFICATION NO. 88024 E-30 

### Charles Tang-Nian I QUALITY CONTROL

**~ER**

## =:v=:?.. RE:..JC: :'?:E:P_"v!cM=:-::::::. ::: . , 

## :)Jc. 2 2 8 LAC:Qtl&'l""Nrl .:o..·;:::c.JUE WEST

**?A~~ERSCN, N~**  

### 07424 (20l) 8:2-7474 R E P 0 R 7 0 2 C A

**~** 

### : 3 R ;;. T - 0 N

**LIQUID-IN-GLASS-7EE~~CME7ER**

**C~:3RA~E:D** 

### BY EVER READY TEE:RMOME7ER CO.

**~ARK2D:** 

### ER7CO CAT 612-3FC S/N-2775

**~~GE:** 

### 0 TO +300 DEGREES F IN 2 DEGREE: GRADUATIONS. THERMOMETER RE:rlDIOJG 32.6 F 100.0 200.0 300.0 

### ** ALL

**TEMPER..~~ES** 

### IN THIS REPORT TEMPERAPJRE SCALE OF 1990 (ITS-90) NO. l, 3/10/90. COR..'<.ECTION (:i:TS-90) 

### ** -0.6 

### F -1.6 -1.4 

### -1.0 ARE BASED ON THE

**I~ERNA~!ONAL** 

### PUBLISHED IN THE METROLGIA 27, THIS THERMOMETER WAS CALIBRATED AGAINST A S7ANDARD CALIBRATED AT THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY (NIST) FORMERLY THE NATIONAL

**Bu~U** 

### OF STANDARDS (NBS) IN

**ACCORD&~CE** 

### WITH ASTM

**MET.~OD** 

### E 77, AND NBS MONOGRAPH 174. FOR A DISCUSSiON OF ACCURACIES ATTAINABLE WITH SUCH

**TdER..~OMETERS** 

### SEE NBS MONOGRAPH 250-23. IF NO SIGN IS GIVEN ON THE CORRECTION, THE TRUE TEMPERATURE IS HIGHER TF..AN THE INDICATED TEMPERATURE; IF THE SIGN GIVE.L'J IS NEGATIVE, THE TRUE TEMPERATuKE IS LOWER THAN THE INDICATED TEMPERATURE. TO USE THE CORRECTIONS PROPERLY, REFERENCE SHOULD BE MADE TO THE NOTES GI'TEN BELOW. THE THERMOMETER WAS TESTED IN A LARGE, CLOSED-TOP, ELECTRICALLY HEATED, LIQUID BATH, BEING "IMMERSED" 76MM. THE TEMPERATURE OF THE ROOM WAS

**.~Ou7** 

### 25 DEGREES C (77 DEGREES F). IF THE THERMOMETER IS USED UNDER CONDITIONS WHICH WOULD CAUSE THE AVERAGE TEMPERATURE OF THE EMERGENT LIQUID COLUMN TO DIFFER MARKEDLY FROM THAT PREVAILING IN THE TEST, APPRECIABLE DIFFERENCES IN THE INDICATIONS OF THE THERMOMETER WOULD RESULT.

TEST NUMBER: 155404 DATE: 04/22/97 ST&'JDARD SERIAL NO. 48511 NIST.IPENTIFICATION NO. 92564 CONTINUED

E-31

### ?AGE 2 CF**~** 

### R E P 0 R T 0 F C A L I B R A T I 0 N**LIQUID-IN-GLASS-THER~OMETER** 

### TH:::: TABul-ATED COR.'<.ECTIONS A.?PLY PROVIDED TI'!E ICE POINT READING IS 32.6 DEGREES F. IF THE ICE-POINT READING IS**FOG~** 

### TO BE 

### HIGHER (OR LOWER) TF.JI..,'l STATED, P...!..L OTHER READINGS WILL BE 

### HIGHER (OR LOWER) TO TEE SAHE EXTENT.

TEST NUMBER: 155404 DATE: 04/22/97 STANuARD SERIAL NO. 48511 NIST.**IDENTIFIC~T!ON** 

### NO. 92564
E-32

# _e__._~~k'~/

# __{ ______ Charles Tang-Nian // 

### QUALITY CONTROL MANAGER 

# ;t/.3

# Bulletin 0-01-82


# NATIONAL WEATHER SERVICE TYPE MERCURIAL BAROMETERS Usable up to 900 metres (3,000 feet) Tne Naticnal Weatr:er 

### Sar,ica :yce ::=arcme!s-r is

**.P~JNCO's** Mighest g:-ace ,--r.erc:.;riai
**:arc~er:r.** It is '.JSec' ::y weat:-:er sar1ices ar.C air;:cf""':s

**~r:e** wcr!c ever. Tne ·;lass :uce ;"':as a :..1r.ifcrm insiCa Ciarr.et:r of 7 mm

**~or** c::nsrant caoilrary

**~ecress:cn** tr:rcugncut 

### :ne len<;th oi the scale. Scales are set at the fac:o'Y

**~Y** ccmpanson with a barometer csrtirleC Cy tr.a

**i'\Ja~fcnal** Sureau ::f StatlCarC:s. ar.d read :r.e local pressure

**witr.o~t** the necessity ol correc:in<; fer capiilal"f decress;cn. The vern1er can :=e smccthly and prec1sely set by means oi a rae:< and ;::inion

**~.we.** c:::ntrcllee :y a <nurlee adjusting :<nee. White ;::lasctc bac!<<;rouncs en 

### :r.e mounting .oanel fac;litate observation ol the Fcrtm :YJ:e c:ster:1 anc
**merc~l"f** column. 

### Tne vem:er .'1as a s1ghting eege. frcnt ai'C rear. tc avcid J:arallax. A sus::ensicn

**brac~<et** anc an
**aC:fus~ac!e nn~**  ·.::amp .'or the

**c!s~am** hc!C: tr:e !:aromerar firmly in the ver::ica! :csit:cn en :r:e
**mcut:rir.~** panel. A C(;aJ scale Cels;us/Fahrennelt merc-:cmetar 'Nith a -25 to 50 "C/-10 :o 120 "F

**ra~<;e** indicates the proper temperatura to t:e usee

**~~cr** tem.cera[TJre cor:-ec:ior.s. An

**ins~rtJc!icn** :cck!et witr: infcrma!icn

**~or ur.terstanc::n~**  and .orccer use of tne barometer is supcliee with eac:O instrument Ccmctete

**ccrrec~cn** tables tcr temperatura and ;ravity ara includee. Tms Oarcrr.eter is ac::::...tra!s

**~c** ::0.3 me. 0.2 r:-:m. or 0.01 inc:"! of merCI.ll"f wnen carefullv set and read. and after tem.cerature and gravity c:::rrec:icns :,a,,e

**~een apcli~.**  For graatest ac::urac·; a Cert1iicate 

### or Calit:raoon may ce obtainee al'd the ccrrecdcn containec there1n also apciiee. Eac:1 NaacnaJ Weather Service barometer has a serial nurr:t:er. The rug<;ec construc:ion of the NaticnaJ Weather Service type barometer is sue:-:

**t.~at** it can be s.'11pcec safely by Un1tec Parcel Serv1ce or excress. Tne kidskin bag, in the For:in tyee reservoir, dampens mercul"f column oscmaoons during shipment Tne lower part of me glass tube is narrcwee dcwn to minimize mercul"f weight. anc is protec:ec by fcam cushions. tnus offering accee resistance to damage dunng st1icment. Tne cistern may be

**~enec** in the field fer cteamng of the cistern glass and c;s:em mercul"f.The barometer contains accroximately

### sao grams (1.5 pounds) ct mercul"f total. It is ;n1ppec completely assemc1ee. filled with :nerc:..r; and reacty to use. Mcunt1ng panel dimensions are 19 x 76 x 1072 mm (3/4 

### x 3 

### x .12

**1nc.~es).** The shipping we1gnt is 5 k<; (11 pounds) and box dimensions are 235 x 250 x 1197 mm (9 x 10 x 47 inc:1es). Catalog Number

**~453** 45381 453MB

E-33 Scales

**inc.~** and millimetre

**inc~** and millibar millibar and millimetre 

### ents

# 00

**~-**

**{-"'"~'-~--\** :';

**~\** '1o :.. '0 , 

# -

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# sartcj>rius BALANCE CERTIFICATE of 

# CAIJBRATION CL'STOME..q;



### ~,.,c C\.. CERTIF1C\.TE #: 

# S20-15813 ( Z.CC



## ·r~'-' **~~':.\'='c.\.,** \)\vc:\DATE OF CALIBRATION: 

## 2. !2,-[ 

### !"'.'f C\,\clv



### \_~ "' C



### -z._<;-.z_~.'\ NEXT CALIBRATION DCE: '2_ 

## .'"-,''C 

# ---===--:-;::::::::;;=...,,------ DEPT: L'\/VlRONMEYrAL CONDITIONS:



## ·~,:O~e'~' 'eoc•i 

## This 

# certifies that the test 

# weights used are traceable to 

# the Natianal Institute ofStandards & 

# Technology Sartorius Weight set ID#: _'L,

**~_l·--=-<::,~?-,._~-'----------** 

# Calibrated to Class: _,0-=.",:,:,.....________ _ 

# Date weight set calibrated: ____,z_=---,_t w-'-·.

## _c_:-\._:'l'--------- 

# Date weight set due: N.I.S.T. Test number: CORNER LOAD ERROR WEIGHT USED: TOLERANCE \'- ") "''':) : 

# -

- 

# A B



# ~s I 

# n* " A B 

## I 

# c TOl.E;(ANCE 

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FROI:'<'T *:-lot applicable ro circular pans 

### LINEARITY CHECK: • RANGE: 

# - '

**~~** TOLERANCE.- ' 

### ., N e: "'-' RA G" TOLERANCE IN IN 

### Nominal Value Before Adjustment TOL.BlANCE 

### After Adjustment 'C\..ffiANC:E 

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## Date

**l~l** He3.rtiand B . Ed ewood

**N~** 7 7

g • Yor ll l (800) 545-3108 (516) 244249 Fa.:'<: (516) 254-4252 E-34 

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# It/)

# sart<j>rius BALANCE CERTIFICATE of 

# CALIBRATION

DEPT.:----------- 

# This certifies that the 

# test weights used are traceable to the National Institute ofStandards & 

# Technology Sartorius Weight set ID#:

**IC(S~ ~**  

## Calibrated to Class: Date weight set calibrated:

**--="::._-_:'-_:'-1.~--q_~'l.:..._**

## ______ _ 

## Date weight set due: 

# a- \'-I - 

# Ci.'C, 

# N IS T T t 

# b 

# '2..b2.-\

**?.S''-V--L~O** 

## . . . . es num er: t WEIGHT US"D c : TOLERANce+

**~:** 

# -



# ~I I 

# n* N 

# I A 

## B 

# c TCl£ilANC; 

## Y Ni I I I 

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## BEFORE ADJ. 

# I& -& 

# 1-B



# I~ I'-" I 

# I AFTER ADJ. 

# -s-j-G I-s

# r[1 I 

### LINEARITY CHECK: RANGE: I I 

### \ · DOG "'- TOLERANCE:- • ""'C 

## Naminal Value Before Adjustment 

## 2CJ c. 

## t.-..0.oao_3 

# 50 

# ;;: 50::::. . 

# aaCYl 

# 'lO 

# ? ;lG.

**Ooc::.~** 

## LOu 

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# ---7 'C\----\



# \)~~**~** 3-5' Q;ln:orius

**~Sen**

**~ce** 

## ReJ :fesentative 131 Heartia.n.d Ed<ewood·



# N~ 11717 (800} 645-3108 (516) 254.4249 

## Date '" TOI.EJt'.NCE 

## YN j./



## v IV' 

## Jv'

**-~1** 

## *:-io< applic:able w circular pans RANGE: TOLERANCE: 

## After Adjustment

2._O,oc:.oc. 

# '3U -GOe,\ 

## 'l 0 . 0<:,() \ 

## laG , **~a** I 

## I 

# I

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## YN '....-' 

# , ........ 

# ,....... ,......}--

Fax: (516) 254.4252 E-3:' REF S2CCO 195

# _W_e_ig.;__n_' t_C_af_i 

# b_r_a_tJ_·o_n_C_e_rt_i_fi_ca_t_e __

# ~~ -!Me- r121Jt1 

### SECTION 1: NA... 'v!E . **.>u~L)** 

### ADDRESS OF Ct;STOMER Sartorius Corp 8106 Counrrv Oaks Rd Charlotte NC 28227 Page 1 of7 Pages Certificate Number: 94962

· **SECTI~A.PPROvcD** 

### SIGNATORY 

## /



# ~--:. **-~-**

**~**

# o--?v·

# 4c.::,

**~-----** Robert Thompson 7 

### SECTION 3: PERSON PERFO&'.-llNG WORK Gayle Carsey SECTION 4: CERTIFICATE INF0&\1ATION Description of :V!asses: Troe=er Sartorius lOOg-lmg Weight Set Class 1 

### Accuracy Class Order Number Construction Material Serial Number ASTM E617-91 Class 1 

### S31705 One Piece, Two Piece Stainless Sreel Stainless Steel (mg) Aluminum 19333 Dare Received Date ofCalibration Date ofIssue Weight Range
SECTION 5: ENVIRONMENTAL CONDmONS DURING TEST 13-JAJ.'<-1997 14-FEB-1997 14-FEB-1997 1 gram 

### & 

### greater 500 mg- 50 mg 30 mg & 

### below Temperature: 22.00°C Pressure: 774.48

# = Hg Relative Humidity: 44% SECTION 6: PERTINENT INF0&\1ATION The Weights listed on this calibration report have been compared to reference mass standards that are directly traceable to the National Instirure of Standards and Technology under Test No. 822/254480. Reference standards and balances used to 

### perform the calibration are listed in Section 10. The weights calibrated for this 

### report have been calibrated in accordance with Troe=er's calibrationprocess. The calibration performed meets Level I criteria as described in the NIST/NYLAP Technical Guide 150-2. This calibration also meets specifications as outlined in ISO 9001. ISO Guide 25. AJ.'<SIINCSL Z540-1-1994, NCR Document 10CFR50 Appendix B, and applicable documents.
This certific:ue ofc::tlibrJ.rion shalt not be reproduced except in full. 

### wirolithe written approval ofTroemner. Inc. This certificate of c::tlibr::trion musr not be used by the customer :o c!::tun product endorsemt:nt by :"lvtAP or Jny Jgency of the U.S. government. 

# it/7

# 7ROeMNER

**-~.....:; ;~""**  _,- 

# Weight Calibration Certificate 

# §:.4..;

**--------~~---------------------------------------------------------------------- ------~**  NA.i'v!E

**A.t~D** 

### ADDRESS OF CUSTOlYIER Sartorius Corp Plge 

### 2 of 7 Pages 8106 Coumrv Oaks Rd Charlotte NC 28227 Cer.ificare Number: SECTION 7: MASS IN A VAC1.Jl.TlY1 (TRUE MASS) CALIBRATION DATA Nominal Serial Mass Value Number 100 q

50 q 20 q 20 q 

### • 10 q

5 q 2 q 2 q 

### • 1 q 500 mg 200 :ng 

### • 200 mg 100 mg

50 mg 20 mg • 20 mg 10 mg

5 mg 2 mg 2 mg • 1 mg

l Density is Jssumed unless olherwise stated • Denotes weight is mJ.r!ced wuh a doc 

### ---- Mass 

### in Vacuum ------ As Found As 

### Left 100.00022738 q 100.00022738

50.00014405 g 5J. 00014405 20.00005846 g 20.00005846 20.00007663 q 20.00007663 10.00001712 g 10.00001712

5. 00001542 q 5. 00001542 2.00001906 g 2.00001906 2.00003807 q 2.00001647 l.00002740 q 1.00002740 0.49999957 q 0.49999957 0.20000545 q 0.20000545 0.20001228 g 0.20000112 0. 09999479 q 0.09999479 0.05000362 q 0.05000362 0. 02001431 q 0.02001431 0.02001798 q 0.02001131 0.01000644 g 0.01000644 0.00500716 q 0.00500716 0.00200529 q 0.00200529 0.00199295 q 0. 00199295 0.00100800 g 0.00100800

[-37 

### Densirvl ofWeighr g 7.8500 q/c:n.3 g 7.8500 q/c:n.3 q 7.8500 q/c:n.3 g 7.8500 q/c:n.3 g 7.8500 g/c:n.3 q 7.8500 q/c:n.3 q 7.8500 g/c:n.3 q 7.8500 g/c:n.3 q 7.8500 q/c:n.3 g 7.9500 q/c:n.3 g 7.9500 g/c:n.3 q 7.9500 q/c:n.3 q 7.9500 q/c:n.3 q 7. 9500 q/c:n.3 q 2.7000 g/c:n.3 q 2.7000 q/c:n.3 q 2.7000 q/c:n.3 q 2.7000 g/c:n.3 q 2.7000 g/c:n.3 q 2.7000 g/c:n.3 g 2.7000 g/c:n.3 -t..c-tiBQ1.2.



### 94962 uncenaimy 0.0774: :::g 0.0395 :::.g 0.0345 :ng 0. 0345 :::g 0.0254 mg 0.0063 :::g 0.0037

**:~>g** 0.0115 :ng 0.0036 :::g 0.0025 :ng 0.0022 :ng O.OOlS :ng 0.0027 :ng O.OOH mg O.OOH mg 0.0022 mg o.oo:4 mg 0.0015 mg 0.0013 mg 0.0013 :ng 0.0022 :ng

# TRO!:MNER
· .**..:~~~7-:**

# /-"'' 

# Weight Calibration Certificate**~~ ------~:-----------------------------------------------------------------------~~~~** **....-e-a~---.,**

- tM'C::dr**'ta7T~** 

### NA..t'v!E Ac'ID ADDRESS OF CUSTOMER Sartorius Corp Page 3 of 7 Pages 8106 Country Oaks Rd Charlotte NC 28227 Certificate Number: 94962 SECTION 8: MASS 

### IN AlR 

### CALIBRATION VALliE VS. REFERE:-.ICE DENSITY 8.0 gicm3 Nominal Serial -Conventional Mass Value ---- Mass Value Number As 

### Found As Left Uncertainty Tolerance 100 g 99.9999407 g 99.9999407 g 0.0774 mg 0.2SOOOO :ng

sa g 50.0000007 g S0.0000007 g 0.039S mg 0.120000 mg 2a g 2a.aaooou g 2a.aaaoou g a.a34S mg a. a74ooo mg 20 g 

### • 20.000a193 g 20.0000193 g a.0345 mg 0. 074000 :ng 1a g 9.999988S g 9.9999885 g 0.02S4 mg a.asaaao mg

s g s.aaoao21 g s.aaaoo21 g a.a058 mg 0.0340a0 mg 2 g 2.000a133 g 2.0000133 g o.aa37 mg a.03400a mg 2 g 

### • 2.0000323 g 2.000a107 g a. allS mg 0.034oaa mg 1 g 1.aaaa24S g 1.a000245 g a.aa35 mg a. oHooo mg sao mg a.4999991 g a.4999991 g a.aa25 mg 0.01aOOO mg 2aa mg 

### • a.2aaoos3 g a.2aoaos3 g a.aa22 mg a.alaooa mg 2aO mg a. 2aaa121 g 0.2aooao9 g a. aa18 mg a.o:ooaa mg 1aa mg a.a999947 g a.a999947 g a. aa21 mg O.Oloaaa mg

so mg a.asaaa35 g a.asooa35 g a. aau mg a.a1aaaa mg 20 mg 

### • a.a2aaa84 g a.a200084 g a.aal4 mg 0.01aooo mg 20 mg a.o2a0121 g 0.0200aS4 g a.aa22 mg 0.01aaoo :ng 1a mg a.a1aao35 g a.a1aa035 g 0.0014 mg 0.010000 mg

s mg a.aosoa57 g a.aasao57 g o.a015 mg a.a1aaoo mg 2 mg a.ao2aa47 g a.aa20047 g 0. aa18 mg a.Olaoao mg 2 mg • o.aa19924 g a.oa19924 g a. aal8 mg a. 01aooa mg 1 mg a. aa1aan g a.aa1a077 g a.oa22 mg a.Oloaao mg

E-38 • DenQ(eS weight is marked with a dQ(.-- 

## ..;-, /.



# _v.,...-Ve_j~g_h_t_C_a_f_j 

# b_r_a_tI_·o_n_C_e_rt_j{_j 

# c_a_t_e__**~~** -UDc- rOIII:nl.


### NAJ.vlE AND ADDRESS OF CUSTOtvlER Sanorius Coro Page 4 of7 Pages 8106 CoumriOaks Rd Charlotte NC 28227 Certificate Number: 94962 SECTION 9: :YIASS IN AIR CALIBRA.TION DATA VS. REFERENCE DENSITY 8.0 g/cm3 Nominal Serial
- Conventional Mass Correction -- Mass Value Number As 

### Found As Left Uncenainry Tolerance 100 g -O.OS93 mq -O.OS93 mg 0.0774 mg 0.2SOOOO :ng

so g

**~0.0007** mq +0.0007 mg 0.039S mg 0.120000 :ng 20 g +0.0011 mq +0.0011 mg 0.034S mg 0.074000 :ng 20 g 

### • +0.0193 mg +0.0193 :ng 0.0345 mq 0.074000 mg 10 g -0. 011S mq -0.011S mg 0.02S4 mg o.osoooo mq

s g +0.0021 mq

**~0.0021** mg 0.0068 mg 0.034000 mg 2 g +0.0133 mq +0.0133 mg 0.0037 mg 0.034000 :ng 2 g 

### • +0.0323 mq +0.0107 mg 0. OllS mg 0.034000 :ng 1 g +0.024S mq +0.024S mq 0.0036 mg 0.034000 mg soo mg -0.0009 mg -0.0009 mg 0.0026 mg 0.010000 mg 200 mg • +0.00S3 mg

**~o.OOS3** mg 0.0022 mg 0.010000 :ng 200 mg +0.0121 mq +0.0009 mg 0. 0018 mg 0.010000 mg 100 mg -O.OOS3 mg -O.OOS3 mg 0.0027 mg 0.010000 mg

so mg +0.0036 mq +0.0036 mq 0.0014 mg 0.010000 mg 20 mg • +0.0084 mg +0.0084 mq 0.0014 mg 0.010000 mg 20 mg +0.0121 mq +0.00S4 mg 0.0022 mg 0.010000 mg 10 mg +0.003S mg +0.003S mg 0.0014 mg 0.010000 mg

s mg +0.00S7 mg +0.00S7 mg 0.0015 mg 0.010000 mg 2 mg +0.0047 mg +0.0047 mg 0.0018 mg 0.010000 mg 2 mg • -0.0076 mg -0.0076 mq 0.0018 mg 0.010000 mg 1 mg +0.0077 mg +0.0077 mg 0.0022 mg 0.010000 mg

E-39 • Denmes weight

**~s** marked with ::1 Jot

## ----- ·' 

# vVejght Calibration Certificate

**::.4..~**

**---------=~---------------------------------------------------------------------~--~~** NA.v!E A."'D ADDRESS OF CUSTOi.V!ER Sartorius Corp 

### 8106 Counrry 

### Oaks Rd Charlorte NC 28227 SECTION 

### 10: CALIBRATION PROCEDURE DATA Nominal Serial Standard Balance Mass Value Nwnber Set No. Used 100 g S007 AT106-007

50 g. S007 A':'l06-007 20 g S007 ATl06-007 20 g 

### • S007 AT106-007 10 g S007 AT106-007

5 g SOl3 1lM'l"5-013 2 g S013 1lM'l"5-0l3 2 g 

### • soo8 MT5-008 1 g S0l3 1lM'l"5-013 500 mg soo8 MTS-008 200 mg 

### • soo8 MTS-008 200 mg soo8 MTS-008 100 mg soo8 MTS-008

50 mg soo8 MTS-008 20 mg 

### • soo8 MTS-008 20 mq soo8 MTS-008 10 mg soo8 MTS-008

5 mg soo8 MTS-008 2 mg soo8 MTS-008 2 mq • soo8 MTS-008 1 mg soo8 MTS-008

• Denou:s weight is marked with l dot ..-Lata-rQSM.1.


### Page 5 of 

### 7 Pages C<!rtificate Nwnber: 94962
Procedure Finish Used Grade Type 3-1 Modi:!ied 3-1 Modi!ied 3-1 Modi!ied 3-1 Modi!ied 3-1 Modi!ied 3-1 Modi:!ied 3-1 Modi!ied 3-1 Modi!ied 3-1 Modified 3-1 Modified 3-1 Modi!ied 3-1 Modified 3-1 Modi!ied 3-1 Modi:ied 3-1 Modified 3-1 Modified 3-1 Modi!ied 3-1 Modified 3-1 Modi:ied 3-1 Modi:ied 3-1 Modified

# 7ROEMNE:R

-:-_---. # -

**~--'** 

# Weight Calibration Certificate

**~~ --------~----------------------------------------------------------------------------** 
NPuY1E A . .;'lD .WDRESS OF CUSTOMER 

### Sanorius Corp 8106 Coumrv Oaks Rd Charlotte NC 

### 28227 SECTION 11: GENER.-\1. INFOR.'<fATION -lMC..

**r~Sr.L**


### Page 6 of 7 Pages Certificate Number: 

### 94962
This calibration was performed in Troemner's High Precision Level I Mass Metrology Laboratory at 6825 Greenway Avenue, Philadelphia, Pennsylvania 19142 unless otherwise noted on page one. 

### SECTION 12: 

### DEFThlTIONS Pu'ffi TER.\-IS MASS IN A VACUt:M -The mass of a weight as if it were measured in a vacuum. Also known as True Mass. MASS IN AIR- Is the mass value of a weight based on conventional mass versus material density 8.0 g/cm3 at 

# zo• C with air density of .0012 g/cmJ. This value takes into account the buoyant effect of air on the weight. The Mass in Air values are reported as corrections above or below nominal value in the calibration report. AS FOUND MASS IN AVACUUM - The estimated value ofthe mass(es) as they were received by Troemner. If the customer requires cleaning prior to calibration, the after cleaning value would be reported. AS LEFT MASS IN A VACUUM - The estimated value ofthe mass(es) after they were adjusted, repaired or replaced when necessary. The As Found Mass in a Vacuum will equal the As Left Mass in a Vacuum if the mass(es) did not require adjustment, repair or replacement. NOMINAL MASS - The mass value as marked on the weight. CORRECTION - the difference berween the mass value of a weight 

### and its nominal value. A positive correction indicates that the mass value 

### is greater than the nominal value by the amount ofthe correction. AS FOUND CONVENTIONAL MASS CORRECTION- The estimated correction ofthe mass(es) as they were received by Troemner, taking into account the buoyant effect ofair. 

### Ifthe customer requires cleaning prior to calibration, the after cleaning value would be reported. The correction 

### is based on mass in Air. AS LEFT CONVENTIONAL MASS CORRECTION -The esrirnated correction ofthe mass(es) after they were adjusted, repaired or replaced when necessary, taking into account the buoyant effect of air. The As Found Conventional Mass Correction will equal the As Left Conventional Mass Correction if the mass(es) did not require adjustment, repair or replacement. UNCERTAINTY- The error in assignment ofthe correction due to the measurement process. Uncertainty is calculated per NIST Technical Note 1297 using a coverage factor ofK 

## = 2 ( K 

## = 2 defines an interval having a level of confidence of approximately 95 percent). TOLERANCE - Defines the limits in which the correction value must fall to meet the tolerance specification for the.given Class. (continued on next page) E-41

# !·zrr. 

# Weight Calibration Certificate §::.#_:;

**--~--~~------------------------------------------------------------------ --~d~** 
NAJ.viE AND ADDRESS OF CuSTOiYIER Sanorius Corp 8106 Counrrv Oaks Rd Charlotte 

## NC 28227 SECTION 12: DEFL'fiTIONS AND TER.VIS (continued) .... **~c-t~**


### Page 7 of7 

### Pages Certificate Number: 94962
AS FOUND CONVENTIONAL MASS VALUE- The estimated value ofthe rnass(es) as they were received by Troemner, taking imo account the buoyant effect ofair. If the customer requires cleaning prior to calibration, the after clean value would be reponed. AS LEFT CONVENTIONAL MASS VALUE- The estimated value ofthe mass(es) after they were adjusted, repaired or replaced when necessary, caking into account the buoyant effect ofair. The As Found Conventional :V[ass Value will equal the As Left Conventional Mass Value 

### ifthe rnass(es) did not require adjusrmem, repair or replacement. 

### SECTION 13: ADDENDUM Next Calibration Due Dace:8/14/98 Regina McHale Krishna Bishnach

E-42

# ..

**~** JamesA.Graham



## ..;-~ -----


## ~arl~ a!arnlimx

comnu.,,on,. 

# \...):s::;_,__..--

**~eparlnumt** 

## af ci\gri.culture



# --

-- 

### ~tzmllm-11!5 **~**

### iDil5iun N. David Smith Direcroc 

# CERTIFICATE OF TRACEABILITY AND 

# REPORT OF CALIBRATION
The standard(s) described on the following page have been compared to 

### standards of the State of North Carolina and have been found to have values as listed. Traceability to the National Institute of Standards and Technology, NIST (formerly The National Bureau of Standards, NBS) is via the NIST test number listed on the report. Adjustments of precision laboratory standards are not recommended. Therefore, no adjustments have been made to these standards and certification to any tolerance classification is neither stated nor implied. The user(s) ofthese standards should examine the deviation from nominal value and the associated uncertainty to ascertain ifthese standards meet their precision requirements. The uncertainty is an expression ofthe overall uncertainty using three standard deviations as the limit ofrandom errors ofmeasurement plus the uncertainty of the State Standard used in comparison. The primary testing methodology used is the Double Substitution Method, NIST Handbook 145, 

## Handbookfor the Quality Assurance of Metrological Measurements, SOP number 4. Three double substitution weighings are averaged to arrive at the listed value.

# NORTH CAROLINA DEPARTMENT OF AGRICULTURE JAMES A.

**GRAHA...~** 

### COMMISSIONER OF AGRICULTURE 

# STANDARDS DIVISION P.O. BOX 27647, RALEIGH, N.C. 27611 (919)733-4411 

### N.DAVIDSMUTH,DlllECTOR 

# STATE:MENT OF TRACEABILITY SUBMI'IIED BY: Trigon Engineering Consultants 1920 Starita Road, Suite J 

### Charlotte, NC 28206 DATE OF TEST: September 24, 1996 TEST NUMBER: NC0996W052 TOLERANCE: ASTM Class 

### 4 PO NUMBER: AM7275 DESCRIPTION: One (1) Set of Ohaus (brand) Weights, Serial Number 6640 1 • 50 g weight 1• 200 mg. weight 1• 30 g weight 1 • 100 mg weight 1 • 20 g weight 1 • 50 mg weight 1• 10 g weight 1• 20 mg weight 1 • 5 g weight 1 • 20 mg. weight 1 . 3 g weight 1 • 10 mg weight 1• 2 g weight 1 • 5 mg weight 1• 1 g weight 1• 2 mg weight 1• 500 mg weight 1• 200 mg weight The items described above have been compared with the standards ofthe State ofNorth Carolina, and are traceable to 

### the National Institute ofStandards and Technology, NIST via 

### the test number shown above. All tests were performed in 

### the North Carolina Standards Laboratory. Environmental conditions are maintained at a temperature of2ZOC 

## ± 2°C and a relative humidity of50%± 10%. 

# J4L METROLOGIST L.F. Eason Sherry Teachey Sharon Denning Van Hyder Karen 

### Bryan page l Ori,UW C.:rtific:atc Has The NCDA Seal Emboued Above Fn.ENAME: F:IOROUPS\ST ANDLAB\Fll.ESYSI TRIGON\199610996W052.WPD 

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### Greensboro \ronh C,lroltnd

336-668-0093 

### Trigon Services • Geotechnical Engineering • Construction Materials Engineering/Testing • Roof Engineering/Inspection • Forensic Engineering • Environmental Audits/Site Assessmerts • Environmental Drilling • Groundwater Studies/Remediation • Storrnwater Permitting • Water Treatment Design • Mechanical Engineering • Waste Minimization Studies • Air Permitting • Atmospheric Computer Dispersion Modeling • Stack Testing • Indoor Air Monitoring



## OFFICE LOCATIONS Raleigh l\:llrth Carolina 919-755-5011 

### Charlotte Nurth Carolma 704-598-1049 

### Greenville South Carnllna cJ64-2n-Js57 

### /