, . '-." ' .. - , '
, 

# TOTAL 

# CHROMIUM**E~SSIONS** 

# REPORT'

AIDeftaed

### By TIle-

.. Codeofll'eclenlRepJatfoas; 

### Title 40

### Part

# ctl.

RMCEINC Project

### ##2006-13527

ARMOLOY CORPORATION CHROME SCRUBBERS til '"

### ##3 DEKALB, ILLINOIS



### PREPARED FOR: ARMOLOY CORPORAnON
BY:


### RMC ENvDtONMENTALt INc.

- CHICAGOREGIONAL OmCE

### Armoloy Corporation DeKaIb, 

# minoa

REPORT CERTIFICATION 

### RMCElNC-Cbfeago Regional 

## Omce Project#2006-13517

The sampling, analysis, 

### and 

### data 

### collection performed for this 

### report 

## were canied out 

### under 

### my direction and 

### supervision. and 

### I 

### hereby 

# catHY that

### the testreport 

### is 

### authentic and ammdc, 10

### the 

### best 

### ofmy

### knowledge.

### Armoloy CorporatioD DeKalb, 

# mino.

TABLE OF CONTENTS RMCEINCChlcago 

### RegioDaI 

## Omce Project

### ##2006-13527



### 1.0 PROJECfIN'FORMATION •.•.. 1.1

.......................... _ .................................................................... '1 

### 11.1.1 1.1 COl\;U»ANY INFORMATION

....................................................................................................................................... 1 

### 1.2 

### TEs11NO FIRM 

### INFoRMAnON

................................................................................................................................. 1 1.3 TEST 1NFORMA11ON

.................................. •

...........••

...•••

..•

..•

..•

..••

............................................................................. 1 

### %.0 SO'URCE mEN'TD'lCATION••..•....•••••..--................................-._......................................--..........................2 

### 3.0 SUMMARY AND DISCUSSION OF RESULTS. I

.....

### 2 

## 4.0 POUUTANTSAND TESTMETHODS_.

.. ......... I

......... IU

.............. , 

### .2
5.0 

### TEST PROCEDURES AND RESULTS

...____ ...**~**

### ....**~I1~** .. ".'

...

'

...**~II_** .... Il

............... _ ..... _ ....

, ..................................................... 11

..... _ ••

_ ............ 11

.........

'

.............. ___

### 2 S.10 

### SAMPImO

### PROCEDtJRES. ••.••••.••••••••••..•••••••..•..•••..•.•.••.•••.••..••••••.•••.••..•••••••••.•••••••••••..••.••••••..••..••••.••••.•••••••••••.•••••••2

5.11 

### 'Y olunretricFlawRota

....................................................................................................................................

### J 5.12 CIIROItIJUM CONCEJlI'RA770NS

..........................................................................................................................

### 3 5.20 

### FJELD DATA 

### SHEETs

.............................................................................................................................................3 6.0 EQUIPMENT

### CALIBRATIONAND QUALITY ASSURANCE

.........n
......... n. , n 

### .3 

## APPENDIX As 

## TEST SUMM.4aY SHEETS

........, ... II. I. I

...."

........................... II .,. 1•• I I Il"" , •• , •••••• , • 

### •

.. A TarALCHROMIUM REsULTS SUMMARY

........................................................................................ :

............................A 

### ,APPENDIX B. 

### FIELDDATA**~ETS-.-.......**

### ........._........" , •••.

_....................-.-................................................. B M£n.IOD 1 • DATA

### SIIEEl"

...........................................................................................................................................B ME'nlOIlS 

### 1-5 DATA 

### SfIEE'I'S

.......................................................................................................................................B 

### APPENDIJ( C. 

### ANAL'Y'I'ICAL »ATA I. "'."'1•• "'1 ••••••••• I", II II '1," '" J 

# ........................ ., .. D 

## APPENDIX: D.

## T'FS1' oNOC'**fPRMS..~.,.,I.** 

# I. ,".,....•..... I

.. ,

......, .."

..1

......--............_ .........................................D PRETEsr&: PosTTEST • 

### MElERBox CALlBRAnON

.....................................................................................................0 

### PrrarlNSPECTION
I •••••••••••••••••••• , .................................................................................................................................

### C

### Armoloy Corporation DeKaIb, 

### DUaols



### 1.0 PROJECI' INFORMATION

1.1 

### Company Informatioa

Name and 

### Address:

Contac:t: 

### Telephone Nwnber:

Source 

### Tested: PermitNumber:
1.2 TestiDg FIrm 

### latormatioD Name 

### and Address:

Contact 

### Telephone Number:



### 1.3 Test InformatioD TestRequested 

### By: Source CoDtact 

### TelephOile Number: 

### TestObjective: Test Methods: TestDates: .EPA I 

### State Represen1atives 

### On-site: Source 

### Test Coordinators:
TestPersonnel:



### Other

### TestPersonnel: Armoloy Corpcr.ttion 114 Simonds Avenue 

### DeKalb. Illinois 60155 

### Mr. William Cor2ene 

### 815-758-7486 Phone ArmoloyLab@msn.com 

### RMCEINC-Chfeaao Regfoaal Oftlce Project#2006-13527

Hard Chrome 

### Taok Scrubbers

- CMP Scrubber

### #2 &; 

### #3 95120329



### RMC f'.NVIRONMFNrAL, 

### INC. 

### 9226North

# -rStreet 

### Machesney

### Park, Dlinois 

### 61115 Gregory Chleborowicz

. 

### 815-318-6155 Direct 

### 800-S32-3391 Voice Mail 

### RMCEGREG@aol.com

ArmoJoy 

### Corpondion 

### Mr. William Comne 

### 815-758-7486 Phone 

### Total ChromiumCompliance Test EPA Methods 

### 1-4.&306 February 28 &: 

### March 1.2006

William 

## Corzine Armoloy Corporation
Eric QWncy 

### RMCEInc Tony SegalJa 

### RMCElnc Andrew 

### McDennand RMCEInc

Ii 

## Page 1

### Armoloy CorporatioD DeKaJb, lDiDois



### 1.0 SOURCE IDENTIFICATION



### Name andAddress:

Contaet: 

### TelephoneNumber:

Source Tested: 

### PermitNumber: Annoloy Corporation 114 Simonds AVeIlue 

### DeKaJb. IDiDois 60155 

### Mr. 

### William COI7.eDe 

### 815-758-7486 Phone 

### AnnoloyLab@mso.com RMCEINC-chfcago RegIoual 

### 0fIlc:e 

### Project 1Il006-13!27

Hard 

### Chrome Tank Scrubbers

- CMP Scrubber

### #2 & 

### #3 95120329

3.0 SUMMARY AND DISCUSSlON OFRESULTS The 

### RSUIIs of the emissions 

### retesting performed on the 

### large chrome 

### tank stacks are preseoted 

### in Table 2-1. 

### Detailed 

### results 

### ofall 

### of1he 

### testing 

### completed on this 

### location are located 

### in Appeadls A. The 

### field data 

### and the analytical results 

### are 

### pn:sented in 

### Appendis B aDd 

## C. n:speaively. 

### Calibration sheets 

### and 

### equipment performance 

### checks are presented 

### in Appendix D. along 

### with 

### the cbain 

### ofcustody. 

### Acyclonic flow 

### chec:kwas 

### conduc:ted and DO 

### cyclonic flow 

### auomalies 

## were noted. As indicated by 

### the average oftile

### three**~** 

### the 

### tested

### resul1s were below the 

### MACl" regulation standards 

### fornewly installed 

### chrome plating 

### uniIs of0.015 mglDSCM 

### for composite mesh pad 

### scrubber systems 

### onbard chrome platina 

### tanks.

LocatioD Saubber

### Unit#2



### ScrubberUnit#3 TABLEl-t 

### SUMMARY OFTOTAL CHROMIUM RESULTS Armoloy Corpontioa February 18'"

### March 1,2006



### TestParameter Result 

### S 

# .- R 

# mWOSCM 0.0042 

## =s 0.015 mglDSCM 

### forbard

### chromeplating 

### sources Flow rate

### ·DSCFM 15,574 IbIHr 

### 0.00005 

## m&'DSCM 0.0047 !S 

### 0.015 mglDSCM for 

### hard 

### chromeplating 

### sources 

### Flow rate 

### DSCFM 16.849 lbIHr 0.00003

4.0 POLLUTANTS AND TESTMETHODS 

### PoUurantTested: Total Chromium 

### EPA Method 306

- 40 CFR 60, Appendix A
5.0 TEST PROCEDURES AND RESULTS

5.10 SampUng Procedures Testing 

## was completed per EPA 

### test methods 1.2.3, and 306 defined in 

### 40 CFR Part 60 

### Appendix A. The 

### sampling and analytical 

### requirements for 

## this proaram include the 

### determination of total chrome. O;iCOz, moisture and

I. 

## Page 2

### Armoloy CorporadOD 

### DeKaJb, DUnois 

### RMCEINC-Chieago Regfoaal Omce Project**#l~13S27**



### volumetric flow rates 

### from the stack 

### etnuent The plating 

### processes were operated at 1000.11 

### capacity. 

### The specific equipment 

### andprocedures that WeR

### used are 

### detailed below.

5.11 Volumetric flow Rates 

### RMCEINC determined 

### the 

### number and location of the traverse points for volumetric flow rate IIle8SURIJmlt 

### acconting to 

### tho procedures 

### outlined in 

### EPA Method 1. When determining 

### the loc:ation and IlUIDbeI" 

### ofsample points, 

### RMCElNC took into 

### account the number 

### ofsample ports, duct 

### configuration, and localion 

### of

## upsaream and 

### dowustream flow 

### cUstmbances. The 

### flue 

### gas velocity and

### volumetric tJow rate 

### were detennined accordiDg to 

### the proc:edures 

### ofEPA Method 2. 

### A**~** 

### S pitot 

### tube with 

### a Type 

### K tbcrmocouple (EPA Method 5 Sample Probe) 

## was used to 

### measure velocity pn:ssure 

### and 

### stack gas b:mpelature 

### at 

### each 

### sample point. Each 

### pitot 

### tube conformed to 

### the geometric specifications 

### ofEPA Method 2 and was 

### assigned a coefIicieDt 

### of0.84. An 

### mnbilic:al 

### cord 

### cozmec:ted the pilot 

### tube to 

### the 

### meter box 

### inclined manometer 

### and digital 

### temperature 

### readout. 

### RMCEINC leak-checked the pilot

### tube prior to 

### conducting 

### the 

## traverse aDd at

## random points 

### during the test. 

### RMCEINC determined the 

### flue gas composition and molec:uJarweight

### using EPA Methods 3 aud

### 4proc:edures. 

### S.12

# mcConeentratioDi The total chrome 

### samples 

### were drawn isokinetically 

### from the source usiDg 

### an EPA method 306 sampling Crain. 

### The sampling 

### train 

### consisted ofa glass 

### nozzle aad 

### probe liner, aD 

### attached Type 

### S 

### Pilot tube, 

### four-gJass impinger chilled and 

### ametering 

### console. No 

### fiIr.et is lued 

### forthis 

### melhod. The 

### first 

### impinger is**left~,** 

### the 

### second and third impingers contain 

### 100 ml 

### of0.1 N sodimn hydroxide 

### (NaOH) in

### place ofwater, and 

### the fourth impingercontains 

### 200g ofpreweighed silica gel fOr 

### moisture removal Each 

### ofthe eight

### points 

## was sampled for 15 minutes resulting 

### in anetrun time of120minutes. 

### After sampling, the 

### reagents 

## were returned to 

### theiroriginal container, weighed, the weights m:orded 

### onthe 

### label and the liquid 

### level marked. 

### The 

### silica gel 

## was returned to 

### the origiDal 

### container, weighed and the weight 

### recorded 

### on the label. 

### The volume ofwatervapor 

### condensed in the impingers 

### and the 

### volume ofwater coUected in the 

### silicagel 

## were summed and entered into 

### tho moisture consent calculations. 

### All 

### sampling componeuts exposed to 

### the 

### eftIueDt 

### were rinsed thn:e 

### times withNaOH and 

### therinses 

## were added to

### the reagent

### comamers. The 

### combined samples and rinses 

### were iIIUIJyzM 

### fortotal chrome

### usiDg Graphite 

### Furnace.

5.20 Field Data

### Sheets 

### Fielddata sheets for the Method 1-4 data 

### are enclosed in Appendix B.

6.0 EQUIPMENT CALIBRATION AND QUALITY ASSURANCE 

### RMCEINC foUowed the calibration and 

### quality 

### assurance procedures 

### of EPA Methods I, 2, 3, 4, 5 and 

### 306 tbroughout 

### the test program. A copy ofthe meter 

### box 

### calibrations, aua1yzer 

### quality assurance checks and the 

### ample Chain ofCustody 

### are included 

### in

### Appendix C.

Page 3

### Armoloy CorporatioD DeKaIb, lJIfaois 

### RMCEJNC-Chicago RegIoaal

# omce Project

### t#2006-J3511



## APPENDIX At 

## TESTSUMMARy SHEETS Total Chromiam 

### Resalts SlUIlID8ry

### RMC environmental. Inc. Emissions Testing & 

### Consulting

Plant: Armoloy Date: 

### 03123106 Project#: 2006-13527 Location: Chrome Scrubber#2 

### Sample Identification 2-M306-1 2-M306-2 2-M306-3 

### TestOate 02128106 03101106 03101106 Start 1025 830 1110 FInish 1227 1040 1315 

### Total 120 120 120 Cp Pilot Coefficient (CF) 0.84 0.84 0.84 A Area 

### ofstack sq. Inches 804.2 804.2 804.2 Pbar 

### Barometric Pressure (in HG) 30.12 30.12 30.12 Wm Volume of

### Condensate (mg) 25.8 32.4 33.8 

### Ta Temperature of 

### Effluent (F) 60.5 

### 63 65 

### Pavg Average Delta P 0.640 0.730 0.740 Pg Static Pressure (In H2O) 0.17 0.17 0.17 OH Delta H, Orfflce pressure differenl (In H2O) 2.06 2.42 2.47 Tm MeterboxTemperature (F) 

### 53.0 43.0 

### SO.O Vm Volume of

### sampte metered (CF) 97.163 100.797 102.423 Y Meter correction factor 0.989 0.989 0.989 On Nozzle Diameter (In) 0.239 0.239 0.239 CO2 Percent Carbon Dioxide (%) 

### 4.00 4.00 4.00 02 Percent Oxygen (%) 

### 20.00 20.00 20.00 CO Percent Carbon Monoxide (%) 

### 0 0 0 N2 

### Percent Nitrogen 

## (%) 76.00 76.00 76.00 

# Ms MolecularWeight (wet) (Ibnb-m) 29.30 29.28 29.27 Laboratory 

### Results
Total Chrome (mg) 

### 4.40E-02 1.24E-02 1.25E-02 AVERAGES Ps Absolute pressure 

### of Flue Gas (in HG) 30.13 30.13 30.13 

### Vwstd Volume of

### WaterVapor (SCF) 1.22 1.53 1.S9 Vmstd Volume 

### ofMetered 

### Gas (DSCF) 

### 100.026 10S.922 106.167 

### M Moisture (%) 

### 1.20 1.42 1.46 Va Velocity (FPS) 44.11 47.24 47.66 Qaw Volumetirc 

### Ftatl (ACFM) 14,781 1S.831 1S.971 QscI 

### Volumetric Flow (DSCF) 14,919 1S,867 15,937 1S,574
Chromium Concentration (mgIDSCM) 0.0155 0.0041 0.0042 0.00418 Chromium Concentration (lblHr) 

### 8.88E-04 2.48E-04 2.48E-04 4.54E-04

Isokenetlc 

## (%) 100.16 99.73 99.52

## RMC Envlronmenta', Inc. Em/ssions Testing & 

### Consulting

Plant: Armoloy Date: 

### 03123/06 Project#: 2006-13527 Locat/on: Chrome Scrubber

### #3 Sample Identification 3-M306-01 3-M306-2 3-M306-3 Test Date 02128106 

### 03101/06 03101106 Start 1030 830 1110 Finish 1240 1040 1320 Total 

### 120 120 120 Cp Pitot Coefficient (CF) 0.84 0.84 0.84 A Area of 

### stack 

### sq. Inches 804.2 804.2 804.2 Pbar Barometric Pressure (in HG) 30.12 30.12 30.12 Wm Volume of

### Condensate (mg) 29.1 29.1 36.8 

### Ta Temperature of

### Effluent (F) 

### 75 73 71 Pavg Average Oelta P 0.840 0.860 0.850 Pg Static Pressure (in H2O) 0.21 0.21 0.21 DH Delta H, Orifice pressure differential (In H2O) 1.77 1.84 1.82 Tm Meterbox Temperature (F) 53.0 51.0 58.0 Vm Volume of

### sample metered (CF) 93.909 93.188 95.461 

### Y Meter correction factor 0.955 0.955 0.955 On Nozzle Diameter (in) 0.217 0.217 0.217 

## ':02 Percent Carbon Dioxide (%) 

### 6.00 6.00 8.00 02 Percent Oxygen (%) 

### 20.00 20.00 20.00 CO Percent Carbon Monoxide (%) 

### 0 0 0 N2 

### Percent Nitrogen (%) 

### 74.00 74.00 74.00 Ms 

### MolecularWeight (wet) 

### (lbIlb-m) 29.59 29.59 29.55 Laboratory Results


### Total Chrome (mg) 

### 1.25E-02 1.24E-02 1.25E'()2

. AVERAGES Pa Absolute pressure of Flue Gas (In HG) 30.14 30.14 30.14 Vwstd Volume ofWater Vapor (SCF) 1.37 1.37 1.74 Vmstd Volume of

### Metered Gas (OSCF) 93.287 92.947 93.924 M 

### Moisture (%) 

### 1.45 1.45 1.81 Va Velocity (FPS) 50.98 51.49 51.13 Qaw 

### Volumetirc Flow (ACFM) 17,084 

### 17,254 17,133 Qsd 

### Volumetric Flow (OSCF) 16,736 18,966 16,848 18,849 Chromium Concentration (mglDSCM) 0.0047 0.0047 0.0047 0.00471 Chromium Concentration (lbMr) 

### 2.97E-04 2.99E-04 2.97E-04 2.98E-04

lsokenetic (%) 

### 101.01 99.29 101.03

### Armoloy Corporation DeKalb, 

### lJIiDols**RMCElNC~ltago** 

### RegfoaaJ Omce Project

### #2006-13517

APPENDIX B. 

### FIELD DATA SHEETS 

### Method 1- DataSheet Method l-S SampbgDlta Sheet FaelUty Process DataMETHOD 5 - DETERMINATION OF PARnCULATE EMISSIONS

- RESULTS

Plant Name**Amtol~** Sampling LocatIon UnltZ Operator 

### TS

Hlstorfcal Data Run Number U2-M306-1 U2-M31l8-2 Run StartTime 10:30 8:30 Run StopTIme 12:30 10:30 Mater Calibration Factor (Y) 0.989 0.989

PItat Tube CoeftIcient**(~** 0.840 0.840 AdUaJ Nozzle DIarMter (0,.) 0.239 0.239 Stack Test Dcta initial MeterVohnno (V".), 633.949 731.878 Final Met

...Volume (V.,), 731.112 832.875 Tatal Meter Volume (Vm> 97.163 100.797 Total TIme (9) 120.0 120.0 AverageM

....TempualUre 

### tY- 52.1 42.8 Average Stack Temperature 

### tl.>- 80.5 63.1 Barometric Pressure 

### (P.) 30.04 30.02 Stllek StaticPressure 

### (P..,) 0.17 0.17 AbsDlute Stack Pressure (P,) 30.05 30.03 Average OrIfIce Prosaure Drop (AH)M 2.18 2.42 Absolute "..,.Pnsaure**(P~** 30.20 30.20 AV1J SqUlllll RaatPIlot Pressure

### (~'~- 0.80 0.85 MoistIn

### eom.ntDIIta Implnaer- 1-3 Weter Volume tJaIn (V,,) 12.0 17.0 Impn"

..... SibQet WeIght (JaIn rN") 13.8 15,4 Total WaterVDlume Collected (V,,,) 25.8 32.4 StandardWater V8INX'Volume (V.J.,., 1.218 1.526 Standard MaterVolume (v..>.t 99.992 105.702 c.Jcu1aled Stack Moishlre**_~**

### .. Jl 1.2 1.4 SaturatH Stack MaistIInt 

### (B..t

....ll 1.71 1.9 Reported StackMoisture COIIIent (e....> 1.2 1.4 

## auAnalysis Data Carbon DIoxIde Percentage ('%COz) 4.0 4.0 Oxygen Percentage (%OZ) 20.0 20.0 Carbon Monoxide Percentaae (%CO) 0.0 0.0 Nitrogen Percentage ('!6Nz) 78.0 78.0 Dfy

## ca.. MaIec:uIarWeIght (M.s) 29.44 29.44 Wet Stack

## ca.. Molecular WeIght (MJ 29.30 29.28 CclculaledFu.I FactDr (F..) 0.225 0.225 Fuel F..flllCtor (Fill 0 

## a Percent Excess AIr**~EA)** 31250.0 31250.0 Vo/umeb1c Flow Rate Oat. Aver

...Stack Gas Velocity 

### (VJ 44.44 47.17 St.ldcCross-secuon.l AIM (N 5.59 5.59 ktuaI StackFlow RIa (a..,) 

### 1.ftm 15807 Wet Standard Stack flow Rate (Q..) 910 

### 981 Dry Standard Stack Flow RIa (0.) 

### 14991 15787 Percent ofisoldnetic Rate (I) 99.8 100.0 Emfsslon Rate 

## oar. Mass 01PartIcu

....on Filter (lilt) Mass ofPatticulide In Acetone (m.')

...dueto Acetone Blank 

### (WJ Total Mass ofPartlculatu (m,,) Stack PartJcuJate Concentrldtan (cJ (cJ Partlculcte Emission Rate (E) (E) 

### (El**IPt75~FSIoct.** 

### 5.2."Heat Input (HI) IONIOI ,olYlOl
Armoloy-Unit 2 - M5

- Re&UIt& Page 1 U2-M308-3 11:10 13:10 0.989 0.840 0.239
832..875 935.298 102.423

120.0 49.8 64.9 30.02 0.17 30.03 2.47 

### 30.3) 0.88
18.0 15.8 33.8 1.592 105.949

1.5 2.1 1.5
4.0 20.0 

### 0.0 78.0 29.44 29.71 0.225

0 31250.0

47.84 5.59 

### 15985 987 15881 99.7

tolVlO! Date 2i28-!I1/2008 Project. 2006-13527 Stack Type Cln:uIar

Averaga hh:mm hh:mm

In
It' 

### tt' 100.128 

# tr

120.0 min 48.1 

### OF 62.8 

### DJ: 30.03 

### InH1a 0.17 InHP 30.04 In HII 2.35 InHP 30.20 In He 0.84 (In Hp)'1l
15.7 nil 15.0 9 

### 30.7 mt 1.445 set 103.881 dscI

1.4 % 1.9 % 1.4 %
4.0 '16 20.0 '16 0.0 '16 78.0 '16 29.44 IblliHnolo 29.28 Iblll>m% 0.225

0 datflmmBlu 31250.0 %

48.42 It/sac ft"_ 15555 acfm 948 Vt'bc:th 15553 dsefm 99.8 %

mg mg 

## rnu mg gJdscf gr/dscf k;/h! Ib&Ihr IbsImmBtu I1l/IISlUIHr



### Printed 3I28l2006 V1.15

### METHOD 1 - SAMPLE AND VELOCITY TRAVERSES FOR CIRCULAR SO.URCES

Plant Name 

### """


# ....., Date 

### 2I28-3I1J2008 SampUJlI LocaUon Unit2 

### Protect' 2006-13527 Operator 

### TS • of Ports Available 2 Stack Type CircuJar • of Ports Used 2 Stack Size

## llargo Port inside Diameter 5 

## L,w Circular Stack or

### Duct Diameter 

### DIstance to Far Wall ofStack (4.) 

### 37.00 

## n 

# V**~** f--LnWDIstance to Near WaD ofStack (L..) 

### 5.00 

## n 

# ;/**I~-\** pUw-1IIW) 

### DIame_of Stack (0) 

### 32.00 

## n r- (-.l.U(DllA:IftIa)21Aru of Stack 

### CA.) 5.59 it" IDlatance from Port to DIs1urbancQ 

### 0 I-- DlstanceU 

### CBl 

### 44.00 

## n

# I~-'i (-lID) Dlamet:en U (80) 

### 1.38 cfiametBra 

### ....... DIstance Downstream 

### CA) 

### 17.00 in f-M)) 

### DIame

..... Downstream (Ao) 

### 0.53 diametIn 

# T'r- Downstream Number ofTraverse PoInts Required Dlametento Minimum Number 

## Ott 

## A 

# + Disturbance Flow DIsturbance Traverse Points

Up Down PartIcUIaIe Velocity**~** 

### -, Measurement 

### strum strum PoInts PoInts**~** I--' 

### Site 

### 2.00-4.99 0.50-1.24 24 16 5.00-5.99 1.25-1.49 20 16 

# t**6.0~.99** 

### 1.50-1.74 16 12 7.00-7.99 1.75-1.99 12 12 

# B

>=8.00 

### >--2.00**8or1~ 8or1~**  U SIHlC 

### 24 16

## ~ceQ,"" Downstresm IDee 

### 24 16 Traverse 

### Pta Required 

### 24 16 Disturbance



# ........ :r Chock MInImum Number 01 PoInts far the Upstream and DDwntJarMm condItJons, Ihun use the IalgISt. Number of

### Traverse Pamts Used
Z 8 fat CImdar Stacks t2 CD 

## :u InchOG 

### 2 portsiW 

### 12 Across

12 fat ctrwIar Stadls 0'IIf'2'" Inches 

### 24 PtsUsed 

### 24 IRequlred 

### [,,] ParUculace [] V.,ocftV
Traverse 

### PoInt LocaIIons lAa$a otTrn

...PalaU IaClrcIdIor

.... 

### FracUon 

### DIstance Dbtance 

### n_ rp_tieDofStack Oiamdcr Ii

.... "'tid

.. Wd II> T

.. _ Poinl\ Travene of 

### tram Including Poi

.. Number alTrav_PoiaI.oa a Ci

___ PoInt Stack 

### Insld. Nip.,. Numb

.. 2 4 Ii II 10 12 1 .1'" .fW1 

## .o.u 

## .m .026 JlZl Number Dfameter 

### Wall LenatIt 2 .854 .1!0 

### .1-" .105 

### .oa .DIi7 In in .J .7!IJ ..%95 _1,. .1'*5 

### .us 1 0.021 5/8 55/8


# .. 3.J,J .704 ..n.J .2l6 .177 5 .15& 

## .m .,3.C .l!IJ 

### 2 0.067 21/8 

### 71/8 6 .9!6 .805 .6!1f .J!6 

### 3 

### 0.118 36/8 86/8 7 .895 

## .77" .6-U 

### 4 

### 0.177 55/8 105/8 8 .9Qt 

## .ss.a _7!IJ 9 .918 

### .au 

### 5 0.250 8 13 10**~**

### .. 

## .-z 8 0.356 113/8 163/8 11 -'lJ 

### 7 0.644 20518 25518 12 

### -'" 8 

### 0.750 24 29 9 

### 0.823 26318 31318 

### 10 0.882 28218 33218 

### 11 0.933 297/8 34 7/8 

### 12 0.979 313/8 36318



### Armoloy-Unit 2 - M1

- Circular Page 1 Printed 312812006 Vt.15

### METHOD 2 • DETERMINATION OF STACK GAS VELOCITY AND VOLUMETRIC FLOW RATE
Plant Name AnnoIq 

### Date 2Q8.3I112OO6 SampUnaLocadon Unit 2 

### Project' 2006-135'Zl OperdOr T8 • of Pods Used 2 StaclcType Circular PIlot lcIeIdItIcdIon PIlot LeakCheck 

## 0 I PleTest 

## 1 

# 0 1 PostTest PItcICoellldenl**(C~** 0.84
Stack Dimensions Ve1oc1y Traverse Data DIameter or length ofStack (D) 

### 32.00 in Run 

### Number U2-M306-V1 

### WIdth ofStacIr 

### lWl in Rlln1lme

AruofStacIe CAs) 

### 5.59 

### tr T,..".,. Velocity Stack Local Point 

### Head 

## Temp Velocity 

### Pressu

.... (Ap) (tJ**(v~** Baromatrtc PressUN**(P~** 

### 30.04 inHg in 

### H 2

### 0 0,: ftJsec StatIc 

### Pressure (P....J 

### 0.17 inH:zO 

### A-1 0.78 

### 72 49.4 AbsoIUIe StacIt PressUN 

### (P.) 30.05 inHg 

### A-2 

## D.n 72 49.1 

### A-3 0.72 

### 72 47.4 StackGas Com 

### A-4 0.74 73 48.1 

### Composition

## Data:1 Actual [,,] 

### EstrmatacI 

### [] A-5 0.68 73 46.1 carbon DIoxide Conc.ntraIIon (%C02l 

### 4.0 

# .. A-8 0.63 

### 72 44.4 OXygen Concentration**~~.** 

### 20.0 

# .. A-7 0.78 73 48.8 carbon MonoXIde ConceIdraIIon (IlftCO) 

### 3.0 

# .. A-8 0.73 73 47.8 Nitrogen Conceldradon**(Ilft~** 

### 73.0 

# .. A-9 0.78 75 49.5 StacIr MoIItUN Conrenl (B.) 

### 2.000 A-10 0.82 75 50.8 Stack DryMofecutarWeIght (Mill 

### 29.44 !bAIHnoftt 

### A-11 0.74 74 48.2 Stack Wet Molecular

### Weltht (M.) 

### 29.21 lbf1b.mole 

### A-12 0.63 74 44.5 B-1 0.78 75 48.9 

### Resulis B-2 0.79 75 49.8 Avg 

### Stack Gas VeiocIly (v.) 

### 47.8 ftIsec 

### B-3 

### 0.72 74 47.5 Avg StacIr Dry 

### 8td Row Rate (Q..) 

### 931418 dac:fltr 

### B-4 0.73 74 47.9 Avg Stack Dry 

### 8td Flow Rate CQ..) 

### 15524 dac:fhnin 

### B-5 0.88 73 48.1 Avg Stacie Wet FlawRate (Q

.. ) 

### 15939 ascfAnin 

### B-6 0.80 73 43.3 B-7 0.66 73 45.5 Stac:t Crass 8ectIon 8chemaItc 

### B-8 0.69 75 48.6



## A. ::I DWIKu for Rectangular 

### Stacks 

### A. ::I (n(Df.2),)A<vfor Circular Staclas where 

## Ku

.. 1 for metric units where 

## Ku " 144 (In2mZ) for English unils p. ::I Pilii' + P1IIIIII13.6 %N2 ::I 100

- %C02

- %02
- %CO 

### Md::l .44{%COz) 

### + .32(%02 } 

### + .2S(%N2

### +%CO) M." Md(1

- 

## B.> + 1SB..**~)'IZ_** •**'/,.E(Jp'~** 

### Armoloy-Unit 2 - M2 8-9 

# o.n 74 49.1 8-10 0.83 74 51.0 8-11 0.79 74 49.8 8-12 0.67 75 45.9

Average 

### 0.85 

### 74 PIMse r.portIl1o cmra;efII tile sqtr8IDRIOIs 01 olp. at. (jp)'IZ

_ .. '/,.t(,lp

## 'a,

Formulas Used TI(I\9I"I/ 

## A +Tu where Tu ::I 273 

### OK formetric unita where 

### Tu

..-480 

### OR for

### Engliih uniCa
v ••**Kp~)'IZ..,** (r.,..q/f1»,Md)'1l when! 

### K, " 34.97 for metric una where 

### K,

... 85.49 for EngIlah units 

# a..s
...**36OO(1-s..)veA.(T.JT~)(PJP~** 

### whet8T lilt '"

### 293 

## X p

...

### 760 

### mm Hg. for meflic units 

### whereTl1li 

### =528 

### 'R. p

...29.921n Hg. for English units 

# ,

Page 1 Printed 

### 312812006 V1.1S

### METHOD 3 - GAS ANALYSIS FOR THE DETERMINATION OF DRY MOLECULAR WEIGHT

Plant Name lA, 

# .... Date 2J28..3I1J2008 &UllaLoc:atlon UnIl2 

### PrOJect" 2QC6.13527 Operator TS , of Porta Used 2 FueJType NlA 

### I MInimum Fuel Factor 

### I Maximum Fuel 

### Factorl Oraat Leak Check**~** 

### I PreTest 

### I

Run Number U2-M306-1 Sample Carbon carbon Analysis DIoxide Oxygen Monoxide

nme Volume Volume Volume (Veaz) 

### (VgJ (VCQ) hh:mm mI 

## m mI 

### FYRITE 4.0 24.0 4.0 24.0 4.0 24.0 Results**Avera~es** AveragecafculatedFuel Factor**(~** Average ExceN AIr (%EA>-

Run Number U2-M306-2 Sample carbon C&rtMIn Analysis Dioxide Oxygen Monoxide

nme Volume Volume Voluma 

### (Veaz) (Voz) (Veo) hh:mm mI mI 

### mI 

### FYRITE 4.0 24.0 

### 4.0 24.0 4.0 24.0 Result. 

### Averages Average calculated Fuel Factor (F.J

... AverageExCttN Air (%EA)

...

Run Number U2-M308-3 Sample Carbon carbon Analpls DIoxide Oxygen Monoxide

nme Volume Volume Volume (Vc:ozl 

### (Voz) (Veo) hh:mm ml mI mI 

### FYRITE 4.0 24.0 

### 4.0 24.0 4.0 24.0 Resulb Averages AveragecaJculatedFuel Factor (FJ

.... Averaae

### EJrceu AIr (%EA)..,

Fuel Factor Po FueJType Minimum MaxImum Coal, Anthraclt. 1.018 1.130 

### CoaI,Ugntte 1.018 1.130 Coal, BHumlnoua 1.083 1.230 Oil, Distillate 1.260 1.413 Oil, Residual 1.210 1.370 Gu, Natura. 1.600 1.838 Cas, 

### f!ropane 1.434 1.588 Gas, Butane 1.405 1.553 Wood 1.000 1.120 Wood Bark 1.003 1.130


### Armoloy-Unit 2 - M3

- Orsat**~** 

### I PostTest Ontat ldentltlcatloni
GIla AnalysIs Data Run Startnme 10:30 RunStopnme carbon CaIbon DIy DIoxide Oxygen Monoxide Nitrogen Molecular Cone. Cone. Cone. Cone. Weight**~** (%Oz) (%CO) (%Nz) (MJ percent pen;ent perad pen:ent lbmHnoIo

4.0 20.0 0.0 76.0 29.44 4.0 20.0 0.0 

### 78.0 29.44 4.0 20.0 0.0 

### 78.0 29.44**~.O** 20.0 0.0 

### L8.0 29.44 0.225 MolecularWI Deviation < 0.3? 31250.0 peReflt Fuel FactorIn Handbook Range? OUAnalysls Data Run StArtnme 8:30 RunStopnme carbon Dioxide Oxygen Cone. Cone.**~** ('lOz) pen:cnt pen:ent

4.0 20.0 4.0 20.0 4.0 20.0 4.0 20.0 0.225 31250.0**~** 

## oaa Analysts Data Run Startnme Carbon Dioxide 0Xy;en Cone. Conc. (%COz) (%Oz)**~** pen:ent

4.0 20.0 4.0 20.0 

### 4.0 20.0 4.0 20.0 0.225 31250.0 pen:ent carbon Dfy Monoxide Nitrogen Molecular

Cone. Cone. WeIght (%CO) (%Nz)**(~** I)eR:eft**~** !bIIb-rnoIe

0.0 78.0 29.44 0.0 78.0 29.44 

### 0.0. 78.0 29.44 0.0 78.0 29.44 MolecularWI DevIaUon < 0.3? Fuel FactorIn Handbook Range?

11:10 RunStopnme carbon Dry Monoxide NItrogen Molecular

Cone. Cone. WelQht (%CO) (%Nz) 

### (IY percent**~** IIIJb.maIe

0.0 78.0 

### 29.44 0.0 78.0 29.44 0.0 78.0 29.44 0.0 1'8.0 29.44 MolecularWI DevIatIon < 0.3? Fuel Factor In Handbook Range?
Formulas Used**~"Vc:oz** 

### %Oz • VOl.

-Vcoa %00:11Veo

- Vea %Nz 

### = 100

- 

### %COz

-**%~** - %CO 12:30 Molecular

Weight DevIatIon**(.1M~** IbIIIHnoIe

0.00 0.00 0.00**~** 

## f [o!)

10:30 Molecular

Weight Deviation

(.l.M,,) lbIIb-mafe

0.00 0.00 0.00**~ ~**  

## I

13:10 Molecular

Weight DeviatIon**(~** Ib.1IHnaIe

0.00 0.00 

### O.CO 

## iii 

## f 

## iii**~** 

### =**.44(~+ .32(%~)+**  .28(%Nz+ %CO)

Page 1 

### Printed 312812008 V1.15

### METHOD 4

- DETERMINATION OF MOISTURE CONTENT IN STACK GASES

Plant Name Annoloy 

### Date 2128-31112006 8ampBna LocatIon Unit 2 Projecttl 2006-13527 r T5 

# "ofPorts Used 2**8tacIr~** Cin:uIar Meter Box Number 1 Train Leak Check [,,] 

## I PreTest 

## I 

## ["1 I PostTest Meter

### Cal Factor (y) 0.989

Run Number 

### U2-M306-1 Total MeterVolume 

## NrJ 97.163 AvgMarTemp 

## ttm>- 52 AVV81ac1r Temp 

### (tJ.., 

### 61 Implnger1 mI Contents NaOH Final Value**M}.~,)** 

### 110.00 InJIIaI

### Value**M).~,)** 

### 100.00

NitValue**N,J.~,J** 

### 10.0

ToCaIVoCuma**N~** 

### 12.00 Total

### Weight**~~** 

### 13.80 Std MeterValwne (V!I(") 

### 99.992 Calc Moisture Content (B.CIIt:,) 

### 1.2

Run Number 

### U2-M306-2 Total MeterVoIume 

## NrJ 100.797 Avg MeterTem, 

## <t.n>- 43 Avg 

### Stacie Temp (t.)

.. 

### 63 fmplnger1 mI 

### contents NaOH FlnalValua 

### M).C'N,) 112.00 !nidalValue 

## N,).(W,) 100.00

NetValue**(vnl.~nl** 

### 12.0
Total VolUme 

### (Vtl 17.00 Total

### WeIght**~tl** 

### 15.40 S1d M

... 

### ,VoIuma (Vrr(aq) 

### 105.702 Calc Moisture 

### content (B..) 

### 1.4

Ran Numbe, 

### U2-M306-3 Total MeterVolume 

### J'ltn> 

### 102.423 AvgM

.....Temp**~** 

### 50 A'll StackTemp 

## tt.lwt 65 

## 1m"",.,' mI 

### ContMts NaOH FlnalVaJ

... 

### M).rNf) 111.00 INUaIVafua**(V,).~,)** 

### 100.00

Net Value 

### Nnl.rNrJ 11.0

Total Volume**(V~** 

### 18.00**TotaI_~ht ~~**  

### 15.80 Std MetarVolume

### "'-~~- 105.949 calc Moisture Content 

## (e.> 1.5
Armoloy-Unit 2 - M4 Moisture Content 

### Data Run Start

### TIme! 10:30 Run StoP

### TIme 12:30 dct Barometric 

### Preu. (PtJ 

### 30.04 

### InHg DF stack 8bIdc

### Press. (PIIIIIIJ 

### 0.17 

### InHzO "'F Avg Orlftce Pntss. 

### (M1lz.v 

### 2.16 

### InHzO ImplnaarZ 

### 1m1llnaer3 Impbtg.,,, 

### ImJ'lngerl lmplnger6 

### Impfnger7 mI 

### rnI 

## a mI mI 

### mI NaOH 

### Sil Gel 102.00 163.80 100.00 150.00

2.0 13.8 Ruub mI 

### WaterVol Candennd 

## NWQ'AII) 0.565 ac:f 9 Water Vol WeIghed (V_san> 

### 0.651 ad dad SaL Moisture

### COftIenI (8...ro.o') 

### 1.8 

# '"

"- final 

### MoIsture ConIanI (B..) 

### 1.2 

# '"
Moisture Content Data Run Start

### Tlmel 8:30 Run 

### Stopnme 

### 10:30 dcf 

### BarometrIc 

### Press. (1\) 

### 30.02 

### inHg**~** 

### Stack 

### StatIc Press. (P....J 

### 0.17 

### inHzO "F 

### Avg

# ormce Pm

..**(~** 

### 2.42 

### inHzO Implngerz 

### Irnlllnfler3 

### rml){ngar " Implnger' flnpfnger6 imPinge, 7 

### mI 

# "" a mI mI ml NaOH Sil Gel 

### 105.00 165.40 100.00 150.00

5.0 15.4 ResufIs 

### mI 

### Water Vol Condensed (V-.1Id)) 

### 0.800 sc:f 9 WIler

### Vol 

### WeIIhtId 

### N

.. 

# -> 0.726 sc:f 

### dsc:f Sat. Moisture CordInt**~** 

## .. \ 

### 1.9 % % final Moisture ContMt (B..) 

### 1.4 %
Moisture

### contentData Run Start

### TIme! 11:10 Run 

### StopTIme 

### 13:10 dcf 

### 8aromeCrfc 

## Press. (P,,) 

### 30.02 

### inHg "F Stacfr 

### StaIIc Press. (P..J 

### 0.17 

### InHzO 

## UF A'll OrHlce Press.**(~** 

### 2.47 

### inHzO hnpfnger2 

### Implng,r3 

### fmllfnler

.. hnplngor5 flnplnferl lrnplnger7 

### mI mI 

## a NaOH Sit Gel 

### 107.00 165.80 100.00 150.00

7.0 15.8 Results 

### ml Water Vol Condensed 0 WalarVoiWefghed 

### dsef Sat. Moisture Content



# '" FInal Moisture Canteftt



### Page 1 mI 

### mI

(V'III:IatIIl 

### 0.847 

## N

... SIIJ)) 

### 0.745 

### .CB..III4I') 2.1

(8".) 

### 1.5 mI

set sc:f 

### % %

Printed 

### 312812006 V1.1S

### ISOKINETIC SAMPLING DATA

Plant Name Annoloy SamSlGna Locatfon UnIl2 18 #I ofPolms Acrau 12 Ideal Nozzle DlMMtwand laoKInetIo Factor Setup PIlot Tube Coefllclent 

### tOp) 0.840 Avg StackTemp (t.) 

### 70 "F Avg Gal .....,Temp (t",) 38 of DH .0.71SCFM (AHO) 

### 1.87 

### "'HaO Avg PIlot Tube DIff. Preaure**{~** 

### 0.75 

### InHaO Stack IIGimn ConfIInt (B..) 

### 2.0 

# '" Stack Dry MoIecuI8rWeIght (M...) 29.44**~** E.stfmated DrIftce Flow RIte (a".) 

### 0.750 IIdm

DP to DH Isoklnetlc FIICtor (K) 

### 3.32
Preuuru &.nMnetrIc: Pntuure (Pill 

### 30.04 In Jig StIIdr Sratlo Pruaure (P-> 

### 0.17 

### "'HaO AbsoIuIe stackPntuun 

### (P.) 30.05 In Jig Absolute MetvPreNunt (P..,) 

### 30.18 InHg

DryGaa DuIJed TraYeIM SanpIIng Clock 

# ..... VeIocfly OrIfIce Point. TIme Time Rudin. Heed**~** (9) (V.,) (Jp)**(~** mill hh:mm:8& 

### It' 

### IIIHzO inHzO 

### A-1 0.0 10:30:00 633.949 0.580 1.928 A-2 5.0 10:35:00 637.701 0.840 2.125 

### A../3 10.0 10:40:00 841.821 0.710 2.358 A-4 

### 15.0 10:45:00 845.832 

### 0.730 2.42" 

### A-5 20.0 10:50:00 650.327 0.690 2.291 

### A-6 25.0 10:55:00 

### 654.<406 0.640 2.125 A-7 30.0 11:00:00 

### 65B.S40 0.750 2.490**A~** 

### 35.0 11:05:00 682.E$33 0.730 2.42" A-9 40.0 11:10:00 668.897 0.680 2.258 

### A-10 45.0 11:15:00 671.023 0.840 2.125 A-11 SO.O 

### 11:20:00 675.021 0.580 1.928 

### A-12 55.0 11:25:00 878.871 0.590 1.959 8-1 60.0 11:30:00 682.776 

### 0.590 1.959 8-2 65.0 11:35:00 888.789 

### 0.870 2.225 B-3 

### 70.0 11:40:00 690.781 0.720 2.391 B-4 

### 75.0 11:45:00 695.192 

### 0.730 2.424 

### B-S SO.O 

### 11:50:00 699.483 

### 0.880 2.258 B-8 

### 65.0 11:55:00 703.587 0.800 1.992 B-7 90.0 12:00:00 707.893 

### 0.580 1.959 B-8 

### 95.0 12:05:00 711.784 0.560 1.B60 

### B-9 100.0 12:10:00 715.223 O.6Sl 2.158 8-10 

### 105.0 12:15:00 719.332 0.610 2.026 8-11 110.0 12:20:00 723.218 0.580 1.928 8-12 115.0 12:25:00 TZl.2B3 0.640 2.125 LaatPt 120.0 12:30:00 731.112

Last PI 

### 120.0 12:30:00 731.112 Average Values 

### 0.65 

### 1

ArmDloy-Unit 2 - M5

- Run 1 

### Page 1 Date 2J28.3I112C08 Project. 200&-13527 

# Run. UZ-M308-1 #I ofPorta U.1d 2 SamplJnj I Equfoment



# ..... , Maerbox CaL FIIdor (Y) 

### 0.989 Nozzle.**~** Nozzle 

### ct.n.t. (On.) 

### I 0.2390 In 

### Reel. Nozzle DIIIIMCer (Dr.) 

### I 0.2274 In Probe .,

### LenGth 48.00 It 

# LIner,...,.., 

# Scm,.. CuelOVen' ImplngerCae• 

## .1v. LeakChacb

Pre 0.002 

# rlnm 

# • 1S InHg Mid**~hnin** 

# • lnHg Pat 0.001 r/mln 

# • 1

.. 

### InHo .1V. c 0.020 

# rlrnkl iii LHkCheck OK? PltatOK? 

# m OnatOK?**~** AcIuaI Meter 

# ... ImpInger 0riIIce Stack 

### rn'-t OUtlet Filter Exit Pump

JH Temp Temp Temp Temp Temp Vacuum (JH) (t,,) (t.,d ('t,.J InHP '"F 

### OF 

## or: OF "F InHO 

### 1.900 83 42 42 40 

### 3.0 2.100 83 48 43 40 

### 3.0 2.400 82 50 

### 44 40 

### 3.0 2.400 81 

### 52 45 40 

### 3.0 2.300 60 54 48 

### 40 3.0 2.100 60 

### 55 47 40 

### 3.0 2.500 

# eo 54 48 

### 40 3.0 2.400 81 55 48 

### 40 3.0 2.300 

# eo 54 

### 47 40 3.0 2.100 58 55 

### 49 40 3.0 1.900 

### 57 

### 55 48 40 3.0 2.000 

### 57 66 50 

### 40 3.0 2.000 

### 56 

### 55 50 

### 39 3.0 2.200 

### 56 54 

### 49 39 3.0 2.400 60 58 

### 51 40 

### 3.0 2.400 58 59 

### 51 39 

### 3.0 2.300 60 59 

### 52 40 

### 3.0 2.000 81 59 51 40 

### 3.0 2.000 64 59 

### 52 41 3.0 1.900 65 60 

### 53 41 3.0 2.200 83 59 53 41 3.0 2.000 62 60 

### 53 

# '" 3.0 1.900 

### 82 59 54 41 3.0 2.100 83 59 

### 53 .f2 

### 3.0

Maxlmum V*'IUm 

### 3.0 2.18 

### j 61 

### I 55 

### 491 

### I 40 

## I 52 

### I

Printed 312812008 V1.1S

### .SDKINETIC SAMPUNG DATA

PlantNamo Annolov 

### SemDftlus Location Unit 2 TS
• ofPoInts Acrou 12 Ideal Nozzle DIametwand 

### lsoKlneClc Fac:tvr Setup PilotTube Coefficient**~~** 0.840 Ava StackTemp (I.) 70 "F Avg Gas MeterTemp (t",) 38 

### OF DH .0.76SCAI (..UfO) 1.87 InHP Avg PIlat Tube DIlL Pressure (Ap..J 0.75 InHP st.cIc IIIDIstIn CGrI1ent (B.) 2.0 

# '" Stack Dry Molecularw.tght (M,.) 

### 29.44 IbIIb-mDie EatImated OrifIce FlowRde (0..,) 0.810 acfm

DPto DH Isakfnetlc Factat (K) 3.32 Preuuru Barometrtc Pressure (Pt,) 30.02 InHg Steck Sialic PrcIAure (P-J 0.17 InHP Absolute Stack PrHsunI (PJ 30.03 In HI Absolute MeterPreuure (P.,,) 30.18 InH.

Dry Gas DesIred Actual Traverse Sampling CIocIc 

# ....... Vdocfty CrtfIce OrIfIce 

# PoInt. Time Time Reading Hud .iH .\If (8) (V.,) (41') (.1H) (.ut) min hh:mm:sa It' InHP InHP InHP A-1 

### 0.0 8:30:00 '731.878 0.830 2.758 2.700 A-2 

### 5.0 8:36:00 738.283 0.820 2.723 2.700 1.-3 10.0 8:40:00 740.602 0.750 2.480 2.500 A-4 15.0 8:46:00 745.078 0.710 2.358 2.400 

### A-5 20.0 8:50:00 748.978 0.670 2.225 2.200 A-6 25.0 8:55:00 752.888 0.&40 2.125 2.100 A-7 30.0 9:00:00 758.952 0.740 2.457 2.500 

### MJ 35.0 9:05:00 

## 781.ose 0.780 2.524 2.500 A-9 40.0 9:10:00 785.421 0.660 2.192 2.200 A-10 46.0 9:15:00 769.454 0.600 1.992 2.000 A-11 50.0 9:20:00 173.384 0.690 2.291 2.300 A-12 

### 55.0 9:25:00 777.424 0.890 2.955 3.000 B-1 60.0 9:30:00 782.112 0.760 2.524 2.500 B-2 

### 85.0 9:35:00 788.389 0.790 2.823 2.600 B-3 70.0 9:40:00 791.089 0.720 2.391 2.400 

### B-4 75.0 9:45:00 795.000 0.130 2.424 2.400 B-6 

### SO.O 9:50:00 799.212 0.680 2.258 2.300 8-6 85.0 9:55:00 803.223 

### 0.600 1.992 2.000 B-7 90.0 10:00:00 807.128 0.660 2.192 2.200 

### B-8 95.0 10:05:00 811.193 0.690 2.291 2.300 

### 8-9 100.0 10:10:00 815.221 0.770 2.567 

### 2.600 B-10 105.0 10:15:00 819.873 0.830 2.758 2.800 8-11 110.0 10:20:00 

### 824.189 0.790 

### 2.823 2.600 8-12 115.0 10:25:00 828.455 0.670 2.225 2.200 

### Last Pt 120.0 10:30:00 832.875

FlnalVaJue 120.0 10:30:00 832.875 AverageValues 0.73 

## J I 2.42 

### 1

Armo/oy--Unit 2 - MS

- Run 2 

### Page 1 Dam 2128-31112008 Praject. 2008-13527 

### Run. U2-M308-2 • of POIts Used 2 Samplinl E

....i-.U...i



### Mar. 1 MeteIbox CaL Fector 

### M 0.989 Nozzle. Aau-' Nazzle

### oc.mew (D"J 0.2390 In



### Reel. Nozzle**~ ~**  10.2363 In Prabo .,

### Lenath 48.00 It U.,., MaterIal SampleCueI Oven tI Can.
olV

.. Lukcttecb life 0.001 

# rmm 

# • 1S inti; IIld 

# rlmln 

# • In HI Post 0.001 rlmln 

# •**1~** InHg olV. < 0.G20 rhnln**~** LeIkCheck OK? PttDtOK?



# ..... StIIcIc fnfe Temp Temp

(t.) (Y 

### OF OF 81 34 

### 65 36 65 :fl 88 39 fil 41 fil 42 68 43 

### 85 43 58 47 

### 69 47 

### 61 47 60 

### 47 

### 59 48 B3 

### 47 82 47 62 47 63 

### 48 62 47 

### 64 49 B3 49 64 

### 49 83 50 64 50 64 50



### 831 45 

## 1 43 

## eJ orsatOK?**~** 

# .... 1mpIngOutlet Fibr 

### exit Pump Temp Temp Temp Vacuum (t...,)



### . OF OF 

### OF InHg



### 32 

## «> 3.0 

### 34 40 3.0 35 40 3.0 

### :fl 

### 40 3.0 

### 38 40 3.0 

## «> 39 3.0 39 

### 39 3.0 

### 40 39 3.0 38 

### 39 3.0 

### 39 

### 39 3.0 

### 40 40 3.0 

## «> 40 3.0 

## «> 40 3.0 42 40 3.0 42 

### 39 3.0 42 

### 39 3.0 41 

### 39 3.0 42 40 3.0 42 40 3.0 41 40 3.0 

### 44 41 3.0 44 41 3.0 

### 43 41 3.0 

### 45 41 3.0

MaxImum Vaewm 3.0 

### 401 1 1 40



### Printed 3I28l2OO8 V1.15ISOKINETlC SAMPUNG DATA

PfantNamo AmtrAay Sampling Locdan Unil2 TS #I ofPolnb Acfou 12 ldell Nozzle Clunetv'andIsol<tnetic Factor Setup PltatTube CoelftcJent 

## <c..> 0.840 Avg StackTemp 

### (tJ 70 of Avg Gas Meter Temp (Y 

### 38 "F DH

..0.7& SCFU (.UfO) 1.87 InHzO Avg PItct Tube DIfI'. Prusan**(~** 0.83 InHzO Sblde Moisture Content (8.) 2.0 'It. Stacll Dry Mvlecular 'NeIgtd <M..) 29.44 IbIIb-maIe EatImat1td Oriftc:e Flow RIde (0,.) 0.840 acfrn

DPto OM Isoldnetlc Factor (IQ 3.32 Pnssuru 8aramebtcPressure (Ptol 30.02 In", Sblde Stade Prenure (P.-) 0.11 InHP Ab8ofu1e**Stack~** (P,,) 30.03 In 

### HI AbIIo/Ufe MeterPresatn (P",) 30.18 InHt
DlyGu DesIred Actual Traver •• Sampling Clock Meter VeioclIy OrifIce Orifice Pointt TIme TIme ReadIng Had JH JH (9) (V",)**(~) (~**  (Mi) min Ith:mm:ss**~** InHzO InHzO IntlzO A-1 0.0 11:10:00 832.875 0.79 2.82 2.80 A-2 5.0 11:15:00 a:r7.289 0.78 2.62 2.50 

### PrJ 10.0 11:20:00 841.632 0.72 2.38 2.40 A-4 15.0 11:25:00 &45.815 0.14 2.48 2.50 

### A-5 :!D.O 11:30:00 850.117 0.68 2.28 2.30 

### A-6 25.0 11:35:00 854.212 0.83 2.09 2.10 A-7 30.0 11:40:00 

### 858.329 0.78 2.52 2.50 A-8 35.0 

### 11:45:00 

### 882.832 0.74 2.48 2.50 

### A-9 40.0 11:50:00 868.721 0.71 

### 2.58 2.60 A-10 45.0 

### 11:55:00 871.223 0.80 2.68 2.10 A-11 50.0 12:00:00 815.788 0.78 2.59 2.60 A-12 55.0 12:05:00 880.228 0.87 2.22 2.20 B-1 60.0 12:10:00 884.013 0.12 

### 2.39 2.40 B-2 85.0 12:15:00 888.214 0.75 

### 2.49 2.50 B-3 70.0 12:20:00 

### 892.004 0.88 2.28 2.30 B-4 75.0 

### 12:25:00 898.528 0.85 2.18 2.20 

### 8-5 SO.D 12:30:00 900.978 0.73 2.42 2.40 B-8 85.0 12:35:00 905.318 0.71 2.58 

### 2.60 8-7 

### SO.D 12:40:00 909.704 0.81 2.69 2.70 B-8 95.0 12:45:00 914._ 0.80 2.68 2.70 8-9 100.0 12:50:00 918.897 0.78 2.59 2.60 8-10 105.0 12:55:00 923.273 0.75 

### 2.49 2.50 8-11 110.0 13:00:00 

### 927.385 0.14 2.48 2.50 8-12 115.0 13:05:00 

### 931.483 0.69 

### 2.29 2.30 

### lastPt 120.0 13:10:00 

### 935.298

0-8 0-7 Last 

### Pt FfnalValue 120.0 13:10:00 935.298**Aver~.** Values 0.74 

### J 

## 1 2.41 

## I

Armdoy-Unit 2 - M5

- Run 3 

### Page 1 Date 2128-31112006 

### Pro.Lect. 1008-13527 

# Run. U2-M30&-3 #I ofPons Used 2 Sampllm**E~~_ent**



### Meter. 1 MeleIbox Cal. Flldor 

## m I 0.989 

## I Nozzle' ActwII Houle DIameter (D,.) 0.2390 In



### Reel. NDUIe DIametw (D,.,) 0.2514 In Probe.I LongIh 48.00 ft lJnIr IIateriaI s.mpleCaalOven. Implnger

# CUe.
.lV. LeIlkChecb

Pre 0.001 

### tt'lmln 

# • 1" InHg MId**~lmln** 

### 0 InHg Put 0 

### r/mln 

# • 13 

### InHG J.V.,. < 0.020**~lmln ~**  Leak Check OK? PttotOK? Meter S

... Inlet TCIIIIJ' Temp

('t.) Ita) 

### OF OF 84 48 

### 85 49 

### 85 49 

### 84 48 

### 63 48 83 49 

### 84 <48 63 49 

### 63 48 

### 68 49 

### 87 50 

### 84 51 

### 87 51 

### 65 51 

### 84 52 68 

### 53 65 

### 53 53 54 f{l 

### 55 68 

### 55 88 

### 55 f{l 58 64 58 

### 65 

### frT

65 

### 51 50 

## eI orsatOK? 

## iii 

# - impingei' 0UdIt FIbr 

### ExIt Pump Temp Temp Temp Vaewm ('t..,) "F "F "F InHg 

### 45 41 3.0 48 41 3.0 48 41 3.0 48 41 3.0 48 

### 41 3.0 45 41 3.0 45 41 3.0 48 41 3.0 45 41 3.0 45 41 3.0 48 40 3.0 48 40 3.0 47 40 3.0 

### 48 40 3.0 

### 48 40 3.0 49 41 3.0 50 

### 41 3.0 50 41 3.0 50 41 3.0 51 42 3.0 51 41 3.0 52 42 3.0 52 42 3.0 52 42 3.0

Maximum Vacuum 3.0 

## 481 

## J I 41



### Printed 3I28l2OO8 V1.15

### METHOD 5 - DETERMINATION OF PARTICULATE EMISSIONS

- RESULTS

HbtoricaI Data Run Number U3-M3Q8.01 U3-M3Q6.0Z tJ3.M306-3 Average Run Start nme 10:30 8:30 11:10 hh:mm RunStDpnme 12:40 10:40 13:20 hh:mm Meter Calibration Factot (V) 0.955 0.955 0.956

PItot Tube CoeflIc:MnI (<;) 0.840 0.840 

### 0.840 Actual Nozzfe DIameter (Dt.) 0.217 0.217 0.217 In Stack Teat Data initial Meter VDfume 

### (V"". 223.048 882.967 984.397 

## r FInal Meter VoWlnO**(V~** 318.955 976.153 1019.858 

## r Total Meter Volume 

### (VrJ 93.909 93.188 

### 95.481 9·'-185 

### Ir Total Samllflna TIme (9) 120.0 120.0 120.0 120.0 min Average MtIter TempendUre 

### (Y_ 52.5 51.2 57.8 53.8 

## or: Aver-ae Stack Tem.,.cture 

### <tJ- 75.'- 

### 73.3 71.1 

### 73.3 of 8arDmeIrtc Prasunt**(P~** 

### 30.04 30.24 30.26 30.18 In Hg Stack StatIc Prusure 

### (P-> 0.21 0.21 0.21 0.21 lnHzO Absolute Stacie Pressure (PO> 30.06 30.26 30.28 30.20 In Hg Average Ortftce Preuure Drop**(~** 

### 1.77 1.84 1.82 1.81 inHzO Absolute

.....Pru.ute (P,.) 30.17 30.38 

### 30.39 30.31 lnHg Avg Square Root PIlatPressure**(~''").."** 0.92 0.93 0.92 0.92 (In Hp)11l MobtinCoIant Data Implngen 1-3 Water VDlume Galn 

### (V,.) 18.0 15.0 19.0 18.7 mI Impfngv" SI8ca Gel Weight GaIn (W,.) 13.1 14.1 17.8 15.0 g TotalWiderVDIume CoUected 

### (V-.) 29.1 29.1 38.8 31.7 /III Standard WaterVaporVoIuIM (V.J.s 1.371 1.371 1.734 1.482 sci Standard MeterVDluru (V.J"" 93.181 93.322 

### 94.435 93.839 dscI Calculated Stack

### MoIaIunt 

## ca...

.... J>_ 1.5 1.4 1.8 1.8 

# ." Satumad Stack Mafature**(B..~** 2.95 2.7 2.5 2.7 % Reported StackMoIsbnCont.nl (8.) 1.5 

### 1.4 1.8 1.8 % 

### caaa AnaIy.1s Data Carbon DIoxfde Pen:entage 

### rAtCOV 8.0 8.0 6.0 8.0 % Oxygen Pemtntage**~** 20.0 20.0 20.0 20.0 .% Carbon Monoxide ('l6CO) 0.0 0.0 0.0 0.0 

# " NI1rogen Pen:elltage (%Nz) 74.0 74.0 74.0 74.0 % Dry

### caaa lfoIecuIarWeIght (M.s) 29.78 

### 29.78 29.18 29.78 lbI1IHnoIe Wet Stack GuMolecular Weight (M.) 

### 29.59 29.59 29.55 29.58 IbItIHnoIo carculated Fuel Factor 

### (F.) 0.150 0.150 0.150 0.150 Fuel F.f=adDt (F.s) d5cU1nmBlu PercentExc:eA ,.**-("I.~-** -4310.3 -4310.3 -4310.3 -4310.3 % VDlumetric FlDw Rate DIa Average Stack Qu Vefocity (YO> 51.03 51.42 51.08 51.17 ftINC SbIck Cron..sectlonalAr. (A.) 4.28 4.28 4.28 

# r Actual Stack FlowRata (Q..,) 13093 13192 13100 13128 adm Wet Standard Stack Flow Rate (e..,) 178 792

. 791 

## m wbcIh Dry Standard Stack FlowRata (Oo.s) 12782 

### 13017 12941 12913 dsdin Percent ofIsoldnellcRata (I) 101.1 99.5 101.2 100.8 % 

## EmJa.ron Rate DIU

.....of Puticulalaon FItter (me) mg

..... ofPattIcufate In Aatone (m.') mg

..... dueto Acelanes.ntr (We> mg ToUI

.....ofpartlcuJatn (m,,) mg Slack PIII1k:uIete Conc:entndIon (c;) g/dscI (c;) trldscf PaJ1lcu/al. Emission Rate (E) kglhr (E) Ib6Itt (E) IbsImmSIu \,.7S**~,** led. U.It

### Heat 

### 'nput (HI) 

### "'AlUEI 

### IVALUE! "'ALUEI mmBtunir 

### ArmcIoy-unit 3 - M5

- Results 

### Page 1 Printed 

### 3J28I2OO8 V1.15

### METHOD 1 - SAMPLE AND VELOCITY TRAVERSES FOR CIRCULAR SOURCES
PlantN...,. 

### ArmcIOY. 

### Date 2128-311Q1YJ6 SampUng 

### Locallon Unit3 

### PraJect. 2008-135ZT 0 EQ II of Ports Avallallie 2 8tactType Circular 

### # of Ports Used 2 StactSlze large Port inside 

### DIameter 5 

## L,w Circular Stack or Duct Clamefer DIstance 

### to Far Wall 

### ofStact (L,.) 

### 33.00 In**~LnW** 

# /**~** DIstance 

### to Near Wall ofStaclt (L..) 

### 5.00 In 

# ! \

- (wUIr.lM) Diamttlll' ofstact (01 

### 28.00 In 

# V\**(-3.f4(~~ma** of Staclr (A.) 

### 4.28 ft'" I--- 

### Dlltance from 

### Port

### to DIsturbuM:ttI 

## D t-- DbtanceU 

### (8l 

### 54.50 In

# \~-~ (alloO) 

### DIameters U (So) 

### 1.95 cfiamatars '- 

### DIstance Downstream 

### CA) 

### 15.00 In (-MIl 

### Dlametln Downstntam (Ae) 

### 0.54 diametI!rs 

# T .--- Down streon"'l Number 

### ofTraverse Polnts 

### Required Minimum Number ofl 

# t Disturbance DIameters to 

## A Flow 

### DIsturbance Traverse Pornts



### Up Down PartIcuI;a Velocity 

# P Meosuren-'l en t SIreanI Stream PoInts PoInts 

### Site 

### 2.OQ.4.

### 99 0.50-1.24 24 16 5.00-5.99 1.25-1.49 20 16 

# t 6.00-6.99 1.50-1.74 16 

### 12 7.00-7.99 1.75-1.99 

### 12 12 

# B

>=S.OO >--2.00**Sor1~ Sor1~**  

### U s.-: 

### 24 16

## ~reo"., Downatrum Spec 

### 24 16 I Traverse Pts Required 

### 24 16 Disturbon ce 

# "'- =-l Check MInImum Numb«vi Points for the Up$tnNUn and Down5IrHrn condIIIcns, then USIt thelargo&t. Number ofTraverse 

### PoInD Used
z 8 fw ClrcWu Staclcl12

### to 241nchas 

### 2 ParbbV 

### 12 Across

12far CIA:uIer StIIcb 0Wf24 indies 

### 24 PtsUsed 

### 24 IReclulred 

### [0!1 PartIcUIatIe 

### [] Veloc:ltY
Traverse 

### PoInt Locallons**~m.~_T~p~q~"b** Fraction DIstance DIstance lhv_ l1"r&ctiOil o(Sl8oi:**Di~** &aaaliuill"W.D CD Tn_Point} Traverse of tram Including

Point Numbor alT_PoidaollaOi.- 

### PoInt Stacie inside 

### Nipple Numbor 2 4 6 II 10 Il 1 .1'" .067 .044 

### .an .026 .IW Number DIameter 

### Wall Length 2

.ut .J!O .1'" .1OS 

# •• JWT In in oJ .750 .l!J6**.~** 

# .J'" .UI 

### 1 0.021 5/8 

### 55/8 4 .W .704 ..513 .ll6 .177 5 JJM .677 

### ..uz .l5O 

### 2 0.067 1718 

### 6718 6 .Hi JI06 .651 ,)56 

### 3 0.118 32/8 82/8 7 .895 .774 .ut 

### 4 0.177 

### 5 10 I .!IQI .S54 .758 9 .911 Ja.J 

### 5 0.250 7 12 10 ".,4 JIG 

### 8 0.356 10 15 1.1 .!W 

### 7 

### 0.644 18 23 

### u .!n9 

### 8 0.750 21 26 

### 9 0.823 23 28 

### 10 0.882 24618 296/8 

### 11 0.933 261/8 311/8 

### 12 0.979 273/S 32 318



### Armoloy-unit 3 - M1

- Circular Page 1 Printed 

### 312812006 Vl.IS

### METHOD 2 • DETERMINATION OF STACK GAS VELOCITY AND VOLUMETRIC FLOW RATE
Plant Name 

### Arrnoloy Date**~/2008** Sampllna Locadon Unit3 

### Prajec:t' 2006-13527 OperalOr EQ .,of

### Ports UncI 

### 2 stackTwe Circulw PItGt IdeIdHIcadon PIlot Leak Check**.~.** 

## 1 PreTest , [-!) 

## I PostTest Pttot CoeftIdW 

### (CPJ 0.84
Stack DImensIons Velodly Traverse Data Dlmneter or 

### Lenatfl ofStack 

### (D) 28.00 in Run Number U3-M3Q6-V1 WIdIh ofStack (W) In RunTIme

Area ofStack (A.) 

### 4.28 

### ft" Traverse VeIocfty Stack Local PoInt Head 

## Temp Velocfty 

### Pressures (Jp) (tJ 

### (vslt BaromeIrIc Pressure (PIJ 

### 30.08 inHg 

### in H20**~** 

### ftJ&ec Stade Pressure (P..J 

### 0.21**inH~** 

### A-1 0.82 69 50.1 Absolute 

### Stack 

### Pressure (Pal 

### 30.10 inHg 

### A-2 0.85 74 51.3 A-3 

### 0.89 75 52.5 StactGas Com 

### A-4 0.86 75 51.6 ComDQSlllon 

## Data:1 Actual [.I] EstImated [] 

### A-5 0.82 75 50.4 Carbon Dloxlde ConceJ1traIfon (%COz) 

### 6.0 % J\.6 

### 0.73 76 47.6 OXygen Concentration 

### J%O:z) 

### 21.0 % 

### A-7 0.71 75 46.9 Carbon Monoxide ConcenbaIIon (%CO) 

### 0.0 % 

### A-8 

### 0.78 75 49.2 Nlbogen ConcenlJadon**(%~** 

### 73.0 % 

### A-9 0.89 75 52.5 

### Stact MoistureContw1t (8.) 

### 2.000 A-10 0.94 75 54.0 Stack 

### Dry MolecularWeIght (Mill 

### 29.80 IbllHnole 

### A-11 1.10 75 58.4 Stack Wet Molecular WeIght (M.) 

### 29.56 IbJIb.moIe 

### A-12 1.00 75 55.7 8-1 0.85 

### 72 51.2 a
..._._ 

### 8-2 0.93 74 53.7 A'll StackGas VeiocIly (val 

### 51.8 ftIsec 

### B-3 '0.91 75 53.1 Avg 8tacfr 

### Dry ltd FlGW Rate (Qm) 

### n5469 d&c:fJhr 

### 8-4 0.90 75 52.8 Ave Stack Dry

### 8td Flow Rate 

### (a..d 12924 dscfhnin 

### 8-5 0.87 75 51.9 Avg StackWet 

### Flow RaSe (Q.> 

### 13278 asdhnin**~** 

### 0.85 76 51.4 8-7 0.83 75 50.7 Stack Crass 

### Sec:tton SdlemaIk: 

### B-8 0.82 75 50.4



### A.

.. DWIKu

### fOf' Rectangular Stac:k8 

### A.

.. (lr(DJ2)2}JKy 

### for CircularStac:ka where 

### Ku =: 1 for 

### metric unita 

### where 

### Ku =: 

### 144

### frn2,onZ) for Engfaah 

### units p
... p.

### +P_tJ13.6 %N

### z

.. 100

- %COz

-

# "°
2

- "CO Md

...**44(%C~** 

### + .32(%02)

### + .28(%N2

### + %CO) 

### M."**M~1-** 

### Sw) + 

### 1SB. (olp)'Q_ a**'/~''i** 

### Arrnoloy-unit 3 - M2 B-9 

### 0.84 76 51.1 8-10 0.96 75 54.6 B-11 0.98 75 55.1 B-12 0.97 76 54.9

Av

..... 

### 0.93 75 Please report 1hoaverago filth.SqtIaI'8**~** fII olP. or. up}'fl

__ ,"**'/"E(.lp'~** Formulas Used Ts(I\1I}

# = '/nIt. +Tu where Tu

.. 273 

### OKfor metric units where Tu

# = 460 

### OR for English 

### units**VI·ICp~)'Q**..(T

..

### ..I(P.M.»IQ where 

### Kp

.. 34.97 for metriG units 

### where 

### Kp

.. 85.49for 

### Engllah uniIs 

# a...
.. 38:0(1

- 8w)v.A.(T 

### sJTSC-.vI)(PJPsW where 

### T SId

..

### 293 

## oK. PSId
.. 

### 760 mm 

### Hg, for 

### metric units 

### where T",

.. 528 

### OR, Pstd

# = 29.92 In 

### Hg, for 

### EngI'l&h units 

# ,

Page 1 Printed 312812006 V1.15

### METHOD 4

- DETERMINAT10N OF MOISTURE CONTENT IN STACK GASES
PfantNamo 

# aam,ana location Operator StacIrTypl Train Leak Check

Run Number Total MtterVolume AvgMlterTemp Avg 

### S1acIr Temp

Contents FInal Value In.IIIaIValue

NetValue
Total Volume Totaf

### WeIght Std 

### MeterVolume Calc MoistureContent

RunNumbe Total Meter Vofwne Avg MeterTemp Avg StackTemp

Contents 

### Final Value 

### fnJtIaI Value

Net Value
Total Volume Total WeIght Std Mete,Volume calc Moisture Content

Run Number Totat MeterVofum, Avg MeterTemp Avg StackTemp

CCMdeftts 

### FtnaiVaJue InftIaI

### Value

Net Value
Total Volume Total Yftlght 

### 8td Mete,Vo!ume Calc Mafslure content 

### Armoloy-unit 3

- M4 Armoloy OGle 2f.Z8.3I1Q006 Unit 3 PrOIecI.**~135'Z1** EQ • ofPorts Used 2 

### CRuIar Meter Box Number

.. 

### [-!I 

## I PreTest 

## I [-!I I PostTest MeterCal FactorM 0.955



### U3-M306-01 (Vm) 

### 93.909 

### Ct..J- 53 

## tt.>.. 75 ImDlg,r1 

### mJ 01 (V,),fN,) 

### 110.00**(VI)'(W~** 

### 100.00 (V.,),(Wn) 

### 10.0

(V,) 

### 16.00 (W,) 

### 13.10 (Vmeatlll 

### 93.161 (8...cS:.) 

### 1.5

U3-M306-02 (V,.,) 

### 93.188 

### <tn.>- 51 (t.).yg 

### 73 Implnaer1 

### ml 01 (V,).(W,) 

### 110.00 (VI).(WI) 

### 100.00 (V.,),(W.,) 

### 10.0 (V.) 

### 15.00 (W.) 

### 14.10 (Vn(.,) 

### 93.322

(B.) 

### 1.4

U3-M306-3 (V,J 

### 95.481 (t...>- 

### 58

### ~ 71 1mp(nger1 mJ 01 (V,),(W,) 

### 112.00 (VI).(W.) 

### 100.00**(V.,),~.,)** 

### 12.0**(V~** 

### 19.00**CN~** 

### 17.80 (Vrrtflltll) 

### 94.435 (B.) 

### 1.8 Mofature ContIIIt 

### Data Run 

### Start 

### 11me1 10:30 RunStoDTfme 

### 12:40 ck:f BarorneIrfc Press. (F\) 

### 30.04 in Hg 

### DF StackSIalIc PrHL 

### CP-l 0.21 InHP "F A'll Oriftce Press. (.»f).g 

## 1.n**InH~** rn'llMaer2 

### lniplftjer 3 

### 1m1ibiGii4 

### Imlifiiier• Im"""iiliiirI bnpll1l.,7 

### nil mI CI mI mI mI 

### 01 SilGef 

### 106.00 163.10 100.00 150.QO

6.0 13.1 Raub 

### mt WaterVol Condennd (V.,..,,) 

### 0.753 

### set 9 

### WaterVol WeIghed 1'1.1
-

# , 0.618 

### set dacf Sat. Moisture Content**m:;-~** 

### 3.0 "At



## or. Fhd Moisture

### content (B.) 

### 1.5 

### %
Moisture Contert

### Data Run Stan

## nmef 8:30 Run StoD 

### TIme 10:40 dcf 

### BarometrIc PrestI. (P.,) 

### 30.24 inHg 

### DF Stact

### 8tadc Press. 

### -(P...J 0.21 

### In H 20 "F Avg Ortllc:e Pross.**(~** 

### 1.84 InHzO ImPlnPr2 Impllller3 Implnger4 

## impInGe,' fml)lnler' ImpinJer7 mI mI 

### a mJ mI ml 01 

### SIlGeI 105.00 164.10 100.00 150.00

5.0 14.1 Resds 

### mI WiderVol Condensed (V.,-) 

### 0.708 scf g WaferVol WeIghed**-tV~~)** 

### 0.665 ad 

### dscf 

### sat. MoI5IUre Content (8.,_11 

### 2.7 

## or.

"At final MoIstUre Content (8.) 

### 1.4 

## or.
Moisture Content 

### Data 

### Run StaItTlme 

### 11:10 Run StoD Time 

### 13:20 dcf 

### Barametrtc 

### Press. .(P;) 30.28 inHg 

### Df Stack Stdc

### Press. 

### CP-l 0.21 inHzO 

### VF Avg Orftlce 

### Press.**(~** 

### 1.82 inHzO ImDlnaer2 3 ImDIMer4 ImDrMer. rmDlnaerl Implnger7 

### mI mI 

### a 01 Sil Gel 107.00 187.80 100.00 150.00

7.0 17.8 Resufts mI WaterVol Condensed 9 

### WaterVol-weilhed dad SaL MoistureContent



# " final MoIstUre Content



### Page 1 mI mI

(\1.,_) 

### 0.894**(V~** 

### 0.839**(e.."._~** 

### 2.5

(B.) 

### 1.8 mJ

Id Id 

# " or.

Printed 312812006 V1.1SISOKINETIC SAMPUNG DATA

Plant Name ArmO/OV Date 2128031112006 SamplinG location Unit 3 Project'**~13S27** EQ 

# Run. U3-M308-01 

# •0' PoInts Acrou 12 

## • orPorts Used 2 Ideal Nozzle DIameter

....d IsoKlnetIc 

### Factor Setup**Sam~** Equipment PIlat TubeCoefficient**(~** 0.840 Ava Stack Temp (tJ 75 Ava CJaa Meter Temp 

### <Y 45 DH

# e 0.71 SCFII (Mf0) 1.78 Avg PbtTube DItl Pruaure**(~** 0.85 Stade MoIsture Contmd (B.) 2.0 Stack Dry MoIecur.rWeight tu.) 29.80 EstfmGed Ortftce Flow Rate (a",) 0.750

DP to OM Isoklnedc 

### Factor (IQ 2.15
Pressures 8atomeIrfc Pressure**(P~** 30.04 Stade Static Pressure (P.-.) 0.21 Absolute St&dl Presan (P.) 30.08 Absolute Meter Pressure (P..,) 30.17

DryOU TravetH SarnpUng Clock 

# .... Velocity Polnt. 

## nlM nme Rudlng Heed (9)**(v~_** (.) min hh:rnm:ss 

## !t" InHzO A-1 0.0 10:30:00 223.048 0.750 A-2 5.0 10:35:00 

### 228.694 0.730 

### A-3 10.0 10:40:00 230.475 

### 0.860 A

.... 15.0 10:45:00 

### 234.253 0.820 A-5 20.0 10:50:00 237.958 0.800 A-8 25.0 10:55:00 2"'.123 0.710 A-1 30.0 11:00:00 245.458 0.700 A-8 35.0 11:05:00 249.352 0.780 

### A-9 40.0 11:10:00 253.158 0.840 A-10 45.0 11:15:00 

### 258.908 0.920 A-11 50.0 11:20:00 260.312 1.000 A-12 55.0 11:25:00 264.758 0.940 8-1 60.0 11:40:00 

### 268.957 0.810 8-2 85.0 11:45:00 

### 272.840 0.900 B-3 70.0 11:50:00 278.833 0.880 

### B-4 75.0 11:55:00 280.812 0.890 

### 8-5 SO.O 12:00:00 284.723 0.850 8-8 85.0 12:05:00 

### 288.784 0.830 

### 8-7 90.0 12:10:00 292.765 0.800 

### B-8 95.0 12:15:00 

### 298.691 0.810 8-9 100.0 12:20:00 300.645 0.830 8-10 105.0 12:25:00 304.684 0.940 8-11 110.0 12:30:00 

### 308.822 0.910 8-12 115.0 12:35:00 312.951 0.870 LastPt 120.0 12:40:00 318.955

LastPt 120.0 12:40:00 316.955 Avereve Values 0.84 

## I

Armcloy-unit3 • M5

- 

### Run 1 M

........**~F** Ueterbox Cal. Factor (Y) 

## I 0.955 

### OF Nozzle • lnHP Adu-' Nozzle Dfameta' (0.,.) 0.2170 in Inttp Req. Nozzle DIameter**~** 10.2200 In



# '" Probe ./Length 48.00 ft lbIfb.mol. 

## u.,., MaterIal 88

ICfrn Sample Cue/ Oven II 

# 1m.,.,., Case• elV. 

### LHkchec:ks InHg Pre 0 _rlmln 

# " 15 InHa InHzO MId 

### tt"1mln 

# • In Hg In Hg Post 0 

# r/mln 

# " 10 

## "'HI InH; .lV. < 0.020 

# r/mln eJ LakCheck OK? PitDtOK?**~** QrsatOK? 

## 0
DesIred Actual Meter M.ur 

## _naw 0I'Ita OrifIce StIIdc Inlet 0Utfet Fill. 

### Exit Pump

.»i .sH Temp Temp Temp Tamp Temp Vacuum (.ut) (.sH) (tJ (t".) It-) InHzO InHzO 

### OF OF OF OF OF InHg 1.811 1.600 78 44 44 

### 43 3.0 1.568 1.600 

### T1 47 46 

### 44 3.0 1.848 1.800 78 

### 48 46 

### 44 3.5 1.782 

### 1.700 

### 78 48 47 

### 44 3.5 1.719 1.700 15 49 47 44 3.5 1.525 1.500 15 

### 49 47 45 3.0 1.504 1.500 78 52 51 45 

### 3.0 1.878 1.600 78 52 50 45 3.0 1.805 1.800 75 

### 53 51 

### 48 

### 3.5 1.978 

### 2.COO 78 54 51 

### 48 

### 3.5 2.148 2.100 75 55 

### 52 41 4.0 2.019 2.000 75 56 53 47 3.5 1.740 1.700 14 54 52 41 3.0 1.933 1.900 704 54 

### 52 47 3.0 1.891 1.800 75 55 53 48 3.0 1.912 1.900 75 

### 58 53 

### 48 3.0 1.828 1.800 78 56 53 

### 48 3.0 1.783 

### 1.700 

### 76 57 54 48 3.0 1.719 1.700 78 57 

### 55 49 3.0 1.740 1.700 78 57 55 49 3.0 1.783 1.700 75 58 56 49 3.0 2.019 2.000 75 

### 58 56 49 3.5 1.955 

### 1.900 75 

### 58 58 49 3.0 1._ 1.BOO 75 

### 58 fiT 50 3.0

MaxImum Vecwm 4.0 

## I 

## 1.n 1 75 

## I 54 

## 521 1 41 

### I 53 

### Page 1 J


### Printed 3128/2008 \l1.1S

### ISOKINETlC SAMPUNG DATA

Pfan'Name MndtIy Sampling location Unit 3 EQ
• of Pomta Acrus 12 Ideal Nozzle Diameter and IloKinetic Fact. Setup Pltot Tube Coefflclent 

### (CJ 0.840 Ava StackTamp (t.) 75 OJ: Avg Oas Meter Tamp (Y 45 of DH

# e 0.76 SCFM (AMet> 1.78 In HaC Avg PItot Tube Diff. Prusul'e**(~** 0.85 "'HaC at.cIc IIDiatunt

### content (B..) 2.0 

# ,. Stack Dry MoIeculirWeIght lMm) 29.78 lbIIIHnoie Eatlmated Oriftce Flow Rata (Q,,) 0.783 aclm

DP to DH lsoldneClc Factor (K) 2.15
Pressures a.ram.tr/c Preaure <P..) 30.24 InHg StacIe StdcPruIure (P-.) 0.21 In HaC AbaoIute StackPreslure 

## (PJ 30.28 InHg Absolute MeterPressure (P..,) 

### 30.37 InHg

DryOU DesIred Actual TraverM SarnpUna Clock 

# ,.., Vllocly OrifIce 0rIIIce 

### PaInt. TImtI "TIIM ReadIng Head**~** .lIf (8) (V",)**(~)** 

### (Mil (AH) min hb:mm;ss It" IJtHaC In HaC 

### InHP A-1 0.0 

### 8:30:00 882.967 0.750 1.611 1.600 A-2 5.0 8:35:00 888.803 0.820 1.782 1.700 A.:J 10.0 8:40:00 890.452 0.870 1.889 1.900 

### A-4 15.0 8:45:00 894.358 0.830 1.783 

### 1.800 A-5 20.0 8:50:00 898.241 0.810 1.740 1.700 A-6 25.0 8:55:00 

### 901.853 0.730 1.568 1.600 A-7 30.0 9:00:00 905.458 0.700 1.SU 1.500 A-8

. 35.0 9:05:00 909.253 0.750 1.811 1.600 

### A-9 40.0 9:10:00 912.958 0.870 1.869 1.900 A-10 45.0 9:15:00 916.553 0.930 1.998 2.000 A-11 

### SO.O 9:20:00 920.154 1.100 2.383 2.400 A-12 

### SS.O 9".25:00 924.857 0.980 2.105 2.100 B-1 60.0 9:40:00 928.986 0.870 1.889 1.800 B-2 65.0 9:45:00 932.872 0.910 1.955 1.900 

### 8-3 70.0 9:50:00 

### 937.042 0.880 

### 1.891 1.900 B-4 75.0 9:55:00 941.343 0.920 1.978 2.000 

### B-5 

### SO.O 10:00:00 945.587 0.850 1.828 1.800 8-6 85.0 10:05:00 949.757 0.810 1.7040 1.700 B-7 90.0 10:10:00 953.453 0.850 1.828 1.800 

### B-8 95.0 10:15:00 

### 951.257 0.800 1.719 1.700 

### B-9 100.0 10".20:00 561.048 0.820 1.182 1.700 B-10 105.0 10:25:00 964.859 0.950 2.041 2.000 8-11 110.0 10:30:00 

### S68.852 0.910 2.084 2.000 8-12 115.0 10:35:00 972.351 0.9040 2.019 2.000 LastPt 120.0 10:40:00 978.153

FInal Value 

### 120.0 10:40:00 978.153 Average Values 0.88 

### I 1.84 

### I

ArmoIoy-unit 3 • M5

- Run 2 

### Pag., Dale 2J28-!I112OO8 Pro}ect. 2C06-13527 

### Run. U3-M3Q8.02
• ofPotts Uled 2 Samplin,**Egul~**



### Meter. 4 M

....Cal. Factor (Y) 

### 0.955 Nozzle. .t.ctu.I NouJo Dfamcar (Dr.) 0.2170 In

Req. Nozzle DIaneW**~** 0.2251 In Pralle .,Length 48.00 It LIner IIateIIII 

### sa Sample Cue I

# OVen. Case. J.V,. LukChec:b

Pre 0.001 rlrnln 

### 0 12 In Hg Mld rlmln 

# • In Hg Post 0.002 rlmln 

# • 10 InHg J.V

m C 0.020 r/mln 

## ItJ LeakCheck 01<7 PitatOK? Meter Stade 

### In

... Ta!!p Temp

(tJ t't...) of "F 70 

### 48 70 

### 48 71 47 71 47 72 

### 48 72 48 72 

### 49 

### 13 50 

### 13 50 74 51 74 51 74 

### 52 

### ·13 53



### 13 53 74 53 75 54 75 

### 55 75 

### 55 75 

### 58 74 57 

### 74 57 74 57 

### 75 

### 58 75 

### 58



### 13 

### I 52 

### I 51 

## I!I orsatOK?

### ~ 

# ....., ImplnQor Outlet FlIer 

### ExIt Pump Temp Temp Temp Vacuum (t".,) "F 

### ·F of 

### lnHl 48 34 2.5 

### 48 34 2.5 

### 48 34 3.0 

### 48 34 3.0 47 35 2.5 47 35 2.5 47 35 2.5 48 35 2.5 48 

### 36 3.0 

### 49 36 3.0 

### 49 38 3.5 49 

### 36 3.0 

### SO 37 2.5 51 37 2.5 51 

### 37 2.5 51 

### 37 3.0 52 

### 38 2.5 

### 53 

### 38 2.5 

### 54 

### 38 2.5 

### 54 

### 38 2.5 

### 54 39 2.5 55 

### 39 3.0 

### 58 39 3.0 

### 58 40 3.0

MaxImum Vacuum 3.5 

### SOl 

### I I 37

Printed 

### 3I28l2OO8 V1.1S

### ISOKINETIC SAMPUNG DATA

Plant Name Almoiay Sampling l.ocdon Unit 3 EQ
• ofPolnts Acrou 12 Ideal Nozzle Dfametllr and IsoKlnetic Factorhtup Pltol TubeCoefficient 

# <Cp) 0.840 AvgStackTemp (t.) 75 

### DF Avg CJaa Meter Temp (t",) 

### 45 of DH • 0.76 SCFU (Mf. 1.78 InHP Avg PIlat Tube Dllr. Pranura**<~** 0.85 In HzO S

..Mobture Content (B.) 2.0 

# '" Stack Dry MolecularWeight 

### tM.tJ 29.78 IbIIIHnoIo EstImIIled Ortftc:e Flow Rate (Q.,J 

## o.m 8I:fm

DP 10 DH Isoldnetlc Factor**(1g~** 2.15
Pressures Barometric Pressure (P.,) 30.2.8 InHg Stade Static Pressure (P.-) 0.21 InHzO Absolute S"Pressure (Pal 30.28 InHg Abaalute M

....Pressure (P.,) 30.39 Intis

Dry CJaa Dafred AduIJ Travern SamplIng Clock 

# .... Ve!odty OrifIce Oriftce Point. TIme 

## nme Radlng Had JH .iff (9) (V.,) (Jp) (Ali) 

### C.1H) min hh:mm:ss 

### tt' InHP InHzO inHP A-1 0.0 11:10:00 984.397 0.77 1.85 1.60 A-2 5.0 11:15:00 

### 988.087. 0.83 1.78 1.eo 

### A-3 10.0 11:20:00 991.956 0.88 1.89 1.SO A-4 15.0 11:25:00 995.952 0.85 1.83 1.80 

### A-5 20.0 11:30:00 999.758 0.81 1.74 1.70 

### A-6 25.0 11:35:00 1003.551 0.75 1.61 1.60 A-7 30.0 11:40:00 1001.259 0.72 1.55 1.60 

### A-8 35.0 11:45:00 1011.057 0.77 1.85 1.60 A-9 40.0 11:50:00 1014.853 0.88 1.85 1.80 A-10 45.0 11:55:00 1018.652 0.92 1.98 2.00 1.-11 50.0 1200:00 1022.412 0.88 1.88 1.SO 1.-12 55.0 1205:00 1028.208 0.14 2.02 2.00 8-1 60.0 12:20:00 1030.558 0.82 1.78 1.80 8-2 85.0 12:25:00 1034.759 0.89 1.91 1.90 

### B-3 70.0 12:30:00 1038.953 0.92 1.98 2.00 B-4 75.0 12:35:00 1042.703 0.87 1.87 1.90 8-5 

### SO.O 12:40:00 1048.954 0.84 1.SO 1.80 B-6 85.0 12:45:00 1051.158 0.81 1.74 1.70 8-7 90.0 12:50:00 1055.352 0.84 1.SO 1.80 

### 8-8 95.0 12:55:00 1059.543 0.80 1.72 1.70 

### 8-8 100.0 13:00:00 1083.252 0.82 1.78 1.70 8-10 105.0 13:05:00 1067.353 0.93 2.00 2.00 8-11 110.0 13:10:00 1011.552 0.98 2.08 2.00 8-12 115.0 13:15:00 1015.741 0.99 2.13 2.10 LastPt 120.0 13:20:00 1079.858

Final Value: 120.0 13:20:00 1079.858**Aver~@VaIuu** 0.85 

### I I 1.82 

### I

ArmoIoy-unit 3 - M5

- Run 3 

### Page 1 Dcte 2128-31112008 Project. 2006-13527 Run. U3-M306-3
• ofPoIb UI. 2**Sam~** Equipment 

### Meter. 4 Meterbox Cal Factor ('I) 

## I 0.955 

## I**~.** AcIuaI Noule DIameter (Q.) 

### I 0.2170 In

R.q. Nozzle DIamaIr (tY 

### I 0.2242 In ProbeIII Length 48.00 It Una MIderi8I 

### sa Sample

## caaeI OVen II I CaseII
.1V. LeakChocka

". 0.001 r/mln 

### CD 12 In Hg MId**~lmln** 

### CD In HI Stoat 0.001 rlmln 

# • 10 In HI .1V,. < 0.020**~Imln** 

## B Leak Check OK? PitDtOK? Meter Stack Inlet Temp T.,.

(I.) (Y "F of 

### 68 49 68 49 89 

### 50 89 

### 50 70 51 

### 70 

### 52 71 

### 52 71 52 72 53 72 

### 54 69 

### 57 69 64 

### 70 64 70 84 71 85 71 

### 65 72 

# sa 72 (f'f 

### 13 (f'f 

### 13 (f'f 

### 13 

### 67 74 68 74 68 75 

### 68

71 

## 1 60 

## J 58**~** orsatOK? 

## B
Meter Impfnget 0UUd FIlter Eldl Pump Temp Temp Temp Vacuum**~**

of of of In 

## HI .48 

### 4S 2.5 48 45 2.5 

### .48 

### 4S 3.0 

### 48 45 2.5 

### 48 48 2.5 49 46 2.5 50 46 2.5 50 47 2.5 50 47 2.5 52 47 3.0 

### 54 48 3.0 55 47 3.0 

### 57 47 2.5 58 47 3.0 

### 59 48 3.0 60 48 3.0 80 48 2.5 

### 82 48 2.5 

### 82 49 2.5 

### 63 49 2.5 64 50 2.5 

### 65 50 3.0 

### 68 50 3.0 

### 68 50 3.0

MaxImum Vacuum 3.0 

### 581 

### I I 47



### Printed 

### 3I2BI2OO8 V1.15

### Armoloy Corporation DeKaIb, llUDois 

### RMCElNC-Chfeago Regional OftIce Project

### #2006-13527



### APPENDIX C. 

### ANALYTICAL DATA Laboratory

### AalIyD QAlQCData

# ENVIRONMENTAL MONITORING AND TECHNOLOGIES, INC.

8100 

### North Austin Avenue· Morton Grove, tL 60053-3203 847.967.6666 • 800.246.0663 • 

### fax: 847.967.6735 • 

### www.emt.com



## Rachel Chleborowicz 

## RMC ENVIRONMENTAL 9226 North 2nd Street Machesney Park, IL 61115 RE: Armology Labs

Dear Ms. Rachel Chleborowicz: Lab Orders: 06030084 

## March 14, 2006

Enclosed are the analytical reports for the EMT Lab Order listed. Also included with this analytical report is a copy ofthe chain of custody associated with these samples. Ifyou have any questions, please contact me at 847-967-6666.
Sincerely,

Arminta P Priddy Project Manager

This Report Contains

# .-!.L pages 

## Approved by,

Mitchell Ostrowski Laboratory Director

The Contenls ofthis report apply 

### to the sample(s) analyzed. No duplicalfon is allowed except in lis enUrety.
State of illinois Chemical Analysls In Drinking Water 

### Accredited Lab. No. 100256 Slate of Wisccnsln Wasrewater and Hazardous Waste No. 999888890 

### J



## environmental laboratory and testing servic,es

# :~~ 

# Iwater 

# I soil, 

# t air.l product

# f~,~~~_l

# ____.--.__No. 100:ZS=-

# ENVIRONMENTAL MONITORING 

# AND TECHNOLOGIES, 

# INC.**------------------~----------------.-------------------------.--~~--.-** 8100 North Austin Avenue • Morton Grove, IL 60053-3203 847.967.6666 • 800.246.0663 • 

### fax: 847.967.6735 • www.emt.com



### CUENT: RMCENV1RONMENTAL Date: I4-Mar-06 

### Project: Armology Labs 

# CASE NARRATIVE Lab Order: 06030084



## Unless other wise noted, analysis conducted according to the Methods specified in 40 CFR Parts 60 or 63.
Unless 

## otherwise noted, all method blanks, laboratory spikes, andlor 

## matrix spikes met quality assurance objectives. Sample 

## results relate only to the analytes of interest tested and to the sample received at the laboratory.

Prep Comments for METHOD 306CR, 06030084-01A: initial volume was 308.2 ml. Prep Comments for METHOD 306CR, 06030084-02A: .initial volume was 295.5 mL. Prep Comments for METHOD 306CR, 06030084-03A: initial volume was 298.3 ml. Prep Comments for METHOD 306CR, 06030084-04A: initial volume was 291.7ml. Prep Comments for METHOD 306CR, 06030084-05A: initial volume was 303.2 mL. Prep Comments for METHOD 306CR. 06030084-06A: initial volume was 298.9 mL. Prep Comments for METHOD 306CR, 06030084-07A: initial volume was 30.9 mL.

# ENVIRONMENTAL MONITORING AND TECHNOLOGIES, INC.



# --------------------.------------------.----------------,------------.------.-------- 8100 

### North Austin 

### Avenue • Morton Grove, IL 60053-3203 

### 847.967.6666 • 800.246.0663 • fax: 

### 847.967.6735 • www.emt.com 

## Report ofLaboratory Analysis CLIENT: 

### RMC ENVIRONMENTAL Project: Armology Labs Report Date: 3/14/2006 

### Lab Order: 06030084**CII~nt** 

### Sample ID: 

### UNm-l Collecdon Date: 3/3/2006 

### Lab 10: 

### 06030084-01 

### EMT Matra: 

### Air Reporting Analyses Result Limit Qual Units Date Analyzed Batch Analyst
ICP Metals Total Method: METHOD 

### 3081 METHOD 308

Chromium 0.144 0.041 C JlglmL 3/9108 29503 

### ES 

### Client Sample ID: 

### Unit2-2 Collecdon Date: 3/3/2006 

### Lab 

### ID: 06030084-02 

### EMT Matra: 

### Air Reporting Analyses Result Limit Qual Units DateAnalyzed Batch Analyst
ICP Metals Total Method: METHOD 

### 3081 METHOD 308

Chromium < 0.042 0.042 C JlglmL 

### 319106 29503 

### ES 

### Client Sample ID: 

### Unit2-3 CoUecdon Date: 3/312006 

### Lab ID: 06030084-03 

### EMT Matm: 

### Air Reporting Analyses Result Limit Qual Units DateAnalyzed Batch Analyst lep Metal. Total Method: METHOD 

### 3081 METHOD 308

Chromium <0.042 0.042 C JlglmL 3/9/06 

### 29503 

### ES 

### Client Sample ID: 

### Unit3-1 Collection Date: 3/3/2006 

### LablD: 

### 06030084-04 EMT Matrix: Air Reporting Analyses Result Limit Qual Units Date Analyzed Batcb Analyst
ICP Metals Total Method: METHOD 

### 3081 METHOD 308

Chromium <0.043 0.043 C JJglmL 

### 319106 29503 

### ES

Qualifiers: B•Analyte detected in Ihe associated Melhod Blank E• Eslimaled 

## s
. Spike Recovery outside accepted recovery limits R· RPD out.dde accepled recovery limits H • Holding Time Exceeded C • Laboralory not accredited for this parameter j 

## environmental laboratory and testing services

__

# ~~



# . I water 

# I soil lair 

# l product waste 

# L_.

__ . __.--.-.____.: No. 1002158 

### =

# ENVIRONMENTAL MONITORING AND TECHNOLOGIES, INC.

8100 North Austin Avenue· Morton Grove. IL 60053-3203 

### 847.967.6666 • 800.246.0663 • fax: 

### 847.967.6735 • www.emt.com



### CUENT: 

## Report ofLaboratory Analysis RMC ENVIRONMEN1'AL Project: Annology Labs 

### Report Date: 3/14/2006 Lab Order: 06030084



### Client Sample ID: Unit3-2 CoUectlon Date: 

### 3/312006 LablD: 0603008+05 

### EMT Matrix: 

### Air Reporting Analyses Result Limit Qllal Units Date ADalyzed Batcb Analyst
ICP Metals Total Method: METHOD 

### 3081 METHOD 308



### Chromium <0.041 0.041 C 

### J,lglmL 319/06 29503 

### ES Client Sample ID: 

### Unitl-3 CoUeetfon Date: 

### 31312006 Lab ID: 06030084-06 

### EMT Matrix: 

### Air Reporting Analyses Result LJmlt Qual 

### Units Date ADalyzed Batcb Analyst
ICP Metal.Total Method: METHOD 

### 3081 METHOD 308



### Chromium < 0.042 0.042 C 

### Jlg/mL 

### 319106 29503 

### ES
CUent Sample ID: 

### blank (NaOH) CoUectlon Date: 

### 3/3/2006 Lab ID: 06030084-07 

### EMT 

### Matrix: Air Reporting Analyses Result LJmit Qual Units DateAnalyzed Batcb Analyst
ICP Metals Total Method: METHOD 

### 3081 METHOD 308



### Chromium <0.405 0.405 C 

### IJglmL 

### 319106 29503 

### ES

QUI/lfien: B • Ana/y1e detected in the associated Method Blank 

### E· Estimated S·Spike Recovery outside accepted recovery limits R· RPD outside accePted recovery limits H • Holding

## nme Exceeded C • Laboratory not acmdiled (or this panuneter 

## environmental laboratory and testing services

__________ ...

# I_w_~e~_1 soil , air

# L~roduct 

# I waste 

# i
No 1002&8

# E.NVI

# RONMENTAL 

# MONITORING AND 

# TECHNOLOGI£S.INC.

8100 NorthAustinAvenue 

### MortonGrove.lIJinois60053-3203


### Company:

__ 

## Wl_C.

__**=E.:...;;.ltfU""'~/..:..;II""'~~~uf-:%S.I-I** 

## ______ _ Address: f2.z. " IV. 

### 2 

# !WI 

# s/-. U/4P/.....,HU,¥ 

# ,l?A, CL

## ull'~

Dote: 

### Time: Relinquished 

### By: Dote: 

### Time: 

## PEClAL INSTRUCTIONS: -.1

- 0 (, 

### Recetved 

### By:



## : ZO Received 

### By: 

# Chain of Custody Record

847-967-6666 FAX: 847-967-6735 

### www.emt.com

7. 1rI Ace S.Other



### Date: 

### TIme: Date: 

## TURNARA JD TIME: 

# o RUSH

__ day turnaround 

# o ROUTINE

# ENVIRONMENTAL 

# rn MONITORING AND 

# CIl-1 TECHNOLOGIES, INC. 

# c:.J

. 

# -----------------_._---_ ....



# _._--------_._---_.-- 8100 Nort,-. Austin Avenue • Morton Grove, IL 60053-3203 847.967.6666 • 800.246.0663 • fax: 847.967.6735 • www.emt.com


## Rachel ChJeborowicz March 22, 2006 RMC ENVIRONMENTAL 9226 

## North 2nd Street 

## Machesney Park, 

## IL 61115 RE: Armology Labs

Dear Ms. Rachel Chleborowicz: Lab Orders: 06030084



## Enclosed are the QC 

## reports for the EMT Lab Order listed. If

## you have any questions, please contact me at 847-967-6666.

Sincerely,

# ~('.**r.~~** Arminta P Priddy Project Manager

The Contents ofthis report apply 

### to the sample(s) analyzed. No dupllcallon Is allowed except in Its enUrety.**..~** 

## ....., "oJ. State ofillinois

### ChamrM~lIltowd~Nilrmtz!IBstj 

## n9**services.~~\** Slate ofWlsc:onsln wastew;tter and 

### H:fJCUS Wa:sta

# r'**~;**

# IlE5DI.



# __ Lwater sOil 

## air product waste 

# I

No 100258



# . ...-**~** 

# ... ...**~~-----.--------.-** 

### ......

# - 

# -

# ENVIRONMENTAL MONITORING AND TECHNOLOGIES, 

# INC.

8100 North Austin Avenue • Morton Grove, IL 60053-3203 847.967.6666 • 800.246.0663 • fax: 847.967.6735· www.emt.com

CLIENT: RMC ENVIRONMENTAL Date: 22-Mar-06


### ProJec:t: Armology Labs 

# CASE NARRATIVE Lab Order: 06030084



## Unless other wise noted, analysis conducted according to the Methods specified in 40 CFR Parts 

## BO or B3. 

## Unless otherwise noted, all method blanks, laboratory spikes, andlor matrix spikes met quality assurance objedives. Sample results relate only to the analytes of interest tested and to the sample received at the laboratory.

Prep Comments for METHOD 30BCR, OB030084-01A: initial volume was 308.2 mL. Prep Comments for METHOD 306CR, 06030084-02A: initial volume was 295.5 mL. Prep Comments for METHOD 30BeR, 060300B4-03A: initial volume was 298.3 mL. Prep Comments for METHOD 306CR, 06030084-04A: initial volume was 291.7mL. Prep Comments 

## for METHOD 30BCR, 06030084-05A: initial volume was 303.2 mL. Prep Comments for METHOD 306CR, 06030084-06A: initial volume was 298.9 mL. Prep Comments for METHOD 30BCR, 06030084-07A: initial volume was 30.9 mL. For air samples a duplicate lCS is prepared to calculate the 

## % recoveries and RSD. No problems with the run.

2

.. ,"**·~r:Q·c** 

## environmental laboratory and testing services 

# ,,:B'!o ---_- ________1**w~ter** 

# I soil

# L:i~ 

# 1**prOd~ct** 

# I waste 

# l

___ -.:.°Noo

# loo:ZlJe_.~

# ENVIRONMENTAL MONITORING AND TECHNOLOGIES, INC.



# ----------------------------------------------------------------------------------- 8100 North Austin Avenue • Morton Grove, IL 60053-3203 847.967.6666 • 800.246.0663 • fax: 847.967.6735 • www.emt.com



### Client: RMC Work Order Number(s): 06030084


### 'Duplicate run on on LeS 

### for RPD%

"inraw data package·· Initial calibration standard results are at start ofruns, linear correlation factors listed below

Method 01l1li. Initial Date or ICV% CCVOA. MS% MSO% Ica (MOLK) MOL LCS% Calibration Analytc**Anal~.** Rcco,,-en' Recovery**~~** Recovery I RPD% Jjn Jll)m) (in DlJrn) (in ppm) 

### Recovery. 

### w'uc:s

Cr 319106 97.9 100.3 

### SeeLCS 107 

### 2.36 <0.0032 <0.0083 0.0032 

### 105 0.99947



### Comments:



# l:OOGC3 environmental laboratory and testing services



# __________**~**

# __. _______**L~vv** 

# __**a_t_e_r~l_s_o** __

# il~l 

# __**a_i_r~l~p_r._o_d** __

# u_c_t~l_vv __ a_s_t_e

__ ••



# I

_______________**~_·,_oo_2a_e** 

# ita

"'::·:'·"""""··

• '.,J .:.

.... 

# ..

. 

# .

# Environmental Monitoring & 

# Technologies, Inc. Date: 22-Mar-06



## CLIENT: Project: RMC 

### Chrome 

### Lab Order: 06030084 Sample 10: 118-21503 Client 10: Analyte Batch /0: 29503

Result 

# QC SUMMARY REPORT Method Blank

Test Code: METHOD 308 Units: pglmL Analysis Date: 319108 Prep Date: 316106 Run 10: T_ICP _060309A SeqNo: 765409 pal. SPK value SPK Ref %REC Low Urnlt High Umit RPD Ref %RPD RPDUmit Qual Val Val 

### .- 

# ---_._------_. --_
.. 

## _ ...

## - ...

## _ ..

### _..

### _.

# __ ...

### - ..

# _._-_._----- Chromium < 

### 0.0083 0.00833



## -----_ ..

# _---_._---_._------- ----- 

# --_._------ Quallnen: NO • Not Dacctcd at the Reporting Limit J• Analyte detected below quantilation limil5 S • Spike Recovay OU15idc accepted recovay limil5 R • RPO ou15idc ac:ceplCd recovery limil5 B • Analyte detected in the wocialCd Method Blank 

### I

## C' 

# o C..,) 

# c·C

# c:, Environmental Monitoring & 

## Technologies, Inc. Date: 22-Mar-06



### CLIENT: Project: RMC Chrome 

### Lab Order: 06030084 Sample 10: LCS-29S03 CllenllO: Analyte Batch 10: 28503

Result •

_ .. - • 0- ••

.**~.-** . 

# --
.... 

## QC SUMMARY REPORT Laboratory Control Spike

- generic

Test 

### Code: METHOD 306 Units: &IQImL Analysis Date: 319108 

### SeqNo: 765410 Run 10: T_ICP _O&0309A 

### PQl SPK value 

### SPK Ref Val %REC Low 

### Umlt High Urnll RPD Ref Val Prep Date: 316106

%RPO RPDUmlt Qual



# .------

..

# -- ---- -- 

# --------_._-_

.... 

# _-_. -_._-_.

# __ .. 

# --.--_. Chromium**SampleIO:LCSDUP~503** ClIent 10: Analyte 0_1747 0_00833 0.1667 

## o 105 88.6 116 0 

### Batch 10: 

### 28503 TeslCoda: METHOD 308 Units: lIg/mL Analysis Date: 319108 

### SeqNo: 765418 

### Run 10: T_lCP _060309A Prep**~ate:** 316108

Result 

### PQl SPK value SPK Ref %REC Low 

### Umlt High Urnlt RPO Ref %RPD RPDUmll Qual Val Val 

### - ._______0---

_______________. ____ . _____________... 

# --.0----
Chromium

QuaUOen: 0.1788 0.00833 0.1667 0 107 88.6 116 0.1747 2.36 20

NO

- Not Dctccled atthe Reportins Limit J - Analyte detected below quantitation limits 5 - Spike Recovery outside accepted recovery limits R - RPD outside acc:cpted recovery limits B - Analyte detected in the associated Method Blank 

### 2

# Environmental Monitoring Technologies, Inc.

Prep 

### Batch 29503 Prep Code: 306_GFAAPR Technician: Mariana Dlmltrova 

### SamplalD Matrix pH wtCKg) 

### Inlvol (mL) SoIAddad
MB-29503 300 0 LCS-29503 

### 300 0 

### Q603OO84.()1A Air 308.2 

### 0 

### 06030084-02A /tJt 295.5 

### 0 06030Q84.03A 

### Nt 298.3 

### 0 06030084-04A 

### AJt 

### 291.7 

### 0 

### 06030084-05A AJt 303.2 

### 0 

### 06030084-06A AJt 298.9 

### 0 06030084-07A 

### Nt 30.9 

### 0 LCSDUP-29503 300 0 

### SpkAddad 

# PREP BATCH REPORT Paga:1of1 

### Prep Start Date: 

### 3/612006 8:34:45 A Prep End Date: 316120064:10:13 P
Sol Racov Fin Vol (mL) 

### factor

0 50 0.1666667 0 50 0.1666667 0 50 0.1622323 0 50 0.1692047 0 50 0.1676165 0 50 0.171409 0 50 0.1649077 0 50 0.1672800 0 50 1.618123 0 50 0.1666667

# . I 

# , I I 

### \ Date:

..; (. ::: Time In: Timeout: 

# Run. Methodtl 

# 3[';.:.- OmeDa's batch 

## # TI3f:ealJlllty

### .nd •**~** mI.

# 01', Rnal 

### Vessel 

### WI. (aJ VaN. M(g} 

# Loa" IJ**~ow.,.** 

### ••tUng 

### number. 

# _------r------+---- / i Powet%:

... m'D' l' I 

## , e _r..' \.,

..**~'.** 

### 1 Blank

2 LCS / I I



### 3 

# L**(.~,)** 

# (./u P );.iiJ ,/

.---**~~--~~~~+_~~r_--_+----~------~--~~~--_+-**

# ~

# ("**.~?** /1; '/ 4

# ~JhC.J)!'{Jdlf -

# PIj) 

# I !I){ 

# J- 

# /1 LCS:

# ~ 

# ,; :J 5 , 

# ;/)!l ) 1 tj

j

- / / 

# '_

.._. _./

. - .**~+_----------i~~._F--'-~----~----+---~--_+-** 

# I (3 fl. I 

# ;g,J

# 3 ;"1 

# I



# .**{~** 

# 1"'}

# 1. 6 

## r--
.. _ ...:
..**-.~~6** 

## ., I 

### 7 

# / 

# /'

.,._

### .. 

## _ .. .. 

### B 

# /

.-

### ..

# -- -- .,

### ...

# ---- 9 

# !

---- -

# --- 10 

# ()I j) I 

# 3tJ 

# B

--- 

# _.

..--- .,---. -".-. -_.-+---1--'-

- 

# --7**11~------------+_4---~----+_-----·-~--·---------·+_·--~~** 12
/ / / / /;

### ~we"'.!..._. 

## ____**.~1:.:3+_------_f__iI__--_+---+---+_---__1~--__4_-** HN03: 14 MS 

### 'f,isnjl{acturer.

# ~ 

# t I 

# Shpt 15 MSD**~/number** 

# .ilO .'1-ltJ) 16

### ~CL 

### 17**~ufac:tuiei. ---~-+------------~1--f---f.--+----I------.;~--4-**  

# F, J),rr 18

## ~fu~r**.~~----------~~~---+----~-----~---~I-----+~**

# ~(~~t·~~~1~9~-----------_f~~--_+----_I_-----+_----__1~--__4_~ H202 20

### ~n~~r.--·~~------------+-~---I----+----~-----+----1~~ //:/ 21 I. I, alnumbsr 

## ':(1 

# '1.) / ('

# /t? 22**~+-------------r-r---~--~~----~----~~--4-~** 23


## 24"

.'

•,J: ; 0"':
.. , , lt

o:'**~:-**

';, r \ .. :-

•.. Ii : 

### ;: 

# , ,;.!


### '.**~**
., ·'i l

.



# .

, 

# - ,

### :'.'- ",


## ...**~-** , " .•**~** :.: 1·-·:**~** 

### ..



### .

# .**~,,-** .q-

: ,.;

, 

### ,



# GDOOeS