# Kleinfelder, Inc.

Air Monitoring Group 6200 Harris Technology Boulevard Charlotte, NC 28269



# Project Number: 109381

Particulate Matter, Antimony, Arsenic, Beryllium, Cadmium, Chromium, Cobalt, Lead, Manganese, Nickel & Selenium

EPA Methods 5 & 29 Analyses

Analytical Report

14360

Element One, Inc. 5022-C Wrightsville Av., Wilmington, NC 28403

910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com 

# el 1

## element One

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## The following data for Analytical Report 14360 has been reviewed for completeness, accuracy, adherence to method protocol, and compliance with quality assurance guidelines.

Review by:

Daphne Woodman, Chemist May 4, 2010

Report Reviewed and Finalized By:

Ken Smith, Laboratory Director May 4, 2010

## element One

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# SUMMARY OF RESULTS

## element One

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# Summary of Analysis

Summary of Method 5 Particulate Analysis

U1 Run 1 U1 Run 2 U1 Run 3

e14360-1 e14360-2 e14360-3 

## Fraction Catch, mg Catch, mg Catch, mg

---------------- --------------- --------------- --------------- 

## Filter 0.9 1.0 0.6

Rinse 4.9 6.1 0.5

Total PM 5.8 7.1 1.1

Train Field Blank Reagent Blank

e14360-4 e14360-5 

## Fraction Catch, mg Catch, mg

---------------- --------------- --------------- 

## Filter 0.5 NA

Rinse < 0.1 0.3

Total PM 0.5 0.3

# Summary of Analysis

Front Half - Summary of Method 29 Metals Analysis

Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 2 Unit 1 Run 3

e14360-1 FH e14360-2 FH e14360-2 FH dup e14360-3 FH 

## Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

## Antimony 0.751 < 0.1 < 0.1 < 0.1

Arsenic 1.75 1.63 1.62 1.17 Beryllium < 0.025 < 0.025 < 0.025 < 0.025

Cadmium 0.264 < 0.1 < 0.1 < 0.1

Chromium 3.15 1.32 1.28 0.934

Cobalt 0.306 < 0.1 < 0.1 < 0.1

Lead 79.5 2.79 2.86 2.35 Manganese 2.35 0.562 0.558 0.676

Nickel 10.5 6.16 6.04 2.68

Selenium 11.0 11.0 11.4 7.75

Back Half - Summary of Method 29 Metals Analysis

Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 2 Unit 1 Run 3

e14360-1 BH e14360-2 BH e14360-2 BH dup e14360-3 BH 

## Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

## Antimony 0.166 0.154 0.160 0.135

Arsenic 0.969 1.63 1.88 1.06 Beryllium < 0.025 < 0.025 < 0.025 < 0.025

Cadmium < 0.1 < 0.1 < 0.1 < 0.1

Chromium 3.36 4.75 4.78 3.15

Cobalt < 0.1 0.114 0.116 < 0.1

Lead 6.29 11.3 11.4 4.10 Manganese 0.724 1.49 1.54 0.864

Nickel 3.53 6.60 6.82 2.81

Selenium 16.1 31.6 32.8 14.5

element One

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## element One

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# Summary of Analysis

Front Half - Summary of Method 29 Blank Analysis

Train Field Blank

Front Half Reagent Blank

Front Half

e14360-4 FH e14360-5 FH 

## Element Total μg Total μg

----------------- --------------- --------------- 

## Antimony 0.553 < 0.1

Arsenic < 0.1 < 0.1 Beryllium < 0.025 < 0.025

Cadmium < 0.1 < 0.1

Chromium 0.645 0.716

Cobalt < 0.1 < 0.1

Lead 0.347 0.283 Manganese 0.433 0.510

Nickel 0.421 0.506

Selenium < 0.1 < 0.1

Back Half - Summary of Method 29 Blank Analysis

Train Field Blank

Back Half Reagent Blank

Back Half

e14360-4 BH e14360-5 BH 

## Element Total μg Total μg

----------------- --------------- --------------- 

## Antimony 0.103 < 0.1

Arsenic < 0.1 < 0.1 Beryllium < 0.025 < 0.025

Cadmium < 0.1 < 0.1

Chromium 4.68 2.78

Cobalt < 0.1 < 0.1

Lead 0.388 0.118 Manganese 0.822 0.428

Nickel 3.07 2.20

Selenium < 0.1 < 0.1

## element One

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# ANALYTICAL NARRATIVE

## element One

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# Element One Analytical Narrative

Client: Kleinfelder, Inc. Element One #: 14360

Client ID: 109381/TECO, Polk Station Analyst: DBW, RDT & KMS

Method: Methods 5 & 29 Dates Received: 04/19/10

Analytes: PM, Sb, As, Be, Cd, Cr, Co, Pb, Mn, Ni &

Se 

## Dates Analyzed: 04/26-28/10

Summary of Analysis

The Method 5 particulate samples were analyzed in accordance with EPA Method 5 guidelines. The Method 29 samples were digested, prepared, and analyzed according to Method 29 protocol . Samples were analyzed for metals using a PerkinElmer ELAN 6100 ICP-MS.

Detection Limits

The ICP-MS instrument reporting limit s were 0.25μg/L for beryllium and 1.0μg/L

for the other metals.

Analysis QA/QC

Duplicate analyses relative percent diffe rence (RPD), spike sample recovery, and

second source calibration verification data are summarized in the Quality Control Section. The beryllium spike recovery fo r the front half fracti on of Unit 1 Run 3 was outside of the ±25% laboratory guidelines with 74%. The sample was analyzed at five-fold dilution resulting in a 94% recovery; indicating matrix interference. The sample was non-det ect therefore this should have no significant impact on the results. All ot her QA/QC data was withi n the criteria of

the method.

Additional Comments

The reported results have not been correct ed for any blank values or spike recovery values. The Method 5 blank co rrection factor has been implemented. The ICP analysis of the Train Field Bl ank and Reagent Blank samples revealed

detectable concentrations of metals.

## element One

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# QUALITY CONTROL SUMMARY

## element One

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# Summary of Quality Control Data

Metals Duplicate Analysis RPD

(Method 29 QC limits: < 20% for RPD) 

## Unit 1 Run 2

Front Half Unit 1 Run 2

Back Half

Element RPD RPD

------------------ ----------------- ----------------- 

## Antimony NA 3.9%

Arsenic 0.4% 14.1% Beryllium NA NA
Cadmium NA NA
Chromium 2.9% 0.6%
Cobalt NA 1.0%

Lead 2.8% 0.9% Manganese 0.7% 2.8%

Nickel 2.0% 3.2%
Selenium 4.1% 3.7%

Metals Analysis Spike Recoveries

(Method 29 QC limits: ±25% for Spike Recoveries) 

## Unit 1 Run 3

Front Half Unit 1 Run 3

Back Half

Element Recovery Recovery

------------------ ----------------- ----------------- 

## Antimony 87% 89%

Arsenic 75% 107% Beryllium 74% 83%
Cadmium 79% 90%
Chromium 98% 102%
Cobalt 96% 99%

Lead 98% 96% Manganese 97% 99%

Nickel 95% 99%
Selenium 84% 123%

## element One

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# Summary of Quality Control Data

Second Source Calibration Check Recoveries

(Method 29 QC limits: ±10% for Second Source Continuing Check Standard*) 

## Element 0.25 ppb 1 ppb 50 ppb 100 ppb* 250 ppb

----------------- ----------------- ----------------- ----------------- ----------------- ----------------- 

## Antimony 97% 100% 102% 100%

Arsenic 108% 100% 102% 98% Beryllium 90% 99% 100% 100% 96%
Cadmium 97% 98% 101% 97%
Chromium 102% 97% 101% 99%
Cobalt 106% 97% 100% 97%

Lead 96% 98% 99% 98% Manganese 95% 94% 97% 93%

Nickel 118% 100% 102% 98%
Selenium 90% 97% 101% 97%

## element One

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# SAMPLE CUSTODY

## element One

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## element One

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# ANALYTICAL DATA

## element One

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# Analytical Calculations

MetalsElement Results (μg) =ICP Result s (μg/L)*Dilution*Final Volume (L)

WhereICP Results= Raw sample concentration (ppb)-- ICP-Data Sheet



## Dilution= Diluted Volume

-- ICP-MS Run Sheet 

## Aliquot

Final Volume=FH=Final Volume (FV)-- Sample Submission 

## BH=Received Volume (BV) .*Final Volume (FV)-- Sample Submission 

## Aliquot (Used)
Combined Results=FH+BH

MercuryMercury Results (μg) =CVAA Results (μg)*Final Volume (ml) Aliquot (ml)

WhereCVAA Results= Raw sample reading (μg)-- Hg-Data Sheet



## Aliquot= Sample Aliquot (Alq.)-- Hg-Data Sheet



## Final Volume=Final Volume (FV)*-- Sample Submission 

## * With the exception of the BH fraction where- =Received Volume (BV)-- Sample Submission

# Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/ L) – Sample Result (μg/L))X100 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)-- ICP-Data Sheet



## Sample Result = Raw sample concentration (ppb)-- ICP-Data Sheet



## Spike Amount-- ICP-MS Spike Table



## Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/ L) - Sample Result (μg/L))X100 Average (μg/L)

WhereSample Result and Duplicate Result s=Raw sample concentration (ppb)-- ICP-Data

Sheet



## Average= (Duplicate + Sample Results)

2



## element One

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## element One

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### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: Blank Sample Date/Time:

Tuesday, April 27, 2010 23:41:13 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 119880.2 ppb |- Be 9 41 ppb |- Sc 45 115625.2 ppb | Cr 52 2515 ppb | Cr 53 9383.9 ppb | Mn 55 1002.1 ppb | Ni 60 138.3 ppb | As 75 122.8 ppb | Se 77 336.3 ppb | Se 82 25.6 ppb |> Rh 103 154365.9 ppb | Cd 111 58.3 ppb |- Cd 114 152.1 ppb |- Sb 121 345 ppb | Sb 123 276 ppb |> Ho 165 461959.2 ppb |- Pb 208 2706.8 ppb

Kr 83 45.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 1 Sample Date/Time:

Tuesday, April 27, 2010 23:43:43 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 120831.4 ppb |- Be 9 706.4 0.92622 ppb |- Sc 45 116631.2 ppb | Cr 52 5976.6 0.96527 ppb | Cr 53 10435.7 2.1849 ppb | Mn 55 6550.4 0.86035 ppb | Ni 60 964.1 0.97196 ppb | As 75 660.4 0.82164 ppb | Se 77 425 1.35985 ppb | Se 82 76.9 0.63189 ppb |> Rh 103 156530.5 ppb | Cd 111 1027.6 0.93155 ppb |- Cd 114 2509.9 0.95368 ppb |- Sb 121 3648.1 0.94509 ppb | Sb 123 2766 0.91976 ppb |> Ho 165 461729.7 ppb |- Pb 208 23039.8 0.92774 ppb

Kr 83 -15.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 2 Sample Date/Time:

Tuesday, April 27, 2010 23:46:14 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 123551.7 ppb |- Be 9 72877 99.25382 ppb |- Sc 45 122141.9 ppb | Cr 52 384620 100.88834 ppb | Cr 53 56259.3 102.77051 ppb | Mn 55 668784.1 97.3608 ppb | Ni 60 92392.5 102.0725 ppb | As 75 70414.5 101.20395 ppb | Se 77 6995 100.22079 ppb | Se 82 8866.1 102.42122 ppb |> Rh 103 166814.3 ppb | Cd 111 113025 101.91452 ppb |- Cd 114 269782.2 102.39935 ppb |- Sb 121 375384.9 100.4768 ppb | Sb 123 293241.3 101.34032 ppb |> Ho 165 493090.2 ppb |- Pb 208 2339372.6 99.83066 ppb

Kr 83 -6493.6 mg/L

ICP-Data 1 of 22 

## element One

e14360-Metals 

## 33.1

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 3 Sample Date/Time:

Tuesday, April 27, 2010 23:48:46 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 115319.9 ppb |- Be 9 342639.8 500.14938 ppb |- Sc 45 117573.8 ppb | Cr 52 1802063.8 499.8224 ppb | Cr 53 222819.6 499.44353 ppb | Mn 55 3265235.2 500.52812 ppb | Ni 60 429521.1 499.58556 ppb | As 75 330226.3 499.75957 ppb | Se 77 31807.5 499.95512 ppb | Se 82 41021.3 499.51649 ppb |> Rh 103 158665.2 ppb | Cd 111 526719.8 499.61723 ppb |- Cd 114 1251076.3 499.52022 ppb |- Sb 121 1777355 499.90475 ppb | Sb 123 1376070.5 499.7321 ppb |> Ho 165 469704.6 ppb |- Pb 208 11148824 500.03401 ppb

Kr 83 -31824.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 2 Sample Date/Time:

Tuesday, April 27, 2010 23:51:19 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 115992.3 ppb |- Be 9 801.7 1.10609 ppb |- Sc 45 117721.7 ppb | Cr 52 6761.9 1.1219 ppb | Cr 53 12309.7 5.65919 ppb | Mn 55 8272.8 1.08457 ppb | Ni 60 1312.1 1.32992 ppb | As 75 901.5 1.14526 ppb | Se 77 486.7 2.08357 ppb | Se 82 101.8 0.89519 ppb |> Rh 103 161954.9 ppb | Cd 111 1242.7 1.0979 ppb |- Cd 114 3024.3 1.12067 ppb |- Sb 121 4245.3 1.09993 ppb | Sb 123 3372.8 1.12762 ppb |> Ho 165 468262.8 ppb |- Pb 208 28313.6 1.15137 ppb

Kr 83 21 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Tuesday, April 27, 2010 23:53:50 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 118330.2 ppb |- Be 9 52.7 0.01749 ppb |- Sc 45 116210.5 ppb | Cr 52 2472.7 -0.0386 ppb | Cr 53 10916.6 2.68955 ppb | Mn 55 1208.4 0.02547 ppb | Ni 60 142 -0.00197 ppb | As 75 149.6 0.03257 ppb | Se 77 368 0.29113 ppb | Se 82 6.4 -0.24313 ppb |> Rh 103 160398.4 ppb | Cd 111 64.7 0.00406 ppb |- Cd 114 171.2 0.00526 ppb |- Sb 121 299.3 -0.01438 ppb | Sb 123 223.7 -0.02067 ppb |> Ho 165 469920.7 ppb |- Pb 208 2366.8 -0.01727 ppb

Kr 83 57.5 mg/L

ICP-Data 2 of 22 

## element One

e14360-Metals 

## 33.2

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Tuesday, April 27, 2010 23:56:21 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 118659.5 ppb |- Be 9 71165.2 100.89545 ppb |- Sc 45 116616.1 ppb | Cr 52 363346.2 100.56515 ppb | Cr 53 53710.7 103.68773 ppb | Mn 55 627220.9 96.34592 ppb | Ni 60 87719.2 102.25193 ppb | As 75 66416.9 100.71824 ppb | Se 77 6603.4 99.80724 ppb | Se 82 8215.7 100.12983 ppb |> Rh 103 158090.4 ppb | Cd 111 105636.4 100.50212 ppb |- Cd 114 256023.1 102.53856 ppb |- Sb 121 352444.4 99.03611 ppb | Sb 123 274621.9 99.62888 ppb |> Ho 165 469726.7 ppb |- Pb 208 2228866.5 99.85545 ppb

Kr 83 -6170 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Tuesday, April 27, 2010 23:58:52 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 117721.2 ppb |- Be 9 45.3 0.00736 ppb |- Sc 45 116535.3 ppb | Cr 52 2497 -0.0238 ppb | Cr 53 11406.2 4.11967 ppb | Mn 55 1152.1 0.01914 ppb | Ni 60 137.3 -0.00509 ppb | As 75 121.1 -0.00596 ppb | Se 77 364 0.29496 ppb | Se 82 8.8 -0.21384 ppb |> Rh 103 158530.6 ppb | Cd 111 74.3 0.01399 ppb |- Cd 114 167.7 0.00487 ppb |- Sb 121 294 -0.01515 ppb | Sb 123 242.4 -0.0131 ppb |> Ho 165 465860.3 ppb |- Pb 208 2931.9 0.00925 ppb

Kr 83 53.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 2 Sample Date/Time:

Wednesday, April 28, 2010 00:01:23 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 121086.5 ppb |- Be 9 752 0.98843 ppb |- Sc 45 122124 ppb | Cr 52 6770.9 1.01876 ppb | Cr 53 13414.3 6.39351 ppb | Mn 55 7788.3 0.94525 ppb | Ni 60 1254.8 1.18286 ppb | As 75 909.4 1.08094 ppb | Se 77 485.7 1.63366 ppb | Se 82 96.2 0.76384 ppb |> Rh 103 171794.4 ppb | Cd 111 1167.9 0.96621 ppb |- Cd 114 2842.4 0.98567 ppb |- Sb 121 4010.2 0.98296 ppb | Sb 123 3082.2 0.97131 ppb |> Ho 165 489822.6 ppb |- Pb 208 25190 0.96016 ppb

Kr 83 -13.3 mg/L

ICP-Data 3 of 22 

## element One

e14360-Metals 

## 33.3

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 3 Sample Date/Time:

Wednesday, April 28, 2010 00:03:55 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 126574.5 ppb |- Be 9 181027.1 240.72931 ppb |- Sc 45 126382.5 ppb | Cr 52 996193.7 247.58233 ppb | Cr 53 129934.6 250.57957 ppb | Mn 55 1692126.1 232.65714 ppb | Ni 60 235940.7 246.16702 ppb | As 75 180519.5 245.05784 ppb | Se 77 17248.3 240.44653 ppb | Se 82 22195 242.34979 ppb |> Rh 103 176799 ppb | Cd 111 285668.6 243.11545 ppb |- Cd 114 680901.9 243.93201 ppb |- Sb 121 957151.6 248.48767 ppb | Sb 123 745925.6 250.02954 ppb |> Ho 165 508701.2 ppb |- Pb 208 5903098.6 244.36533 ppb

Kr 83 -17499.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 00:06:26 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 120486.3 ppb |- Be 9 71484.1 99.80149 ppb |- Sc 45 121788 ppb | Cr 52 390342.9 101.0243 ppb | Cr 53 58450.1 105.89962 ppb | Mn 55 674555.1 96.89082 ppb | Ni 60 93642.6 102.06343 ppb | As 75 71862.2 101.89467 ppb | Se 77 7180.5 101.57602 ppb | Se 82 8880.8 101.21543 ppb |> Rh 103 169073.1 ppb | Cd 111 113213.1 100.71486 ppb |- Cd 114 271007.9 101.49151 ppb |- Sb 121 379583.9 101.9757 ppb | Sb 123 293881 101.92882 ppb |> Ho 165 491280.4 ppb |- Pb 208 2317227.9 99.24341 ppb

Kr 83 -6522.3 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 5 Sample Date/Time:

Wednesday, April 28, 2010 00:08:57 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 120786.6 ppb |- Be 9 35805.4 49.84836 ppb |- Sc 45 122165 ppb | Cr 52 191427.5 48.68824 ppb | Cr 53 35813.5 55.38211 ppb | Mn 55 332058.4 47.14985 ppb | Ni 60 46385.7 49.98056 ppb | As 75 35844.2 50.23361 ppb | Se 77 3695.1 49.06437 ppb | Se 82 4305.9 48.42916 ppb |> Rh 103 170751.4 ppb | Cd 111 55704.2 49.04122 ppb |- Cd 114 134093.2 49.69207 ppb |- Sb 121 187547.6 50.05362 ppb | Sb 123 145625.4 50.18128 ppb |> Ho 165 494044 ppb |- Pb 208 1151375.1 48.97757 ppb

Kr 83 83.3 mg/L

ICP-Data 4 of 22 

## element One

e14360-Metals 

## 33.4

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 6 Sample Date/Time:

Wednesday, April 28, 2010 00:11:28 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 116103.4 ppb |- Be 9 49.7 0.01438 ppb |- Sc 45 120145.2 ppb | Cr 52 6572.4 1.14641 ppb | Cr 53 15625.8 14.79409 ppb | Mn 55 19942.9 2.96454 ppb | Ni 60 3405.3 3.8803 ppb | As 75 238.4 0.17753 ppb | Se 77 870 8.62542 ppb | Se 82 -39.7 -0.81334 ppb |> Rh 103 155353.5 ppb | Cd 111 460.5 0.38969 ppb |- Cd 114 3316.5 1.28996 ppb |- Sb 121 590.7 0.06268 ppb | Sb 123 453.7 0.05807 ppb |> Ho 165 483965.3 ppb |- Pb 208 15228.7 0.53965 ppb

Kr 83 21 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 7 Sample Date/Time:

Wednesday, April 28, 2010 00:14:00 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 105021.3 ppb |- Be 9 31 -0.00787 ppb |- Sc 45 111333.6 ppb | Cr 52 39298.4 11.12263 ppb | Cr 53 19906.8 28.00438 ppb | Mn 55 72960 11.97598 ppb | Ni 60 16489.3 20.64487 ppb | As 75 6207.4 10.00335 ppb | Se 77 1417.4 18.94035 ppb | Se 82 678.8 8.64955 ppb |> Rh 103 146265.3 ppb | Cd 111 4919.3 5.00466 ppb |- Cd 114 14118.9 6.05327 ppb |- Sb 121 322 -0.00323 ppb | Sb 123 248.8 -0.00667 ppb |> Ho 165 445657.5 ppb |- Pb 208 3033.9 0.02 ppb

Kr 83 70.2 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 8 Sample Date/Time:

Wednesday, April 28, 2010 00:16:32 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 94450 ppb |- Be 9 158 0.22403 ppb |- Sc 45 107894.2 ppb | Cr 52 4366.1 0.52667 ppb | Cr 53 16226.9 16.40138 ppb | Mn 55 2177.9 0.18526 ppb | Ni 60 291.7 0.1831 ppb | As 75 164.3 0.06526 ppb | Se 77 543 3.37022 ppb | Se 82 23.9 -0.01864 ppb |> Rh 103 154496.2 ppb | Cd 111 270.5 0.20689 ppb |- Cd 114 608.4 0.18729 ppb |- Sb 121 900 0.17694 ppb | Sb 123 738.4 0.19023 ppb |> Ho 165 431451.5 ppb |- Pb 208 5634.3 0.15178 ppb

Kr 83 25.9 mg/L

ICP-Data 5 of 22 

## element One

e14360-Metals 

## 33.5

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-FH Sample Date/Time:

Wednesday, April 28, 2010 00:19:04 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 83249.6 ppb |- Be 9 9.7 -0.03776 ppb |- Sc 45 95693.2 ppb | Cr 52 2165.3 -0.04707 ppb | Cr 53 4311 -11.31907 ppb | Mn 55 5516 0.78519 ppb | Ni 60 411.7 0.3688 ppb | As 75 96.1 -0.02848 ppb | Se 77 57.7 -4.47193 ppb | Se 82 17 -0.08794 ppb |> Rh 103 142281.7 ppb | Cd 111 33.1 -0.0219 ppb |- Cd 114 61.8 -0.03489 ppb |- Sb 121 4355 1.3075 ppb | Sb 123 3401.4 1.31604 ppb |> Ho 165 409211.1 ppb |- Pb 208 14475.5 0.62186 ppb

Kr 83 23.2 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-FH Sample Date/Time:

Wednesday, April 28, 2010 00:21:34 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 85751.4 ppb |- Be 9 22286.6 43.69321 ppb |- Sc 45 98188.6 ppb | Cr 52 135288.6 40.73784 ppb | Cr 53 18614 25.52456 ppb | Mn 55 239176.8 40.29979 ppb | Ni 60 33911.8 43.36953 ppb | As 75 23380.5 38.86631 ppb | Se 77 2124.9 31.76065 ppb | Se 82 2716.7 36.20623 ppb |> Rh 103 143800.6 ppb | Cd 111 37289.8 38.96608 ppb |- Cd 114 90049.3 39.60833 ppb |- Sb 121 101498.4 32.09683 ppb | Sb 123 78418.6 32.01351 ppb |> Ho 165 416478.2 ppb |- Pb 208 832879.9 42.01262 ppb

Kr 83 39.2 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 00:24:05 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 96486.2 ppb |- Be 9 31.3 -0.00289 ppb |- Sc 45 106842.3 ppb | Cr 52 2451 -0.00754 ppb | Cr 53 9077.3 -0.41296 ppb | Mn 55 887.4 -0.0158 ppb | Ni 60 102 -0.04132 ppb | As 75 217.8 0.15265 ppb | Se 77 393.7 1.03962 ppb | Se 82 7.8 -0.21798 ppb |> Rh 103 151993.3 ppb | Cd 111 47.8 -0.00943 ppb |- Cd 114 99.7 -0.02089 ppb |- Sb 121 1064.7 0.2247 ppb | Sb 123 846.7 0.2301 ppb |> Ho 165 433809.1 ppb |- Pb 208 1919.7 -0.03015 ppb

Kr 83 52.2 mg/L

ICP-Data 6 of 22 

## element One

e14360-Metals 

## 33.6

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 00:26:36 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 98401.6 ppb |- Be 9 62773 107.32884 ppb |- Sc 45 105959.4 ppb | Cr 52 343739.1 100.39145 ppb | Cr 53 51342 104.75991 ppb | Mn 55 583156.3 94.52544 ppb | Ni 60 81907.1 100.74833 ppb | As 75 61292.9 98.07467 ppb | Se 77 6207.1 98.92836 ppb | Se 82 7623.3 98.03485 ppb |> Rh 103 149831 ppb | Cd 111 99421.4 99.83021 ppb |- Cd 114 237469.4 100.35586 ppb |- Sb 121 332907.4 102.05824 ppb | Sb 123 257660 101.97856 ppb |> Ho 165 430525.7 ppb |- Pb 208 2100024.5 102.63575 ppb

Kr 83 -5581.3 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-1FH Sample Date/Time:

Wednesday, April 28, 2010 00:29:07 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 96229.4 ppb |- Be 9 42.7 0.01737 ppb |- Sc 45 519116.1 ppb | Cr 52 105663.3 31.50693 ppb | Cr 53 16004.8 18.59222 ppb | Mn 55 140596.8 23.51474 ppb | Ni 60 82447.3 105.20122 ppb | As 75 10651.6 17.53008 ppb | Se 77 5168.8 84.7099 ppb | Se 82 6768.4 90.28527 ppb |> Rh 103 144461.5 ppb | Cd 111 2591.4 2.6441 ppb |- Cd 114 5334.8 2.27732 ppb |- Sb 121 25436.9 7.5004 ppb | Sb 123 19732.1 7.50698 ppb |> Ho 165 442781.2 ppb |- Pb 208 17143501 815.88541 ppb

Kr 83 -515.5 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 00:31:39 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 102038.2 ppb |- Be 9 26.3 -0.01379 ppb |- Sc 45 932855.4 ppb | Cr 52 45700.3 13.17096 ppb | Cr 53 9380.2 1.42115 ppb | Mn 55 34430.1 5.61815 ppb | Ni 60 48541.7 61.62197 ppb | As 75 9948.6 16.28542 ppb | Se 77 5434 88.98107 ppb | Se 82 7049.5 93.66527 ppb |> Rh 103 145014.6 ppb | Cd 111 423.4 0.38348 ppb |- Cd 114 325.8 0.08017 ppb |- Sb 121 2460.7 0.62106 ppb | Sb 123 1872.9 0.60564 ppb |> Ho 165 451621.9 ppb |- Pb 208 625172.3 29.04427 ppb

Kr 83 -5.1 mg/L

ICP-Data 7 of 22 

## element One

e14360-Metals 

## 33.7

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 00:34:10 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 105065 ppb |- Be 9 27 -0.01455 ppb |- Sc 45 780117.7 ppb | Cr 52 46446.2 12.79698 ppb | Cr 53 10034.9 2.00654 ppb | Mn 55 35701 5.57752 ppb | Ni 60 49664.1 60.39785 ppb | As 75 10355.7 16.22467 ppb | Se 77 5577.7 87.36465 ppb | Se 82 7198.3 91.5988 ppb |> Rh 103 151426 ppb | Cd 111 406.3 0.34761 ppb |- Cd 114 289.6 0.05856 ppb |- Sb 121 2412.7 0.56562 ppb | Sb 123 1822.9 0.54617 ppb |> Ho 165 479748.5 ppb |- Pb 208 619206.2 27.07624 ppb

Kr 83 27.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 00:36:41 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 110205.3 ppb |- Be 9 21.7 -0.02458 ppb |- Sc 45 1368204.1 ppb | Cr 52 33645.9 9.34397 ppb | Cr 53 9196 0.56312 ppb | Mn 55 41944.1 6.75912 ppb | Ni 60 21533.5 26.79728 ppb | As 75 7308.6 11.70112 ppb | Se 77 3868.8 60.68433 ppb | Se 82 4757.2 62.04116 ppb |> Rh 103 147411 ppb | Cd 111 415.7 0.36919 ppb |- Cd 114 431.8 0.12325 ppb |- Sb 121 3595.7 0.8951 ppb | Sb 123 2749.6 0.87939 ppb |> Ho 165 478168.8 ppb |- Pb 208 536535.3 23.52251 ppb

Kr 83 202.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 00:39:13 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 117939.1 ppb |- Be 9 25870.8 36.88539 ppb |- Sc 45 1026159.2 ppb | Cr 52 207962.6 58.45085 ppb | Cr 53 29690.8 48.66563 ppb | Mn 55 353357.3 55.33957 ppb | Ni 60 62610.3 74.46962 ppb | As 75 31675 48.93178 ppb | Se 77 5844.2 89.67622 ppb | Se 82 7428.6 92.42434 ppb |> Rh 103 154836.1 ppb | Cd 111 40689.9 39.49577 ppb |- Cd 114 96952.2 39.61673 ppb |- Sb 121 165452.1 43.48904 ppb | Sb 123 128833.9 43.71251 ppb |> Ho 165 501583.2 ppb |- Pb 208 1687116.5 70.74244 ppb

Kr 83 219.5 mg/L

ICP-Data 8 of 22 

## element One

e14360-Metals 

## 33.8

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-4FH Sample Date/Time:

Wednesday, April 28, 2010 00:41:44 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 106385.1 ppb |- Be 9 30 -0.01007 ppb |- Sc 45 301249.3 ppb | Cr 52 24949.2 6.45445 ppb | Cr 53 6191.4 -7.57777 ppb | Mn 55 28256.2 4.32609 ppb | Ni 60 3634.7 4.21094 ppb | As 75 269.3 0.23122 ppb | Se 77 81.7 -4.14698 ppb | Se 82 -97 -1.54844 ppb |> Rh 103 153264.9 ppb | Cd 111 308.1 0.24556 ppb |- Cd 114 -200.4 -0.14584 ppb |- Sb 121 20238.2 5.55874 ppb | Sb 123 15594.2 5.52541 ppb |> Ho 165 472666.6 ppb |- Pb 208 80547.9 3.46701 ppb

Kr 83 22.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-5FH Sample Date/Time:

Wednesday, April 28, 2010 00:44:16 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 101410.9 ppb |- Be 9 18.3 -0.02674 ppb |- Sc 45 250343.8 ppb | Cr 52 26605.9 7.15831 ppb | Cr 53 5694.1 -8.37703 ppb | Mn 55 32165.3 5.09511 ppb | Ni 60 4212 5.05636 ppb | As 75 261.8 0.23284 ppb | Se 77 66.7 -4.36464 ppb | Se 82 -72.7 -1.26178 ppb |> Rh 103 148874.8 ppb | Cd 111 361.1 0.30696 ppb |- Cd 114 174 0.01179 ppb |- Sb 121 2775.4 0.7029 ppb | Sb 123 2165.9 0.70631 ppb |> Ho 165 457189.8 ppb |- Pb 208 64093.2 2.8305 ppb

Kr 83 4.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-BH Sample Date/Time:

Wednesday, April 28, 2010 00:46:48 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 108149.2 ppb |- Be 9 13.7 -0.03612 ppb |- Sc 45 120593.1 ppb | Cr 52 5756.5 0.73566 ppb | Cr 53 2778.1 -16.67737 ppb | Mn 55 13486.7 1.72102 ppb | Ni 60 5754.8 5.91934 ppb | As 75 88.9 -0.06918 ppb | Se 77 47.3 -4.80844 ppb | Se 82 8.3 -0.22573 ppb |> Rh 103 174618.7 ppb | Cd 111 40.7 -0.02181 ppb |- Cd 114 83.3 -0.03211 ppb |- Sb 121 20600.3 5.29457 ppb | Sb 123 16021 5.31442 ppb |> Ho 165 504515.5 ppb |- Pb 208 28646 1.0728 ppb

Kr 83 30.9 mg/L

ICP-Data 9 of 22 

## element One

e14360-Metals 

## 33.9

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-BH Sample Date/Time:

Wednesday, April 28, 2010 00:49:20 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 103714.8 ppb |- Be 9 25995.5 42.13734 ppb |- Sc 45 114271 ppb | Cr 52 221776.9 57.65038 ppb | Cr 53 27641.7 38.78532 ppb | Mn 55 376523.3 54.55697 ppb | Ni 60 52684.1 57.91868 ppb | As 75 27588.5 39.38613 ppb | Se 77 2214.3 27.84321 ppb | Se 82 2753.7 31.48274 ppb |> Rh 103 167398.2 ppb | Cd 111 45151.1 40.53196 ppb |- Cd 114 109350.1 41.32381 ppb |- Sb 121 153273.3 41.59336 ppb | Sb 123 118224.7 41.42821 ppb |> Ho 165 485776.3 ppb |- Pb 208 1125416.3 48.69754 ppb

Kr 83 70.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-1BH Sample Date/Time:

Wednesday, April 28, 2010 00:51:52 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 137189.6 ppb |- Be 9 19.7 -0.03344 ppb |- Sc 45 121528.2 ppb | Cr 52 126408.2 33.55474 ppb | Cr 53 17657.1 17.78398 ppb | Mn 55 49413.3 7.23714 ppb | Ni 60 31206.5 35.27078 ppb | As 75 6676.5 9.6912 ppb | Se 77 10859.5 162.95413 ppb | Se 82 13548.1 160.81262 ppb |> Rh 103 162552.1 ppb | Cd 111 -2393.9 -2.27349 ppb |- Cd 114 -6139.1 -2.44227 ppb |- Sb 121 6936.6 1.67463 ppb | Sb 123 5335.1 1.65851 ppb |> Ho 165 517146.8 ppb |- Pb 208 1547011.2 62.90721 ppb

Kr 83 -35.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 00:54:23 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 132264.6 ppb |- Be 9 22 -0.02965 ppb |- Sc 45 121477.7 ppb | Cr 52 1463.5 -0.33915 ppb | Cr 53 8638.2 -3.72684 ppb | Mn 55 803.4 -0.04304 ppb | Ni 60 135.3 -0.01854 ppb | As 75 168.8 0.04831 ppb | Se 77 263 -1.59839 ppb | Se 82 27.2 -0.01208 ppb |> Rh 103 170180.7 ppb | Cd 111 27.7 -0.03228 ppb |- Cd 114 -23.2 -0.07159 ppb |- Sb 121 307.7 -0.0199 ppb | Sb 123 240 -0.02255 ppb |> Ho 165 516032.2 ppb |- Pb 208 2642.5 -0.01553 ppb

Kr 83 50.8 mg/L

ICP-Data 10 of 22 

## element One

e14360-Metals 

## 33.10

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 00:56:54 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 129634.9 ppb |- Be 9 74942.1 97.24425 ppb |- Sc 45 117893 ppb | Cr 52 374317.4 99.11547 ppb | Cr 53 53985.1 98.8189 ppb | Mn 55 658401.1 96.77714 ppb | Ni 60 88894.6 99.15652 ppb | As 75 69094.9 100.25814 ppb | Se 77 6759.8 97.64147 ppb | Se 82 8797.3 102.62211 ppb |> Rh 103 165217.2 ppb | Cd 111 111774.6 101.767 ppb |- Cd 114 265063.3 101.59249 ppb |- Sb 121 375550.5 98.60188 ppb | Sb 123 294273.4 99.74806 ppb |> Ho 165 502687.9 ppb |- Pb 208 2391688.4 100.11041 ppb

Kr 83 -6396.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2BH Sample Date/Time:

Wednesday, April 28, 2010 00:59:26 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 136415.5 ppb |- Be 9 42.3 -0.00511 ppb |- Sc 45 112496.1 ppb | Cr 52 161535.8 47.48105 ppb | Cr 53 24006.7 37.85656 ppb | Mn 55 91684.8 14.94655 ppb | Ni 60 52938 66.02764 ppb | As 75 10153.4 16.33295 ppb | Se 77 18831.2 315.94341 ppb | Se 82 24133 315.5782 ppb |> Rh 103 147686.3 ppb | Cd 111 -2205.9 -2.30394 ppb |- Cd 114 854.7 0.3061 ppb |- Sb 121 5973.6 1.52596 ppb | Sb 123 4667.4 1.53763 ppb |> Ho 165 485804.3 ppb |- Pb 208 2600927 112.67838 ppb

Kr 83 -98.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2BH Sample Date/Time:

Wednesday, April 28, 2010 01:01:59 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 134921.9 ppb |- Be 9 24 -0.02761 ppb |- Sc 45 110967.5 ppb | Cr 52 156044.4 47.75843 ppb | Cr 53 21638.7 34.10554 ppb | Mn 55 90524 15.36565 ppb | Ni 60 52524.7 68.19025 ppb | As 75 11208.8 18.80229 ppb | Se 77 18140.8 316.92755 ppb | Se 82 24061.2 327.56296 ppb |> Rh 103 141840.9 ppb | Cd 111 -1988.4 -2.16949 ppb |- Cd 114 -5796.6 -2.66397 ppb |- Sb 121 6181.1 1.61225 ppb | Sb 123 4755.7 1.59824 ppb |> Ho 165 477139.9 ppb |- Pb 208 2576970 113.65811 ppb

Kr 83 -74.4 mg/L

ICP-Data 11 of 22 

## element One

e14360-Metals 

## 33.11

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3BH Sample Date/Time:

Wednesday, April 28, 2010 01:04:32 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 136555.5 ppb |- Be 9 16.3 -0.03745 ppb |- Sc 45 110735 ppb | Cr 52 105097.1 31.4952 ppb | Cr 53 15565.3 17.64795 ppb | Mn 55 51996.6 8.63925 ppb | Ni 60 22036 28.12558 ppb | As 75 6459.2 10.60366 ppb | Se 77 8271.4 139.54292 ppb | Se 82 10818.3 145.15778 ppb |> Rh 103 143769 ppb | Cd 111 -2407.8 -2.57753 ppb |- Cd 114 -4702.6 -2.14811 ppb |- Sb 121 5101.4 1.32704 ppb | Sb 123 4010.2 1.34544 ppb |> Ho 165 472839.1 ppb |- Pb 208 921794 40.9543 ppb

Kr 83 38.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3BH Sample Date/Time:

Wednesday, April 28, 2010 01:07:04 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 132117.2 ppb |- Be 9 32415 41.24427 ppb |- Sc 45 108435.8 ppb | Cr 52 264164.9 82.46455 ppb | Cr 53 33457.8 66.27141 ppb | Mn 55 336119.8 58.26295 ppb | Ni 60 58985.5 77.63183 ppb | As 75 37474.7 64.12152 ppb | Se 77 11780.3 206.73437 ppb | Se 82 14986.3 206.66332 ppb |> Rh 103 139942.3 ppb | Cd 111 39401.5 42.31283 ppb |- Cd 114 91124.2 41.19335 ppb |- Sb 121 159641.8 45.74251 ppb | Sb 123 123733.5 45.77066 ppb |> Ho 165 460065.9 ppb |- Pb 208 1939911.7 88.70845 ppb

Kr 83 111.5 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-4BH Sample Date/Time:

Wednesday, April 28, 2010 01:09:36 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 112673.3 ppb |- Be 9 22.3 -0.024 ppb |- Sc 45 96110.6 ppb | Cr 52 133929.5 46.79745 ppb | Cr 53 16613.8 27.11417 ppb | Mn 55 42782.2 8.21906 ppb | Ni 60 20744.3 30.65656 ppb | As 75 274.6 0.33921 ppb | Se 77 42.7 -4.62427 ppb | Se 82 30 0.14426 ppb |> Rh 103 124212.6 ppb | Cd 111 -3731.9 -4.58113 ppb |- Cd 114 -17727.2 -9.08196 ppb |- Sb 121 3845.5 1.11582 ppb | Sb 123 2780.2 1.03127 ppb |> Ho 165 418533 ppb |- Pb 208 79461.9 3.87715 ppb

Kr 83 -790.9 mg/L

ICP-Data 12 of 22 

## element One

e14360-Metals 

## 33.12

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-5BH Sample Date/Time:

Wednesday, April 28, 2010 01:12:08 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 128149 ppb |- Be 9 11 -0.04315 ppb |- Sc 45 108686.6 ppb | Cr 52 98331.8 27.80643 ppb | Cr 53 12363.8 7.64545 ppb | Mn 55 27716.4 4.28131 ppb | Ni 60 18276.1 22.04529 ppb | As 75 207.5 0.13675 ppb | Se 77 28.7 -5.01343 ppb | Se 82 4.2 -0.26456 ppb |> Rh 103 151983.4 ppb | Cd 111 -3170.5 -3.20753 ppb |- Cd 114 -5086.8 -2.10456 ppb |- Sb 121 1239.1 0.23762 ppb | Sb 123 904.6 0.21562 ppb |> Ho 165 486460.1 ppb |- Pb 208 29981.4 1.17669 ppb

Kr 83 -689.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 01:14:39 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 134090.8 ppb |- Be 9 22.7 -0.02914 ppb |- Sc 45 126974 ppb | Cr 52 2038.6 -0.18428 ppb | Cr 53 9094.3 -2.53423 ppb | Mn 55 755 -0.04864 ppb | Ni 60 107.7 -0.04705 ppb | As 75 75.1 -0.08218 ppb | Se 77 361.7 -0.0763 ppb | Se 82 14.2 -0.15573 ppb |> Rh 103 168206.9 ppb | Cd 111 4.9 -0.05256 ppb |- Cd 114 -4.6 -0.06483 ppb |- Sb 121 328.7 -0.01167 ppb | Sb 123 275.7 -0.00773 ppb |> Ho 165 498067.2 ppb |- Pb 208 1603.1 -0.05563 ppb

Kr 83 43.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 01:17:09 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 128869.2 ppb |- Be 9 75323.5 98.33788 ppb |- Sc 45 120795.9 ppb | Cr 52 372604.8 100.64763 ppb | Cr 53 55517.9 104.7751 ppb | Mn 55 656172.2 98.37881 ppb | Ni 60 89568.8 101.90859 ppb | As 75 67603 100.05077 ppb | Se 77 6735.2 99.32984 ppb | Se 82 8588.9 102.17121 ppb |> Rh 103 161983.2 ppb | Cd 111 109921.5 102.07425 ppb |- Cd 114 263479.1 102.99621 ppb |- Sb 121 367193.4 98.99295 ppb | Sb 123 287337.3 100.00993 ppb |> Ho 165 489618 ppb |- Pb 208 2324677.7 99.92175 ppb

Kr 83 -6323.5 mg/L

ICP-Data 13 of 22 

## element One

e14360-Metals 

## 33.13

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-1FH Sample Date/Time:

Wednesday, April 28, 2010 08:16:22 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 108570.6 ppb |- Be 9 10.7 -0.04104 ppb |- Sc 45 199248.5 ppb | Cr 52 38781.6 6.58987 ppb | Cr 53 16828.1 4.11916 ppb | Mn 55 49364.4 4.9759 ppb | Ni 60 28584.6 22.39508 ppb | As 75 4022.3 3.94045 ppb | Se 77 2828.1 24.99503 ppb | Se 82 2705.1 22.03978 ppb |> Rh 103 233852.3 ppb | Cd 111 832.6 0.47888 ppb |- Cd 114 1535.8 0.35395 ppb |- Sb 121 8445.6 1.86902 ppb | Sb 123 6438.9 1.8351 ppb |> Ho 165 567005.5 ppb |- Pb 208 4285349.5 159.08908 ppb

Kr 83 -75.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 08:18:53 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 110472.3 ppb |- Be 9 8 -0.04539 ppb |- Sc 45 238396.7 ppb | Cr 52 15928.6 2.52067 ppb | Cr 53 16778.3 6.18451 ppb | Mn 55 11773.3 1.16341 ppb | Ni 60 14935.6 12.5549 ppb | As 75 3512.2 3.70146 ppb | Se 77 2580.4 24.52209 ppb | Se 82 2499.1 21.96825 ppb |> Rh 103 216741.3 ppb | Cd 111 106.9 0.0174 ppb |- Cd 114 80.9 -0.03879 ppb |- Sb 121 819.7 0.09671 ppb | Sb 123 672.8 0.10504 ppb |> Ho 165 554657 ppb |- Pb 208 149922 5.57245 ppb

Kr 83 85.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 08:21:25 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 108750.2 ppb |- Be 9 6.7 -0.04721 ppb |- Sc 45 226799.6 ppb | Cr 52 15157.6 2.54115 ppb | Cr 53 16902.5 8.02647 ppb | Mn 55 11804.3 1.24335 ppb | Ni 60 14793.7 13.15723 ppb | As 75 3530.9 3.9484 ppb | Se 77 2506.3 25.33222 ppb | Se 82 2460.1 22.88401 ppb |> Rh 103 204946.1 ppb | Cd 111 115.9 0.02817 ppb |- Cd 114 107.5 -0.02917 ppb |- Sb 121 744.4 0.08205 ppb | Sb 123 578 0.07917 ppb |> Ho 165 544057.1 ppb |- Pb 208 151136.4 5.72924 ppb

Kr 83 97.6 mg/L

ICP-Data 14 of 22 

## element One

e14360-Metals 

## 33.14

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 08:23:57 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 110161.1 ppb |- Be 9 10.7 -0.04119 ppb |- Sc 45 347391.6 ppb | Cr 52 10461.7 1.60086 ppb | Cr 53 16323.1 7.89441 ppb | Mn 55 11747.6 1.27952 ppb | Ni 60 6311.2 5.69564 ppb | As 75 2343.7 2.63936 ppb | Se 77 1890.2 18.46626 ppb | Se 82 1627.6 15.50017 ppb |> Rh 103 198816.9 ppb | Cd 111 110.9 0.02721 ppb |- Cd 114 123.3 -0.02306 ppb |- Sb 121 1025.7 0.15144 ppb | Sb 123 804.3 0.1512 ppb |> Ho 165 542203.2 ppb |- Pb 208 123979.6 4.6946 ppb

Kr 83 203.3 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 08:26:29 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 99757.3 ppb |- Be 9 27755.6 46.79639 ppb |- Sc 45 318754.6 ppb | Cr 52 206002.7 49.67952 ppb | Cr 53 39227.4 58.33229 ppb | Mn 55 349954.9 47.10411 ppb | Ni 60 52369.1 53.49942 ppb | As 75 35495.5 47.13627 ppb | Se 77 4782.9 61.45322 ppb | Se 82 5404.2 57.66951 ppb |> Rh 103 180127.5 ppb | Cd 111 52873 44.12074 ppb |- Cd 114 128266 45.04877 ppb |- Sb 121 193364.4 51.33225 ppb | Sb 123 148555.2 50.91016 ppb |> Ho 165 496770.9 ppb |- Pb 208 1269631.4 53.72333 ppb

Kr 83 146.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 08:41:43 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 120002.7 ppb |- Be 9 40 -0.00133 ppb |- Sc 45 129018.6 ppb | Cr 52 1861.5 -0.2909 ppb | Cr 53 13406.7 3.31421 ppb | Mn 55 1065.7 -0.02275 ppb | Ni 60 118.7 -0.05102 ppb | As 75 92 -0.07627 ppb | Se 77 421.3 0.0378 ppb | Se 82 26.2 -0.05397 ppb |> Rh 103 192031.6 ppb | Cd 111 48.4 -0.01878 ppb |- Cd 114 128.2 -0.02008 ppb |- Sb 121 222.3 -0.04323 ppb | Sb 123 187.5 -0.04167 ppb |> Ho 165 530590.2 ppb |- Pb 208 2522.5 -0.02312 ppb

Kr 83 45.5 mg/L

ICP-Data 15 of 22 

## element One

e14360-Metals 

## 33.15

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 08:44:14 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit |> Li 6 123006.6 ppb |- Be 9 71670.1 98.0343 ppb |- Sc 45 131089 ppb | Cr 52 434816.5 99.04202 ppb | Cr 53 64543.4 102.29017 ppb | Mn 55 753874.6 95.31179 ppb | Ni 60 103294 99.10809 ppb | As 75 78983.7 98.57946 ppb | Se 77 7869.4 97.79115 ppb | Se 82 9644.7 96.72569 ppb |> Rh 103 192084.5 ppb | Cd 111 126392.6 98.9813 ppb |- Cd 114 300391.4 99.02616 ppb |- Sb 121 425681.8 105.16511 ppb | Sb 123 327894.4 104.58981 ppb |> Ho 165 534235.3 ppb |- Pb 208 2507634.5 98.76316 ppb

Kr 83 -7360.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Blank Sample Date/Time:

Wednesday, April 28, 2010 10:33:36 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 106525.7 ppb |- Sc 45 177878.8 ppb | Co 59 190.3 ppb |> Rh 103 281306.4 ppb

Ho 165 605061.1 ppb

Kr 83 77.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 1 Sample Date/Time:

Wednesday, April 28, 2010 10:35:08 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 111207.4 ppb |- Sc 45 170050.1 ppb | Co 59 6891.6 0.96122 ppb |> Rh 103 266427.5 ppb

Ho 165 602279.3 ppb

Kr 83 -8 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 2 Sample Date/Time:

Wednesday, April 28, 2010 10:36:40 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 112307.6 ppb |- Sc 45 163518.7 ppb | Co 59 653480.4 99.65978 ppb |> Rh 103 249939.3 ppb

Ho 165 590157.3 ppb

Kr 83 -9124.1 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: Standard 3 Sample Date/Time:

Wednesday, April 28, 2010 10:38:13 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 107314 ppb |- Sc 45 154277.8 ppb | Co 59 3032149.7 500.06812 ppb |> Rh 103 231141.1 ppb

Ho 165 560630.9 ppb

Kr 83 -42721.2 mg/L

ICP-Data 16 of 22 

## element One

e14360-Metals 

## 33.16

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 10:39:46 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 112749.8 ppb |- Sc 45 157459.1 ppb | Co 59 1924.9 0.28179 ppb |> Rh 103 239683.6 ppb

Ho 165 576889.2 ppb

Kr 83 100.2 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 2 Sample Date/Time:

Wednesday, April 28, 2010 10:41:18 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 115434 ppb |- Sc 45 150407.4 ppb | Co 59 6626.4 1.06414 ppb |> Rh 103 231866.8 ppb

Ho 165 566148.2 ppb

Kr 83 11.1 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 3 Sample Date/Time:

Wednesday, April 28, 2010 10:42:51 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 121939 ppb |- Sc 45 157101.1 ppb | Co 59 1509728.3 243.60674 ppb |> Rh 103 236328.6 ppb

Ho 165 590054 ppb

Kr 83 -22263.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 10:44:23 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 118633.7 ppb |- Sc 45 149312.2 ppb | Co 59 586676.9 99.81326 ppb |> Rh 103 224032.8 ppb

Ho 165 567283.6 ppb

Kr 83 -8333.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 5 Sample Date/Time:

Wednesday, April 28, 2010 10:45:55 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 119161.3 ppb |- Sc 45 147729.5 ppb | Co 59 282551 48.51676 ppb |> Rh 103 221936 ppb

Ho 165 562655.3 ppb

Kr 83 122 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 6 Sample Date/Time:

Wednesday, April 28, 2010 10:47:28 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 114540 ppb |- Sc 45 141715.4 ppb | Co 59 5824.2 1.09507 ppb |> Rh 103 198017.2 ppb

Ho 165 538723.4 ppb

Kr 83 16 mg/L

ICP-Data 17 of 22 

## element One

e14360-Metals 

## 33.17

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 7 Sample Date/Time:

Wednesday, April 28, 2010 10:49:01 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 110152.8 ppb |- Sc 45 142481 ppb | Co 59 105777 20.14182 ppb |> Rh 103 199978.4 ppb

Ho 165 528304.1 ppb

Kr 83 54.8 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 11:05:58 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 124951.5 ppb |- Sc 45 139030.8 ppb | Co 59 237.3 0.01942 ppb |> Rh 103 199910.4 ppb

Ho 165 557029.4 ppb

Kr 83 70.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 11:07:30 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 122425.9 ppb |- Sc 45 133576.5 ppb | Co 59 499195.5 99.31293 ppb |> Rh 103 191608.8 ppb

Ho 165 537159.3 ppb

Kr 83 -7373.8 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-FH Sample Date/Time:

Wednesday, April 28, 2010 11:15:17 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 111597.6 ppb |- Sc 45 117314.6 ppb | Co 59 198 0.01629 ppb |> Rh 103 179754.3 ppb

Ho 165 512325.7 ppb

Kr 83 36.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-FH Sample Date/Time:

Wednesday, April 28, 2010 11:16:49 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 113463.2 ppb |- Sc 45 121984.1 ppb | Co 59 193362.1 40.57797 ppb |> Rh 103 181563.2 ppb

Ho 165 520580.6 ppb

Kr 83 47 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-1FH Sample Date/Time:

Wednesday, April 28, 2010 11:18:21 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 116504 ppb |- Sc 45 401994.9 ppb | Co 59 14484.2 3.05607 ppb |> Rh 103 179248.3 ppb

Ho 165 539838.1 ppb

Kr 83 -656.4 mg/L

ICP-Data 18 of 22 

## element One

e14360-Metals 

## 33.18

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 11:19:54 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 121485.4 ppb |- Sc 45 623121.1 ppb | Co 59 3762.1 0.77761 ppb |> Rh 103 178548.3 ppb

Ho 165 545839.3 ppb

Kr 83 -18.3 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2FH Sample Date/Time:

Wednesday, April 28, 2010 11:21:27 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 126254.9 ppb |- Sc 45 542075.2 ppb | Co 59 3752.1 0.75749 ppb |> Rh 103 182687.2 ppb

Ho 165 561811.3 ppb

Kr 83 0.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 11:23:00 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 121671.9 ppb |- Sc 45 924994.6 ppb | Co 59 3019.5 0.6544 ppb |> Rh 103 169247.2 ppb

Ho 165 538344.7 ppb

Kr 83 235.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3FH Sample Date/Time:

Wednesday, April 28, 2010 11:24:32 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 122873.3 ppb |- Sc 45 804753 ppb | Co 59 214502.1 47.76937 ppb |> Rh 103 171079.8 ppb

Ho 165 548091.5 ppb

Kr 83 222.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 11:26:04 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 119786 ppb |- Sc 45 128666.2 ppb | Co 59 332.7 0.04126 ppb |> Rh 103 189295.7 ppb

Ho 165 545176 ppb

Kr 83 52.5 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 11:27:36 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 118476.8 ppb |- Sc 45 127913.5 ppb | Co 59 480576.5 98.04773 ppb |> Rh 103 186827.7 ppb

Ho 165 538923.7 ppb

Kr 83 -7119.5 mg/L

ICP-Data 19 of 22 

## element One

e14360-Metals 

## 33.19

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-4FH Sample Date/Time:

Wednesday, April 28, 2010 11:29:09 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 102409 ppb |- Sc 45 270063.9 ppb | Co 59 646.4 0.1271 ppb |> Rh 103 161574.3 ppb

Ho 165 497409.7 ppb

Kr 83 44.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-5FH Sample Date/Time:

Wednesday, April 28, 2010 11:30:42 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 102020.6 ppb |- Sc 45 233130.3 ppb | Co 59 413 0.06908 ppb |> Rh 103 166107.8 ppb

Ho 165 499697.6 ppb

Kr 83 29.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-BH Sample Date/Time:

Wednesday, April 28, 2010 11:32:15 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 103505.4 ppb |- Sc 45 111863.6 ppb | Co 59 164.3 0.00938 ppb |> Rh 103 177643.7 ppb

Ho 165 523133.6 ppb

Kr 83 30.5 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: LRB-BH Sample Date/Time:

Wednesday, April 28, 2010 11:33:49 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 96551.4 ppb |- Sc 45 108345.7 ppb | Co 59 200569.9 46.83406 ppb |> Rh 103 163165.7 ppb

Ho 165 487631.6 ppb

Kr 83 26.9 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-1BH Sample Date/Time:

Wednesday, April 28, 2010 11:35:22 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 125815.6 ppb |- Sc 45 122865.3 ppb | Co 59 3957.2 0.84953 ppb |> Rh 103 172365.2 ppb

Ho 165 537003.9 ppb

Kr 83 -49.3 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2BH Sample Date/Time:

Wednesday, April 28, 2010 11:36:56 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 126378.5 ppb |- Sc 45 120011.1 ppb | Co 59 5088.8 1.14422 ppb |> Rh 103 165876.2 ppb

Ho 165 526518.8 ppb

Kr 83 114.1 mg/L

ICP-Data 20 of 22 

## element One

e14360-Metals 

## 33.20

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-2BH Sample Date/Time:

Wednesday, April 28, 2010 11:38:30 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 130507 ppb |- Sc 45 120683.5 ppb | Co 59 5123.8 1.15555 ppb |> Rh 103 165413.7 ppb

Ho 165 522252 ppb

Kr 83 90 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3BH Sample Date/Time:

Wednesday, April 28, 2010 11:40:04 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 132188.7 ppb |- Sc 45 119294 ppb | Co 59 2062.6 0.43953 ppb |> Rh 103 168967 ppb

Ho 165 528329.2 ppb

Kr 83 109.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-3BH Sample Date/Time:

Wednesday, April 28, 2010 11:41:37 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 132179.4 ppb |- Sc 45 120653.6 ppb | Co 59 221670.7 49.71577 ppb |> Rh 103 169925.5 ppb

Ho 165 524751.4 ppb

Kr 83 199.6 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-4BH Sample Date/Time:

Wednesday, April 28, 2010 11:43:10 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 108413 ppb |- Sc 45 106278.5 ppb | Co 59 2524.4 0.60815 ppb |> Rh 103 151890.2 ppb

Ho 165 481879.8 ppb

Kr 83 -947.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 11:44:42 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 134560.4 ppb |- Sc 45 133201.7 ppb | Co 59 212 0.0159 ppb |> Rh 103 194000.8 ppb

Ho 165 561682.6 ppb

Kr 83 56.7 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 11:46:14 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 132971.1 ppb |- Sc 45 131690 ppb | Co 59 497314.1 99.87926 ppb |> Rh 103 189851 ppb

Ho 165 558103.5 ppb

Kr 83 -7386 mg/L

ICP-Data 21 of 22 

## element One

e14360-Metals 

## 33.21

### PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report Sample ID: 14360-5BH Sample Date/Time:

Wednesday, April 28, 2010 11:47:47 Sample Description:

kLEINFLEDER

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 120418.3 ppb |- Sc 45 116151.6 ppb | Co 59 1638.8 0.32596 ppb |> Rh 103 177669.8 ppb

Ho 165 535355.6 ppb

Kr 83 -794.4 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 1 Sample Date/Time:

Wednesday, April 28, 2010 11:49:19 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 130715.3 ppb |- Sc 45 132817 ppb | Co 59 221.7 0.01809 ppb |> Rh 103 192665.8 ppb

Ho 165 547365.1 ppb

Kr 83 54 mg/L Method 6020 & 200.8 Metals Summary Report Sample ID: QC Std 4 Sample Date/Time:

Wednesday, April 28, 2010 11:50:52 Sample Description:

Concentration Results

Analyte Mass Meas. Intens. Mean Conc. Mean Report Unit

Li 6 130063.4 ppb |- Sc 45 131044 ppb | Co 59 498469.3 98.72186 ppb |> Rh 103 192447.2 ppb

Ho 165 547673.2 ppb

Kr 83 -7366.5 mg/L

ICP-Data 22 of 22 

## element One

e14360-Metals 

## 33.22