### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10771 Hopewell Power Station 1 and 2 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 10771 Hopewell Power Station 1 and 2 As Received Higher Heating Value 

### 10771 Hopewell Power Station 1 and 2 As Received % Moisture 

### 10771 Hopewell Power Station 1 and 2 As Received % Ash 

### 10771 Hopewell Power Station 1 and 2 As Received % Sulfur 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Higher Heating Value 

### 10771 Hopewell Power Station 1 and 2 Dry

basis % Ash 

### 10771 Hopewell Power Station 1 and 2 Dry

basis % Sulfur 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Antim ony 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Arsenic 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Bery llium 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Cadmium 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Chlorine 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Chromium 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Cobalt 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Fluorine 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Lead 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Manganese 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Mercury 

### 10771 Hopewell Power Station 1 and 2 Dry

basis Nickel 

### 10771 Hopewell Power Station 1 and 2 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D2015 ASTM D-3173 ASTM D-3174 ASTM D 4239 ASTM D2015 ASTM D-3174 ASTM D 4239 SW 846 7041 SW 846 7060A SW 846 6010B SW 846 6010B ASTM D4208 SW 846 6010B SW 846 6010B ASTM D3761 SW 846 6010B SW 846 6010B EPA 7473 SW 846 6010B SW 846 7740EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10771 Hopewell Power Station 1 and 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units U1/2 Coal-4 

### 4/22/2010 4/22/2010 12534.00 Btu/lb U1/2 Coal-6 

### 4/24/2010 4/24/2010 12740.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 5.47 11.09 0.83 13300 Btu/lb 11.74 0.87 5.87 9.31 0.86 13500 Btu/lb 9.9 0.91Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 1676 ppm 0.082 ppm 1.41 ppm 3.63 ppm < 5.00 2293 ppm 0.114 ppm 1.28 ppm 4.56 ppm < 5.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm < 1.00 ppm 24.5 ppm 13 ppm 7.51 ppm ppm < 1.00 ppm 21.6 ppm 11.9 ppm 8.88 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 20.1 ppm 3.61 ppm 47.9 ppm 13.8 ppm 3.95 22.7 ppm 2.97 ppm 42.6 ppm 14.5 ppm 4.3 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 11.74 78.85 78.85 5.03 1.31 0.87 9.89 80.72 80.72 5.13 1.36 0.91 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 2.2 1.97EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10771 Hopewell Power Station 1 and 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units U1/2 Coal-1 

### 4/19/2010 4/19/2010 12674.00 Btu/lb U1/2 Coal-2 

### 4/20/2010 4/20/2010 12698.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.06 9.62 0.83 13500 Btu/lb 10.24 0.88 5.6 10.14 0.84 13500 Btu/lb 10.74 0.89Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 1407 ppm 0.085 ppm 1.08 ppm 3.98 ppm < 5.00 1419 ppm 0.092 ppm 1.000 ppm 3.77 ppm < 5.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm < 1.00 ppm 23.3 ppm 7.6 ppm 8.56 ppm ppm < 1.00 ppm 14.4 ppm 12.7 ppm 11 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 21.7 ppm 4.29 ppm 46.6 ppm 13.7 ppm 22.1 ppm 3.79 ppm 49.7 ppm 14.4 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 4.65 10.24 79.98 79.98 5.11 1.35 0.88 4.1 10.74 79.95 79.95 5.1 1.39 0.89 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 2.44 1.92EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10771 Hopewell Power Station 1 and 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units U1/2 Coal-5 

### 4/23/2010 4/23/2010 12351.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.7 11.06 0.83 13200 Btu/lb 11.85 0.89Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 2163 ppm 0.121 ppm 1.52 ppm 3.84 ppm < 5.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm < 1.00 ppm 25.5 ppm 8.62 ppm 12.8 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 21.5 ppm 3.44 ppm 45.3 ppm 14.8 ppm 5.15 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 11.85 78.28 78.28 5.03 1.29 0.89 2.65 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10771 Hopewell Power Station 1 and 2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units U1/2 Coal-1 

### 4/19/2010 4/19/2010 12674.00 Btu/lb U1/2 Coal-2 

### 4/20/2010 4/20/2010 12698.00 Btu/lb U1/2 Coal-3 

### 4/21/2010 4/21/2010 12726.00 Btu/lb U1/2 Coal-6 

### 4/24/2010 4/24/2010 12740.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.06 9.62 0.83 13500 Btu/lb 10.24 0.88 5.6 10.14 0.84 13500 Btu/lb 10.74 0.89 5.46 9.69 0.81 13500 Btu/lb 10.25 0.85 5.87 9.31 0.86 13500 Btu/lb 9.9 0.91Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 1407 ppm 0.085 ppm 1.08 ppm 3.98 ppm < 5.00 1419 ppm 0.092 ppm 1.000 ppm 3.77 ppm < 5.00 1713 ppm 0.069 ppm 1.27 ppm 3.15 ppm < 5.00 2293 ppm 0.114 ppm 1.28 ppm 4.56 ppm < 5.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm < 1.00 ppm 23.3 ppm 7.6 ppm 8.56 ppm ppm < 1.00 ppm 14.4 ppm 12.7 ppm 11 ppm ppm < 1.00 ppm 21.9 ppm 6.29 ppm 8.87 ppm ppm < 1.00 ppm 21.6 ppm 11.9 ppm 8.88 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 21.7 ppm 4.29 ppm 46.6 ppm 13.7 ppm 4.65 22.1 ppm 3.79 ppm 49.7 ppm 14.4 ppm 4.1 20.6 ppm 4.7 ppm 42.3 ppm 13.7 ppm 3.95 22.7 ppm 2.97 ppm 42.6 ppm 14.5 ppm 4.3 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 10.24 79.98 79.98 5.11 1.35 0.88 2.44 10.74 79.95 79.95 5.1 1.39 0.89 1.92 10.25 79.96 79.96 5.06 1.35 0.85 2.53 9.89 80.72 80.72 5.13 1.36 0.91 1.97 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm