### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10641 Cambria Cogen B1 

### coal refuse (culm or gob)Fuel Type 2 Fuel Type 3 Other Fuel Description



### other natural gasEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 10641 Cambria Cogen B1 As Received Higher Heating Value 

### 10641 Cambria Cogen B1 As Received % Moisture 

### 10641 Cambria Cogen B1 As Received % Ash 

### 10641 Cambria Cogen B1 As Received % Sulfur 

### 10641 Cambria Cogen B1 Dry basis Higher Heating Value 

### 10641 Cambria Cogen B1 Dry basis % Ash 

### 10641 Cambria Cogen B1 Dry basis % Sulfur 

### 10641 Cambria Cogen B1 Dry basis Antim ony 

### 10641 Cambria Cogen B1 Dry basis Arsenic 

### 10641 Cambria Cogen B1 Dry basis Beryllium 

### 10641 Cambria Cogen B1 Dry basis Cadmium 

### 10641 Cambria Cogen B1 Dry basis Chlorine 

### 10641 Cambria Cogen B1 Dry basis Chromium 

### 10641 Cambria Cogen B1 Dry basis Cobalt 

### 10641 Cambria Cogen B1 Dry basis Fluorine 

### 10641 Cambria Cogen B1 Dry basis Lead 

### 10641 Cambria Cogen B1 Dry basis Manganese 

### 10641 Cambria Cogen B1 Dry basis Mercury 

### 10641 Cambria Cogen B1 Dry basis Nickel 

### 10641 Cambria Cogen B1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### D5865 D2961 D3302 D3173 D3174 D4239 D5865 D3174 D4239 D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3761 D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 Mod D3683 D3684 D3684 ModEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Metals, PM 1 

### 5/12/2010 5/12/2010 7438.00 Btu/lb Metals 2 5/12/2010 5/12/2010 7226.00 Btu/lb Metals 3, PM 2 5/13/2010 5/13/2010 7965.00 Btu/lb PM 3 5/13/2010 5/13/2010 7913.00 Btu/lb 30B -1 5/14/2010 5/14/2010 7915.00 Btu/lb 30B-2 5/14/2010 5/14/2010 7920.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 5.48 40.04 2.00 7869.00 Btu/lb 42.36 2.11 5.49 39.43 1.97 7646.00 Btu/lb 41.72 2.08 4.94 38.42 2.13 8380.00 Btu/lb 40.41 2.24 5.47 38.24 2.2 8371.00 Btu/lb 40.45 2.33 4.23 39.23 1.96 8265.00 Btu/lb 40.97 2.05 4.50 38.34 1.98 8293.00 Btu/lb 40.14 2.07Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 10.00 % 659.250 ppb <4.98 ppm 30.21 ppm <0.04 1001.00 ppm 971.090 ppb <4.73 ppm 29.62 ppm <0.04 0.10 % 650.480 ppb <4.87 ppm 25.57 ppm <0.04 941.00 ppm 712.250 ppb <4.7 ppm 23.42 ppm <0.04 140.00 ppm 502.480 ppb <4.89 ppm 28.15 ppm <0.04 0.11 % 516.860 ppb <4.64 ppm 30.88 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 49.00 ppm 26.20 ppm 35.30 ppm ppm <0.05 ppm 52.00 ppm 31.10 ppm 35.70 ppm ppm <0.05 ppm 55.50 ppm 29.40 ppm 33.70 ppm ppm <0.05 ppm 53.60 ppm 24.70 ppm 31.10 ppm ppm <0.05 ppm 51.00 ppm 29.30 ppm 32.60 ppm ppm <0.05 ppm 50.60 ppm 27.00 ppm 31.20 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 18.20 ppm 1.50 ppm 137.00 ppm <0.25 ppm 5.48 18.40 ppm 1.41 ppm 155.00 ppm <0.25 ppm 5.49 21.00 ppm 1.60 ppm 135.00 ppm <0.25 ppm 4.94 15.00 ppm 1.40 ppm 137.00 ppm <0.25 ppm 5.47 17.40 ppm 1.53 ppm 140.00 ppm <0.25 ppm 4.23 18.30 ppm 0.89 ppm 138.00 ppm <0.25 ppm 4.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 20.42 42.36 37.22 45.66 2.66 0.81 2.11 19.79 41.72 38.49 45.71 2.89 0.79 2.08 20.61 40.41 38.98 47.69 2.68 0.83 2.24 20.33 40.45 39.22 48.27 3.06 0.85 2.33 20.77 40.97 38.26 46.89 3.04 0.85 2.05 20.68 40.14 39.18 47.95 2.71 0.82 2.07 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 6.40 6.81 6.15 5.04 6.2 6.31EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 6C,7E -1 5/14/2010 5/14/2010 7915.00 Btu/lb 6C,7E-2 5/14/2010 5/14/2010 7920.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 4.23 39.23 1.96 8265.00 Btu/lb 40.97 2.05 4.50 38.34 1.98 8293.00 Btu/lb 40.14 2.07Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 140.00 ppm 502.480 ppb <4.89 ppm 28.15 ppm <0.04 0.11 % 516.860 ppb <4.64 ppm 30.88 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 51.00 ppm 29.30 ppm 32.60 ppm ppm <0.05 ppm 50.60 ppm 27.00 ppm 31.20 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 17.40 ppm 1.53 ppm 140.00 ppm <0.25 ppm 18.30 ppm 0.89 ppm 138.00 ppm <0.25 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 4.23 20.77 40.97 38.26 46.89 3.04 0.85 2.05 4.5 20.68 40.14 39.18 47.95 2.71 0.82 2.07 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 6.2 6.31EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### M10-1 5/14/2010 5/14/2010 7915.00 Btu/lb M10-2 5/14/2010 5/14/2010 7920.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 4.23 39.23 1.96 8265.00 Btu/lb 40.97 2.05 4.50 38.34 1.98 8293.00 Btu/lb 40.14 2.07Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 140.00 ppm 502.480 ppb <4.89 ppm 28.15 ppm <0.04 0.11 % 516.860 ppb <4.64 ppm 30.88 ppm <0.04Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm <0.05 ppm 51.00 ppm 29.30 ppm 32.60 ppm ppm <0.05 ppm 50.60 ppm 27.00 ppm 31.20 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 17.40 ppm 1.53 ppm 140.00 ppm <0.25 ppm 4.23 18.30 ppm 0.89 ppm 138.00 ppm <0.25 ppm 4.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 20.77 40.97 38.26 46.89 3.04 0.85 2.05 6.2 20.68 40.14 39.18 47.95 2.71 0.82 2.07 6.31 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 10641 Cambria Cogen B1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm