p. 1 

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~(qq 
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p. 14 

r 

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p. 17 

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p. 21 
p. 22 
p. 23 
p. 24 

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p. 27 
PreManufacture Notice and 

Notice of Commencement Forms 

EPA. Form 7710-25 (Rev. 5-95) 

EPA Form 7710-56 (Rev. -96) 

Installation and Use Instructions 

MS Word 6. Ofor Windows 

U.S . EPA Approved December 12,1996 

by Anthony Cheatham 

TSCA Data Administration Section 

© 

'COMPI~I:~EVC 

.ASSIST,~ ~CE 

T () O L S 

`~~ Responsible Care" 

1 A Pubric CannMnent 
reg-e-dancTConfidentia 

For Internal Review Only 

January 4, 2008 

Subject 

Handling 

Audience FTA Customers 

Purpose

based on 

: 

N10SH 

%9 e 

guidance 

product stewardship 

and the OSHA 

and 

Hazcom 

safe handling information km standard. Planned usage a 

foreseeable/potential exposure scenarios are considered. 

Potential hazards and exposure scenarios, as well as hea 

and recommended practices, a r worke 

personnel that could come in con 

nd safety precautions 

pervisors, and other 

o ~I 

A xpertise in de 

ch y un er ie core princip 

industry's Responsible Card* Global Ch 

our products are handled safely and with 

and handling 

the chemical 

ensure that 

ry stage 

of the RMdM& life cycle. As part of 

a 

ram for 

arej=AIra ft Safe Ha 

research a 

information Is available 

kno 

roduct stewardship 

nd ongoing product 

,y.r.ti: abiifty mak ideal additives f 

or itional produ a echnica! information, n o 

nsert ii rip 

: J PUBLIC HAZARD INFO"

.. . COnr 1 '" ,, "N 

Before handling ant s;111111 far to the product Materlal Safety Data Sheet (MSDS) for safe ha ng recommendations such as exposure control, PPE, spill clean up, and disposal, as well as toxicological and ecotoxicological data. 

P _ 

re stab low dust 

pofentlal, and hazardou$ po e n no occur. During fire or extreme heat conditions, hazardous decomposition products could be released such as carbon 

uct data a mTa on; 
p. 30 

afe Handling Guidelines 

eg and Confidential Information 

For Internal Review Only 

January 4, 2008 

W 

actlve fety 

rese ~ponsored b Y and 

Research ': 

. roject is focused on researching inorgan 

characteri Wtshino hazard and exposure assessmentlMs and 

information e project also features planned Implementation of a 

public resea 

'~re used exclusively as 

also 

n ders 'MW- ngof 

studies performed u 

effects, Sensitization and mutage 

DUNG 

itibiliiy testing . 

vance the 

soyst("Ps. Toxicity 

acute oral, dermal, or eye 

so been negative. 

are not available to co 

ditives in polymer a there. handling products 

and use, 

mated systems, 

:?;~.ya 

ExilbiAire Control 

r consumer contact from 

to investiga 

workplace ere 

ready r9duceT"ikpo-s-u-re-p-5!5Fn 

Where N. . possibility extits for geherating dust or liquid aerosols into the air, control 

techniquiii, . ~uch as sourti"11 enclosure (i .e., isolating the generation source from the 

worker) antf: ; i well~cies~hed exhaust ventilation system 

particulate air (Tyf~PA~.~~ should effectively remove any airbom 
Safe Handling Guidelines 

riviieged and Confidential Information 

For Internal Review Only 

January 4, 2008 

Work areas should be cleaned at the end of each shift (at a minimum), using either a 

HEPA-flltered vacuum cleaner or wet wiping methods. Dry sweeping or air hoses 

should not be used to clean work areas. Cleanup should be conducted in a manner 

that prevents contact with wastes; the disposal of all waste material should comply 

with all applicable Federal and State, and local regulations. 

consumption of food or beverages should be prevented wh 

re handled. In addition, hand-washing facilities should be provk3"d and 

workers Instructed to use them before eating, smoking, or leaving the woricsite. 

Where contact ' possible, facilities, 

changing clothes shou e eU o prevent the ina 

other areas (including take-home) caused by the tra 

clothing and skin . 

Persona! Protective Equipment 

Permeation resistant gloves (butyl or nit 

protection . In addition, disposable cove 

contamination Is possible. 

At a minimum, a NIO41jift ed, fulf 

P 

-pu 

elation potential exists while handling 

with water. If eye Irritation develops or 

In addition to the usual medical history, the attending physician may find the following exposure information useful: date and time, duration, circumstances, 

concentration, body area exposed/affected, performed first aid measures. 
p. 32 

1111l,Safe Handling Guidelines 

Privileged and Confidential Information 

For internal Review Only 

January 4, 2008 

,

Rw

w~~ONTACT -INFORMATION 

For further information and assistance with understand 

contact t 

For transportation emergencies, call CHEMTREC at 800-4249300. 

For other emergencies, call th ur emergency number 

DISCLAIMER 

REFERENCES 

' The Responsible CarO Global Charter: A Worldwide 

Arnerican Chemistry CouncY. 

i1 " . li1w =.ll =11 .N= l.hl .=ift F 1y- . c' 11/a 
Measuring body for hazardous 

substances*) 

Of 
UBLIC COPY 
p. 35 

Ode: 2008-01-17 

NO: 3 

Col'IteAb 

1 Reason for and scope of the exercise . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 

2 fdentificafion of hazardous substances . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 

3 Description of the workinp am . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 

4 Nature of ft plant and resources used . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . 5 

5 Description of the process . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 

8 Technical protective measurea . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 

7 Measuring method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 5 

8 Sampling conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 

9 Analytical method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 

10 Test reaults: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 

11 Evaluation, findings, measures to be taken . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 

Appendix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 
p. 36 

- 

cda: 2008-01-17 

Pop: 4 

1 Reason for and scope of the exercise 

To determine the ooncentratiorn 

when conducting experiments 

. , ) 

R 12, R 87 

Dust (inhatable) 10 

Dust rable 3 9 ? 

Explanation : 

l~~l~ COP 

R-PAraw 

R12 _ 

R e cam "fine" snd ~aln~u I 

3 DowAp*m of #W world 

oEated on the ground floor of 

a whole the air exchange rate is 20000 n?/h. 

The laboratory measures approximately 3.5 x 5 m with a height of approx. 3.2 m. The free-standing fume hood measures approx. 4 x 1 m and is approx. 2.5 m high. 

The tedmc;ai area is ' normai fume hoods and with walk-in free- fume mehoods. carried out in the free-standing fume hood, which slims an air rate of 2000 m'Ih. An air exchange rate of approx 5000 m'Ih is specified for the bench row, while for the laboratory as 

y7~ 
Doe: 2008-01-17 

Pop: 5 

One member of staff is responsible far the test. In total there are 4 members of 

staff in the technical service laboratory. 

.ed in a discontinuous 

to the heated reactor, the 

s`, i~esseis, eta. are used. The laboratory is supplied 

with the gas required via a compressed gas line. 

Description of the process 

The tectxical service laboratory employee is entrusted with the following tasks: 

Filling the vessel 

Controlling the plant 

Emptying the reactor 

Removing the product 

Determining the bulk density. PUBLIC COP 

One run taices apprax. 45 min. Four runs were . completed durkV the 

measurement period. 

d Technical protective measures 

- The experimental equipment is Installed in a walk-in fume hood. 

- Weighing takes place in the laboratory fume hood. 

7 Measuring method 

The ambient air caonoeritration was determined by means of measurements at 

fixed ioc~s in accordance with the Technical Regulations fbr Hazardous 

Substances (TRGS 402) "Determination and Evaluation of Concentrations of 

Hazardous Substarncss in the Air in Woiidrg Arose and with the standards 

DIN EN 482 "Workplace Atmospheres - General Requirements for the 

Pe~ormanae of Pracedures for the MeasuremOnt of Chemical Agents" and DIN 

EN 689 Workplace Atmospheres - Guidance for the Assessment of Exposure 

by Inhalation to Chemical Agents for Comparison with Limit Values and 

Measurement Strategy" . 

Sampling was perfamed using the criteria contained in DIN EN 481 

"Workplace Atmosphere; Size Fraction Definitions for Measurement of 

Airbome Parficles' . This is implemented with the criteria for determining the 

inhaiable dust frection in accordance with the procedune "Measurement of 

Hazardous Substances", No. 3010 in the BGIA instruction manual. 

When using these sampling heads, an aspiration rate of 1 .25 m/s is assured 

; ~/ 72 

I 
8 Sannpling conditlons 

The working and operating conditions during amblent air measurements 

corresponded with normal working and operating condbons. 

The measurements at fixed locations were carried out using a small batteryoperated pump of the type Buck-Cenie YSS 5 (company AP. Buck, Orlando, 

USA). 

The dust sampiinp heads used were of the type BIA GSP 3.5 fitted with a 

sudion cone for a flow rate of up to 3.5 Umin to determine the inhalabie dust 

fraction. 

Atmospheric humidity and temperature data were measured using equipment 

made by EBRO Electronic (3mbH. 

Equipment type: EBt-2TH-811 (RS 2321) 

Serial no. : 305072 

See the remits tebie for atmospheric data values. 

8 Anaiyticai nathod 

Following equilibration, the dust load on the filter was measured grevimetricaliy 

by ditferentiai weighing. 

For adaptation puupoees, the glass fiber fltter was protected from dust and left 

to stand for two days in a chamber at room temperature before use and after 

loading. 

Scales made by the company Mettler, type AE 163, accurate to 10 pp, were used for diifenentiai weighing. 
o,t~: 2008-01-17 

: 7 

10 Test fewft: 

Substance: Inhaisble d 

Filling station in thlM 

No inhalable dust could be measured In the fted-location measurement at the 

filling station up to the determination twestiol 

reshold limit is demonstrated/ 

_ fixther tx~otective meaaixes 

PUBLIC COPY 

q7 Z~ 
p. 40 

odr. 200e-o1-17 

Pspr: $ 

` 

c. ; 

I 

\ 

PUBLIC-16,COPY 
p. 41 

Autbor: 

Measurement 

INN in Ambient Air at Worlc,olare 

Performing Laboratory: 

Laboratory Project ID: 

i BL IC COPY 

CONTAINS CdNFIDF.NTIAL BUSJNESSINFoRAI,lTI©N 

2008-01-1S - Page I of 13. . y7(e 
.42 

Participants in the 

determination on site: 

LIC COPY 

CONTAINS CONFIDEIVTIAL BU'SIIVESSINFORMATION 

2008-01-15 - Page 2 of 13 

q'7 -7 
p. 43 

Table of Content 

1 Reason for and scope of the exercise. . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . .. . . . . . .. . . . . . . . . . . . . . . . . 5 

2 Description of the working area . . .. . . . . . . . . . . . . . . . . . . .. . .. . . . . . . . . . . . . . .. . . .. . . . . . .. . . .. . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . . . 5 

3 Nature of the plant and resources used. . . . . . . . .. . . . . . . . .. . . . . . . . . . ... . . . . . . . . . . . . . . . . .. . ... . . . . . . . . .. . . . . . .. . . .. . . . . . . . . . 5 

4 Description of the process . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . ... . . . . . . . . . . . . . . . . . . . . . . ... . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . 5 

5 Technical protective measures.. . . . . . . . . . . . . . . . . . . . . . . .. . . .. . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . .. . . . . . . . ... . . . . . 6 

6 Measuring System . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . .. . .. . . .. . . . . . . . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . .. . . . . . . . . . . . . . 6 

6.1 

6.2 

6.3 

S) .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . .. . 6 

L .. . . . . . . . . . .. . . .. . . .. . .. . . . . . .. . . .. . ... . . . . . .. . . . . . . . . . .. . . . . . . . .. . . . . . . 7 

e Dust Monitor (PDM). . . . . . . . . .. . . .. . .. . .. . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . .. . . . . . . 7 

6.4 Transmission Electron Microscopy (TEM). . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . 7 

7 

8 

Sampling conditions . . . . . . . . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . . . .. . . . . . .. . . . .. . . . . . . . . .. . . . . . .. . . . .. . . . . . . . . .. . . . . . . . . . . . . . . . . . . . 8 

Test Results. . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . .. ... . . .. . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . .. . . . . . . . . .. 8 

Az . . . . . . . . . . .. . . . . . . . .. . ... . . . . . .. . . . . . . . . . .. . . . . . . . . . .. . . .. . . .. . .. . . . . . . . .. . . . . . . . . ... . 8 

r . .. . . .. . . . . . . . . . . . . . . .. . . . . . . . . . .. .. . . . . . . . .. . . . . . . .. . .. . . .. . . . . . .. . . . . . . . .. . . . 8 

8 .2 .1 

8.3 Long-term m easuremenmut (6h) during routine batch-prod . . .. . . . . .10 

8.4 . . . . . .. . . . . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . ...-~~. . .. . .. . . . .11 

9 Discussion. . . . . . . . . . . . . . . .. . ... . . . . . .. . . .. . . . . . . . . . . . . . .. . . . . . .. . . . . . . . .. . .. . . . . . . .. . . .. . . . . . .. . . .. . . . . . .. . . . . . . . . . .. . . . . . . . .. . . . . . . . . .ll 

10 Conclusion . . . . . . . . .. . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . . .. . .. . . .. . . . . . . . . . . . . . . .. . . . . . . .. . . . . . .. . . .. . .. . . . . . . . . . .. . . .. . . . . . .. . . . ... . ..12 

11 Annex. . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . .. . . . . . . . ... . . . . .. . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . .. . . . .13 

Table of Figures 

Figure 1: Schematic representation of an SMPS (Source Grimm Aerosoltechnik) . . . . . . .. . .. . . . . . . . . . . . . 7 

Figure 2: SMPS Measurement for Background . . . . . .. . . . . . . . .. . . .. . . . . . . . . . . . . . .. . .. . . . . . .. . .. . . . . . . .. . . .. . . . . .. . .. . . . . 9 

Figure 3 : SMPS measurement during normal production/sampling/fi . . . . . . .10 

Figure 4: SUPS meas ents during batch-production 

~~

.. . . . . . . . . . . . . . . . . . . . . . . . . . . . .11 

Figure 5: Positio . . . .. . . .. . .. . . . . . . . . . . . . . . . . . . .. . . . . . . .. . . . . . .. . . . . . . . . . .. . . . . . . . . . . . . . . . .. .. .13 

Table of Tables 

Table 1 : Description of the Measuring Devices used . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..

. . . .. . . .. . . . . . 8 

CONTAIIVS CONFIDENTIAL BU, 

_ . 20e8-01-r5 -= Page 3 of ff ~C COPY 

y7F 
Abbreviations 

CPC Con Particle Counter 

DMA D' ' Mobility W Analyzer 

PDM Portable Dust Monitor 

SEM Scanning Electron Microscopy 

SMPS Scanning Mobility Particle Sizer 

TEM Transmission Electron Microscopy 

UHV Ultra-High Vacuum 

XPS X-ray Electron Spectroscopy 

CO 

CONTAINS CONFIDENTTAL BiISINESSINFORMATlON 

200"1-15- Page 4 of 13 

y 
1 Reason for and scope of'b"ise 

To determine the area of the production station when 

working wi ork involves production as well as 

routine sampling and filling activities. The measurement takes place at a fixed location. 

Measurements of the concentratio be conducted 

40t 

the same time. 

2 Description of the working area 

The technical dep 

The technical area is equipped with normal fume hoods and with walk-in free-standing fume 

hoods which deliver an sir exchange rate of 2000 m3/h. - test is carried out just outside the 

free-standing fume hood where the prod~~cti place in a batch mama. 

Sampling and filliag are taking place in the other free-standing fume hood. An air exchange rate 

of approx. 5000 m'/h is specified for the bench row, while for the laboratory as a whole the air 

exchange rate is 20000 m'/h. 

The laboratory measures approximately 3.5 x 5 m with a height of approx. 3.2 m. The fivestanding fume hoods measure approx. 4 x 1 m and are approx . 2.5 m high. 

One member of staff is responsible for the tesL In total there are 4 members of staff in the 

teclhnical service laboratory . 

3 Nature o the plant and resources used 

synthesized in a discontinuous process in 

addition to the heated reactor, the usual technical resources es, 

are used. `The laboratory is supplied with the gas required via a compressed gas line. 

4 Description of the process 

The technical service laboratory employee is entrusted with the following tasks: 

- Filling the vessel 

- Controlling the plant 

- Emptying the reactor 

- Removing the product 

- Determining the bulk density 

PUBLIC COPY 

One run takes approx. 45 min. Four runs were completed during the measurement period. 

CONTAINS CONFIDENTIAL BUSINESSMFORMATION 

20t}8-~1-15 - Page 5 ~1~0 

laborato 

such as *v V a S . ebc a WS . 
p. 46 

S Technical protective measures 

- The experimental equipment is installed in a walk-in fume hood. 

- Weighing takes place in the laboratory fume hood. 

6 Measuring System 

6.1 Scanning Mobility Particle Slur (SMPS) 

Scanning Mobility Particle Sizer (SMPS) spectrometer is commonly used to measure size 

distributions in the range e SMPS spectrometer uses electrical mobility to 

measure the particle size . This technique utilizes a bipolar charga to impart a known charge 

distribution on the aerosol sample . The particles are then classified according to their ability to 

traverse an electric field. The classified particles are used as a seed for a butanol dropplet, which 

can measured/counted with simple light scatter methods. 

The SMPS system consists of a Differential Mobility Analyzer (DMA) coupled to a 

Condensation Particle Counter (CPC). The DMA uses the mass dependent mobility of fine 

partic er electrical field in order to prepare a monodisperse aerosol for the 

CPC. Particle counting is then performed with the CPC. 

Through sequential run with different electrical currents in DMA it is possible to sort up to 44 

size classes. The DMA-L used in this study is suited for a range The 

gas flow In the system is produced by a regulable pump b ' ia the CPC. An impactor is build 

in the gas inlet o the DMA with a separation ' 

radioactiv isotop (Americanuam 241) is used to ensure that the particles are 

charged in a definite manner after passing through the impactor. SMPS is shown schematically 

in Figure 1 . 

LIC C 

CONTAINS CONFIDENTLlL BIIsINESS INFORN"TION 

"N-M-15 - Page 6 of 13 
p. 47 

6.3 Portable Dust Monitor (PD11) 

The dust particles are measured/counted by the physical principle of orthogonal light scattering . 

The measurement rang~ . 

6.4 Transmission Electron Microscopy (TEM) 

Traasmission electron microscopy (TE1Vn is an imaging technique whereby a beam of electrons 

is transmitted through a specimen, then an image is formed, magnified and directed to be 

detected by a sensor such as a C M allowed the production of images with 

sufficient resolution in the range 

Specific instruments used in this study are listed in Table 

PUBLIC 

1 . COPY 

CONTAINS CONFIDENTIdL BUSINESS INFORM4TION 

2009-01-15 - Page 7 of 2 3 

~~Z 
Table 1: Description of the Measuring Devices used 

Measuring devices 

Description Type Manufacturer Particle Gas Additional 

Size range Flow information 

[ca. nmj' [1/min] 

SMPS-L 5403 Grimm Aerosoltechnik 0.3 Condensation 

GmbH particle counter 

PDM 1.108 Grimm Aerosolteehnik 1.3 Optical particle 

GmbH ~--r counter 

3089 TSI Inc. 1 .5 Collector /TEM 

, 

7 Sampling conditions 

in Figure 2. 

The working and operating conditions during ambient air measurements corresponded with 

normal working and operating conditions . The sampling is performed in front of the fume hood 

with the reactor located inside . The door is closed. The point of entry from SN1PS is at a height 

of 1 .5m. (see Figure 5 in Annex). 

8 Test Results 

8.1 Backgound measurement 

8.1 .1 S ---

The background consisted in having no activity at all within the lab (incl ' 

production). At least 24h elapsed between the last production campagne and the background 

measurement. The measurement was performed on 2005-10-26 (09:32 . :7 10:04). The 

atmospheric conditions were: P,b,=1011 hPa, f j= 45.8 %; 

e concentration of particles in the 

UBLIC COPY 

CONTAINS CONFIDE]VTLU BUSINESS INFOMUTION 

2008-O1-15 - Page 8 of 13 

L{ S3 
Figure 2: SMP9lkisatonaent for Hwkgroand 

8.1.2 P 

The number Of particles (in the range the background was perfinmed 

using PDM. 'The measn~ements showed a conce~tion of 0.18N/cm3 (181 scans,181 min.). 

8.2 Measurement during routine produtdoWump

ling4m.- W--~) 

The measurement was performed on 2005-10-26 (10:13 - 10:53). no atmospheric conditions 

were: Paw- 1011 hPa, &- 44.6 OA, T- 23.3 °C. . . . . 

The measurement is . . -shwA%-yn Figure 3. 

concentration of particles in the 

LIC 

CONTAINS CONFIDENTIAL BUSINESS INF08MATION 

-- -13, -- ------ - ------ 
Figure 3: SMPS measurement during normal production/sampling/titling of Baytubes 

8.2.1 PDMINO 

The number of particles . 

productionlsamDlin filling 

8.3 Long-term measurement (6h) during routine batchP u 6 L(G 0 P ~ 

CONTAINS CONFIDENTIAL BUSIIVESS INFORMATION 

2008-01-15 - Page 10 of 13 

y f S-