## SGS Work Order:

Contents: Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 3354-003 Red Hill The Environmental Company, Inc. (TEC) 1103478

# Case Narrative THEENVC The Environmental Company, Inc. (TEC) 1103478 3354-003 Red Hill Customer: Project: 

# SGS North America Inc.

Refer to the sample receipt form for information on sample condition. 

### 1103478005 PS RHMW01-WG20 Revised Report – Sample ID was changed from “RHMWA01” to “RHMW01” at client’s request. Sample ID was changed to match COC. 

### 1103478007 PS RHMW02-WG20 AK102 - The pattern is consistent with a weathered middle distillate. 

### 1103478008 PS RHMWA01-WG20 AK102 - The pattern is consistent with a weathered middle distillate. 

### 1103478002 BMS RHMW2254-WG20 MS 8270D SIM - BMS recoveries for multiple analytes are outside of QC criteria. Refer to LCS for accuracy. 8260B - BMS recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected above the LOQ in the original sample. 

### 974519 MS 1103478001MS 8270D SIM - MS recoveries for multiple analytes are outside of QC criteria. Refer to LCS for accuracy. 

### 1103478003 BMSD RHMW2254-WG21 MSD 8270D - BMS/BMSD RPD for multiple analytes does not meet QC criteria. Results for these analytes are estimated in the original sample. 8260B - BMSD recoveries for chloroethane and benzene do not meet QC criteria (biased high). These analytes were not detected above the LOQ in the original sample. 

### 974520 MSD 1103478001MSD 8270D - MS/MSD RPD for multiple analytes does not meet QC criteria. Results for these analytes are estimated in the original sample. 

### 974727 LCSD VXX/20956 8260B - LCSD recovery for 1,1,-Trichloroethane does not meetQC criteria (biased low). Refer to LCS for accuracy. 

### 974730 CCV VMS/11399] 8260B - ICV recovery for vinyl chloride was biased high. Results may be estimated where detected.Print Date: 8/17/2010 10:37 am 

### Report of Manual Integrations
Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS 2-Methylnaphthalene PNF 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Anthracene RP 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo(a)Anthracene PNF 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo[b]Fluoranthene PNF 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo[k]fluoranthene RP 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Chrysene RP 974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Phenanthrene RP 

### Manual Integration Reason Code Descriptions Code Description O Original Chromatogram M Modified Chromatogram SS Skimmed surrogate BLG Closed baseline gap RP Reassign peak name PIR Pattern integration required IT Included tail SP Split peak RSP Removed split peak FPS Forced peak start/stop BLC Baseline correction PNF Peak not found by software All DRO/RRO analysis are integrated per SOP.

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### 3354-003 Red Hill

Project Manager jennifer.serna@sgs.com Jennifer Serna T: (808)528-1445 F:(808)528-0768 Attn: Rick Adkisson 1003 Bishop Street, Pauahi Tower Suite 1550 Honolulu, HI 96813

Certification: This data package is in compliance with the terms and conditions of the contract, both technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager. 

### 1103478 The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project: 

# Laboratory Analytical Report

Contents (Bookmarked in PDF): Cover Page Glossary Sample Summary Forms Case Narrative Sample Results Forms Batch Summary Forms (by method) Quality Control Summary Forms (by method) Chain of Custody/Sample Receipt Forms Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343f( 907)561 .5301 w ww.us.sgs.com Member of SGSGroup

### Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions (<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits. ! Surrogate out of control limits. B Indicates the analyte is found in a blank associated with the sample. CCV Continuing Calibration Verification CL Control Limit D The analyte concentration is the result of a dilution. DF Dilution Factor DL Detection Limit (i.e., maximum method detection limit) E The analyte result is above the calibrated range. F Indicates value that is greater than or equal to the DL GT Greater Than ICV Initial Calibration Verification J The quantitation is an estimation. JL The analyte was positively identified, but the quantitation is a low estimation. LCS(D) Laboratory Control Spike (Duplicate) LOD Limit of Detection (i.e., 2xDL) LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit) LT Less Than M A matrix effect was present. MB Method Blank MS(D) Matrix Spike (Duplicate) ND Indicates the analyte is not detected. Q QC parameter out of acceptance range. R Rejected RL Reporting Limit RPD Relative Percent Difference U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP. Print Date: 8/17/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-003 Red Hill Workorder No.: 1103478 

## Analytical Methods
Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS Dissolved Metals by ICP-MS SW6020 DRO by 8015C (W) SW8015C GRO (W) SW8015C Volatile Organic Compounds (W) FULL SW8260B Print Date: 8/17/2010 10:37 am



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1103478001 RHMW2254-WG20 1103478002 RHMW2254-WG20 MS 1103478003 RHMW2254-WG21 MSD 1103478004 RHMW05-WG20 1103478005 RHMW01-WG20 1103478006 RHMW03-WG20 1103478007 RHMW02-WG20 1103478008 RHMWA01-WG20 1103478009 TB01-WG20

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6555 MXX23263 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6555 Analytical Method: SW6020 Analysis Date/Time: 07/27/10 17:02 Prep Batch: MXX23263 Prep Method: SW3010A Prep Date/Time: 07/21/10 23:00 Container ID:1103478001-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 60.0 U 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 99.1 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 13:40 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478001-B Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 0.320 U 0.426 mg/L XFC9360 XXX23089 0.160 1 5a Androstane <surr> 83.1 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 940 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 18:39 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478001-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11403 VXX20964 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11403 VXX20964 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11403 VXX20964 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11403 VXX20964 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11403 VXX20964 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11403 VXX20964 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11403 VXX20964 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11403 VXX20964 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11403 VXX20964 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11403 VXX20964 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11403 VXX20964 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11403 VXX20964 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11403 VXX20964 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11403 VXX20964 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11403 VXX20964 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11403 VXX20964 0.940 1 1,2-Dichloroethane-D4 <surr> 119 73-120 % VMS11403 VXX20964 1 4-Bromofluorobenzene <surr> 92.1 76-120 % VMS11403 VXX20964 1 Toluene-d8 <surr> 96.3 80-120 % VMS11403 VXX20964 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11403 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 19:27 Prep Batch: VXX20964 Prep Method: SW5030B Prep Date/Time: 07/19/10 14:07 Container ID:1103478001-A Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW2254-WG20 SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 2-Methylnaphthalene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Acenaphthene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Acenaphthylene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Anthracene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Benzo(a)Anthracene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Benzo[a]pyrene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Benzo[b]Fluoranthene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Benzo[g,h,i]perylene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Benzo[k]fluoranthene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Chrysene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Dibenzo[a,h]anthracene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Fluoranthene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Fluorene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Indeno[1,2,3-c,d] pyrene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Naphthalene 0.0664 U 0.107 ug/L XMS5528 XXX23075 0.0332 1 Phenanthrene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Pyrene 0.0320 U 0.0535 ug/L XMS5528 XXX23075 0.0160 1 Terphenyl-d14 <surr> 93 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 935 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/19/10 23:07 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478001-I Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6543 MXX23243 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6543 Analytical Method: SW6020 Analysis Date/Time: 07/21/10 19:22 Prep Batch: MXX23243 Prep Method: SW3010A Prep Date/Time: 07/16/10 18:10 Container ID:1103478004-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 60.0 U 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 99.2 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 15:56 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478004-B Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 0.320 U 0.426 mg/L XFC9360 XXX23089 0.160 1 5a Androstane <surr> 81.7 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 940 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 19:43 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478004-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 107 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 102 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 97.7 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 08:50 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478004-A Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW05-WG20 SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 2-Methylnaphthalene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Acenaphthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Acenaphthylene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo(a)Anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[a]pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[b]Fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[g,h,i]perylene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[k]fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Chrysene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Dibenzo[a,h]anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Fluorene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Indeno[1,2,3-c,d] pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Naphthalene 0.0643J 0.105 ug/L XMS5528 XXX23075 0.0326 1 Phenanthrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Terphenyl-d14 <surr> 90.3 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 950 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 00:01 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478004-I Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6543 MXX23243 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6543 Analytical Method: SW6020 Analysis Date/Time: 07/21/10 19:40 Prep Batch: MXX23243 Prep Method: SW3010A Prep Date/Time: 07/16/10 18:10 Container ID:1103478005-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 60.0 U 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 105 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 16:15 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478005-B Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 0.228J 0.435 mg/L XFC9360 XXX23089 0.163 1 5a Androstane <surr> 85.1 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 920 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 20:04 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478005-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 1.08 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 106 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 94.8 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 99.2 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 09:24 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478005-A Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW01-WG20 SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 2-Methylnaphthalene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Acenaphthene 0.0321J 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Acenaphthylene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo(a)Anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[a]pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[b]Fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[g,h,i]perylene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Benzo[k]fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Chrysene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Dibenzo[a,h]anthracene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Fluoranthene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Fluorene 0.0350J 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Indeno[1,2,3-c,d] pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Naphthalene 0.184 0.105 ug/L XMS5528 XXX23075 0.0326 1 Phenanthrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Pyrene 0.0316 U 0.0526 ug/L XMS5528 XXX23075 0.0158 1 Terphenyl-d14 <surr> 93.2 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 950 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 00:19 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478005-I Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6543 MXX23243 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6543 Analytical Method: SW6020 Analysis Date/Time: 07/21/10 19:42 Prep Batch: MXX23243 Prep Method: SW3010A Prep Date/Time: 07/16/10 18:10 Container ID:1103478006-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 60.0 U 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 101 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 16:35 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478006-B Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 0.324 U 0.432 mg/L XFC9360 XXX23089 0.162 1 5a Androstane <surr> 81.3 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 925 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 21:07 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478006-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 107 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 95.2 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 09:57 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478006-A Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW03-WG20 SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 2-Methylnaphthalene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Acenaphthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Acenaphthylene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo(a)Anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[a]pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[b]Fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[g,h,i]perylene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[k]fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Chrysene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Dibenzo[a,h]anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Fluorene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Naphthalene 0.0666 U 0.108 ug/L XMS5528 XXX23075 0.0333 1 Phenanthrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Terphenyl-d14 <surr> 88.1 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 930 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 00:36 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478006-I Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6543 MXX23243 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6543 Analytical Method: SW6020 Analysis Date/Time: 07/21/10 19:44 Prep Batch: MXX23243 Prep Method: SW3010A Prep Date/Time: 07/16/10 18:10 Container ID:1103478007-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 46.5J 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 122 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 16:54 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478007-C Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 3.06 0.435 mg/L XFC9360 XXX23089 0.163 1 5a Androstane <surr> 83.6 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 920 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 21:28 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478007-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.360J 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 107 20.0 ug/L VMS11403 VXX20964 6.20 10 n-Butylbenzene 4.41 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 7.92 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.690J 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 4.17 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 1.52 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 107 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 100 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 94.2 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 10:31 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478007-A Dilution Factor: 1 Analyst: SCL Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11403 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 23:58 Prep Batch: VXX20964 Prep Method: SW5030B Prep Date/Time: 07/19/10 14:07 Container ID:1103478007-B Dilution Factor: 10 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMW02-WG20 SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 7.43 2.15 ug/L XMS5529 XXX23075 0.645 40 2-Methylnaphthalene 1.06 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Acenaphthene 0.287 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Acenaphthylene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo(a)Anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[a]pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[b]Fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[g,h,i]perylene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Benzo[k]fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Chrysene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Dibenzo[a,h]anthracene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Fluoranthene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Fluorene 0.159 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Naphthalene 59.9 4.30 ug/L XMS5529 XXX23075 1.33 40 Phenanthrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Pyrene 0.0322 U 0.0538 ug/L XMS5528 XXX23075 0.0161 1 Terphenyl-d14 <surr> 90.7 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 930 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 00:54 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478007-I Dilution Factor: 1 Analyst: CDE Initial Prep Wt./Vol.: 930 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5529 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 08:57 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478007-I Dilution Factor: 40 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6543 MXX23243 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6543 Analytical Method: SW6020 Analysis Date/Time: 07/21/10 19:46 Prep Batch: MXX23243 Prep Method: SW3010A Prep Date/Time: 07/16/10 18:10 Container ID:1103478008-G Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 45.4J 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 120 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 17:14 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478008-C Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF
Diesel Range Organics 3.11 0.426 mg/L XFC9360 XXX23089 0.160 1 5a Androstane <surr> 83.4 50-150 % XFC9360 XXX23089 1
Batch Information Initial Prep Wt./Vol.: 940 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9360 Analytical Method: SW8015C Analysis Date/Time: 07/21/10 21:49 Prep Batch: XXX23089 Prep Method: SW3520C Prep Date/Time: 07/20/10 09:30 Container ID:1103478008-J Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 102 20.0 ug/L VMS11403 VXX20964 6.20 10 n-Butylbenzene 4.89 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 8.85 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.660J 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 4.66 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 1.61 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 110 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 100 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 94.1 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 11:05 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478008-A Dilution Factor: 1 Analyst: SCL Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11403 Analytical Method: SW8260B Analysis Date/Time: 07/21/10 00:31 Prep Batch: VXX20964 Prep Method: SW5030B Prep Date/Time: 07/19/10 14:07 Container ID:1103478008-B Dilution Factor: 10 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: 

### RHMWA01-WG20 SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF
1-Methylnaphthalene 7.05 2.09 ug/L XMS5529 XXX23075 0.628 40 2-Methylnaphthalene 0.937 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Acenaphthene 0.309 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Acenaphthylene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Anthracene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Benzo(a)Anthracene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Benzo[a]pyrene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Benzo[b]Fluoranthene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Benzo[g,h,i]perylene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Benzo[k]fluoranthene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Chrysene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Dibenzo[a,h]anthracene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Fluoranthene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Fluorene 0.165 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Indeno[1,2,3-c,d] pyrene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Naphthalene 61.1 4.19 ug/L XMS5529 XXX23075 1.30 40 Phenanthrene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Pyrene 0.0314 U 0.0524 ug/L XMS5528 XXX23075 0.0157 1 Terphenyl-d14 <surr> 87.5 50-135 % XMS5528 XXX23075 1
Batch Information Initial Prep Wt./Vol.: 955 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5528 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 01:12 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478008-I Dilution Factor: 1 Analyst: CDE Initial Prep Wt./Vol.: 955 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5529 Analytical Method: 8270D SIMS Analysis Date/Time: 07/20/10 09:15 Prep Batch: XXX23075 Prep Method: SW3520C Prep Date/Time: 07/19/10 09:05 Container ID:1103478008-I Dilution Factor: 40 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID:

### TB01-WG20 SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF
Gasoline Range Organics 60.0 U 100 ug/L VFC10038 VXX20986 30.0 1 4-Bromofluorobenzene <surr> 105 50-150 % VFC10038 VXX20986 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC10038 Analytical Method: SW8015C Analysis Date/Time: 07/25/10 14:57 Prep Batch: VXX20986 Prep Method: SW5030B Prep Date/Time: 07/25/10 10:00 Container ID:1103478009-A Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID:

### TB01-WG20 SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 2-Hexanone 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11399 VXX20956 3.10 1 Benzene 0.240 U 0.400 ug/L VMS11399 VXX20956 0.120 1 Bromobenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Bromoform 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 Carbon disulfide 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID:

### TB01-WG20 SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Chloroform 0.600 U 1.00 ug/L VMS11399 VXX20956 0.300 1 Chloromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11399 VXX20956 0.150 1 Dibromomethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Methylene chloride 2.00 U 5.00 ug/L VMS11399 VXX20956 1.00 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11399 VXX20956 1.50 1 Naphthalene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 o-Xylene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11399 VXX20956 0.620 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Toluene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11399 VXX20956 0.310 1 Xylenes (total) 1.88 U 3.00 ug/L VMS11399 VXX20956 0.940 1 1,2-Dichloroethane-D4 <surr> 107 73-120 % VMS11399 VXX20956 1 4-Bromofluorobenzene <surr> 102 76-120 % VMS11399 VXX20956 1 Toluene-d8 <surr> 99.6 80-120 % VMS11399 VXX20956 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID:

### TB01-WG20 SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05 Receipt Date/Time: 07/15/10 12:35 Project ID: 3354-003 Red Hill Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11399 Analytical Method: SW8260B Analysis Date/Time: 07/20/10 08:16 Prep Batch: VXX20956 Prep Method: SW5030B Prep Date/Time: 07/19/10 08:14 Container ID:1103478009-B Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518t(907 )562.2343f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S GroupMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974243 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) XXX23075 SW3520C 07/19/2010 QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units Analysis Date DL


### Polynuclear Aromatics GC/MS 

### 1-Methylnaphthalene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 2-Methylnaphthalene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Acenaphthene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Acenaphthylene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Anthracene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Benzo(a)Anthracene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Benzo[a]pyrene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Benzo[b]Fluoranthene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Benzo[g,h,i]perylene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Benzo[k]fluoranthene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Chrysene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Dibenzo[a,h]anthracene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Fluoranthene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Fluorene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Naphthalene 0.0620 U 0.100 ug/L 07/19/10 

### 0.0310 Phenanthrene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Pyrene 0.0300 U 0.0500 ug/L 07/19/10 

### 0.0150 Surrogates 

### Terphenyl-d14 <surr> 97.1 50-135 % 07/19/10

Instrument Method Batch XMS5528

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974420 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) MXX23243 SW3010A 07/16/2010 QC results affect the following production samples: 

### 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units Analysis Date DL


### Metals by ICP/MS



### Lead 0.620 U 1.00 ug/L 07/21/10 

### 0.310

Instrument Method Batch MMS6543

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974677 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) XXX23089 SW3520C 07/20/2010 QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units Analysis Date DL


### Semivolatile Organic Fuels Department 

### Diesel Range Organics 0.300 U 0.400 mg/L 07/21/10 

### 0.150 Surrogates


### 5a Androstane <surr> 77.6 60-120 % 07/21/10

Instrument Method Batch XFC9360

SW8015C HP 7890A FID SV E RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974725 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010 QC results affect the following production samples: 

### 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974725 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,1,1-Trichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,1,2-Trichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloropropene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,3-Trichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 07/20/10 

### 0.620 1,2-Dibromoethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dichloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,2-Dichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3-Dichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3-Dichloropropane 0.240 U 0.400 ug/L 07/20/10 

### 0.120 1,4-Dichlorobenzene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 2,2-Dichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 2-Butanone (MEK) 6.20 U 10.0 ug/L 07/20/10 

### 3.10 2-Chlorotoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 2-Hexanone 6.20 U 10.0 ug/L 07/20/10 

### 3.10 4-Chlorotoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 4-Isopropyltoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 07/20/10 

### 3.10 Benzene 0.240 U 0.400 ug/L 07/20/10 

### 0.120 Bromobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromochloromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromodichloromethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Bromoform 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromomethane 1.88 U 3.00 ug/L 07/20/10 

### 0.940 Carbon disulfide 1.24 U 2.00 ug/L 07/20/10 

### 0.620 Carbon tetrachloride 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Chlorobenzene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Chloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Chloroform 0.600 U 1.00 ug/L 07/20/10 

### 0.300 Chloromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974725 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Dibromochloromethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Dibromomethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Dichlorodifluoromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Ethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Hexachlorobutadiene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Methylene chloride 2.00 U 5.00 ug/L 07/20/10 

### 1.00 Methyl-t-butyl ether 3.00 U 5.00 ug/L 07/20/10 

### 1.50 Naphthalene 1.24 U 2.00 ug/L 07/20/10 

### 0.620 n-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 n-Propylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 o-Xylene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 P & M -Xylene 1.24 U 2.00 ug/L 07/20/10 

### 0.620 sec-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Styrene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 tert-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Tetrachloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Toluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Trichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Trichlorofluoromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Vinyl chloride 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Xylenes (total) 1.88 U 3.00 ug/L 07/20/10 

### 0.940 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 108 73-120 % 07/20/10 

### 4-Bromofluorobenzene <surr> 102 76-120 % 07/20/10 

### Toluene-d8 <surr> 100 80-120 % 07/20/10

Instrument Method Batch VMS11399

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975092 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010 QC results affect the following production samples: 

### 1103478001, 1103478007, 1103478008

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975092 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,1,1-Trichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,1,2-Trichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,1-Dichloropropene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,3-Trichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 07/20/10 

### 0.620 1,2-Dibromoethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,2-Dichloroethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 1,2-Dichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3-Dichlorobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 1,3-Dichloropropane 0.240 U 0.400 ug/L 07/20/10 

### 0.120 1,4-Dichlorobenzene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 2,2-Dichloropropane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 2-Butanone (MEK) 6.20 U 10.0 ug/L 07/20/10 

### 3.10 2-Chlorotoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 2-Hexanone 6.20 U 10.0 ug/L 07/20/10 

### 3.10 4-Chlorotoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 4-Isopropyltoluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 07/20/10 

### 3.10 Benzene 0.240 U 0.400 ug/L 07/20/10 

### 0.120 Bromobenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromochloromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromodichloromethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Bromoform 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Bromomethane 1.88 U 3.00 ug/L 07/20/10 

### 0.940 Carbon disulfide 1.24 U 2.00 ug/L 07/20/10 

### 0.620 Carbon tetrachloride 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Chlorobenzene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Chloroethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Chloroform 0.600 U 1.00 ug/L 07/20/10 

### 0.300 Chloromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975092 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Dibromochloromethane 0.300 U 0.500 ug/L 07/20/10 

### 0.150 Dibromomethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Dichlorodifluoromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Ethylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Hexachlorobutadiene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Methylene chloride 2.00 U 5.00 ug/L 07/20/10 

### 1.00 Methyl-t-butyl ether 3.00 U 5.00 ug/L 07/20/10 

### 1.50 Naphthalene 1.24 U 2.00 ug/L 07/20/10 

### 0.620 n-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 n-Propylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 o-Xylene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 P & M -Xylene 1.24 U 2.00 ug/L 07/20/10 

### 0.620 sec-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Styrene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 tert-Butylbenzene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Tetrachloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Toluene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Trichloroethene 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Trichlorofluoromethane 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Vinyl chloride 0.620 U 1.00 ug/L 07/20/10 

### 0.310 Xylenes (total) 1.88 U 3.00 ug/L 07/20/10 

### 0.940 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 119 73-120 % 07/20/10 

### 4-Bromofluorobenzene <surr> 93.2 76-120 % 07/20/10 

### Toluene-d8 <surr> 93.8 80-120 % 07/20/10

Instrument Method Batch VMS11403

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975359 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) MXX23263 SW3010A 07/21/2010 QC results affect the following production samples: 

### 1103478001

Parameter Results LOQ/CL Units Analysis Date DL


### Metals by ICP/MS



### Lead 0.620 U 1.00 ug/L 07/27/10 

### 0.310

Instrument Method Batch MMS6555

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 976050 Method Blank The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20986 SW5030B 07/25/2010 QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Fuels Department 

### Gasoline Range Organics 60.0 U 100 ug/L 07/25/10 

### 30.0 Surrogates


### 4-Bromofluorobenzene <surr> 101 50-150 % 07/25/10

Instrument Method Batch VFC10038

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974244 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) XXX23075 SW3520C 07/19/2010

QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### 1-Methylnaphthalene LCS 0.436 87 ( 58-114 ) 0.5 ug/L 07/20/2010
2-Methylnaphthalene LCS 0.398 80 ( 54-105 ) 0.5 ug/L 07/20/2010
Acenaphthene LCS 0.429 86 ( 57-110 ) 0.5 ug/L 07/20/2010
Acenaphthylene LCS 0.440 88 ( 58-105 ) 0.5 ug/L 07/20/2010

Anthracene LCS 0.458 92 ( 63-120 ) 0.5 ug/L 07/20/2010
Benzo(a)Anthracene LCS 0.477 95 ( 61-120 ) 0.5 ug/L 07/20/2010
Benzo[a]pyrene LCS 0.420 84 ( 57-120 ) 0.5 ug/L 07/20/2010
Benzo[b]Fluoranthene LCS 0.505 101 ( 66-130 ) 0.5 ug/L 07/20/2010
Benzo[g,h,i]perylene LCS 0.513 103 ( 60-125 ) 0.5 ug/L 07/20/2010
Benzo[k]fluoranthene LCS 0.476 95 ( 67-125 ) 0.5 ug/L 07/20/2010
Chrysene LCS 0.500 100 ( 71-120 ) 0.5 ug/L 07/20/2010
Dibenzo[a,h]anthracene LCS 0.498 100 ( 56-125 ) 0.5 ug/L 07/20/2010

Fluoranthene LCS 0.455 91 ( 63-125 ) 0.5 ug/L 07/20/2010

Fluorene LCS 0.461 92 ( 59-120 ) 0.5 ug/L 07/20/2010
Indeno[1,2,3-c,d] pyrene LCS 0.510 102 ( 59-125 ) 0.5 ug/L 07/20/2010
Naphthalene LCS 0.473 95 ( 56-108 ) 0.5 ug/L 07/20/2010

Phenanthrene LCS 0.427 86 ( 60-115 ) 0.5 ug/L 07/20/2010
Pyrene LCS 0.464 93 ( 62-130 ) 0.5 ug/L 07/20/2010

Surrogates 

### Terphenyl-d14 <surr> LCS 92 ( 50-135 ) 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974244 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) XXX23075 SW3520C 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5529

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974421 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) MXX23243 SW3010A 07/16/2010

QC results affect the following production samples: 

### 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 07/21/2010

Batch Method Instrument 

### MMS6543

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974679 Lab Control Sample 974681 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) XXX23089 SW3520C 07/20/2010

QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.19 84 ( 75-125 ) 5 mg/L 07/21/2010 LCSD 4.28 86 2 (< 20 ) 5 mg/L 07/21/2010

Surrogates 

### 5a Androstane <surr> LCS 84 ( 60-120 ) 07/21/2010 LCSD 84 0 07/21/2010

Batch Method Instrument 

### XFC9360

SW8015C HP 7890A FID SV E RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

QC results affect the following production samples: 

### 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1,1,2-Tetrachloroethane LCS 29.1 97 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 28.9 96 1 (< 20 ) 30 ug/L 07/20/2010
1,1,1-Trichloroethane LCS 24.4 82 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 23.4 78 * 5 (< 20 ) 30 ug/L 07/20/2010
1,1,2,2-Tetrachloroethane LCS 29.1 97 ( 76-123 ) 30 ug/L 07/20/2010 LCSD 27.4 91 6 (< 20 ) 30 ug/L 07/20/2010
1,1,2-Trichloroethane LCS 29.4 98 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 28.8 96 2 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloroethane LCS 26.7 89 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 28.5 95 6 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloroethene LCS 26.9 90 ( 76-130 ) 30 ug/L 07/20/2010 LCSD 27.6 92 3 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloropropene LCS 31.4 105 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 30.5 102 3 (< 20 ) 30 ug/L 07/20/2010
1,2,3-Trichlorobenzene LCS 30.7 102 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 29.9 100 3 (< 20 ) 30 ug/L 07/20/2010
1,2,3-Trichloropropane LCS 30.5 102 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.2 97 4 (< 20 ) 30 ug/L 07/20/2010
1,2,4-Trichlorobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.7 99 6 (< 20 ) 30 ug/L 07/20/2010
1,2,4-Trimethylbenzene LCS 30.7 102 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 29.1 97 5 (< 20 ) 30 ug/L 07/20/2010
1,2-Dibromo-3-chloropropane LCS 28.9 96 ( 73-130 ) 30 ug/L 07/20/2010 LCSD 28.9 96 0 (< 20 ) 30 ug/L 07/20/2010
1,2-Dibromoethane LCS 31.3 104 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.2 101 4 (< 20 ) 30 ug/L 07/20/2010
1,2-Dichlorobenzene LCS 29.4 98 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 27.9 93 5 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichloroethane LCS 29.4 98 ( 80-129 ) 30 ug/L 07/20/2010 LCSD 28.8 96 2 (< 20 ) 30 ug/L 07/20/2010
1,2-Dichloropropane LCS 30.6 102 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 30.4 101 1 (< 20 ) 30 ug/L 07/20/2010
1,3,5-Trimethylbenzene LCS 30.7 102 ( 80-128 ) 30 ug/L 07/20/2010 LCSD 29.0 97 6 (< 20 ) 30 ug/L 07/20/2010
1,3-Dichlorobenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.3 101 6 (< 20 ) 30 ug/L 07/20/2010
1,3-Dichloropropane LCS 31.7 106 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 30.3 101 5 (< 20 ) 30 ug/L 07/20/2010
1,4-Dichlorobenzene LCS 32.7 109 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.4 105 4 (< 20 ) 30 ug/L 07/20/2010
2,2-Dichloropropane LCS 27.7 92 ( 80-132 ) 30 ug/L 07/20/2010 LCSD 29.0 97 5 (< 20 ) 30 ug/L 07/20/2010
2-Butanone (MEK) LCS 92.8 103 ( 66-136 ) 90 ug/L 07/20/2010 LCSD 90.2 100 3 (< 20 ) 90 ug/L 07/20/2010

2-Chlorotoluene LCS 33.2 111 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 31.2 104 6 (< 20 ) 30 ug/L 07/20/2010

2-Hexanone LCS 99.3 110 ( 68-130 ) 90 ug/L 07/20/2010 LCSD 95.3 106 4 (< 20 ) 90 ug/L 07/20/2010

4-Chlorotoluene LCS 33.4 111 ( 79-128 ) 30 ug/L 07/20/2010 LCSD 31.6 105 5 (< 20 ) 30 ug/L 07/20/2010
4-Isopropyltoluene LCS 31.4 105 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 29.7 99 6 (< 20 ) 30 ug/L 07/20/2010
4-Methyl-2-pentanone (MIBK) LCS 90.9 101 ( 69-134 ) 90 ug/L 07/20/2010 LCSD 85.2 95 6 (< 20 ) 90 ug/L 07/20/2010

Benzene LCS 31.7 106 ( 80-120 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 31.1 104 2 (< 20 ) 30 ug/L 07/20/2010

Bromobenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 28.2 94 5 (< 20 ) 30 ug/L 07/20/2010

Bromochloromethane LCS 27.0 90 ( 77-129 ) 30 ug/L 07/20/2010 LCSD 28.9 97 7 (< 20 ) 30 ug/L 07/20/2010

Bromodichloromethane LCS 29.8 99 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.2 98 2 (< 20 ) 30 ug/L 07/20/2010

Bromoform LCS 28.1 94 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 28.0 93 0 (< 20 ) 30 ug/L 07/20/2010

Bromomethane LCS 28.9 96 ( 30-140 ) 30 ug/L 07/20/2010 LCSD 30.6 102 6 (< 20 ) 30 ug/L 07/20/2010

Carbon disulfide LCS 42.2 94 ( 72-123 ) 45 ug/L 07/20/2010 LCSD 43.6 97 3 (< 20 ) 45 ug/L 07/20/2010

Carbon tetrachloride LCS 27.0 90 ( 80-126 ) 30 ug/L 07/20/2010 LCSD 28.8 96 7 (< 20 ) 30 ug/L 07/20/2010

Chlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.2 101 1 (< 20 ) 30 ug/L 07/20/2010

Chloroethane LCS 29.4 98 ( 67-133 ) 30 ug/L 07/20/2010 LCSD 30.1 100 3 (< 20 ) 30 ug/L 07/20/2010

Chloroform LCS 26.4 88 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 27.9 93 5 (< 20 ) 30 ug/L 07/20/2010

Chloromethane LCS 25.6 86 ( 67-125 ) 30 ug/L 07/20/2010 LCSD 27.5 92 7 (< 20 ) 30 ug/L 07/20/2010
cis-1,2-Dichloroethene LCS 26.1 87 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 28.1 94 8 (< 20 ) 30 ug/L 07/20/2010
cis-1,3-Dichloropropene LCS 30.3 101 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.3 98 4 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Dibromochloromethane LCS 29.7 99 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.2 97 2 (< 20 ) 30 ug/L 07/20/2010

Dibromomethane LCS 28.5 95 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 27.3 91 4 (< 20 ) 30 ug/L 07/20/2010

Dichlorodifluoromethane LCS 26.8 89 ( 62-153 ) 30 ug/L 07/20/2010 LCSD 28.1 94 5 (< 20 ) 30 ug/L 07/20/2010
Ethylbenzene LCS 31.9 106 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.4 105 2 (< 20 ) 30 ug/L 07/20/2010

Hexachlorobutadiene LCS 30.5 102 ( 77-125 ) 30 ug/L 07/20/2010 LCSD 28.2 94 8 (< 20 ) 30 ug/L 07/20/2010
Isopropylbenzene (Cumene) LCS 30.1 100 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 29.8 100 1 (< 20 ) 30 ug/L 07/20/2010
Methylene chloride LCS 26.5 89 ( 63-131 ) 30 ug/L 07/20/2010 LCSD 27.6 92 4 (< 20 ) 30 ug/L 07/20/2010
Methyl-t-butyl ether LCS 40.6 90 ( 80-120 ) 45 ug/L 07/20/2010 LCSD 42.8 95 5 (< 20 ) 45 ug/L 07/20/2010
Naphthalene LCS 32.3 108 ( 75-120 ) 30 ug/L 07/20/2010 LCSD 30.5 102 6 (< 20 ) 30 ug/L 07/20/2010
n-Butylbenzene LCS 31.7 106 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 30.4 101 4 (< 20 ) 30 ug/L 07/20/2010
n-Propylbenzene LCS 34.2 114 ( 80-129 ) 30 ug/L 07/20/2010 LCSD 32.5 108 5 (< 20 ) 30 ug/L 07/20/2010
o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.7 102 1 (< 20 ) 30 ug/L 07/20/2010
P & M -Xylene LCS 59.6 99 ( 80-120 ) 60 ug/L 07/20/2010 LCSD 59.3 99 0 (< 20 ) 60 ug/L 07/20/2010
sec-Butylbenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.7 99 5 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 30.1 100 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.7 99 1 (< 20 ) 30 ug/L 07/20/2010
tert-Butylbenzene LCS 30.2 101 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 28.3 95 6 (< 20 ) 30 ug/L 07/20/2010

Tetrachloroethene LCS 29.6 99 ( 79-122 ) 30 ug/L 07/20/2010 LCSD 29.2 97 1 (< 20 ) 30 ug/L 07/20/2010

Toluene LCS 29.3 98 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 29.0 97 1 (< 20 ) 30 ug/L 07/20/2010
trans-1,2-Dichloroethene LCS 26.0 87 ( 79-132 ) 30 ug/L 07/20/2010 LCSD 26.9 90 4 (< 20 ) 30 ug/L 07/20/2010
trans-1,3-Dichloropropene LCS 30.3 101 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 30.0 100 1 (< 20 ) 30 ug/L 07/20/2010

Trichloroethene LCS 29.4 98 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 29.4 98 0 (< 20 ) 30 ug/L 07/20/2010

Trichlorofluoromethane LCS 25.3 84 ( 68-145 ) 30 ug/L 07/20/2010 LCSD 26.1 87 3 (< 20 ) 30 ug/L 07/20/2010
Vinyl chloride LCS 26.7 89 ( 72-145 ) 30 ug/L 07/20/2010 LCSD 28.2 94 5 (< 20 ) 30 ug/L 07/20/2010
Xylenes (total) LCS 90.5 101 ( 80-120 ) 90 ug/L 07/20/2010 LCSD 90.0 100 1 (< 20 ) 90 ug/L 07/20/2010

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 07/20/2010 LCSD 98 0 07/20/2010

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 07/20/2010 LCSD 101 2 07/20/2010

Toluene-d8 <surr> LCS 101 ( 80-120 ) 07/20/2010 LCSD 104 3 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 974726 Lab Control Sample 974727 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20956 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS11399

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

QC results affect the following production samples: 

### 1103478001, 1103478007, 1103478008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1,1,2-Tetrachloroethane LCS 29.9 100 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.2 97 2 (< 20 ) 30 ug/L 07/20/2010
1,1,1-Trichloroethane LCS 29.5 98 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 31.3 104 6 (< 20 ) 30 ug/L 07/20/2010
1,1,2,2-Tetrachloroethane LCS 29.7 99 ( 76-123 ) 30 ug/L 07/20/2010 LCSD 29.8 99 0 (< 20 ) 30 ug/L 07/20/2010
1,1,2-Trichloroethane LCS 30.3 101 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 30.5 102 0 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloroethane LCS 29.1 97 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.1 100 4 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloroethene LCS 27.5 92 ( 76-130 ) 30 ug/L 07/20/2010 LCSD 29.4 98 7 (< 20 ) 30 ug/L 07/20/2010
1,1-Dichloropropene LCS 30.8 103 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 32.5 108 5 (< 20 ) 30 ug/L 07/20/2010
1,2,3-Trichlorobenzene LCS 32.0 107 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 31.8 106 1 (< 20 ) 30 ug/L 07/20/2010
1,2,3-Trichloropropane LCS 31.1 104 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.6 102 2 (< 20 ) 30 ug/L 07/20/2010
1,2,4-Trichlorobenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.7 106 0 (< 20 ) 30 ug/L 07/20/2010
1,2,4-Trimethylbenzene LCS 32.0 107 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 32.3 108 1 (< 20 ) 30 ug/L 07/20/2010
1,2-Dibromo-3-chloropropane LCS 28.1 94 ( 73-130 ) 30 ug/L 07/20/2010 LCSD 28.7 96 2 (< 20 ) 30 ug/L 07/20/2010
1,2-Dibromoethane LCS 31.8 106 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.7 106 0 (< 20 ) 30 ug/L 07/20/2010
1,2-Dichlorobenzene LCS 29.2 98 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.5 98 1 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichloroethane LCS 29.2 97 ( 80-129 ) 30 ug/L 07/20/2010 LCSD 29.2 97 0 (< 20 ) 30 ug/L 07/20/2010
1,2-Dichloropropane LCS 30.8 103 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 32.2 107 5 (< 20 ) 30 ug/L 07/20/2010
1,3,5-Trimethylbenzene LCS 31.9 106 ( 80-128 ) 30 ug/L 07/20/2010 LCSD 32.1 107 1 (< 20 ) 30 ug/L 07/20/2010
1,3-Dichlorobenzene LCS 31.8 106 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 32.5 108 2 (< 20 ) 30 ug/L 07/20/2010
1,3-Dichloropropane LCS 32.5 108 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 32.2 107 1 (< 20 ) 30 ug/L 07/20/2010
1,4-Dichlorobenzene LCS 33.6 112 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 34.0 113 1 (< 20 ) 30 ug/L 07/20/2010
2,2-Dichloropropane LCS 30.8 103 ( 80-132 ) 30 ug/L 07/20/2010 LCSD 33.6 112 9 (< 20 ) 30 ug/L 07/20/2010
2-Butanone (MEK) LCS 96.4 107 ( 66-136 ) 90 ug/L 07/20/2010 LCSD 84.4 94 13 (< 20 ) 90 ug/L 07/20/2010

2-Chlorotoluene LCS 34.6 115 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 34.7 116 0 (< 20 ) 30 ug/L 07/20/2010

2-Hexanone LCS 94.8 105 ( 68-130 ) 90 ug/L 07/20/2010 LCSD 99.1 110 4 (< 20 ) 90 ug/L 07/20/2010

4-Chlorotoluene LCS 35.0 117 ( 79-128 ) 30 ug/L 07/20/2010 LCSD 35.5 118 1 (< 20 ) 30 ug/L 07/20/2010
4-Isopropyltoluene LCS 31.7 106 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 32.7 109 3 (< 20 ) 30 ug/L 07/20/2010
4-Methyl-2-pentanone (MIBK) LCS 83.6 93 ( 69-134 ) 90 ug/L 07/20/2010 LCSD 89.4 99 7 (< 20 ) 90 ug/L 07/20/2010

Benzene LCS 33.9 113 ( 80-120 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 34.7 116 3 (< 20 ) 30 ug/L 07/20/2010

Bromobenzene LCS 30.0 100 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.2 101 1 (< 20 ) 30 ug/L 07/20/2010

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 07/20/2010 LCSD 33.0 110 6 (< 20 ) 30 ug/L 07/20/2010

Bromodichloromethane LCS 28.7 96 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.2 97 1 (< 20 ) 30 ug/L 07/20/2010

Bromoform LCS 27.8 93 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 27.4 91 2 (< 20 ) 30 ug/L 07/20/2010

Bromomethane LCS 27.3 91 ( 30-140 ) 30 ug/L 07/20/2010 LCSD 30.4 101 11 (< 20 ) 30 ug/L 07/20/2010

Carbon disulfide LCS 43.0 96 ( 72-123 ) 45 ug/L 07/20/2010 LCSD 47.1 105 9 (< 20 ) 45 ug/L 07/20/2010

Carbon tetrachloride LCS 27.7 92 ( 80-126 ) 30 ug/L 07/20/2010 LCSD 29.0 97 5 (< 20 ) 30 ug/L 07/20/2010

Chlorobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.5 105 1 (< 20 ) 30 ug/L 07/20/2010

Chloroethane LCS 29.5 99 ( 67-133 ) 30 ug/L 07/20/2010 LCSD 30.5 102 3 (< 20 ) 30 ug/L 07/20/2010

Chloroform LCS 28.5 95 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 29.6 99 4 (< 20 ) 30 ug/L 07/20/2010

Chloromethane LCS 29.2 97 ( 67-125 ) 30 ug/L 07/20/2010 LCSD 32.8 109 12 (< 20 ) 30 ug/L 07/20/2010
cis-1,2-Dichloroethene LCS 29.1 97 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 31.6 105 8 (< 20 ) 30 ug/L 07/20/2010
cis-1,3-Dichloropropene LCS 29.8 99 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 30.8 103 3 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Dibromochloromethane LCS 28.5 95 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 28.8 96 1 (< 20 ) 30 ug/L 07/20/2010

Dibromomethane LCS 29.4 98 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 29.7 99 1 (< 20 ) 30 ug/L 07/20/2010

Dichlorodifluoromethane LCS 27.6 92 ( 62-153 ) 30 ug/L 07/20/2010 LCSD 31.0 103 12 (< 20 ) 30 ug/L 07/20/2010
Ethylbenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.4 105 0 (< 20 ) 30 ug/L 07/20/2010

Hexachlorobutadiene LCS 30.2 101 ( 77-125 ) 30 ug/L 07/20/2010 LCSD 29.6 99 2 (< 20 ) 30 ug/L 07/20/2010
Isopropylbenzene (Cumene) LCS 32.1 107 ( 80-121 ) 30 ug/L 07/20/2010 LCSD 32.6 109 1 (< 20 ) 30 ug/L 07/20/2010
Methylene chloride LCS 29.8 99 ( 63-131 ) 30 ug/L 07/20/2010 LCSD 32.2 107 8 (< 20 ) 30 ug/L 07/20/2010
Methyl-t-butyl ether LCS 40.7 91 ( 80-120 ) 45 ug/L 07/20/2010 LCSD 44.6 99 9 (< 20 ) 45 ug/L 07/20/2010
Naphthalene LCS 32.8 109 ( 75-120 ) 30 ug/L 07/20/2010 LCSD 33.0 110 1 (< 20 ) 30 ug/L 07/20/2010
n-Butylbenzene LCS 32.2 107 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 32.9 110 2 (< 20 ) 30 ug/L 07/20/2010
n-Propylbenzene LCS 35.3 118 ( 80-129 ) 30 ug/L 07/20/2010 LCSD 35.7 119 1 (< 20 ) 30 ug/L 07/20/2010
o-Xylene LCS 32.0 107 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 32.8 109 3 (< 20 ) 30 ug/L 07/20/2010
P & M -Xylene LCS 63.2 105 ( 80-120 ) 60 ug/L 07/20/2010 LCSD 63.9 107 1 (< 20 ) 60 ug/L 07/20/2010
sec-Butylbenzene LCS 31.9 106 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 32.7 109 2 (< 20 ) 30 ug/L 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 31.7 106 ( 80-120 ) 30 ug/L 07/20/2010 LCSD 31.8 106 1 (< 20 ) 30 ug/L 07/20/2010
tert-Butylbenzene LCS 30.8 103 ( 80-122 ) 30 ug/L 07/20/2010 LCSD 31.4 105 2 (< 20 ) 30 ug/L 07/20/2010

Tetrachloroethene LCS 29.8 99 ( 79-122 ) 30 ug/L 07/20/2010 LCSD 30.1 100 1 (< 20 ) 30 ug/L 07/20/2010

Toluene LCS 33.2 111 ( 77-120 ) 30 ug/L 07/20/2010 LCSD 32.0 107 4 (< 20 ) 30 ug/L 07/20/2010
trans-1,2-Dichloroethene LCS 29.6 99 ( 79-132 ) 30 ug/L 07/20/2010 LCSD 31.9 106 8 (< 20 ) 30 ug/L 07/20/2010
trans-1,3-Dichloropropene LCS 30.9 103 ( 80-124 ) 30 ug/L 07/20/2010 LCSD 30.5 102 1 (< 20 ) 30 ug/L 07/20/2010

Trichloroethene LCS 28.4 95 ( 80-125 ) 30 ug/L 07/20/2010 LCSD 30.6 102 7 (< 20 ) 30 ug/L 07/20/2010

Trichlorofluoromethane LCS 27.5 92 ( 68-145 ) 30 ug/L 07/20/2010 LCSD 28.8 96 5 (< 20 ) 30 ug/L 07/20/2010
Vinyl chloride LCS 27.9 93 ( 72-145 ) 30 ug/L 07/20/2010 LCSD 32.7 109 16 (< 20 ) 30 ug/L 07/20/2010
Xylenes (total) LCS 95.2 106 ( 80-120 ) 90 ug/L 07/20/2010 LCSD 96.7 107 2 (< 20 ) 90 ug/L 07/20/2010

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 99 ( 73-120 ) 07/20/2010 LCSD 97 2 07/20/2010

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 07/20/2010 LCSD 100 0 07/20/2010

Toluene-d8 <surr> LCS 107 ( 80-120 ) 07/20/2010 LCSD 102 5 07/20/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975093 Lab Control Sample 975094 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20964 SW5030B 07/19/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS11403

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 975360 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) MXX23263 SW3010A 07/21/2010

QC results affect the following production samples: 

### 1103478001

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1110 111 ( 80-120 ) 1000 ug/L 07/27/2010

Batch Method Instrument 

### MMS6555

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Prep 

### 976051 Lab Control Sample 976052 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-003 Red Hill Water (Surface, Eff., Ground) VXX20986 SW5030B 07/25/2010

QC results affect the following production samples: 

### 1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Fuels Department 

### Gasoline Range Organics LCS 206 103 ( 80-116 ) 200 ug/L 07/25/2010 LCSD 210 105 2 (< 20 ) 200 ug/L 07/25/2010

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 104 ( 50-150 ) 07/25/2010 LCSD 106 2 07/25/2010

Batch Method Instrument 

### VFC10038

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep



### 974422 Matrix Spike 974423 Matrix Spike Duplicate

1103478004 Water (Surface, Eff., Ground) MXX23243 3010 H20 Digest for Metals ICP-MS 07/16/2010

QC results affect the following production samples: 

### 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Metals by ICP/MS


### Lead MS (0.620) U 1040 104 ( 80-120 ) 1000 ug/L 07/21/2010 MSD 1020 102 1 (< 15 ) 1000 ug/L07/21/2010
Batch Method Instrument 

### MMS6543

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) MXX23263 3010 H20 Digest for Metals ICP-MS 07/21/2010

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS (0.620) U 959 96 ( 80-120 ) 1000 ug/L 07/27/2010 BMSD 1100 110 13 (< 15 ) 1000 ug/L07/27/2010
Batch Method Instrument 

### MMS6555

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS (60.0) U 484 108 ( 80-116 ) 450 ug/L 07/25/2010 BMSD 469 104 3 (< 20 ) 450 ug/L07/25/2010 Surrogates 

### 4-Bromofluorobenzene <surr> BMS 52.4 105 ( 50-150 ) 07/25/2010 BMSD 52.8 106 1 07/25/2010
Batch Method Instrument 

### VFC10038

SW8015C HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS (0.320) U 4.42 82 ( 75-125 ) 5.41 mg/L 07/21/2010 BMSD 4.85 91 9 (< 30 ) 5.32 mg/L07/21/2010 Surrogates 

### 5a Androstane <surr> BMS .0884 82 ( 50-150 ) 07/21/2010 BMSD 0.0926 87 5 07/21/2010
Batch Method Instrument 

### XFC9360

SW8015C HP 7890A FID SV E R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) VXX20964 Volatiles Extraction 8240/8260 FULL 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1,1,2-Tetrachloroethane BMS (0.300) U 30.3 101 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 29.2 97 4 (< 20 ) 30.0 ug/L07/20/2010 1,1,1-Trichloroethane BMS (0.620) U 33.1 110 ( 80-122 ) 30.0 ug/L 07/20/2010 BMSD 33.1 110 0 (< 20 ) 30.0 ug/L07/20/2010 1,1,2,2-Tetrachloroethane BMS (0.300) U 29.6 99 ( 76-123 ) 30.0 ug/L 07/20/2010 BMSD 28.7 96 3 (< 20 ) 30.0 ug/L07/20/2010 1,1,2-Trichloroethane BMS (0.620) U 30.2 101 ( 77-120 ) 30.0 ug/L 07/20/2010 BMSD 29.4 98 3 (< 20 ) 30.0 ug/L07/20/2010 1,1-Dichloroethane BMS (0.620) U 31.5 105 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 30.6 102 3 (< 20 ) 30.0 ug/L07/20/2010 1,1-Dichloroethene BMS (0.620) U 31.4 105 ( 76-130 ) 30.0 ug/L 07/20/2010 BMSD 30.2 101 4 (< 20 ) 30.0 ug/L07/20/2010 1,1-Dichloropropene BMS (0.620) U 35.1 117 ( 80-122 ) 30.0 ug/L 07/20/2010 BMSD 34.6 115 2 (< 20 ) 30.0 ug/L07/20/2010 1,2,3-Trichlorobenzene BMS (0.620) U 31.1 104 ( 77-120 ) 30.0 ug/L 07/20/2010 BMSD 31.8 106 2 (< 20 ) 30.0 ug/L07/20/2010 1,2,3-Trichloropropane BMS (0.620) U 29.4 98 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 28.7 96 3 (< 20 ) 30.0 ug/L07/20/2010 1,2,4-Trichlorobenzene BMS (0.620) U 31.7 106 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.7 106 0 (< 20 ) 30.0 ug/L07/20/2010 1,2,4-Trimethylbenzene BMS (0.620) U 32.2 107 ( 80-125 ) 30.0 ug/L 07/20/2010 BMSD 31.9 106 1 (< 20 ) 30.0 ug/L07/20/2010 1,2-Dibromo-3-chloropropane BMS (1.24) U 30.3 101 ( 73-130 ) 30.0 ug/L 07/20/2010 BMSD 29.8 99 2 (< 20 ) 30.0 ug/L07/20/2010 1,2-Dibromoethane BMS (0.620) U 32.1 107 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 30.2 101 6 (< 20 ) 30.0 ug/L07/20/2010 1,2-Dichlorobenzene BMS (0.620) U 29.3 98 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 29.0 97 1 (< 20 ) 30.0 ug/L07/20/2010 1,2-Dichloroethane BMS (0.300) U 30.6 102 ( 80-129 ) 30.0 ug/L 07/20/2010 BMSD 30.6 102 0 (< 20 ) 30.0 ug/L07/20/2010 1,2-Dichloropropane BMS (0.620) U 33.3 111 ( 80-121 ) 30.0 ug/L 07/20/2010 BMSD 33.7 112 1 (< 20 ) 30.0 ug/L07/20/2010 1,3,5-Trimethylbenzene BMS (0.620) U 32.7 109 ( 80-128 ) 30.0 ug/L 07/20/2010 BMSD 32.3 108 1 (< 20 ) 30.0 ug/L07/20/2010 1,3-Dichlorobenzene BMS (0.620) U 32.6 109 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 32.2 107 1 (< 20 ) 30.0 ug/L07/20/2010 1,3-Dichloropropane BMS (0.240) U 32.5 108 ( 80-121 ) 30.0 ug/L 07/20/2010 BMSD 31.5 105 3 (< 20 ) 30.0 ug/L07/20/2010 1,4-Dichlorobenzene BMS (0.300) U 34.2 114 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 34.2 114 0 (< 20 ) 30.0 ug/L07/20/2010Matrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) VXX20964 Volatiles Extraction 8240/8260 FULL 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2,2-Dichloropropane BMS (0.620) U 37 123 ( 80-132 ) 30.0 ug/L 07/20/2010 BMSD 37.3 124 1 (< 20 ) 30.0 ug/L07/20/2010 2-Butanone (MEK) BMS (6.20) U 81.5 91 ( 66-136 ) 90.0 ug/L 07/20/2010 BMSD 86.8 97 6 (< 20 ) 90.0 ug/L07/20/2010 2-Chlorotoluene BMS (0.620) U 34.7 116 ( 80-125 ) 30.0 ug/L 07/20/2010 BMSD 34.2 114 1 (< 20 ) 30.0 ug/L07/20/2010 2-Hexanone BMS (6.20) U 97.7 109 ( 68-130 ) 90.0 ug/L 07/20/2010 BMSD 91.3 101 7 (< 20 ) 90.0 ug/L07/20/2010 4-Chlorotoluene BMS (0.620) U 36 120 ( 79-128 ) 30.0 ug/L 07/20/2010 BMSD 36.1 120 0 (< 20 ) 30.0 ug/L07/20/2010 4-Isopropyltoluene BMS (0.620) U 33.1 110 ( 80-125 ) 30.0 ug/L 07/20/2010 BMSD 33.0 110 0 (< 20 ) 30.0 ug/L07/20/2010 4-Methyl-2-pentanone (MIBK) BMS (6.20) U 91.5 102 ( 69-134 ) 90.0 ug/L 07/20/2010 BMSD 88.7 99 3 (< 20 ) 90.0 ug/L07/20/2010 Benzene BMS (0.240) U 36.1 120 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 36.9 123* 2 (< 20 ) 30.0 ug/L07/20/2010 Bromobenzene BMS (0.620) U 30 100 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 30.1 100 0 (< 20 ) 30.0 ug/L 07/20/2010 Bromochloromethane BMS (0.620) U 33.5 112 ( 77-129 ) 30.0 ug/L 07/20/2010 BMSD 33.9 113 1 (< 20 ) 30.0 ug/L07/20/2010 Bromodichloromethane BMS (0.300) U 30.2 101 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 30.5 102 1 (< 20 ) 30.0 ug/L07/20/2010 Bromoform BMS (0.620) U 28.2 94 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 26.9 90 5 (< 20 ) 30.0 ug/L07/20/2010 Bromomethane BMS (1.88) U 34.5 115 ( 30-140 ) 30.0 ug/L 07/20/2010 BMSD 32.0 107 8 (< 20 ) 30.0 ug/L 07/20/2010 Carbon disulfide BMS (1.24) U 51.5 114 ( 72-123 ) 45.0 ug/L 07/20/2010 BMSD 49.2 109 5 (< 20 ) 45.0 ug/L07/20/2010 Carbon tetrachloride BMS (0.620) U 31.1 104 ( 80-126 ) 30.0 ug/L 07/20/2010 BMSD 31.6 105 2 (< 20 ) 30.0 ug/L07/20/2010 Chlorobenzene BMS (0.300) U 32.3 108 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.3 104 3 (< 20 ) 30.0 ug/L07/20/2010 Chloroethane BMS (0.620) U 74.4 248* ( 67-133 ) 30.0 ug/L 07/20/2010 BMSD 66.7 222* 11 (< 20 ) 30.0 ug/L 07/20/2010 Chloroform BMS (0.600) U 31.3 104 ( 80-124 ) 30.0 ug/L 07/20/2010 BMSD 31.7 106 1 (< 20 ) 30.0 ug/L07/20/2010 Chloromethane BMS (0.620) U 36.2 121 ( 67-125 ) 30.0 ug/L 07/20/2010 BMSD 35.8 119 1 (< 20 ) 30.0 ug/L07/20/2010 cis-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 80-125 ) 30.0 ug/L 07/20/2010 BMSD 34.6 115 3 (< 20 ) 30.0 ug/L07/20/2010Matrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) VXX20964 Volatiles Extraction 8240/8260 FULL 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### cis-1,3-Dichloropropene BMS (0.300) U 31.3 104 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.7 106 1 (< 20 ) 30.0 ug/L07/20/2010 Dibromochloromethane BMS (0.300) U 29.2 97 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 28.2 94 3 (< 20 ) 30.0 ug/L07/20/2010 Dibromomethane BMS (0.620) U 30.4 101 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.1 104 2 (< 20 ) 30.0 ug/L07/20/2010 Dichlorodifluoromethane BMS (0.620) U 34.2 114 ( 62-153 ) 30.0 ug/L 07/20/2010 BMSD 34.7 116 1 (< 20 ) 30.0 ug/L07/20/2010 Ethylbenzene BMS (0.620) U 32.5 108 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.5 105 3 (< 20 ) 30.0 ug/L07/20/2010 Hexachlorobutadiene BMS (0.620) U 30.6 102 ( 77-125 ) 30.0 ug/L 07/20/2010 BMSD 32.8 109 7 (< 20 ) 30.0 ug/L07/20/2010 Isopropylbenzene (Cumene) BMS (0.620) U 33.6 112 ( 80-121 ) 30.0 ug/L 07/20/2010 BMSD 32.6 109 3 (< 20 ) 30.0 ug/L07/20/2010 Methylene chloride BMS (2.00) U 33 110 ( 63-131 ) 30.0 ug/L 07/20/2010 BMSD 31.2 104 6 (< 20 ) 30.0 ug/L07/20/2010 Methyl-t-butyl ether BMS (3.00) U 46.4 103 ( 80-120 ) 45.0 ug/L 07/20/2010 BMSD 43.4 97 7 (< 20 ) 45.0 ug/L07/20/2010 Naphthalene BMS (1.24) U 33.1 110 ( 75-120 ) 30.0 ug/L 07/20/2010 BMSD 32.9 110 1 (< 20 ) 30.0 ug/L07/20/2010 n-Butylbenzene BMS (0.620) U 34.1 114 ( 80-124 ) 30.0 ug/L 07/20/2010 BMSD 34.2 114 0 (< 20 ) 30.0 ug/L07/20/2010 n-Propylbenzene BMS (0.620) U 36.2 121 ( 80-129 ) 30.0 ug/L 07/20/2010 BMSD 36.2 121 0 (< 20 ) 30.0 ug/L07/20/2010 o-Xylene BMS (0.620) U 33.1 110 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 32.2 107 3 (< 20 ) 30.0 ug/L07/20/2010 P & M -Xylene BMS (1.24) U 66.1 110 ( 80-120 ) 60.0 ug/L 07/20/2010 BMSD 63.7 106 4 (< 20 ) 60.0 ug/L07/20/2010 sec-Butylbenzene BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 32.9 110 0 (< 20 ) 30.0 ug/L07/20/2010 Styrene BMS (0.620) U 32.3 108 ( 80-120 ) 30.0 ug/L 07/20/2010 BMSD 31.4 105 3 (< 20 ) 30.0 ug/L07/20/2010 tert-Butylbenzene BMS (0.620) U 31.5 105 ( 80-122 ) 30.0 ug/L 07/20/2010 BMSD 31.4 105 0 (< 20 ) 30.0 ug/L07/20/2010 Tetrachloroethene BMS (0.620) U 31.4 105 ( 79-122 ) 30.0 ug/L 07/20/2010 BMSD 30.9 103 2 (< 20 ) 30.0 ug/L07/20/2010 Toluene BMS (0.620) U 33 110 ( 77-120 ) 30.0 ug/L 07/20/2010 BMSD 31.6 105 4 (< 20 ) 30.0 ug/L07/20/2010 trans-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 79-132 ) 30.0 ug/L 07/20/2010 BMSD 31.9 106 5 (< 20 ) 30.0 ug/L07/20/2010Matrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) VXX20964 Volatiles Extraction 8240/8260 FULL 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### trans-1,3-Dichloropropene BMS (0.620) U 30.6 102 ( 80-124 ) 30.0 ug/L 07/20/2010 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L07/20/2010 Trichloroethene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 07/20/2010 BMSD 30.8 103 5 (< 20 ) 30.0 ug/L07/20/2010 Trichlorofluoromethane BMS (0.620) U 29.5 98 ( 68-145 ) 30.0 ug/L 07/20/2010 BMSD 27.7 92 7 (< 20 ) 30.0 ug/L07/20/2010 Vinyl chloride BMS (0.620) U 35.9 120 ( 72-145 ) 30.0 ug/L 07/20/2010 BMSD 35.0 117 3 (< 20 ) 30.0 ug/L07/20/2010 Xylenes (total) BMS (1.88) U 99.3 110 ( 80-120 ) 90.0 ug/L 07/20/2010 BMSD 95.9 107 3 (< 20 ) 90.0 ug/L07/20/2010 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 29.9 100 ( 73-120 ) 07/20/2010 BMSD 29.9 100 0 07/20/2010 4-Bromofluorobenzene <surr> BMS 29.5 98 ( 76-120 ) 07/20/2010 BMSD 29.6 99 1 07/20/2010 Toluene-d8 <surr> BMS 31.3 104 ( 80-120 ) 07/20/2010 BMSD 30.7 102 2 07/20/2010
Batch Method Instrument 

### VMS11403

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) XXX23075 3520 Liquid/Liquid Ext for 8270 SIM 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### 1-Methylnaphthalene BMS (0.0320) U .281 52* ( 58-114 ) 0.543 ug/L 07/19/2010 BMSD 0.439 83 44 (< 30 ) 0.529 ug/L07/19/2010 * 2-Methylnaphthalene BMS (0.0320) U .256 47* ( 54-105 ) 0.543 ug/L 07/19/2010 BMSD 0.397 75 43 (< 30 ) 0.529 ug/L07/19/2010 * Acenaphthene BMS (0.0320) U .315 58 ( 57-110 ) 0.543 ug/L 07/19/2010 BMSD 0.412 78 27 (< 30 ) 0.529 ug/L07/19/2010 Acenaphthylene BMS (0.0320) U .319 59 ( 58-105 ) 0.543 ug/L 07/19/2010 BMSD 0.432 82 30 (< 30 ) 0.529 ug/L07/19/2010 * Anthracene BMS (0.0320) U .396 73 ( 63-120 ) 0.543 ug/L 07/19/2010 BMSD 0.468 89 17 (< 30 ) 0.529 ug/L07/19/2010 Benzo(a)Anthracene BMS (0.0320) U .42 77 ( 61-120 ) 0.543 ug/L 07/19/2010 BMSD 0.490 93 15 (< 30 ) 0.529 ug/L07/19/2010 Benzo[a]pyrene BMS (0.0320) U .364 67 ( 57-120 ) 0.543 ug/L 07/19/2010 BMSD 0.424 80 15 (< 30 ) 0.529 ug/L07/19/2010 Benzo[b]Fluoranthene BMS (0.0320) U .408 75 ( 66-130 ) 0.543 ug/L 07/19/2010 BMSD 0.459 87 12 (< 30 ) 0.529 ug/L07/19/2010 Benzo[g,h,i]perylene BMS (0.0320) U .403 74 ( 60-125 ) 0.543 ug/L 07/19/2010 BMSD 0.475 90 16 (< 30 ) 0.529 ug/L07/19/2010 Benzo[k]fluoranthene BMS (0.0320) U .4 74 ( 67-125 ) 0.543 ug/L 07/19/2010 BMSD 0.482 91 19 (< 30 ) 0.529 ug/L07/19/2010 Chrysene BMS (0.0320) U .427 79 ( 71-120 ) 0.543 ug/L 07/19/2010 BMSD 0.499 94 16 (< 30 ) 0.529 ug/L07/19/2010 Dibenzo[a,h]anthracene BMS (0.0320) U .394 73 ( 56-125 ) 0.543 ug/L 07/19/2010 BMSD 0.459 87 15 (< 30 ) 0.529 ug/L07/19/2010 Fluoranthene BMS (0.0320) U .437 81 ( 63-125 ) 0.543 ug/L 07/19/2010 BMSD 0.505 95 14 (< 30 ) 0.529 ug/L07/19/2010 Fluorene BMS (0.0320) U .371 68 ( 59-120 ) 0.543 ug/L 07/19/2010 BMSD 0.482 91 26 (< 30 ) 0.529 ug/L07/19/2010 Indeno[1,2,3-c,d] pyrene BMS (0.0320) U .401 74 ( 59-125 ) 0.543 ug/L 07/19/2010 BMSD 0.477 90 17 (< 30 ) 0.529 ug/L07/19/2010 Naphthalene BMS (0.0664) U .27 50* ( 56-108 ) 0.543 ug/L 07/19/2010 BMSD 0.480 91 56 (< 30 ) 0.529 ug/L07/19/2010 * Phenanthrene BMS (0.0320) U .395 73 ( 60-115 ) 0.543 ug/L 07/19/2010 BMSD 0.460 87 15 (< 30 ) 0.529 ug/L07/19/2010 Pyrene BMS (0.0320) U .435 80 ( 62-130 ) 0.543 ug/L 07/19/2010 BMSD 0.493 93 13 (< 30 ) 0.529 ug/L07/19/2010 Surrogates 

### Terphenyl-d14 <surr> BMS .411 76 ( 50-135 ) 07/19/2010 BMSD 0.476 90 15 07/19/2010Matrix SGS Ref.# Printed Date/Time 

### 08/17/2010 10:37 Batch Method Date Original Prep 

### 1103478002 Billable Matrix Spike 1103478003 Billable Matrix Spike Dup.

1103478001 Water (Surface, Eff., Ground) XXX23075 3520 Liquid/Liquid Ext for 8270 SIM 07/19/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5528

8270D SIMS HP 6890/5973 MS SVQA