Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

990 AES Harding Street Boiler 70 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

990 AES Harding Street Boiler 70 As Received Higher Heating Value 990 AES Harding Street Boiler 70 As Received % Moisture 990 AES Harding Street Boiler 70 As Received % Ash 990 AES Harding Street Boiler 70 As Received % Sulfur 990 AES Harding Street Boiler 70 Dry basis Higher Heating Value 990 AES Harding Street Boiler 70 Dry basis % Ash 990 AES Harding Street Boiler 70 Dry basis % Sulfur 990 AES Harding Street Boiler 70 Dry basis Antimony 990 AES Harding Street Boiler 70 Dry basis Arsenic 990 AES Harding Street Boiler 70 Dry basis Beryllium 990 AES Harding Street Boiler 70 Dry basis Cadmium 990 AES Harding Street Boiler 70 Dry basis Chlorine 990 AES Harding Street Boiler 70 Dry basis Chromium 990 AES Harding Street Boiler 70 Dry basis Cobalt 990 AES Harding Street Boiler 70 Dry basis Fluorine 990 AES Harding Street Boiler 70 Dry basis Lead 990 AES Harding Street Boiler 70 Dry basis Manganese 990 AES Harding Street Boiler 70 Dry basis Mercury 990 AES Harding Street Boiler 70 Dry basis Nickel 990 AES Harding Street Boiler 70 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) D4809/D5865 160.3 MOD/D3173 D482/D3174 D1552/D4239 D4809/D5865 D482/D3174 D1552/D4239 ASTM-6020 ASTM-6020 ASTM-6020 ASTM-6020 ASTM-9056 ASTM-6020 ASTM-6020 NA ASTM-6020 ASTM-6020 ASTM-7471A ASTM-6020 ASTM-6020EIA Facility Code Facility

Name Boiler ID HAPs Test Group 990 AES Harding Street Boiler 70 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units U70 R1 PM/Metals 4/13/2010 4/13/2010 11346.00 Btu/lb U70 R2 PM/Metals 4/13/2010 4/13/2010 11140.00 Btu/lb U70 R3 PM/Metals 4/14/2010 4/14/2010 11289.00 Btu/lb U70 R1 Hg 4/14/2010 4/14/2010 11551.00 Btu/lb U70 R2 Hg 4/15/2010 4/15/2010 11318.00 Btu/lb U70 R3 Hg 4/15/2010 4/15/2010 10284.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 13 9.16 13042 Btu/lb 10.53 4.14 11 8.48 12517 Btu/lb 9.52 4.18 13 8.7 12805 Btu/lb 9.89 3.98 12 8.02 13126 Btu/lb 9.12 3.86 13 8.22 13009 Btu/lb 9.45 3.76 13 7.4 11821 Btu/lb 8.51 3.71Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 420 ppm 0.0829 mg/Kg 2.1 mg/Kg 3 mg/Kg 2 460 ppm 0.0578 mg/Kg 1.8 mg/Kg 3 mg/Kg 1.9 330 ppm 0.075 mg/Kg 1.9 mg/Kg 3.4 mg/Kg 2.1 470 ppm 0.0733 mg/Kg 1.6 mg/Kg 3.6 mg/Kg 2.2 500 ppm 0.0573 mg/Kg 1.8 mg/Kg 3.3 mg/Kg 2.1 510 ppm 0.0512 mg/Kg 2 mg/Kg 2.6 mg/Kg 2.4Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg 0.63 mg/Kg 11 mg/Kg 6.1 mg/Kg 19 mg/Kg mg/Kg [<0.15] mg/Kg 12 mg/Kg 5.5 mg/Kg 14 mg/Kg mg/Kg [<0.15] mg/Kg 10 mg/Kg 7.3 mg/Kg 23 mg/Kg mg/Kg [<0.15] mg/Kg 13 mg/Kg 7.3 mg/Kg 22 mg/Kg mg/Kg 1.5 mg/Kg 12 mg/Kg 5.6 mg/Kg 11 mg/Kg mg/Kg 0.72 mg/Kg 14 mg/Kg 6.1 mg/Kg 14 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 12 mg/Kg [<0.6] mg/Kg 3 mg/Kg 13 12 mg/Kg [<0.6] mg/Kg 2.8 mg/Kg 11 13 mg/Kg [<0.6] mg/Kg 3.2 mg/Kg 13 14 mg/Kg [<0.6] mg/Kg 3.3 mg/Kg 12 11 mg/Kg 3.1 mg/Kg 2.9 mg/Kg 13 14 mg/Kg [<0.6] mg/Kg 3.4 mg/Kg 13 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 38.55 10.53 50.91 73.56 5.4 1.34 4.14 39.19 9.52 51.28 75.67 5.41 1.29 4.18 39.17 9.89 50.94 73.99 5.19 1.36 3.98 39.29 9.12 51.59 74.56 4.64 1.27 3.86 39.28 9.45 51.27 74 4.43 1.25 3.76 39.82 8.51 51.66 76.29 5.37 1.4 3.71 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

5.03 3.92 5.58 6.56 7.12 4.71Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm