Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-001 Date Collected: 07/24/2013 Date Received: 7/24/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 51.2 ug/L 0.050 0.010 DPC 07/31/2013 13:21 EPA 200.8

Arsenic, As 332 ug/L 0.10 0.030 DPC 07/31/2013 13:21 EPA 200.8

Barium, Ba 4910 ug/L 0.10 0.020 DPC 07/31/2013 13:21 EPA 200.8

Beryllium, Be 12 ug/L J 50 10 DAM 08/01/2013 13:21 EPA 200.7

Cadmium, Cd 231 ug/L 0.050 0.010 DPC 07/31/2013 13:21 EPA 200.8

Chromium, Cr 1900 ug/L 0.20 0.040 DPC 07/31/2013 13:21 EPA 200.8

Cobalt, Co 303 ug/L 0.020 0.0040 DPC 07/31/2013 13:21 EPA 200.8

Copper, Cu 808 ug/L 0.050 0.010 DPC 07/31/2013 13:21 EPA 200.8

Lead, Pb 372 ug/L 0.010 0.0020 DPC 07/31/2013 13:21 EPA 200.8

Mercury, Hg 236000 ng/L 5000 2000 TLT 07/31/2013 EPA 1631E

Molybdenum, Mo 793 ug/L 0.050 0.010 DPC 07/31/2013 13:21 EPA 200.8

Nickel, Ni 2580 ug/L 0.20 0.050 DPC 07/31/2013 13:21 EPA 200.8

Selenium, Se 1650 ug/L 0.50 0.20 DPC 07/31/2013 13:21 EPA 200.8

Silver, Ag 1.78 ug/L 0.010 0.0020 DPC 07/31/2013 13:21 EPA 200.8

Thallium, Tl 23.9 ug/L 0.050 0.0020 DPC 07/31/2013 13:21 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:22 EPA 200.7

Titanium, Ti 1140 ug/L 200 30 DAM 08/01/2013 13:21 EPA 200.7

Zinc, Zn 5780 ug/L 0.50 0.10 DPC 07/31/2013 13:21 EPA 200.8

Aluminum, Al 292 mg/L 0.0010 0.0003 DPC 07/31/2013 13:21 EPA 200.8

Boron, B 438 mg/L 2.0 0.40 DAM 08/01/2013 13:21 EPA 200.7

Calcium, Ca 4940 mg/L 2.0 0.40 DAM 08/01/2013 13:21 EPA 200.7

Iron, Fe 457 mg/L 5.0 1.0 DAM 08/01/2013 13:21 EPA 200.7

Magnesium, Mg 3830 mg/L 1.0 0.20 DAM 08/01/2013 13:21 EPA 200.7

Manganese, Mn 64.3 mg/L 0.050 0.010 DAM 08/01/2013 13:21 EPA 200.7

Potassium, K 143 mg/L 5.0 0.70 DAM 08/01/2013 13:20 EPA 200.7

Sodium, Na 306 mg/L 5.0 0.80 DAM 08/01/2013 13:20 EPA 200.7

Strontium, Sr 41.5 mg/L 0.10 0.030 DAM 08/01/2013 13:20 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 38.5 mg/L 0.10 0.020 DMM 07/26/2013 SM20 4500NO3 H

Mountaineer Plant, 133027 Page 1 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-001A Date Collected: 07/24/2013 Date Received: 7/24/2013

CPS Influent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.80 ug/L 0.050 0.010 DPC 07/31/2013 13:26 EPA 200.8

Arsenic, As 2.47 ug/L 0.10 0.030 DPC 07/31/2013 13:26 EPA 200.8

Barium, Ba 90.2 ug/L 0.10 0.020 DPC 07/31/2013 13:26 EPA 200.8

Beryllium, Be 12 ug/L J 50 10 DAM 08/01/2013 13:39 EPA 200.7

Cadmium, Cd 173 ug/L 0.050 0.010 DPC 07/31/2013 13:26 EPA 200.8

Chromium, Cr < 0.040 ug/L U 0.20 0.040 DPC 07/31/2013 13:26 EPA 200.8

Cobalt, Co 201 ug/L 0.020 0.0040 DPC 07/31/2013 13:26 EPA 200.8

Copper, Cu 8.08 ug/L 0.050 0.010 DPC 07/31/2013 13:26 EPA 200.8

Lead, Pb 0.095 ug/L 0.010 0.0020 DPC 07/31/2013 13:26 EPA 200.8

Molybdenum, Mo 247 ug/L 0.050 0.010 DPC 07/31/2013 13:26 EPA 200.8

Nickel, Ni 1550 ug/L 0.20 0.050 DPC 07/31/2013 13:26 EPA 200.8

Selenium, Se 365 ug/L 0.50 0.20 DPC 07/31/2013 13:26 EPA 200.8

Selenite, Se+4 (Hydride) 152 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag 0.028 ug/L 0.010 0.0020 DPC 07/31/2013 13:26 EPA 200.8

Thallium, Tl 10.6 ug/L 0.050 0.0020 DPC 07/31/2013 13:26 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:39 EPA 200.7

Titanium, Ti < 30 ug/L U 200 30 DAM 08/01/2013 13:39 EPA 200.7

Zinc, Zn 784 ug/L 0.50 0.10 DPC 07/31/2013 13:26 EPA 200.8

Aluminum, Al 0.115 mg/L 0.0010 0.0003 DPC 07/31/2013 13:26 EPA 200.8

Boron, B 438 mg/L 2.0 0.40 DAM 08/01/2013 13:39 EPA 200.7

Calcium, Ca 806 mg/L 2.0 0.40 DAM 08/01/2013 13:39 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:39 EPA 200.7

Magnesium, Mg 3510 mg/L 1.0 0.20 DAM 08/01/2013 13:39 EPA 200.7

Manganese, Mn 61.8 mg/L 0.050 0.010 DAM 08/01/2013 13:39 EPA 200.7

Potassium, K 62.8 mg/L 5.0 0.70 DAM 08/01/2013 13:37 EPA 200.7

Sodium, Na 307 mg/L 5.0 0.80 DAM 08/01/2013 13:37 EPA 200.7

Strontium, Sr 12.4 mg/L 0.10 0.030 DAM 08/01/2013 13:37 EPA 200.7

Mountaineer Plant, 133027 Page 2 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-002 Date Collected: 07/24/2013 Date Received: 7/24/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.32 ug/L 0.050 0.010 DPC 07/31/2013 13:31 EPA 200.8

Arsenic, As 2.57 ug/L 0.10 0.030 DPC 07/31/2013 13:31 EPA 200.8

Barium, Ba 74.2 ug/L 0.10 0.020 DPC 07/31/2013 13:31 EPA 200.8

Beryllium, Be 11 ug/L J 50 10 DAM 08/01/2013 13:25 EPA 200.7

Cadmium, Cd 0.21 ug/L 0.050 0.010 DPC 07/31/2013 13:31 EPA 200.8

Chromium, Cr 2.1 ug/L 0.20 0.040 DPC 07/31/2013 13:31 EPA 200.8

Cobalt, Co 2.53 ug/L 0.020 0.0040 DPC 07/31/2013 13:31 EPA 200.8

Copper, Cu 1.15 ug/L 0.050 0.010 DPC 07/31/2013 13:31 EPA 200.8

Lead, Pb 0.144 ug/L 0.010 0.0020 DPC 07/31/2013 13:31 EPA 200.8

Mercury, Hg 123 ng/L 20 8.0 TLT 08/01/2013 EPA 1631E

Molybdenum, Mo 236 ug/L 0.050 0.010 DPC 07/31/2013 13:31 EPA 200.8

Nickel, Ni 139 ug/L 0.20 0.050 DPC 07/31/2013 13:31 EPA 200.8

Selenium, Se 195 ug/L 0.50 0.20 DPC 07/31/2013 13:31 EPA 200.8

Silver, Ag 0.013 ug/L 0.010 0.0020 DPC 07/31/2013 13:31 EPA 200.8

Thallium, Tl 1.13 ug/L 0.050 0.0020 DPC 07/31/2013 13:31 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:25 EPA 200.7

Titanium, Ti 45 ug/L J 200 30 DAM 08/01/2013 13:25 EPA 200.7

Zinc, Zn 11.7 ug/L 0.50 0.10 DPC 07/31/2013 13:31 EPA 200.8

Aluminum, Al 0.102 mg/L 0.0010 0.0003 DPC 07/31/2013 13:31 EPA 200.8

Boron, B 257 mg/L 2.0 0.40 DAM 08/01/2013 13:25 EPA 200.7

Calcium, Ca 675 mg/L 2.0 0.40 DAM 08/01/2013 13:25 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:25 EPA 200.7

Magnesium, Mg 2000 mg/L 1.0 0.20 DAM 08/01/2013 13:25 EPA 200.7

Manganese, Mn 31.1 mg/L 0.050 0.010 DAM 08/01/2013 13:25 EPA 200.7

Potassium, K 56.8 mg/L 5.0 0.70 DAM 08/01/2013 13:23 EPA 200.7

Sodium, Na 208 mg/L 5.0 0.80 DAM 08/01/2013 13:23 EPA 200.7

Strontium, Sr 8.30 mg/L 0.10 0.030 DAM 08/01/2013 13:23 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 22.2 mg/L 0.10 0.020 DMM 07/26/2013 SM20 4500NO3 H

Mountaineer Plant, 133027 Page 3 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-002A Date Collected: 07/24/2013 Date Received: 7/24/2013

CPS Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.84 ug/L 0.050 0.010 DPC 07/31/2013 13:35 EPA 200.8

Arsenic, As 2.39 ug/L 0.10 0.030 DPC 07/31/2013 13:35 EPA 200.8

Barium, Ba 72.0 ug/L 0.10 0.020 DPC 07/31/2013 13:35 EPA 200.8

Beryllium, Be 11 ug/L J 50 10 DAM 08/01/2013 13:42 EPA 200.7

Cadmium, Cd 0.09 ug/L 0.050 0.010 DPC 07/31/2013 13:35 EPA 200.8

Chromium, Cr 1.3 ug/L 0.20 0.040 DPC 07/31/2013 13:35 EPA 200.8

Cobalt, Co 1.98 ug/L 0.020 0.0040 DPC 07/31/2013 13:35 EPA 200.8

Copper, Cu 0.77 ug/L 0.050 0.010 DPC 07/31/2013 13:35 EPA 200.8

Lead, Pb 0.073 ug/L 0.010 0.0020 DPC 07/31/2013 13:35 EPA 200.8

Molybdenum, Mo 235 ug/L 0.050 0.010 DPC 07/31/2013 13:35 EPA 200.8

Nickel, Ni 129 ug/L 0.20 0.050 DPC 07/31/2013 13:35 EPA 200.8

Selenium, Se 184 ug/L 0.50 0.20 DPC 07/31/2013 13:35 EPA 200.8

Selenite, Se+4 (Hydride) 87.5 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag 0.013 ug/L 0.010 0.0020 DPC 07/31/2013 13:35 EPA 200.8

Thallium, Tl 1.06 ug/L 0.050 0.0020 DPC 07/31/2013 13:35 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:43 EPA 200.7

Titanium, Ti 44 ug/L J 200 30 DAM 08/01/2013 13:42 EPA 200.7

Zinc, Zn 8.5 ug/L 0.50 0.10 DPC 07/31/2013 13:35 EPA 200.8

Aluminum, Al 0.0625 mg/L 0.0010 0.0003 DPC 07/31/2013 13:35 EPA 200.8

Boron, B 257 mg/L 2.0 0.40 DAM 08/01/2013 13:42 EPA 200.7

Calcium, Ca 674 mg/L 2.0 0.40 DAM 08/01/2013 13:42 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:43 EPA 200.7

Magnesium, Mg 2010 mg/L 1.0 0.20 DAM 08/01/2013 13:42 EPA 200.7

Manganese, Mn 31.0 mg/L 0.050 0.010 DAM 08/01/2013 13:42 EPA 200.7

Potassium, K 43.4 mg/L 5.0 0.70 DAM 08/01/2013 13:41 EPA 200.7

Sodium, Na 205 mg/L 5.0 0.80 DAM 08/01/2013 13:41 EPA 200.7

Strontium, Sr 8.29 mg/L 0.10 0.030 DAM 08/01/2013 13:41 EPA 200.7

Mountaineer Plant, 133027 Page 4 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-003 Date Collected: 07/24/2013 Date Received: 7/24/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.5 ug/L 0.050 0.010 DPC 07/31/2013 13:40 EPA 200.8

Arsenic, As 45.8 ug/L 0.10 0.030 DPC 07/31/2013 13:40 EPA 200.8

Barium, Ba 36.1 ug/L 0.10 0.020 DPC 07/31/2013 13:40 EPA 200.8

Beryllium, Be 13 ug/L J 50 10 DAM 08/01/2013 13:28 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/31/2013 13:40 EPA 200.8

Chromium, Cr 0.5 ug/L 0.20 0.040 DPC 07/31/2013 13:40 EPA 200.8

Cobalt, Co 3.05 ug/L 0.020 0.0040 DPC 07/31/2013 13:40 EPA 200.8

Copper, Cu 1.48 ug/L 0.050 0.010 DPC 07/31/2013 13:40 EPA 200.8

Lead, Pb 4.52 ug/L 0.010 0.0020 DPC 07/31/2013 13:40 EPA 200.8

Mercury, Hg 75.5 ng/L 10 4.0 TLT 08/01/2013 EPA 1631E

Molybdenum, Mo 6190 ug/L 0.050 0.010 DPC 07/31/2013 13:40 EPA 200.8

Nickel, Ni 9.31 ug/L 0.20 0.050 DPC 07/31/2013 13:40 EPA 200.8

Selenium, Se 236 ug/L 0.50 0.20 DPC 07/31/2013 13:40 EPA 200.8

Silver, Ag 0.011 ug/L 0.010 0.0020 DPC 07/31/2013 13:40 EPA 200.8

Thallium, Tl 2.21 ug/L 0.050 0.0020 DPC 07/31/2013 13:40 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:29 EPA 200.7

Titanium, Ti < 30 ug/L U 200 30 DAM 08/01/2013 13:28 EPA 200.7

Zinc, Zn 7.4 ug/L 0.50 0.10 DPC 07/31/2013 13:40 EPA 200.8

Aluminum, Al 0.0620 mg/L 0.0010 0.0003 DPC 07/31/2013 13:40 EPA 200.8

Boron, B 54.0 mg/L 2.0 0.40 DAM 08/01/2013 13:28 EPA 200.7

Calcium, Ca 421 mg/L 2.0 0.40 DAM 08/01/2013 13:28 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:29 EPA 200.7

Magnesium, Mg 397 mg/L 1.0 0.20 DAM 08/01/2013 13:28 EPA 200.7

Manganese, Mn 1.91 mg/L 0.050 0.010 DAM 08/01/2013 13:29 EPA 200.7

Potassium, K 105 mg/L 5.0 0.70 DAM 08/01/2013 13:27 EPA 200.7

Sodium, Na 1750 mg/L 5.0 0.80 DAM 08/01/2013 13:27 EPA 200.7

Strontium, Sr 5.45 mg/L 0.10 0.030 DAM 08/01/2013 13:27 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 4.74 mg/L 0.10 0.020 DMM 07/26/2013 SM20 4500NO3 H

Mountaineer Plant, 133027 Page 5 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-003A Date Collected: 07/24/2013 Date Received: 7/24/2013

Landfill Leachate Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.5 ug/L 0.050 0.010 DPC 07/31/2013 13:59 EPA 200.8

Arsenic, As 42.4 ug/L 0.10 0.030 DPC 07/31/2013 13:59 EPA 200.8

Barium, Ba 34.2 ug/L 0.10 0.020 DPC 07/31/2013 13:59 EPA 200.8

Beryllium, Be 13 ug/L J 50 10 DAM 08/01/2013 13:57 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/31/2013 13:59 EPA 200.8

Chromium, Cr 0.15 ug/L J 0.20 0.040 DPC 07/31/2013 13:59 EPA 200.8

Cobalt, Co 2.13 ug/L 0.020 0.0040 DPC 07/31/2013 13:59 EPA 200.8

Copper, Cu 0.89 ug/L 0.050 0.010 DPC 07/31/2013 13:59 EPA 200.8

Lead, Pb 0.099 ug/L 0.010 0.0020 DPC 07/31/2013 13:59 EPA 200.8

Molybdenum, Mo 6170 ug/L 0.050 0.010 DPC 07/31/2013 13:59 EPA 200.8

Nickel, Ni 8.97 ug/L 0.20 0.050 DPC 07/31/2013 13:59 EPA 200.8

Selenium, Se 193 ug/L 0.50 0.20 DPC 07/31/2013 13:59 EPA 200.8

Selenite, Se+4 (Hydride) 82.7 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag 0.011 ug/L 0.010 0.0020 DPC 07/31/2013 13:59 EPA 200.8

Thallium, Tl 2.14 ug/L 0.050 0.0020 DPC 07/31/2013 13:59 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:57 EPA 200.7

Titanium, Ti < 30 ug/L U 200 30 DAM 08/01/2013 13:57 EPA 200.7

Zinc, Zn 7.0 ug/L 0.50 0.10 DPC 07/31/2013 13:59 EPA 200.8

Aluminum, Al 0.0227 mg/L 0.0010 0.0003 DPC 07/31/2013 13:59 EPA 200.8

Boron, B 51.0 mg/L 2.0 0.40 DAM 08/01/2013 13:57 EPA 200.7

Calcium, Ca 401 mg/L 2.0 0.40 DAM 08/01/2013 13:57 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:57 EPA 200.7

Magnesium, Mg 379 mg/L 1.0 0.20 DAM 08/01/2013 13:57 EPA 200.7

Manganese, Mn 1.73 mg/L 0.050 0.010 DAM 08/01/2013 13:57 EPA 200.7

Potassium, K 98.1 mg/L 5.0 0.70 DAM 08/01/2013 13:55 EPA 200.7

Sodium, Na 1680 mg/L 5.0 0.80 DAM 08/01/2013 13:55 EPA 200.7

Strontium, Sr 5.26 mg/L 0.10 0.030 DAM 08/01/2013 13:55 EPA 200.7

Mountaineer Plant, 133027 Page 6 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-004 Date Collected: 07/24/2013 Date Received: 7/24/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.71 ug/L 0.050 0.010 DPC 07/31/2013 14:04 EPA 200.8

Arsenic, As 19.0 ug/L 0.10 0.030 DPC 07/31/2013 14:04 EPA 200.8

Barium, Ba 60.2 ug/L 0.10 0.020 DPC 07/31/2013 14:04 EPA 200.8

Beryllium, Be < 10 ug/L U 50 10 DAM 08/01/2013 13:32 EPA 200.7

Cadmium, Cd 0.28 ug/L 0.050 0.010 DPC 07/31/2013 14:04 EPA 200.8

Chromium, Cr 1.6 ug/L 0.20 0.040 DPC 07/31/2013 14:04 EPA 200.8

Cobalt, Co 2.47 ug/L 0.020 0.0040 DPC 07/31/2013 14:04 EPA 200.8

Copper, Cu 1.96 ug/L 0.050 0.010 DPC 07/31/2013 14:04 EPA 200.8

Lead, Pb 0.286 ug/L 0.010 0.0020 DPC 07/31/2013 14:04 EPA 200.8

Mercury, Hg 98.5 ng/L 10 4.0 TLT 08/01/2013 EPA 1631E

Molybdenum, Mo 2580 ug/L 0.050 0.010 DPC 07/31/2013 14:04 EPA 200.8

Nickel, Ni 93.8 ug/L 0.20 0.050 DPC 07/31/2013 14:04 EPA 200.8

Selenium, Se 204 ug/L 0.50 0.20 DPC 07/31/2013 14:04 EPA 200.8

Silver, Ag 0.013 ug/L 0.010 0.0020 DPC 07/31/2013 14:04 EPA 200.8

Thallium, Tl 1.66 ug/L 0.050 0.0020 DPC 07/31/2013 14:04 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:32 EPA 200.7

Titanium, Ti < 30 ug/L U 200 30 DAM 08/01/2013 13:32 EPA 200.7

Zinc, Zn 9.6 ug/L 0.50 0.10 DPC 07/31/2013 14:04 EPA 200.8

Aluminum, Al 0.0727 mg/L 0.0010 0.0003 DPC 07/31/2013 14:04 EPA 200.8

Boron, B 178 mg/L 2.0 0.40 DAM 08/01/2013 13:32 EPA 200.7

Calcium, Ca 568 mg/L 2.0 0.40 DAM 08/01/2013 13:32 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:32 EPA 200.7

Magnesium, Mg 1390 mg/L 1.0 0.20 DAM 08/01/2013 13:32 EPA 200.7

Manganese, Mn 19.0 mg/L 0.050 0.010 DAM 08/01/2013 13:32 EPA 200.7

Potassium, K 62.9 mg/L 5.0 0.70 DAM 08/01/2013 13:30 EPA 200.7

Sodium, Na 788 mg/L 5.0 0.80 DAM 08/01/2013 13:30 EPA 200.7

Strontium, Sr 6.94 mg/L 0.10 0.030 DAM 08/01/2013 13:30 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 15.1 mg/L 0.10 0.020 DMM 07/26/2013 SM20 4500NO3 H

Mountaineer Plant, 133027 Page 7 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-004A Date Collected: 07/24/2013 Date Received: 7/24/2013

1st Stage Feed Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.45 ug/L 0.050 0.010 DPC 07/31/2013 14:09 EPA 200.8

Arsenic, As 17.2 ug/L 0.10 0.030 DPC 07/31/2013 14:09 EPA 200.8

Barium, Ba 59.5 ug/L 0.10 0.020 DPC 07/31/2013 14:09 EPA 200.8

Beryllium, Be < 10 ug/L U 50 10 DAM 08/01/2013 14:00 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/31/2013 14:09 EPA 200.8

Chromium, Cr 1.0 ug/L 0.20 0.040 DPC 07/31/2013 14:09 EPA 200.8

Cobalt, Co 2.01 ug/L 0.020 0.0040 DPC 07/31/2013 14:09 EPA 200.8

Copper, Cu 0.85 ug/L 0.050 0.010 DPC 07/31/2013 14:09 EPA 200.8

Lead, Pb 0.047 ug/L 0.010 0.0020 DPC 07/31/2013 14:09 EPA 200.8

Molybdenum, Mo 2560 ug/L 0.050 0.010 DPC 07/31/2013 14:09 EPA 200.8

Nickel, Ni 83.4 ug/L 0.20 0.050 DPC 07/31/2013 14:09 EPA 200.8

Selenium, Se 188 ug/L 0.50 0.20 DPC 07/31/2013 14:09 EPA 200.8

Selenite, Se+4 (Hydride) 79.0 ug/L 20 4.0 TLT 08/05/2013 AEP Method

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 07/31/2013 14:09 EPA 200.8

Thallium, Tl 1.26 ug/L 0.050 0.0020 DPC 07/31/2013 14:09 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 14:01 EPA 200.7

Titanium, Ti < 30 ug/L U 200 30 DAM 08/01/2013 14:00 EPA 200.7

Zinc, Zn 7.4 ug/L 0.50 0.10 DPC 07/31/2013 14:09 EPA 200.8

Aluminum, Al 0.0434 mg/L 0.0010 0.0003 DPC 07/31/2013 14:09 EPA 200.8

Boron, B 161 mg/L 2.0 0.40 DAM 08/01/2013 14:00 EPA 200.7

Calcium, Ca 510 mg/L 2.0 0.40 DAM 08/01/2013 14:00 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 14:01 EPA 200.7

Magnesium, Mg 1240 mg/L 1.0 0.20 DAM 08/01/2013 14:00 EPA 200.7

Manganese, Mn 17.0 mg/L 0.050 0.010 DAM 08/01/2013 14:00 EPA 200.7

Potassium, K 59.9 mg/L 5.0 0.70 DAM 08/01/2013 13:59 EPA 200.7

Sodium, Na 746 mg/L 5.0 0.80 DAM 08/01/2013 13:59 EPA 200.7

Strontium, Sr 6.57 mg/L 0.10 0.030 DAM 08/01/2013 13:59 EPA 200.7

Mountaineer Plant, 133027 Page 8 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-005 Date Collected: 07/24/2013 Date Received: 7/24/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.40 ug/L 0.050 0.010 DPC 07/31/2013 14:14 EPA 200.8

Arsenic, As 0.88 ug/L 0.10 0.030 DPC 07/31/2013 14:14 EPA 200.8

Barium, Ba 79.6 ug/L 0.10 0.020 DPC 07/31/2013 14:14 EPA 200.8

Beryllium, Be 14 ug/L J 50 10 DAM 08/01/2013 13:35 EPA 200.7

Cadmium, Cd 0.011 ug/L J 0.050 0.010 DPC 07/31/2013 14:14 EPA 200.8

Chromium, Cr 1.2 ug/L 0.20 0.040 DPC 07/31/2013 14:14 EPA 200.8

Cobalt, Co 0.050 ug/L 0.020 0.0040 DPC 07/31/2013 14:14 EPA 200.8

Copper, Cu 3.89 ug/L 0.050 0.010 DPC 07/31/2013 14:14 EPA 200.8

Lead, Pb 0.163 ug/L 0.010 0.0020 DPC 07/31/2013 14:14 EPA 200.8

Mercury, Hg 2.7 ng/L 1.0 0.40 TLT 08/01/2013 EPA 1631E

Molybdenum, Mo 6.74 ug/L 0.050 0.010 DPC 07/31/2013 14:14 EPA 200.8

Nickel, Ni 2.65 ug/L 0.20 0.050 DPC 07/31/2013 14:14 EPA 200.8

Selenium, Se 2.4 ug/L 0.50 0.20 DPC 07/31/2013 14:14 EPA 200.8

Silver, Ag 0.015 ug/L 0.010 0.0020 DPC 07/31/2013 14:14 EPA 200.8

Thallium, Tl < 0.0020 ug/L U 0.050 0.0020 DPC 07/31/2013 14:14 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 13:36 EPA 200.7

Titanium, Ti 54 ug/L J 200 30 DAM 08/01/2013 13:35 EPA 200.7

Zinc, Zn 6.2 ug/L 0.50 0.10 DPC 07/31/2013 14:14 EPA 200.8

Aluminum, Al 2.48 mg/L 0.0010 0.0003 DPC 07/31/2013 14:14 EPA 200.8

Boron, B 185 mg/L 2.0 0.40 DAM 08/01/2013 13:35 EPA 200.7

Calcium, Ca 594 mg/L 2.0 0.40 DAM 08/01/2013 13:35 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 13:36 EPA 200.7

Magnesium, Mg 1430 mg/L 1.0 0.20 DAM 08/01/2013 13:35 EPA 200.7

Manganese, Mn 19.2 mg/L 0.050 0.010 DAM 08/01/2013 13:35 EPA 200.7

Potassium, K 63.2 mg/L 5.0 0.70 DAM 08/01/2013 13:34 EPA 200.7

Sodium, Na 730 mg/L 5.0 0.80 DAM 08/01/2013 13:34 EPA 200.7

Strontium, Sr 7.02 mg/L 0.10 0.030 DAM 08/01/2013 13:34 EPA 200.7

Nitrate-Nitrite, NO3-NO2, as N 0.80 mg/L 0.10 0.020 DMM 07/26/2013 SM20 4500NO3 H

Mountaineer Plant, 133027 Page 9 of 10
Location: Mountaineer Plant Report Date: 8/7/2013

Sample Number: 133027-005A Date Collected: 07/24/2013 Date Received: 7/24/2013

Bioreactor Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.40 ug/L 0.050 0.010 DPC 07/31/2013 14:18 EPA 200.8

Arsenic, As 0.83 ug/L 0.10 0.030 DPC 07/31/2013 14:18 EPA 200.8

Barium, Ba 74.1 ug/L 0.10 0.020 DPC 07/31/2013 14:18 EPA 200.8

Beryllium, Be 14 ug/L J 50 10 DAM 08/01/2013 14:04 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 07/31/2013 14:18 EPA 200.8

Chromium, Cr 1.0 ug/L 0.20 0.040 DPC 07/31/2013 14:18 EPA 200.8

Cobalt, Co 0.050 ug/L 0.020 0.0040 DPC 07/31/2013 14:18 EPA 200.8

Copper, Cu 0.61 ug/L 0.050 0.010 DPC 07/31/2013 14:18 EPA 200.8

Lead, Pb 0.0030 ug/L J 0.010 0.0020 DPC 07/31/2013 14:18 EPA 200.8

Molybdenum, Mo 4.01 ug/L 0.050 0.010 DPC 07/31/2013 14:18 EPA 200.8

Nickel, Ni 2.11 ug/L 0.20 0.050 DPC 07/31/2013 14:18 EPA 200.8

Selenium, Se 1.4 ug/L 0.50 0.20 DPC 07/31/2013 14:18 EPA 200.8

Selenite, Se+4 (Hydride) < 0.80 ug/L U 4.0 0.80 TLT 08/05/2013 AEP Method

Silver, Ag 0.0060 ug/L J 0.010 0.0020 DPC 07/31/2013 14:18 EPA 200.8

Thallium, Tl < 0.0020 ug/L U 0.050 0.0020 DPC 07/31/2013 14:18 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 08/01/2013 14:04 EPA 200.7

Titanium, Ti 52 ug/L J 200 30 DAM 08/01/2013 14:04 EPA 200.7

Zinc, Zn 4.7 ug/L 0.50 0.10 DPC 07/31/2013 14:18 EPA 200.8

Aluminum, Al 2.26 mg/L 0.0010 0.0003 DPC 07/31/2013 14:18 EPA 200.8

Boron, B 182 mg/L 2.0 0.40 DAM 08/01/2013 14:04 EPA 200.7

Calcium, Ca 579 mg/L 2.0 0.40 DAM 08/01/2013 14:04 EPA 200.7

Iron, Fe < 1.0 mg/L U 5.0 1.0 DAM 08/01/2013 14:04 EPA 200.7

Magnesium, Mg 1400 mg/L 1.0 0.20 DAM 08/01/2013 14:04 EPA 200.7

Manganese, Mn 18.9 mg/L 0.050 0.010 DAM 08/01/2013 14:04 EPA 200.7

Potassium, K 62.9 mg/L 5.0 0.70 DAM 08/01/2013 14:02 EPA 200.7

Sodium, Na 731 mg/L 5.0 0.80 DAM 08/01/2013 14:02 EPA 200.7

Strontium, Sr 6.93 mg/L 0.10 0.030 DAM 08/01/2013 14:02 EPA 200.7

Sample Number: 133027-006 Date Collected: 07/24/2013 Date Received: 7/24/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.31 ng/L J 0.50 0.20 TLT 08/01/2013 EPA 1631E

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133027 Page 10 of 10