SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-003 Red Hill

The Environmental Company, Inc. (TEC)

1103478

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Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1103478 3354-003 Red Hill

Customer:

Project:

SGS North America Inc.

Refer to the sample receipt form for information on sample condition.

1103478005 PS RHMW01-WG20

Revised Report – Sample ID was changed from “RHMWA01” to “RHMW01” at client’s request. Sample ID was 

changed to match COC.

1103478007 PS RHMW02-WG20

AK102 - The pattern is consistent with a weathered middle distillate.

1103478008 PS RHMWA01-WG20

AK102 - The pattern is consistent with a weathered middle distillate.

1103478002 BMS RHMW2254-WG20 MS

8270D SIM - BMS recoveries for multiple analytes are outside of QC criteria. Refer to LCS for accuracy.

8260B - BMS recovery for chloroethane does not meet QC criteria (biased high). This analyte was not detected 

above the LOQ in the original sample.

974519 MS 1103478001MS

8270D SIM - MS recoveries for multiple analytes are outside of QC criteria. Refer to LCS for accuracy.

1103478003 BMSD RHMW2254-WG21 MSD

8270D - BMS/BMSD RPD for multiple analytes does not meet QC criteria. Results for these analytes are estimated 

in the original sample.

8260B - BMSD recoveries for chloroethane and benzene do not meet QC criteria (biased high). These analytes 

were not detected above the LOQ in the original sample.

974520 MSD 1103478001MSD

8270D - MS/MSD RPD for multiple analytes does not meet QC criteria. Results for these analytes are estimated in 

the original sample.

974727 LCSD VXX/20956

8260B - LCSD recovery for 1,1,-Trichloroethane does not meet QC criteria (biased low). Refer to LCS for accuracy.

974730 CCV VMS/11399]

8260B - ICV recovery for vinyl chloride was biased high. Results may be estimated where detected.

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Report of Manual Integrations Print Date: 8/17/2010 10:37 am

Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS 2-Methylnaphthalene PNF

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Anthracene RP

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo(a)Anthracene PNF

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo[b]Fluoranthene PNF

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Benzo[k]fluoranthene RP

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Chrysene RP

974244 LCS for HBN 550180 [XXX/23075] XMS5529 8270D SIMS Phenanthrene RP

Manual Integration Reason Code Descriptions

Code Description

O Original Chromatogram

M Modified Chromatogram

SS Skimmed surrogate

BLG Closed baseline gap

RP Reassign peak name

PIR Pattern integration required

IT Included tail

SP Split peak

RSP Removed split peak

FPS Forced peak start/stop

BLC Baseline correction

PNF Peak not found by software

All DRO/RRO analysis are integrated per SOP.

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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3354-003 Red Hill

Project Manager

jennifer.serna@sgs.com

Jennifer Serna

T: (808)528-1445 F:(808)528-0768

Attn: Rick Adkisson

1003 Bishop Street,

Pauahi Tower Suite 1550

Honolulu, HI 96813

Certification:

This data package is in compliance with the terms and conditions of the contract, both 

technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or 

case narrative. This certification applies only to the tested parameters and the specific 

sample(s) received at the laboratory. If you have any questions regarding this report, or if we 

can be of further assistance, please contact your SGS Project Manager.

1103478

The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project:

Laboratory Analytical Report

Contents (Bookmarked in PDF):

Cover Page

Glossary

Sample Summary Forms

Case Narrative

Sample Results Forms

Batch Summary Forms (by method)

Quality Control Summary Forms (by method)

Chain of Custody/Sample Receipt Forms

Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

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Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not 

responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please 

contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions 

(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this 

program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for 

ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 

8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all 

statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental 

Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 2xDL)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RL Reporting Limit

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

Print Date: 8/17/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-003 Red Hill

Workorder No.: 1103478

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Volatile Organic Compounds (W) FULL SW8260B

Print Date: 8/17/2010 10:37 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1103478001 RHMW2254-WG20

1103478002 RHMW2254-WG20 MS

1103478003 RHMW2254-WG21 MSD

1103478004 RHMW05-WG20

1103478005 RHMW01-WG20

1103478006 RHMW03-WG20

1103478007 RHMW02-WG20

1103478008 RHMWA01-WG20

1103478009 TB01-WG20

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6555 MXX23263

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6555

Analytical Method: SW6020

Analysis Date/Time: 07/27/10 17:02

Prep Batch: MXX23263

Prep Method: SW3010A

Prep Date/Time: 07/21/10 23:00 Container ID:1103478001-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 99.1 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 13:40

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478001-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.320 U 0.426 0.160 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 83.1 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 18:39

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478001-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11403 VXX20964

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11403 VXX20964

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11403 VXX20964

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11403 VXX20964

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11403 VXX20964

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11403 VXX20964

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11403 VXX20964

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11403 VXX20964

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11403 VXX20964

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11403 VXX20964

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11403 VXX20964

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11403 VXX20964

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11403 VXX20964

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11403 VXX20964

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11403 VXX20964

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11403 VXX20964

1,2-Dichloroethane-D4 <surr> 119 73-120 % 1 VMS11403 VXX20964

4-Bromofluorobenzene <surr> 92.1 76-120 % 1 VMS11403 VXX20964

Toluene-d8 <surr> 96.3 80-120 % 1 VMS11403 VXX20964

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11403

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 19:27

Prep Batch: VXX20964

Prep Method: SW5030B

Prep Date/Time: 07/19/10 14:07 Container ID:1103478001-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW2254-WG20

SGS Ref. #: 1103478001 Collection Date/Time: 07/13/10 09:40

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

2-Methylnaphthalene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Chrysene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Fluorene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Naphthalene 0.0664 U 0.107 0.0332 ug/L 1 XMS5528 XXX23075

Phenanthrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 93 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 935 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/19/10 23:07

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478001-I

Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:22

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103478004-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 99.2 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 15:56

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478004-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

15 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.320 U 0.426 0.160 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 81.7 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 19:43

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478004-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

16 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

17 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 107 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 97.7 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

18 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 08:50

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478004-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

19 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW05-WG20

SGS Ref. #: 1103478004 Collection Date/Time: 07/13/10 17:20

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

2-Methylnaphthalene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Chrysene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Fluorene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Naphthalene 0.0643J 0.105 0.0326 ug/L 1 XMS5528 XXX23075

Phenanthrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 90.3 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 00:01

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478004-I

Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

20 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:40

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103478005-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

21 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 16:15

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478005-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

22 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.228J 0.435 0.163 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 85.1 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 20:04

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478005-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

23 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

24 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 1.08 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 106 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 94.8 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 99.2 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

25 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 09:24

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478005-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

26 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW01-WG20

SGS Ref. #: 1103478005 Collection Date/Time: 07/13/10 15:55

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

2-Methylnaphthalene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.0321J 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Chrysene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Fluorene 0.0350J 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Naphthalene 0.184 0.105 0.0326 ug/L 1 XMS5528 XXX23075

Phenanthrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Pyrene 0.0316 U 0.0526 0.0158 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 93.2 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 00:19

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478005-I

Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

27 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:42

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103478006-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

28 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 101 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 16:35

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478006-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

29 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.324 U 0.432 0.162 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 81.3 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 925 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 21:07

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478006-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

30 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

31 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 107 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 95.2 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

32 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 09:57

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478006-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

33 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW03-WG20

SGS Ref. #: 1103478006 Collection Date/Time: 07/13/10 11:35

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

2-Methylnaphthalene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Chrysene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Fluorene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Naphthalene 0.0666 U 0.108 0.0333 ug/L 1 XMS5528 XXX23075

Phenanthrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 88.1 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 00:36

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478006-I

Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

34 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:44

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103478007-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

35 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 46.5J 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 122 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 16:54

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478007-C

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

36 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 3.06 0.435 0.163 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 83.6 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 21:28

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478007-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

37 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.360J 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

38 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 107 20.0 6.20 ug/L 10 VMS11403 VXX20964

n-Butylbenzene 4.41 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 7.92 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.690J 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 4.17 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 1.52 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 107 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 94.2 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

39 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 10:31

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478007-A

Dilution Factor: 1 Analyst: SCL

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11403

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 23:58

Prep Batch: VXX20964

Prep Method: SW5030B

Prep Date/Time: 07/19/10 14:07 Container ID:1103478007-B

Dilution Factor: 10 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

40 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMW02-WG20

SGS Ref. #: 1103478007 Collection Date/Time: 07/13/10 14:10

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 7.43 2.15 0.645 ug/L 40 XMS5529 XXX23075

2-Methylnaphthalene 1.06 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.287 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Chrysene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Fluorene 0.159 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Naphthalene 59.9 4.30 1.33 ug/L 40 XMS5529 XXX23075

Phenanthrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Pyrene 0.0322 U 0.0538 0.0161 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 90.7 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 00:54

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478007-I

Dilution Factor: 1 Analyst: CDE

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5529

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 08:57

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478007-I

Dilution Factor: 40 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

41 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:46

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103478008-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

42 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 45.4J 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 120 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 17:14

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478008-C

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

43 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 3.11 0.426 0.160 mg/L 1 XFC9360 XXX23089

5a Androstane <surr> 83.4 50-150 % 1 XFC9360 XXX23089

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9360

Analytical Method: SW8015C

Analysis Date/Time: 07/21/10 21:49

Prep Batch: XXX23089

Prep Method: SW3520C

Prep Date/Time: 07/20/10 09:30 Container ID:1103478008-J

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

44 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

45 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 102 20.0 6.20 ug/L 10 VMS11403 VXX20964

n-Butylbenzene 4.89 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 8.85 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.660J 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 4.66 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 1.61 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 110 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 94.1 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

46 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 11:05

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478008-A

Dilution Factor: 1 Analyst: SCL

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11403

Analytical Method: SW8260B

Analysis Date/Time: 07/21/10 00:31

Prep Batch: VXX20964

Prep Method: SW5030B

Prep Date/Time: 07/19/10 14:07 Container ID:1103478008-B

Dilution Factor: 10 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

47 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: RHMWA01-WG20

SGS Ref. #: 1103478008 Collection Date/Time: 07/13/10 12:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 7.05 2.09 0.628 ug/L 40 XMS5529 XXX23075

2-Methylnaphthalene 0.937 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Acenaphthene 0.309 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Acenaphthylene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Anthracene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Benzo(a)Anthracene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Benzo[a]pyrene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Benzo[b]Fluoranthene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Benzo[g,h,i]perylene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Benzo[k]fluoranthene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Chrysene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Dibenzo[a,h]anthracene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Fluoranthene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Fluorene 0.165 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Indeno[1,2,3-c,d] pyrene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Naphthalene 61.1 4.19 1.30 ug/L 40 XMS5529 XXX23075

Phenanthrene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Pyrene 0.0314 U 0.0524 0.0157 ug/L 1 XMS5528 XXX23075

Terphenyl-d14 <surr> 87.5 50-135 % 1 XMS5528 XXX23075

Batch Information

Initial Prep Wt./Vol.: 955 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5528

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 01:12

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478008-I

Dilution Factor: 1 Analyst: CDE

Initial Prep Wt./Vol.: 955 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5529

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/20/10 09:15

Prep Batch: XXX23075

Prep Method: SW3520C

Prep Date/Time: 07/19/10 09:05 Container ID:1103478008-I

Dilution Factor: 40 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

48 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: TB01-WG20

SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10038 VXX20986

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC10038 VXX20986

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10038

Analytical Method: SW8015C

Analysis Date/Time: 07/25/10 14:57

Prep Batch: VXX20986

Prep Method: SW5030B

Prep Date/Time: 07/25/10 10:00 Container ID:1103478009-A

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

49 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: TB01-WG20

SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

2-Hexanone 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11399 VXX20956

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11399 VXX20956

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

Carbon disulfide 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

50 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: TB01-WG20

SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11399 VXX20956

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11399 VXX20956

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11399 VXX20956

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11399 VXX20956

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11399 VXX20956

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11399 VXX20956

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11399 VXX20956

1,2-Dichloroethane-D4 <surr> 107 73-120 % 1 VMS11399 VXX20956

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS11399 VXX20956

Toluene-d8 <surr> 99.6 80-120 % 1 VMS11399 VXX20956

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

51 of 103
The Environmental Company, Inc. (TEC) Print Date: 8/17/2010 10:37 am

Client Sample ID: TB01-WG20

SGS Ref. #: 1103478009 Collection Date/Time: 07/13/10 08:05

Project ID: 3354-003 Red Hill Receipt Date/Time: 07/15/10 12:35

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11399

Analytical Method: SW8260B

Analysis Date/Time: 07/20/10 08:16

Prep Batch: VXX20956

Prep Method: SW5030B

Prep Date/Time: 07/19/10 08:14 Container ID:1103478009-B

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

52 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974243 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

XXX23075

SW3520C

07/19/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 07/19/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 07/19/10

Surrogates 

Terphenyl-d14 <surr> 97.1 50-135 % 07/19/10

Instrument

Method

Batch XMS5528

8270D SIMS

HP 6890/5973 MS SVQA

53 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974420 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

MXX23243

SW3010A

07/16/2010

QC results affect the following production samples:

1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 07/21/10

Instrument

Method

Batch MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

54 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974677 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

XXX23089

SW3520C

07/20/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter Results LOQ/CL Units

Analysis

DL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 07/21/10

Surrogates 

5a Androstane <surr> 77.6 60-120 % 07/21/10

Instrument

Method

Batch XFC9360

SW8015C

HP 7890A FID SV E R

55 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974725 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

QC results affect the following production samples:

1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

56 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974725 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 07/20/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 07/20/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 07/20/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 07/20/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/20/10

2-Hexanone 6.20 U 10.0 3.10 ug/L 07/20/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/20/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 07/20/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 07/20/10

Benzene 0.240 U 0.400 0.120 ug/L 07/20/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 07/20/10

Bromoform 0.620 U 1.00 0.310 ug/L 07/20/10

Bromomethane 1.88 U 3.00 0.940 ug/L 07/20/10

Carbon disulfide 1.24 U 2.00 0.620 ug/L 07/20/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 07/20/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 07/20/10

Chloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

Chloroform 0.600 U 1.00 0.300 ug/L 07/20/10

Chloromethane 0.620 U 1.00 0.310 ug/L 07/20/10

57 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974725 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 07/20/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 07/20/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 07/20/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 07/20/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 07/20/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 07/20/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 07/20/10

Naphthalene 1.24 U 2.00 0.620 ug/L 07/20/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

o-Xylene 0.620 U 1.00 0.310 ug/L 07/20/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 07/20/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Styrene 0.620 U 1.00 0.310 ug/L 07/20/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

Toluene 0.620 U 1.00 0.310 ug/L 07/20/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/20/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 07/20/10

Xylenes (total) 1.88 U 3.00 0.940 ug/L 07/20/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 108 73-120 % 07/20/10

4-Bromofluorobenzene <surr> 102 76-120 % 07/20/10

Toluene-d8 <surr> 100 80-120 % 07/20/10

Instrument

Method

Batch VMS11399

SW8260B

HP 5890 Series II MS3 VNA

58 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975092 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

QC results affect the following production samples:

1103478001, 1103478007, 1103478008

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

59 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975092 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 07/20/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 07/20/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 07/20/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 07/20/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/20/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 07/20/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/20/10

2-Hexanone 6.20 U 10.0 3.10 ug/L 07/20/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/20/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 07/20/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 07/20/10

Benzene 0.240 U 0.400 0.120 ug/L 07/20/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 07/20/10

Bromoform 0.620 U 1.00 0.310 ug/L 07/20/10

Bromomethane 1.88 U 3.00 0.940 ug/L 07/20/10

Carbon disulfide 1.24 U 2.00 0.620 ug/L 07/20/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 07/20/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 07/20/10

Chloroethane 0.620 U 1.00 0.310 ug/L 07/20/10

Chloroform 0.600 U 1.00 0.300 ug/L 07/20/10

Chloromethane 0.620 U 1.00 0.310 ug/L 07/20/10

60 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975092 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 07/20/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 07/20/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 07/20/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 07/20/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 07/20/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 07/20/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 07/20/10

Naphthalene 1.24 U 2.00 0.620 ug/L 07/20/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

o-Xylene 0.620 U 1.00 0.310 ug/L 07/20/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 07/20/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Styrene 0.620 U 1.00 0.310 ug/L 07/20/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/20/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

Toluene 0.620 U 1.00 0.310 ug/L 07/20/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/20/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 07/20/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 07/20/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 07/20/10

Xylenes (total) 1.88 U 3.00 0.940 ug/L 07/20/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 119 73-120 % 07/20/10

4-Bromofluorobenzene <surr> 93.2 76-120 % 07/20/10

Toluene-d8 <surr> 93.8 80-120 % 07/20/10

Instrument

Method

Batch VMS11403

SW8260B

HP 5890 Series II MS3 VNA

61 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975359 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

MXX23263

SW3010A

07/21/2010

QC results affect the following production samples:

1103478001

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 07/27/10

Instrument

Method

Batch MMS6555

SW6020

Perkin Elmer Sciex ICP-MS P3

62 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

976050 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20986

SW5030B

07/25/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Fuels Department

Gasoline Range Organics 60.0 U 100 30.0 ug/L 07/25/10

Surrogates 

4-Bromofluorobenzene <surr> 101 50-150 % 07/25/10

Instrument

Method

Batch VFC10038

SW8015C

HP 5890 Series II PID+FID VCA

63 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974244 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

XXX23075

SW3520C

07/19/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

1-Methylnaphthalene LCS 0.436 87 ( 58-114 ) 0.5 ug/L 07/20/2010

2-Methylnaphthalene LCS 0.398 80 ( 54-105 ) 0.5 ug/L 07/20/2010

Acenaphthene LCS 0.429 86 ( 57-110 ) 0.5 ug/L 07/20/2010

Acenaphthylene LCS 0.440 88 ( 58-105 ) 0.5 ug/L 07/20/2010

Anthracene LCS 0.458 92 ( 63-120 ) 0.5 ug/L 07/20/2010

Benzo(a)Anthracene LCS 0.477 95 ( 61-120 ) 0.5 ug/L 07/20/2010

Benzo[a]pyrene LCS 0.420 84 ( 57-120 ) 0.5 ug/L 07/20/2010

Benzo[b]Fluoranthene LCS 0.505 101 ( 66-130 ) 0.5 ug/L 07/20/2010

Benzo[g,h,i]perylene LCS 0.513 103 ( 60-125 ) 0.5 ug/L 07/20/2010

Benzo[k]fluoranthene LCS 0.476 95 ( 67-125 ) 0.5 ug/L 07/20/2010

Chrysene LCS 0.500 100 ( 71-120 ) 0.5 ug/L 07/20/2010

Dibenzo[a,h]anthracene LCS 0.498 100 ( 56-125 ) 0.5 ug/L 07/20/2010

Fluoranthene LCS 0.455 91 ( 63-125 ) 0.5 ug/L 07/20/2010

Fluorene LCS 0.461 92 ( 59-120 ) 0.5 ug/L 07/20/2010

Indeno[1,2,3-c,d] pyrene LCS 0.510 102 ( 59-125 ) 0.5 ug/L 07/20/2010

Naphthalene LCS 0.473 95 ( 56-108 ) 0.5 ug/L 07/20/2010

Phenanthrene LCS 0.427 86 ( 60-115 ) 0.5 ug/L 07/20/2010

Pyrene LCS 0.464 93 ( 62-130 ) 0.5 ug/L 07/20/2010

Surrogates 

Terphenyl-d14 <surr> LCS 92 ( 50-135 ) 07/20/2010

64 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974244 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

XXX23075

SW3520C

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5529

8270D SIMS

HP 6890/5973 MS SVQA

65 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974421 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

MXX23243

SW3010A

07/16/2010

QC results affect the following production samples:

1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 07/21/2010

Batch

Method

Instrument

MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

66 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974679 Lab Control Sample

974681 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

XXX23089

SW3520C

07/20/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.19 84 ( 75-125 ) 5 mg/L 07/21/2010

LCSD 4.28 86 2 (< 20 ) 5 mg/L 07/21/2010

Surrogates 

5a Androstane <surr> LCS 84 ( 60-120 ) 07/21/2010

LCSD 84 0 07/21/2010

Batch

Method

Instrument

XFC9360

SW8015C

HP 7890A FID SV E R

67 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

QC results affect the following production samples:

1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

68 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 29.1 97 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 28.9 96 1 (< 20 ) 30 ug/L 07/20/2010

1,1,1-Trichloroethane LCS 24.4 82 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 23.4 78 * 5 (< 20 ) 30 ug/L 07/20/2010

1,1,2,2-Tetrachloroethane LCS 29.1 97 ( 76-123 ) 30 ug/L 07/20/2010

LCSD 27.4 91 6 (< 20 ) 30 ug/L 07/20/2010

1,1,2-Trichloroethane LCS 29.4 98 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 28.8 96 2 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloroethane LCS 26.7 89 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 28.5 95 6 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloroethene LCS 26.9 90 ( 76-130 ) 30 ug/L 07/20/2010

LCSD 27.6 92 3 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloropropene LCS 31.4 105 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 30.5 102 3 (< 20 ) 30 ug/L 07/20/2010

1,2,3-Trichlorobenzene LCS 30.7 102 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 29.9 100 3 (< 20 ) 30 ug/L 07/20/2010

1,2,3-Trichloropropane LCS 30.5 102 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.2 97 4 (< 20 ) 30 ug/L 07/20/2010

1,2,4-Trichlorobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.7 99 6 (< 20 ) 30 ug/L 07/20/2010

1,2,4-Trimethylbenzene LCS 30.7 102 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 29.1 97 5 (< 20 ) 30 ug/L 07/20/2010

1,2-Dibromo-3-chloropropane LCS 28.9 96 ( 73-130 ) 30 ug/L 07/20/2010

LCSD 28.9 96 0 (< 20 ) 30 ug/L 07/20/2010

1,2-Dibromoethane LCS 31.3 104 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.2 101 4 (< 20 ) 30 ug/L 07/20/2010

1,2-Dichlorobenzene LCS 29.4 98 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 27.9 93 5 (< 20 ) 30 ug/L 07/20/2010

69 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichloroethane LCS 29.4 98 ( 80-129 ) 30 ug/L 07/20/2010

LCSD 28.8 96 2 (< 20 ) 30 ug/L 07/20/2010

1,2-Dichloropropane LCS 30.6 102 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 30.4 101 1 (< 20 ) 30 ug/L 07/20/2010

1,3,5-Trimethylbenzene LCS 30.7 102 ( 80-128 ) 30 ug/L 07/20/2010

LCSD 29.0 97 6 (< 20 ) 30 ug/L 07/20/2010

1,3-Dichlorobenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.3 101 6 (< 20 ) 30 ug/L 07/20/2010

1,3-Dichloropropane LCS 31.7 106 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 30.3 101 5 (< 20 ) 30 ug/L 07/20/2010

1,4-Dichlorobenzene LCS 32.7 109 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.4 105 4 (< 20 ) 30 ug/L 07/20/2010

2,2-Dichloropropane LCS 27.7 92 ( 80-132 ) 30 ug/L 07/20/2010

LCSD 29.0 97 5 (< 20 ) 30 ug/L 07/20/2010

2-Butanone (MEK) LCS 92.8 103 ( 66-136 ) 90 ug/L 07/20/2010

LCSD 90.2 100 3 (< 20 ) 90 ug/L 07/20/2010

2-Chlorotoluene LCS 33.2 111 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 31.2 104 6 (< 20 ) 30 ug/L 07/20/2010

2-Hexanone LCS 99.3 110 ( 68-130 ) 90 ug/L 07/20/2010

LCSD 95.3 106 4 (< 20 ) 90 ug/L 07/20/2010

4-Chlorotoluene LCS 33.4 111 ( 79-128 ) 30 ug/L 07/20/2010

LCSD 31.6 105 5 (< 20 ) 30 ug/L 07/20/2010

4-Isopropyltoluene LCS 31.4 105 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 29.7 99 6 (< 20 ) 30 ug/L 07/20/2010

4-Methyl-2-pentanone (MIBK) LCS 90.9 101 ( 69-134 ) 90 ug/L 07/20/2010

LCSD 85.2 95 6 (< 20 ) 90 ug/L 07/20/2010

Benzene LCS 31.7 106 ( 80-120 ) 30 ug/L 07/20/2010

70 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 31.1 104 2 (< 20 ) 30 ug/L 07/20/2010

Bromobenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 28.2 94 5 (< 20 ) 30 ug/L 07/20/2010

Bromochloromethane LCS 27.0 90 ( 77-129 ) 30 ug/L 07/20/2010

LCSD 28.9 97 7 (< 20 ) 30 ug/L 07/20/2010

Bromodichloromethane LCS 29.8 99 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.2 98 2 (< 20 ) 30 ug/L 07/20/2010

Bromoform LCS 28.1 94 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 28.0 93 0 (< 20 ) 30 ug/L 07/20/2010

Bromomethane LCS 28.9 96 ( 30-140 ) 30 ug/L 07/20/2010

LCSD 30.6 102 6 (< 20 ) 30 ug/L 07/20/2010

Carbon disulfide LCS 42.2 94 ( 72-123 ) 45 ug/L 07/20/2010

LCSD 43.6 97 3 (< 20 ) 45 ug/L 07/20/2010

Carbon tetrachloride LCS 27.0 90 ( 80-126 ) 30 ug/L 07/20/2010

LCSD 28.8 96 7 (< 20 ) 30 ug/L 07/20/2010

Chlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.2 101 1 (< 20 ) 30 ug/L 07/20/2010

Chloroethane LCS 29.4 98 ( 67-133 ) 30 ug/L 07/20/2010

LCSD 30.1 100 3 (< 20 ) 30 ug/L 07/20/2010

Chloroform LCS 26.4 88 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 27.9 93 5 (< 20 ) 30 ug/L 07/20/2010

Chloromethane LCS 25.6 86 ( 67-125 ) 30 ug/L 07/20/2010

LCSD 27.5 92 7 (< 20 ) 30 ug/L 07/20/2010

cis-1,2-Dichloroethene LCS 26.1 87 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 28.1 94 8 (< 20 ) 30 ug/L 07/20/2010

cis-1,3-Dichloropropene LCS 30.3 101 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.3 98 4 (< 20 ) 30 ug/L 07/20/2010

71 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Dibromochloromethane LCS 29.7 99 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.2 97 2 (< 20 ) 30 ug/L 07/20/2010

Dibromomethane LCS 28.5 95 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 27.3 91 4 (< 20 ) 30 ug/L 07/20/2010

Dichlorodifluoromethane LCS 26.8 89 ( 62-153 ) 30 ug/L 07/20/2010

LCSD 28.1 94 5 (< 20 ) 30 ug/L 07/20/2010

Ethylbenzene LCS 31.9 106 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.4 105 2 (< 20 ) 30 ug/L 07/20/2010

Hexachlorobutadiene LCS 30.5 102 ( 77-125 ) 30 ug/L 07/20/2010

LCSD 28.2 94 8 (< 20 ) 30 ug/L 07/20/2010

Isopropylbenzene (Cumene) LCS 30.1 100 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 29.8 100 1 (< 20 ) 30 ug/L 07/20/2010

Methylene chloride LCS 26.5 89 ( 63-131 ) 30 ug/L 07/20/2010

LCSD 27.6 92 4 (< 20 ) 30 ug/L 07/20/2010

Methyl-t-butyl ether LCS 40.6 90 ( 80-120 ) 45 ug/L 07/20/2010

LCSD 42.8 95 5 (< 20 ) 45 ug/L 07/20/2010

Naphthalene LCS 32.3 108 ( 75-120 ) 30 ug/L 07/20/2010

LCSD 30.5 102 6 (< 20 ) 30 ug/L 07/20/2010

n-Butylbenzene LCS 31.7 106 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 30.4 101 4 (< 20 ) 30 ug/L 07/20/2010

n-Propylbenzene LCS 34.2 114 ( 80-129 ) 30 ug/L 07/20/2010

LCSD 32.5 108 5 (< 20 ) 30 ug/L 07/20/2010

o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.7 102 1 (< 20 ) 30 ug/L 07/20/2010

P & M -Xylene LCS 59.6 99 ( 80-120 ) 60 ug/L 07/20/2010

LCSD 59.3 99 0 (< 20 ) 60 ug/L 07/20/2010

sec-Butylbenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.7 99 5 (< 20 ) 30 ug/L 07/20/2010

72 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 30.1 100 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.7 99 1 (< 20 ) 30 ug/L 07/20/2010

tert-Butylbenzene LCS 30.2 101 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 28.3 95 6 (< 20 ) 30 ug/L 07/20/2010

Tetrachloroethene LCS 29.6 99 ( 79-122 ) 30 ug/L 07/20/2010

LCSD 29.2 97 1 (< 20 ) 30 ug/L 07/20/2010

Toluene LCS 29.3 98 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 29.0 97 1 (< 20 ) 30 ug/L 07/20/2010

trans-1,2-Dichloroethene LCS 26.0 87 ( 79-132 ) 30 ug/L 07/20/2010

LCSD 26.9 90 4 (< 20 ) 30 ug/L 07/20/2010

trans-1,3-Dichloropropene LCS 30.3 101 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 30.0 100 1 (< 20 ) 30 ug/L 07/20/2010

Trichloroethene LCS 29.4 98 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 29.4 98 0 (< 20 ) 30 ug/L 07/20/2010

Trichlorofluoromethane LCS 25.3 84 ( 68-145 ) 30 ug/L 07/20/2010

LCSD 26.1 87 3 (< 20 ) 30 ug/L 07/20/2010

Vinyl chloride LCS 26.7 89 ( 72-145 ) 30 ug/L 07/20/2010

LCSD 28.2 94 5 (< 20 ) 30 ug/L 07/20/2010

Xylenes (total) LCS 90.5 101 ( 80-120 ) 90 ug/L 07/20/2010

LCSD 90.0 100 1 (< 20 ) 90 ug/L 07/20/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 07/20/2010

LCSD 98 0 07/20/2010

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 07/20/2010

LCSD 101 2 07/20/2010

Toluene-d8 <surr> LCS 101 ( 80-120 ) 07/20/2010

LCSD 104 3 07/20/2010

73 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

974726 Lab Control Sample

974727 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20956

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS11399

SW8260B

HP 5890 Series II MS3 VNA

74 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

QC results affect the following production samples:

1103478001, 1103478007, 1103478008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

75 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 29.9 100 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.2 97 2 (< 20 ) 30 ug/L 07/20/2010

1,1,1-Trichloroethane LCS 29.5 98 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 31.3 104 6 (< 20 ) 30 ug/L 07/20/2010

1,1,2,2-Tetrachloroethane LCS 29.7 99 ( 76-123 ) 30 ug/L 07/20/2010

LCSD 29.8 99 0 (< 20 ) 30 ug/L 07/20/2010

1,1,2-Trichloroethane LCS 30.3 101 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 30.5 102 0 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloroethane LCS 29.1 97 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.1 100 4 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloroethene LCS 27.5 92 ( 76-130 ) 30 ug/L 07/20/2010

LCSD 29.4 98 7 (< 20 ) 30 ug/L 07/20/2010

1,1-Dichloropropene LCS 30.8 103 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 32.5 108 5 (< 20 ) 30 ug/L 07/20/2010

1,2,3-Trichlorobenzene LCS 32.0 107 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 31.8 106 1 (< 20 ) 30 ug/L 07/20/2010

1,2,3-Trichloropropane LCS 31.1 104 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.6 102 2 (< 20 ) 30 ug/L 07/20/2010

1,2,4-Trichlorobenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.7 106 0 (< 20 ) 30 ug/L 07/20/2010

1,2,4-Trimethylbenzene LCS 32.0 107 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 32.3 108 1 (< 20 ) 30 ug/L 07/20/2010

1,2-Dibromo-3-chloropropane LCS 28.1 94 ( 73-130 ) 30 ug/L 07/20/2010

LCSD 28.7 96 2 (< 20 ) 30 ug/L 07/20/2010

1,2-Dibromoethane LCS 31.8 106 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.7 106 0 (< 20 ) 30 ug/L 07/20/2010

1,2-Dichlorobenzene LCS 29.2 98 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.5 98 1 (< 20 ) 30 ug/L 07/20/2010

76 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichloroethane LCS 29.2 97 ( 80-129 ) 30 ug/L 07/20/2010

LCSD 29.2 97 0 (< 20 ) 30 ug/L 07/20/2010

1,2-Dichloropropane LCS 30.8 103 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 32.2 107 5 (< 20 ) 30 ug/L 07/20/2010

1,3,5-Trimethylbenzene LCS 31.9 106 ( 80-128 ) 30 ug/L 07/20/2010

LCSD 32.1 107 1 (< 20 ) 30 ug/L 07/20/2010

1,3-Dichlorobenzene LCS 31.8 106 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 32.5 108 2 (< 20 ) 30 ug/L 07/20/2010

1,3-Dichloropropane LCS 32.5 108 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 32.2 107 1 (< 20 ) 30 ug/L 07/20/2010

1,4-Dichlorobenzene LCS 33.6 112 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 34.0 113 1 (< 20 ) 30 ug/L 07/20/2010

2,2-Dichloropropane LCS 30.8 103 ( 80-132 ) 30 ug/L 07/20/2010

LCSD 33.6 112 9 (< 20 ) 30 ug/L 07/20/2010

2-Butanone (MEK) LCS 96.4 107 ( 66-136 ) 90 ug/L 07/20/2010

LCSD 84.4 94 13 (< 20 ) 90 ug/L 07/20/2010

2-Chlorotoluene LCS 34.6 115 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 34.7 116 0 (< 20 ) 30 ug/L 07/20/2010

2-Hexanone LCS 94.8 105 ( 68-130 ) 90 ug/L 07/20/2010

LCSD 99.1 110 4 (< 20 ) 90 ug/L 07/20/2010

4-Chlorotoluene LCS 35.0 117 ( 79-128 ) 30 ug/L 07/20/2010

LCSD 35.5 118 1 (< 20 ) 30 ug/L 07/20/2010

4-Isopropyltoluene LCS 31.7 106 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 32.7 109 3 (< 20 ) 30 ug/L 07/20/2010

4-Methyl-2-pentanone (MIBK) LCS 83.6 93 ( 69-134 ) 90 ug/L 07/20/2010

LCSD 89.4 99 7 (< 20 ) 90 ug/L 07/20/2010

Benzene LCS 33.9 113 ( 80-120 ) 30 ug/L 07/20/2010

77 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 34.7 116 3 (< 20 ) 30 ug/L 07/20/2010

Bromobenzene LCS 30.0 100 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.2 101 1 (< 20 ) 30 ug/L 07/20/2010

Bromochloromethane LCS 31.0 103 ( 77-129 ) 30 ug/L 07/20/2010

LCSD 33.0 110 6 (< 20 ) 30 ug/L 07/20/2010

Bromodichloromethane LCS 28.7 96 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.2 97 1 (< 20 ) 30 ug/L 07/20/2010

Bromoform LCS 27.8 93 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 27.4 91 2 (< 20 ) 30 ug/L 07/20/2010

Bromomethane LCS 27.3 91 ( 30-140 ) 30 ug/L 07/20/2010

LCSD 30.4 101 11 (< 20 ) 30 ug/L 07/20/2010

Carbon disulfide LCS 43.0 96 ( 72-123 ) 45 ug/L 07/20/2010

LCSD 47.1 105 9 (< 20 ) 45 ug/L 07/20/2010

Carbon tetrachloride LCS 27.7 92 ( 80-126 ) 30 ug/L 07/20/2010

LCSD 29.0 97 5 (< 20 ) 30 ug/L 07/20/2010

Chlorobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.5 105 1 (< 20 ) 30 ug/L 07/20/2010

Chloroethane LCS 29.5 99 ( 67-133 ) 30 ug/L 07/20/2010

LCSD 30.5 102 3 (< 20 ) 30 ug/L 07/20/2010

Chloroform LCS 28.5 95 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 29.6 99 4 (< 20 ) 30 ug/L 07/20/2010

Chloromethane LCS 29.2 97 ( 67-125 ) 30 ug/L 07/20/2010

LCSD 32.8 109 12 (< 20 ) 30 ug/L 07/20/2010

cis-1,2-Dichloroethene LCS 29.1 97 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 31.6 105 8 (< 20 ) 30 ug/L 07/20/2010

cis-1,3-Dichloropropene LCS 29.8 99 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 30.8 103 3 (< 20 ) 30 ug/L 07/20/2010

78 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Dibromochloromethane LCS 28.5 95 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 28.8 96 1 (< 20 ) 30 ug/L 07/20/2010

Dibromomethane LCS 29.4 98 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 29.7 99 1 (< 20 ) 30 ug/L 07/20/2010

Dichlorodifluoromethane LCS 27.6 92 ( 62-153 ) 30 ug/L 07/20/2010

LCSD 31.0 103 12 (< 20 ) 30 ug/L 07/20/2010

Ethylbenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.4 105 0 (< 20 ) 30 ug/L 07/20/2010

Hexachlorobutadiene LCS 30.2 101 ( 77-125 ) 30 ug/L 07/20/2010

LCSD 29.6 99 2 (< 20 ) 30 ug/L 07/20/2010

Isopropylbenzene (Cumene) LCS 32.1 107 ( 80-121 ) 30 ug/L 07/20/2010

LCSD 32.6 109 1 (< 20 ) 30 ug/L 07/20/2010

Methylene chloride LCS 29.8 99 ( 63-131 ) 30 ug/L 07/20/2010

LCSD 32.2 107 8 (< 20 ) 30 ug/L 07/20/2010

Methyl-t-butyl ether LCS 40.7 91 ( 80-120 ) 45 ug/L 07/20/2010

LCSD 44.6 99 9 (< 20 ) 45 ug/L 07/20/2010

Naphthalene LCS 32.8 109 ( 75-120 ) 30 ug/L 07/20/2010

LCSD 33.0 110 1 (< 20 ) 30 ug/L 07/20/2010

n-Butylbenzene LCS 32.2 107 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 32.9 110 2 (< 20 ) 30 ug/L 07/20/2010

n-Propylbenzene LCS 35.3 118 ( 80-129 ) 30 ug/L 07/20/2010

LCSD 35.7 119 1 (< 20 ) 30 ug/L 07/20/2010

o-Xylene LCS 32.0 107 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 32.8 109 3 (< 20 ) 30 ug/L 07/20/2010

P & M -Xylene LCS 63.2 105 ( 80-120 ) 60 ug/L 07/20/2010

LCSD 63.9 107 1 (< 20 ) 60 ug/L 07/20/2010

sec-Butylbenzene LCS 31.9 106 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 32.7 109 2 (< 20 ) 30 ug/L 07/20/2010

79 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 31.7 106 ( 80-120 ) 30 ug/L 07/20/2010

LCSD 31.8 106 1 (< 20 ) 30 ug/L 07/20/2010

tert-Butylbenzene LCS 30.8 103 ( 80-122 ) 30 ug/L 07/20/2010

LCSD 31.4 105 2 (< 20 ) 30 ug/L 07/20/2010

Tetrachloroethene LCS 29.8 99 ( 79-122 ) 30 ug/L 07/20/2010

LCSD 30.1 100 1 (< 20 ) 30 ug/L 07/20/2010

Toluene LCS 33.2 111 ( 77-120 ) 30 ug/L 07/20/2010

LCSD 32.0 107 4 (< 20 ) 30 ug/L 07/20/2010

trans-1,2-Dichloroethene LCS 29.6 99 ( 79-132 ) 30 ug/L 07/20/2010

LCSD 31.9 106 8 (< 20 ) 30 ug/L 07/20/2010

trans-1,3-Dichloropropene LCS 30.9 103 ( 80-124 ) 30 ug/L 07/20/2010

LCSD 30.5 102 1 (< 20 ) 30 ug/L 07/20/2010

Trichloroethene LCS 28.4 95 ( 80-125 ) 30 ug/L 07/20/2010

LCSD 30.6 102 7 (< 20 ) 30 ug/L 07/20/2010

Trichlorofluoromethane LCS 27.5 92 ( 68-145 ) 30 ug/L 07/20/2010

LCSD 28.8 96 5 (< 20 ) 30 ug/L 07/20/2010

Vinyl chloride LCS 27.9 93 ( 72-145 ) 30 ug/L 07/20/2010

LCSD 32.7 109 16 (< 20 ) 30 ug/L 07/20/2010

Xylenes (total) LCS 95.2 106 ( 80-120 ) 90 ug/L 07/20/2010

LCSD 96.7 107 2 (< 20 ) 90 ug/L 07/20/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 99 ( 73-120 ) 07/20/2010

LCSD 97 2 07/20/2010

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 07/20/2010

LCSD 100 0 07/20/2010

Toluene-d8 <surr> LCS 107 ( 80-120 ) 07/20/2010

LCSD 102 5 07/20/2010

80 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975093 Lab Control Sample

975094 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20964

SW5030B

07/19/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS11403

SW8260B

HP 5890 Series II MS3 VNA

81 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

975360 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

MXX23263

SW3010A

07/21/2010

QC results affect the following production samples:

1103478001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1110 111 ( 80-120 ) 1000 ug/L 07/27/2010

Batch

Method

Instrument

MMS6555

SW6020

Perkin Elmer Sciex ICP-MS P3

82 of 103
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Prep

976051 Lab Control Sample

976052 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill

Water (Surface, Eff., Ground)

VXX20986

SW5030B

07/25/2010

QC results affect the following production samples:

1103478001, 1103478004, 1103478005, 1103478006, 1103478007, 1103478008, 1103478009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 206 103 ( 80-116 ) 200 ug/L 07/25/2010

LCSD 210 105 2 (< 20 ) 200 ug/L 07/25/2010

Surrogates 

4-Bromofluorobenzene <surr> LCS 104 ( 50-150 ) 07/25/2010

LCSD 106 2 07/25/2010

Batch

Method

Instrument

VFC10038

SW8015C

HP 5890 Series II PID+FID VCA

83 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

974422 Matrix Spike

974423 Matrix Spike Duplicate

1103478004

Water (Surface, Eff., Ground)

MXX23243

3010 H20 Digest for Metals ICP-MS

07/16/2010

QC results affect the following production samples:

1103478004, 1103478005, 1103478006, 1103478007, 1103478008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead MS (0.620) U 1040 104 ( 80-120 ) 1000 ug/L 07/21/2010

MSD 1020 102 1 (< 15 ) 1000 ug/L 07/21/2010

Batch

Method

Instrument

MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

84 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

MXX23263

3010 H20 Digest for Metals ICP-MS

07/21/2010

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS (0.620) U 959 96 ( 80-120 ) 1000 ug/L 07/27/2010

BMSD 1100 110 13 (< 15 ) 1000 ug/L 07/27/2010

Batch

Method

Instrument

MMS6555

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS (60.0) U 484 108 ( 80-116 ) 450 ug/L 07/25/2010

BMSD 469 104 3 (< 20 ) 450 ug/L 07/25/2010

Surrogates 

4-Bromofluorobenzene <surr> BMS 52.4 105 ( 50-150 ) 07/25/2010

BMSD 52.8 106 1 07/25/2010

Batch

Method

Instrument

VFC10038

SW8015C

HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS (0.320) U 4.42 82 ( 75-125 ) 5.41 mg/L 07/21/2010

BMSD 4.85 91 9 (< 30 ) 5.32 mg/L 07/21/2010

Surrogates 

5a Androstane <surr> BMS .0884 82 ( 50-150 ) 07/21/2010

BMSD 0.0926 87 5 07/21/2010

Batch

Method

Instrument

XFC9360

SW8015C

HP 7890A FID SV E R

Volatile Gas Chromatography/Mass Spectroscopy

85 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

VXX20964

Volatiles Extraction 8240/8260 FULL

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane BMS (0.300) U 30.3 101 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 29.2 97 4 (< 20 ) 30.0 ug/L 07/20/2010

1,1,1-Trichloroethane BMS (0.620) U 33.1 110 ( 80-122 ) 30.0 ug/L 07/20/2010

BMSD 33.1 110 0 (< 20 ) 30.0 ug/L 07/20/2010

1,1,2,2-Tetrachloroethane BMS (0.300) U 29.6 99 ( 76-123 ) 30.0 ug/L 07/20/2010

BMSD 28.7 96 3 (< 20 ) 30.0 ug/L 07/20/2010

1,1,2-Trichloroethane BMS (0.620) U 30.2 101 ( 77-120 ) 30.0 ug/L 07/20/2010

BMSD 29.4 98 3 (< 20 ) 30.0 ug/L 07/20/2010

1,1-Dichloroethane BMS (0.620) U 31.5 105 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 30.6 102 3 (< 20 ) 30.0 ug/L 07/20/2010

1,1-Dichloroethene BMS (0.620) U 31.4 105 ( 76-130 ) 30.0 ug/L 07/20/2010

BMSD 30.2 101 4 (< 20 ) 30.0 ug/L 07/20/2010

1,1-Dichloropropene BMS (0.620) U 35.1 117 ( 80-122 ) 30.0 ug/L 07/20/2010

BMSD 34.6 115 2 (< 20 ) 30.0 ug/L 07/20/2010

1,2,3-Trichlorobenzene BMS (0.620) U 31.1 104 ( 77-120 ) 30.0 ug/L 07/20/2010

BMSD 31.8 106 2 (< 20 ) 30.0 ug/L 07/20/2010

1,2,3-Trichloropropane BMS (0.620) U 29.4 98 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 28.7 96 3 (< 20 ) 30.0 ug/L 07/20/2010

1,2,4-Trichlorobenzene BMS (0.620) U 31.7 106 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.7 106 0 (< 20 ) 30.0 ug/L 07/20/2010

1,2,4-Trimethylbenzene BMS (0.620) U 32.2 107 ( 80-125 ) 30.0 ug/L 07/20/2010

BMSD 31.9 106 1 (< 20 ) 30.0 ug/L 07/20/2010

1,2-Dibromo-3-chloropropane BMS (1.24) U 30.3 101 ( 73-130 ) 30.0 ug/L 07/20/2010

BMSD 29.8 99 2 (< 20 ) 30.0 ug/L 07/20/2010

1,2-Dibromoethane BMS (0.620) U 32.1 107 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 30.2 101 6 (< 20 ) 30.0 ug/L 07/20/2010

1,2-Dichlorobenzene BMS (0.620) U 29.3 98 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 29.0 97 1 (< 20 ) 30.0 ug/L 07/20/2010

1,2-Dichloroethane BMS (0.300) U 30.6 102 ( 80-129 ) 30.0 ug/L 07/20/2010

BMSD 30.6 102 0 (< 20 ) 30.0 ug/L 07/20/2010

1,2-Dichloropropane BMS (0.620) U 33.3 111 ( 80-121 ) 30.0 ug/L 07/20/2010

BMSD 33.7 112 1 (< 20 ) 30.0 ug/L 07/20/2010

1,3,5-Trimethylbenzene BMS (0.620) U 32.7 109 ( 80-128 ) 30.0 ug/L 07/20/2010

BMSD 32.3 108 1 (< 20 ) 30.0 ug/L 07/20/2010

1,3-Dichlorobenzene BMS (0.620) U 32.6 109 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 32.2 107 1 (< 20 ) 30.0 ug/L 07/20/2010

1,3-Dichloropropane BMS (0.240) U 32.5 108 ( 80-121 ) 30.0 ug/L 07/20/2010

BMSD 31.5 105 3 (< 20 ) 30.0 ug/L 07/20/2010

1,4-Dichlorobenzene BMS (0.300) U 34.2 114 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 34.2 114 0 (< 20 ) 30.0 ug/L 07/20/2010

86 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

VXX20964

Volatiles Extraction 8240/8260 FULL

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2,2-Dichloropropane BMS (0.620) U 37 123 ( 80-132 ) 30.0 ug/L 07/20/2010

BMSD 37.3 124 1 (< 20 ) 30.0 ug/L 07/20/2010

2-Butanone (MEK) BMS (6.20) U 81.5 91 ( 66-136 ) 90.0 ug/L 07/20/2010

BMSD 86.8 97 6 (< 20 ) 90.0 ug/L 07/20/2010

2-Chlorotoluene BMS (0.620) U 34.7 116 ( 80-125 ) 30.0 ug/L 07/20/2010

BMSD 34.2 114 1 (< 20 ) 30.0 ug/L 07/20/2010

2-Hexanone BMS (6.20) U 97.7 109 ( 68-130 ) 90.0 ug/L 07/20/2010

BMSD 91.3 101 7 (< 20 ) 90.0 ug/L 07/20/2010

4-Chlorotoluene BMS (0.620) U 36 120 ( 79-128 ) 30.0 ug/L 07/20/2010

BMSD 36.1 120 0 (< 20 ) 30.0 ug/L 07/20/2010

4-Isopropyltoluene BMS (0.620) U 33.1 110 ( 80-125 ) 30.0 ug/L 07/20/2010

BMSD 33.0 110 0 (< 20 ) 30.0 ug/L 07/20/2010

4-Methyl-2-pentanone (MIBK) BMS (6.20) U 91.5 102 ( 69-134 ) 90.0 ug/L 07/20/2010

BMSD 88.7 99 3 (< 20 ) 90.0 ug/L 07/20/2010

Benzene BMS (0.240) U 36.1 120 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 36.9 123* 2 (< 20 ) 30.0 ug/L 07/20/2010

Bromobenzene BMS (0.620) U 30 100 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 30.1 100 0 (< 20 ) 30.0 ug/L 07/20/2010

Bromochloromethane BMS (0.620) U 33.5 112 ( 77-129 ) 30.0 ug/L 07/20/2010

BMSD 33.9 113 1 (< 20 ) 30.0 ug/L 07/20/2010

Bromodichloromethane BMS (0.300) U 30.2 101 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 07/20/2010

Bromoform BMS (0.620) U 28.2 94 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 26.9 90 5 (< 20 ) 30.0 ug/L 07/20/2010

Bromomethane BMS (1.88) U 34.5 115 ( 30-140 ) 30.0 ug/L 07/20/2010

BMSD 32.0 107 8 (< 20 ) 30.0 ug/L 07/20/2010

Carbon disulfide BMS (1.24) U 51.5 114 ( 72-123 ) 45.0 ug/L 07/20/2010

BMSD 49.2 109 5 (< 20 ) 45.0 ug/L 07/20/2010

Carbon tetrachloride BMS (0.620) U 31.1 104 ( 80-126 ) 30.0 ug/L 07/20/2010

BMSD 31.6 105 2 (< 20 ) 30.0 ug/L 07/20/2010

Chlorobenzene BMS (0.300) U 32.3 108 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.3 104 3 (< 20 ) 30.0 ug/L 07/20/2010

Chloroethane BMS (0.620) U 74.4 248* ( 67-133 ) 30.0 ug/L 07/20/2010

BMSD 66.7 222* 11 (< 20 ) 30.0 ug/L 07/20/2010

Chloroform BMS (0.600) U 31.3 104 ( 80-124 ) 30.0 ug/L 07/20/2010

BMSD 31.7 106 1 (< 20 ) 30.0 ug/L 07/20/2010

Chloromethane BMS (0.620) U 36.2 121 ( 67-125 ) 30.0 ug/L 07/20/2010

BMSD 35.8 119 1 (< 20 ) 30.0 ug/L 07/20/2010

cis-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 80-125 ) 30.0 ug/L 07/20/2010

BMSD 34.6 115 3 (< 20 ) 30.0 ug/L 07/20/2010

87 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

VXX20964

Volatiles Extraction 8240/8260 FULL

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,3-Dichloropropene BMS (0.300) U 31.3 104 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.7 106 1 (< 20 ) 30.0 ug/L 07/20/2010

Dibromochloromethane BMS (0.300) U 29.2 97 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 07/20/2010

Dibromomethane BMS (0.620) U 30.4 101 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.1 104 2 (< 20 ) 30.0 ug/L 07/20/2010

Dichlorodifluoromethane BMS (0.620) U 34.2 114 ( 62-153 ) 30.0 ug/L 07/20/2010

BMSD 34.7 116 1 (< 20 ) 30.0 ug/L 07/20/2010

Ethylbenzene BMS (0.620) U 32.5 108 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.5 105 3 (< 20 ) 30.0 ug/L 07/20/2010

Hexachlorobutadiene BMS (0.620) U 30.6 102 ( 77-125 ) 30.0 ug/L 07/20/2010

BMSD 32.8 109 7 (< 20 ) 30.0 ug/L 07/20/2010

Isopropylbenzene (Cumene) BMS (0.620) U 33.6 112 ( 80-121 ) 30.0 ug/L 07/20/2010

BMSD 32.6 109 3 (< 20 ) 30.0 ug/L 07/20/2010

Methylene chloride BMS (2.00) U 33 110 ( 63-131 ) 30.0 ug/L 07/20/2010

BMSD 31.2 104 6 (< 20 ) 30.0 ug/L 07/20/2010

Methyl-t-butyl ether BMS (3.00) U 46.4 103 ( 80-120 ) 45.0 ug/L 07/20/2010

BMSD 43.4 97 7 (< 20 ) 45.0 ug/L 07/20/2010

Naphthalene BMS (1.24) U 33.1 110 ( 75-120 ) 30.0 ug/L 07/20/2010

BMSD 32.9 110 1 (< 20 ) 30.0 ug/L 07/20/2010

n-Butylbenzene BMS (0.620) U 34.1 114 ( 80-124 ) 30.0 ug/L 07/20/2010

BMSD 34.2 114 0 (< 20 ) 30.0 ug/L 07/20/2010

n-Propylbenzene BMS (0.620) U 36.2 121 ( 80-129 ) 30.0 ug/L 07/20/2010

BMSD 36.2 121 0 (< 20 ) 30.0 ug/L 07/20/2010

o-Xylene BMS (0.620) U 33.1 110 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 32.2 107 3 (< 20 ) 30.0 ug/L 07/20/2010

P & M -Xylene BMS (1.24) U 66.1 110 ( 80-120 ) 60.0 ug/L 07/20/2010

BMSD 63.7 106 4 (< 20 ) 60.0 ug/L 07/20/2010

sec-Butylbenzene BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 32.9 110 0 (< 20 ) 30.0 ug/L 07/20/2010

Styrene BMS (0.620) U 32.3 108 ( 80-120 ) 30.0 ug/L 07/20/2010

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 07/20/2010

tert-Butylbenzene BMS (0.620) U 31.5 105 ( 80-122 ) 30.0 ug/L 07/20/2010

BMSD 31.4 105 0 (< 20 ) 30.0 ug/L 07/20/2010

Tetrachloroethene BMS (0.620) U 31.4 105 ( 79-122 ) 30.0 ug/L 07/20/2010

BMSD 30.9 103 2 (< 20 ) 30.0 ug/L 07/20/2010

Toluene BMS (0.620) U 33 110 ( 77-120 ) 30.0 ug/L 07/20/2010

BMSD 31.6 105 4 (< 20 ) 30.0 ug/L 07/20/2010

trans-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 79-132 ) 30.0 ug/L 07/20/2010

BMSD 31.9 106 5 (< 20 ) 30.0 ug/L 07/20/2010

88 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

VXX20964

Volatiles Extraction 8240/8260 FULL

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

trans-1,3-Dichloropropene BMS (0.620) U 30.6 102 ( 80-124 ) 30.0 ug/L 07/20/2010

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 07/20/2010

Trichloroethene BMS (0.620) U 32.5 108 ( 80-125 ) 30.0 ug/L 07/20/2010

BMSD 30.8 103 5 (< 20 ) 30.0 ug/L 07/20/2010

Trichlorofluoromethane BMS (0.620) U 29.5 98 ( 68-145 ) 30.0 ug/L 07/20/2010

BMSD 27.7 92 7 (< 20 ) 30.0 ug/L 07/20/2010

Vinyl chloride BMS (0.620) U 35.9 120 ( 72-145 ) 30.0 ug/L 07/20/2010

BMSD 35.0 117 3 (< 20 ) 30.0 ug/L 07/20/2010

Xylenes (total) BMS (1.88) U 99.3 110 ( 80-120 ) 90.0 ug/L 07/20/2010

BMSD 95.9 107 3 (< 20 ) 90.0 ug/L 07/20/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 29.9 100 ( 73-120 ) 07/20/2010

BMSD 29.9 100 0 07/20/2010

4-Bromofluorobenzene <surr> BMS 29.5 98 ( 76-120 ) 07/20/2010

BMSD 29.6 99 1 07/20/2010

Toluene-d8 <surr> BMS 31.3 104 ( 80-120 ) 07/20/2010

BMSD 30.7 102 2 07/20/2010

Batch

Method

Instrument

VMS11403

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS

89 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

XXX23075

3520 Liquid/Liquid Ext for 8270 SIM

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

1-Methylnaphthalene BMS (0.0320) U .281 52* ( 58-114 ) 0.543 ug/L 07/19/2010

BMSD 0.439 83 44 * (< 30 ) 0.529 ug/L 07/19/2010

2-Methylnaphthalene BMS (0.0320) U .256 47* ( 54-105 ) 0.543 ug/L 07/19/2010

BMSD 0.397 75 43 * (< 30 ) 0.529 ug/L 07/19/2010

Acenaphthene BMS (0.0320) U .315 58 ( 57-110 ) 0.543 ug/L 07/19/2010

BMSD 0.412 78 27 (< 30 ) 0.529 ug/L 07/19/2010

Acenaphthylene BMS (0.0320) U .319 59 ( 58-105 ) 0.543 ug/L 07/19/2010

BMSD 0.432 82 30 * (< 30 ) 0.529 ug/L 07/19/2010

Anthracene BMS (0.0320) U .396 73 ( 63-120 ) 0.543 ug/L 07/19/2010

BMSD 0.468 89 17 (< 30 ) 0.529 ug/L 07/19/2010

Benzo(a)Anthracene BMS (0.0320) U .42 77 ( 61-120 ) 0.543 ug/L 07/19/2010

BMSD 0.490 93 15 (< 30 ) 0.529 ug/L 07/19/2010

Benzo[a]pyrene BMS (0.0320) U .364 67 ( 57-120 ) 0.543 ug/L 07/19/2010

BMSD 0.424 80 15 (< 30 ) 0.529 ug/L 07/19/2010

Benzo[b]Fluoranthene BMS (0.0320) U .408 75 ( 66-130 ) 0.543 ug/L 07/19/2010

BMSD 0.459 87 12 (< 30 ) 0.529 ug/L 07/19/2010

Benzo[g,h,i]perylene BMS (0.0320) U .403 74 ( 60-125 ) 0.543 ug/L 07/19/2010

BMSD 0.475 90 16 (< 30 ) 0.529 ug/L 07/19/2010

Benzo[k]fluoranthene BMS (0.0320) U .4 74 ( 67-125 ) 0.543 ug/L 07/19/2010

BMSD 0.482 91 19 (< 30 ) 0.529 ug/L 07/19/2010

Chrysene BMS (0.0320) U .427 79 ( 71-120 ) 0.543 ug/L 07/19/2010

BMSD 0.499 94 16 (< 30 ) 0.529 ug/L 07/19/2010

Dibenzo[a,h]anthracene BMS (0.0320) U .394 73 ( 56-125 ) 0.543 ug/L 07/19/2010

BMSD 0.459 87 15 (< 30 ) 0.529 ug/L 07/19/2010

Fluoranthene BMS (0.0320) U .437 81 ( 63-125 ) 0.543 ug/L 07/19/2010

BMSD 0.505 95 14 (< 30 ) 0.529 ug/L 07/19/2010

Fluorene BMS (0.0320) U .371 68 ( 59-120 ) 0.543 ug/L 07/19/2010

BMSD 0.482 91 26 (< 30 ) 0.529 ug/L 07/19/2010

Indeno[1,2,3-c,d] pyrene BMS (0.0320) U .401 74 ( 59-125 ) 0.543 ug/L 07/19/2010

BMSD 0.477 90 17 (< 30 ) 0.529 ug/L 07/19/2010

Naphthalene BMS (0.0664) U .27 50* ( 56-108 ) 0.543 ug/L 07/19/2010

BMSD 0.480 91 56 * (< 30 ) 0.529 ug/L 07/19/2010

Phenanthrene BMS (0.0320) U .395 73 ( 60-115 ) 0.543 ug/L 07/19/2010

BMSD 0.460 87 15 (< 30 ) 0.529 ug/L 07/19/2010

Pyrene BMS (0.0320) U .435 80 ( 62-130 ) 0.543 ug/L 07/19/2010

BMSD 0.493 93 13 (< 30 ) 0.529 ug/L 07/19/2010

Surrogates 

Terphenyl-d14 <surr> BMS .411 76 ( 50-135 ) 07/19/2010

BMSD 0.476 90 15 07/19/2010

90 of 103
Matrix

SGS Ref.# Printed Date/Time 08/17/2010 10:37

Batch

Method

Date

Original

Prep

1103478002 Billable Matrix Spike

1103478003 Billable Matrix Spike Dup.

1103478001

Water (Surface, Eff., Ground)

XXX23075

3520 Liquid/Liquid Ext for 8270 SIM

07/19/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5528

8270D SIMS

HP 6890/5973 MS SVQA

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