# Instructions The EPA secondary aluminum production test program requires emissions and other test data for several pollutants. EPA understands that you own one or more secondary aluminum production facilities. For at least one thermal chip dryer and at least one scrap dryer/delacquering kiln/decoating kiln that you own, you must perform a stack test for volatile and semi-volatile organic HAPs as specified in the letter and instructions accompanying this file. You should collect emissions samples for the identified pollutants downstream of the last relevant emissions control device (i.e., stack or other point representing the composition of the flue gases at the exit to the atmosphere), unless otherwise indicated. (Contact the EPA project lead for situations with multiple stacks or other complex emissions points for the unit.) Sample and analyze the particulate matter collected in the hopper from at least one bag house used to control particulate matter from each type of affected source subject to 40 CFR 63, subpart RRR at your secondary aluminum production facilities. Choose bag houses that are used to control particulate matter from each of the six different types of affected sources (i.e.group 1 furnaces, scrap shredders, chip dryers, scrap dryers/delacquering kilns/decoating kilns, dross only furnaces, and rotary dross coolers) if you have these controlled affected sources at your facilities. Where more than one bag house discharges solids to a common hopper, a single sample will be adequate. In cases where solids from different compartments of a single bag house are collected in multiple hoppers or multiple collection sacks, a single composite sample will be adequate. If you have a total of three or fewer bag houses at all of your facilities, sample and analyze particulate matter from all of them, even if they are controlling the same type of affected source. It is not necessary to conduct a stack test for multi-metals analysis.
Sample and analyze the lime used for injection to any of the lime-injected bag houses from which particulate matter samples were collected. If lime of the same type, obtained from the same supplier, is used for more than one lime injected bag house, a single sample will be adequate to represent the lime used in these bag houses.
You must report the results of these tests and chemical analyses in this Microsoft® Excel Emission Test Template. The Excel templates are specific to each type of pollutant. You must report the results of each test on the appropriately labeled worksheet corresponding to the specific tests and analyses conducted at your facilities. If more than one source was tested, you must make a copy of the worksheet and update the source ID in order to distinguish between each separate test of a chip dryer or scrap dryer/ delacquering kiln/decoating kiln at each facility and each different source of particulate matter. After completing the worksheet, you must also submit an electronic copy of the emission test report and the chemical analyses. (PDF format preferred). Please refer to the cover letter of this packet (CAA section 114 letter) for additional testing information. Please note that you do not have to submit a test plan to EPA for approval prior to testing; however, we recommend that you prepare a test plan for your own use to assist in the planning and to verify that you address all of the testing and reporting requirements. You must follow all of the procedures as specified in the test methods, including the quality assurance and quality control measures, and document the results in any test report provided to EPA.**Facility Name and Address Unit Description**  **Process Unit ID Control Device ID** 

Aluminum Recovery Technologies, Inc Chip Dryer Dryer #1 Baghouse #3 2170 Production Rd Kendallville IN 46970

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing 8/5/2010 8/6/2010 8/6/2010 Feed/Charge Rate 3.196 3.205 3.196Mg/hr Afterburner Operating Temperature 1300 1305 1305degree F
Type of Charge:_______________________________________________________________________ Aluminum Chips

**Compound Volatile Organic HAP**  **Emission Rate Sample 1**

**(kg/hr) Volatile Organic HAP**  **Emission Rate Sample 1 (kg/Mg of feed/charge)** **Volatile Organic HAP Emission Rate Sample**  **2 (kg/hr) Volatile Organic HAP** 

**Emission Rate Sample 2 (kg/Mg of**  **feed/charge) Volatile Organic HAP** 

**Emission Rate Sample 3**

**(kg/hr) Volatile Organic HAP** 

**Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method**  **Used Detection Limit** 

**Information (BDL,DLL,ADL)** **Other Supporting Information**  Acrylonitrile 107-13-1 0.00012 0.00004 0.00018 0.00006 0.0001594 0.0000499 M0031 

### DLL Benzene 71-43-2 0.00019 0.00006 0.00031 0.00010 0.0002517 0.0000788 M0031 

### DLL Bromodichloromethane 75-27-4 [<0.0000049] [<0.0000015] [<0.0000065] [<0.0000020] [<0.0000058] [<0.0000018]M0031 

### BDL Carbon disulfide 75-15-0 0.000013 0.000004 0.000016 0.000005 0.000012 0.0000038 M0031 

### DLL Carbon tetrachloride 56-23-5 0.000035 0.000011 0.000036 0.000011 0.000032 0.0000099 M0031 

### DLL Chlorodibromomethane 124-48-1 [<0.0000075] [<0.0000024] [<0.000010] [<0.0000031] [<0.0000089] [<0.0000028]M0031 

### BDL Chloroform 67-66-3 0.000036 0.000011 0.000025 0.000008 0.0000306 0.0000096 M0031 

### DDL Chloroprene 126-99-8 [<0.000038] [<0.000012] [<0.000063] [<0.000020] [<0.000044] [<0.000014] M0031 

### BDL Dibromomethane 74-95-3 [<0.0000079] [<0.0000025] [<0.000011] [<0.0000033] [<0.0000093] 0.0000029 M0031 

### BDL 1,1-Dichloroethane 75-34-3 [<0.0000038] [<0.0000012] [<0.0000050] [<0.0000016] [<0.0000044] [<0.0000014]M0031 

### BDL 1,2-Dichloroethane 107-06-2 0.0000065 0.0000020 0.0000089 0.0000028 0.0000078 0.0000024 M0031 

### DLL 1,1-Dichloroethene 75-35-4 [<0.0000056] [<0.0000018] [<0.00045] [<0.00014] [<0.0000067] [<0.0000021]M0031 

### BDL trans-1,2-Dichloroethene 156-60-5 [<0.0000045] [<0.0000014] [<0.0000098] [<0.0000031] 0.0000067 0.0000021 M0031 

### BDL 1,2-Dichloropropane 78-87-5 [<0.0000064] [<0.0000020] [<0.0000085] [<0.0000027] [<0.0000076] [<0.0000024]M0031 

### BDL 1,3-Dichloropropene 542-75-6 0.0000067 0.0000021 [<0.0000085] [<0.0000027] [<0.0000076] [<0.0000024]M0031 

### DLL Methylene chloride 75-09-2 0.000078 0.000024 0.00038 0.00012 0.00065 0.00020 M0031 

### ADL Tetrachloroethene 127-18-4 0.0000078 0.0000024 0.000011 0.0000035 0.000010 0.0000033 M0031 

### DLL Toluene 108-88-3 0.00018 0.000055 0.00020 0.000061 0.00016 0.000051 M0031 

### ADL 1,1,1-Trichloroethane 71-55-6 [<0.0000041] [<0.0000013] [<0.0000050] [<0.0000016] [<0.0000044] [<0.0000014]M0031 

### BDL 1,1,2-Trichloroethane 79-00-5 [<0.000038] [<0.000012] [<0.000050] [<0.0000016] [<0.000044] [<0.000014] M0031 

### BDL Trichloroethene 79-01-6 [<0.0000083] [<0.0000026] [<0.000011] [<0.0000034] [<0.0000098] [<0.0000031]M0031 

### BDL Trichlorofluoromethane 75-69-4 0.000071 0.000022 0.000075 0.000023 0.000074 0.000023 M0031 

### ADL **Speciated Volatile Organic HAP Emission Data Facility Name and Address**  **Unit Description Process Unit ID**  **Control Device ID** Aluminum Recovery Technologies, IncChip Dryer Dryer #1 Baghouse #3 2170 Production Rd Kendallville IN 46970

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing 8/5/2010 8/6/2010 8/6/2010 Feed/Charge Rate 3.196 3.205 3.196Mg/hr Afterburner Operating Temperature 1300 1305 1305degree F
Type of Charge:_______________________________________________________________________ Aluminum Chips

**Compound Semi-volatile Organic HAP**  **Emission Rate Sample 1**

**(kg/hr) Semi-volatile Organic HAP** 

**Emission Rate Sample 1 (kg/Mg of feed/charge)** **Semi-volatile Organic HAP Emission Rate**  **Sample 2 (kg/hr) Semi-volatile Organic HAP**  **Emission Rate Sample 2 (kg/Mg of feed/charge)** **Semi-volatile Organic HAP Emission Rate**  **Sample 3 (kg/hr) Semi-volatile Organic**  **HAP Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method Used** **Detection Limit Information**  **(BDL,DLL,ADL) Other Supporting**  **Information** Acenaphthene 83-32-9 0.00000356 0.00000111 0.00000031 0.00000010 0.0000020 0.0000006 M0010 ADL Acenaphthylene 208-96-8 0.00000617 0.00000193 0.00000012 0.00000004 0.0000066 0.0000021 M0010 ADL Anthracene 120-12-7 0.00000057 0.00000018 0.00000031 0.00000010 0.0000002 0.0000001 M0010 DLL Benz[a]anthracene 56-55-3 0.00000019 0.00000006 0.00000004 0.00000001 0.0000001 0.0000000 M0010 DLL Benzo[a]pyrene 50-32-8 0.00000016 0.00000005 [<0.00000003] [<0.00000001] 0.0000001 0.0000000 M0010 DLL Benzo[b]fluoranthene 205-99-2 0.00000237 0.00000074 0.00000012 0.00000004 0.0000013 0.0000004 M0010 DLL Benzo[g,h,i]perylene 191-24-2 0.00000025 0.00000008 [<0.00000008] [<0.00000002] 0.0000002 0.0000001 M0010 DLL Benzo[k]fluoranthene 207-08-9 0.00000140 0.00000044 0.00000004 0.00000001 0.0000013 0.0000004 M0010 DLL Chrysene 218-01-9 0.00000111 0.00000035 0.00000019 0.00000006 0.0000010 0.0000003 M0010 ADL Dibenz[a,h]anthracene 53-70-3 [<0.00000016] [<0.00000005] [<0.00000004] [<0.00000001] 0.0000001 0.0000000 M0010 DLL Fluoranthene 206-44-0 0.00001451 0.00000454 0.00000059 0.00000018 0.0000071 0.0000022 M0010 ADL Fluorene 86-73-7 0.00005065 0.00001585 0.00000062 0.00000019 0.0000109 0.0000034 M0010 ADL Indeno(1,2,3-cd)pyrene 193-39-5 0.00000019 0.00000006 0.00000004 0.00000001 0.0000001 0.0000000 M0010 DLL Naphthalene 91-20-3 0.00007046 0.00002205 0.00000675 0.00000211 0.0000557 0.0000174 M0010 ADL Phenanthrene 85-01-8 0.00004836 0.00001513 0.00000166 0.00000052 0.0000198 0.0000062 M0010 ADL Pyrene 129-00-0 0.00000528 0.00000165 0.00000084 0.00000026 0.0000025 0.0000008 M0010 DLL **Speciated Volatile Organic HAP Emission Data**

# Facility Name and A**ddress**

AluminumRecovery

Technologies, Inc 2170 Production Rd Kendallville IN 46970

**Parameter Sample 1**  **Date of Testing** 8/5/2010 Feed/Charge Rate 3.19616 Afterburner residence time 1.1 Afterburner Operating Temperature 1300



# 1 8/5/2010 2 8/6/2010 3 8/6/2010

**Run Number THC Emission Rate (kg/hr)**  

# 1 9.36E-02 

# 2 0 

# 3 0 *** See Appendix A to Enclosure 1

**Run Number Test Start Date** 

# Unit ID **Unit Type (Chip dryer or scrap**
**dryer /delacq /decoating kiln)** Dryer #1 Chip Dryer

**Sample 2 Sample 3**  **Unit of Measure** 8/6/2010 8/6/2010

3.20524 3.19616Mg/hr 1.1 1.1sec 1305 1305degree F



# 17:00 8/5/2010 19:32 8:35 8/6/2010 11:22 12:02 8/6/2010 14:38
**THC Emission Rate (kg/Mg of feed/charge)**  **Data Flag (A DL, BDL, DDL)** *****Detection Limit (ng/dscm)**  2.93E-02 ADL 4.25E+04 0 BDL 4.25E+04 0 BDL 4.25E+04 **Test End Time Test Start Time**  **Test End Date**

# Other Supporting

**Information**

### Facility Name and A**ddress Unit Description**  **Process Unit ID Control Device ID** 

Aluminum Recovery Technologies, Inc Chip Dryer Dryer #1 Baghouse #3 2170 Production Rd Kendallville IN 46970

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing 8/6/2010 8/6/2010 8/6/2010 Feed/Charge Rate 3.19616 3.20524 3.19616Mg/hr Afterburner Operating Temperature 105.8 94.7 104.6degree F Flow Rate 45,745.87 45,454.84 45,780.40

## actual M3

## /min Flow Rate 36,765.89 36,812.88 36,725.79

## dry sM3

## /min

**Emission Test Results Constituent**  **Composition Sample 1**  **(%) Composition** 

**Sample 2 (%)**  **Composition**

**Sample 3 (%)**  **Test Method Used**

**(ex. U.S. EPA**

**Method 3B) Other Supporting Information**  O2 

## 18 21 21US EPA Method 3A CO2 

## 2 0 0US EPA Method 3A H2

### O 1.1 0.92 0.74US EPA Method 3A

## Facility

**Name and A ddress**  **Unit Description Process Unit ID**  **Control Device ID*** Aluminum Recovery Technologies, Inc Chip Dryer Dryer #1 Baghouse #3 2170 Production Rd Kendallville IN 46970 

# Sample ID No._HOH120406-002____________________ **Ty pe of Sample (Lime or Particulate):_____________________________**  Composite Particulate and Lime Dust


# Date Sampled **Date(s) Analyzed** 8/6/2010 08/23-08/25/10



# HAP Metal **mg/kg** Antimony 11.2 Beryllium [<2.5] Chromium 226.0 Hexavalent chromium [<23.2] Lead 689.0 Mercury [<0.17] Selenium [<3.7] Arsenic [<4.4] Cadmium 6.4 Cobalt [<10.1] Manganese 1590.0 Nickel 312.0
*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**