# Evaluatio n o fMetals , Particulat e Matte r

a n d PCDD/PCD FEmission s fo rFixe d Heart h Incinerato rUni t3 Jun e 200 6 RECEIVE D
S E P 2 2Z00 6 AI R ENFORCEMEN TBRANC H I U.S
. EPA
. REGIO N 5



### ENS R Corporatio n Septembe r200 6 Documen tNo. : 10002-01 7

### Prepare d for :

Veoli aE S Technica l Solution s Sauget , Illinoi s



# Evaluatio n o fMetals , Particulat e Matte r a n d PCDD/PCD FEmission s fo rFixe d Heart h Incinerato rUni t3 Jun e 200 6

Prepare d By : Jeffre yT
. Gorman , ProjectManage r

Revtewe d By : Crai g R
. Doolittle , rE , Manager , Ai rMeasurement s

ENS R Corporatio n Septembe r200 6 Documen tNo. : 10002-01 7

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# Contents 1. 0 Introductio n 1- 1 1. 1 Progra m Summar y1- 1 2. 0 Incinerato rProces s Descriptio n 2- 1 2. 1 Proces s Overvie w2- 1 2. 2 Wast e Fee d System s [4 0 CF R §63.1207(f)(1)(iii)(D)(E ) an d (f)(1)(ii)(C) ] 2- 1 2. 3 Manufacturer , Mak e an d Mode l o fth e Incinerato r[4 0 CF R §63.1207(f)(1)(iii)(A) ] 2- 1 2. 4 Ai rPollutio n Contro l Equipmen t[4 0 CF R §63.1207(f)(1)(iii)(G) ] 2- 2 2.4. 1 Lim e Syste m 2- 2 2.4. 2 Spra yDr yAbsorbe r2- 3 2.4. 3 Fabri cFilte r2- 3 2.4. 4 Induce d Draf tFa n an d Stac k - 2- 3 3. 0 Summar yo fResult s 3- 1 3. 1 Introductio n 3- 1 3. 2 Stac k

Emissio n Result s fo rPCDDs/PCDF s 3- 1 3. 3 Stac k

Emissio n Result s fo rTarge tMetal s an d Particulat e Matte r3- 1 3. 4 Metal s Sampl e Contaminatio n 3- 2 4. 0 Samplin g an d Analytica l Procedure s 4- 1 4. 1 Samplin g Procedure s 4- 1 4.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s 4- 1 4.1. 2 PCDD/PCD FSamplin g 4- 1 4.1. 3 Metal s an d Particulat e Samplin g 4- 1 4. 2 Analytica l Procedure s 4- 1 4.2. 1 PCDD/PCD FAnalyse s .... „ 4- 1 4.2. 2 Metal s Analyse s 4- 2 4. 3 Proces s Operatin g Condition s 4- 2 5. 0 Qualit yAssurance.
. •• ••5- 1 5. 1 Introductio n 5- 1 5.1. 1 Pre-Samplin g Activitie s 5- 1 5.1. 2 Equipmen tCalibratio n 5- 1 5.1. 3 Glasswar e Preparatio n 5- 2

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# Listo fAppendice s Appendi xAFacilit yOperatin g Dat a Appendi xB Referenc e Metho d Fiel d Dat aan d Calculation s Appendi xC Referenc e Metho d Calibrations , Verifications , an d Certification s Appendi xD Stac k

Configuration , Samplin g Por tan d Travers e Poin tLocation s Appendi xE Laborator yDat a 

# Listo fTable s Tabl e 3- 1 PCD D /

PCD FEmissio n Result s - TE Q Basi s 3- 3 Tabl e 3- 2 Emissio n Result s fo rLV M Metal s - Ma y200 6 , 3- 4 Tabl e 3- 3 Emissio n Result s fo rLV M Metal s - Jun e 200 6 3- 5 Tabl e 3- 4 Emissio n Result s fo rSV M Metal s an d Mercur y3- 6 Tabl e 3- 5 Summar yo fTarge tMetal s 3- 7 Tabl e 3- 6 Emissio n Result s fo rParticulat e Matte r- Ma y200 6 3- 8 Tabl e 3- 7 Emissio n Result s fo rParticulat e Matte r- Jun e 200 6 3- 9

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# 1.0 Introductio n
1. 1 Progra m Summar y ENS R wa s retaine d b yVeoli aE S Technica l Solution s (Veolia) , formerl yOny xEnvironmenta l Service s t o conduc tstac k ga s emissio n samplin g durin g th e week s ofMa y8 , 200 6 an d Jun e 19 , 2006
. Th e samplin g wa s performe d o n th e Fixe d Heart h Hazardou s Wast e Incinerato rUni t3 a tthei r facilit yi n Sauget , Illinois
. Th e purpos e ofthi s Performanc e Tes twa s t o evaluat e th e performanc e o f th e incinerato rrelativ e t o th e emission s standard s fo rexistin g incinerator s foun d i n 4 0 CF R Par t63 , Subpar tEE E (th e HW C MAC Tregulations)
. T o thi s end , th e specifi cobjective s o fthi s Performanc e Tes twer e t o demonstrat e emission s o fth e followin g pollutants :

•Mercur y •Lo wVolatil e Metal s (arsenic , beryllium , an d chromium )
•Semi-volatil e Metal s (lea d an d cadmium )
•Dioxin s an d Furan s •Particulat e Matte r Th e Performanc e Tes tinclude d feedin g certai n type s o fwaste s an d material s int o th e incinerator , samplin g an d analyzin g thes e feedstreams , monitorin g certai n proces s parameter s whil e concurrentl yconductin g emission s testing
. Th e result s fro m thi s testin g indicat e tha temission s fo rth e abov e pollutant s me tth e emissio n standard s fo rth e HW C MAC Tregulations
. Asummar yofth e tes tresult s ca n b e foun d i n Sectio n 3 o fthi s report .

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# 2.0 Incinerato rProces s Descriptio n
2. 1 Proces s Overvie w Veoli aoperate s 2 Fixe d Heart h Dua l Chambere d Incinerator s (Unit s 2 an d 3 ) an d on e rotar ykil n (Uni t4 ) a tth e Sauget , I Lfacility
. Th e tw o fixe d heart h unit s ar e rate d a t1 6 millio n Btu/h reach
. Incineratio n Uni tNo
. 3 i s amirro rimag e o fUni tNo
. 2
. Bot h ofthes e unit s hav e thei row n wast e handlin g system s a s describe d i n th e section s tha tfollow
. Th e onl ydifferenc e bein g Uni tNo
. 2 i s equippe d wit h fou r(4 ) baghous e modules , whil e Uni tNo
. 3 i s equippe d wit h thre e (3 ) baghous e modules
. Uni t4 i s rate d a t5 0 millio n Btu/h ran d i s equippe d wit h it s ow n tan k far m system , dru m storage , bul k

solid s storag e an d fee d systems . 2. 2
. Wast e Fee d System s [4 0 CF R §63.1207(f)(1)(iii)(D)(E ) an d (f)(1)(ii)(C) ] Fixe d heart h incinerato rno . 3 i s designe d t o receiv e containers , aqueou s liqui d wastes , organi c liqui d waste s fe d throug h air-atomizin g nozzles , specialt yliqui d feed s an d direc tinjec tliquid s fe d throug h th e aqueou s o rorgani cliqui d fee d systems . Thi s uni tca n receiv e an ycombinatio n o f waste s - - liquid , semi-solid , o rsoli d - wit h ahea tvalu e o fu p t o 1 6 millio n Btu/hr
. Eac h o fth e fixe d heart h incinerator s ar e supporte d b ystorage/blen d tank s locate d i n Tan k Far m #1
. Rate s o ffee d ar e controlle d a teac h incinerator
. Segregate d liqui d waste s ar e store d unti l utilize d i n th e wast e blendin g facilities
. A ttha ttime , liquid s ar e delivere d t o th e blendin g tank s wher e th e dail y liqui d fee d t o th e incinerato ri s formulated , tested , an d release d t o th e incinerator
. Blendin g o f store d liqui d waste s t o achiev e optimu m heatin g valu e an d viscosit yfo rincineratio n take s plac e i n Tank s 2 , 4 , 6 &8
. Si xadditiona l tank s (10,20 , 30,40 , 5 0 &60 ) ar e use d t o segregat e differen t wast e strea m type s fo rblendin g o fliqui d fee d t o th e incinerator
. Severa l criteri aar e importan ti n designin g ablen d fro m availabl e waste s tha thav e bee n segregate d principall yb yphysica l an d chemica l properties
. Thes e includ e compatibility , prope rrang e o fheatin g value , an d permi t restriction s regardin g elementa l compositio n (base d o n emissio n limitations)
. I n complianc e wit h th e Benzen e NESHAP , al l tank s ar e vente d t o individua l carbo n adsorptio n canister s fo rremova l o forganic s befor e vapo ri s discharge d t o th e atmosphere
. Eac h carbo n adsorbe rcaniste ri s essentiall yequivalen tt o a5 5 gallo n containe ro rgreater , i fnecessary . Al l tank s ar e equippe d wit h conservatio n vents , i n additio n t o th e carbo n caniste radsorber
. Al l tank s ar e grounded , an d flam e arrestor s ar e installe d betwee n th e carbo n adsorber s an d th e tanks
. 2. 3 Manufacturer , Mak e an d Mode l o fth e Incinerato r[4 0 CF R §63.1207(f)( 1 )(iii)(A) ] Incinerato runi tno . 3 feature s atwo-stag e combustio n process . Ignitio n o fwast e materia l take s plac e i n th e primar y(lower ) combustio n chamber
. Asecondar y(upper ) combustio n chambe rserve s a s a n "after-burner " fo rproces s gases . Ignitio n o fth e wast e take s plac e a ttemperature s i n exces s o f1,60 0 degree s F
. Th e secondar ycombustio n chambe rmaintain s aminimu m temperatur e o f 1,80 0 degree s F
. Thes e temperature s ar e presente d i n curren toperatin g conditions
. Th e Serie s 2 incinerato rha s atota l o ftw o burners , on e burner , aNort h America n burner , rate d a t 12. 0 millio n Btu/hr. , i s use d i n th e lowe rchambe rt o maintai n temperatures . I twil l bu m onl ynatura l ga s o rNo
. 2 fue l oil
. Asecon d burne ri s mounte d i n th e uppe rchamber ; i tto o wil l b e use d t o suppl y additiona l hea tan d wil l b e fuele d with natura l ga s o r# 2 fue l oil
. Thi s burne ri s aNort h America n

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Burner , rate d a t6. 0 millio n Btu/hr
. Liqui d o rgaseou s waste s ar e injecte d throug h separat e fee d nozzle s a s describe d i n sectio n 2.2 , above
. Th e primar yan d secondar ychamber s hav e a n externa l diamete ro f9 feet , an d ar e 17. 5 fee tlong
. Th e interio rwall s o fbot h chamber s ar e line d wit h approximatel y1 0 inche s o fbric k refractoryan d insulatio n backing , makin g th e interna l operatin g diamete rapproximatel y7'2"
. Th e cross-sectiona l are ao fth e chamber s i s thu s 40. 3 squar e feet
. Combustio n ai ri s controlle d separatel yi n th e uppe r an d lowe rchambers
. Followin g ignitio n o fth e wast e materia l unde rcontrolle d o rstarved-ai rcondition s i n th e lowe r chamber , off-gase s trave l throug h arefractory-line d flu e ga s passag e int o th e uppe rchamber , whic h act s a s a n afterburner
. Turbulenc e i s achieve d b yth e tangentia l introductio n ofai ran d additiona l fue l i n th e uppe rchamber
. Ga s temperature s ar e normall ymaintaine d a t1,800-2,20 0 degree s F i n th e uppe rchambe ran d 1500-190 0 degree s F i n th e lowe rchamber , pursuan tt o curren tIllinoi s EP A permi toperatin g conditions
. Leavin g th e uppe rchamber , th e ho tga s strea m travel s throug h 2 8 fee to frefractory-line d stac k section s befor e reachin g th e star to fth e ga s scrubbin g system . Th e combine d volum e o fth e uppe r an d lowe rchambers , th e flu e ga s passag e an d th e ho tcrossove rsectio n i s approximatel y1,56 7 cubi cfeet
. Th e tota l retentio n tim e ofcombustio n gase s withi n th e syste m i s approximatel y5 seconds
. Th e incinerato ri s rate d a t1 6 millio n Btu/hr. , wit h adesig n uni thea treleas e o f approximatel y10,00 0 Bt u pe rcubi cfoot
. Maximu m ga s volum e whe n firin g ahea treleas e o f1 6 millio n Btu/hr
. i s abou t15,00 0 acf m a t40 0 degree s F
. 2. 4 Ai rPollutio n Contro l Equipmen t[4 0 CF R §63.1207(f)( 1 )(iii)(G) ] Th e ai rpollutio n contro l syste m consist s o faspra ydrye rabsorbe ran d fabri cfilte rbaghouse
. Th e ai rpollutio n contro l syste m neutralize s acidi ccompound s an d remove s particulat e fro m th e exhaus t gas . Tw o subsystems , th e spra ydrye rabsorbe ran d th e fabri cfilter , carr you tth e chemica l neutralizatio n an d particulat e remova l functions , respectively
. Athir d subsystem , th e lim e system , i s use d t o prepar e an d provid e lim e slurr yt o th e spra ydrye rabsorbe rfo rus e i n th e chemica l neutralizatio n process . Th e induce d draf tfa n an d stac k provid e th e mechanica l energ yrequire d t o transpor tth e flu e ga s throug h th e interconnectin g ductwork , t o it s eventua l discharg e poin tt o atmosphere
. 2.4. 1 Lim e Syste m Th e lim e syste m prepare s lim e slurr yfo rus e i n th e chemica l neutralizatio n proces s i n sufficien t suppl yan d concentratio n t o maintai n continuou s flu e ga s treatmen ti n th e spra ydrye rabsorber
. Th e syste m ha s bee n designe d fo rbatc h mixin g t o provid e thi s service
. Hydrate d lim e i s store d i n astorag e bi n abov e th e lim e preparatio n area . Th e storag e bi n i s size d t o hol d enoug h hydrate d lim e t o maintai n severa l day s o fsyste m operatio n a tth e maximu m combustio n rat e ofth e incinerator
. Lim e i s discharge d throug h th e conica l storag e bi n bottom
. Th e flo wo fth e materia l fro m th e bi n i s aide d b yavibratin g "liv e bottom, " o rbi n activator
. Avariabl e spee d rotar yfeede ri s use d t o mete rth e hydrate d lim e i n th e proportion s require d fo rbatc h mixin g lim e slurry
. Th e lim e i s mixe d wit h wate ri n atan k beneat h th e lim e storag e bin
. Th e rotaryfeede r spee d an d th e rat e tha twate ri s adde d t o th e lim e slurr ytan k ar e variabl e s o tha tth e desire d 20 % lim e solid s concentratio n ca n b e achieve d i n th e tank
. Th e variabl e fee d adjustment s allo wwate r an d lim e t o b e adde d t o th e lim e slurr ytan k a tarat e tha twil l allo wabatc h mod e ofmixing
. A n agitato ri s provide d i n th e slurr ytan k t o mi xth e wate ran d lim e an d t o maintai n th e suspensio n o f

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lim e solids
. Th e mixe d lim e slurr yi s pumpe d a tacontinuou s rat e offlo wthroug h arecirculatio n loo p t o th e atomizer
. 2.4. 2 Spra yDr yAbsorbe r Slurr yflo wt o th e spra ydrye rabsorbe ri s metere d b yaflo wcontro l valv e t o obtai n th e prope rfee d concentratio n t o th e spra ydrye rabsorbe ratomizer
. Automati c(o rmanual ) adjustmen tt o th e flo wi s mad e a s afunctio n o fth e outpu tfro m ahydrochlori caci d (HCI ) analyze ri n th e ga s duc tdownstrea m o fth e Fabri cfilter
. Th e amoun to fslurr ymetere d i s proportiona l t o th e amoun to fHC I monitored
. Th e slurr ypasse s throug h astationar yswirl-typ e liqui d distributo rint o th e atomize rwhee l wher e induce d centrifuga l forc e fro m th e rapidl yspinnin g whee l discharge s th e slurr ythroug h th e whee l nozzle s a thig h velocity
. Th e desig n o fth e atomize rwheel , it s rat e o fspin , an d th e discharg e velocit yo fth e slurry , creat e aclou d o ffinel ydivide d droplet s aroun d th e peripher yo fth e atomize r wheel
. Afeedbac k

signa l fro m th e atomize rpowe rtransmitte rprovide s verificatio n tha twate rflo wt o th e atomize rincrease s o rdecrease s i n proportio n t o th e spra ydrye rabsorbe routle ttemperature . Flu e ga s enter s fro m th e botto m o fth e spra ydrye rabsorbe rthroug h avertical , centrall ylocate d disperser
. Th e disperse rdirect s th e flu e ga s throug h th e zon e fille d b yth e atomize d slurr yclou d wher e th e flu e ga s an d slurr ymix , an d mos tofth e absorptio n occurs . Th e spra ydrye rabsorbe rfeature s atwo-poin tproduc tdischarge
. Aportio n o fth e drie d spen t chemical s an d as h settl e t o th e botto m o fth e chamber
. Thi s materia l i s discharge d a tth e bas e o f th e powde rdischarg e cone . I tthe n passe s throug h alum p breake rwhic h reduce s larg e agglomeration s o fmateria l t o amanageabl e size
. Finally , i ti s discharge d throug h arotar yvalv e t o th e conveyin g system . Th e remainde ro fth e spen tchemical s i s carrie d fro m th e modul e entraine d i n th e flu e gas . 2.4. 3 Fabri cFilte r Ga s exhauste d fro m th e spra ydrye rabsorbe ri s distribute d b ymanifol d duct s t o thre e fabri cfilte r module s a tUni t3
. Withi n eac h filte rmodule , th e ga s i s passe d throug h Teflon-coate d fiberglas s clot h bags
. Th e ga s passe s fro m th e outsid e t o th e insid e o fth e filte rbags
. Particulate , entraine d i n th e ga s stream , i s mechanicall ydeposite d o n th e outsid e o fth e filte rbag s a s th e ga s passe s throug h th e cloth
. Th e fabri cfilte rcleanin g mechanis m utilize s jet s o fai rt o clea n th e filte rbags
. Periodically , th e cleanin g sequenc e wil l b e initiated
. Th e sequenc e i s eithe rstarte d a tth e en d ofatime d cycle , o r whe n th e differentia l pressur e acros s th e filte rreache s apredetermine d setpoin to fapproximatel y 7.0 " w.c . Th e controlle rthe n sequence s t o eac h ro wo ffilte rbag s i n eac h module , releasin g aburs t o fai ropposit e t o th e directio n o fga s flow
. Th e quickl yrelease d burs to fai rdislodge s dus tcak e o n th e exterio ro feac h ba g a s i ttravel s fro m th e to p t o th e botto m o fth e bags
. Release d fro m th e bag , th e dus tcak e fall s b ygravit yint o th e hoppe ra tth e botto m o fth e module
. Th e dus tcleane d fro m th e filte rbag s i s remove d a tth e bas e o fth e hoppe rthroug h arotar yvalv e fo r discharg e t o th e conveyin g system . Treate d b yth e spra ydrye rabsorbe ran d filtere d b yth e fabri c filter , th e cleane d flu e ga s exit s th e fabri cfilte rmodule s t o a n outle tmanifol d fo rexhaust
. 2.4. 4 Induce d Draf tFa n an d Stac k Th e induce d draf tfa n an d stac k ar e locate d downstrea m o fth e fabri cfilter
. Combustio n gase s ar e draw n throug h th e syste m b ya7 5 h p induce d draf t(ID ) fan , rate d a t15,00 0 acf m a t400 ° F saturated , an d 22 " wate rcolum n pressure . Th e induce d draf tfa n provide s th e mechanis m fo r
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transportin g th e incinerato rflu e ga s throug h th e spra ydrye rabsorber , Fabri cfilter , an d al l interconnectin g ducts
. Th e velocit yo fth e ga s withi n th e ductin g an d treatmen tdevice s i s regulate d b yth e dampe rassociate d wit h th e fan
. Treate d gasse s exhauste d fro m th e induce d draf tfa n t o th e atmospher e throug h a90-ft
. hig h stack
. Th e stac k diamete rfo rUni t3 i s 3 9 inche s I.D
. Th e stac k i s equippe d wit h instrumen tsamplin g port s an d asamplin g platfor m fo remission s testing
. Appendi xD provide s detail s o n th e desig n an d sampl e portlocation s an d configuration s fo rUni t3
.

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# 3.0 Summar yo fResult s ENS R

3. 1 Introductio n Thi s sectio n summarize s th e tes tprogra m results
. Appendi xB present s copie s ofENSR' s fiel d dat a an d calculations
. Emissio n dat ai s summarize d i n thi s sectio n an d fee d an d proces s operatin g dat a ar e include d i n Appendi xA
. 3. 2 Stac k

Emissio n Result s fo rPCDDs/PCDF s Metho d 0023 Arequire d separat e analysi s o fth e front-hal fan d back-hal fsampl e trai n fractions
. Progra m sample s wer e submitte d t o Alt aAnalytica l Laboratorie s i n E l Dorad o Hills , C Afo ral l analysi s o fal l targe tparameters . Asummar yo fth e PCDD/PCD Femissio n result s o n aTE Q basi s fo rUni t3 ar e include d i n Tabl e 3-1
.
•Th e PCDD/PCD Femission s fo rUni t3 (averag e emission s fo rrun s 1 , 2 an d 3 wer e 0.02 4 ng/m 3

### @ 7 % 0 2 

### ) ar e belo wth e HW C MAC Temissio n standar d of0. 2 ng/m 3

### @ 7 % 0 2 

### . 3. 3 Stac k

Emissio n Result s fo rTarge tMetal s an d Particulat e Matte r Asummar yo fth e metal s an d particulat e matte remission s fo rUni t3 i s include d i n Table s 3- 2 throug h 3-7
. Table s 3- 2 an d 3- 3 provid e adetaile d summar yo fth e Lo wVolatil e Metal s (LVM ) emission s fro m th e Ma y200 6 an d Jun e 200 6 testing
. Adetaile d summar yo fmetal s emission s categorize d b ySemi-volatil e Metal s (SVM ) an d mercur yi s provide d i n Tabl e 3-4
. Tabl e 3- 5 provide s asummar yo fal l si xtarge tmetals
. Table s 3- 6 an d 3- 7 summariz e th e particulat e matte remission s fro m th e Ma y200 6 an d Jun e 200 6 testing
.

. Th e LV M metal s emission s fo rUni t3 fro m th e Ma y200 6 testin g (averag e emission s fo rrun s 1 , 2 an d 3 wer e 24 9 pg/m 3

### @ 7 % 0 2 

### fo rLVMs ) wer e highe rtha n th e HW C MAC Temissio n standard s o f9 7 pg/m 3 

### ;

. Th e LV M metal s emission s fo rUni t3 fro m th e Jun e 200 6 testin g (averag e emission s fo rrun s 1 , 2 an d 3 wer e 7.6 1 pg/m 3

### @ 7 % 0 2 

### fo rLVMs ) wer e lowe rtha n th e HW C MAC Temissio n standard s o f9 7 pg/m 3 

### ;
•Th e SV M an d mercur yemission s fo rUni t3 (averag e fo rrun s 1 , 2 an d 3 wer e 16. 6 pg/m 3

### @ 7 % 0 2 

### f o rSVM s an d 61. 5 pg/m 3

### @ 7 % 0 2 

### fo rmercury ) wer e belo wth e HW C MAC Temissio n standard s o fan d 24 0 pg/m 3

### (correcte d t o 7 % 0 2 

### ) an d 13 0 pg/m 3

### @ 7 % 0 2

### fo rSVM s an d mercur yrespectively ;

. Th e particulat e matte remission s fo rUni t3 fro m th e Ma y200 6 testin g (averag e emission s fo r run s 1 , 2 an d 3 wer e 6.3 9 mg/m 3

### @ 7 % 0 2 

### ) i s belo wth e HW C MAC Temissio n standar d o f3 4 mg/m 3

### @ 7 % 0 2 

### ;

. Th e particulat e matte remission s fo rUni t3 fro m th e Jun e 200 6 testin g (averag e emission s fo r run s 1 , 2 an d 3 wer e 2.6 6 mg/m 3

### @ 7 % 0 2 

### ) i s belo wth e HW C MAC Temissio n standar d o f3 4 mg/m 3

### @ 7 % 0 2 

### .

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### ENS R

3. 4 Metal s Sampl e Contaminatio n Durin g th e Ma y200 6 testing , hig h arseni clevels , whic h wer e inconsisten tamon g th e thre e runs , wer e detecte d i n sampl e result s fro m th e Metho d 2 9 train
. Adetaile d revie wwa s conducte d b ybot h ENS R an d Veoli apersonne l t o asses s possibl e cause s and/o rsource s ofcros s contamination
. Thi s revie wincluded :

•Sampl e trai n clean-u p an d preparatio n procedure s •Sampl e portacces s an d preparatio n fo rsamplin g •Samplin g anomalie s (i.e. , observation s o ffilter , sampl e trai n an d procedures ) •La b contaminatio n o rincorrec tresult s (duplicat e sample s wer e analyze d a taseparat e laboratory ) •Operatin g o requipmen tissue s tha tcoul d hav e cause d non-representativ e particulat e matte r containin g hig h arseni ct o b e collecte d i n th e sampl e trai n I twa s conclude d tha tther e wa s cross-contaminatio n o fth e sampl e trai n durin g samplin g tha twa s mos tlikel ycause d b ydislodgemen tan d re-entrainmen ti n th e flu e ga s o fscal e tha tha d buil tu p o n th e insid e o fth e stac k sampl e portove rtime , causin g anon-representativ e result
. Also , durin g thi s revie wi twa s determine d tha tth e numbe ro ftravers e point s fo rth e port s use d fo rth e dioxi n an d fura n samplin g wa s incorrec tbase d o n Metho d 1 criteria , althoug h result s wer e wel l withi n th e MAC Temissio n standards
. A s aresult , Uni t3 wa s re-teste d i n Jun e t o furthe revaluat e lo wvolatil e meta l an d dioxi n an d fura n emission s performance
. Port s wer e cleane d prio rt o testin g an d th e correc tnumbe ro ftravers e point s wa s use d fo rth e selecte d samplin g locations
. Dioxi n an d fura n result s wer e agai n wel l withi n th e emissio n standard
. Lo wvolatil e meta l result s wer e als o wel l withi n th e emissio n standard
.

C:\Document s an d SetBngs\jwoodward\Loca l Settings\Temporar

yInterne tFiles\OLK7C\Onyx200 6 Tes t Reportdo c 

### 3- 2 Septembe r200 6

### ENS R

Tabl e 3- 1 PCD D /

PCD FEmissio n Result s - TE Q Basi s Ru n No
. 

### Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 Star tTim e 

### 14:4 0 09:3 0 09:3 0 Sto p Tim e 

### 17:5 9 13:0 5 11:4 3 Unit s Sampl e Volum e dsc f 128.36 3 129.71 0 126.37 9 Sampl e Volum e m 3 

### 3.6 3 3.6 7 3.5 8 Moistur e Conten t % v/v 44. 4 47. 7 45. 6 0 2

### Concentratio n % v/ v(dry ) 

### 10.0 0 8.2 0 9.6 0 C 0 2

### Concentratio n % v/ v(dry ) 

### 7.4 0 7.6 0 7.4 0 Isokinetic s 

## % 9 9 10 4 10 0 Stac k Flowrat e dscf m 5,44 1 5,21 2 5,28 0 PCDD/PCD F p g ng/m 3 

### p g ng/m 3 

### p g ng/m 3 

### Parameter s TEF a 

### T E Q T E Q T E Q 2,3,7,8-TCD D 1.0 0 - 

### 0.0 0 O.OE+0 0 3.4 4 9.4E-0 4 0.0 0 0.0E+0 0 1,2,3,7,8-PeCD D 0.5 0 17. 0 2.3E-0 3 17. 6 2.4E-0 3 16. 7 2.3E-0 3 1,2,3,4,7,8-HxCD D 0.1 0 19. 1 5.3E-0 4 16. 8 4.6E-0 4 14. 6 4. 1 E-0 4 1,2,3,6,7,8-HxCD D 0.1 0 46. 1 1.3E-0 3 34. 7 9.4E-0 4 35. 7 1 .OE-0 3 1 2,3,7,8,9-HxCD D 0.1 0 37. 0 1 .OE-0 3 27. 1 7.4E-0 4 26. 3 7.3E-0 4 1,2,3,4,6,7,8-HpCD D 0.0 1 19 0 1 

### 5.2E-0 4 17 5 4.8E-0 4 156. 0 4.4E-0 4 OCD D 0.00 1 24 7 " 6.8E-0 5 17 5 4.8E-0 5 15 1 4.2E-0 5 2,3,7,8-TCD F 0.1 0 3 0 8. 1 E-0 4 32. 8 8.9E-0 4 31. 8 8.9E-0 4 1,2,3,7,8-PeCD F 0.0 5 3 6 1 

### 4.9E-0 4 4 1 5.6E-0 4 4 1 5.7E-0 4 2,3,4,7,8-PeCD F 0.5 0 6 5 9.0E-0 3 7 0 9.6E-0 3 7 6 1. 1 E-0 2 1,2,3,4,7,8-HxCD F 0.1 0 3 6 1 9.9E-0 4 3 3 9.0E-0 4 3 8 1. 1 E-0 3 1,2,3,6,7,8-HxCD F 0.1 0 32~ 1 8.8E-0 4 3 2 8.6E-0 4 -3 4 9.4E-0 4 2,3,4,6,7,8-HxCD F 0.1 0 4 4 1.2E-0 3 4 2 1 . 1 

### E-0 3 4 5 1.3E-0 3 1,2,3,7,8,9-HxCD F 0.1 0 1 0 2.8E-0 4 1 2 3.2E-0 4 1 1 3 . 1 

### E-0 4 1,2,3,4,6,7,8-HpCD F 0.0 1 7 8 2. 1 E-0 4 6 7 1.8E-0 4 7 1 2.0E-0 4 1,2,3,4,7,8,9-HpCD F 0.0 1 8 2.2E-0 5 5 1.4E-0 5 7 2.0E-0 5 OCD F 0.00 1 2 0 5.6E-0 6 1 5 4.0E-0 6 1 3 3.7E-0 6 Tota l TEQ s (ng/m 3 

### ) — 

### 0.02 0 0.02 0 0.02 1 Tota l TEQ s (ng/m 3

### @ 7% 0 2 

### ) 

## = 0.02 5 0.02 2 0.02 6 % o fStandar d b 

## = 12 % 1 1 % 13 %

a

### U.S.EP A(1989) Toxi cEquivalenc yFacto r b

### PCDD/PCD FStandard = 0.20 ng/dsc m @ 7 % Q 2

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### ENS R

Tabl e 3- 2 Emissio n Result s fo rLV M Metal s - Ma y200 6
Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e lO-May-0 6 10-May-06 11-May-06 

### Star tTim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samplin g Parameters « Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d dcf 81.24 8 83.54 6 76.76 1 80.51 8 Sampl e Volum e dsc f 79.59 8 84.05 6 76.26 9 79.97 4 Moistur e % v/ v 43. 0 43. 6 44. 6 43. 7 0 2

### atStac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 Avg
. Stac k

Temp
. ° F 38 1 37 1 37 1 37 5 Stac k Flowrat e dscf m 5,57 6 5,69 1 5,08 8 5,45 1 Isokinetic s % 10 9 10 1 10 2 10 4 Arseni c(As ) ~ LV M Quantit yCollecte d M 9 8.5 0 24 8 94 5 40 1 Stac k Cone
. @ 7 % O z 

### pg/m 3 

### 6.1 4 12 6 55 7 23 0 Stac k Emissio n Rat e Ib/h r 7.88E-0 5 2.22E-0 3 8.34E-0 3 3.55E-0 3

g/se c 9.92E-0 6 2.80E-0 4 1.05E-0 3 4.47E-0 4 Berylliu m (Be ) - - LV M QuantityCollecte d M 9 0.1 0 0.1 0 0.1 0 0.1 0 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 0.0 7 0.0 5 0.0 6 0.0 6 Stac k Emissio n Rat e Ib/h r 9.27E-0 7 8.96E-0 7 8.82E-0 7 9.02E-0 7

g/se c 1.17E-0 7 1.13E-0 7 1.11E-0 7 0.0 0 Tota l Chromiu m (Cr ) - - LV M Quantit yCollecte d 16. 7 28. 0 54. 8 33. 2 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 12. 1 14. 2 32. 3 19. 5 Stac k Emissio n Rat e Ib/h r 1.55E-0 4 2.5 1 E-0 4 4.83E-0 4 2.96E-0 4

g/se c 1.95E-0 5 3.16E-0 5 6.09E-0 5 0.0 0

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yInterne tFiles\OLK7C\Onyx200 6 Test Report.do c 

### 3- 4 Septembe r2 00 6

### ENS R

Tabl e 3- 3 Emissio n Result s fo rLV M MefaS s - Jun e 200 6 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### Star tTim e Unit s 15:1 2 10:0 6 10.0 6 Sto p Tim e 17:2 9 12:2 9 12:4 4 AVG S Samplin g Parameters - - Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Volum e Metere d dc f 78.24 4 82.90 2 81.74 5 80.96 4 Sampl e Volum e dsc f 72.24 7 76.48 2 75.57 3 74.76 8 Moistur e % v/v 46. 7 47. 8 45. 5 46. 7 0 2

### a tStac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 Avg
. Stac k

Temp
. ° F 38 6 38 8 38 6 38 7 Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic s 

## % 10 4 10 6 10 1 10 4 Arseni c (As

) — LV M Quantit yCollecte d u g 5.5 3 3.6 9 5.2 0 4.8 1 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 3.4 4 1.8 6 2.9 8 2.7 6 Stac k Emissio n Rat e Ib/h r 4.79E-0 5 3.14E-0 5 4.65E-0 5 4.19E-0 5 g/se c 6.03E-0 6 3.95E-0 6 0.0 0 0.0 0 Berylliu m (Be

) — LV M Quantit yCollecte d p g 0.0 0 0.087 0 0.0 0 0.029 0 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 0.0 0 0.043 9 0.0 0 0.014 6 Stac k Emissio n Rat e Ib/h r O.OOE+0 0 7.39E-0 7 0.0OE+0 0 2.46E-0 7 g/se c 0.00E+0 0 9.32E-0 8 0.00E+0 0 3.11E-0 8 Tota l Chromiu m (Cr ) « LV M Quantit yCollecte d p g 9.9 1 3.8 5 11. 2 8.3 0 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 6.1 7 1.9 4 6.4 0 4.8 4 Stac k Emissio n Rat e Ib/h r 8.58E-0 5 3.27E-0 5 9.98E-0 5 7.28E-0 5 g/se c 1.08E-0 5 4.12E-0 6 1.26E-0 5 9.17E-0 6

C:\Documents an d Settings\jwoodward\Loca l SettingsYTemporar

yInternetFiles\OLK7C\Onyx200 6 Test Reportdo c 

### 3- 5 Septembe r200 6

### ENS R Tabl e 3- 4 Emissio n Result s fo rSV M Metal s an d Mercur y Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-06 10-May-06 11-May-06 

### Star tTim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samplin g Parameters - Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d dc f 81.24 8 83.54 6 76.76 1 80.51 8 Sampl e Volum e dsc f 79.59 8 84.05 6 76.26 9 79.97 4 Moistur e % v/v 43. 0 43. 6 44. 6 43. 7 0 2

### a tStac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 Avg
. Stac k

Temp
. ° F 38 1 37 1 37 1 37 5 Stac k Flowrat e dscf m 5,57 6 5,69 1 5,08 8 5,45 1 Isokinetic s 

## % 10 9 10 1 10 2 10 4 Cadmiu m (Cd ) - S V M Quantit yCollecte d u g 0.3 4 1.0 4 2.4 2 1.2 7 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 0.2 5 0.5 3 1.4 3 0.7 3 Stac k Emissio n Rat e Ib/h r 3.15E-0 6 9.3 1 E-0 6 2.14E-0 5 1.13E-0 5 g/se c 3.97E-0 7 1.17E-0 6 2.69E-0 6 0.0 0 Lea d (Pb) - - S V M Quantit yCollecte d p g 21. 2 19. 6 37. 9 26. 2 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 15. 3 9. 9 22. 3 15. 9 Stac k Emissio n Rat e Ib/h r 1.96E-0 4 1.76E-0 4 3.34E-0 4 2.35E-0 4 g/se c 2.47E-0 5 2.2 1 E-0 5 4.2 1 E-0 5 2.97E-0 5 Mercur y(He ) - V M Quantit yCollecte d p g 97. 3 12 1 89. 4 10 3 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 70. 3 61. 5 52. 7 61. 5 Stac k Emissio n Rat e Ib/h r 9.0 1 E-0 4 1.09E-0 3 7.88E-0 4 9.25E-0 4 cj/se c 1.14E-0 4 1.37E-0 4 9.93E-0 5 1.17E-0 4

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yInterne tFiles\OLK7C\Onyx2006 Test ReDOrt.doc 

### 3- 6 Septembe r200 6

### ENS R

Tabl e 3- 5 Summar yo fTarge tMetal s

L o wVolatil e Metal s Emission s - micrograms/m 3 

### Ma y200 6 Tes t Metal s Ru n 1 Ru n 2 Ru n 3 Averag e A s 6.1 4 12 6 55 7 23 0 B e 0.0 7 0.0 5 0.0 6 0.0 6 C r 12.0 5 14. 2 32. 3 19. 5 Tota l LV M 18. 3 14 0 58 9 24 9 Jun e 200 6 Tes t Metal s Ru n 1 Ru n 2 Ru n 3 Averag e A s 3. 4 1. 9 2.9 8 2. 8 B e 0.0 0 0.0 4 0.0 0 0.0 1 C r 6.1 7 1.94 6.4 0 4.8 4 Tota l LV M 9.6 1 3.8 5 9.3 8 7.6 1

LV M RegulatoryStandar d = 9 7 micrograms/ m 3 

### Semi-Volatil e M eta l Em i ssion s - micrograms/m 3 

### Metal s Run l Ru n 2 Ru n 3 Averag e P b 15. 3 9. 9 22. 3 15. 9 C d 0.2 5 0.5 3 1.4 3 0.7 3 Tota l SV M 15. 6 10. 5 23. 8 16. 6

SV M RegulatoryStandar d = 24 0 micrograms/m 3 

### Mercur yEmission s - micrograms/m 3 

### Metal s Ru n 1 Ru n 2 Ru n 3 Averag e H g 70. 3 61. 5 52. 7 61. 5 MercuryRegulatoryStandar d = 13 0 micrograms/m 3

C:\Documents an d SetSngs\jwoodward\Loca l SettingsYTemporar

yInterne tFiles\OLK7CYOny

x200 6 Tes t Reportdo c 

### 3- 7 Septembe r200 6

### ENS R

Tabl e 3- 6 Emissio n Result s fo rParticulat e Matte r- Ma y200 6 Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-06 10-May-06 11-May-06 

### Star tTim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samolin q Parameter s ~ Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d dc f 81.99 1 84.12 8 81.69 9 82.60 6 Volum e ofGa s Collecte d dscf 79.52 6 83.46 2 80.40 2 81.13 0 Moistur e % v/ v 44. 4 44. 8 44. 1 44. 4 0 2

### a tStac k %dr y 12.5 0 9.4 0 10.0 0 10.6 3 C 0 2

### atStac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 Avg
. Stac k

Temp
. ° F 37 6 36 6 36 4 36 9 Stac k Flowrat e dscf m 5,46 8 5,48 3 5,28 7 5,41 3 Isokinetic s % 10 9 10 0 10 0 10 3 Particulat e Emissio n Result s - Fron tHal fRins e g 0.003 1 0.006 6 0.005 8 0.005 2 Particulat e Filte r g 0.003 0 0.008 1 0.007 1 0.006 1 Tota l Particulat e m g 6.1 0 14. 7 12. 9 11. 2 P M Loadin g @ 7 % 0 2 

### mg/dsc m 4.4 6 7.5 1 7.2 1 6.3 9 Grai n Loadin g gr/dscf 0.001 2 0.002 7 0.002 5 0.002 1 Grai n Loadin g @ 7 % 0 2 

### gr/dscf 0.001 9 0.003 3 0.003 1 0.002 8

3

### Particulate Matte rStandar d = 34 mg/dscm @

7 % 0 2

C:\Documertts an d Settings\jwoodward\Loca l SettmgsYTemporar

yInterne tFiles\OLK7C\Onyx200 6 Test Reportdo c 

### 3- 8 Septembe r200 6

### ENS R

Tabl e 3- 7 Emissio n Result s fo rParticulat e Matte r- Jun e 200 6 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### Star tTim e Unit s 15:1 2 10:0 6 10:0 6 Sto p Tim e 17:2 9 12:2 9 12:4 4 AVG S Samplin g Parameters - - Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Volum e Metere d dc f 78.24 4 82.90 2 81.74 5 80.96 4 Volum e o fGa s Collecte d dsc f 72.24 7 76.48 2 75.57 3 74.76 8 Moistur e % v/v 46. 7 47. 8 45. 5 46. 7 0 2

### a tStac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C 0 2

### a tStac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 Avg
. Stac k

Temp
. ° F 38 6 38 8 38 6 38 7 Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic s 

## % 10 4 L

### 10 6 10 1 ^ 10 4 Particulate Emissio n Results - Fron tHal fRins e g 

### 0.004 0 0.002 8 0.001 7 0. 0 Particulat e Filte r g 

### 0.002 2 0.001 7 0.001 6 0. 0 Tota l Particulat e m g 6.2 0 4.4 6 3.2 5 4.6 4 P M Loadin g @ 7 % 0 2 

### mg/dsc m 3.8 6 2.2 5 1.8 7 2.6 6 Grai n Loadin g gr/dsc f 0.001 3 0.0009 0 0.0006 6 0.001 0 Grai n Loadin g @ 7 % 0 2 

### gr/dsc f 0.001 7 0.001 0 0.000 8 0.001 2

a

### Particulate Matte rStandard = 34 mg/dscm @ 7% Q 2

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yInterne tFiles\OLK7C\Onyx2 00 6 Test Reportdo c 

### 3- 9 Septembe r2 00 6

### ENS R



# 4.0 Samplin g an d Analytica l Procedure s
4. 1 Samplin g Procedure s Severa l differen tsamplin g an d monitorin g technique s wer e use d t o provid e th e require d dat at o mee tth e goal s o fthi s tes tprogram . Thre e (3 ) run s eac h wer e conducte d o n Uni t3 fo rEP AMetho d 0023A , EP AMetho d 29 , an d EP AMetho d 5
. Th e samplin g activitie s describe d belo wwer e conducte d durin g al l runs . Al l fiel d activitie s wer e documente d i n accordanc e wit h EP Aaccepte d procedure s an d copie s o fal l fiel d note s an d dat asheet s ar e include d i n Appendi xB o fthi s report . 4.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s Ga s strea m velocit yan d temperatur e wer e determine d i n conjunctio n wit h eac h manua l samplin g method
. Atyp e "S " pito ttub e connecte d t o a n incline d wate rmanomete rwa s use d t o determin e velocit yhea d o fth e flu e ga s a teac h duc ttravers e poin ta s specifie d i n EP AReferenc e Metho d 2
. Th e temperatur e profil e ofth e flu e ga s a teac h duc ttravers e poin twa s obtaine d b ytakin g reading s wit h athermocoupl e an d pyromete rconcurren twit h th e velocit yhea d measurements . Moistur e conten twa s determine d a s specifie d i n EP AMetho d 4
. Velocit yan d temperatur e measuremen t profile s wer e establishe d prio rt o testin g t o ai d i n sampl e trai n set-up . Sample s fo rth e determinatio n o fth e fixe d ga s compositio n wer e collecte d usin g th e integrate d ba g techniqu e detaile d i n EP A Referenc e Metho d 3
. 4.1. 2 PCDD/PCD FSamplin g Samplin g fo rdioxin s an d furan s wa s complete d i n accordanc e wit h EP AMetho d 23 A(4 0 CF R 60 , Appendi xA)
. Eac h samplin g ru n wa s 19 2 minute s i n duratio n coverin g 1 6 samplin g point s a t1 2 minute s pe rpoint
. 4.1. 3 Metal s an d Particulat e Samplin g Th e EP AMultipl e Metal s Trai n (EP AMetho d 29 , 4 0 CF R 6 0 Appendi xA ) wa s utilize d durin g th e testin g progra m fo rth e collectio n o fth e followin g metals : arsenic , beryllium , cadmium , chromium , lead , an d mercury . Prio rt o metal s analyse s th e tare d filte ran d fron thal faceton e rins e wer e analyze d gravimetricall yfo rparticulat e matte ri n accordanc e wit h EP AR M 5
. Eac h ru n wa s 12 0 minute s i n duratio n coverin g 1 6 samplin g point s a t7. 5 minute s pe rpoint
. 4. 2 Analytica l Procedure s 4.2. 1 PCDD/PCD FAnalyse s PCDD/PCD Fanalyse s wer e performe d b yAlt aAnalytica l Laboratory , Inc
. i n E l Dorad o Hills , CA
. Sampl e fraction s wer e extracted , concentrate d an d analyze d b yEP AMetho d 829 0 (Hig h Resolutio n Ga s Chromatograp h / Hig h Resolutio n Mas s Spectrophotomete r(HRGC/HRMS))
. Th e trai n fraction s recovere d fo ranalysi s o fPCDDs/PCDF s includ e th e fron thal frinse, th e particulat e filter , th e bac k

hal frins e an d th e XA D resi n trap . Th e analytica l result s fo rth e fron thal fan d bac k hal ffraction s wer e analyze d an d reporte d separately
.

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### 4- 1 Septembe r200 6

### ENS R

4.2. 2 Metal s Analyse s Metal s analyse s fo rth e wast e fee d sample s wer e complete d usin g tw o separat e procedures
. First , sample s wer e prepare d an d analyze d fo rarsenic , beryllium , cadmium , chromium , an d lea d a s specifie d i n EP AMetho d 602 0 (ICP-MS) , SW846,3 r d

### Edition
. Mercur ywa s analyze d vi ametho d 747 1 A . Metal s analyse s wer e performe d b yMaxxa m Analytica l Inc
. ofBurlington , Ontari o (Canada)
. 4. 3 Proces s Operatin g Condition s Throughou tth e fiel d program , detaile d proces s informatio n wa s collecte d continuousl yb yth e facility' s proces s contro l computer s an d dat aacquisitio n syste m (DAS)
. Proces s dat aincludin g minimum , maximu m an d averag e value s fo rke yproces s variable s recorde d durin g eac h tes t condition
. I n general , target-operatin g condition s specifie d wer e achieved
.

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yInterne tFiles\OLK7C\Onyx200 6 Test Report.do c 

### 4- 2 Septembe r200 6

### ENS R



# 5.0 QuaSft

yAssuranc e
5. 1 Introductio n Thi s sectio n present s th e result s ofal l QA/Q C measure s implemente d durin g th e fiel d samplin g progra m an d al l phase s o fsubsequen tanalysis
. Dat agenerate d fo rth e progra m ar e judge d t o b e vali d a s overal l accurac yan d precisio n result s ar e consisten twit h genera l objectives
. Analytica l QA/Q C dat aar e presente d t o suppor tal l sampl e result s use d fo rdeterminin g complianc e wit h performanc e criteri ao remissio n standards
. Throughou tth e overal l program , al l samplin g wa s performe d usin g samplin g protocol s describe d herei n an d approve d b yUSEP Aan d th e Illinoi s Environmenta l Protectio n Agency
. 5.1. 1 Pre-Samplin g Activitie s Pre-samplin g activitie s include d equipmen tcalibration , sampl e medi apreparation , cleanin g o f sampl e trai n glassware , preparatio n o fcomputer-generate d sampl e label s an d othe rmiscellaneou s tasks
. Eac h o fthes e activitie s ar e describe d o rreference d i n th e followin g subsections
. Othe rpre samplin g activitie s include d suc h detail s a s tea m meetings , equipmen tpackin g an d shipment , equipmen tsetup , an d finalizatio n o fal l detail s leadin g u p t o th e coordinate d initiatio n o fth e samplin g program . 5.1. 2 Equipmen tCalibratio n Amos timportan taspec to fpre-samplin g preparation s wa s th e inspectio n an d calibratio n o fal l equipmen tuse d fo rth e fiel d effort
. Equipmen twa s inspecte d fo rprope roperatio n an d durabilit y prio rt o calibration
. Calibratio n o fequipmen twa s conducte d i n accordanc e wit h th e procedure s outline d i n th e EP Adocumen tentitle d "Qualit yAssuranc e Handboo k fo rAi rPollutio n Measuremen t Systems ; Volum e III—StationarySourc e Specifi cMethods " (EPA-600/4-77-027b)
. Equipmen t calibratio n wa s performe d i n accordanc e with EP Aguideline s and/o rmanufacturer' s recommendations
. Copie s ofthese s calibration s ar e presente d i n Appendi xC
. Example s o ffiel d equipmen tuse d an d typica l calibratio n requirement s follows :

•PROB E NOZZLE S

### (Q AHandboo k Sectio n 3.4.2 , pg . 19 ) - measurement s o fth e nozzl e I D (t o th e neares t0.001-in. ) alon g thre e differen tdiameter s wit h amicrometer
. Differenc e betwee n th e hig h an d lo wvalue s shoul d no texcee d 0.00 4 in
. Post-tes tcheck s - inspec tfo rdamage
.
•PITO TTUBE S

### (Q AHandboo k Sectio n 3.1.2 , pp . 1-13 ) - measure d fo rappropriat e spacin g an d dimension s o rcalibrat e i n awin d tunnel
. Rejectio n criteri agive n o n th e calibratio n sheet
. Post-tes tcheck s - inspec tfo rdamage
.
•THERMOCOUPLE S

### (Q AHandboo k Sectio n 3.4.2 , pp . 15-18 ) - verif yagains tamercury-in-glas s thermomete ra ttw o o rmor e point s includin g th e anticipate d measuremen trange . Acceptanc e limit s - impinge r±2°F ; DG M ±5.4°F ; stac k ±1. 5 percen to fstac k temperature .
•D R YGA S METER S

### (Q AHandboo k Sectio n 3.4.2 , pp . 1-12 ) - calibrat e agains tawe ttes tmeter . Acceptanc e criteri a- pretes tY i = Y±0.2 ; pos ttes tY= ±0.0 5 Yi
.
•FIEL D BAROMETER S

### (Q AHandboo k Sectio n 3.4.2 , pp . 18-19 ) - compar e agains tamercury in-glas s baromete ro rus e Airpor tStatio n B P an d correc tfo relevation
. Acceptanc e criteri a- ±0.0 2 in
. Hg ; post-tes tcheck s - same .

C:\Doouments an d Settings\jwoodward\Loca l Settings\Temporar

yinternetFiles\OLK7C\Onyx200 6 Test Report.do c 

### 5- 1 Septembe r200 6

### ENS R

5.1. 3 Glasswar e Preparatio n Sampl e trai n glasswar e an d sampl e container s require d specialize d pre-cleanin g t o avoi d contaminatio n o fth e sampl e fro m th e collectio n containe ro rdevices
. Cleaning/storag e procedure s fo rsampl e trai n glasswar e ar e summarize d below
. Not e tha tal l bottl e cap s ar e fitte d wit h Teflo n liners , whic h wer e cleane d i n th e sam e manne ra s th e bottle s themselves
. Sampl e container s use d fo rwast e fee d stream s ar e purchase d pre-cleane d an d seale d t o specifie d EP Aprotocols
.
•EP AMETHO D

### 001 0 / 0023 AGLASSWAR E AN D CONTAINER S

### (PCDDs/PCDFs ) - washe d wit h soa p an d water , rinse d thre e time s wit h deionize d (DI ) water , bake d a t400° C fo r2-hours , rinse d thre e time s wit h pesticid e grad e methylen e chloride , rinse d thre e time s wit h pesticid e grad e toluen e an d ai rdry
.
•EP AMETHO D

### 5/29 / 006 0 GLASSWAR E AN D CONTAINER S (METAL S AN D PARTICULAT E MATTER )



### - washe d with soa p an d water , rinse d wit h ho tta p wate ran d rinse d thre e time s wit h reagen t water . Th e glasswar e wa s soake d i n a10 % nitri caci d solutio n fo raminimu m o f4-hours , rinse d thre e time s wit h reagen twater , rinse d afina l tim e wit h aceton e an d air-dried
. Al l glasswar e opening s wher e contaminatio n ca n occu rar e covere d wit h Parafil m unti l th e samplin g trai n wa s assemble d prio rt o sampling
. 5.1.3. 1 Sampl e Medi aPreparatio n Al l reagent s wer e checke d i n accordanc e wit h ENSR' s existin g Q C Progra m t o minimiz e th e probabilit yo fusin g contaminate d solvents
. Thi s include d th e us e o fth e prope rgrad e reagents/solvent s a s specifie d i n th e tes tmethod , selectio n o freagent s fro m th e sam e lo tan d collectio n an d analysi s o fth e appropriat e blanks
. Samplin g medi awa s procure d an d prepare d i n accordanc e wit h th e appropriat e tes tmethod s a s describe d below :

•XA D resi n use d i n th e Metho d 0023 Atrai n wa s purchase d ne wan d packe d i n speciall y designe d sorben ttraps . Al l glas s cleanin g an d sorben tpackin g procedure s followe d th e protocol s specifie d i n EP AMetho d 0023A
.
•Quart z filter s use d i n th e Metho d 5 / 2 9 / 006 0 samplin g trai n wer e supplie d b yMaxxa m Analytics , Inc
. wh o pre-scree n filter s fo rmetal s content .

C:\Document s an d Settings\jwoodward\Loca l SettingsYTemporar

yInterne tFiles\0l_K7C\0nyx200 6 Test Reportdo c 

### 5- 2 Septembe r200 6

# ENS R

Appendi xA FacilityOperatin g Data

S:\_JOB\2006\Onyx\Performano e Test\Report\Ony x200 6 TestReport.do c Septembe r200 6

### Uni t#

3 Ru n # 1 

### Date : 05/10/0 6 Tes tTime : 09:4 7 t o 13:5 1 Ru n Length : 19 9 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 682 0 0. 5 0. 3 0.1 3 2. 5 1 5 PC C LowBt u 50 0 0. 5 0.3 3 0.0 5 2. 5 ! 

### 5 (Chlorin e Spike ) 50 0 85. 5 0. 1 0.1 3 2. 5 1 

### 5 PC C S p Fd r 50 0 0. 5 0. 1 0.0 5 2. 5 - I 5 (Chromiu m Spike ) 50 0 0. 5 23. 4 0.1 3 2. 5 1 

### 1. 3 PC C Soli d Charge s 50 0 0. 5 81. 8 0.2 1 20. 1 1 8. 6 (Lea d Spike ) 50 0 0. 5 66. 4 0.1 3 63000 0 20 8 6 (Chlorin e Spike ) 50 0 63. 5 96. 3 0.1 3 2. 5 1 5 (MercurySpike ) 50 0 0. 5 0. 1 60 0 2. 5 1 5 Total s

### Averag e Therma l Chlorin e As h Mercury Lea d PP M Fee d rate Loadin g Loadin g Loadin g Loadin g Loadin g liu m Chromiu m (Ib/hr ) (MMBtu/hr) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2. 5 98 2 6.7 0 4.9 1 2.9 5 0.00012 8 0.0 0 0. 1 2. 5 171 5 0.8 6 8.5 8 5.6 6 0.00008 6 0.0 0 0. 1 2. 5 11 7 0.0 6 100.0 4 0.1 2 0.00001 5 0.0 0 0. 1 2. 5 45 8 0.2 3 2.2 9 0.4 6 0.00002 3 0.0 0 0. 1 18000 0 25 1 0.1 3 1.2 6 58.7 3 0.00003 3 0.0 0 0.2 9 26. 1 61 9 0.3 1 3.1 0 506.3 4 0.00013 0 0.0 1 0. 1 2. 5 9 2 0.0 5 0.4 6 61.0 9 0.00001 2 57.9 6 0. 1 2. 5 13 8 0.0 7 87.6 3 132.8 9 0.00001 8 0.0 0 0. 1 2. 5 1.35 0.0 0 0.0 1 0.0 0 0.00081 0 0.0 0 437 3 8.3 9 208.2 6 768.2 4 0.0012 5 57.9 8

### Cadmiu m

Loadin g (Ib/hr ) Arseni cBerylliu m Chromiu m Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 2 0.0 0 0.0 0 0.0 0

0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 45.1 8 0.0 2 0.0 0 0.0 0 0.0 0 0.0 2 0.0 2 0.0 0 45.2 0

### Unit#

3 Ru n # 2 Date : 05/10/0 6 Tes tTime : 14:5 1 t o 18:1 7 Ru n Length : 20 6 minute s PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury PC C Hig h Bt u 672 0 0.5 6 0.2 8 0.1 3 PC C Lo wBt u (Chlorin e Spike ) 50 0 50 0 0. 5

85. 5 0.3 2

0. 1 0.0 5

0.1 3 PC C S p Fd r (Chromiu m Spike ) 50 0 50 0 0. 5

0. 5 0. 1

23. 4 0.0 5

0.1 3 PC C Soli d Charge s (Lea d Spike ) (Chlorin e Spike ) (Mercur ySpike ) 50 0 50 0 50 0 50 0 0. 5

0. 5 63 5 0. 5 8 2

66. 4 96. 3 0. 1 0.1 9

0.1 3 0.1 3 60 0 PP M PP M PP M Lea d Cadmiu m Arseni c 2. 5 1 5 2. 5 1 5 2. 5 1 5 2. 5 1 5 2. 5 1 2. 6 19. 6 1 9. 5 63000 0 22 1 1. 6 2. 5 1 5 2. 5 1 5
Total s

### PP M PP M

Berylliu m Chromiu m Averag e Therma l Chlorin e As h Mercury Feedrat e Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (MMBtu/hr) (Ib/hr

) (Ib/hr

) (Ib/hr

) Lea d Loadin g (Ib/hr ) 0. 1 2. 5 99 2 6.6 7 5.5 6 2.7 8 0.00012 9 0. 1 2. 5 168 1 0.8 4 8.4 1 5.3 8 0.00008 4 0. 1 2. 5 10 0 0.0 5 85.5 0 0.1 0 0.00001 3 0. 1 2. 5 46 1 0.2 3 2.3 1 0.4 6 0.00002 3 0.1
. 18000 0 25 5 0.1 3 1.2 8 59.6 7 0.00003 3 0.4 3 28. 1 71 9 0.3 6 3.6 0 589.5 8 0.00013 7 0. 1 2. 5 10 8 0.0 5 0.5 4 71.7 1 0.00001 4 0. 1 2. 5 16 1 0.0 8 102.2 4 155.0 4 0.00002 1 0. 1 2. 5 1.5 8 0.0 0 0.0 1 0.0 0 0.00094 8 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 68.0 4 0.0 0 0.0 0 447 9 8.4 1 209.4 2 884.7 2 0.0014 0 68.0 6

### Cadmiu m Arseni cBerylliu m Chromiu m

Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (lb/hr) (Ib/hr ) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 45.9 0 0.0 0 0.0 1 0.0 0 0.0 2 0.0 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 3 0.0 2 0.0 0 45.9 3

### Uni t#

3 Ru n # 3 Date : 05/11/06 Tes tTime : 11:2 5 t o 14:4 8 Ru n Length : 20 3 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 763 0 0.6 6 0.2 8 0.1 3 2. 5 1 5 PC C Lo wBt u 50 0 0. 5 0.3 1 0.0 5 2. 5 ! 

### 5 (Chlorin e Spike ) 50 0 85. 5 0. 1 0.1 3 2. 5 1 

### 5 PC C S p Fd r 50 0 0. 5 0. 1 0.0 5 2. 5 1 

### 5 (Chromiu m Spike ) 50 0 0. 5 23. 4 0.1 3 2. 5 1 

### 2 PC C Soli d Charge s 50 0 0. 5 82. 6 0.3 5 36. 8 ! 

### 11. 2 (Lea d Spike ) 50 0 0. 5 66. 4 0.1 3 63000 0 28 3 9. 1 (Chlorin e Spike ) 50 0 63. 5 96. 3 0.1 3 15 0 1 5 (MercurySpike ) 50 0 0. 5 0. 1 60 0 2. 5 1 5 Total s

### PP M PP M

Berylliu m Chromiu m Averag e Therma l Chlorin e As h MercuryLea d Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (MMBtu/hr) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2. 5 100 0 7.6 3 6.6 0 2.8 0 0.00013 0 0. 1 2. 5 193 1 0.9 7 9.6 6 5.9 9 0.00009 7 0. 1 2. 5 9 2 0.0 5 78.6 6 0.0 9 0.00001 2 0. 1 2. 5 44 8 0.2 2 2.2 4 0.4 5 0.00002 2 0. 1 18000 0 24 5 0.1 2 1.2 3 57.3 3 0.00003 2 0. 9 26. 3 72 3 0.3 6 3.6 2 597.2 0 0.00025 3 0. 1 1. 3 10 6 0.0 5 0.5 3 70.3 8 0.00001 4 0. 1 2. 5 15 8 0.0 8 100.3 3 152.1 5 0.00002 1 0. 1 2. 5 1.55 0.0 0 0.0 1 0.0 0 0.00093 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 3 66.7 8 0.0 2 0.0 0 470 5 9.4 8 202.8 6 886.3 9 0.0015 1 66.8 4

### Cadmiu m

Loadin g (Ib/hr ) Arseni cBerylliu m Chromiu m Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 3 0.0 0 0.0 0 0.0 1

0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 44.1 0 0.0 2 0.0 0 0.0 0 0.0 0 0.0 3 0.0 3 0.0 0 44.1 3

### Uni t#

3 Ru n #1 Date : 06/19/0 6 Tes tTime : 14:4 0 t o 18:0 5 Ru n Length : 20 5 minute s Wast e Typ e PC C Hig h Bt u PC C LowBt u (Chlorin e Spike ) P C C S p Fd r (Chromiu m Spike ) P C C Soli d Charge s (Lea d Spike ) (Chlorin e Spike ) (MercurySpike ) Btu/l b %Chlorin e 993 0 50 0 317 0 3. 2

0. 5 85. 5 PP M %As h Mercury PP M PP M PP M Lea d Cadmiu m Arseni c 1. 5 0. 2 0. 1 0.41 3 0.020 2 0.01 1 18. 8

1.27 0. 1 1.9 8 0.037 2 0.0 2 2. 5

0.27 2 0. 2 50 0 0. 5 0. 1 0.0003 5 1.38 0.005 2 12. 1 50 0 0. 5 25. 9 0.00 2 80 0 97 0 88 0 88 0 0. 6 70. 6 0.02 5 12.9 3 0.3 0 6.7 3 50 0 0. 5 65. 6 0.0 2 63000 0 2 7 2 5 50 0 63. 5 97. 4 0.0 2 17 0 5 2 5 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2
Total s

### PP M PP M

Berylliu m Chromiu m 0. 1 13. 3 0.00 1 0.46 2 0.0 5 0.0 4 0.0 1 0.012 1 96 0 18000 0 0.3 7 157.8 1 4. 8 2 2. 5 2 0.0 5 0.0 4 Averag e Therma l Chlorin e Feedrat e Loadin g Loadin g (Ib/hr ) (MMBtu/hr ) (Ib/hr ) 111 0 11.0 2 35.5 2 189 6 0.9 5 9.4 8 9 5 0.3 0 81.2 3 56 9 0.2 8 2.8 5 25 1 0.1 3 1.2 6 79 8 0.7 0 4.7 1 11 9 0.0 6 0.6 0 17 9 ' 0.09 113.6 7 1.7 5 0.0 0 0.0 1 501 9 13.5 3 249.3 0 As h MercuryLea d Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) 16.6 5 0.00045 8 0.0 2 3.7 9 0.00003 8 0.0 0 0.1 0 0.00000 1 0.0 0 0.5 7 0.00000 0 0.0 0 65.0 1 0.00000 1 0.2 0 563.7 4 0.00002 0 0.0 1 78.0 6 0.00000 2 74.9 7 174.3 5 0.00000 4 0.0 3 0.0 0 0.00113 1 0.0 0 902.2 7 0.0016 6 75.2 4

### Cadmiu m

Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.2 4 0.0 0 0.0 0 0.0 0 0.0 0 Arseni c Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 1 0.2 2 0.0 1 0.0 0 0.0 0 0.0 0 Berylliu m Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.2 4 0.0 0 0.0 0 0.0 0 0.0 0 Chromiu m Loadin g (Ib/hr ) 0.0 1 0.0 0 0.0 0 0.0 0 45.1 8 0.1 3 0.0 0 0.0 0 0.0 0 0.2 5 0.2 4 0.2 4 45.3 2

### Uni t#

3 Ru n # 2 Date : 06/20/0 6 Tes tTime : 09:3 0 t o 13:0 5 Ru n Length : 21 5 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 900 0 2. 3 4. 9 0.41 3 4 0.3 5 2. 5 PC C Lo wBt u 50 0 0. 5 0. 2 0.0019 2 0.0 4 0.003 4 0.25 3 (Chlorin e Spike ) 317 0 85. 5 0. 1 0.01 4 0. 1 0.0 2 0. 2 PC C S p Fd r 50 0 0. 5 0. 1 0.000 2 0.091 4 0.00 2 0.18 6 (Chromiu m Spike ) 50 0 0. 5 25. 9 0.00 2 10 0 2 0 20 0 PC C Soli d Charge s 82 4 0. 6 69. 9 0.03 8 16.4 5 0.3 7 6.2 5 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 3 2 2 5 (Chlorin e Spike ) 50 0 63. 5 97. 4 0.0 2 4 2 5 2 5 (MercurySpike ) 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2 Total s

### Averag e Therma l Chlorin e As h Mercury Lea d

PP M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 1 3 112 6 10.1 3 25.9 0 55.1 7 0.00046 5 0.0 0 0.00 1 0.057 9 195 9 0.9 8 9.8 0 3.9 2 0.00000 4 0.0 0 0.0 5 0.04 6 10 2 0.3 2 87.2 1 0.1 0 0.00000 1 0.0 0 0.00 1 0.011 6 54 3 0.2 7 2.7 2 0.5 4 0.00000 0 0.0 0 5 0 18000 0 25 0 0.1 3 1.2 5 64.7 5 0.00000 1 0.0 3 0.3 1 11.8 8 80 5 0.6 6 4.9 6 563.0 1 0.00003 0 0.0 1 7. 8 2 11 7 0.0 6 0.5 9 76.7 5 0.00000 2 73.7 1 2. 5 2 17 6 0.0 9 111.7 6 171.4 2 0.00000 4 0.0 1 0.0 5 0.0 4 1.72 0.0 0 0.0 1 0.0 0 0.00111 1 0.0 0 508 0 12.6 4 244.1 8 935.6 7 0.0016 2 73.7 6

### Cadmiu m

Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 Arseni c Loadin g (Ib/hr) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 5 0.0 1 0.0 0 0.0 0 0.0 0 Berylliu m Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 Chromiu m Loadin g (Ib/hr ) 0.0 1 0.0 0 0.0 0 0.0 0 45.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 7 0.0 1 45.0 2

### Uni t#

3 Ru n # 3 Date : 06/21/0 6 Tes tTime : 09:3 0 t o 13:1 9 Ru n Length : 22 9 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 1022 0 3. 1 0. 4 0.67 9 3.8 5 0.8 3 6.7 7 PC C Lo wBt u 50 0 0. 5 0. 2 0.0018 4 0.0 4 0.005 4 0.25 7 (Chlorin e Spike ) 317 0 85. 5 0. 1 0.004 5 0. 1 0.0 2 0. 2 P C C S p Fd r 50 0 0. 5 0. 1 0.000 2 0.043 2 0.00 2 0.070 9 (Chromiu m Spike ) 50 0 0. 5 25. 9 0.00 2 10 0 2 0 20 0 PC C Soli d Charge s 79 3 0. 5 70. 8 0.15 7 18.4 6 0.4 4 5.7 6 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 4 2 2 5 (Chlorin e Spike ) 50 0 63. 5 97. 4 0.0 2 1 8 5 2 5 (MercurySpike ) 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2 Total s

### Averag e Therma l Chlorin e

PP M PP M Feedrat e Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr) (Ib/hr ) 0. 1 5.7 4 107 9 11.0 3 33.4 5 1.00 1 0.058 6 203 9 1.02 10.2 0 0.0 5 0.0 4 9 6 0.3 0 82.0 8 ).O0 1 0.040 8 54 7 0.2 7 2.7 3 5 0 18000 0 24 9 0.1 2 1.2 5 0.3 5 12.4 7 81 5 0.6 5 4.3 1 8. 1 2 11 9 0.0 6 0.6 0 2. 5 2 17 8 0.0 9 113.0 3 0.0 5 0.0 4 1.74 0.0 0 0.0 1 512 4 13.5 5 247.6 5 As h MercuryLea d Loadin g Loadin g Loadin g (Ib/hr ) (lb/hr) (Ib/hr ) 4
. .32 0
. .00073 3 0.0 0 4
. ,0 8 0
. .00000 4 0.0 0 0 .1 0 0 , .00000 0 0.0 0 0
. .5 5 0 .00000 0 0.0 0 64
. .4 9 0 , .00000 0 0.0 2 577 , .2 9 0 .00012 8 0.0 2 78 , ,0 6 0 .00000 2 74.9 7 173 , .3 7 0 .00000 4 0.0 0 0 , .0 0 0 .00112 4 0.0 0 90 2 .2 5 0.0020 0 75.0 2

### Cadmiu m Arseni cBerylliu m Chromiu m

Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0 1 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 5 0.0 1 44.8 2 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 7 0.0 1 44.8 4

### Baghous e Inle tTemp
. (De g F )

(Ave
. o ftes tru n ave.'s ) PC C Temp
. (De g F ) (Ave
. oftes tru n ave.'s ) SC C Temp
. (De g F ) (Ave
. o ftes tru n ave.'s ) Stackflo w(ACFM ) (Ave
. ofmax . HRA' s o

feac h tes trun ) Pumpabl e Wast e Fee d (Lb/hr ) (Ave
. o fmax . HRA' s o

feac h tes trun ) (Includes average spiked liquids flows) Tota l Wast e Fee d (Lb/hr ) (Ave
. o fmax . HRA' s o

feac h tes trun ) (Includes average spiked liquids flows) Mercur yFee d (Lb/hr ) (Ave
. o ftes tru n ave.'s ) As h Fee d (Lb/hr ) (Ave
. o ftes tru n ave.'s ) LV M Fee d (Lb/hr ) (Ave
. o ftes tru n ave.'s ) SV M Fee d (Lb/hr ) (Ave
. o ftes tru n ave.'s ) Chlorin e Fee d (Lb/hr ) (Ave
. o ftes tru n ave.'s ) Uni t3 Operatin g Parameter s June , 200 6

Ru n 1 Ru n 2 Ru n 3 Averag e 42 0 42 1 42 1 42 0 173 5 172 5 174 1 173 4 184 5 185 0 185 1 184 9 1488 8 1534 9 1526 7 1516 8 414 7 416 1 417 2 416 0
346 352

345



### na 527 3 536 7 539 1 534 4
346 352

345



### n a 0.001 7 0.001 6 0.002 0 0.001 8 90 2 93 6 90 2 91 3 4 6 4 5 4 5 4 5 7 5 7 4 7 5 7 5 24 9 24 4 24 8 24 7

### Uni t3 Operatin g Parameter s

May , 200 6

Ru n 1 

### 42 0 171 3 184 5 1487 3 371 8

368 

### AIM
368 

### 0.001 3 76 8 4 5 5 8 20 8 Ru n 2

42 0 171 5 184 5 1542 8 368 3

355 

### 486 2
355 

### 0.001 4 88 5 4 6 68 20 9 Ru n 3

42 0 171 2 184 6 1446 8 380 0

337 

### 479 3
337 

### 0.001 5 88 6 4 4 6 7 20 3 Averag e

42 0 171 3 184 5 1492 3 373 4 na 479 1 na 0.001 4 84 6 4 5 6 4 20 7

### ENS R



# Appendi xB Reference Method Fiel d Data an d Calculation s

S:\_JOB\2006\Onyx\Performanc e Test\Report\Ony x2006 TestReport.do c Septembe r200 6

# Ma y2006 Tes t

# Particulate Matte rData

### Veoli aE S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 5 Samplin g Parameter s Ru n No
. Ru n 1 Ru n 2 Ru n 3 AVG S Dat e 10-May-0 6 10-May-0 6 11-May-0 6 AVG S Star tTim e Unit s 10:0 8 15:0 0 11:2 5 AVG S Sto p Tim e 12:5 1 17:1 6 13:3 9 Nozzl e Diamete r inche s 0.41 2 0.44 0 0.44 0 0.43 1 Barometri cPressur e !. n .:.H g 29.1 0 29.0 2 29.0 5 29.0 6 NetSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 81.99 1 84.12 8 81.69 9 82.60 6 Avg
. DG M Temp
. 1 85. 9 72. 5 77. 1 78. 5 Av g Delt aH i n H 2 0 1.57 1.73 1.56 1.62 Av g Delt aH [ IELB S 0.115 8 0.127 4 0.114 6 "6.119 3 DG M Calibratio n Facto r 1.027 0 1.0270 1.027 0 1.027 0 Ga s Sampl e Volum e i dsc f I 79.52 6 83.46 2 80.40 2 81.13 0 Tota l Wate rCollecte d m L 1344. 7 1438. 7 1343. 8 1375. 7 Volum e o

fWate rVapo r scf ' 63.40 3 67.83 5 63.36 0 64.86 6 Moisture (measured ) % v/ v I 44. 4 44. 8 44. 1 44. 4 Moisture ( @ saturation ) % v/ v 102. 8 103. 0 103. 0 102. 9 Dr yMol e Fraction , 100-% M



## - 0.556 4 0.551 6 0.559 3 0.555 8 C 0 2a tStac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 0 2atStac k %dr y 12.5 0 9.4 0 10.0 0 10.6 3 C O + N 2 %dr y 81.1 0 83.8 0 83.0 0 82.6 3 Dr yMolecula rWeigh t lb/lb-mole 29.5 2 29.4 6 29.5 2 29.5 0 We tMolecula rWeigh t Ib/lb-mol e 24.4 1 24.3 2 24.4 4 24.3 9 Exces s Ai ra

tStac k 0 / /o 140. 3 73. 9 83. 9 99. 4 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 i 194. 6 1194. 6 Stati cPressur e i n H 2 0 0.2 2 0.2 2 0.0 7 0.1 7 Stac k Pressur e in
. H g 29.1 2 29.0 4 29.0 6 29.0 7 Avg
. Stac k

Temp
. ° F 376. 4 366. 2 364. 3 369. 0 Avg
. Sqroo to

fDelt aP - - 0.412 5 0.414 5 0.394 6 0.407 2 SD E Averag e ~ 11.93 1 11.91 5 11.33 0 11.72 5 PitotCoefficien t


## - 0.8 4 0.8 4 0.84 0.84 Stac k Ga s Velocity afp m 1,92 8 1,932 1,832 1,89 7 Stac k Flowrat e wetacf m 15,99 8 16,02 7 15,19 8 15,74 1 Stac k Flowrat e wetscf m 9,82 7 9,94 0 9,45 3 9,74 0 Stac k Flowrat e dscf m 5,46 8 5,48 3 5,28 7 5,41 3 Isokinetic s % 10 9 10 0 10 0 10 3 Mete rBo xNo
. — 8061 0 8061 0 8061 0 

## - Delt aH @ i n H 2 0 1.80 3 1.803 1.803 

## - Fiel d Q AYq c 

## - 1.0465 1.059 1 , 1.0375 1.047 7 [Deviation ] Pre- Y % 1.90% 3.13 % 1.02 % 2.02% S,\_JOB\2006\Onyx\Performanc e TestVTes tOataKtny

xMa y2006V[M5 P M #

3 Ma y2006 da

y2.xls]OAT

A

### Metho d 5 Samplin g Parameter s

P T 

### Ru n 

### 1 Ru n 

### 2 Ru n 

### 3 P T Delt aP SQR T

Delt aP DG M

I N DG M

OU T Delt aH STAC K TEM P Delt aP SQR T Delt aP DG M

I N DG M

OU T Delt aH STAC K

TEM P Delt aP SQR T Delt aP DG M

I N DG M

OU T Delt aH STAC K

TEM P a 1 

### 0.1 5 0.387 3 7 0 7 0 1.38 34 6 0.1 8 0.424 3 7 6 7 5 1.90 37 0 0.1 3 0.360 6 7 0 6 9 1.30 35 0 a 2 

### 0.2 0 0.447 2 7 7 7 2 1.8 1 37 8 0.2 0 0.447 2 7 5 74 1.99 37 0 0.1 6 0.400 0 7 4 6 9 1.58 36 4 a 3 

### 0.2 0 0.447 2 82 7 4 1.8 1 37 8 0.2 1 0.458 3 7 6 7 3 2.0 9 36 8 0.1 7 0.412 3 7 7 7 0 1.68 36 9 a 4 

### 0.2 1 0.458 3 8 5 7 5 1.89 38 8 0.2 0 0.4472 7 7 72 1.99 36 6 0.1 9 0.435 9 8 0 7 1 1.88 36 9 a 5 

### 0.2 0 0.447 2 8 6 8 0 1.82 39 0 0.1 9 0.435 9 7 5 7 1 1.90 36 3 0.1 7 0.412 3 8 1 72 1.70 36 8 a 6 

### 0.1 8 0.424 3 9 0 8 2 1.66 37 4 0.1 9 0.435 9 7 1 6 9 1.90 36 4 0.1 6 0.400 0 8 2 7 3 1.60 36 2 a 7 

### 0.1 5 0.387 3 92 8 2 1.3 8 37 5 0.1 5 0.387 3 7 6 6 9 1.50 36 2 0.1 6 0.400 0 8 3 7 4 1.60 36 4 a 8 

### 0.1 1 0.331 7 9 3 8 3 1.02 37 4 0.1 1 0.331 7 7 6 6 9 1.1 0 36 3 0.1 4 0.374 2 8 3 7 5 1.40 36 5 b 1 

### 0.1 6 0.400 0 8 6 8 4 1.48 37 4 0.1 2 0.346 4 6 9 6 8 1.20 36 5 0.1 5 0.387 3 7 5 7 4 1.50 36 3 b 2 

### 0.1 8 0.424 3 9 3 8 5 1.67 37 7 0.1 6 0.400 0 7 4 6 8 1.60 36 5 0.1 7 0.412 3 8 0 7 5 1.70 36 6 b 3 

### 0.1 8 0.424 3 94 8 6 1.67 37 8 0.1 8 0.424 3 7 5 6 8 1.80 36 5 0.1 7 0.412 3 8 3 7 5 1.70 36 6 b 4 

### 0.1 6 0.400 0 9 6 8 8 1.48 37 9 0.1 8 0.424 3 7 6 6 9 1.80 36 6 0.1 7 0.412 3 8 4 7 6 1.70 36 5 b 5 

### 0.1 8 0.424 3 9 6 8 8 1.66 37 9 0.1 8 0.424 3 7 5 6 8 1.80 36 4 0.1 6 0.400 0 8 4 7 6 1.60 36 5 b 6 

### 0.1 9 0.435 9 9 6 8 8 1.75 37 8 0.2 0 0.447 2 7 6 6 8 1.98 372 0.1 5 0.387 3 8 5 7 7 1.50 36 8 b 7 

### 0.1 5 0.387 3 9 7 9 0 1.39 37 8 0.1 8 0.424 3 7 7 6 8 1.78 37 2 0.1 3 0.360 6 8 2 7 7 1.30 36 4 b 8 

### 0.1 4 0.374 2 9 8 9 1 1.3 2 37 7 0.1 4 0.374 2 7 8 6 8 1.40 36 4 0.1 2 0.346 4 8 4 7 7 1.20 36 1 AV G 0.1 7 0.412 5 85. 9 1.57 37 6 0.1 7 0.414 5 72. 5 1.73 36 6 0.1 6 0.394 6 77. 1 1.56 36 4

# ENS . SAMPLIN G TRAIN : PLANT : DATE : 

### MtC O E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T
M5 / Particulat e ONY XEnvironmenta l Q 5 -iO-Ok. TES TLOCATION : RU N NUMBER : Stac k Diamete r- inches :

Uni t# 3 Fixe d Heart h J J 39 " OPERATOR : STAR TTIME : STO P TIME : loc i



# mi BAROMETRI C PRESSURE :

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. MI D VAC
. FINA LVAC
. LEA KCHECKS : ) Tin
. CF M

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# Metal s Data

### Veoli aE S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 006 0 (Metals ) Samplin g Parameter s Ru n No
. Ru n 1 Ru n 2 Ru n 3
AVG S Dat e 10-May-0 6 10-May-0 6 11-May-0 6 

### AVG S StartTim e Unit s 10:0 8 15:0 0 11:2 5 AVG S Sto p Tim e 12:5 1 17:1 6 13:3 9 Nozzl e Diamete r inche s 0.40 8 0.43 1 0.43 1 0.42 3 Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dcf 81.24 8 83.54 6 76.76 1 80.51 8 Avg
. DG M Temp
. ° F 86. 8 71. 2 78. 0 78. 7 Av g Delt aH i n H 2 

### 0 1.5 7 1.76 1.42 1.5 8 Av g Delt aH in
. H g 0.115 6 0.129 2 0.104 1 0.116 3 DG M Calibratio n Facto r 

# - 1.039 0 1.039 0 1.039 0 1.039 0 Ga s Sampl e Volum e dsc f 79.59 8 84.05 6 76.26 9 79.97 4 Tota l Wate rCollecte d m L 1271. 1 1380. 4 1300. 2 1317. 2 Volum e ofWate rVapo r scf 59.93 2 65.08 6 61.30 4 62.10 8 Moistur e (measured ) % v/ v 43. 0 43. 6 44. 6 43. 7 Moistur e ( @ saturation ) % v/ v 102. 8 103. 0 103. 0 102. 9 Dr yMol e Fraction , 100-% M 

# - 0.570 5 0.563 6 0.554 4 0.562 8 C 0 2

### atStac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 0 2

### atStac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 C O + N 2 

### %dr y 81.2 0 83.8 0 83.0 0 82.6 7 Dr yMolecula rWeigh t Ib/lb-mol e 

### 29.5 2 29.4 6 29.5 2 29.5 0 We tMolecula rWeigh t Ib/lb-mol e 

### 24.5 7 24.4 6 24.3 9 24.4 7 Exces s Ai ratStac k / o 137. 2 73. 9 83. 9 98. 3 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 

### 0 0.2 2 0.2 1 0.0 7 0.1 7 Stac k Pressur e in
. H g 29.1 2 29.0 4 29.0 6 29.0 7 Avg
. Stac k

Temp
. ° F 381. 2 371. 1 371. 4 374. 6 Avg
. Sqroo to

fDelt aP 

# - 0.412 8 0.423 5 0.384 3 0.406 9 SD E Averag e — 

### 11.97 2 12.20 9 11.08 2 11.75 4 Pito tCoefficien t 

# - 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,92 9 1,974 1,79 4 1,89 9 Stac k Flowrat e we tacf m 16,00 1 16,37 7 14,88 3 15,75 3 Stac k Flowrat e we tscf m 9,77 4 10,09 7 9,17 8 9,68 3 Stac k Flowrat e dscf m 5,57 6 5,69 1 5,08 8 5,45 1 Isokinetic s % 

### 10 9 10 1 10 2 10 4 Mete rBo xNo
. — 

### 8018 4 8018 4 8018 4 - - Delt aH @ i n H z 

### O 1.881 0 1.881 0 1.881 0 

# - Fiel d Q AYq c — 

### 1.034 0 1.050 0 1.031 3 1.03 8 [Deviation ! Pre- Y % 0.48 % 1.06 % 0.74 % 0.8 %

### Metho d 006 0 (Metals ) Samplin g Parameter s

P T Run l AVGS - METAL S Run 2 AVG S -METAL S R u n 3 AVG S - MET A L S P T Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH STAC K

TEM P Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH | STAC K

TEM P Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH STAC K

TEM P a 1 0.1 5 0.387 3 7 3 7 2 1.38 36 6 0.1 2 0.346 4 7 9 7 7 1.2 0 35 9 0.1 6 0.400 0 7 1 7 1 1.5 0 36 7 2 0.2 0 0.447 2 7 8 7 4 1.8 0 37 9 0.2 1 0.458 3 7 6 7 5 2.0 0 37 5 0.1 7 0.412 3 7 5 7 1 1.6 0 37 2 3 0.2 0 0.447 2 8 1 7 5 1.8 0 38 1 0.2 0 0.447 2 7 4 7 4 1.9 0 37 6 0.1 8 0.424 3 7 7 7 2 1.70 37 3 4 0.2 1 0.458 3 8 4 7 7 1.92 38 5 0.2 1 0.458 3 7 2 7 3 2.0 0 37 6 0.1 7 0.412 3 7 9 7 2 1.6 0 37 3 5 0.2 1 0.458 3 8 8 8 3 1.92 38 2 0.2 1 0.458 3 7 2 7 1 2.0 0 37 3 0.1 6 0.400 0 8 0 7 4 1.5 0 37 4 6 0.1 8 0.424 3 8 9 8 4 1.6 5 38 3 0.2 0 0.447 2 7 0 6 8 1.9 0 37 1 0.1 5 0.387 3 8 1 7 5 1.4 5 37 3 7 0.1 5 0.387 3 9 0 85 1.4 0 38 2 0.1 7 0.412 3 7 1 6 8 1.6 0 36 8 0.1 2 0.346 4 8 1 7 6 1.1 5 37 2 8 0.1 1 0.3317 9 1 85 1.0 0 38 1 0.1 2 0.346 4 7 2 6 8 1.2 0 36 7 0.1 0 0.316 2 8 1 7 6 0.9 5 35 7 b 1 0.1 4 0.374 2 8 8 8 6 1.3 0 36 7 0.1 5 0.387 3 6 9 6 8 1.45 35 8 0.1 2 0.346 4 7 8 7 7 1.1 5 36 9 2 0.1 7 0.412 3 9 3 8 7 1.5 6 38 5 0.1 7 0.412 3 7 2 6 8 1.6 0 37 1 0.1 6 0.400 0 8 1 7 7 1.5 5 36 6 3 0.2 0 0.447 2 9 4 8 8 1.8 0 38 6 0.2 0 0.447 2 7 3 6 9 1.9 0 37 5 0.1 8 0.424 3 8 3 7 8 1.7 0 37 4 4 0.1 8 0.424 3 95 8 9 1.65 38 6 0.1 7 0.412 3 7 2 6 8 1.6 0 37 6 0.1 7 0.412 3 8 3 7 8 1.6 0 37 5 5 0.1 8 0.424 3 95 9 0 1.6 5 38 6 0.2 0 0.447 2 7 1 6 7 1.9 0 37 6 0.1 5 0.387 3 8 3 7 9 1.4 5 37 5 6 0.2 0 0.447 2 9 6 9 1 1.8 0 38 5 0.2 0 0.447 2 7 2 6 8 1.9 0 37 6 0.1 5 0.387 3 8 3 7 9 1.4 5 37 5 7 0.1 5 0.387 3 9 6 9 1 1.40 38 3 0.1 9 0.435 9 7 3 6 8 1.8 0 37 6 0.1 2 0.346 4 8 2 7 9 1.1 5 37 4 8 0.1 2 0.346 4 9 7 9 2 1.1 2 38 2 0.1 7 0.412 3 7 3 6 8 1.6 0 36 4 0.1 2 0.346 4 8 4 8 0 1.1 5 37 4 AV G 0.1 7 0.412 8 L86. 8 1.57 38 1 0.1 8 0.423 5 71. 2 1.76 37 1 0.1 5 0.384 3 78. 0 1.42 37 1

### ENS R Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L Correcte d F H + B H H g Elemen t Sampl e

H g Fi d Bl k

H g Defaul t

Valu e (a) H g 5%

o f Sampl e H g Correcte d

Fron tHal f M g Sampl e Fi d Bl k M S Defaul t

Valu e H g 5%

o f Sampl e Correcte d

Bac k Hal f H g TOTA L

Correcte d F H + B H H g Silve r(Ag ) 0.0 0 0.0 0 13.78 0.0 0 0.0 0 0.0 0 1.0 0 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Arseni c(As ) 9.2 6 0.7 6 * 13.78 0.4 6 8.5 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 8.5 0 Bariu m (Ba ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Berylliu m (Be ) 0.1 0 (0.10 ) 13.78 0.0 1 0.1 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.1 0 Cadmiu m (Cd ) 0.6 8 0.34 * 13.78 0.0 3 0.3 4 0.0 0 0.0 0 1.00 

### - 0.0 0 0.3 4 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - 0.0 0 0.0 0 Chromiu m (Cr) 17.7 0 1.0 1 * 13.78 0.8 9 16.69 0.0 0 0.0 0 1.0 0 

### - 0.0 0 16.6 9 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0,0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.7 8 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Lea d (Pb ) 23.9 0 2.7 0 * 13.78 1.20 21.2 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 21.2 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 0.0 0 0.0 0 0.0 0 LO O 

### - 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 - - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Zin c(Zn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0

- - 0.0 0 0.0 0 I fFH B i s betwee n 0 t

o 1 3 .78 u g use blan k

valu e to correc

t I fFH B > 13.78 u g the n us e th e greate ro f13.7 8 u g o rth e lesse rvalu e betwee n FH B o r5 % o fFH S
.

* - valu e use d fo rblan k

correctio n MERCURY : (a) - base d o n a3.5 4 - in
. filtersiz e I fBH B i s > 0 but< = I u g the n use th e BH B valu e t o correc t I fBH B i s > 1 (i g use th e greate ro feithe r1 n g o r5 % o fB H ( ) No tDetecte d /

Reportabl e Detectio n Limi t

Mercury Fractio n Sampl e

H g Fi d Bl k

t' g Defaul t

Valu e H g 5%

o f Sampl e H g Correcte d

Amoun tH g H g FRON THAL F (0.03 ) (0.03 ) 6.0 0 (0.00 ) (0.03 ) BAC KHAL F 97.3 3 0.0 4 * 6.0 0 4.8 7 97.2 9 

# I I TOTA LH g 97.2 9 

### CLIEN T: Ony xEnvironmenta l Service , Inc
. PROGRA M : Fixe d Heart h Kil n # 3 RU N NO
. Ru n 1

I fF B i s >0 bu t<=

6 n g the n us e th e F B valu e to correc t I fF B i s >6 (i g us e th e greate ro feithe r6 u g o r5 % o fF H ( ) No tDetecte d / Reportabl e Detectio n Limi t * Indicate s valu e use d fo rblan k correctio n

### ENS R Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L Correcte d F H + B H M g Elemen t Sampl e

u g Fi d Bl k

u g Defaul t

Valu e (a) u g 5 % o f

Sampl e u g Correcte d

Fron tHal f u g Sampl e

u g Fi d Bl k

u g Defaul t

Valu e u g 5 % o f

Sampl e Correcte d

Bac k Hal f u g TOTA L

Correcte d F H + B H M g Silve r(Ag ) 0.0 0 0.0 0 13.78 „ 0.0 0 0.0 0 0.0 0 1.0 0 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Arseni c(As ) 249.0 0 0.7 6 * 13.78 12.45 248.2 4 0.0 0 0.0 0 1.00 

### - 0.0 0 248.2 4 Bariu m (Ba ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Berylliu m (Be ) 0.1 0 (0.10 ) 13.78 0.0 1 0.1 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.1 0 Cadmiu m (Cd ) 1.3 8 0.3 4 * 13.78 0.0 7 1.0 4 0.0 0 0.0 0 1.0 0 

### - 0.0 0 1.04 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Chromiu m (Cr ) 29.0 0 1.0 1 * 13.78 1.4 5 27.9 9 0.0 0 0.0 0 1.0 0 

### - 0.0 0 27.9 9 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 — 0.0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Lea d (Pb ) 22.3 0 2.7 0 * 13.78 1.1 2 19.6 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 19.6 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 „ 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 — 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 — 0.0 0 0.0 0 Zin c(Zn ) 0.0 0 0.0 0 13.78


### - 0.0 0 0.0 0 0.0 0 1.00


### - 0.0 0 0.0 0 I fFH B i s betwee n 0 t

o 13.78 n g us e blan k

valu e t o correc t I fFH B > 13.78 u.gthe n us e th e greate ro f13.78 n g o rth e lesse rvalu e betwee n FH B o r5 % o fFH S
.

* - valu e use d fo rblan k

correctio n (a) - base d o n a3.5 4 - in
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e 

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Amoun tH g u g 

### CLIEN T: Ony xEnvironmenta l Service , Inc
.

PROGRA M : Fixe d Heart h Kil n # 3 RU N NO
. Ru n 2 FRON THAL F 0.1 0 (0.03 ) 6.0 0 0.0 1 0.1 0 

### CLIEN T: Ony xEnvironmenta l Service , Inc
. PROGRA M : Fixe d Heart h Kil n # 3 RU N NO
. Ru n 2 BAC KHAL F 121.2 3 0.0 4 * 6.0 0 6.0 6 121.1 9 

### CLIEN T: Ony xEnvironmenta l Service , Inc
. PROGRA M : Fixe d Heart h Kil n # 3 RU N NO
. Ru n 2
| TOTA LH g 121.2 9 

### CLIEN T: Ony xEnvironmenta l Service , Inc
. PROGRA M : Fixe d Heart h Kil n # 3 RU N NO
. Ru n 2

I fF B i s >0 bu t<=

6 n g the n us e th e F B valu e t o correct I fF B i s > 6 n g us e th e greate ro feithe r6 n g o r5 % o fF H ( ) NotDetecte d / Reportabl e Detectio n Limi t * Indicate s valu e use d fo rblan k correctio n

### ENS R Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L
Elemen t Sampl e Fi d Bl k u g Defaul t

Valu e (a) u g 5 % o f

Sampl e u g Correcte d

Fron tHal f u g Sampl e

u g Fi d Bl k

u g Defaul t

Valu e u g 5 % o f

Sampl e u g Correcte d

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F H + B H Mg Silve r(Ag ) 0.0 0 0.0 0 13.78 . . 0.0 0 0.0 0 0.0 0 1.0 0

_. 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 0.0 0 0.0 0 Arseni c(As ) 946.0 0 0.7 6 * 13.78 47.3 0 945.2 4 0.0 0 0.0 0 1.0 0 

### - 0.0 0 945.2 4 Bariu m (Ba ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Berylliu m (Be ) 0.1 0 (0.10 ) 13.78 0.0 1 0.1 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.1 0 Cadmiu m (Cd ) 2.7 6 0.3 4 * 13.78 0.1 4 2.4 2 0.0 0 0.0 0 1.0 0 

### - 0.0 0 2.4 2 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - - 0.0 0 0.0 0 Chromiu m (Cr ) 55.8 0 1.0 1 * 13.78 2.7 9 54.7 9 0.0 0 0.0 0 1.00 

### - 0.0 0 54.7 9 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Lea d (Pb ) 40.6 0 2.7 0 * 13.78 2.0 3 37.9 0 0.0 0 0.0 0 i.0 0 

### - 0.0 0 37.9 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Zin c(Zn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 0.0 0 0.0 0 I fFH B i s betwee n 0 to 13.78 p g use blan k valu e to correct I fFH B > 13.78 p g the n us e th e greate ro f13.7 8 u g o rth e lesse rvalu e betwee n FH B o r5 % o fFH S
.

* - valu e use d fo rblan k

correctio n MERCURY : (a) - base d o n a3.5 4 - in
. filte rsiz e i fBH B i s >0 but<= 1 p g the n us e th e BH B valu e to correc t I fBH B i s > 1 p g us e th e greate ro feithe r1 p g o r5% o fB H ( ) No tDetecte d /

Reportabl e Detectio n Limi t

Mercury Fractio n Sampl e

u g Fi d Bl k

u g Defaul t

Valu e Mg 5%

o f Sampl e Mg Correcte d

Amoun tH g Mg FRON THAL F 0.2 7 (0.03 ) 6.0 0 0.0 1 0.2 7 BAC KHAL F 89.1 2 0.0 4 * 6.0 0 4.4 6 89.0 8 

# I I TOTA LH g 89.3 5 

### CLIENT : PROGRAM : RU N NO
. Ony xEnvironmenta l Service , Inc
.

Fixe d Heart h Kil n #

3 Ru n 3

I fF B i s >0 bu t<=

6 p g the n us e th e F B valu e t o correct I fF B i s >6 p g us e th e greate ro feithe r6 p g o r5 % o fF H ( ) No tDetecte d / Reportabl e Detectio n Limi l * Indicate s valu e use d fo rblan k correctio n

# E N S
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. Whe n les s tha n 4% , difference betwee n reading s shal l b e 0.2 % o rless
. Whe n greate rtha n o requa l to 15% , difference betwee n reading s shal l be 0.2 % o rless
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.

Net0 2

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# Jun e 200 6 Tes t

# Particulat e Matte rDat a

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 5 Samplin g Parameter s Ru n No
. 

### Ru n 1 Ru n 2 Ru n 3 

### AVG S Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### AVG S Star tTim e 

### Unit s 15:1 2 10:0 6 10:0 6 

### AVG S Sto p Tim e 17:2 9 12:2 9 12:4 4 Nozzl e Diamete r inche s 0.43 1 0.43 1 0.43 1 0.43 1 Barometri cPressur e !.n-Hf l 29.5 5 29.5 5 29.5 0 29.5 3 Ne tSamplin g Tim e mm . 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dcf 78.24 4 82.90 2 81.74 5 80.96 4 Avg
. DG M Temp
. ° F 110. 6 111. 2 109. 0 110. 3 Av g Delt aH i n H 2 

### 0 1.3 1 1.4 3 1.4 1 1.3 8 Av g Delt aH ! n 

### ,.H.g
. 0.096 4 0.104 9 0.103 4 0.101 6 DG M Calibratio n Facto r 1.007 0 1.007 0 1.007 0 1.007 0 Ga s Sampl e Volume 

### dsc f 72.24

7 76.48

2 75.57

3 74 .768 Tota l Wate rCollecte d m L 1341. 0 1487. 9 1340. 1 1389. 7 Volum e o fWate rVapo r sc f 63.22 8 70.15 4 63.18 6 65.52 3 Moistur e (measured ) % v/v 46. 7 47. 8 45. 5 46. 7 Moistur e ( @ saturation ) % v/v 101. 3 101. 3 1 

### 101. 5 101. 3 DryMol e Fraction , 100-% M -- 0.533 3 0.521 6 0.544 6 0.533 2 C 0 2

### atStac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 O z

### atStac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C O + N 2 

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### 29.5 8 29.5 4 29.5 7 29.5 7 We tMolecula rWeigh t Ib/lb-mol e 

### 24.1 8 24.0 2 24.3 0 24.1 7 Exces s Ai ratStac k % 84. 7 58. 5 78. 0 73. 7 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 

### 0 -0.1 5 -0.1 5 -0.1 3 -0.1 4 Stac k Pressur e 

# !. n 

# ..-..E a 29.5 4 29.5 4 29.4 9 29.5 2 Avg
. Stac k

Temp
. ° F 386. 2 387. 9 385. 9 386. 6 Avg
. Sqroo tofDelt aP - - 0.370 1 0.392 2 0.393 0 0.385 1 SD E Averag e 

# - 10.76 5 11.42 0 11.42 9 11.20 5 Pito tCoefficien t ~ 

### 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,73 6 1,84 7 1,84 0 1,80 8 Stac k Flowrat e we tacf m 14,39 9 15,32 6 15,26 2 14,99 6 Stac k Flowrat e we tscf m 8,87 0 9,42 2 9,39 0 9,22 8 

### Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic s % 10 4 

### 10 6 10

1 10

4 Mete rBo xNo
. — 

### 8075 4 8075 4 8075 4 — 

### Delt aH @ i n H 2 

### 0 1.83 2 1.83 2 1.83 2 

# - Fiel d Q AYq c ~ 

### i.006 6 0.991 8 0.997 4 0.998 6 [Deviation ] Pre- Y % 0.04 % 1.51 % 0.95 % 0.84 % S:VJOB\2006\Onyx\Performanc e TesftTes tDataVJun e 2006\2n d Retesft[PM.xlsJDAT A

### Metho d 5 Samplin g Parameter s

P T Run l Ru n 2 Ru n 3 P T Delt aP SQR

T Delt aP DGM

IN DGM OU T Delt

aH STACK TEM P Delt

aP SQR

T Delt aP DGM

IN DGM OU T Delt aH STACK TEM P DeliaP SQR T Delt aP DGM

I N DGM OU T DeliaH STACK

TEM P a 1 0.0 7 0.264 6 10 4 10 2 0.6 6 38 2 0.1 0 0.316 2 10 2 9 9 0.9 2 38 2 0.1 7 0.412 3 8 9 8 7 1.5 3 37 9 a 2 0.1 2 0.346 4 10 4 10 2 1.1 3 38 7 0.1 0 0.316 2 10 6 10 2 0.9 2 38 3 0.1 5 0.387 3 9 2 8 9 1.3 5 38 0 a 3 0.1 9 0.435 9 10 9 10 4 1.7 9 38 6 0.1 6 0.400 0 10 8 10 3 1.4 7 38 6 0.1 4 0.374 2 9 5 9 0 1.2 6 37 9 a 4 0.1 9 0.435 9 11 1 10 4 1.7 9 38 7 0.1 8 0.424 3 11 1 10 4 1.6 6 38 9 0.1 4 0.374 2 10 8 10 6 1.2 6 38 4 a 5 0.1 5 0.387 3 11 4 10 6 1.4 1 38 8 0.1 4 0.374 2 11 2 10 5 1.2 9 38 7 0.1 8 0.424 3 11 2 10 6 1.6 2 38 8 a 6 0.1 6 0.400 0 11 5 10 7 1.5 0 38 8 0.1 5 0.387 3 11 2 10 6 1.3 8 38 5 0.1 8 0.424 3 11 4 10 7 1.6 2 38 8 a 7 0.1 2 0.346 4 11 5 10 6 1.1 3 38 3 0.1 8 0.424 3 11 5 10 7 1.6 6 38 5 0.1 2 0.346 4 11 6 10 8 1.0 8 38 7 a 8 0.1 5 0.387 3 11 6 10 4 1.4 1 38 2 0.1 5 0.387 3 11 6 10 9 1.3 8 38 8 0.1 0 0.316 2 11 7 10 9 0.9 0 38 1 b 1 0.0 7 0.264 6 11 3 11 1 0.6 6 38 2 0.1 8 0.424 3 11 0 11 0 1.6 6 38 6 0.2 2 0.469 0 11 2 11 1 1.9 8 38 4 b 2 0.1 4 0.374 2 11 3 11 1 1.3 2 38 3 0.1 8 0.424 3 11 4 11 1 1.6 6 38 8 0.1 7 0.412 3 11 2 11 1 1.5 3 38 8 D 3 0.1 1 0.331 7 11 5 11 1 1.0 3 38 9 0.1 8 0.424 3 11 6 11 2 1.6 6 39 0 0.1 8 0.424 3 11 6 11 2 1.6 2 38 9 b 4 0.1 3 0.360 6 11 6 11 1 1.2 2 39 1 0.1 6 0.400 0 11 8 11 2 1.4 7 39 1 0.1 9 0.435 9 11 8 11 3 1.7 1 39 0 b 5 0.1 4 0.374 2 11 6 11 2 1.3 2 39 0 6 .1 8 0.424 3 11 9 11 3 1.6 6 39 2 0.1 8 0.424 3 12 0 11 4 1.6 2 39 0 b 6 0.1 5 0.387 3 11 6 11 2 1.4 1 38 7 0.1 6 0.400 0 12 1 11 4 1.4 7 39 5 0.1 6 0.400 0 12 0 11 5 1.4 4 39 2 b 7 0.1 7 0.412 3 11 7 11 2 1.6 0 38 8 0.1 4 0.374 2 12 1 11 4 1.2 9 39 2 0.1 2 0.346 4 12 0 11 5 1.0 8 39 1 b 8 0.1 7 0.412 3 11 7 11 2 1.6 0 38 6 0.1 4 0.374 2 12 2 11 5 1.2 9 38 7 0.1 0 0.316 2 12 0 11 5 0.9 0 38 4


### AV G 0.1 4 0.370 1 110. 6 1.3 1 38 6 0.1 6 0.392 2 111. 2 1.4 3 38 8 0.1 6 0.393 0 109. 0 1.4 1 38 6

### ENS R Samplin g Trai n Ru n Numbe r Clicu l FacilityLocatio n Source Dat e , Operato r Slac k Dia . - In . Star t Tim e Slo p Time 

### E P A ISOKINETI C SAMPLIN G- FIEL D DAT A SHEE T



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## 7.1 1- 1

Fina l Purg e Rate

# Metal s Dat a

### Veoli aE S Technica l Solution s Fixe d Heart h Incinerato rUni t3 Metho d 006 0 (Metals ) Samplin g Parameter s Ru n No
. 

### Ru n 1 Ru n 2 Ru n 3


### AVG S Dat e 19-Jun-0 6 20-Jun-0

6 21-Jun-0

6 

### AVG S Star tTim e 

### Unit s 15:1 2 10:0 6 10:0 6 

### AVG S Sto p Tim e 17:2 9 12:2 9 12:4 4 Nozzl e Diamete r inche s 0.43 1 0.43 1 0.43 1 0.43 1 Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dcf 78.24 4 82.90 2 81.74 5 80.96 4 Avg
. DG M Temp
. ° F 110. 6 111. 2 109. 0 110. 3 Av g Delt aH i n H 2 

### 0 1.3 1 1.43 1.4 1 1.3 8 Av g Delt aH in
. H g 0.096 4 0.104 9 0.103 4 0.101 6 DG M Calibratio n Facto r 1.007 0 1.007 0 1.007 0 1.007 0 Ga s Sample Volum e 

### dsc f 72.24 7 76.48 2 75 .57 3 74 .768 Tota l Wate rCollecte d m L 1341. 0 1487. 9 1340. 1 1389. 7 Volum e ofWate rVapo r sc f 63.22 8 70.15 4 63.18 6 65.52 3 Moistur e (measured ) % v/ v 46. 7 47. 8 45. 5 46. 7 Moistur e ( @ saturation ) % v/ v 101. 3 101. 3 101. 5 101. 3 Dr yMol e Fraction , 100-% M — 

### 0.533 3 0.521 6 0.544 6 0.533 2 C 0 2

### a tStac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 0 2

### atStac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C O + N 2 

### %dr y 82.6 0 84.2 0 83.0 0 83.2 7 Dr yMolecula rWeigh t Ib/lb-mole 29.5 8 29.5 4 29.5 7 29.5 7 We tMolecula rWeigh t Ib/lb-mole 24.1 8 24.0 2 24.3 0 24.1 7 Exces s Ai ratStac k / o 84. 7 58. 5 78. 0 73. 7 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 

### 0 -0.1 5 -0.1 5 -0.1 3 -0.1 4 Stac k Pressur e in
. H g 29.5 4 29.5 4 29.4 9 29.5 2 Avg
. Stac k

Temp
. ° F 386. 2 387. 9 385. 9 386. 6 Avg
. Sqroo tofDelt aP — 

### 0.370 1 0.392 2 0.393 0 0.385 1 SD E Averag e — 

### 10.76 5 11.42 0 11.42 9 11.20 5 Pito tCoefficien t — 

### 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,73 6 1,84 7 1,84 0 1,80 8 Stac k Flowrat e we tacf m 14,39 9 15,32 6 15,26 2 14,99 6 Stac k Flowrat e wetscf m 8,87 0 9,42 2 9,39 0 9,22 8 Stac k Flowrat e 

### dscfm 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic

s % 

### 10 4 10 6 10 1 

### 10 4 Mete rBo xNo
. - - 

### 8075 4 8075 4 8075 4 

# - Delt aH @ inH z 

### O 1.832 0 1.832 0 1.832 0 

# - Fiel d Q AYq c — 

### 1.006 6 0.991 8 0.997 4 0.99 9 ^Deviation ] Pre- Y % 0.04 % 1.51 % 0.95 % 0.8 %

### Metho d 006 0 (Metals ) Samplin g Parameter s

P T 

### Ru n 1 AVGS--METAL S Ru n 2 AVG S - -METAL S Ru n 3 AVGS--METAL S P T Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH STAC K

TEM P Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH STAC K

TEM P Delt aP SQR T

Delt aP DG M

I N DG M OU T Delt aH STAC K

TEM P a 1 0.0 7 0.264 6 10 4 10 2 0.6 6 38 2 0.1 0 0.316 2 10 2 9 9 0.9 2 38 2 0.1 7 0.412 3 8 9 8 7 1.5 3 37 9 2 0.1 2 0.346 4 10 4 10 2 1.1 3 38 7 0.1 0 0.316 2 10 6 10 2 0.9 2 38 3 0.1 5 0.387 3 9 2 8 9 1.3 5 38 0 3 0.1 9 0.435 9 10 9 10 4 1.7 9 38 6 0.1 6 0.400 0 10 8 10 3 1.47 38 6 0.1 4 0.374 2 9 5 9 0 1.2 6 37 9 4 0.1 9 0.435 9 11 1 10 4 1.7 9 38 7 0.1 8 0.424 3 11 1 10 4 1.6 6 38 9 0.1 4 0.374 2 10 8 10 6 1.2 6 38 4 5 0.1 5 0.387 3 11 4 10 6 1.4 1 38 8 0.1 4 0.374 2 11 2 10 5 1.2 9 38 7 0.1 8 0.424 3 11 2 10 6 1.62 38 8 6 0.1 6 0.400 0 11 5 10 7 1.5 0 38 8 0.1 5 0.387 3 11 2 10 6 1.38 38 5 0.1 8 0.424 3 11 4 10 7 1.62 38 8 7 0.1 2 0.346 4 11 5 10 6 1.1 3 38 3 0.1 8 0.424 3 11 5 10 7 1.6 6 38 5 0.1 2 0.346 4 11 6 10 8 1.0 8 38 7 8 0.1 5 0.387 3 11 6 10 4 1.4 1 38 2 0,1 5 0.387 3 11 6 10 9 1.38 38 8 0.1 0 0.316 2 11 7 10 9 0.9 0 38 1 b 1 0.0 7 0.264 6 11 3 11 1 0.6 6 38 2 0.1 8 0.424 3 11 0 11 0 1.6 6 38 6 0.2 2 0.469 0 11 2 11 1 1.9 8 38 4 2 0.1 4 0.374 2 11 3 11 1 1.32 38 3 0.1 8 0.424 3 11 4 11 1 1.6 6 38 8 0.1 7 0.412 3 11 2 11 1 1.5 3 38 8 3 0.1 1 0.331 7 11 5 11 1 1.0 3 38 9 0.1 8 0.424 3 11 6 11 2 1.6 6 39 0 0.1 8 0.424 3 11 6 11 2 1.62 38 9 4 0.1 3 0.360 6 11 6 11 1 1.22 39 1 0.1 6 0.400 0 11 8 11 2 1.47 39 1 0.1 9 0.435 9 11 8 11 3 1.7 1 39 0 5 0.1 4 0.374 2 11 6 11 2 1.32 39 0 0.1 8 0.424 3 11 9 11 3 1.66 39 2 0.1 8 0.424 3 12 0 11 4 1.62 39 0 6 0.1 5 0.387 3 11 6 11 2 1.4 1 38 7 0.1 6 0.400 0 12 1 11 4 1.47 39 5 0.1 6 0.400 0 12 0 11 5 1.44 39 2 7 0.1 7 0.412 3 11 7 11 2 1.6 0 38 8 0.1 4 0.374 2 12 1 11 4 1.2 9 39 2 0.1 2 0.346 4 12 0 11 5 1.0 8 39 1 8 0.1 7 0.412 3 11 7 11 2 1.6 0 38 6 0.1 4 0.374 2 12 2 11 5 1.2 9 38 7 0.1 0 0.316 2 12 0 11 5 0.9 0 38 4 AV G 0.1 4 0.370 1 110. 6 1.3 1 38 6 0.1 6 0.392 2 111. 2 1.43 38 8 0.1 6 0.393 0 109. 0 1.4 1 | 38 6

## ENS R 

# AECO M Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L
Elemen t Sampl e H g Fi d Bl k

H g Defaul t

Valu e (a) H g 5 % o f

Sampl e H g Correcte d

Fron tHal f H g Sampl e

H g Fi d Bl k

H g Defaul t

Valu e H g 5 % o f

Sampl e Hg Correcte d

Bac k Hal f HS Correcte d

F H + B H H g Silve r(Ag ) 0.0 0 0.0 0 13.78 „ 0.0 0 0.0 0 0.0 0 1.0 0 _ 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Arseni c(As ) 5.8 1 0.6 1 * 13.78 0.2 9 5.2 0 0.3 3 0.0 0 1.00 0.0 2 0.3 3 5.5 3 Bariu m (Ba ) 0.0 0 0.0 0 13.7 8 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

## - 0.0 0 0.0 0 Berylliu m (Be ) 0.0 0 0.0 0 13.7 8 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Cadmiu m (Cd ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

## - 0.0 0 0.0 0 Chromiu m (Cr ) 9.64 0.7 9 * 13.78 0.4 8 8.8 5 1.0 6 0.0 0 1.0 0 0.0 5 1.06 9.9 1 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.78 

## - 0.0 0 0.0 0 0.0 0 1.0 0 - 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - 0.0 0 0.0 0 Lea d (Pb ) 0.0 0 0.0 0 13.78 

## - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 — 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 — 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Zin c(Zn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

## - 0.0 0 0.0 0 I fFH B i s betwee n 0 to 13.7 8 |i g us e blan k valu e to correct I fFH B > 13.78 u.g the n us e th e greate ro f13.78 p g o rth e lesse rvalu e betwee n FH B o r5% o fFH S
.

* - valu e use d fo rblan k

correctio n MERCURY : (a) - base d o n a3.5 4 - in
. filtersiz e I fBH B i s > 0 bu t<= 1 p g the n us e th e BH B valu e t o conect I fBH B i s > 1 n g us e th e greate ro feithe r1 (i g o r5 % o fB H ( ) No tDetecte d /

Reportabl e Detectio n Limi t

Mercury Fractio n Sampl e H g Fi d Bl k

H 8 Defaul t

* Valu e H g 5 % o f

Sampl e H g Correcte d

Amoun tH g H g FRON THAL F 0.0 0 0.0 0 6.0 0 0.0 0 0.0 0 BAC KHAL F 0.0 0 0.0 0 6.0 0 0.0 0 0.0 0 

# I I TOTA LH g 0.0 0 

### CLIEN T: Veoli aE S Technica l Solution s PROGRA M : Fixe d Heart h Incinerato rUni t3 R U N 

### NO
. Ru n 

### 1

I fF B i s >0 bu t<=

6 p g the n us e th e F B valu e t o correct I fF B i s >6 n g us e th e greate ro feithe r6 p g o r5% o fF H ( ) NotDetecte d / Reportabl e Detectio n Limi t * Indicate s yalu e use d fo rblan k correctio n

# ENS R AECO i Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L
Elemen t Sampl e H g Fi d Bl k

H g Defaul t

Valu e (a) H g 5 % o f

Sampl e H g Correcte d

Fron tHal f H g Sampl e

H g Fi d Bl k

H g Defaul t

Valu e H g 5 % o f

Sampl e Hg Correcte d

Bac k Hal f H g Correcte d

F H + B H H 6 Silve r(Ag ) 0.0 0 0.0 0 13.78 0.0 0 0.0 0 0.0 0 1.00

_ . 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - - 0.0 0 0.0 0 Arseni c(As ) 4.3 0 0.6 1 * 13.78 0.2 2 3.6 9 0.0 0 0.0 0 1.0 0 

### - 0.0 0 3.6 9 Bariu m (Ba ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Berylliu m (Be ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.C 9 0.0 0 1.00 0.0 0 0.0 9 0.0 9 Cadmiu m (Cd ) 0.0 0 0.0 0 13,78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Chromiu m (Cr ) 3.9 8 0.7 9 * 13.78 0.2 0 3.1 9 0.6 6 0.0 0 1.0 0 0.0 3 0.6 6 3.8 5 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0,0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.7 8 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Lead(Pb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 ' 

### - 0.0 0 0.0 0 0.0 0 LO O
- - 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - 0.0 0 0.0 0 Zin c(Zn ) 0.0 0 0.0 0 13.78


### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 I fFH B i s betwee n 0 t

o 13.78 p g us e blan k

valu e to correct I fFH B > 13.78 p g the n us e th e greate ro f13.78 p g o rth e lesse rvalu e betwee n FH B o r5 % o fFH S
.

* - valu e use d fo rblan k

correctio n MERCURY : (a) - base d o n a3.5 4 - in
. Filte rsiz e I fBH B i s > 0 bu t<= 1 p g the n us e th e BH B valu e to correc t I fBH B i s > 1 p g us e th e greate ro feithe r1 p g o r5 % o fB H ( ) No tDetecte d /

Reportabl e Detectio n Limi t

Mercury Fractio n Sampl e H g Fi d Bl k

H g Defaul t

Valu e H g 5 % o f

Sampl e H g Correcte d

Amoun tH g H g FRON THAL F 0.0 0 0.0 0 6.0 0 0.0 0 0.0 0 BAC KHAL F 0.0 0 0.0 0 6.0 0 0.0 0 0.0 0

1 TOTA LH g 0.0 0 

### CLIEN T: Veoli aE S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato rUni t3 RU N NO
. Ru n 2

I fF B i s >0 bu t<=

6 p g the n use th e F B valu e to correct I fF B i s >6 p g use th e greate ro feithe r6 p g o r5% o fF H ( ) No tDetecte d / Reportabl e Detectio n Limi t * Indicate s valu e use d fo rblan k correctio n

## ENS R 

# AECO I Multi-Metal s Blan k Correctio n
FRON THAL F BAC KHAL F TOTA L
Elemen t Sampl e H g Fi d Bl k

H g Defaul t

Valu e (a) H g 5%

o f Sampl e H g Correcte d

Fron tHal f H g Sampl e

H g Fi d Bl k

H g Defaul t

Valu e H g 5 % o f

Sampl e Hg Correcte d

Bac k Hal f H g Correcte d

F H + B H H g Silve r(Ag ) 0.0 0 0.0 0 13.78 _ 0.0 0 0.0 0 0.0 0 1.0 0 _ 0.0 0 0.0 0 Aluminu m (Al ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 - 0.0 0 0.0 0 Arseni c(As ) 5.6 0 0.6 1 * 13.78 0.2 8 4.9 9 0.2 1 0.0 0 1.00 0.0 1 0.2 1 5 .2 0 Bariu m (Ba ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Berylliu m (Be ) 0.0 0 0.0 0 13.78 _ 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Cadmiu m (Cd ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Cobal t(Co ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Chromiu m (Cr) 11.1 0 0.7 9 * 13.78 0.5 6 10.3 1 0.8 4 0.0 0 1.00 0.0 4 0.84 11.1 5 Coppe r(Cu ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 

### - 0.0 0 0.0 0 Manganes e (Mn ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Nicke l (Ni ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 LOO 

### - 0.0 0 0.0 0 Lea d (Pb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.00 - 0.0 0 0.0 0 Antimon y(Sb ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 LOO 

### - 0.0 0 0.0 0 Seleniu m (Se ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 LOO 

### - 0.0 0 0.0 0 Thalliu m (Tl ) 0.0 0 0.0 0 13.78 

### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 Vanadiu m (V ) 0.0 0 0.0 0 13.78 

### - 0,0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0

- Zin c(Zn ) 0.0 0 0.0 0 13.78


### - 0.0 0 0.0 0 0.0 0 1.0 0 

### - 0.0 0 0.0 0 I fFH B i s betwee n 0 to 13.7 8 p g us e blan k valu e to correct I fFH B > 13.78 p g the n us e th e greate ro f13.78 p g o rth e lesse rvalu e betwee n FH B o r5 % o fFH S
.

* - valu e use d fo rblan k

correctio n MERCURY : (a) - base d o n a3.5 4 - in
. filte rsiz e I fBH B i s >0 bu t<= 1 p g the n us e th e BH B valu e to correc t I fBH B i s > 1 p g use th e greate ro feithe r1 p g o r5 % o fB H ( ) NotDetecte d /

Reportabl e Detectio n Limi t

Mercury Fractio n Sampl e H g Fi d Bl k

H g Defaul t

Valu e HS 5 % o f

Sampl e H g Correcte d

Amoun tH g H g FRON THAL F 0.0 0 0.0 0 6.0 0 0.0 0 0.0 0 BAC KHAL F 0.0 0 0,0 0 6.0 0 0.0 0 0.0 0



# ! TOTA LH g 0.0 0 

### CLIENT : Veoli aE S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato rUni t3 RU N NO
. Ru n 3

I fF B i s > 0 bu t<=

6 p g the n us e th e F B valu e to correct I fF B i s >6 p g us e th e greate ro feithe r6 p g o r5 % o fF H ( ) No tDetecte d / Reportabl e Detectio n Limi t * Indicate s valu e use d fo rblan k correctio n

### ENS R j ALC.Oiv i EF AISOKINETI C SAMPLIN G -FIEL D DAT ASHEE T : : : JMPiJ«;Kftvoi' &: : 1 Orsa t Samplin g Trai n f\ Barometri cPressur e J ^ ,5 5 LEA KCHECK S I n "H g x-iwrr.x- x :TJNXL:::- : tRINS E :co2 : or Ku n Numbe r(K{ Stati cPressur e (+/- ) — 

### n INITIA LVAC
. (C
. In
. CF M •oc/- l /0£, 0 j/ 7 5 Clien t ProbeyPlto tNumbe rf\S

' MI D VAC
. In
. CF M 7 5 FacilityLocatlo u U N . i i 3- Wt£. f, X L PitotCoefficicu t 

### •S' l
. . . FINA LVAC
. In
. CF M . 0 0 ' 10. 0 Source Kille rBo xNo
. 

### U B +/- / + - < 0 1 Vo o 10. 0 Dat e Of, - Mete rBo i No
. fioTSM INIT
. PITO T* * FINA LPITO T T T loo Operato r Cf
. til, - AU S J Orific e Coefficien t(V ) | .OP" ? FILTE R DAT A T T loo Slac k Ula
. - lu
. 1 ? " DeltaH (ii; 1.9,33 1 I : :NOMBER : T.ARf c • Star tTim e 

### 3( 3 /fill
. Nozzl e Slie/No
. 

### •M* l Sto p Tim e XA D Thermocoupl e ID : - — : ::--.-:SIUCASEL:-:-:-:- : 1 Fina l Purg e Rate Im p OutletT C ID : L I - 

### u Fina l P H SAMPLE ; CLOC K VELOCIT Y ORitflCr ! C A SMETE R TEMPERATUR E READINGS
. ° F PUM P POIN T XJM K MJETTKRVOL
. VOLUM E OR (S4ifiJ$:: ; VACUUM ; Oel/iiP , I n w

c l>e|ffiH,ln* c r e STAC K PROH E IMPIfWiE K •N fed* 0 o i 

### 2M 1 — bl 102 

# r 2 •\ a M X 

### <}<?/.lo J O ? W — 

## foH \b1 

### i 3 I S 

### •t s n q 

### 2 ^ 2 £\ 2 * 3 — /<5 < 7 

### ioo l
. 9 3 8 1 

### AU G 3 ^ —" 

### 5f t 

## IM lo<-( J i 1 5 i q ( 1* 9 — 

## lob 3

3 1 5 

### •i t I-5 D lfl ? 9 AS S a m V\K — 

### M l >C 7 

### 3 1 

### ^ 5 1.( 3 10( 5 

### . 0 XH1 

# - 16 6 I T 

## \.H( l o JJ.< ? J&A
. 23 § — 

### lo w R ( 6 0 

## • 

## lob lon
. 1 as a 6 ( I K a 61
. S •i f 1,3 2 / o 31. 5 

### 32. 3 — 

### S O 11 3 

### l/ l

• n 

### 1.0 3 J8< ? S o M S II I Si T M l 

### ,oqo.< ? A

## HI — 

### 5"/ uc» K I 5 9 0 • « " 

### i O %. 0 19 0 2HO 2H1 

### 5 3 K G t a 

## a.

I T 1.4

/ 1 0 SB- 4 38 7 

## US ZHO — 112 - 7 

### (0 5 U O 10 5 C •I 

## M$ — 

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### ^-<5..
. •1 7 \.L0 

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## TjH i n ^ ? r

• - '" - — r

• i !!;:•:::::•;:: : j:;;;:;;:!;:;::; ^

### ENS R EP AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n <H3 ^ Ru n Numbe r C'llcu t FacilityLocatio n Source Dat e 

### -E2
. /

fU WjeVr - , I L Barometri cPressur e Stati cPressur

e 07- ) Probe/PilotNumbe r PilotCoefficien t
_ Filte rBo xNo
. Mete rBo xNo
. 

### ^5-1- B

•JtL ..HfiJ L _aeis! L LEA KCHECK S l a"H g

INITIA LVAC
. | fIn
. CF M '.Q 6 3 MI D VAC
. lu
. CF M FINA LVAC
. ~J

+ INIT
. PITO T CF M •j .QQ l FINAL PITO

Tj/'t X FILTE R DAT A Stack Dia
. - in
. V i " DeltaH (t t 

### 1.93

2 -XNUMBER-:- : :-::-TABE : Star tTim e 

### roo k Nozzl e Size/No
. Sto p Tim e XA D Thermocoupl e ID : Im p OullctT C ID : 

### H3o , a IMRINRBltVOt'S .

IMT: ! IP C Jc< ? 

### 56
_ TbTAX. •MMXL-:- : 

# 3 ^ RINS E

to o

SILIC AGE L SAMPL E ?QiN T t-'LOC K

XtM K VELOCIT Y

HEA D Delta? , I n W

f MBTKRVO L Pe|laH,|n* f CA S MfcfU R

VOLUM E r e TEMPERATUR E 

### READINGS , " F ttmr VACUU M 

### *r>H « COMMENT S SAMPL E ?QiN T t-'LOC K

XtM K VELOCIT Y

HEA D Delta? , I n W

f MBTKRVO L Pe|laH,|n* f CA S MfcfU R

VOLUM E r e STAC K OVE N IMPINGE * f!;||:li (^WE *8K!!!i: | 

### ttmr VACUU M 

### *r>H « COMMENT S SAMPL E ?QiN T t-'LOC K

XtM K VELOCIT Y

HEA D Delta? , I n W

f MBTKRVO L Pe|laH,|n* f CA S MfcfU R

VOLUM E r e STAC K OVE N IMPINGE * iliiiSillli r :i:;:i«)r|i1r;:i;; ; 

### ttmr VACUU M 

### *r>H « COMMENT S 

### A l 0 JOfVr , .77 A 2 S3
. 5 1 1 — 

### 2 l.< • 1 0 

### .q a 393
. — 

### & l 10 6 i 

## i< •If e 1015
. 2 

### 7<? k 

## stHo ZYf i 

## & 10 3 H 22.< 1-4 4 3 9 ^ 

## 2 HO 2 ^ 

### 5 7 (I I s I T 

### i.a q 3 2 7 

### 0H^ - 

### r« r 1( 1 io s l 11.< 1 5 1.3 9 loQ o - 9 J95 > 

## XH< 

# . ux /£>6 7 

### HC •1 8 1.6 6 

### /o<Jk
. | 5 3 / 0 7 

## 8 i).< \S * llo\ 8 

## no f « iit , l o ? Sk*Pfc / ( S HOf o 

### J H 

## LO •1 8 1-4 4 3 9 P I ? W H o n o T 

### a . - ty 

### 3S « 

## ?Hr> — 

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### « / H 3 |.4f e isn. » p ^ f M l 1 H A 

### 1 H u - r .» £ 1-H I 1133. 1 — 

### l 6 11 3 

### 5 s •W l . a aM I . a s i

9 7

### 5 it> l H 7 II3 N
. 5 p t MY
. 7 

### •N f l/Ji. S an a (2 ( I W fl . W H«W, 4 

# - 1 ^ uc 

### y

;

— i i i j -
—j_ , ., . 

## ! 1 Oru t C02 .02 : 7 - 6

Fina l Purg e Bate Fina l P H

### ENS R i Ai.CGrv , E P A ISOKINETI C SAMPLIN G- FIEL D DAT A SHEE T Samplin g Trai n Ru n Nu m be r Clicu t FacilityLocatlo u Sourc e Dat e Operato r Stack Ola
. - lu
. Star tTlin e Sto p Tim e 3 -fWM g 3 1 3 ^ " Barometri cPressur e Stati cPressure(•»/•

) - •| C Probe/Pleo

tNumbe r PitotCoefficien t Filte rBo * No
. Mete rBo i No
. Orific e Coefficien t(Y) DeltaI I (S > Noizl cSize/No , XA D Thcrmocoupi e ID : Im p OutletT C ID : LEA KCHECK S I n "H g INITIA LVAC
. It
. MI D VAC
. 

## MI FINAL VA C H , M ia. CF M •OOg L In. CF M CF M IN1T . PITO T FINA LPITO T 

### V A \0Q1 FILTE R DAT A 

## JUL : :NDMBER : : :-:-:-TXBE:-

X iMPixcEiivofs : : :

•.•ma,. 

### JJiR. FINA L

## /as

# zz z

SILIC AGEL : 

### mz, ?- 1 v3i T •RINS E O rsa t C02 : ::o2: - 7 M < U 

# 1 - 1 

# U I f 

### U
Fina l Purg e Rate Fina l P H SAMPLK : POIN T CLOC K

TSM E VELO C U V

HLA B OtUap,|ow c 

### MKT

HU. VOL Oe|taH,(B¥(c <

! A *METE R YOLOMF. f f 

### TEMPERATUR E READINGS , " F PROB E ORGSANf C MO^UUj : «A S METE R 

### . tf?ne VACUU M ^nnr i 1 1 I n i T i COMMENT S 

### A L 

## XL 

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2 s o 1/ 6 

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3

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J L < n c

IPS ' 

# 10, 5 13 0 •1 0 

### J^L L

I-oft 277. q 

### ,

3 1 0 A H

JiL L 2J±L S 3 

### J I L _liiL
. U S

T

4 -

# PCDD/PCD FDat a

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 0023 ASamplin g Parameter s Ru n No
. R u n 

### 1 Ru n 2 Ru n 3 AVG S Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### AVG S StartTim e Unit s 14:4 0 9:3 0 9:3 0 AVG S Sto p Tim e 17:5 9 13:0 5 11:4 3 Nozzl e Diamete r inche s 0.43 5 0.43 5 0.43 5 0.43 5 Barometri cPressur e in
. H g 29.5 5 29.5 0 29.5 0 29.5 2 Ne tSamplin g Tim e min
. 192. 0 192. 0 192. 0 192. 0 Volum e Metere d , dc f 135.21 5 136.33 1 133.04 6 134.86 4 Avg
. DG M Temp
. ° F 109. 3 [ ib'7. i 107. 9 108. 1 Av g Delt aH i n H a 

### O 1.7 1 1.74 1.6 7 1.7 1 Av g Delt aH in
. H g 0.125 7 0.128 2 0.122 5 0.125 5 DG M Calibratio n Facto r 

# - 1.032 0 1.032 0 1.032 0 1.032 0 Ga s Sampl e Volum e dscf 128.36 3 129.71 0 126.37 9 128.151 Tota l Wate rCollecte d m L 2171. 7 2509. 0 2250. 4 2310. 4 Volum e o

fWate rVapo r scf 102.39 6 118.29 9 106.10 6 108.93 4 Moistur e (measured ) % v/ v 44. 4 47. 7 45. 6 45. 9 Moistur e ( @ saturation ) % v/ v 101. 3 101. 5 101. 5 101. 4 Dr yMol e Fraction , 100-% M " 

### 0.556 3 0.523 0 0.543 6 0.541 0 C 0 2

### atStac k % d r y 7.4 0 7.6 0 7.4 0 7.4 7 6 2

### atStac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C O + N 2 

### %dr y 82.6 0 84.2 0 83.0 0 83.2 7 Dr yMolecula rWeigh t Ib/lb-mol e 

### 29.5 8 29.5 4 29.5 7 29.5 7 We tMolecula rWeigh t Ib/lb-mol e 

### 24.4 4 24.0 4 24.2 9 24.2 6 Exces s Ai ra

tStac k % 84. 7 58. 5 78. 0 73. 7 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 

### 0 -0.1 3 -0.1 5 -0.1 7 -0.1 5 Stac k Pressur e in
. H g 29.5 4 29.4 9 29.4 9 29.5 1 Avg
. Stac k

Temp
. ° F 390. 4 393. 1 385. 0 389. 5 Avg
. Sqroo to

fDelt aP 

# - 0.411 3 0.416 6 0.406 2 0.411 4 SD E Averag e - - 11.99 4 12.16 8 11.80 8 11.99 0 Pito tCoefficien t - - 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,92 3 1,96 9 1,90 1 1,93 1 Stac k Flowrat e wetacf m 15,95 6 16,33 8 15,77 3 16,02 2 Stac k Flowrat e wetscf m 9,78 1 9,96 6 9,71 3 9,82 0 Stac k Flowrat e dscf m 5,441 5 2 5,28 0 5,31 1 Isokinetic s % 9 9 10

4 10

0 10

1 Mete rBo xNo
. — 

### 8064 5 8064 5 8064 5 ~ 

### Delt aH @ in
. H g 1.88 1 1.88 1 1.88 1 

# - Fiel d Q AYq c 

# - 1.04 8 1.05 0 1.05 2 1.05 0 [Deviation ] Pre- Y / o 

### 1.6 % 1.7 % 1.9 % 1.7% S:\_JOB\2006\Onyx\Performanc e TesftTes tDataVlun e 2006\2n d Retest\lM23 ASeparat e Front , Bac k Hal fjun e 200S.xls]DAT A

### Metho d 0023 ASamplin g Parameter s

P T 

### RU N 1 AVG S - - PCDDs/PCDF s RU N 2 AVG S - - PCDDs/PCDF s RU N 3 AVG S - - PCDDs/PCDF s P T D P SQR T D P DG M

I N DG M

OU T D H STAC K TEM P D P SQR T D P DG M

I N DG M

OU T D H STAC K TEM P D P SQR T D P DG M

I N DG M

OU T D H STAC K TEM P A 1 0.2 2 0.469 0 10 3 10 0 2.2 0 38 9 0.1 4 0.374 2 9 4 9 3 1.4 0 38 7 0.1 4 0.374 2 9 6 9 5 1.4 0 37 0 1 0.2 5 0.500 0 10 5 10 1 2.5 0 38 9 0.1 4 0.374 2 9 5 9 3 1.4 0 38 6 0.1 1 0.331 7 9 7 9 5 1.1 0 38 0 2 0.2 5 0.500 0 11 4 10 3 2.5 0 38 9 0.2 0 0.447 2 9 6 9 4 2.0 0 38 9 0.1 5 0.387 3 9 8 9 6 1.5 0 38 2 2 0.2 1 0.458 3 11 5 10 5 2.1 0 38 9 0.2 0 0.447 2 9 9 9 5 2.0 0 38 8 0.1 6 0.400 0 10 1 9 7 1.6 0 38 5 3 0.2 2 0.469 0 11 6 10 6 2.2 0 39 0 0.2 0 0.447 2 10 1 9 6 2.0 0 39 0 0.1 5 0.387 3 10 2 9 7 1.5 0 38 5 3 0.2 1 0.458 3 11 7 10 8 2.1 0 38 9 0.2 0 0.447 2 10 5 9 7 2.0 0 39 0 0.1 5 0.387 3 10 5 9 9 1.5 0 38 6 4 0.1 2 0.346 4 11 7 10 9 1.2 0 39 0 0.2 0 0.447 2 10 4 9 9 2,0 0 39 1 0.1 7 0.412 3 10 7 10 0 1.7 0 38 8 4 0.1 6 0.400 0 11 5 10 8 1.6 0 38 9 0,1 5 0.387 3 10 6
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### AV G 0.1 7 0.411 3 109. 3 1.7 1 39 0 0.1 7 0.416 6 107. 1 1.74 39 3 0.1 7 0.406 2 107. 9 1.6 7 38 5

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Appendi xC Reference Method Calibrations , Verifications , an d Certification s

S:\_JOB\2006\Onyx\Performano e Test\Report\Ony x200 6 TestReport.do c Septembe r200 6

## ENS R 

# AECO M DR YGA S METE R CALIBRATIO N Mete rBo xNo. : 8075 4
Chec k one : Annua l Calibratio n Recalibratio n
Date : 3/14/200 6 1 Operato rJame s Ruckdesche l | Barometri c Pressure : 28.5 5 (i n Hg) | Theoretica l Critica l Vacuum : 13.4 7 (i n Hg) f Pretes tLea k Check s

Manufacturer . Dat e Received/Place d i n service : Seria l No. : Anderso n NUTEC H Pr e 199 0 8075 4 

# I Allowabl e Actua l g | Positiv e 0 0.0 0 | 

### 1 (a l 5 -7 in . H 2 0 ) in . H 2 0 pe rmin . 

### I | Negativ e 0 0.00 0 | | (a

t 3 in . Hg ) cf m d m |

DR YGA S METE R DAT A CRITICA L ORIFIC E DAT A

Tim e (min ) Volum e Ter n 3 Critica l Orific e Seria l # K' Orific e

Calibratio n Coefficien t Actua l

Vacuu m (i n Hg ) Ambien tTemperatur e | A H (i n H 2 0 ) Tim e (min ) Initia l

(ft 3) Fina l

(ft 3) Tota l

(ft3) Initia l Fina l Critica l Orific e Seria l # K' Orific e

Calibratio n Coefficien t Actua l

Vacuu m (i n Hg ) Initia l Fina l Averag e I A H (i n H 2 0 ) Tim e (min ) Initia l

(ft 3) Fina l

(ft 3) Tota l

(ft3) ° F ° F Critica l Orific e Seria l # K' Orific e

Calibratio n Coefficien t Actua l

Vacuu m (i n Hg ) ° F ° F ° F| 0.2 4 2 0 677.30 0 683.17 0 5.87 0 6 9 7 0 4 8 0.22 5 1 5 6 8 6 8 6 8

### j 0.9 1 1 5 691.80 0 700.15 6 8.35 6 7 4 7 4 5 2 0.42 7 1 5 6 9 7 3 7 1 

### I 1.5 0 1 5 711.60 0 722.61 3 11.01 3 7 6 7 9 6 3 0.56 2 1 5 7 3 7 4 7 4 j 3.8 0 1 0 733.80 0 744.59 0 10.79 0 8 1 8 3 7 6 0.83 1 1 5 7 2 7 3 7 3 I

CORRECTE D VOLUM E DryGa s Mete r V m (st d ft 3 ) Critica l | I DR YGA S METE R Orific e I J CALIBRATIO N Ve r(st d ft 3 ) j J FACTO R Y | DR YGA S METE R I CALIBRATIO N I FACTO R AH ® 5.587 5.59 1 J 1.00 1 -0.00 6 | 1.72 7 -0.10 4 7.89 9 7.93 6 J 1.00 5 0.0 0 1.82 9 -0.00 3 10.35 9 10.42 0 

### I 1.00 6 0.0 0 J 1.74 8 -0.08 3 10.12 4 10.28 1 I 1 - 0 1 6 0.0 1 j 2.02 2 0.19

### I s r°Avg.AH @ 1_jg2_ J
Notes : 1 ) Fo rvali d tes tresults , th e Actua l Vacuu m shoul d b e 1 t o 2 in . H g greate rtha n th e Theoretica l Critica l Vacuu m show n above .

2 ) Th e Critica l Orific e Coefficient , K' , mus tb e entere d i n Englis h units , (fl^'lde g Rv>0.5/((in.Hg)*(min)) . 3 ) Th e minimu m numbe ro tsampl e volum e require d pe roritic e i s 5 cubi c feet . 4 ) Fo rCalibratio n Facto rY , th e rati o o fth e readin g o

fth e calibratio n mete rto th e dryga s meter , acceptabl e toleranc e o findividua l value s fro m th e averag e i s ±0. C 5 ) ForOrific e Calibratio n Facto rAH® , th e orific e differentia l pressur e i n inche s o fH 2 0 that equate s to 0.7 5 cf m o fai rat 6 8 Fan d 29.9 2 inche s ofHg , acceptabl e toleranc e o findividua l value s Iro m th e averag e i s ±0.2 .

Dr yGa s Mete rThermocoupl e Calibratio n I Ref . TCID #Fluke RT D 213103 J Inle t ID# : 80754-IN OutletID# : 80754-OU T I Ref . Sourc e Ref , ° F ° F A °F A I Amb . Ai r 6 5 6 6 •- 1 6 6 1
rHotWate r 10 6 10 6 0 10 4 - 2 Potentiomete rCalibratio n Lo w 5 0 ° F 5 0 | Mi d 45 0 ° F 45 0 La? h 95 0 ° F. 95 2

Notes : 1 ) H ° tWate rt o b e i n th e rang e o f10 4 -12 2 °F .

2) Toleranc e allowe d fo ral i thermocoupl e individua l reading s : ±5. 4 ° F 3 ) Toleranc e allowe d fo ral l potentiomete rindividua l readings : ±2 ° F



### ,,,„, = n .6 4 (v, )- n + AH 1 3 . 6

-460 Vr ^ +46 0 

### Y

= ^ CT 

### ( sld
m {sid ) ' .150 

# Y

## ENS R 

# AECO M DR YGA S METE R CALIBRATIO N Mete rBo xNo. : 80645
Chec k one : Annua l Calibratio n Recalibratio n [bate : 12/27/200 5 j Ijoperator : Rya n Burn s j Barometri c Pressure : 29.5 0 (inHpj J [Theoretica l Critica l Vacuum : 13.9 2 (i n Hg) |
Manufacturer . Dat e Received/Place d i n service : Seria l No. : Anderso n NUTEC H Pretes tLea k Check s | Allowabl e Actua l | Positiv e 0 0.0 0

## i I (a t 5 -7 in . H 2 0 ) in . H 2 0 pe rmin . 1 Negativ e 0 0.00 0 J (a t3 in . Hg ) cf m cf m S

DR YGA S METE R DAT A CRITICA L ORIFIC E DAT A

Volum e Tem p Critica l K ' Orific e Actua l Ambien tTemperatur e | A H Tim e Initia l Fina l Tota l Initia l Fina l Orific e Calibratio n Vacuu m Initia l Fina l Averag e § (i n H 2 0 ) (min ) (ft3) (ft 3) (ft 3) ° p ° F Seria l t t Coefficien t (i n Hg ) ° F ° F ° Fi 0.2 6 2 0 826.50 0 832.32 7 5.82 7 8 1 8 1 4 0 0.22 5 1 5 6 8 6 8 6 8

## I 0.9 9 1 5 811.80 0 819.95 0 8.15 0 8 3 8 3 5 2 0.42 7 1 5 6 8 6 8 6 8 1.8 0 1 5 777.40 0 788.20 5 10.80 5 8 0 8 0 6 3 0.56 2 1 5 6 8 6 8 6 8

## J 4.0 0 1 0 857.40 0 868.22 8 10.82 8 8 0 8 0 7 6 0.83 1 1 5 6 8 6 8 6 8

## I 

# I I

CORRECTE D VOLUM E J DryGa s Critica l | Mete r Orific e I V m (st d ft 3 ) Ve r(st d ft 3 ) J 5.60 9 5.78 2 j 7.83 0 8.22 3 | 10.45 9 10.82 5 j 10.53 9 10.66 7 1 I I DR YGA S METE R I DR YGA S METE R CALIBRATIO N I CALIBRATIO N FACTO R Y| FACTO R AH ® 1.03 1 -0.00 1 I 1.75 0 -0.13 1 1.05 0 0.0 2 j 1.85 3 -0.02 8 1.03 5 0.0 0

### I 1.94 4 0.06 3 1.01 2 -0.0 2 | 1.97 7 0.1 0

8

### I

Notes : 1 ) Fo rvali d tes tresults , th e Actua l Vacuu m shoul d b e 1 to 2 in . H g greate rlha n th e Theoretica l Critica l Vacuu m show n above .

2 ) Th e Critica l Orific e Coefficient , K\ mus tb e entere d i n Englis h units , (ftyv3*(de g R)*0.5/((in.Hg) - (min)) . 3 ) Th e minimu m numbe rofsampl e volum e require d pe rorific e i s 5 cubi c feet . 4 ) Fo rCalibratio n Facto rY . th e rati o ofth e readin g ofth e calibratio n mete rto th e dryga s meter , acceptabl e toleranc e o findividua l value s fro m th e averag e 5 ) Fo rOrific e Calibratio n Facto rAH® , th e orific e differentia l pressur e i n inche s ofH 2 0 tha t equate s to 0.7 6 cf m ofai ra t 6 8 Fan d 29.9 2 inche s o fHg , acceptabl e toleranc e ofindividua l value s fro m th e averag e i s ±0.2 .
| Dr yGa s Mete rThermocoupl e Calibratio n i Ref . T C ID

#213103 5 Inle t ID# : 80645-I N Outle tID# : 80645-OU T S Rel . Sourc e Ref , ° F ° F 6 8 A ° F AI | Amb . Ai r 6 8 ° F 6 8 0 6 8 

### I I HotWate r 11 2 11 2 0 11 1 - 1 | Potentiomete rCalibratio n Lo w 5 0 ° F 5 0 Mi d 45 0 ° F 44 9 Hig h 95 0 ° F 94 8

Notes : 1 ) HotWate rt o b e i n th e rang e o f104-12 2 °F . 2 ) Toleranc e allowe d fo ral l thermocoupl e individua l reading s : ±5. 4 ° F 3 ) Toleranc e allowe d fo ral l potentiomete rindividua l reading s : ±2 ° F

A H / . + 460 

# r

Y = r(sid

'
n (sid )

## ENS R 

# AECO M D R YGA S METE R CALIBRATIO N Mete rBo xNo. : 80184
Chec k one : Annua l Calibratio n Recalibratio n
Date : 12/27/200 5 [ Operator : Rya n Burn s \ Barometri c Pressure : 29.5 0 (i n Hg) | Theoretica l Critica l Vacuum : 13.9 2 (i n Hg) j
Manufacture r Dat e Received/Place d i n service : Seria l No. : Anderso n NUTEC H

DR YGA S METE R DAT A g Pretes tLea k Check s i Allowabl e Actua l | Positiv e 0 0.0 0 | (a

t 5 -7 in . H 2 0 ) in . H 2 0 pe rmin . S Negativ e 0 0.00 0 1 (a

t 3 in . Hg ) cf m cf m

CRITICA L ORIFIC E DATA ! Volum e Tem p Critica l K ' Orific e Actua l Ambien tTemperatur e | A H Tim e Initia l Fina l Tota l Initia l Fina l Orific e Calibratio n Vacuu m Initia l Fina l Averag e (i n H 2 0 ) (min ) (ft 3) (ft3) (ft 3) ° F ° F Seria l # Coefficien t (i n Hg ) ° F ° F ° F 0.2 6 2 0 103.30 0 109.11 5 5.81 5 7 8 7 9 4 0 0.22 5 1 5 6 8 6 8 6 8 0.9 9 1 5 83.30 0 91.38 5 8.08 5 7 5 7 6 5 2 0.42 7 1 5 6 8 6 8 6 8 1.8 0 1 5 161.70 0 172.46 8 10.76 8 8 2 8 3 6 3 0.56 2 1 5 6 8 6 8 6 8 | 4.0 0 1 0 134.00 0 144.63 1 10.63 1 8 3 8 4 7 6 0.83 1 1 5 6 8 6 8 6 8

CORRECTE D VOLUM E | Dr yGa s Mete r V m (st d ft 3 ) Critica l I

Orific e Ve r(st d ft 3) ] 5.62 3 5.78 2 7.87 6 8.22 3 10.37 5 10.82 5 10.28 0 10.66 7 DR YGA S METE R CALIBRATIO N I FACTO R Y 1.02 8 -0.01 0 1.044 0.0 1 1.04 3 0.0 0

## I 1.03 8 0.0 0

## I

1.03 B 

## [ DR YGA S METE R | CALIBRATIO N FACTO R AH ®

| 1.75 0 -0.13 1 1.85 3 -0.02 8 1.94 4 0.06 3 1.97 7 0.1 0
| [ Avg . AH ®

1.88 1 

### 1
Notes : 1 ) Fo rvali d testresults , th e Actua l Vacuu m shoul d b e 1 to 2 in . H g greatertha n th e Theoretica l Critica l Vacuu m show n above .

2 ) Th e Critica l Orific e Coefficient , K' , mus tb e entere d i n Englis h units , (ftv^'fde g RV*j.o7((in.Hg)*(min)) . 3 ) Th e minimu m numbe rofsampl e volum e require d pe rorific e i s S cubi c feet . 4) Fo rCalibratio n Facto rY , th e rati o o fth e readin g ofth e calibratio n mete rt o th e dryga s meter , acceptabl e toleranc e o findividua l value s fro m th e averag e is : 5 ) Fo rOrific e Calibratio n Facto rAH® , th e orific e differentia l pressur e i n inche s ofH 2 0 that equate s t o 0.7 5 cf m o fai rat 6 8 F an d 29.9 2 inche s ofHg , acceptabl e toleranc e o findividua l value s fro m th e averag e i s ±0.2 .

Dr yGa s Mete rThermocoupl e Calibratio n f Potentiomete rCalibratio n Ref , T C ID

#213103 5 Inle t ID# : 80184-I N OutletID# : 80184-OUT | Lo w 5 0 ° F 5 0 Ref . Sourc e Ref , ° F ° F A ° F A

### S Mi d 45 0 ° F 45 0 Amb . Ai r 6 8 6 8 0 6 8 0 i I Hig h 95 0 ° F 95 1 HotWate r 11 1 11 1 0 11 1 0 j
Notes : 1 ) HotWate rt o b e i n th e rang e o f10 4 -12 2 °F . 2 ) Toleranc e allowe d fo ral l thermocoupl e individua l readings : ±5. 4 ° F 3 ) Toleranc e allowe d fo ral i potentiomete rindividua l reading s : ±2 ° F

1 7 .64 (V „ ) 13. 6

r+ 46 0 

# V f 

# - +46 0 Y = '(ad

) ,(std) 

### Afl a

### =AH ( .159 

# Y -4s,d)J

# ENS R AECO M SAMPL E PROB E CALIBRATIO N DAT AFOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Thermocoupl e Calibratio n PROB E ID : M5-4- A Referenc e Themomat

wI D * ENS R RTD #213103 5 Omega CI1000 , K06022JC

O Omeg a CI1O00 . W602220

0 PROB E ID : M5-4- A Referenc e Themomat

wI D * Tut »hmwo (300 - - SCO * F) PROB E ID : M5-4- A Referenc e Themomat

wI D *
^.-^• r——.... . ... —.^..,...........~....„_i•.,..., . Mw*MIliu m—tfi. * r" * « _.t^.. - TT ir%to

ni . • >

. ... . -- . • F - . f.P . .. . it> : 3/6/200

6 M5-4- A 32.5 9 273.4 8 3 4 27 4 1 212. 2 373. 3 21 4 37 4 0. 3 450. 0 505. 3 45 1 50 6 0. 1

M5-4- A 32.5 9 273.4 8 3 4 27 4 1 212. 1 373. 2 21 4 37 4 0. 3 450. 0 505. 3 45 1 50 6 0. 1

32.6 0 273.4 8 3 4 27 4 1 212. 0 373. 1 21 4 37 4 0. 3 450. 0 505. 3 45 1 50 6 0. 1 Sworn * tri ePmuur s »Hgl - 296 5 32.5 9 273.4 8 3 4 27 4 1 212. 1 373. 2 21 4 37 4 0. 3 450. 0 505. 3 45 1 50 6 0. 1 

### Tvp e "S " Ptto tTub e Calibration :

Dsgr* e in d restin g hav e I poniUo n fo r deter m inin g ©
. Leve l an d Perpendicula r Obstructio n Damaged
a, (-10 ° £a , £+ 10° )
a j (-10 ° £o^ s +10° ) B , (-5 ° £B , S + 5° ) G 2(-5° £B 2 s +5° ) y 

### e 2 = ATany(± £0.125" ) W= ATan9(± £0.03125* ] D , (3/1 6 s D t s 3/8" ) A A/2D , (1.0 5 S PA/D, S 1.5) N o

0.00 8 0.00 8 0.37 5

Dagrc cindicatin g tevol posHto

n for 

### Pito tTub e t o Nozzl e Calibration :

y»7.B3gnrair.. )

1 ) Prto i t o nozU o separatio

n 2 ) Thermocoupl

e l o pilo tseoor . 3 ) Pito ten d t o prob e unio n db t >3/4 * (w/,50 0 noate )


### Prob e EntormafEor r
Manufacturer_ bate Receive

d and place

d I n Service : _ Conditio n o tProb e whe n place d i n service : Ape x pre-199 5 QA/QC

Check (Completenes

s X Legibilit y__X
_ RECONDITIONE D (circl e one )
Accurac yX
_ Reasonablenes s X
_ certif ytha t th e Typ e S plto ttube/prob

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_ _meet s orexceeds al l Specifications , criteria and/orapplicable desig n teature s an d i s hereb

yassigne

d a pito ttub e calibration (acto

rC D o ! 0.8

4
Certilte d by: Fre

d Sanguedolc

e / 03-13-200

6 , , Personnel {Signature/Date ) Team Leade r(Signature/Date ) Al l constructio

n criteria foran isolate

d "S*typ e pilo tar e wfthin gtve

n toterance

s prescribe

d I n Qualit yAssuranc

e Handbook

torAi rPollution Measuremen tSystems : Volum

e III , Stationar

ySource-Sped!i c Methods , EPA/600/R-94/O38C , September199 4 -1 /067PS
NOTES :

# ENS R AtCU M SAMPL E PROB E CALIBRATIO N DA I At-UH M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Tnonnoc v3

aCalibratio n

273.5 2 273.5 2 273.5 2 3 4

3 4 , 3 5 2 7 4

2 7 4 2 7 5 Omaga CI1000, #0602220 0

212. 2 373. 3

373. 3 21 0

21 0 21 0 3 7 2 Omaga C110OO , #0602220

0

505. 3 505. 3 50 3 -0. 4 50 4 -0. 3
273.5 2 2 7 4 212. 2 373. 3 21 0 -0. 3 450. 0 505. 3 44 7 5 0 3 

### Typ e "S ' Plto tTub s eviration :

- £
Degre eindicatin g leve lpositio nlo r ootominlng'ythe ncalculat eZ. Leve l an d Perpendicula r Obstructio n Damage d

a , (-10 ° £a , £+10" ) (-10 ° s Ot

j £+ 10° ) B , (-5° £B , £+5° ) B 2(-5 ° s B 2£+ 5° ) f e

z= ATany(± £0.125" ) W= ATan8(± £0.03125" ) D , (3/1 6 £D, £3/8" ) A A/2D , (1.0 5 S PA/D, £1.5 ) Yes N o N o

0. 1

0.01 4 0.37 5

1.1 8



### Plto tTub e t o Nozzl e Calibration :

T B I Vt»T.

Mc mfflo.)

|1 ) Pito t t o nozzl e separatio

n 2 ) Thttmocoupl

e t o ptto t sopor . 3 ) Plto t en d t o prob e unio n dis t >3/4 -(W/.50 0 nozzle )

>3.0 * 0.37 6 0.97 S 

### Prob e Informatio n
Manutacturer

. Dat e Receive

d and place

d I n Service : jCondttlo n o fProb e whe n place d I n service : Ape x pre-199 5
QA/Q C Check ICompletenes

s X Legibilit y_X
_ RECONDITIONE D (circle one )
Accurac yX certif ytha t th e Type S pilo

t tube/prob

e 1D#
_ _MS-4'-B
_ criteria and/orapplicable design feature s an d I s hereb yassigne

d a plto t tub e calibration (actorCpO t0.8 4
Certifie d by: Fred Sanguedolc e / 03-13-200

6 Personnel (Signature/Date ) Team Leader(Signature/Date ) Al l constructio

n criteria fora

n Isolated'S ' typ

e pilo t ar e within gtve

n tolerance

s prescribe

d i n Qualtt yAssuranc

e Handboo

k forAi rPollution Measuremen t Systems : Volum

e III , Stationar

ySource-Specifi c Methods. EPA/60O/R-94/038C , September199 4 **> v06/P S
•PTES :

### ENS R AECO M SAMPL E PROB E CALIBRATIO N DAT AFOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Thermocoupl e GelOr^tior
. PROB E D : M5-5-F Reloroie* . Thermomat

w10 « : ENS R RT D #213103 5 Omeg a CI1000. #0502220 0 Omeg a CI1O00 . #0602220

0 PROB E D : M5-5-F Reloroie* . Thermomat

w10 « : Boilin g Wate . Tub s Fum»£ » (MC -SOO

*F ) PROB E D : M5-5-F 15 - » ^ > W"Tw o ^ -.0»fs—

P —-• « 3n*wh *

. > - » « jst , K J *Vl»»t " 3A5/200 6 M5-5- F 32.1 8 273.2 5 3 3 27 4 0 211. 8 373. 0 20 9 37 1 -0. 4 450. 0 505. 3 44 4 50 2 -0. 7

M5-5- F 32.1 8 273.2 5 3 3 27 4 0 211. 8 373. 0 20 9 37 1 -0. 4 450. 0 505. 3 44 3 50 1 -0. 8

32.1 8 273.2 5 3 3 27 4 0 211. 8 373. 0 20 9 37 1 -0. 4 450. 0 505. 3 44 3 50 1 -0. 8
* — 32.1 8 273.2 5 3 3 27 4 0 211. 8 373. 0 20 9 37 1 -0. 4 450. 0 505. 3 44 3 50 2 -0. 7



### Typ e "S " Pito tTub e CaKbtJfictt : Leve l an d Perpendicula

r Obstructio n Damage d
a , (-10 ° £a , £+10° )
a j (-10 ° s aj S +10° ) (3 , (-5 ° £13

, £+ 5° ) 8 2(-5° £3 2 £+5° ) T 0
z= ATany(±- . 0.125" ) W= ATan©(± £0.03125" ) D , (3/1 6 £0,- 5 3/8" ) A A/2D , (1.0 5 £PVD, £1.5) N o
0. 3 0. 9

0. 7
-0.00 6

0.37 5

Oegro o in dteatin g Vava lposh£o* i(o r dat-t mInlng ? tha ncafcutat * Z. 

### Fitc tTub s t o Nozzl e Calibration :

I " H i Va 7.0

3 o n ( 3 In. ) 

### il
— [HS U

1 ) Ptto tt o nozzl e saparaBo n 2 ) Inem>ocoupi « t s pilo tsapar3 ) Pito ten d t o proba unio n dis

t >aW ' (W /.50 0 nozzle ) >3JA~ >3.£ T 1.02 7 1.84 5 

### Prob e informatio n .ManufacturerApe x Dat e Receive

d an d place

d t n Service : pre-l& i Conditio n o ! Prob e whe n place d i n service : NE

WI QA/Q C Chec k Completenes

s X
_ Legibilit y_X_
_ RECONDITIONE D (circl e one }
Accurac yX certif ytha t th e Typ e S plto ttube/prob

e IDfi
_ _meet s orexceeds al l Specifications. criteria and/orapplicable design feature s an d I s hereb yassigne d a pilo ttub e calibration factorC fl o l 0.8 4
'Certifie d by : Fred SanouedolC

Q / 03-13-200 6 Personnel (Signature/Date ) Team Leader(Signature/Date ) I Al l constructio

n criteria foran Isolate

d "S " typ e prto ta m within given tolerance s prescribe

d I n Qualit yAssuranc

e Handboo

k forAi rPollution Measuremen tSystems : Volum

e lit, Stationar

ySource-Specttk: Methods. IEPA/600/R-94/03SC

. September199 4 V06/P S NOTES :

## ENS R Rya n Burn s 3/6/200 6 Referenc e Thremomete rID : DV M CCL05015241 7

Las tImpinge rThermocoupl e Calibratio n 200 6 Thermocoupl e Referenc e Differenc e (+/ - 2° ) Thermocoupl e Referenc e Differenc e (+/ - 2° ) LI- 2 Ho t 21 2 21 2 0 LI-2 1 Ho t 21 1 21 1 0 LI- 2 Col d 3 3 3 2 1 LI-2 1 Col d 3 3 3 2 1 Manufacturer . Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI- 4 Ho t 21 1 21 1 0 LI-2 2 Ho t 21 3 21 2 1 LI- 4 Col d 3 3 3 3 0 LI-2 2 Col d 3 5 3 3 2 Manufacture rAnderso n NUTEC H Manufacturer : Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI- 6 Ho t 0 LI-2 3 Ho t 21 1 21 2 - 1 LI- 6 Col d 0 LI-2 3 Col d 3 5 3 3 2 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI- 7 Ho t 21 2 21 2 0 LI-2 4 Ho t 0 LI- 7 Col d 3 3 3 2 1 LI-2 4 Col d 0 Manufacture rAnderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI- 8 Ho t 21 2 21 2 0 U-2 5 Ho t 21 2 21 2 0 LI- 8 Col d 3 4 3 3 1 U-2 5 Col d 3 3 3 2 1 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI- 9 Ho t 21 1 21 2 - 1 LI-2 6 Ho t 21 4 21 2 2 LI- 9 Col d 3 3 3 3 0 LI-2 6 Col d 3 5 ' 3 4 1 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-1 0 Ho t 21 2 21 2 0 LI-2 7 Ho t 21 0 21 2 - 2 LI-1 0 Col d 3 2 3 2 0 LI-2 7 Col d 3 4 3 3 1 Manufacturer : Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-1 1 Ho t 0 LI-2 8 Ho t 21 2 21 2 0 LI-1 1 Col d 0 LI-2 8 Col d 3 3 3 3 0 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-1 2 Ho t 21 1 21 2 - 1 LI-2 9 Ho t 21 2 21 2 0 LI-1 2 Col d 3 2 3 2 0 LI-2 9 Col d 3 3 3 3 0 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-1 3 Ho t 21 3 21 2 1 LI- 5 Ho t 21 3 21 2 1 LI-1 3 Col d 3 3 3 3 0 LI- 5 Col d 3 4 3 3 1 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-2 0 Ho t 21 1 21 1 0 LI-1 4 Ho t 21 1 21 1 0 LI-2 0 Col d 3 4 3 3 1 LI-1 4 Col d 3 2 3 3 - 1 Manufacture rAnderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e r e ceived/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0 

### ^^^^^^^^^^^^^^^^^^^^^^^^^ ^ENS R AECO M
CaJbrato rFre d Sanguedob e flelerence Thermomete rFluke RT D 213103 5
Fitte rBo xCalibratio n Ho tBo x# 1 H o tBo x#1 1 Manufacturer : Anderso n NUTEC H l \ Seria l No. : N/ A£ Dat a received/place d In service : Pre 199 5 tAanulacture n Anderso n NUTEC H >ena 1 No. : N/ A at e received/place d I

n service : Pre 199 5 Calibratio n Date : 16-Feb-O S C Calibratio n Date : 16-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 9 24 7 Reference Temperature s 7 2 24 6 Actua l Temperature s 6 9 24 9 Actua l Temperature s 7 1 24 9 Tem p Differenc e (tol . = +-2 1 0 • 2 em p Differenc e (tol . = 1 - 1 Ho tBo x# 2 Ho tBo x#1 2 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e recerved/place d I n service : Pr e 199 5 vlanufacturer . Anderso n NUTEC H Seria l No. : N/ A Dat e received/place d i n service : Pre 1995 Calibratio n Date : 15-Feb-0 6 Calibratio n Date : 16-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 8 24 9 Referenc e Temperature s 7 0 246 Actua l Temperature s 7 0 24 7 Actua l Temperature s 7 1 247 Tem p Differenc e (tol . = +-2 ) -2 2 Tem p Dttlorenc e (tol . = +-2 ) -

1 -

1 Ho t8 O X# 3 H o tBo x#1 3 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place d i n sen/lea : Pr e 199 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/place d I n service : Pre 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 16-F e b-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 9 24 4 Referenc e Temperature s 6 7 246 Actua l Temperature s 6 9 24 4 Actua l Temperature s 6 7 24 6 Tem p Differenc e (tol . = +-2 ) 0 0 Tem p Differenc e (tol . = -t-2 ) 0 0 Hot B O X# 4 Ho tBo x#1 4 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place d I n service : Pr e 199 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dal e received/place d In service : Pir* 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 16-Feb-0 6 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = *-2 ) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = *-2 ) 7 1 24 4 Referenc e Temperature s 6 8 24 7 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = *-2 ) 7 1 24 3 (Actua l Temperature s 7 0 24 7 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = *-2 ) 0 1 Tem p Differenc e (lot, = +-2) -2 0 Ho tE o x# 5 Ho tBo x#1 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place d i n service : Pr e 199 5 Manufacture rAnderso n NUTEC H Seria l No. : N/ A •at e received/place d I n servfce : Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 15-Feb-0 6 Referenc e Temperature s Actua l Temperature s Tem p Difference (tol . - *-2 ) Ambien t Ho t Referenc e Temperature s Actua l Temperature s Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Difference (tol . - *-2 ) 6 6 25 1 Referenc e Temperature s Actua l Temperature s 68 247 Referenc e Temperature s Actua l Temperature s Tem p Difference (tol . - *-2 ) 6 6 25 2 Referenc e Temperature s Actua l Temperature s 6 6 247 Referenc e Temperature s Actua l Temperature s Tem p Difference (tol . - *-2 ) 0 • 1 Tem p Differenc e (loi . = +-2 ) 2 0 H o U 3ox# 6 Ho tBo x#1 6 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place d t n sen/tee ; Pr e 199 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/place d i n service : Pre 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 17-Feb-0 6 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = t-2) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = t-2) 6 9 245 Referenc e Temperature s 71 24 1 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = t-2) 7 0 24 5 Actua l Temperature s 6 9 24 1 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (to). = t-2) - 1 0 Tem p Differenc e (tol . = -t-2) 2 0 Ho t BO X# 7 Ho tBo x#1 7 Manufacturer : Anderso n NUTEC H Seria l No. : N/A Dat e received/place d I n service ; Pr e 199 5 Manufacture rAnderso n NUTEC H Seria l No. : N/ A Date received/place d I n service : Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 16-Feb-0 6 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (tol . = +-2 ) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Differenc e (tol . = +-2 ) 7 1 24 6 Referenc e Temperature s 6 9 24 5 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (tol . = +-2 ) 7 1 25 0 Actua l Temperature s 7 0 24 7 Referenc e Temperature s Actua l Temperature s Tem p Differenc e (tol . = +-2 ) 0 -2 Tem p DWerence (tol . = +-2) - 1 -2 Ho t Bo x# 8 Ho tBO X#1 8 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date recefved/piace d I n service : Pr e 199"5 Manufacture rAnderso n NUTEC H Seria l No. : N/ A Date received/place d I n servce : Pr e 1995 Calibratio n Date : 16-Feb-G 6 Calibratio n Date : 15-Feb-0 6 Referenc e Temperature s Actua l Temperature s Tem p Differenc e {tol . = +-2) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Differenc e {tol . = +-2) 7 0 244 - Referenc e Temperature s 72 24 7 Referenc e Temperature s Actua l Temperature s Tem p Differenc e {tol . = +-2) 7 1 24 6 Actua l Temperature s 70 24 8 Referenc e Temperature s Actua l Temperature s Tem p Differenc e {tol . = +-2) • 1 -2 Tem p Differenc e (tol . = -t-2) 2 - 1 Ho tBo x# 9 Ho tBo x#1 9 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date recerved'olace d I n service : Pr e 199 S
_ Manufacturer : Anderso n NUTEC H Seria l No. : N/ A •at e recarvBd/place d i n service : Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 16-Feb-0 8 Referenc e Temperature s Actua l Temperature s Tem p Differenc e flol . = +-2 ) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Differenc e flol . = +-2 ) 6 9 24 9 Referenc e Temperature s 70 24 4 Referenc e Temperature s Actua l Temperature s Tem p Differenc e flol . = +-2 ) 7 0 25 1 Actua l Temperature s 7 1 24 4 Referenc e Temperature s Actua l Temperature s Tem p Differenc e flol . = +-2 ) -

1 -2 Tem p Differenc e (tol . = +-2) - 1 0 Ho t 3o x#1 0 Ho tBo x#2 1 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/place d I n service : Pr e 199 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/placed I n service : Pr e 199 5 Calibratio n Date : 1&-Feb-0 5 Calibratio n Date : 17-Feb-O S Referenc e Temperature s Actua l Temperature s Tem p Drfterence (tol . = +-2 ) Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s Tem p Drfterence (tol . = +-2 ) 7 3 24 7 Referenc e Temperature s 68 24 1 Referenc e Temperature s Actua l Temperature s Tem p Drfterence (tol . = +-2 ) 7 2 24 6 Actua l Temperature s 6 9 24 3 Referenc e Temperature s Actua l Temperature s Tem p Drfterence (tol . = +-2 ) 1 1 Tam p Differenc e {tol . = +-2 ] -

1 -2

# ENS R AECO M
XA D Thermocoupl e Calibration s - 200 6 date 3/13/200 6 BP : 29. 1 Referenc e Thermomete rID# : Manufacture : Dat e place d i n Service : Calibrator : Jame s Ruckdesche l Ambien tTem p (F) : 6 3 Fluk e Digita l RT D 213103 5 Fluk e Pr e 198 0 Ic e Bat h Ambien t Thermocoupl e ID# Referenc e

Tem p XA D

Tem p Tem p

Differenc e To l = + - 2 F Referenc e

Tem p XA D

Tem p Tem p

Differenc e To l = + - 2 F XAD- 1 3 3 3 2 - 1 6 2 6 2 0 XAD- 2 3 3 3 3 0 6 2 6 3 1 XAD- 3 3 3 3 1 - 2 6 2 6 2 0 XAD- 4 3 1 3 1 0 6 3 6 3 0 XAD- 5 3 1 3 3 2 6 3 6 3 0 XAD- 6 3 2 3 2 0 6 3 6 3 0 XAD- 7 3 2 3 2 0 6 4 6 4 0 XAD- 8 3 2 3 2 0 6 5 6 3 - 2 XAD- 9 0 0 XAD-1 0 3 2 3 2 0 6 6 6 4 - 2 XAD-1 1 0 0 XAD-1 2 0 0

# ENS R

Appendi xD Stac k Configuration , Samplin g Por tan d Travers e Poin tLocation s

S:V_JOB\2006\Onyx\Performance Test\Report\Ony x200 6 Tes tReport.do c Septembe r200 6GROUN D LEVE L TES TPORT S

32 '

FLO W



### ENS R AECO M ENS R CORPORATIO N 660 1 Klrkvlll aRoo

d Eas tSyraeuM
. Ns

wYor k 1305 7 PHONE: (315 ) 432-050 6 FAX : (315 ) 437-050 9 WEB : HTTP://WWW.ENSR.AECOM.CO M 

### FIXE D HEART H INCINERATO R UNI T3 VEOLI AE S TECHNICA L SOLUTION S

Sauget, Illinois FIGUR E NUHnb ENS R AECO M ENS R CORPORATIO N 660 1 Klrkvlll aRoo

d Eas tSyraeuM
. Ns

wYor k 1305 7 PHONE: (315 ) 432-050 6 FAX : (315 ) 437-050 9 WEB : HTTP://WWW.ENSR.AECOM.CO M 

### FIXE D HEART H INCINERATO R UNI T3 VEOLI AE S TECHNICA L SOLUTION S

Sauget, Illinois 

# 1 ENS R AECO M ENS R CORPORATIO N 660 1 Klrkvlll aRoo

d Eas tSyraeuM
. Ns

wYor k 1305 7 PHONE: (315 ) 432-050 6 FAX : (315 ) 437-050 9 WEB : HTTP://WWW.ENSR.AECOM.CO M 

### DRAW N BY : CHECKE D BY : DATE

: PROJEC

TNUMBER : DRAWIM

O NUMBER : ENS R AECO M ENS R CORPORATIO N 660 1 Klrkvlll aRoo

d Eas tSyraeuM
. Ns

wYor k 1305 7 PHONE: (315 ) 432-050 6 FAX : (315 ) 437-050 9 WEB : HTTP://WWW.ENSR.AECOM.CO M LL M WW 9/11/0 6 10002-01 7 1 O F 1

### TRAVERS E POIN TLOCATION S (Particulat e Travers e - Circula rStack)

FACILTY : Ony xEnvironmenta l Service s STAC KIDENTIFICATION : Uni t3 STAC KDIAMETER : 3 9 inche s SAMPLIN G LOCATIONS : 14.9 5 diameters downstrea m 9.8 5 diameters upstrea m MINIMU M NUMBE R O FTRAVERS E POINT S A S SPECIFIE D B YEP AMETHO D 1 : 1 6
NUMBE R O FTRAVERS E POINT S SAMPLED : 1 6

Travers e Poin tPercen tofStac k Diamete r Numbe rFro m Insid e Wal l Distanc e i n Inche s Fro m Insid e Wall * 1 3. 2 1. 2 2 10. 5 4. 1 3 19. 4 7. 6 4 32. 3 12. 6 5 67. 7 26. 4 6 80. 6 31. 4 7 89. 5 34. 9 8 96. 8 37. 8

* Fo rstack s wit h a n insid e diamete r(ID ) of2 4 inche s o rless , n o travers e poin tma yb e locate d withi n 0. 5 inche s o

fth e insid e wall
. Fo rstack s wit h a n I D greate rtha n 2 4 inches , n o travers e poin tmayb e locate d withi n 1. 0 inche s ofth e insid e wall
. An ypoin tnotmeetin g th e criteri ashal l b e adjusted
.

# ENS R

Appendi xE Laborator

yDat a

S:\JOB\2006\Onyx\Performanc e Test\Report\Ony x200 6 TestReport.do c Septembe r200 6

### ENS R AECO M

ENS R Ai rToxic s TS P Laborator y

Analytica l Repor t

Client : Jef fGorma n

ENS R 660 1 Kirkvill e Roa d E
. Syracuse , N Y1305 7
Laborator yID : 06-06 7 Clien tID : 10002-01 7

Dat e Received : 5/12/0 6

Al lwor kcontaine

dintM s repor tha s bee ndon ei naccordanc

ewit hlaborator

ystandar doperatin

gprocedures

. ENSR' s Ai r Toxic s TS PLaborator

yfollow s methodologie

s base dupo nstandar dEPA/NIOSH/OSHA Methods. Dat acontaine

dherei n shoul db econsidere

daccurat ean dcomplet

et o th ebes tof ou rknowledge

. Thi s repor tcanno tb eduphcate

dinpar twithou t th ewritte npermissio

nof ENSR. ;

Arthu rCarpenit

o / Dat e Laborator

yAnalys t ENS RAi rToxic

s TSPLaborator

y

NYSDO H/

NELA C #1163

1

pag e 1 o f6

### ENS R Metho d 5 Expose d Filte rDat aShee t Balanc e Used : Projec tManager : Projec tName : Projec tNumber : Analysi s Mathod : JeffGorma n Onyx 10002-01 7 Start Friday 05/12/0 6 16:34 4 5 72 A C Wt
. 1 Monday 05/15/0 6 15.3 0 3 6 7 2 A C Wt. 2 Tuesday 05/16/0 6 9:2 8 3 7 72 A C Wt
. 3 Wt
. 4

. Filter * Ru n Dll a ly' ' *i<W i ' "IV r, V^ 1 « W t 

### •tes t 20 4 01/09/0 6 0.409 3 G383 2 N/ A LA B FILTE R BLAN K 9 0 m m 0.409 2 0.409 4 0.000 2 o k byWt
. 0.409 3 0,000 3 20 4 01/09/0 6 0.406 7 G382 5 05/09/0 6 PRETEST-M5-FILTE R 9 0 m m 0.410 1 0.410 2 0.000 1 o k byWt , 0.410 2 0.003 5 20 4 01/09/0 6 0.405 7 G382 7 05/10/0 6 U3-M5-F-R 1 9 0 m m 0.408 6 0.408 8 0.000 2 o k byWl
. 0.408 7 0.003 0 20 4 01/09/0 8 0.405 4 G382 4 05/10/0 6 U3-M5-F-R 2 9 0 m m 0.413 6 0.4134 0.000 2 o k byWt
. 0.413 5 0.008 1 20 4 :01/09/0 6 0.405 4 G382 8 05/11/0 6 U3-M5-F-R 3 9 0 m m 0.412 6 0.412 4 0.000 2 o k byWl
. 0.412 5 0.007 1 0 3 C O C D 

### w o

Eillo rTypo : 

### iSiJJgfei ' Teflo n 

### Quart z 1 . Delta Weigh ttolerance +/-0.0005 Q o ftota l weightles s tar e weightbetwee n tw

o consecutive weighting s or averag e weight . 2 . Filler s mustb e weighe d wili i (h a prope rcondition s (R H = 25-5 0 % an d R T= 50-78 de g f ) 3 . Filler s mus

tb e properl yconditione d (24 hou rdesiccation : Furthe rConditionin g > 6 hours) . 4 . Conditionin g forove n method , Ove n drio d a t105 de g c f

o 2-3 hours ; Furthe rconditionin g > 6 hours . 5 . Tota l gram s belowo requa l t o .000 5 (I.DL) i s presente d a s .0003 .

### ENS R j M

Metho d 5 Fron tHal fAceton e Prob e Rins e Dat aShee t

Je( tGorma n Balanc e Used : Mettle r3 Projec tManager : Projec tName : Projec tNumber : Analysi s Method : Onyx 10002-01 7 

### •RE M Star t Tuesda y 05/16/0 6 15:4 0 4 4 7 2 A C Wt . 1 Wednesda y 05/17/0 8 17:0 6 4 1 7 1 A C Wt . 2 Thursda y 05/18/0 6 8:4 7 4 7 6 9 A C Wl . 3 Thursda y 05/18/0 6 14:4 8 4 0 7 3 A C Wt . 4 O ASlveaf , ....EM*.*'
. 

### wssm&missm •©-Smil e M . ;tsiwt . i I l ^*'* , t $ 43 4 06/11/0 6 115.166 8 3 2 N/ A LA B ACETON E BLAN K 5 0 115.168 8 115.167 8 0.000 8 115.167 8 0,000 0 o k byWt . 115.167 8 0.001 0 43 4 05/11/0 6 B6.295 6 3 9 05/09/0 6 PRETEST-M5-ACETON E 5 2 5 0 86.299 2 66.298 8 0.000 4 o k byWt . 86.289 0 0.003 4 43 4 05/11/0 6 103.534 7 6 4 05/10/0 6 U3-MS-AR-R 1 6 3 5 0 103.538 1 103,537 7 0.000 6 103.537 8 0.000 1 o k byWt . 103.537 8 0.003 1 43 4 05/11/0 6 101.047 5 12 0 05/10/0 6 U3-M5-AR-R2 11 1 5 0 101.054 2 101.054 0 0.O002 o k byWt . 101.054 1 0.006 6 43 4 05/11/0 6 105.363 2 154 05/11/0 6 U3-M5-AR-R 3 9 5 5 0 105.369 1 105.368 9 0.000 2 o k byWt . 105.369 0 0.005 8 C O ( Q < D O

— H O

Aceton e Manufacturer/Lo tNo. : Rsher/052584_
_ Aceton q Rins e = 2 5 mi s twico -(S O nil s tolal ) 1 . Deli a Weigh l toleranc e +/ -0.0005 g o

ftola l weigh l les s lare weigh tbetwee n tw o consecutive weighting s o raverag e weight . 2 . Beaker s mustb o weighe d wit h In o prope rcondition s {R H = 25-5 0 %an d R T= 59-7 8 de g 0 3 . Beaker s mustb o propert yconditione d (24 hou rdesiccation ; Furthe rConditionin g > 6 hours) , 4 . Natura l Evaporatio n Motho d = Evaporat e t o drynos s a

troo m temperature unde ra hoo d / watc h glas s cove r 5 . HeatAppiicalio n = Unde ra hoo d an d watc h glass ove rsample , appl yheatbelow(h e boilin g poin to fsampl e unti l evaporate d t o 2 5 mis ; the n followsle p 4 (above ) fo rremainin g portion . 0 . Tota l gram s belo wo requa l l o .000 5 (LDL ) i s presente d a s .0003 .

### PROJEC TNARRATIV E



### Maxxa m Analytic s (Bariragton ON ) 

### Maxxam ; Jo b # : A64446 9 

### Client : ENS R 

### Internationa l 

### Qien tProject : 10002-017-01 7 ONYX L SAMPL E RECEIPT/ANALYSI S a ) Sampl e Listin g Maxxa m Clien t Dat e 

### Dat e Dat

e Dat

e I D Sampi

e I D Sample

d Receive

d Proppe

d Ru n Mercury IB via EPAMethod

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 7 06705/1 8 

### Mercury 2B via EPAMethod

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 

### Mercury 3Avia EPAMethod

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 0 U3-M29 T R 2 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 1 U3-M29-R 3 06705/1 0 06/05/1 2 06/05/1 5 06/05/1 6 

### Mercury 3B via EPAMethod

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 

### Mercury 3C via EPAMethod

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 

### Metals in Ab (Combined)

via EPAMethod

29 (ICP/MS) L9982 8 U3-M29-R B 06/05/1 0 06705/1 2 06/05/1 7 06/05/1 9 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 

### Ru n Dat e is de&ne

d a s th e dat

e o finjectio n o

fth e las tcalibratio n standar d (1 2 hour s orless ) prio rt o tli e sample s analyze d withi n tha tran sequence . Therefor e th e tim e o fcalibratio n injectio atha tdefine

s th e n m dat

e i s alway s withi n 1 2 hour s o fth e tim e o

fsampl e injection
. 

### b ) Shipping Problems: non e encountere d c ) Documentatio n Problems : non e encountere d 

### J H Pag e 1 of2

### aSAMPL E PREP :

N o problem s encountere d ffl. SAMPL E ANALYSIS : See als o comment s withi n tli e appropriat e Certificat e o fAnalysi s a ) Hol d Times : al l withi n recommende d hol d times b ) Instrumen tCalibration : al l withi n contro l limit s c ) Qualit yControl : Al l applicabl e Q C meets contro l criteria , excep twher e otherwis e noted
. I certif ytha tthi s dat apackag e i s i n complianc e wit h th e term s an d condition s o fth e contract , bot h technicall yan d forothe rtha n th e condition s detaile d above
. I n addition , I certify , tha tt o th e besto fm yknowledg e an d belief , th e dat aa s reporte d ar e tru e an d accurate . Releas e o fth e dat acontaine d i n mi s dat apackag e ha s bee n authorize d b y th s cognizan tlaboratoryofficia l o rhis/he rdesignee , a s verifie d b ythi s signature
.

Mary-AnneT S



### J H Pag e 2 o f2

### 2
. DAT ASUMMAR Y

- Certificat e o fAnalysi s -
Sampl eanalyt eresul t Metho dblan kresul t LC S Result

s wit h% Recoverie

s Matri xSpik edat awit h% Recoverie

s Matri xSpik eDuplicat

edat awit h% Recoverie

s Surrogat erecoverie

sDriven by service

and Science 

### You rProject* : 10002-017-01 7 Site : ONY X
Attention : Jef

f Gorma n ENSRInternationa

l 6601KirkvilleR

d Eas tSyracuse

, N Y US A 1305

7 Repor tDate : 2006/05/2

0 CERTIFICAT EO F ANALYSI S MAXXA MJO B #

: A64446 9 Received : 2006/05/12,12:0 0 Sampl eMatrix: Filte

r #Sample s Received : 4 Dat e Dat e Metho d Analyse s ; QuantityExtracte d Analyze d Laborator yMetho d Referenc e MercuryI B -Ai r(Filtcr+Acetone ) b yCVA AQ 4 2006/05/1 7 2006705/1 8 SO P IN G 11 1
. EP ACF R PT M 2 9 Metal s i n Ai r(Combined ) byICP/MS© 4 2006/05/1 7 2006705/1 9 SO P IN G 108/10 9 EP A5W846-602 0 

### Sampl eMatrix: Impinge

rSolutio n #Sample s Received : 4 Analyse s Mercury3 C i n Ai r(HC I Impinger) b yCVA AQ 4 Mercury3 Ai n Ai r(HN0 3 Rinse ) b yCVA A$ 4 Mercury2 B i n Air(HN03/H20 2 Imp ) b yCVA A0 4 Mercury3 B i n Ai r(KMn04/H2S04 ) b yCVAA © 4 Date Dat e Metho d Extracte d Analyze d LaboratoryMetho d Referenc e 2006/05/1 6 2006705/1 8 SO P IN G 11 1 EP ACF R PT M 2 9 2006/05/1 5 2006/05/1 6 SO P IN G 11 1 EP ACF R PT M 2 9 2006/05/1 6 2006/05/1 6 SO P IN G 11 1 EP ACF R PT M 2 9 2006/05/1 5 2006705/1 6 SO P IN G 11 1 EP ACF R PT M 2 9 Quantity



### (1 ) Thi s tes twa s performe

db yMaxxa mAnalytic

s Burlingto

n



### Jl Pagelof 1 1 674 0 Campobell o Road
. Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7*r'\ Driven by service

and Science £ 1 5^5 ^ S I IT" 1 - • ——" ^vww.ma3CXffliaai»alytf«-« 4 ' m 

### You rProjects : 10002-017-01 7 Site : ONYX

Attention : -Tef

f Gorma n ENS RInternationa

l 6601KirkvilleR

d Eas tSyracuse

, NY US A 1305

7 Repor tDate : 2006/05/2

0
f-F.RTIFICATF
. O FANALYSI S

-2 -

Valldate dby :

Tota lcove rpages: 2
Page2oM 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7

### Maxxa m Jo b # : A64446 9

Repor tDate : 2006/05/2 0 Driven by service

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### ENS R Internationa l Clien tProjec

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### MERCUR YBYCOL D VAPOU R AA(FILTER ) Maxxa m I D L9982 8 L9982 9 L9982 9 L9983 0 L9983 1 Samplin g Dat e 2006/05/1 0 2006/05/1 0 2006705/1 0 2006/05/1 0 2006/05/1 0 Unit s U3-M29-R B U3-M2&-R 1 U3-M29-R 1 Lab-Du p U3-M29-R 2 U3-M29-R 3 RD L O C Batc h MD L
Tota l Mercury- 1 B " 9 . N D N D N D 0.1 0 0.2 7 0.0 3 97239 5 0.0 3 N D = No tdetecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h

Pag e 3 o f1 1 

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### I V I £ 1 l^^S Analytics irt c Drh'en by s&n>ice

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### Maxxa m Jo b # : A64446 9 Repor tDate : 2006/05/2 0 ENS R Internationa l Clien tProjec

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### ELEMENT

S B YICP/MS (FILTER

) Maxxa m I D L9982 8 L9982 9 L9982 9 L9983 0 L9983 1 Samplin g Dat e 2006/05/1 0 2006/05/1 0 2006/05/1 0 2006/05/1 0 2006/05/1 0 Unit s U3-M29-R B U3-M29-R 1 U3-M29-R 1 Lab-Du p U3-M29-R 2 U3-M29-R 3 RD L 3 C Batc h MO L
Tota l Arseni c (As ) u g 0.7 6 9.2 9 9.6 2 24 9 94 6 0.40 . 97201 2 0.4 0 Tota l Berylliu m (Be ) u g N D N D N D N D N D 0.1 0 97201 2 0.1 0 Tota l Cadmiu m (Cd ) u g 0.3 4 0.6 8 0.7 1 1.3 8 2.7 6 0.1 0 97201 2 0.1 0 Tota l Chromiu m (Cr ) u g ^ 1.0 1 17. 7 19. 8 29. 0 55. 8 0.3 Q 97201 2 0.3 0 Tota i Lea d (Pb ) u g 2.7 0 23. 9 24. 1 22. 3 40. 6 0.2 0 97201 2 0.2 0 N D = No t detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h

Pag e 4 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7M



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### Maxxa m Jo b # : A64446 9 Repor tDate : 2006/05/2 0 Driven by service

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### ENS R Internationa l Clien tProjec

t# : 10002-017-01 7 Projec tname : ONY X Sample rInitials : 

### MERCUR YBYCOL D VAPOU R AA(IMPINGER SOLUTION ) Maxxa m I D L9982 8 L9982 9 L9982 9 Samplin g Dat e 2005705/1 0 2006/05/1 0 2006/05/1 0 Unit s U3-M29-R B RD L U3-M29-R 1 U3-M29-R 1 Lab-Du p RD L E2 C Batc h MD L
Total Mercury-2 B u g N D 0. 3 74. 7 75. 4 1. 6 97009 1 0.0 1 Tota l Mercury-3 A u g N D 0.0 1 3.3 8 3 4 0 0.1 3 97004 5 0.0 5 Tota l Mercury-3 B u g 0.0 4 0.0 2 10. 7 10. 7 0. 5 97006 6 0.0 5 Tota l Mercury-3 C u g N D 0.05 8.5 5 8.5 8 0.2 5 97132 2 0.0 5 N D = No t detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h 

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Maxxa m I D L9983 0 L9983 1 I Samplin g Dat e 2006/05/1 0 2006/05/1 0 I Unit s U3-M29-R 2 RD L U3-WI29-R 3 RD L 3 C Batc h 

### MD L Tota l Mercury-2 B u g 10 4 1. 7 78. 6 1. 5 97009 1 0.0 1 Tota l Mercury-3 A u g 1.2 9 0.0 2 1.2 6 0.0 2 97004 5 0.0 5 Tota l Metcuty-3 B u g 7.9 9 0.2 5 1.5 6 0.0 5 97006 6 0.0 5 Tota l Mercuiy-3 C u g 7.95 0.2 5 7.7 0 0.2 5 97132 2 0.0 5 RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h

Pag e 5 o f1 1 

### 674 0 Campobell o Road
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### ENS R Internationa l Clien tProjec

t# : 10002-017-01 7 Projec tname : ONY X Sample rInitials : Tes tSummar y
Maxxa m I D Sampl e I D Matri x L9982 8

U3-M29-R B Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinqer ) b yCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 FF S Mercury . 3 Ai n Ai r(HN0 3 Rinse ) b vCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 • FF S Mercur y2 8 i n Air(HN03/H20 2 Imp) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 FF S Mercur y3 B i n Ai r(KMn04/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 FF S Mercur y1 B -Ai r(Filter+Acetone ) bvCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 F F S Metal s i n A r(Combined ) b yICP/M S ICP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R
Maxxa m I D Sampl e I D Matri x L9982 9

U3-M29-R 1 Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinger ) b yCVA A CVA A 971.32 2 2006/05/1 6 2006705/1 8 FF S Mercur y3 Ai n Ai r(HN0 3 Rinse ) b vCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 ' FF S Mercur y2 B i n Air(HN03/H20 2 Imp) b vCV A CVA A 97009 1 2006/05/1 6 2006705/1 6 FF S Mercur y3 B i n Ai r(KMn04/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 F F S • Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 v. . F F S Metal s i n Ai r(Combined ) b vICP/M S IC P 1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R
Maxxa m I D Sampl e I D Matri x L99629Du p

U3-M29-R 1 Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinger ) b yCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 F F S Mercur y3 AI n Ai r(HN0 3 Rinse ) b vCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 •FF S Mercur y2 B i n AMHN03/H2C- 2 Imp) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 F F S Mercur y3 B i n Ai r(KMn04/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 ' FF S Mercur y1 B -Ai r(Filter+Acetone ) b yCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 FF S Metal s i n Ai r(Combined ) b vICP/M S ICP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R
Maxxa m I D Sampl e I D Matri x L9983 0

U3-M2S-R 2 Filte r Collecte d Shippe d Receive d 2006/0571 0

2006/05/1 2 Tes tDescriptio n instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I impingerlp yCVA A CVA A -97132 2 2006/05/1 6 2006/05/1 8 FF S Mercur y3 Ai n Ai r(HN0 3 Rinse ) b vCVA A CVA A 97004 5 2006/0571 5 2006/05/1 6 F F S Mercur y2 B I n AWHN03/H20 2 Imp) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 F F S Mercur y3 B i n Ai r(KMn04/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 F F S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 F F S Metal s i n Ai r(Combined ) b vICP/M S ICP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R

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### Maxxa m Jo b # : A64446 9 Repor tDate : 2006/05720

Pag e 6 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7J>rivctt by service

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### ENS R Internationa l Clien tProjec

t# : 1 0002-017-01 7 Projec tname : ONY X Sample rInitials : Tes tSummar y
Maxxa m I D L9983 1 Collecte d 2006/05/1 0 Sampi e I D U3-M29-R 3 Shippe d Matri x Filte r Receive d 2006705/1 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinqer) b yCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 F F S Mercur y3 Ai n Ai r(HN0 3 Rinse ) b yCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 FF S Mercur y2 B i n AMHNO3/H20 2 Imp ) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 F F S Mercur y3 B i n Ai r(KMn04/H2SQ4 ) b vCV A CVA A 97006 6 -2006/05/1 5 2006/05/1 6 F F S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 FF S Metal s i n Ai r(Combined ) b y.ICP/M S ICP1/M S 972012 . 2006/05/1 7 2006/05/1 9 N R

Page7o f1 1 

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### ENS R Internationa l Clien tProjec

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### Maxxa m Jo b #:A64446 9 Repor tDate : 2006/05/2 0

GENERA L COMMENT S ICPMS : Pos tdigestio n duplicat e an d spik e o n sampl e L9982 9
Result s relate onl yt o th e item s tested , .

Pag e 8 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax
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### ENS KInternationa l •www .1na22ramanniytic3.c01 n Attention : JeffGorma n Clien tProjec

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QA/Q C • Batc h Nu m Ini t QCTvp e Paramete r Dat e Analyze d ww/mm/d d Valu e %Recover y Unit s Q C Limit s 97004 5 FF S MATRI XSPIK E

(L99829 ) Tota l Mercury-3 A 2006/05/1 6 0.00 , RDL=0.1 3 10 2 u g 85-11 5 MATRI XSPIK E DUP(L99829 ) Tota l Mercury-3 A 2006/05/1 6 0.00 , RDL=0.1 3 10 5 " 9 85-11 5 Spike d Blan k

- Tota l Mercuty-3 A 2006/05/1 6 0.11 , RDL=0.0 1 10 6 u g 90-11 0 Spike d Blan k

DU P Tota l Mercury-3 A 2006/05/1 6 0.11,RDL=0.0 1 10 7 u g 90-11 0 Metho d Blan k Tota l Mercury-3 A 2006/05/1 6 ND , RDL=0.0 1 u g R P D Tota l Mercury-3 A 2006/05/1 6 0. 6 % 2 0 97006 6 FF S MATRI XSPIK E

(L99829 ) Tota l Mercury-3 B 2006/05/1 6 0.5 , RDL=0. 5 10 5 u g 85-11 5 MATRI XSPIK E D U P (L99829 ) Tota l Mercury-3 B 2006/05/1 6 0.5 , RDL=0. 5 10 7 u g 85-11 5 Spike d Blan k Tota l Mercury-3 B 2006/05/1 6 0.55 , RDL=0.0 5 11 0 u g 90-11 0 Spike d Blan k

DU P Tota l Mercury-3 B 2006/05/1 6 0.54 , RDL=0.0 5 10 8 u g 90-11 0 Metho d Blan k Tota l Mercury-3 B 2006/05/1 6 ND , RDL=0.0 5 u g RP D Tota l Mercury-3 B 2006/05/1 6 0.05 % 2 0 97009 1 FF S MATRI XSPIK E

(L99829 ) Tota l Mercury-2 B 2006/05/1 6 0.0,RDL=1. 6 10 0 u g 85-11 5 MATRI XSPIK E D U P (L99829 ) Tota l Mercury-2 B 2006/0571 6 0.0 , RDL=1. 6 9 5 u g 85-11 5 Spike d Blan k Tota l Mercuiy-2 B 2006/05/1 6 0.11 , RDL=0.0 1 10 7 u g 9 0 - 11 0 Spike d Blan k

DU P Tota l Mercury-2 B 2006/05/1 6 0.11 , RDL=0.0 1 10 9 u g 9 0 - 11 0 Metho d Blan k Tota l Mercury-2 B 2006/05/1 6 ND , RDL=0.0 1 u g R P D Tota l Mercury-2 B 2006/05/1 6 0. 9 % 2 0 97132 2 FF S MATRI XSPIK E

(L99829 ) Tota l Mercury-3 C 2006/05/1 8 0.54 , RDL=0.2 5 10 8 u g 85-11 5 MATRI XSPIK E D U P (L99829 ) Tota l Mercuiy-3 C 2006/05/1 8 0.54 , RDL=0.2 5 10 8 u g 85-11 5 Spike d Blan k Tota l Mercuiy-3 C 2006/05/1 8 0.51 , RDL=0.0 5 10 2 u g 90-11 0 Spike d Blan k

DU P Tota l Mercury-3 C 2006705/1 8 0.52 , RDL=0.0 5 10 3 u g 9 0 -11 0 Metho d Blan k Tota l Mercury-3 C 2006/05/1 8 ND , RDL=0.0 5 u g R P D Tota l Mercury-3 C 2006/05/1 8 0. 4 % 2 0 97201 2 N_ R MATRI XSPIK E

(L99829 ) Tota l Arseni c (As ) 2006705/1 9 49.5 , RDL=0.4 0 9 9 u s 70-13 0 MATRI XSPIK E D U P (L99829 ) Tota l Arseni c (As ) 2006/05/1 9 49.5 , RDL=0.4 0 9 9 u g 7 0 -13 0 MATRI XSPIK E (L99829 ) Tota l Berylliu m (Be ) 2006/05/1 9 44.5 , RDL=0.1 0 8 9 u g 70-13 0 MATRI XSPIK E D U P (L99829 ) Tota l Berylliu m (Be ) 2006/0571 9 45.5 , RDL=0.1 0 9 1 u g 70-13 0 MATRI XSPIK E (L99829 ) Tota l Cadmiu m (Cd ) 2006/05/1 9 26.0 , RDL=0.1 0 10 4 u g 7 0 -13 0 MATRI XSPIK E D U P (L99829 ) Tota l Cadmiu m (Cd ) 2006/0571 9 26.3 , RDL=0.1 0 10 5 u g 70-13 0 MATRI XSPIK E (L99829 ) Tota l Chromiu m (Cr ) 2006/05/1 9 52.5 , RDL=0.3 0 10 5 u g 70-13 0 MATRI XSPIK E D U P (L99829 ) Tota l Chromiu m (Cr ) 2006705/1 9 51.5 , RDL=0.3 0 10 3 u g 70-13 0 MATRI XSPIK E (L99829 ) Tota l Lea d (Pb ) 2006/05/1 9 50.5 , RDL=0.2 0 10 1 u g 70-13 0 MATRI XSPIK E D U P (L99829 ) Tota l Lea d (Pb ) 2006/05/1 9 50.5 , RDL=0.2 0 10 1 ug 70-13 0 Spike d Blan k Tota l Arseni c (As ) 2006/05/1 9 51.5 , RDL=0.4 0 10 3 u g 85-11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006/05/1 9 51.5 , RDL=0.4 0 10 3 ug 85-11 5 Spike d Blan k Tota l Berylliu m (Be ) 2006/05/1 9 47.0 . RDL=0.1 0 9 4 u g 85-11 5 Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006/05/1 9 47.0 , RDL=0.1 0 9 4 u g 85-11 5 

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### Qualit yAssuranc e Repor t Maxxa m Jo b Number . GA64446 9



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### Clien tProjec

t# : 10002-017-01 7 P.O
. # : Projectname : ONY X Qualit yAssuranc e Report(Continued ) Maxxa m Jo b Numbe rGA64446 9 QA/Q C Batc h Nu m Init QCTyp e Paramete r Dat e Analyze d yyyy/mm/d d Valu e %Recover y Unit s Q C Limit s 97201 2 N_ R Spike d Blan k Tota l Cadmiu m (Cd ) 2006/0571 9 25.8 , RDL=0.1 0 10 3 u g 8 5 - 11 5

Spike d Blan k

DU P Tota l Cadmiu m (Cd ) 2006705/1 9 25.8 , RDL=0.1 0 10 3 u g 85 - 11 5 Spike d Blan k Tota l Chromiu m (Cr ) 2006/05/1 9 53.0 . RDL=0.3 0 10 6 " 9 85 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/05/1 9 53.5 . RDL=0.3 0 10 7 u g 8 5 - 11 5 Spike d Blan k Tota l Lea d (Pb ) 2006/0571 9 51.0 , RDL=0.2 0 10 2 u g 85 - 11 5 Spike d Blan k

DU P Tota l Lea d (Pb ) 2006/0571 9 52.0 , RDL=0.2 0 10 4 u g 85 - 11 5 Metho d Blan k Tota l Arseni c (As ) 2006/05/1 9 ND , RDL=0.4 0 u g Metho d Blan k

DU P -Tota l Arseni c (As ) 2006/05/1 9 ND , RDL=0.4 0 u g Metho d Blan k Tota l Berylliu m (Be ) 2006/05/1 9 ND , RDL=0.1 0 . u g Metho d Blan k

DU P Tota l Berylliu m (Be ) 2006/05/1 9 ND . RDL=0.1 0 u g Metho d Blan k Tota l Cadmiu m (Cd ) 2006/05/1 9 ND , RDI=0.1 0 u g Metho d Blan k

DU P Tota l Cadmiu m (Cd ) 2006/05/1 9 ND , RDL=0.1 0 u g Metho d Blan k Tota l Chromiu m (Cr ) 2006705/1 9 ND , RDL=0.3 0 u g Metho d Blan k

DU P Tota l Chromiu m (Cr ) 2006/05/1 9 ND , RDL=0.3 0 •u g Metho d Blan k Tota l Lea d (Pb ) 2006/05/1 9 ND , RDL=0.2 0 u g Metho d Blan k

DU P Tota l Lea d (Pb ) 2006/05/1 9 ND , RDL=0.2 0 u g RP D Tota l Arseni c (As ) 2006/05/1 9 3. 5 % 2 0 Tota l Berylliu m (Be ) 2006/05/1 9 N C % 2 0 Tota i Cadmiu m (Cd ) 2006/05/1 9 3. 9 % 2 0 Tota l Chromiu m (Cr ) 2006/05/1 9 11. 2 % 2 0 Tota l Lea d (Pb ) 2006/05/1 9 0. 7 % 2 0 97239 5 FF S • MATRI XSPIK E

(L99829 ) Tota l Mercury-1 B 2006/05/1 8 0.30 , RDL=0.0 3 9 9 u g 85 - 11 5 MATRI XSPIK E DU P (L99829 ) Tota l Mercury- 1 B 2006/05/1 8 0.30 , RDL=0.0 3 10 0 u g 85 - 11 5 Spike d Blan k Tota l Mercury- 1 B 2006/05/1 8 0.31 , RDL=0.0 3 10 3 u g 90 - 11 0 Spike d Blan k

DU P Tota l Mercury- 1 B 2006/05/1 8 0.31,RDL=0.0 3 10 3 u g 90 - 11 0 Metho d Blan k Tota l Mercury- 1 B 2006/05/1 8 ND , RDL=0.0 3 u g RP D Tota l Mercury- 1 B 2006/05/1 8 N C % 2 0 N D = No t detecte d SS C = Non-calculabl e RP D = Relativ e Percen tDifferenc e SPIK E = Fortifie d sampl e 

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### Validatio n Signatur e Pag e

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FRAN KMO , B.Sc , Inorgani cLab. Manage

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### Maxxa m Jo b # : A64446 9

Pag e 1 1 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7

### Sectio n I : Sampl e Inventor yRepor t Date Received : 

### ProjectNo. : ProjectName : 6/22/200 6 2780 3 10002-01

7
Lab
. Sampl e I D Clien tSampl e I D Componen tI D 

### 001 00 2 00 3 00 4 00 5 00 6 00 7 U3-M23A-XAD-R 1 U3-M23A-PF-R 1 U3-M23A-XAD-R 2 U3-M23A-PF-R2 U3-M23A-XAD-R 3 U3-M23A-PF-R3 U3-M23A-XAD-F B B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R BH/F HACE/MeC12/TO L FILTE R XA D

Projec t2780 3 Smpinvgnmm5,rpt



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### Metho d Blan k . .Method,0023 A

Matrix : MM 5 Q C Batc hNo. : 812

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### Dat eAnalyzedDB-5 : 26-Jun-0 6 Dat

eAnalyzedDB-225 : N A AnalyteCone . (pg/Sample) D L a

### EMP C -u 

### Qualifiers Labele dStandard % R LCL-UCL d

### Qualifier s 2,3^>TCDD: : 0.87 9 IS 13C-2,3,7,8-TCDD 93. 8 40 - 13

5 1,2,3,7,8-PeCDD N D 0.80 2 13C-l,2,3,7,8-PeCD D 88. 8 40-13 5 1,2,3,4,7,8-HxCDD N D 1.6 9 13C-l,2,3,6,7,8-HxCD D 85. 3 40-13 5 1,2,3,6,7,8-HxCDD N D 1.4 3 13C-1,2,3,4,6,7,8-HpCDD 77. 3 40 - 13

5 1,2,3,7,8,9-HxCDD N D 1.5 5 13C-OCD D 59. 8 40-13 5 1,2,3,4,6,7,8-HpCDD N D 1.8 2 13C-2,3,7,8-TCDF 82.1 40 - 13 5 OCD D : 

### :ND 6.9 5 13C-l,2,3,7,8-PeCD F 77. 9 40-13 5 2,3,7,8-TCD F N D 1.0 8 13C-l,2,3,6,7,8-HxCD F 95. 9 40-13 5 1,2,3,7,8-PeCDFi 1.4 5 - 13C-1,2,3,4,6,7,8-HpCDF ; 

### 79. 6 40-13 5 2,3,4,7,8-PeCDF N D 1.3 3 13C-OCD F 23. 2 40 - 13

5 H l^a^^HxCD F N D 0.58 7 ; 

### PS 37Ci-2,3,7,8-TCD D 10 1 70-13 0 v 

### 1,2,3,6,7,8-HxCDF N D 0.46 9 13C-2,3,4,7,8-PeCDF 99. 6 70-13 0 2,3,4i6,7i8-HxCp F N D 0.55 2 ; 13C-l,2,3,4,7,8-HxCD D 95. 2 70-13 0 1,2,3,7,8,9-HxCDF N D 0.70 7 13C-1,2,3,4,7,8-HxCDF 88. 0 70-13 0 l^^^.S-HpCD F : 0.38 6 , • J 13C-l,2,3,4,7,8,9-HpCDF : - 73.1 . 70 - 1.30 , 1,2,3,4,7,8,9-HpCDF N D 0.84 6 A S 13C-1,2,3,7,8,9-HxCDF 83. 3 40-13 5 OCD F N D 7.4 6 \ Total s Toxi cEquivalentQuotient(TEQ ) Data e Tota lTCD D N D 0.87 9 TE Q (Min-Max) : 0.0038 6 - 2.8 7 TotalPeCD D •'-'N D 0.66 9 Tota lHxCD D N D 1.5 5 a . Sampl e specifi cestimate d detectio n limit
. 

### TotalHpCDD : ; :;ND \. 1.8 2 b
. Estimate d maximu m possibl e concentration
. 

### Tota lTCD F N D 1.0 8 c . Metho d detectio n limit
. 

### TotaiyPeCDF 

### ; NDy- 1.3

9 7 d
. Lowe rcontro l limi t- uppe rcontro l limit
. 

### Tota lHxCD F N D 0.56 6 e . TE Q base d o n (1989 ) Internationa l Toxi cEquivalen tFactor s (ITEF)
. 

### Tota iHpCD F 0.38 6 Analyst-
. 

### j^ gApprove d By : 

### WilliamJ
. 

### Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t4 o f 46 6O P R Result s 

### Metho d 0023 A Matrix : MM 5 Q C Batc h No. : 812 0 La b Sample : 0-OPR00 1 Sampl e Size : Sampl e Dat e Extracted : 22-Jun-0 6 Dat

eAnalyzedDB - 5 : 26-Jun-0 6 Dat

eAnalyzedDB-225 : N A Analyte SpikeCone . Cone . (ng/mL ) OP RLimits LabeledStandard % R LCL-UC L 2 ,3 ,7 ,8 -TCD D 2.5 0 2.4

8 1 .75 -3 .2 5 I S 13C-2 ,3 ,7 ,8 -TCD D 84 . 5 40-13 5 1 ,2 ,3 ,7 ,8 -PeCD D 12. 5 12.

6 8 .75 -16.25 13C-l,2 ,3 ,7 ,8 -PeCD D 82
. 3 40 - 13 5 1 ,2 ,3 ,4,7 ,8 -HxCD D 12. 5 12
. 8 8 .75 - 16.2 5 13C-l,2 ,3 ,6,7 ,8 -HxCD D 79
. 1 40 - 13 5 1,2 ,3 ,6,7 ,8 -HxCD D 12. 5 14.

0 8 .75 -16.25 13C-l,2 ,3 ,4,6,7 ,8 -HpCD D 77. 4 40 - 13

5 1 ,2 ,3 ,7 ,8 ,9-HxCD D 12. 5 1

4 0 8 .75 - 16 .25 13C-OCD D 62.9 40 - 13 5 1 ,2 ,3 ,4,6,7 ,8 -HpCD D 12. 5 12.

0 8 .75-16.2 5 13C-2 ,3 ,7 ,8 -TCD F 78
. 1 40 - 13 5 OCD D 25. 0 • 24.

7 \17.5-32. 5 13C-l,2 ,3 ,7 ,8 -PeCD F 75
. 4 4 0 - 13 5 : : 2 ,3 ,7 ,8 -TCD F 2.5 0 2.4

0 1.75-3.25 13C -l,2 ,3 ,6,7 ,8 -HxCD F 83. 5 40-13 5 l,2 ,3 ,7 ,8irPeCDF , : J ; . 

## 7 / K12. 5 ; 12.

5 : 8 .75 - 16.2 5 13C-1,2 ,3 ,4,6,7 ,8 -HpCD F 7 8 7 40-13 5 2 ,3 ,4,7 ,8 -PeCDF 12. 5 11. 8 8 .75-16.2 5 13C-OCD F 27. 2 40-13 5 1,2 ,3, 4 j , 8 . H ^Cr)F, v 12. 5 12
. 3 8 .75 - 16.2 5 ; A S 13C -1, 2 ,3 ,7 ,8 ,9- 1 IxCD l 90. 7 40-13 5 1,2 ,3 ,6,7 ,8 -HxCD F 12. 5 13.

9 8 .75 -16.25 2 ,3,4 ,6,7 ,8 -HxCD F 13. 6 8 .75-16,2 5 1 ,2 ,3 ,7 ,8 ,9-HxCD F 12. 5 12.

9 8 .75 -16.25 1 ,2 ,3 ,4,6,7 ,8 -HpCD F 12. 5 12
. 8 8,7 5 -16.25 , 1 ,2 ,3 ,4,7 ,8 ,9-HpCD F 12. 5 8 .92 8 .75 - 16.2 5 OCD F 25.0 24. 7 17,5-32. 5 : Analyst : RA S Approve d By : WilliamJ . Luksembur g27-Jun-200

6 15 :1 1

Projec t2780 3 Projec t5 o f 46 6Sampl eID : U3-M2 3 A-XAD--R 1 • 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : ENS R Project : 10002-01 7 Dat e Collected : 19-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : MM 5

Sampl e La b Sample : 27803-001

Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 26-Jutl-0 6 Dat e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Date s Analyze d DB-22 5 : 27-Jun-0 6 Analyte Cone . (pg/Sample) D L a EMPC b Qualifiers Labele dStandard % R LCL-UCL dQualifier s 2,3,7,8-TCD D 7 N D 3.6 4 I S 13C-2,3,7,8-TCDD 91.6 40 - 13 5 1,2,3,7,8-PeCDD 17. 0 J 13C-1,2,3,7,8-PeCDD 88. 7 40-13 5 1,2,3,4,7,8-HxCDD : 19. 1 . J 13C-l,2,3,6,7,8-HxCD D 89. 2 V40-13 5 1,2,3,6,7,8-HxCDD 46. 1 J 13C-1,2,3,4,6,7,8-HpCDD 96. 7 40-13 5 1,2,3,7,8,9- HXCPD ; 37.0
. J 13C-OCDD . 10 5 . 4 0 - 13 5 1,2,3,4,6,7,8-HpCDD 19 0 13C-2,3,7,8-TCD F 88. 3 40-13 5 OCD D ^ 23 6 13C-l,2,3,7,8-PeCD F 80. 4 40-13 5 2,3,7,8-TCD F 29. 5 13C-l,2,3,6,7,8-HxCD F 97.0 40-13 5 l,2,3;7,8-PeCD F r : I 35. 5 J 13C-1,2,3,4,6,7,8-HpCDF 92. 7 40-13 5 2,3,4,7,8-PeCDF 65. 4 13C-OCD F 83. 4 40 - 13

5 1,2,3,4,7,8-HxCDF 36.0 ": . i" P J 37Cl-2,3,7,8-TCD D 86.1 7 0 - 13 0 1,2,3,6,7,8-HxCDF 31. 9 J,D 13C-2,3,4,7,8-PeCDF 91. 4 70-13 0 2;3i4;6,7,8-HxCP

F • 43. 8 . J' 13C-1,2,3,4,7,8-HxCDD • J : 85.

7 70- : 13

0 1,2,3,7,8,9-HxCDF 10. 3 J 13C-1,2,3,4,7,8-HxCDF 85. 9 70-13 0 1,2,3,4 X 7,8- HRCD F 78.1 B 13C-l,2,3,4,7,8,9-HpCD F 77.9 ,70-130 ; . 1,2,3,4,7,8,9-HpCDF 8.10 J A S 13C-1,2,3,7,8,9-HxCDF 95. 2 40 - 13

5 OCD F :

" 20.

4 J 

### Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota lTCD D 118 0 TE Q (Min-Max) : 71. 4 - 75.0 Tota lPeCD D 86 9 ; Tota lHxCD D 147 0 a . Sampl e specifi cestimate d detectio n limit
. Tota lHpCD D 412 b
. Estimate d maximu m possibl e concentration
. Tota lTCD F 108 0 c . Metho d detectio n limit
. Tota lPeCD F 80 0 D d
. Lowe rcontro l limi t- uppe rcontro l limit
. Tota lHxCD F 39 1 39 5 D e . TE Q base d o n (1989 ) Internationa l Toxi cEquivalen tFactor s (ITEF)
. Tota lHpCD F 11 2 : ' B Analyst : RA S Approve d By : WilliamJ
. Luksembur g27-Jun-200

6 15:11
Proiec t2780 3 Projec t6 o f 46 6

### SamplelD : U3-M23A-PF-R 1 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 19-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 

### 27803-00 2 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 26-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Dat e Analyze d DB-225 : 

### Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifiers Labele dStandard % R LCL-UCL d

### Qualifier s 2,3,7,8-TCD D 7^:

: - N D 1.1 8 I S : 

### ;i3C-2,3,7,8-TCDD : , \ 91. 5 40-13 5 1,2,3,7,8-PeCDD N D 1.3 8 13C-l,2,3,7,8-PeCD D 92. 8 40-13 5 1,2,3,4,7,8-HxCtlD ' ••'ND- ; -• : 

### 2.7 6 >: : 13C-l,2,3,6;7,8-HxCD D ; 89. 4 40-13 5 1,2,3,6,7,8-HxCDD N D 2.3 3 13C-1,2,3,4,6,7,8-HpCDD 83.1 40 - 13 5 1,2,3,7,8,9-HxCDD :. ' N D 2.5 3 13C-OCD D 86. 7 40 - 13

5 1,2,3,4,6,7,8-HpCDD N D 2.5 2 13C-2,3,7,8-TCDF 85. 3 40-13 5 OCD D 10. 8 J 13C-l,2,3,7,8-PeCD F 82. 3 4 0 - 13 5 2,3,7,8-TCD F N D 1.2 7 13C-l,2,3,6,7,8-HxCD F 97. 8 4 0 - 13 5 1,2,3,7,8-PeCDF :.ND,.... . 1.5 1 13C-l,2,3,4,6,7,8-HpCD F ^ 80. 9 40 - 13

5 . 2,3,4,7,8-PeCDF N D 1.3 8 13C-OCD F 69.1 40-13 5 1,2,3,4,7,8-HxCDF N D 0.92 3 ES ; 37Cl-2,3,7,8-TCD D i: 94. 4 7 0-13 0 1,2,3,6,7,8-HxCDF N D 0.73 7 13C-2,3,4,7,8-PeCDF 93. 9 70 - 13

0 2,3,4,6,7,8-HxCDF N D 0.86 8 13C-1,2,3,4,7,8-HxCDD 90. 7 ; : 

### 70>:i3 0 : • 1,2,3,7,8,9-HxCDF N D 1.11 13C-l,2,3,4,7,8-HxCD F 87. 4 70-13 0 1,2,3,4,6,7,8-HpCDF "N D 1.2 9 13C-1,2,3,4,7,8,9- 1 lpCD F 79.0 70-13 0 1,2,3,4,7,8,9-HpCDF N D 1.11 A S 13C-l,2,3,7,8,9-HxCD F 93. 7 40-13 5 OCD F ::'NDv 5.0 2 Total s Toxi cEquivalentQuotient(TEQ ) Data c 

### Tota lTCD D N D 1.1 8 TE Q (Min-Max) : 0.010 8 - 3.9 5 TotalPeCP D 7ND:,; : 

### A 1-3 8 Tota lHxCD D N D 3.3 4 a . Sampl e specifi c estimate d detectio n limit . 

### Tota lHpCD D 1.7 7 b . Estimate d maximu m possibl e concentration . 

### Tota lTCD F N D 1.2 7 c . Metho d detectio n limit . 

### Tota lPeCDF : ; /

; 7 ii4 4 - d . Lowe rcontro l limi t-uppe rcontro l limit . 

### Tota lHxCD F N D 0.89 0 e . TE Q base d o n (1989 ) Internationa l Toxi c Equivalen tFactor s (ITEF) . 

### Tota lHpCD F ; NI) 1.4 9 : " Analyst : 

### RA S Approve d By : 

### WilliamJ . Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t7 of 46 6

### SamplelD : TJ3-M23A-XAD-R 2 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 20-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 

### 27803-00 3 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 27-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Date s Analyze d DB-225 : 

### 27-Jun-0 6 Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifier s LabeledStandard % R LCL-UCL d

### Qualifier s 2,3,7,8-TCD D : ; 

### ; : 3.4 4 

### . V J IS ; 13a2,3,7;8-TCD D 90. 7 40-13 5 1,2,3,7,8-PeCDD 17. 6 J 13C-1,2,3,7,8-PeCDD 96. 2 40-13 5 1,2,3,4,7,8-HxCDD ; 

### 16. 8 J 13e-J,2,3,6,7,8-HxCDD ; 90.0 ;;40--135 : • 1,2,3,6,7,8-HxCDD 34. 7 J 13C-l,2,3,4,6,7,8-HpCD D 89.1 40 - 13 5 1,2,3,7,8,9-HxCp b 27. 1 J" • 13C-OCD D 88. 8 40-13 5 1,2,3,4,6,7,8-HpCDD 17 5 13C-2,3,7,8-TCD F 84. 8 40 - 13

5 OCD D 17 5 i :i3C-l,2,3,7,8-PeCD F 91. 8 40-13 5 2,3,7,8-TCD F 32. 8 13C-l,2,3,6,7,8-HxCD F 96. 2 40-13 5 U^^PeCDF / : 41.2 • J 13C- 1,2,3,4,6,7,8-HpCDF 83.0 • ; ; 

### ;.40;-;i35-: - 2,3,4,7,8-PeCDF 70. 2 13C-OCD F 59. 8 

### 40-135 1,2i3,4,7,8-HxCDF 33.0 : •'•>'"' J E S 37Cl-2,3,7,8-TCD D : 99. 4 70-13 0 1,2,3,6,7,8-HxCDF 31. 7 J,D 13C-2,3,4,7,8-PeCDF 89. 2 70 - 13

0 2,3,4,6,7,8-HxCDF ,

; . 41.8 J 130-1,2,3,4,7,8^x00 0 92. 3 • 70 - 13

0 ; 1,2,3,7,8,9-HxCDF 11. 6 J 13C-l,2,3,4,7,8-HxCD F 92. 3 70 - 13

0 1,2,3,4,6,7,8-HpCDF : 

### 66. 8 B 13C-l,2,3,4,7,8,9-HpCD F 83, 2 70 - 13

0 1,2,3,4,7,8,9-HpCDF 5.2 1 J A S 13C-l,2,3,7,8,9-HxCD F 99. 2 40 - 13

5 OCD F • 14. 8 J Total s Toxi cEquivalentQuotient(TEQ ) Dat a e 

### Tota lTCD D 121 0 TE Q (Min-Max) : 75. 0 - 75.0 TotalPeCD D : ; 84 8 Tota lHxCD D 133 0 a . Sampl e specifi c estimate d detectio n limit . 

### Tota lHpCD D ,.•'381 ' b , Estimate d maximu m possibl e concentration . 

### Tota lTCD F 135 0 c . Metho d detectio n limit . 

### Tota lPeCD F 86 2 D d . Lowe rcontro l limi t- uppe rconlro l limit . 

### Tota lHxCD F 39 0 D e . TE Q base d o n (1989 ) Internationa l Toxi c Equivalen tFactor s (ITEF) . 

### Tota lHpCD F 987 0 . B Analyst : RA S Approve d By : 

### WilliamJ . Luksembur g 27-Jun-200

6 15:11 Projec t2780 3 Projec t8 of 46 6

### SamplelD : U3-M23A-PF-R 2 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 20-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 

### 27803-00 4 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 27-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Dat e Analyze d DB-225 : N A 

### Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifier s Labele dStandard % R LCL-UCL d

### Qualifier s 1.2 1 . IS13C-2,3,7,8-TCD D 95. 2 40-13 5 1,2,3,7,8-PeCDD N D 3.2 6 13C-l,2,3,7,8-PeCD D 10 1 40 - 13

5 1,2,3,4,7,8-HxCDP;i - 

### hNp;;'' " 2.6 3 13C-1,2,3,6,7,8-HxCDD 94. 3 40 - 13

5 1,2,3,6,7,8-HxCDD N D 2.2 3 13C-l,2,3,4,6,7,8-HpCD D 83. 0 40-13 5 1,2,3,7,8,9-HxCDD N D ; 2.41 13C-OCD D 88. 2 40-13 5 .. ; 1,2,3,4,6,7,8-HpCDD N D 4.12 13C-2,3,7,8-TCD F 92.6 40-13 5 OCD D : : 

### :;ND - . 6.3 3 DC -i ^SJ^-PeCD F 88.9 40-13 5 2,3,7,8-TCD F N D 0.951 13C-l,2,3,6,7,8-HxCD F 10 1 40-13 5 l,2,3i7iB-PeCD F : 

### •' ' 

### NP,: ' 

### ; • 3:4 4 13C-l,2,3,4,6,7,8-HpCD F 79. 5 40-13 5 2,3,4,7,8-PeCDF N D 3.14 13C-OCD F 61. 5 40-13 5 1,2,3,4,7,8-HxCDF N D : 0:68 4 ; w E S 37 C 1 T 2,3,7,8- TCD D 97. 5 70-13 0 1,2,3,6,7,8-HxCDF N D 0.54 6 13C-2,3,4,7,8-PeCDF 99. 4 70 - 13

0 2,3,4,6,7,8- HXCPF " 

### ; 'Npr : 

### : r v 

### -- , 0,64 3 • 13C-l,2,3,4,7,8-HxCD D 95.0 70-13 0 1,2,3,7,8,9-HxCDF N D 0.82 3 13C-1,2,3,4,7,8-HxCDF 88. 7 70 - 13

0 1,2,3,4,6,7,8-HpCDF : 

### N D 0.70 5 13C-l,2,3,4,7,8,9-HpCD F 79. 4 70 - 13

0 1,2,3,4,7,8,9-HpCDF N D 0.971 A S 13C-l,2,3,7,8,9-HxCD F 92.8 40-13 5 OCD F : 

### ^ND ; 

### - 6.3 8 Total s Toxi cEquivalentQuotient(TEQ ) Data e 

### Tota lTCD D N D 1.2 1 TE Q (Min-Max) : 0-5 .7 4 "TatalP ^CDP ^ 

### : : N D 3.2 6 Tota lHxCD D N D 2.4 1 a . Sampl e specifi c estimate d detectio n limit . 

### TotalHpCD D N D 4.12 b . Estimate d maximu m possibl e concentration . 

### Tota lTCD F N D 0.951 c . Metho d detectio n limit . 

### Tota lPeCD F N D 3 2 8 d . Lowe rcontro l limit : uppe rcontro l limit . 

### Tota lHxCD F N D 0.66 0 e . TE Q base d o n (1989 ) Internationa l Toxi c Equivalen tFactor s (ITEF) . 

### tota l HpCD F N D 0.817 Analyst : 

### RA S Approve d By : 

### WilliamJ . Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t9 o f 46 6

## Sample ^i;.-\-:^3-ya3A'XA^-^t3 - Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 2

1 -Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 

### 27803-00 5 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 27-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Date s Analyze d DB-225 : 

### 27-Jun-0 6 Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifier s Labele dStandard 

### % R LCL-UCL d

### Qualifier s 2,3,7,8-TCD D 7 : 

### ND; . > , 3.9 2 I § 13C-2,3,7,8-TCDD 88. 3 40 - 13

5 1,2,3,7,8-PeCDD 16. 7 

### J 13C-1,2,3,7,8-PeCDD 94.0 40 - 13 5 l,2,3;4,7i8rHxCDE> 14.6 : ''••V.'J. :

### 7' - 13C-l,2,3;6,7,8-HxCDD 89. 7 40 - 135 -7'
. 1,2,3,6,7,8-HxCDD 35. 7 

### J 13C - 1,2,3,4,6,7,8-HpCDD 95. 2 40 - 13

5 1,2,3,7,8,9- 1 IxCD D 26. 3 • 'J"'' : 

### . 13C-OCD D 95. 9 40-13 5 1,2,3,4,6,7,8-HpCDD 15 6 13C-2,3,7,8-TCDF 86. 6 40 - 13

5 OCD D 14 1 13C-l,2,3,7,8-PeCD F 84. 3 40 - 13

5 2,3,7,8-TCD F 31. 8 13C-l,2,3,6,7,8-HxCD F 95.9 40-13 5 1,2,3,7,8-PeCDF 41.1 J 13C-l,2,3,4,6,7,8-HpCD F : r 

### 90. 8 40-13 5 2,3,4,7,8-PeCDF 76. 2 13C-OCD F 81. 0 40 - 13

5 1,2,3,4,7,8-HxCP

F 37.8 7"-'J7/ £ S 37Cl-2,3,7,8-TCD D : 98. 2 70 - 13

0 1,2,3,6,7,8-HxCDF 33. 6 J,D 13C-2,3,4,7,8-PeCDF 97. 8 70 - 13

0 2,3,4,6,7,8-HxCDF 44.9 ; 

### J 13C-l,2,3,4,7,8-HxCD D 92. 9 70 - 13

0

### 77 7 1,2,3,7,8,9-HxCDF 11. 1 J 13C-1,2,3,4,7,8-HxCDF 90. 7 70-13 0 i,2,3y4,6,7,8-HpCDF 70. 7 B 13C-l,2,3,4,7,8,9-HpCDl ; 

### 92. 5 70 - 13

0 1,2,3,4,7,8,9-HpCDF 7.15 J A S 13C-l,2,3,7,8,9-HxCD F 91. 1 40 - 13 5 OCD F 13. 2 j ; 

### - 7 Total s Toxi cEquivalentQuotient(TEQ ) Data e 

### Tota lTCD D 87

9 89 9 TE Q (Min-Max) : 74.6 - 78 . 5 Tota lPeCD D .\-686 : 

### 7 :; 

### ' Tota lHxCD D 111 0 a . Sampl e specifi c estimate d detectio n limit . 

### TotalHpCD D '33 5 b . Estimate d maximu m possibl e concentration . 

### Tota lTCD F 131 0 c . Metho d detectio n limit . 

### Tota lPeCD F > ' 

### 794

8 ' : 

### D d . Lowe rcontro l limi t- uppe rcontro l limit . 

### Tota lHxCD F 410 D e . TE Q base d o n (1989 ) Internationa l Toxi c Equivalen tFactor s (ITEF) . 

### TotalHpCD F 10 2 ' B Analyst : RA S Approve d By : 

### WilliamJ . Luksembur g 27-Jun-200

6 15:11 Projec t2780 3 Projec t1 0 of 46 6

### Sampl eID- ' •; ; i7U3-M23A-PF-R 3 : 

### Metho;d : 

### 0.023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 21-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 27803-00 6 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 27-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Dat e Analyze d DB-225 : N A 

### Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifiers Labele dStandard % R LCL-UCL d

### Qualifier s 2,3,7,8-TCD D N D 1.4 0 IS 13C-2,3,7,8-TCDD 8 8 4 40-13 5 1,2,3,7,8-PeCDD N D 3.8 3 13C-l,2,3,7,8-PeCD D 93.9 40 - 13 5 1,2,3,4,7,8-HxCDD N D 2.1 3 13C- 1,2,3,6,7,8-HxCDD . 92. 5 40 - 13

5 1,2,3,6,7,8-HxCDD N D 1.8 1 13C-1,2,3,4,6,7,8-HpCDD 95.6 40 - 13 5 ] ,2,3,7,8,9-HxCD D 

# •I N D - 1,9 6 13C-OCD D 94.0 40 - 13 5 1,2,3,4,6,7,8-HpCDD N D 2.5 3 13C-2,3,7,8-TCDF 89. 7 40 - 13

5 OCD D 

## 'j ;:lp\l,; . '] . 13C-J,2,3,7,8-PeCDF 84.1 40-13 5 2,3,7,8-TCD F N D 1.1 5 13C-l,2,3,6,7,8-HxCD F 99. 3 40 - 13

5 1,2,3,7,8-PcCDF N D 3.0 0 13C-1,2,3,4,6,7.8- 1 IpCDI ' 97. 3 40 - 13

5 2,3,4,7,8-PeCDF N D 2.7 4 13C-OCD F 85. 9 40-13 5 1,2,3,4,7,8-HxCDF 

# ; : r0.641 ^ 3701-2,3,7,8^00 0 10 0 70 - 13

0 1,2,3,6,7,8-HxCDF N D 0.512 13C-2,3,4,7,8-PeCDF 10 4 70-13 0 :i3l4,6,7,;8-HxCPF 0.60 3 13C-l,2,3,4,7,8-HxCD D 94. 3 70 - 13

0 1,2,3,7,8,9-HxCDF N D 0.771 13C-l,2,3,4,7,8-HxCD F 90. 4 70-13 0 1,2,3,4,6,7,8-HpCDF N D 0.819 13C-l,2,3,4,7,8,9-HpeD F 91. 8 70-13 0 1,2,3,4,7,8,9-HpCDF N D 0.60 2 A S J3C-1,2,3,7,8,9-HxCDF 99. 0 40-13 5 OCD F N D 3.8 4 Total s Toxi cEquivalentQuotient(TEQ ) Data e 

### Tota lTCD D N D 1.4 0 TE Q (Min-Max) : 0.0101 - 5.8 5 Tota lPeCP D : ;N P 3.8 3 Tota lHxCD D 3.3 5 a . Sampl e specifi cestimate d detectio n limit
. 

### Tota lHpCD D ,,ND::,.7\:: ; 

### ' 

# i- 2.5 3 b
. Estimate d maximu m possibl e concentration , i 

### Tota lTCD F N D 1.1 5 c . Metho d detectio n limit
. 

### TotalPeCD F ; - : ;N D 2.8 6 ; 

### ; d
. Lowe rcontro l limi t- uppe rcontro l limit
. 

### Tota lHxCD F N D 0.618 e . TE Q base d o n (1989 ) Internationa l Toxi cEquivalen tFactor s (ITEF)
. 

### TotalT$CDF /

; / N D ' 0,95 0 V ; Analyst : 

### RA S Approve d By : 

### WilliamJ . Luksembur g27-Jun-200

6 15:1 1 Projec t2780 3 Projec t1 1 o f 46 6

### SamplelD : U3-M23A-XAD--F B 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : 

### ENS R Project : 

### 10002-01 7 Dat e Collected : 

### 20-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : 

### MM 5

Sampl e La b Sample : 

### 27803-00 7 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 

### 26-Jun-0 6 Dat e Received : 

### 22-Jun-0 6 Dat e Extracted : 

### 22-Jun-0 6 Dat e Analyze d DB-225 : ]\J A 

### Analyte Cone . (pg/Sample) D L a 

### EMPC b 

### Qualifiers LabeledStandard 

### % R LCL-UCL d

### Qualifier s 2,3,7,8-TCD D ; : • • ND . 0.84 5 IS ,13C-2,3,7,8-TCDD 88. 4 40-13 5 1,2,3,7,8-PeCDD N D 0.84 4 13C-1,2,3,7,8-PeCDD 89. 2 40-13 5 1,2,3,4,7,8-HxCDD N D 1.3 8 13C-l,2,3,6,7,8-HxCD D i 93. 7 ,\40-:i35.' ! 

### ^ 1,2,3,6,7,8-HxCDD N D 1.1 6 13C-1,2,3,4,6,7,8-HpCDD 80. 2 40 - 13

5 1,2,3,7,8,9-HxCDD, , N D 1.2 6 13C-.QCDD 84. 5 ;40;-,13

5 1,2,3,4,6,7,8-HpCDD N D 1.4 2 13C-2,3,7,8-TCDF 85. 9 40-13 5 OCD D N D 4 29. ; 13G-l,2,3;7,8-PeCDF 81. 7 40 - 13

5 2,3,7,8-TCD F N D 0.73 2 13C-i;2,3,6,7,8-HxCD F 96. 2 40 - 13

5 1,2,3 ,7 ,8-PeCDF :-

. N D "; . 1.1

5 I3C-l,2,3,4,6,7,8-HpCD F 81.1 40 - 13 5 2,3,4,7,8-PeCDF N D 1.0 5 13C-OCD F 59.9 40 - 13 5
,1,2,3,4,7,8-HxCDF : 0.401 E § 37Cl-2,3,7,8-TCPD 95. 3 70 - 13

0 1,2,3,6,7,8-HxCDF N D 0.32 0 13C-2,3,4,7,8-PeCDF 96. 5 70-13 0 2,3,4,6,7,8-HxCDF •;.Nb : 7 0.377; : 13C-l,2,3,4 ,7 ,8-HxCD D 88. 0 70 - 13

0 ,:] • ' 1,2,3,7,8,9-HxCDF 0.48 3 13C-1,2,3,4,7,8-HxCDF 90. 4 70-13 0 1,2,3,4,6,7,8-HpCDF N D 0.66 6 13C^,2,3,4,7,8,9-HpCD F : 

### 76. 2 .7 0 K130 • 1,2,3,4,7,8,9-HpCDF N D 0.918 A S 13C-1,2,3,7,8,9-HxCDF 90. 6 40-13 5 OCD F N D 3.7 0 Total s Toxi cEquivalentQuotient(TEQ ) Dat a e 

### Tota lTCD D N D 0.84 5 TE Q (Min-Max) : 0-2 .5 0 TotaiPeCD D N D 0.84 4 Tota lHxCD D N D 1.2 6 a . Sampl e specifi c estimate d detectio n limit . 

### Tota lHpCD D N D 1.4 2 b . Estimate d maximu m possibl e concentration , 

### Tota lTCD F N D 0.73 2 c . Metho d detection , limit . 

### Tota lPeCD F N D 1.1 0 : d . Lowe rcontro l limi t- uppe rcontro l limit . 

### Tota lHxCD F N D 0.38 7 e . TE Q base d o n (1989 ) Internationa l Toxi c Equiv s len tFactor s (ITEF) . 

### Tota lHpCD F N D 0.77 2 Analyst : Approve d By : 

### WilliamJ . Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t1 2 of 46 6

### PROJEC T NARRATIV E

MaxxamAnalytic s (BurlingtonON ) MaxxamJo b #

: A66217

5 Client : ENS RInternationa l ClientProject : 10002-017-82 0 ONY X I . SAMPL ERECEIPT/ANALYSI S
a ) Sampl eListing MaxxamClientDat eDat

eDat

eDat

e ID Samplel D Sample dReceivedPreppedRu n Metals i nAi r(BackHalf ) vi aEP A Method2

9 M7314 6 M29-RBB H2006/06/21 2006/06/2 2 2006/06/2

9 2006/06/2

9 M7314 7M29-U3-R1B H2006/06/19 2006/06/2 2 2006/0672

9 2006/06/2

9 M7314 7Du p M29-U3-R 1 B H2006/0671 9 2006/06/2

2 2006/06/2

9 2006/06/2

9 M7314 8 M29-U3-R2B H2006/06/2 0 2006/06/2

2 2006/06/2

9 2006/06/2

9 M7314 9 M29-U3-R

3 B H2006/06/21 2006/06/2 2 2006/06/2

9 2006/06/2

9 Metals i nAi r(FrontHalf ) vi aEP A Method2 9 M7314 2M29-RB F H2006/06/21 2006706/2 2 2006/06/2

8 2006/06/2

9 M7314 3 M29-U3-R 1 F H2006/06/19 2006/06/2 2 2006/06/2

8 2006/06/2

9 M7314 3 Dup M29-U3-R 1 F H2006/06/19 2006/06/2 2 2006/06/2

8 2006/06/2

9 M7314 4 M29-U3-R

2F H2006/06/2

0 2006/06/2

2 2006/06/2

8 2006/06/2

9 M7314 5 M29-U3-R

3 F H2006/06/21 2006/06/2 2 2006/06/2

8 2006/06/2

9 Particulates i nAi r(Aceton eRinse) viaEP A Metho d5 M7314 2M29-RBF H2006/06/21 2006/06/2 2 2006/06/2

7 2006706/2

8 M7314 3 M29-U3-R 1 F H2006/06/19 2006/06/2 2 2006/06/2

7 2006/06/2

8 M7314 4 M29-U3-R

2F H2006/06/2

0 2006/06/2

2 2006/06/2

7 2006/06/2

8 M7314 5 M29-U3-R

3 F H2006/06/21 2006706/2 2 2006/06/2

7 2006/06/2

8 Particulates i nAi r(Filter) vi aEP A Metho d5 M7314 2M29-RBF H2006/06/21 2006/06/2 2 2006/06/2

6 2006/06/2

6 M7314 3 M29-U3-R1F H2006/06/19 2006/06/2 2 2006/06/2

6 2006/06/2

6 M7314 4 M29-U3-R2F H2006/06/2 0 2006/0672

2 2006/06/2

6 2006/06/2

6 M7314 5 M29-U3-R

3 F H2006/06/21 2006/06/2 2 2006/06/2

6 2006/06/2

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Sampl eanalyt eresul t Metho dblan kresul t LC S Result

s wit h% Recoverie

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# IV S 

# axx a

# m l>riven by service

and Science www.maxxamanalytlcs.co m 

### YourProjec

t# : 10002-017-82 0 Site : ONY X
Attention : Jef fGorma n ENS RInternationa

l 660 1 KirkvilleR d Eas tSyracuse

, N Y US A 1305 7 Repor tDate : 2006/09/1 1

CERTIFICAT E O F ANALYSI S 

### MAXXA M JO B # : A66217 5 Received : 2006/06/22,13:5 0 Sampl eMatrix : Filter #Sample

s Received : 4 Dat e Dat e Metho d Analyse s Quantit y Extracte d Analyze d LaboratoryMetho d Referenc e Metal s i n Ai r(Fron tHalf ) b yICP/M S ( 5 4 2006/06/2 8 2006/0672 9 SO P IN G 108/10 9 EP ASW846-602 0 Particulate s i n Ai r(Aceton e Rinse ) (M5 ) fl> 4 2006/06/2 7 2006/06/2 8 SO P IN G 50 5 EP ACF R PT M 5 Particulate s i n Ai r(Filter ) © 4 2006/06/2 6 2006/06/2 6 SO P IN G 50 5 EP ACF R PT M 5 Fina l Volum e o fAceton e Prob e Rins e ( D 4 2006/09/1 1 2006/09/1 1 

### Sampl eMatrix : Impinge

rSolutio n #Sample

s Received : 4 Dat e Dat e Metho d Analyse s Quantit y Extracte d Analyze d LaboratoryMetho d Referenc e Metal s i n Ai r(Bac k

Half ) b yICP/M S J

t 4 2006/06/2 9 2006/06/2 9 SO P IN G 108/10 9 EP ASW846-3010A,6 0 

### (1 ) Thi s tes twa s performe

db yMaxxa mAnalytic

s Burlingto

n

MAXXA MANALYTIC S INC .
MARY-ANN EJOHNSON , B.A ,B.Sc . Projec tManage

r MAJ/ma j encl.

..12 

### Pag e1 o f 1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7

# IV ! 

# arr i Driven by service

and Science "—•~ " ~ ' ~ www.Miaxxaiiiaiialytics-co m { Analytic s In c 

### YourProjec t# : 10002-017-82

0 Site : ONY X
Attention : Jef fGorman ENS RInternationa

l 660 1 KirkvilleR d Eas tSyracuse

, N Y US A 1305

7 Repor tDate : 2006/09/1 1
CERTIFICAT EO F ANALYSI S

-2-

Validate d b y:

Tota lcove rpages : 2
Pag e 2 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Toi l free:800-563-626 6 Fax:905-817-577 7Driven try serine

and

Science 

# f / Analytic s in c www .maxxaman3lvtlcs .co m 

### ENS R Internationa l Maxxa m Jo b # : A66217 5 Clien tProject# : 10002-017-82 0 Repor tDate : 2006/09/1 1 Projectname : ONY X Sample rInitials : RESULT S O FANALYSE S O FFILTE R Maxxa m I D M7314 2 M7314 3 M7314 4 M7314 5 Samplin g Dat e 2006/06/2 1 2006/06/1 9 2006/06/2 0 2006/06/2 1 Jnit s M29-R B F H M29-U3-R 1 F H M29-U3-R 2

F H M29-U3-R 3

F H R D L Q C Batc h M D L

Particulat e Weigh ti n Aceton e Rins e m g N D 4. 0 2. 8 1. 7 0. 5 100127 5 0. 5 Volum e m l 9 8 5 7 8 7 5 6 1 104987 0 1 Particulat e Weigh to n Filte r m g 0.6 5 2.2 0 1.6 5 1.5 5 0.3 0 100126 5 0.3 0 N D = No tdetecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h

Pag e 3 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7

# TsAa m Driven by service

and Science 

### Maxxa m Jo b # : A66217 5 Repor tDate : 2006/09/1 1 www.maxxamanalyUcs.co m 

### ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### ELEMENTS BYICP/M S (FILTER)
Maxxa m I D M7314 2 M7314 3 M7314 3 M7314 4 M7314 5 Samplin g Dat e 2006/06/2 1 2006/06/1 9 2006/06/1 9 2006/06/2 0 2006/06/2 1 Unit s M29-R B F H M29-U3-R 1 F H M29-U3-R 1

F H Lab-Du p M29-U3-R 2 F H M29-U3-R 3

F H R D L Q C Batc h M D L

Tota l Arseni c (As ) u g 0.6 1 5.8 1 6.0 1 4.2 7 5.6 2 0.4 0 100100 8 0.4 0 Tota l Berylliu m (Be ) N D N D N D N D N D 0.1 0 100100 8 0.1 0 Tota l Chromiu m (Cr ) u g 0.7 9 9.6 4 11.9(1 ) 3.9 8 11. 1 0.3 0 100100 8 0.3 0 |N D = No t detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h ( 1 ) Pleas e refe rt o Genera l Comment s pag e fo rspecifi c clarification .

Pag e 4 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7Driven by service

and Science www.maxxamanalytics.co m 

### ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### ELEMENTS BYICP/M S (IMPINGE R SOLUTION )
Maxxa m I D M7314 6 M7314 7 M7314 7 M7314 8 M7314 9 Samplin g Dat e 2006/06/2 1 2006/06/1 9 2006/06/1 9 2006/06/2 0 2006/06/2 1 Unit s M29-R B B H M29-U3-R 1 B H M29-U3-R 1

B H Lab-Du p M29-U3-R 2 B H M29-U3-R 3

B H R D L 3 C Batc h M D L

Tota l Arseni c (As ) u g N D 0.3 3 0.3 3 N D 0.2 1 0.2 0 100175 8 0.2 0 Tota l Berylliu m (Be ) u g N D N D N D 0.08 7 N D 0.05 0 100175 8 0.05 0 Tota l Chromiu m (Cr ) u g N D 1.0 6 1.0 2 0.6 6 0.8 4 0.1 5 100175 8 0.1 5 N D = No t detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit yContro l Batc h ' Analytic s In c 

### Maxxa m Jo b #:A66217 5 Repor tDate : 2006/09/1 1

Pag e 5 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7Driven by servive

and Science www.maxxamasialytlcs.co m ENS R Internationa l Clien tProject* : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### Tes tSummar y

Maxxa m I D Sampl e I D Matri x M7314 2

M29-R B F H Filte r Collecte d Shippe d Receive d 2006/06/2 1

2006/06/2 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron tHalf) b vICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 F M O
Maxxa m I D Sampl e I D Matri x M7314 3

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006/06/1 9

2006/06/2 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron tHalf ) b vICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 F M O
Maxxa m I D Sampl e I D Matri x M7314 3 Du p

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006/06/1 9

2006/06/2 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t IMetal s i n Ai r(Fron tHalf ) b yICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/06/2 9 NL R I
Maxxa m I D Sampl e I D Matri x M7314 4

M29-U3-R 2 F H Filte r Collecte d Shippe d Receive d 2006/06/2 0

2006/06/2 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron tHalf ) b yICP/M S 1CP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 F M O
Maxxa m I D Sampl e I D Matri x M7314 5

M29-U3-R 3 F H Filte r Collecte d Shippe d Receive d 2006/06/2 1

2006/06/2 2 Tes tDescriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron tHalf ) b yICP/M S 1CP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 F M O 

# IS/ I

# a

# x5^ am t i c s I n c f Anol y Maxxa m Jo b # : A66217 5 Repor tDate : 2006/09/1 1

Pag e 6 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7

# M a f Analytk i In c Driven by service

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### Maxxa m Jo b #:A66217 5 Repor tDate : 2006/09/1 1 Tes tSummar y mvw.maixamaiialytics.co m 

### ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials :

Tes tDescriptio n Maxxa m I D M7314 6 Samplel D M29-R B B H Matri xImpinge rSolutio n

Instrumentatio n Batc h Prepare d Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2

Analyze d Analys t IMetal s i n Ai r(Bac k Halt ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N R

Tes tDescriptio n Maxxa m I D M7314 7 Sampl e I D M29-U3-R 1 B H Matri xImpinge rSolutio n

Instrumentatio n Batc h Prepare d Collecte d 2006/06/1 9 Shippe d Receive d 2006/06/2 2

Analyze d Analys t IMetal s i n Ai r(Bac k Half ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 IM_ R

Tes tDescriptio n Maxxa m I D M7314 7 Du p Sampl e I D M29-U3-R 1 B H Matri xImpinge rSolutio n

Instrumentatio n Batc h Prepare d Collecte d 2006/06/1 9 Shippe d Receive d 2006/06/2 2

Analyze d Analys t IMetal s i n Ai r(Bac k Half ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N R

Tes tDescriptio n Maxxa m I D M7314 8 Samplel D M29-U3-R2B H Matri xImpinge rSolutio n

Instrumentatio n Batc h Prepare d Collecte d 2006/06/2 0 Shippe d Receive d 2006/06/2 2

Analyze d Analys t IMetal s i n Ai r(Bac k Half ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N_ R

Tns tDescriptio n Maxxa m I D M7314 9 Samplel D M29-U3-R 3 B H Matri xImpinge rSolutio n

Instrumentatio n Batc h [Metal s i n Ai r(Bac k Half ) b yICP/M S Prepare d Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2

Analyze d Analys t ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N R

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### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Toi l free:800-563-626 6 Fax:905-817-577 7

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### Maxxa m Jo b # : A66217 5 Repor tDate : 2006/09/1 1 Driven by service

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t# : 10002-017-82 0 Projectname : ONY X Sample rInitials :

GENERA L COMMENT S
Result s relat e onl yt o th e item s tested .

Pag e 8 o f1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7

## IV Iay^yi^x r n > a A n n ly : Driven by service

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### hNS H tnternationa l Attention : JeffGorma n Clien tProject# : 10002-017-82 0 P.O
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### QualityAssuranc e Repor t Maxxa m Jo b Numbe rGA66217 5 QA/Q C Batc h Nu m Ini t Q C Typ e Paramete r Dat e Analyze d wyy/mm/d d Valu e %Recover y Unit s Q C Limit s 100100 8 N_ R MATRI XSPIK E

(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49.5 , RDU0.4 0 9 9 u g 7 0 - 13 0 MATRI XSPIK E DUP(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49.5 , RDL=0.4 0 9 9 u g 7 0 - 13 0 MATRI XSPIK E (M73143 ) Tota l Berylliu m (Be ) 2006/06/2 9 48.0 , RDL=0.1 0 9 6 u g 7 0 - 13 0 MATRI XSPIK E D U P (M73143 ) Tota l Berylliu m (Be ) 2006/06/2 9 47.0 , RDL=0.1 0 9 4 u g 7 0 - 13 0 MATRI XSPIK E (M73143 ) Tota l Chromiu m (Cr ) 2006/06/2 9 48.5 , RDL=0.3 0 9 7 u g 7 0 - 13 0 MATRI XSPIK E DUP(M73143 ) Tota l Chromiu m (Cr ) 2006/06/2 9 47.5 , RDL=0.3 0 9 5 u g 7 0 - 13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 48.5 , RDL=0.4 0 9 7 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 49.0 , RDL=0.4 0 9 8 u g 8 5 - 11 5 Spike d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 59.5 , RDL=0.1 0 119(1 ) u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDL=0.1 0 117(1 ) u g 8 5 - 11 5 Spike d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 53.0 , RDL=0.3 0 10 6 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 53.0 , RDL=0.3 0 10 6 u g 8 5 - 11 5 Metho d Blan k Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.4 0 u g Metho d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.4 0 u g Metho d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDL=0.1 0 u g Metho d Blan k

DU P Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDL=0.1 0 u g Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.3 0 u g Metho d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.3 0 u g R P D Tota l Arseni c (As ) 2006/06/2 9 3. 4 % 2 0 Tota l Berylliu m (Be ) 2006/06/2 9 N C % 2 0 Tota l Chromiu m (Cr ) 2006/06/2 9 21.2(1 ) % 2 0 100127 5 IM R Metho d Blan k Particulat e Weigh t i n Aceton e Rins e 2006/06/2 8 ND , RDL=0. 5 m g 100175 8 N_ R MATRI XSPIK E

(M73147 ) Tota l Arseni c (As ) 2006/06/2 9 48.5 , RDL=0.2 0 9 7 u g 7 0 - 13 0 MATRI XSPIK E D U P (M73147 ) Tota l Arseni c (As ) 2006/06/2 9 50.0 , RDU0.2 0 10 0 u g 7 0 - 13 0 MATRI XSPIK E (M73147 ) Tota l Berylliu m (Be ) 2006/06/2 9 57.5 , RDL=0.05 0 11 5 u g 7 0 - 13 0 MATRI XSPIK E DUP(M73147 ) Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDL=0.05 0 11 7 u g 7 0 - 13 0 MATRI XSPIK E (M73147 ) Tota l Chromiu m (Cr ) 2006/06/2 9 50.0 , RDL=0.1 5 10 0 u g 7 0 - 13 0 MATRI XSPIK E D U P (M73147 ) Tota l Chromiu m (Cr ) 2006/06/2 9 51.0 , RDL=0.1 5 10 2 u g 7 0 - 13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 50.5 , RDL=0.2 0 10 1 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 50.0 , RDL=0.2 0 10 0 u g 8 5 - 11 5 Spike d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDL=0.05 0 11 7 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006/06/2 9 58.0 , RDL=0.05 0 11 6 u g 8 5 - 11 5 Spike d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 52.0 , RDL=0.1 5 10 4 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 52.0 , RDL=0.1 5 10 4 u g 8 5 - 11 5 Metho d Blan k Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.2 0 u g Metho d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.2 0 u g Metho d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDL=0.05 0 u g Metho d Blan k

DU P Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDL=0.05 0 u g Metho d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.1 5 u g Metho d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.1 5 u g R P D Tota l Arseni c (As ) 2006/06/2 9 N C % 2 0 Tota l Berylliu m (Be ) 2006/06/2 9 N C % 2 0 Tota l Chromiu m (Cr ) 2006/06/2 9 4. 2 % 2 0 N D = No t detecte d 

### Pag e 9 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7I Analy t 

### hNS H Internationa l Attention : JeffGorma n Clien tProject* : 10002-017-82 0 P.O
. # : Projectname : ONY X Driven by service

and Science www.m

a xx a m anal

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### Qualit yAssuranc e Repor t(Continued )

Maxxa m Jo b Numbe rGA66217 5
N C = Non-calculabl e iRP D = Relativ e Percen tDifferenc e |SPIK E = Fortifie d sampl e 1 ) Pleas e refe rt o Genera l Comment s pag e fo rspecifi c clarification .



### Pag e 1 0 o

f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7^ t /Anolytic a In c Driven by ser\->ice

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### Validatio n Signatur e Pag e Maxxa m Jo b # : A66217 5

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Maxxa m has procedure s i n plac e to guard agains timprope rus e o fth e electroni csignatur e an d hav e th e require d "signatories" , a s pe rsectio n 5.10. 2 o f ISO/IE C 17O25:2O05(E) , signin g th e reports . SC C an d CAEA Lhav e approve d thi s reportin g proces s an d electroni creportformat
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### 674 0 Campobell o Road , Mississauga , Ontari o Canad aL5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7