ND 

Oil & Grease (HEM) 

ND 

Specific conductance 

ND 

Su1fate 

Total Alkalinity 

Total Dissolved 

Solids 

Total. Recoverabl.e 

Phenolics 

Total Suspended 

Solids 

NOTB(S}: 

0.22 B 

2.3 B 

ND 

0.0068 B 

ND 

0.050 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

Work Order #: MAALD1AA 

5.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 10:35 

Work Order #: MAK241AA 

1.0 umhos/cm 

Dilution Factor: 1 

Analysis Time .. : 00:00 

Work Order #: MACXL1AA 

1.. 0 urg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

Work Order #: MANJJ1AA 

5.0 urg/L 

Dilution Factor: 1 

Analysis Time .. : 00:00 

MCAWW 300.0A 11/18/10 

MB Lot-Sample #: COK190000-244 

CFR136A 1664A HEM 11/19/10 

MB Lot-Sample #: COK290000-041 

SM20 2510B 11/29/10 

MB Lot-Sample #: COK200000-043 

MCAKW 300.0A 11/18/l.O 

MB Lot-Sample #: COLOl0000-025 

SM18 2320 B 12/02/10 

0324045 

0323244 

0333041 

0324043 

0335025 

Work Order #: MAAQV1AA MB Lot-Sample #: COK190000-271 

10.0 mg/L 

Dilution Factor: l 

Analysis Time .• : 11:15 

SM20 2540C 11/19-11/20/10 0323271 

work Order #: MAGG01AA MB Lot-Sample #: COK230000-071 

0.010 urg/L 

Dilution Factor: 1 

Analysis Time .. : 10:33 

MCA1IW 420.4 11/23-11/24/10 0327071 

Work Order #: MAAP91AA MB Lot-Sample #: C·JK190000-267 

4.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 06:15 

SM20 2540D 1L/l9-11/20/10 0323267 

Calculations are performed before rounding 10 avoid round-off errors in calculated results. 

B Estimated result. Result is less !han RL. 

COK180501 31 of 57 
PARAMETER 

RECOVERY 

Biochemical Oxygen 

Demand (BOD) 

Bromide 

Chloride 

Nitrate as N 

Nitrite as N 

Oil & Grease 

Sulfate 

BOTB(S): 

105 

105 

104 

104 

104 

104 

108 

108 

104 

103 

(HEM) 

82 

86 

104 

104 

LIMITS RPD LIMITS :..:MET=:.:.HO:;D:._ _____ ANALYSIS DATE 

BATCH # 

WO#:L99RA1AC-LCS/L99RA1AD-LCSD LCS Lot-Sample#: COK190000-082 

(85 - 115) SM20 5210B 

(85 - 115) 0.24 (0-20) SM20 5210B 

11/19-11/24/10 0323082 

11/19-11/24/10 0323082 

Dilution Factor: 1 Analysis Time .. : 09: OS 

WO#:MACXR1AC-LCS/MACXR1AD-LCSD LCS Lot-Sample#: COK200000-044 

(90- 110) MCAWW 300.0A 11/18/:.o 0324044 . 

(90 - 110) 0.09 (0-20) MCAWW 300.0A 11/18/:.0 0324044 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MACXH1AC-LCS/MACXH1AD-LCSD LCS Lot-Sample#: COK200000-040 

(90 - 110) MCAWW 300. OA 11/18/:.o 0324040 

(90 - 110) 0.13 (0-20) MCAWW 300.0A 11/18/:.0 0324040 

Dilution Factor : 1 Analysis Time .. : 14 : 13 

WO#:MACXF1AC-LCS/MACXF1AD-LCSD LCS Lot-Sample#: COK200000-039 

(90- 110) MCAWWJOO.OA 11/18/:.0 0324039 

(90- 110) 0.14 (0-20) MCAWW 300.0A 11/18/:.0 0324039 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MACXX1AC-LCS/MACXX1AD-LCSD LCS Lot-Sample#: COK200000-045 

(90 - 110) MCAWW 300. OA 11/18/:.0 0324045 

(90 - 110) 0. 07 (0-20) MCAWW 300. OA 11/18/:.o 0324045 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MAALD1AC-LCS/MAALD1AD-LCSD LCS Lot-Sample#: COK190000-244 

(78 - 114) CFR136A 1664A HEM 11/19/:.0 0323244 

(78 - 1H) 3.9 (0-18) CFRJ.36A 1664A HEM 11/1!:1/:.0 0323244 

Dilution Factor: 1 Analysis Time .. : 10:35 

WO#:MACXLlAC-LCS/MACXLlAD-LCSD LCS Lot-Sample#: COK200000-043 

(90 - 110) MCAWW 300. OA 11/18/:.o 0324043 

(90- 110) 0.17 (0-20) MCAWW 300.0A 11/18/:. 0 0324043 

Dilut~n Factor: 1 Analysis Time .. : 14:13 

C11CUiatlons lrt performecl before rouncling 10 1110id round-off emil'S in calcullled resuhs. 

COK180501 32 of 57 
pH 

100 

Acidity 

99 

Ammonia Nitrogen 

92 

Chemical Oxygen 

Demand (COD} 

Hardness, 

as CaC03 

103 

100 

Specific Conductance 

111 

Total Alkalinity 

91 

Total Dissolved 

Solids 

109 

Total Recoverable 

Phenolics 

100 

COK180501 

Work Order #: L985AlAA LCS Lot-Sample#: CoJK180000-329 

(99 - 101} SM20 4500-H+B 11/18/10 0322329 

Dilution Factor: l Analysis Time .. : 15:05 

Work Order #: MAKRLlAC LCS Lot-Sample#: CI)K270000-042 

(80 - 120) SM20 2310B (4a) ll./27 /10 0331042 

Dilution Factor: l Analysis Time .. : 13:38 

Work Order #: L999G1AC 

(90 - 110) MCAWW 350.1 

LCS Lot-Sample#: COK190000-198 

11/19-11/23/10 0323198 

Dilution Factor: 1 Analysis Time .. : 13:26 

Work Order#: MAK8T1AC LCS Lot-Sample#: COK290000-068 

(90 - 110) MCAWW 410.4 11/29/:.o 0333068 

Dilution Factor: 1 Analysis Time .. : 13:14 

Work Order #: MAKSOlAC LCS Lot-Sample#: C(IK290000-050 

(90 - 110) SM2D 2340C 11/29/J.D 0333050 

Dilution Factor: 1 Analysis Time .. : 08:45 

Work Order #: MAK241AC 

(80 - 120) SM20 251DB 

LCS Lot-Sample#: CCK290000-041 

11/29/JO 0333041 

Dilution Factor: 1 Analysis Time .. : 00:00 

Work Order #: MANJJ1AC 

(80 - 120) SM18 2320 B 

LCS Lot-Sample#: CCL010000-025 

12/02/lO 0335025 

Dilution Factor: 1 Analysis Time .. : 00:00 

Work Order #: MAAQV1AC LCS Lot-Sample#: COK190000-271 

(80 - 120) SM20 2540C 11/19-11/20/10 0323271 

Dilution Factor: 1 Analysis Time .. : 11:15 

Work Order #: MAGG01AC LCS Lot-Sample#: COK230000-071 

(90 - 110} MCAWW 420.4 11/23-11/24/10 0327071 

Dilution Factor: 1 Analysis Time .. : 10 : 33 

(Continued on next page) 

33 of 57 
Total Suspended Work Order #: MAAP91AC LCS Lot-Sample#: C•)K190000-267 

Solids 

97 (80 - 120) SM20 25400 11/19-11/:20/10 0323267 

Dilution Factor: 1 Analysis Time .. : 06 : 15 

ROTB(S): 

Calculatioos are performed before I'OWlding 10 avoid round-off errors in atk:ulalcd results. 

COK180501 34 of 57 
114 N. (90 - 110} 

112 N (90 - 110) 1.4 (0-20) 

Dilution Factor: 1 

Analysis Time . . : 13:49 

MCAWW 350.1 11/19-11/23/10 0323198 

MCAWW 350.1 11/19-11/23/10 0323198 

MS Run# ....... : 0323115 

Chemical oxygen 

Demand (COD) 

WO#: MAEP3lAH-MS/MAEP3LAJ-MSD MS Lot-Sample #: COK220467-001 

92 

100 

(90 - 110) MCAWW 410.4 

(90 - 110} 6.0 (0-20} MCAWW 410.4 

Dilution Factor: 1 

Analysis Time .. : 13:17 

MS Run# ..... . . : 0333032 

11/29/10 

11129no 

0333068 

0333068 

Total Recoverable 

Phenolics 

WO#: L98HL1AF-MS/L98HL1AG-MSD MS Lot-Sample #: COK180491-002 

ROTB(S): 

102 

102 

(90 - 110) MCAWW 420.4 

(90 - 110} 0.19 (0-20} MCAWW 420.4 

Dilution Factor: 1 

Analysis Time .. : 10:33 

MS Run# .... . . . : 0327181 

Calculalions are performed before rounding to avoid round-ilff errors in calculaled results. 

N Spiked analyte recovery is oullide stated COPITOllimits. 

COK180501 35 

11/23-11/24/10 0327071 

11/23-11/24/10 0327071 

of 57 
Biochemical Oxygen 

SD Lot-Sample #: COK180463-001 

Demand (BOD) 

ND ND mg/L 0 

Dilution Factor: 1 

COK180501 

{0-20) SM20 5210B 

Analysis Time .. : 09:05 

11/19-11/24/10 0323082 

MS Run Number .. : 0323050 

36 

FEB 2 8 2011 

DEP, SOUTHWEST REGION 

OIL.& GAS 

of 57 
Total Suspended 

Solids 

ND ND 

COK180501 

SD Lot-Sample #: COK19042l-001 

mg/L 0.0 (0-20) SM20 25400 11/19-11/20/10 0323267 

Dilution Factor: 1 Analysis Time .• : 06:15 MS Run Number .. : 0323145 

37 of 57 
Total Dissolved 

Solids 

259 215 

COK180501 

E BATCH # 

SD Lot-Sample #: COK170523-001 

mg/L 19 (0-20) SM20 2540C 11/19-11/20/10 0323271 

Dilution Factor: 1 Analysis Time . . : 11:15 MS Run Number . . : 0323149 

38 of 57 
~cidity 

ND ND 

COK180501 

S DATE 

SD Lot-Sample #: COK1805.29-003 

mg/L 0 (0-.20) SM20 2310B (4a) 11/27/10 

Dilution Factor: 1 Analysis Time •. : 13:38 MS Run Number . . : 

39 

BATCH # 

033104.2 

0331019 

of 57 
Acidity 

ND ND 

COK180501 

SD Lot-Sample #: COK220465-001 

mg/L 0 (0-20) SM20 23108 {4a) 11/27/10 

Dilution Factor: 1 Analysis Time .. : 13:38 MS Run Number .. : 

40 

0331042 

0331019 

of 57 
Specific Conductance 

523 528 

COK180501 

SD Lot-Sample #: C•JK160529-001 

umhos/cm 0.95 (0-20) SM20 2510B 11/29/10 

Dilution Factor: 1 Analysis Time .. : oo:oo MS Run Number •. : 

41 

0333041 

0333014 

of 57 
Hardness, 

as CaC03 

200 200 

COK180501 

SD Lot-Sample #: COK04043l-004 

mg/L 0.0 (0-20) SM20 2340C :Ll/29/10 0333050 

Dilution Factor: 10 Analysis Time .. : 08:45 )IS Run Number .. : 0333025 

42 of 57 
Hardness, 

as CaC03 

36000 35000 

pH 

6.6 6.6 

COK180501 

S DATE BATCH # 

SD Lot-Sample #: ::OK180438-001 

mg/L 2.8 (0-20) SM20 2340C 11/29/10 0333050 

Dilution Factor: 500 Analysis Time .• : 08:45 MS RWl Number .. : 0333025 

SD Lot-Sample #: <::OK180438 -001 

0.0 (0-2.0) SM20 4500-H+B 11/18/10 0322329 

Dilution Factor: 1 Analysis Time .. : 15:07 MS RWl Num:ber .• : 0322185 

43 of 57 
Total Alkalinity SD Lot-Sample #: CJK180490-00l 

103 J 103 mg/L 0.068 (0-20) SM18 2320 B 12/02/10 0335025 

Dilution Factor: 1 Analysis Time .• : 00:00 MS Run Nulllber . . : 0336085 

NOTB'(S): 

Calculations are performed before roundiniiO avoid round-off arors in calculaud results. 

J Medtocl blauk conwnination. The aSIIOCillred method blaDit contains lhe larget analyte at a reponable level. 

COK180501 44 of 57 
Project Description(s) 

Equitable Production Company 

Equitable Production Company 

For: 

Chris Kovitch 

TestAmerica Pittsburgh 

301 Alpha Drive; RIDC Park 

Pittsburgh, PA 15238 

Melissa Deyo For Sally Hoffman 

Project Manager 

melissa.deyo@testamericainc.com 

Tuesday, November 30,2010 

The test results in this report meet all NELAP requirements for analytes for which accreditation is required or 

available. Any exception to NELAP requirements are noted in this report. Persuant to NELAP, this report may not 

be reproduced, except in full, without the written approval of the laboratory. All questions regarding this test report 

should be directed to the TestAmerica Project manager who has signed this report. 

COK180501 45 

of 57 
As of 08/16/2010 

STATE Program Cert #I Lab /D 

Arkansas CWA, RCRA, SOIL 88-0686 

California* NELAP CWA, RCRA 01169CA 

Connecticut SDWA, CWA, RCRA, SOIL PH-0568 

Florida* NELAP CWA, RCRA E87672 

Georgia* SDWA,NELAP CWA, RCRA 956 

Illinois* NELAP SDWA, CWA, RCRA 200003 Iowa SWIGS 374 

Kansas* NELAP SDWA, CWA, RCRA E-10187 Kentucky SDWA 90029 Kentucky UST UST 30 

Louisiana* NELAP CWA, RCRA 2031 

Maine SDWA, CWA NY0044 

Maryland SDWA 294 Massachusetts SDWA, CWA M-NY044 Michigan SDWA 9937 

Minnesota SDWA, CWA, RCRA 036-999-337 

New Hampshire* NELAP SDWA, CWA 233701 New Jersey* NELAP,SDWA, CWA, RCRA, NY455 

New York* NELAP, AIR, SDWA, CWA, RCRA · 10026 North Dakota CWA, RCRA R-176 

Oklahoma CWA, RCRA 9421 Oregon* CWA,RCRA NY200003 

Pennsylvania* NELAP CWA,RCRA 68-00281 

Tennessee SDWA 02970 Texas* NELAP CWA, RCRA T1 04704412 -08-TX 

USDA FOREIGN SOIL PERMIT 

Virginia SDWA 

Washington* NELAP CWA,RCRA Wisconsin CWA, RCRA West Virginia CWA,RCRA 

*As required under the indicated accreditation, the test results i1 this report meet all NELAP 

requrements for parame ters for which accreditation is required or avaiable. Any exceptions to 

NELAP requirements are noted in this report. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

S-41579 

278 

C1677 

998310390 

252 

COK180501 46 Page 2 of 1.1 of 57 
field-pH), they were not analyzed immediately, but as soon as possible after laboratory receipt. 

I certify that this data package is in compliance with the terms and conditions of the contract, both technically 

and for completeness, for other than the conditions detailed within the body of this report. Release of the data 

contained in this sample data package and in the electronic data deliverables has been authorized by the 

Laboratory Manager or his/her designee, as verified by the following signature. 

Melissa Deyo For Sally Hoffman 

Project Manager 

Tuesday, November 30,2010 

There are pertinent documents appended to this report, 2 pages, are included and are an integral part of this report. 

Reproduction of this analytical report is permitted only in Its entirety. This report shall not be reproduced except in 

full without the written approval of the laboratory. 

TestAmerica Laboratories, Inc. certifies that the analytical results contained herein apply only to the samples tested 

as received by our Laboratory. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 47 Page 3 of t.1 of 57 
p

y

p

g 

Z3 The sample required a dilution, the surrogate spike concentration in the sample are reduced to a level where the 

recovery calculation does not provide useful information. 

NR Any inclusion of NR indicates that the project specific requirements do not require reporting estimated values below 

the laboratory reporting limit. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 48 Page 4 of 1..1 of 57 
General Chemlstrv Parameters 

Total Kjeldahl Nitrogen 34.3 008 2.00 1.50 mg/L 10.0 11/24/10 14:08 JME 10K2404 351.2 

TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 49 Page 5 of 1..1 of 57 
HURD DRILL PIT-590398 HURD DRILL PIT -590398 

RTK1396-01 

RTK1536-01 

Water Water 

11/17/10 11:30 

11/17/10 11:30 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 50 

11119/10 09:00 11/23/10 09:15 

Page 6 of 1..1 of 57 
General Chemistrv Parameters 

Methylene Blue Active NO H3 0.0250 0.0130 mg/L 1.00 11/19/1016:30 JFR 10K2067 5540C 

Substances 

Total Kjeldahl Nitrogen 34.3 008 2.00 1.50 mg/L 10.0 11/24/10 14:08 JME 10K2404 351.2 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 51 Page 7 of 1...1 ot 57 
Non-Halogenated Volatile Organics 

Ethylene Glycol NO 010 1000 NR mg!L 100 11/24/10 20:15 GFD 10K2446 8015 

1,4-Butanedio/ 303% D10,Z3 Surr Limits: (66-130016) 11124/10 20:15 GFD 10K2446 8015 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 52 Page 8 of L1 of 57 
y 

351.2 10K2404 RTK1396-01 25.00 mL 25.00 mL 11/23/10 10:20 

5540C 10K2067 RTK1396-01 400.00 mL 400.00 mL 11/19/10 16:30 

SAMPLE EXTRACTION DATA 

WWol Extract 

Parameter Batch Lab Number Extracte Units Volume Units Date Prepared 

Non-Halogenated Volatile Organics 

8015 10K2446 RTK1536-01 0.50 mL 1.00 mL 11/24/10 06:26 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 53 

JME 

JFR 

Lab 

Tech 

GFD 

TKN Digestion 

MBAS 

Extraction Method 

8015 Glycols 

Page 9 of 1.1 ot 57 
Blank Analyzed: 11/24/10 (Lab Number:10K2446-BLK1, Batch: 101<2446) 

Ethylene Glycol 10 NR mgfl NO 

Surrogate: 1,4-Butanedio/ mg!L 

LCS Analyzed: 11/24/10 (Lab Number:10K2446-BS1, Batch: 101<2446) 

Ethylene Glycol 20.0 10 NR mg/L 19.8 

Surrogate: 1, 4-Butanediol mg!L 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 54 

109 

99 

109 

66-130 

50-150 

66-130 

Page 1 0 off11 0 57 
Blank Analyzed: 11/19/10 (Lab Number:10K2067-BLK1, Batch: 101<2067) 

Methylene Blue Active 

Substances 

0.0250 0.0130 

LCS Analyzed: 11/19/10 (Lab Number:10K2067-BS1, Batch: 101<2067) 

Methylene Blue Active 

Substances 

0.400 0.0250 0.0130 

mg/L 

mg/L 

Matrix Spike Analyzed: 11/19/10 (Lab Number:10K2067-MS1, Batch: 101<2067) 

QC Source Sample: RTK1391H11 

Methylene Blue Active 

Substances 

ND 

General Chemistry Parameters 

0.100 0.0250 0.0130 

Blank Analyzed: 11/24/10 (Lab Number:10K2404-BLK1, Batch: 101<2404) 

Total Kjeldahl Nitrogen 0.20 0.15 

LCS Analyzed: 11/24/10 (Lab Number:10K2404-BS1, Batch: 101<2404) 

Total Kjeldahl Nitrogen 2.50 0.20 0.15 

mg/L 

mg/L 

mg/L 

NO 

0.380 95 

0.105 105 

ND 

2.46 98 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180501 55 

90-110 

79-117 

90-110 

Page 11 off11 0 57 
WORK

LOCA TION: WS 

ADDRESS: .2.960 Faster CreighiDil Oriwe 

·I Nastwi~ TN 37:.!04 

CLIENT ID: HURD DRILL PIT·59D3gll DATE/TIME SAMPLED; 20101117 1130 MATRIX: I WATER 

j - SAMP:._:; COMMENT ~:i;iTHQD: Zll IliON: NONE WATER. 351.2 TJ!;N TA. Na•hvllht 

EXTRACTION; 8.!1 NO SAMP!.!: PREPARATION PSRFORMED I QC IV;;>E; 01 STANDARD TEST SET 

WOFU<OBQER LQSK11.t,O ~ KX 

!!!!;;1HOO: zo NONE NONE WATER, 415.1 MBAS T,t.. ~shville EXIRJ\C:D!Z:!: 8S NO SA.Mr~LE PREPARAiiO~ PEFiFORM~D I OC T"YFS· 01 STA.N!)AR:J TEST SET 

WORKORDER L981<\ 1A1 ~ XX 

rhe sample(s} lis led on this form tue being senllo your location for the specified anelysis. If you have any (!Uesuons, please 

contact Lhe Projsc:~ Mar1agerlisled Olb~;Jve. PLEASE RETURN T:~E ORIGINA!. SIGNED FORM WITH THE REPOrtT AT THE 

COMPLETION OF ANALYSIS. 

Thank You 

TestAmerir:a Pittsburgh ~ampfe Receilo'ing 

pr\ntect on: Thnl"!i~l6 N•Jvcmber 1 e. 2D1 o 01 :2e PM Pa9P. 1 of 57 
WORK LOCA710N; IJ 

ADORESS: 10 Haelwoad Dr;W! 

• Amhe'st NY 1-4228 SM~ ' 1 

I 

CI..I&.NT 10: liURD DRI;.L. PrT·90lt8 

S.o.MPLE COr.AMENT 

t.i!A'rRI)( I 

EXTBACIIPN: Be lifO SN.WLE PREPARATION PERF=~MED I CC TYP~; 01 STANOARO TEST SET 

WATI;;R 

J 

ME!HOO: %D NO,.E HONE. WA.TER,I01S l!.th.-fene Gt-,~t TA Bllffab WORKOR~B t98K11A2 ~ XX 

The !H.'ft'lp\e(s) listed on Ulis form are be"ng sent to your locallon fCJt the spec! (jed analysis. If~ haw any queslioJ &, plea sa Contact the Project Manager listed above. PlEASE RETURN n-tE ORIGINAL SIGNED FORM WrTH THE REPOR'" AT THE 

COMPlETION OF ANALYSIS. 

1: 

Tnank Vou 

• 

TestAmerica Pittsburgh 

Sample Receiving 

• 

RELINQUISHED BV: ---+--~"5oo"'::.o-~~;;..,;t....._ _____ DATE:_......_._f-~--

le:sW!Ierit'.o!l Pittsbu~h COK180501 

:>'¥-____..,;;;....;lO;;=-rf------- DATE: TIME: b~l,tl d'iljprinled on: ThuP.Id:av, Ho..-nber 18, 4'010 01:28PM 

57 Pa~e 1 of 57 

ANALYTICAL REPORT 

Fonn 26R 

Lot #: COK180490 

Maryamla Babich 

Equitable Production Co. 

225 North Shore D.ri ve 

Pittsburgh, PA 15212-5861 

TESTAMERICA LABORAT·:lRIES, INC. 

Christi:c;: M., KO\"'itch 

Proj ~ ;': Ma~ December 6, 2010 

301 Alpha Drive Pittsburgh, PA 15238 tel412.963.7058 fax412.963.2468 www.testamericalnc.com 

COK180490 1 of 57 
y 

p

C standards and held accreditation for all analyses performed unless noted by a qualifier. The labs accreditation numbers are listed below. The format and contents of the report meets all applicable NELAC standards except as noted in the narrative and shall not be reproduced except in full, without the written approval of the laboratory. The table below presents a summary of the certifications held by TestAmerica Pittsburgh. Our primary accreditation authority for the Non-potable water and Solid & Hazardous waste programs is Pennsylvania DEP. A more detailed parameter list is available upon request. Please ask your project manager for this information when required. 

TestAmerlca 

X 

f-·----Califomia- NELAC 

Connecticut 

- -

ww X 

HW X 

ww X 

HW X 

ww X 

HW X 

ww X 

~-------~N~ort~h-C~a-ro~l

i-n-a·---------+

----

~(#4~34~~)·------,------~~~-----~-·-----~~----

--­

r--

----~P-e-nn-s-~~va--n~ia---N~E=L~A~C------

+----

-(~#0~2~~-04~~1~6~)---~-------~~-----

-~

-------~-------

HW X 

ww X 

1------south caio-=l,....in_a _____ . __ +---(:-:-:#8""'oo=-:1-:4o~o:::-::2"') _____ ----~:.,-------it------·---':-:------

HW X 

ww X 

--------~~-~~~~-- Utah- NELAC ---- --- ----<S-T~L~P)~-----~-----~~~---- -------~-- ---

HW 

ww 

HW 

ww 

--

r--------West_Vi_rg-in-ia --------·---=-(#::-1'"4"c=:-2:-) ----+---·- ---, 

-------

---~w~,~--n-si~n----------

;----~99~80~2~7~8~00~

---+------~~~~------

HW 

The codes utilized for program types are described below: 

HW Hazardous Waste certification 

VlfN Non-potable Water and/or Wastewater certification 

X 

X 

X 

X -----~- -----

X 

X Laboratory has some form of certification under the specific program. Many states certify laboratories for specific parameters or tests within a category. The Information In the table Indicates the lab is certified In a general category of testing. Please contact the laboratory if parameter speclflc certification information is required. 

Updated: 0.5/19/10 N:\Reporting\NELAC NARRATIVE Pttsburgh_Updated 051910.doc 

COK180490 2 of 57 
There were no problems associated with the analysis. 

Metals: 

The total and dissolved sample was analyzed at a dilution for the ICP analytes, due to over range analytes and matrix interference. 

The total method blank had aluminum detected at a concentration between the MDL and the reporting limit. The result was flagged with a "B" qualifier. Any sample associated with a method blank that had the same analyte detected had the result flagged with a "J" qualifier. 

General Chemistry: 

The test for pH is a field parameter. The laboratory pH analysis was completed at the request of the client. 

The sample was analyzed at a dilution for various parameters. Results flagged with a "G" qualifier indicate dilution due to matrix interference. 

The method blanks had analytes detected at concentrations between the MDL and the reporting limit. The results were flagged with a "B" qualifier. Any sample associated with a method blank that had the same analyte detected had the result flagged with a "J" qualifier. 

8015: 

TestArnerica's Buffalo laboratory performed the 8015 analysis. Their report is included. 

TKNIMBAS: 

TestArnerica's Nashville laboratory performed the MBAS and TKN analyses. Their report is included. 

COK180490 3 of 57 
n 

0 

~ 

1-' 

CD 

0 

~ 

\0 

0 

~ 

0 

1-h 

(Jl 

-.J 

-... .-......~ -.,:.~ ......,.. 

,...,...._.~ .... ...._..Oi f...._..t__...tnc.. 

Chain of Custody Record 

TettA...tca Laboratorylo<atln: __________________________________ _ 

Rep ... ry p........... c::J D'lll CJ NPDES c:::J RCRA CJ Ol1ler ----------

Test America TH£ l-IN E~loi&MTAL TUTINO 

MoDIIoa 

SaiQio Speclllc N-I 

s,odlll ........ 

TAL 0018- t (04110) 
pH (Electrometric) 

Acidity (Titrimetric) 2310B (4a) 

Alkalinity, Total 

Biochemical Oxygen Demand 5210B 

Bromide 

Chemical Oxygen Demand 

Chloride 

Conductivity 2510B 

HARDNESS, TOTAL 

Mercury in Liquid Waste (Manual Cold-Vapor) 

N-Hexane Extractable Material (1664A) 

Nitrate as N Nitrite as N 

Nitrogen, Ammonia 

Sulfate 

Total Dissolved Solids SM 2540C (SM 20) Total Phenolics 420.4 Total Suspended Solids SM 2540 D 

Trace Inductively Coupled Plasma (ICP) Metals Trace Inductively Coupled Plasma (ICP) Metals 

Volatile Organics by GC/MS 

References: 

SM20 4500-H+B SM20 2310B (4a) SM18 2320 B SM20 52 lOB 

MCAWW 300.0A MCAWW 410.4 MCAWW 300. OA 

SM20 2510B SM20 2340C SW846 7470A 

CFR136A 1664A H 

MCAWW 300.0A MCAWW 300.0A MCAWW 350.1 MCAWW 300.0A 

SM20 2540C 

MCAWW 420.4 

SM20 2540D SW846 6010B 

SW846 6010B SW846 8260B 

CFR136A "Methods for Organic Chemical Analysis of Municipal and 

Industrial Wastewater", 40CFR, Part 136, Appendix A, 

October 26, 1984 and subsequent revisions. 

MCAWW "Methods for Chemical Analysis of Water and Wastes", 

EPA-600/4-79-020, March 1983 and subsequent revisions. 

SM18 "Standard Methods for the Examination of Water and 

Wastewater", 18th Edition, 1992. 

SM20 "STANDARD METHODS FOR THE EXAMINATION OF WATER AND 

WASTEWATER", 20TH EDITION." 

SM20 4500-H B 

SM18 2320 B 

SM20 52 lOB 

MCAWW 300.0A MCAWW 410.4 MCAWW 300. OA 

SM20 2510B 

SM20 2340C SW846 7470A 

EPA 1664A 

MCAWW 300.0A 

MCAWW 300. OA MCAWW 350.1 MCAWW 300.0A 

SM20 2540C 

SM20 2540D SW846 3005A SW846 3010A SW846 5030B 

SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical 

Methods", Third Edition, November 1986 and its updates. 

COK180490 5 of 57 
L98MC 

NOTE (S): 

002 

9

98 

TRIP BLANK 

- The analytical results of the samples listed above are presented on the following pages. 

- All calculations are performed before rounding to avoid round-off errors In calculated results. 

- Results noted as "ND" were not detected at or above the stated limit. 

- This report must not be reproduced, except In full, without the written approval of the laboratory. 

-Results for the following parameters are never reported on a dry weight basis: color, corroslvity, density, flashpolnt. lgnltability, layers, odor. 

paint filter test, pH, porosity pn!S$Ure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight. 

COK180490 6 

/

7/

0 11:30 

11/17/10 

of 57 
Prep Date ...... : 11/30/10 

Prep Batch t ... : 0334067 

Dilution Factor: 1 

PARAMETER 

Benzene 

Toluene 

SURROGATE 

1,2-Dichloroethane-d4 

Toluene-d8 

4-Bromofluorobenzene 

Dibromofluoromethane 

COK180490 

Analysis Date .. : 11/30/10 

Analysis Time .. : 10:58 

Method ......... : SW846 8260B 

REPORTING 

RESULT LIMIT 

ND 5.0 

ND 5 . 0 

PERCENT RECOVERY 

RECOVERY LIMITS 

93 (62 - 123) 

108 (80 - 120) 

95 (75 - 120) 

101 (80 - 120) 

7 

UNITS MDL 

ug/L 0.99 

ug/L 0.85 

of 57 
Prep Date ...... : 11/30/10 Analysis Date .. : 11/30/10 Prep Batch f ... : 0334067 Analysis Time .. : 07:28 

Dilution Factor: 1 

Method ......... : SW846 8260B 

REPORTING 

PARAMETER RESULT LIMIT UNITS MDL 

Benzene ND 5.0 ug/L 0.99 

Toluene ND 5.0 ug/L 0.85 

PERCENT RECOVERY 

SURROGATE RECOVERY LIMITS 

1,2-Dichloroethane-d4 96 (62 - 123) 

Toluene-d8 113 (80 - 120) 

4-Brornofluorobenzene 99 (75 - 120) 

Dibrornofluorornethane 106 (80 - 120) 

COK180490 8 of 57 
Analysis Date .. : 11/30/10 

Dilution Factor: 1 

PARAMETER 

Benzene 

Toluene 

SURROGATE 

1,2-Dichloroethane-d4 

Toluene-d8 

4-Bromofluorobenzene 

Dibromofluoromethane 

NOTE(S): 

Prep Date .•• • •• : 11/30/10 

Prep Batch# ••• : 0334067 

REPORTING 

RESULT LIMIT 

ND 5.0 

ND 5.0 

PERCENT RECOVERY 

RECOVERY LIMITS 

94 (62 - 123) 

108 (80 - 120) 

93 (75 - 120) 

102 (80 - 120) 

Calculations are performed before rounding to avoid round-off errors In calculated results. 

COK180490 9 

Analysis Time •• : 06:20 

UNITS METHOD 

ug/L SW846 8260B 

ug/L SW846 8260B 

of 57 
Analysis Date •• : 11/30/10 Analysis Time .. : 07:51 

Prep Date •••••• : 11/30/10 Prep Batch f ••• : 0334067 

Dilution Factor: 1 

PARAMETER 

1,1-Dichloroethene 

Trichloroethene 

Chlorobenzene 

Benzene 

Toluene 

SURROGATE 

1,2-Dichloroethane-d4 

Toluene-dB 

4-Bromofluorobenzene 

Dibromofluoromethane 

NOTE(S): 

PERCENT 

RECOVERY 

92 98 

101 103 

110 

115 

97 

101 

107 

110 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

Bold print denotes control parameters 

COK180490 

RECOVERY RPD 

LIMITS RPD LIMITS METHOD 

(69 - 127) SW846 8260B 

(69 - 127) 6.6 (0-20) SW846 8260B (80 - 120) SW846 8260B 

(80 - 120) 2.6 (0-20) SW846 8260B 

(83 - 120) SW846 8260B 

(83 - 120) 3.8 (0-20) SW846 8260B 

(80 - 120) SW846 8260B (80 - 120) 3.9 (0-20) SW846 8260B (80 - 124) SW846 8260B 

(80 - 124) 2.8 (0-20) SW846 8260B 

PERCENT RECOVERY 

RECOVERY LIMITS 

88 (62 - 123) 

87 (62 - 123) 

104 (80 - 120) 

102 (80 - 120) 

92 (75 - 120) 91 (75 - 120) 97 (80 - 120) 97 (80 - 120) 

10 of 57 
PARAMETER ;:...:RE=S-=-U;:...:L::.cT=------ -=.U::..:.N=IT::..:S:..__ __ :.:M.:::E..::.T=H-=-O=D _____ ANALYSIS DATE ORDER 4t 

Prep Batch t ... : 0327129 

Silver ND 

Aluminum 297 B,J 

Arsenic ND 

Barium 9920 

Beryllium ND 

Boron 1510 B 

Calcium 373000 

Cadmium ND 

Cobalt ND 

COK180490 

50.0 ug/L 

Dilution Factor: 10 

MDL ....•...•.•• : 6.8 

2000 ug/L 

Dilution Factor: 10 

MDL ..........•. : 96.8 

100 ug/L 

Dilution Factor: 10 

MDL •........... : 27.4 

2000 ug/L 

Dilution Factor: 10 

MDL ....•.•..... : 6.2 

40.0 ug/L 

Dilution Factor: 10 

MDL .....•...... : 2.3 

2000 ug/L 

Dilution Factor: 10 

MDL ..•......... : 13.1 

50000 ug/L 

Dilution Factor: 10 

MDL ......••.... : 96.8 

50.0 ug/L 

Dilution Factor: 10 

MDL ............ : 1.3 

500 ug/L 

Dilution Factor: 10 

MDL ........•... : 4.0 

SW846 6010B 

Analysis Time •• : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time •. : 

SW846 6010B 

Analysis Time .. : 

SW846 6010B 

Analysis Time .. : 

(Continued on next page) 

11 

11/23-11/29/10 L98HC1CL 

14:16 MS Run 11 ....•.. : 0327079 

11/23-11/29/10 L98HC1A3 

14:16 MS Run II •.....• : 0327079 

11/23-11/29/10 L98HC1A4 

14:16 MS Run II ..•.... : 0327079 

11/23-11/29/10 L98HC1A5 

14:16 MS Run II .••.... : 0327079 

11/23-11/29/10 L98HC1A6 

14:16 MS Run II ....... : 0327079 

11/23-11/29/10 L98HC1A7 

14:16 MS Run II ..•...• : 0327079 

11/23-11/29/10 L98HC1A9 

14:16 MS Run II ....•.. : 0327079 

11/23-11/29/10 L98HC1A8 

14:16 MS Run II ....... : 0327079 

11/23-11/29/10 L98HC1CA 

14:16 MS Run 11 ....•.. : 0327079 

of 57 
REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Chromium NO 50.0 ug/L SW846 6010B 11/23-11/29/10 L98HC1CQ 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run t ....... : 0327079 

MDL ............ : 5.7 

Copper NO 250 ug/L SW846 6010B 11/23-11/29/10 L98HC1CC 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL .•.•........ : 27.1 

Iron 6800 1000 ug/L SW846 6010B 11/23-11/29/10 L98HC1CD 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ............ : 119 

Lithium 3200 500 ug/L SW846 6010B 11/23-12/02/10 L98HC1CE 

Dilution Factor: 10 Analysis Time .. : 00:45 MS Run# ....... : 0327079 

MDL ..••.•...... : 27.8 . 

Magnesium 44300 B 50000 ug/L SW846 6010B 11/23-11/29/10 L98HC1CF 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ............ : 207 

Manganese 646 150 ug/L SW846 6010B 11/23-11/29/10 L98HC1CG 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ..•......... : 6.8 

Molybdenum NO 400 ug/L SW846 6010B 11/23-11/29/10 L98HC1CH 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # .•..... : 0327079 

MDL .••....•.... : 13.8 

Sodium 1570000 50000 ug/L SW846 6010B 11/23-11/29/10 L98HC1CM 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ............ : 2150 

Nickel NO 400 ug/L SW846 6010B 11/23-11/29/10 L98HC1CJ 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ..••........ : 15.6 

Lead NO 30.0 ug(L SW846 6010B 11/23-11/29/10 L98HC1CR 

Dilution Factor: 10 Analysis Time .. : 14:16 MS Run # ....... : 0327079 

MDL ............ : 12.6 

(Continued on next page) 

COK180490 12 of 57 
PARAMETER RESULT 

Selenium ND 

Strontium 117000 

Zinc 66.2 B 

Prep Batch f ... : 0330011 

Mercury ND 

NOTE(S): 

B Estimated result. Result is less than RL. 

REPORTING 

LIMIT 

50.0 

UNITS 

ug/L 

Dilution Factor: 10 

MDL .....•...... : 30.4 

1000 ug/L 

Dilution Factor: 20 

MDL ...•........ : 1. 9 

200 ug/L 

Dilution Factor: 10 

MDL ........•... : 24.6 

0.20 ug/L 

Dilution Factor: 1 

MDL ............ : 0.038 

METHOD 

SW846 6010B 

Analysis Time •• : 14:16 

SW846 6010B 

Analysis Time .. : 11:10 

SW846 6010B 

Analysis Time .• : 14:16 

SW846 7470A 

Analysis Time .. : 13:48 

J Method blank contamination. The associated method blank contains the target analyte at a reportable level. 

COK180490 13 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

11/23-11/29/10 L98HC1CK 

MS Run il ....... : 0327079 

11/23-11/30/10 L98HC1CN 

MS Run# ...•... : 0327079 

11/23-11/29/10 L98HC1CP 

MS Run 41 •...•.. : 0327079 

11/26/10 L98HC1AW 

MS Run# ....... : 0330003 

of 57 
REPORTING 

PREPARATION- WORK 

_PARAME ______ T_E_R _______ R_E_S_U_L_T ________ L_I_M_I_T ____ _____ ___________ ANALYSIS DATE ORDER # 

Prep Batch t ... : 0327127 

Iron 3280 1000 ug/L SW846 6010B 11/23-11/29/10 L98HC1AX 

Dilution Factor: 10 Analysis Time .. : 15:38 MS Run f ....... : 0327078 

MDL •••••••••••• : 119 

COK180490 14 of 57 
MB Lot-Sample f: COK230000-129 Prep Batch f ... : 0327129 

Aluminum 30.1 B 200 ug/L SW846 6010B 11/23-11/29/10 MAFPD1AD 

Arsenic ND 

Barium ND 

Beryllium ND 

Boron ND 

Cadmium ND 

Calcium ND 

Chromium ND 

Cobalt ND 

Copper ND 

Iron ND 

COK180490 

Dilution Factor: 1 

Analysis Time .. : 13:54 

10.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

200 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

4.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

200 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5000 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

50.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

25.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

100 ug/L . 

Dilution Factor: 1 

Analysis Time .. : 13:54 

SW846 6010B 

SW846 6010B 

SW846 6010B 

SW846 6010B SW846 6010B 

SW846 6010B SW846 6010B SW846 6010B SW846 6010B 

SW846 6010B 

11/23-11/29/10 MAFPD1AE 11/23-11/29/10 MAFPD1AF 

11/23-11/29/10 MAFPD1AG 11/23-11/29/10 MAFPD1AH 11/23-11/29/10 MAFPD1AJ 

11/23-11/29/10 MAFPD1AK 

11/23-11/29/10 MAFPD1AA 11/23-11/29/10 MAFPD1AL 

11/23-11/29/10 MAFPD1AM 

11/23-11/29/10 MAFPD1AN 

.... 

(Continued on next p age) FEB 2 8 2011 

15 

DEP, SOUTHWEST REGION 

OIL&GkS 

of 57 
Lead ND 

Lithium ND 

Magnesium ND 

Manganese ND 

Molybdenum ND 

Nickel ND 

Selenium ND 

Silver ND 

Sodium ND 

Strontium ND 

Zinc ND 

COK180490 

3.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

50.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 23:57 

5000 ug/L 

Dilution Factor: 1 

Analysis Time •• : 13:54 

15.0 ug/L 

Dilution Factor: 1 

Analysis Time .• : 13:54 

40.0 ug/L 

Dilution Factor: 1 

Analysis Time .• : 13:54 

40.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

5000 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

50.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

20.0 ug/L 

Dilution Factor: 1 

Analysis Time .. : 13:54 

SW846 6010B 11/23-11/29/10 MAFPD1A2 

SW846 6010B 11/23-12/01/10 MAFPD1AP 

SW846 6010B 11/23-11/29/10 MAFPD1AQ 

SW846 6010B 11/23-11/29/10 MAFPD1AR 

SW846 6010B 11/23-11/29/10 MAFPD1AT 

SW846 6010B 11/23-11/29/10 MAFPD1AU 

SW846 6010B 11/23-11/29/10 MAFPDlAV 

SW846 6010B 11/23-11/29/10 MAFPD1AW 

SW846 6010B 11/23-11/29/10 MAFPD1AX 

SW846 6010B 11/23-11/29/10 MAFPD1AO 

SW846 6010B 11/23-11/29/10 MAFPD1A1 

(Continued on next page) 

16 of 57 
MB Lot-Sample f: COK260000-011 Prep Batch t ... : 0330011 

Mercury ND 0.20 ug/L SW846 7470A 

Dilution Factor: 1 

Analysis Time .. : 13:28 

NOTE(S): 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

8 Estimated result. Result Is less than RL. 

COK180490 17 

11/26/10 MAKNK1AA 

of 57 
MB Lot-Sample f: COK230000-127 Prep Batch f ... : 0327127 

Iron ND 100 ug/L SW846 6010B 11/23-11/29/10 MAFN81AD 

Dilution Factor: 1 

Analysis Time .. : 15:16 

NOTE(S): 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

COK180490 18 of 57 
PERCENT RECOVERY PREPARATIONPARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER # 

LCS Lot-Samplef: COK230000-129 Prep Batch t ... : 0327129 

Chromium 104 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlAC 

Dilution Factor: 1 Analysis Time .• : 13:59 

Aluminum 106 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A3 

Dilution Factor: 1 Analysis Time .. : 13:59 

Arsenic 104 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A4 

Dilution Factor: 1 Analysis Time .. : 13:59 

Barium 106 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A5 

Dilution Factor: 1 Analysis Time •. : 13:59 

Beryllium 105 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A6 

Dilution Factor: 1 Analysis Time .. : 13:59 

Boron 104 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A7 

Dilution Factor: 1 Analysis Time .. : 13:59 

Cadmium 101 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A8 

Dilution Factor: 1 Analysis Time .. : 13:59 

Calcium 104 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1A9 

Dilution Factor: 1 Analysis Time .. : 13:59 

Cobalt 102 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlCA 

Dilution Factor: 1 Analysis Time .. : 13:59 

Copper 106 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlCC 

Dilution Factor: 1 Analysis Time .. : 13:59 

Iron 95 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlCD 

Dilution Factor: 1 Analysis Time .• : 13:59 

Lithium 104 (80 - 120) SW846 6010B 11/23-12/02/10 MAFPDlCE 

Dilution Factor: 1 Analysis Time .. : 00:02 

Magnesium 103 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlCF 

Dilution Factor: 1 Analysis Time .. : 13:59 

Manganese 102 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPDlCG 

Dilution Factor: 1 Analysis Time .. : 13:59 

(Continued on next page) 

COK180490 19 of 57 
PERCENT RECOVERY PREPARATIONPARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER # 

Molybdenum 104 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CH 

Dilution Factor: 1 Analysis Time .. : 13:59 

Nickel 102 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CJ 

Dilution Factor: 1 Analysis Time .. : 13:59 

Selenium 103 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CK 

Dilution Factor: 1 Analysis Time .• : 13:59 

Silver 106 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CL 

Dilution Factor: 1 Analysis Time .. : 13:59 

Sodium 107 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CM 

Dilution Factor: 1 Analysis Time .. : 13:59 

Strontium 106 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CN 

Dilution Factor: 1 Analysis Time .. : 13:59 

Zinc 105 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CP 

Dilution Factor: 1 Analysis Time •. : 13:59 

Lead 102 (80 - 120) SW846 6010B 11/23-11/29/10 MAFPD1CQ 

Dilution Factor: 1 Analysis Time •. : 13:59 

LCS Lot-Samplet: COK260000-011 Prep Batch t •.. : 0330011 

Mercury 100 (80 - 120) SW846 7470A 11/26/10 MAKNK1AC 

Dilution Factor: 1 Analysis Time .. : 13:29 

NOTE (S): 

Calculations ere performed before rounding to avoid round-off errors In calculated results. 

COK180490 20 of 57 
PARAMETER 

PERCENT 

RECOVERY 

RECOVERY 

LIMITS 

PREPARATIONMETHOD ANALYSIS DATE WORK ORDER # 

LCS Lot-Samplef: COK230000-127 Prep Batch t ... : 0327127 

Iron 94 (80 - 120) SW846 6010B 11/23-11/29/10 MAFN81AE 

Dilution Factor: 1 Analysis Time .. : 15:21 

NOTE(S): 

Calculations are performed before rounding to avoid round-off errors In calculated results. 

COK180490 21 of 57 
PARAMETER RECOVERY LIMITS RPD LIMITS DATE ORDER# 

MS Lot-Sample 1: COK170523-001 Prep Batch 1 ... : 0330011 

Mercury 101 (75 - 125) SW846 7470A 

103 (75 - 125) 2. 0 (0-20) SW846 7470A 

Dilution Factor: 1 

Analysis Time .• : 13:43 

MS Run# .•..•.. : 0330003 

NOTE(S): 

Calculations are performed before rounding to avoid round-off errors In calculated results. 

COK180490 22 

11/26/10 11/26/10 

L96421DJ 

L96421DK 

of 57 
PARAMETER RECOVERY LIMITS RPD LIMITS ~ME~TH~O~D~--------- ANALYSIS DATE ORDER # 

MS Lot-Sample t: COK180494-017 Prep Batch t ... : 0327129 

Aluminum 107 (75 - 125) SW846 6010B 

Arsenic 

Barium 

Beryllium 

Boron 

Cadmium 

Calcium 

COK180490 

105 (75 - 125) 1.1 (0-20) SW846 6010B 

105 

103 

106 

104 

106 

105 

105 

104 

103 

102 

103 

103 

(75 

(75 

(75 

(75 

(75 

(7 5 

(75 

(75 

(75 

(75 

(75 

(75 

-

-

-

-

-

-

-

-

-

-

-

-

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....... : 0327079 

125) SW846 6010B 

125) 1.3 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .• : 14:37 

MS Run II .••..•. : 0327079 

125) SW846 6010B 

125) 1.1 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....... : 0327079 

125) SW846 6010B 

125) 1.2 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....•.. : 0327079 

125) SW846 6010B 

125) 1.3 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II .•••... : 0327079 

125) SW846 6010B 

125) 1.0 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....... : 0327079 

125) SW846 6010B 

125) 0.35 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ..•.... : 0327079 

(Continued on next page) 

23 

11/23-11/29/10 L98LQ1AH 

11/23-11/29/10 L98LQ1AJ 

11/23-11/29/10 L98LQ1AL 

11/23-11/29/10 L98LQ1AM 

11/23-11/29/10 L98LQ1AP 

11/23-11/29/10 L98LQ1AQ 

11/23-11/29/10 L98LQ1AT 

11/23-11/29/10 L98LQ1AU 

11/23-11/29/10 L98LQ1AW 

11/23-11/29/10 L98LQ1AX 

11/23-11/29/10 L98LQ1A1 

11/23-11/29/10 L98LQ1A2 

11/23-11/29/10 L98LQ1A4 

11/23-11/29/10 L98LQ1A5 

of 57 
Chromium 

Cobalt 

Copper 

Iron 

Lead 

Lithium 

Magnesium 

COK180490 

105 

104 

103 

102 

107 

106 

97 

97 

102 

101 

106 

105 

103 

103 

ME~T~H~O~D~---------- ANALYSIS DATE ORDER i 

(75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1AE 

(75 - 125) 1.1 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1AF 

(75 -

(75 -

(75 -

(75 -

(75 -

(75 -

(75 -

(75 -

(7 5 -

(75 -

(75 -

(75 -

Dilution Factor: 1 

Analysis Time .• : 14:37 

MS Run # ..••..• : 0327079 

125) SW846 6010B 

125) 1.3 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....... : 0327079 

125) SW846 6010B 

125) 1.2 (0-20) SW846 601.0B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run # .•.••.• : 0327079 

125) SW846 6010B 

125) 0.30 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14 : 37 

MS Run II ..•.... : 0327079 

125) SW846 6010B 

125) 1.1 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run # •.••.•. : 0327079 

125) SW846 6010B 

125) 0.17 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 00:16 

MS Run # ......• : 0327079 

125) SW846 6010B 

125) 0.32 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run II ....... : 0327079 

(Continued on next page) 

24 

11/23-11/29/10 L98LQ1A7 

11/23-11/29/10 L98LQ1A8 

11/23-11/29/10 L98LQ1CA 

11/23-11/29/10 L98LQ1CC 

11/23-11/29/10 L98LQ1CE 

11/23-11/29/10 L98LQ1CF 

11/23-11/29/10 L98LQ1DH 

11/23-11/29/10 L98LQ1DJ 

11/23-12/02/10 L98LQ1CH 

11/23-12/02/10 L98LQ1CJ 

11/23-11/29/10 L98LQ1CL 

11/23-11/29/10 L98LQ1CM 

of 57 
PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER # 

Manganese 104 (7 5 - 125) SW846 6010B 11/23-11/29/10 L98LQ1CP 

103 (7 5 - 125) 0.99 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1CQ 

Dilution Factor: 1 

Analysis Time .• : 14:37 

MS ......• : 0327079 

Molybdenum 104 (75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1CT 

104 (75 - 125) 0.27 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1CU 

Dilution Factor: 1 

Analysis Time •• : 14:37 

MS Run # ..•.... : 0327079 

Nickel 103 (75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1CW 

102 (75 - 125) 1.4 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1CX 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run # ..•••.. : 0327079 

Selenium 104 (75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1Cl 

103 (7 5 - 125) 1.2 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1C2 

Dilution Factor: 1 

Analysis Time .• : 14:37 

MS Run # .••.••. : 0327079 

Silver 108 (7 5 - 125) SW846 6010B 11/23-11/29/10 L98LQ1C4 

106 (75 - 125) 1.5 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1C5 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run # ..••••• : 0327079 

Sodium 107 (75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1C7 

106 (75 - 125) 0.50 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1C8 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run # .....•. : 0327079 

Strontium 105 (75 - 125) SW846 6010B 11/23-11/29/10 L98LQ1DA 

104 (75 - 125) 1.1 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1DC 

Dilution Factor: 1 

Analysis Time .. : 14:37 

MS Run# .....•. : 0327079 

(Continued on next page) 

COK180490 25 of 57 
PARAMETER 

Zinc 

NOTE (S): 

RECOVERY 

104 

103 

LIMITS RPD 

(75 - 125) 

(75 - 125) 1.1 

LIMITS 

(0-20) 

Dilution Factor: 1 

Analysis Time .. : 14:37 

METHOD 

SW846 6010B 

SW846 6010B 

MS Run# ....... : 0327079 

Calculations are performed before rounding to avoid round-off errors in calculated results. . 

COK180490 26 

ANALYSIS DATE 

11/23-11/29/10 

11/23-11/29/10 

ORDER # 

L98LQ1DE 

L98LQ1DF 

of 57 
PARAMETER 

RECOVERY LIMITS RPD LIMITS ME~~TH~O~D~----------

ANALYSIS DATE ORDER # 

MS Lot-Sample f: COK180494-016 Prep Batch f ... : 0327127 

Iron 94 (75 - 125) SW846 6010B 

96 (75 - 125) 0.30 (0-20) SW846 6010B 

Dilution Factor: 1 

Analysis Time .. : 16:16 

MS Run# ....... : 0327078 

NOTE(S): 

Calculations are performed before rounding to avoid round-off erron in calculated results. 

COK180490 27 

11/23-11/29/10 L98LL1AH 

11/23-11/29/10 L98LL1AJ 

of 57 
PARAMETER 

pH 

Acidity 

Ammonia Nitrogen 

Biochemical Oxygen 

Demand (BOD) 

Bromide 

Chemical Oxygen 

Demand (COD) 

Chloride 

Hardness, 

as CaC03 

Nitrate as N 

Nitrite as N 

COK180490 

RESULT 

7.4 

ND 

8.0 

53.2 

28.0 

286 

3490 

1320 

ND G 

ND G 

RL UNITS 

Dilution Factor: 1 

MDL ............ : 0.0 

5.0 mg/L 

Dilution Factor: 1 

MDL ............ : 5.0 

0.50 mg/L 

Dilution Factor: 5 

MDL ............ : 0.041 

2.0 mg/L 

Dilution Factor: 1 

MDL ............ : 0. 79 

2.0 mg/L 

Dilution Factor: 10 

MDL ............ : 0.42 

10.0 mg/L 

Dilution Factor: 1 

MDL ............ : 3.9 

100 mg/L 

Dilution Factor: 100 

MDL ............ : 19.5 

50.0 mg/L 

Dilution Factor: 10 

MDL ............ : 15.4 

0.50 mg/L 

Dilution Factor: 10 

MDL ............ : 0.14 

0.50 mg/L 

Dilution Factor: 10 

MDL ............ : 0.15 

METHOD 

SM20 4500-H+B 

Analysis Time .. : 15:13 

SM20 2310B (4a) 

Analysis Time .. : 13:38 

MCAWW 350.1 

Analysis Time .. : 14:46 

SM20 5210B 

Analysis Time .. : 09:05 

MCAWW 300.0A 

Analysis Time .. : 20:10 

MCAWW 410.4 

Analysis Time .. : 13:16 

MCAWW 300. OA 

Analysis Time .. : 20:31 

SM20 2340C 

Analysis Time .. : 08:45 

MCAWW 300.0A 

Analysis Time .. : 20:10 

MCAWW 300.0A 

Analysis Time .. : 20:10 

(Continued on next page) 

28 

PREPARATIONANALYSIS DATE 

11/18/10 

PREP 

BATCH # 

0322329 

MS Runt ....... : 0322185 

11/27/10 0331042 

MS Run t ....... : 0331019 

11/19-11/23/10 0323198 

MS Run# ....... : 0323115 

11/19-11/24/10 0323082 

MS Runt ....... : 0323050 

11/18/10 0324044 

MS Runt ....... : 

11/29/10 0333068 

MS Run t ....... : 0333032 

11/18/10 0324040 

MS Run f ....... : 

11/29/10 0333050 

MS Runt ....... : 0333025 

11/18/10 0324039 

MS Run II .•..... : 

11/18/10 0324045 

MS Run# ....... : 

of 57 
PARAMETER RESULT 

Oil & Grease (HEM) 13.1 

Specific Conductance 12300 

Sulfate 

Total Alkalinity 

Total Dissolved 

Solids 

Total Recoverable 

Phenolics 

Total Suspended 

Solids 

NOTE (S): 

RL Reporting Limit 

126 J 

103 J 

6740 

0.016 J 

25.6 

RL UNITS 

4.7 mq/L 

Dilution Factor: 0.94 

MDL .•.......... : 1.5 

25.0 umhos/cm 

Dilution Factor: 25 

MDL •.....••••.• : 

10.0 mq/L 

Dilution Factor: 10 

MDL •........•.. : 2.1 

5.0 mg/L 

Dilution Factor: 1 

MDL ............ : 0.41 

50.0 mg/L 

Dilution Factor: 5 

MDL ............ : 50.0 

0.010 mq/L 

Dilution Factor: 1 

MDL ... · ..•...... : 0. 0062 

4.0 mg/L 

Dilution Factor: 1 

MDL •...•...•... : 2 . 0 

G Elevated reporting limit. The reporting limit Is elevated due to matrix interference. 

PREPARATION- PREP 

METHOD ANALYSIS DATE BATCH f 

CFR136A 1664A HEM 11/19/10 0323244 

Analysis Time .. : 10:35 

SM20 2510B 

Analysis Time .. : 00:00 

MCAWW 300 . OA 

Analysis Time .. : 20:10 

SM18 2320 B 

Analysis Time .. : 00:00 

SM20 2540C 

Analysis Time .. : 11 : 15 

MCAWW 420.4 

Analysis Time .. : 10:33 

SM20 25400 

Analysis Time .. : 06:15 

MS Run II .....•. : 

11/29/10 0333041 

MS Run II ....•.• : 0333014 

11/18/10 0324043 

MS Run t ....... : 

12/02/10 0335025 

MS Run t ....... : 0336085 

11/19-11/20/10 0323271 

MS Run II ....... : 0323149 

11/23-11/24/10 0327071 

MS Run# ....... : 0327181 

11/19-11/20/10 0323267 

MS Run# ....... : 0323145 

J Method blank contamination. The associated method blank contains the target analyte at a reportable level. 

COK180490 29 of 57 
Ammonia Nitrogen 

Biochemical Oxygen 

Demand (BOD) 

Bromide 

Chemical Oxygen 

Demand (COD) 

Chloride 

Hardness, 

as CaC03 

Nitrate as N 

COK180490 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

5.0 mg/L 

Dilution Factor: 1 

Analysis Time •• : 13:38 

Work Order #: L999G1AA 

SM20 2310B (4a) 11/27/10 

MB Lot-Sample #: COK190000-198 

0331042 

0.10 mg/L MCAWW 350.1 11/19-11/23/10 0323198 

Dilution Factor: 1 

Analysis Time .. : 13:28 

Work Order #: L99RA1AA MB Lot-Sample #: COK190000-082 

2.0 mg/L SM20 5210B 11/19-11/24/10 0323082 

Dilution Factor: 1 

Analysis Time .. : 09:05 

Work Order #: MACXR1AA 

0.20 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

MB Lot-Sample #: COK200000-044 

MCAWW 300.0A 11/18/10 

Work Order #: MAK8T1AA MB Lot-Sample #: COK290000-068 

10.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 13:14 

Work Order #: MACXH1AA 

1. 0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

MCAWW 410.4 11/29/10 

MB Lot-Sample #: COK200000-040 

MCAWW 300.0A 11/18/10 

Work Order #: MAK501AA MB Lot-Sample #: COK290000-050 

5.0 mg/L 

Dilution Factor: 1 

Analysis Time . . : 08:45 

Work Order #: MACXF1AA 

0.050 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14 : 34 

SM20 2340C 11/29/10 

MB Lot-Sample #: COK200000-039 

MCAWW 300.0A 11/18/10 

(Continued on next page) 

30 

0324044 

0333068 

0324040 

0333050 

0324039 

of 57 
Nitrite as N 

ND 

Oil & Grease (HEM) 

ND 

Specific Conductance 

ND 

Sulfate 

Total Alkalinity 

Total Dissolved 

Solids 

Total Recoverable 

Phenolics 

Total Suspended 

Solids 

NOTE (S): 

0.22 B 

2.3 B 

ND 

0.0068 B 

ND 

Work Order #: MACXX1AA 

0.050 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

Work Order #: MAALD1AA 

5.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 10:35 

Work Order #: MAK241AA 

1.0 umhos/cm 

Dilution Factor: 1 

Analysis Time .. : 00:00 

Work Order #: MACXL1AA 

1.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 14:34 

Work Order #: MANJJ1AA 

5.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 00:00 

MB Lot-Sample #: COK200000-045 

MCAWW 300.0A 11/18/10 

MB Lot-Sample #: COK190000-244 

CFR136A 1664A HEM 11/19/10 

MB Lot-Sample #: COK290000-041 

SM20 25108 11/29/10 

MB Lot-Sample #: COK200000-043 

MCAWW 300.0A 11/18/10 

MB Lot-Sample #: COL010000-025 

SM18 2320 B 12/02/10 

0324045 

0323244 

0333041 

0324043 

0335025 

Work Order #: MAAQV1AA MB Lot-Sample #: COK190000-271 

10.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 11:15 

SM20 2540C 11/19-11/20/10 0323271 

Work Order #: MAGG01AA MB Lot-Sample #: COK230000-071 

0.010 mq/L 

Dilution Factor: 1 

Analysis Time •. : 10:33 

MCAWW 420.4 11/23-11/24/10 0327071 

Work Order #: MAAP91AA MB Lot-Sample #: COK190000-267 

4.0 mg/L 

Dilution Factor: 1 

Analysis Time .. : 06:15 

SM20 2540D 11/19-11/20/10 0323267 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

B Estimated result. Result is less than RL. 

COK180490 31 of 57 
PARAMETER RECOVERY LIMITS RPD LIMITS ~ME~TH_O~D ____________ ANALYSIS DATE BATCH # 

Biochemical Oxygen 

Demand (BOD) 

Bromide 

Chloride 

Nitrate as N 

Nitrite as N 

Oil & Grease 

Sulfate 

NOTE(S): 

105 

105 

104 

104 

104 

104 

108 

108 

104 

103 

(HEM) 

82 

86 

104 

104 

WO#:L99RA1AC-LCS/L99RA1AD-LCSD LCS Lot-Sample#: COK190000-082 

(85 - 115) SM20 5210B 

(85 - 115) 0.24 (0-20) SM20 5210B 

11/19-11/24/10 0323082 

11/19-11/24/10 0323082 

Dilution Factor: 1 Analysis Time •. : 09:05 

WO#:MACXR1AC-LCS/MACXR1AD-LCSD LCS Lot-Sample#: COK200000-044 

(90 - 110) MCAWW 300.0A 11/18/10 0324044 

(90 - 110) 0.09 (0-20) MCAWW 300.0A 11/18/10 0324044 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MACXH1AC-LCS/MACXH1AD-LCSD LCS Lot-Sample#: COK200000-040 

(90 - 110) MCAWW 300.0A 11/18/10 0324040 

(90 - 110) 0.13 (0-20) MCAWW 300.0A 11/18/10 0324040 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MACXF1AC-LCS/MACXF1AD-LCSD LCS Lot-Sample#: COK200000-039 

(90 - 110) MCAWW 300.0A 11/18/10 0324039 

(90 - 110) 0.14 (0-20) MCAWW 300.0A 11/18/10 0324039 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MACXX1AC-LCS/MACXX1AD-LCSD LCS Lot-Sample#: COK200000-045 

(90 - 110) MCAWW 300.0A 11/18/10 0324045 

(90 - 1~0) 0.07 (0-20) MCAWW 300.0A 11/18/10 0324045 

Dilution Factor: 1 Analysis Time .. : 14:13 

WO#:MAALD1AC-LCS/MAALD1AD-LCSD LCS Lot-Sample#: COK190000-244 

(78 - 114) CFR136A 1664A HEM 11/19/10 0323244 

(78 - 114) 3.9 (0-18) CFR136A 1664A HEM 11/19/10 0323244 

Dilution Factor: 1 Analysis Time .. : 10:35 

WO#:MACXL1AC-LCS/MACXL1AD-LCSD LCS Lot-Sample#: COK200000-043 

(90 - 110) MCAWW 300.0A 11/18/10 0324043 

(90 - 110) 0.17 (0-20) MCAWW 300.0A 11/18/10 0324043 

Dilution Factor: 1 Analysis Time .. : 14:13 

Calculations are performed before rounding to avoid round-off errors In calculated results. 

COK180490 32 of 57 
PARAMETER RECOVERY 

pH 

100 

Acidity 

99 

Ammonia Nitrogen 

92 

Chemical Oxygen 

Demand (COD) 

Hardness, 

as CaC03 

103 

100 

Specific Conductance 

111 

Total Alkalinity 

91 

Total Dissolved 

Solids 

109 

Total Recoverable 

Phenolics 

100 

COK180490 

LIMITS METHOD 

ANALYSIS DATE 

BATCH # 

Work Order #: L985AlAA LCS Lot-Sample#: COK180000-329 

(99 - 101) SM20 4500-H+B 11/18/10 0322329 

Dilution Factor: 1 Analysis Time .. : 15:05 

Work Order #: MAKRLlAC LCS Lot-Sample#: COK270000-042 

(80 - 120) SM20 2310B (4a) 11/27/10 0331042 

Dilution Factor: 1 Analysis Time .. : 13:38 

Work Order #: L999GlAC 

(90 - 110) MCAWW 350.1 

LCS Lot-Sample#: COK190000-198 

11/19-11/23/10 0323198 

Dilution Factor: 1 Analysis Time .. : 13:26 

Work Order #: MAK8TlAC LCS Lot-Sample#: COK290000-068 

(90 - 110) MCAWW 410.4 11/29/10 0333068 

Dilution Factor: 1 Analysis Time . . : 13:14 

Work Order #: MAK501AC LCS Lot-Sample#: COK290000-050 

(90 - 110) SM20 2340C 11/29/10 0333050 

Dilution Factor: 1 Analysis Time •• : 08:45 

Work Order #: MAK241AC 

( 80 - 120) SM20 2510B 

LCS Lot-Sample#: COK290000-041 

11/29/10 0333041 

Dilution Factor: 1 Analysis Time .. : 00:00 

Work Order #: MANJJlAC 

(80 - 120) SM18 2320 B 

LCS Lot-Sample#: COLOl0000-025 

12/02/10 0335025 

Dilution Factor: 1 Analysis Time .• : 00:00 

Work Order #: MAAQVlAC LCS Lot-Sample#: COK190000-271 

(80 - 120) SM20 2540C 11/19-11/20/10 0323271 

Dilution Factor: 1 Analysis Time . . : 11:15 

Work Order #: MAGGOlAC LCS Lot-Sample#: COK230000-071 

(90 - 110) MCAWW 420.4 11/23-11/24/10 0327071 

Dilution Factor: 1 Analysis Time . . : 10:33 

(Continued on next page) 

33 of 57 
PARAMETER RECOVERY 

Total Suspended 

Solids 

97 

NOTE(S): 

LIMITS 

~ME~TH~O~D~----------

PREPARATION

ANALYSIS DATE PREP BATCH # 

Work Order #: MAAP91AC LCS Lot-Sample#: COK190000-267 

(80 - 120) SM20 25400 11/19-11/20/10 0323267 

Dilution Factor: 1 Analysis Time .. : 06:15 

Calculations are performed before rounding to avoid I'OUJ1d.off errors In calculated results. 

COK180490 34 of 57 
Ammonia Nitrogen 

114N 

112N 

WO#: L96GV1A1-MS/L96GV1A2-MSD MS Lot-Sample #: COK170441-001 

Chemical Oxygen 

Demand (COD) 

92 

100 

Total Recoverable 

Phenolics 

NOTE (S): 

102 

102 

(90 - 110) MCAWW 350.1 11/19-11/23/10 0323198 

(90 - 110) 1.4 (0-20) MCAWW 350.1 11/19-11/23/10 0323198 

Dilution Factor: 1 

Analysis Time •. : 13:49 

MS Run# •.• • ... : 0323115 

WO#: MAEP31AH-MS/MAEP31AJ-MSD MS Lot-Sample #: COK220467-001 

(90 - 110) 

(90 - 110) 6.0 

MCAWW 410.4 

(0-20) MCAWW 410.4 

Dilution Factor: 1 

Analysis Time .. : 13:17 

MS Run# •.•.•.. : 0333032 

11/29/10 

11/29/10 

0333068 

0333068 

WO#: L98HL1AF-MS/L98HL1AG-MSD MS Lot-Sample #: COK180491-002 

(90 - 110) MCAWW 420.4 

(90 - 110) 0.19 (0-20) MCAWW 420.4 

Dilution Factor: 1 

Analysis Time .. : 10:33 

MS Run# ....... : 0327181 

11/23-11/24/10 0327071 

11/23-11/24/10 0327071 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

N Spiked analyte recovery Is outside stated control limils. 

COK180490 35 of 57 
PARAM RESULT RESULT 

Biochemical Oxygen 

Demand (BOD) 

NO NO 

COK180490 

RPD 

ARATION

PREP 

UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH # 

SD Lot-Sample #: COK180463-001 

mg/L 0 (0-20) SM20 5210B 11/19-11/24/10 0323082 

Dilution Factor: 1 Analysis Time .. : 09:05 MS Run Number .. : 0323050 

36 of 57 
DUPLICATE 

PARAM RESULT RESULT 

Total Suspended 

Solids 

ND ND 

COK180490 

RPD 

UNITS RPD LIMIT METHOD 

PREPARATION

PREP 

ANALYSIS DATE BATCH # 

SD Lot-Sample #: COK190421-001 

mg/L 0.0 (0-20) SM20 2540D 11/19-11/20/10 0323267 

Dilution Factor: 1 Analysis Time .. : 06:15 MS Run Number .. : 0323145 

37 of 57 
PARAM RESULT RESULT 

Total Dissolved 

Solids 

259 215 

COK180490 

RPD 

UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH # 

SD Lot-Sample #: COK170523-001 

mg/L 19 (0-20) SM20 2540C 11/19-11/20/10 0323271 

Dilution Factor: 1 Analysis Time .. : 11:15 MS Run Number .. : 0323149 

38 of 57 
PARAM RESULT RESULT 

Acidity 

ND ND 

COK180490 

UNITS RPD LIMIT METHOD ANALYSIS DATE 

SD Lot-Sample i: COK180529-003 

mg/L 0 (0-20) SM20 231GB (4a) 11/27/10 

Dilution Factor: 1 Analysis Time •. : 13:38 MS Run Number .. : 

39 

BATCH # 

0331042 

0331019 

of 57 
U

CATE 

PARAM RESULT RESULT 

Acidity 

ND ND 

COK180490 

RPD PREPARATION

UNITS RPD LIMIT METHOD ANALYSIS DATE 

SD Lot-Sample #: COK220465-001 

mg/L 0 (0-20) SM20 231GB (4a) 11/27/10 

Dilution Factor: 1 Analysis Time .. : 13:38 MS Run Number .. : 

40 

PREP 

BATCH # 

0331042 

0331019 

of 57 
PARAM RESULT 

RESULT 

Specific Conductance 

523 528 

COK180490 

UNITS RPD 

umhos/cm 0.95 

Dilution Factor: 1 

RPD 

LIMIT METHOD 

SO Lot-Sample #: 

(0-20) SM20 2510B 

Analysis Time .. : 00:00 

41 

PREPARATION

ANALYSIS DATE 

COK160529-001 

11/29/10 

MS Run Number .. : 

PREP 

BATCH # 

0333041 

0333014 

of 57 
PARAM RESULT RESULT 

Hardness, 

as CaC03 

200 200 

COK180490 

UNITS RPD LIMIT METHOD ANALYSIS DATE 

SD Lot-Sample #: COK040431-004 

mg/L 0.0 (0-20) SM20 2340C 11/29/10 

Dilution Factor: 10 Analysis Time .. : 08:45 MS Run Number .. : 

42 

BATCH # 

0333050 

0333025 

of 57 
PARAM RESULT RESULT 

Hardness, 

as CaC03 

36000 35000 

pH 

6.6 6.6 

COK180490 

UNITS RPD LIMIT METHOD ANALYSIS DATE 

SD Lot-Sample #: COK180438-001 

mg/L 2.8 (0-20) SM20 2340C 11/29/10 

Dilution Factor: 500 Analysis Time .. : 08:45 MS Run Number .. : 

SD Lot-Sample #: COK180438-001 

0.0 (0-2.0) SM20 4500-H+B 11/18/10 

Dilution Factor: 1 Analysis Time .. : 15:07 MS Run Number .• : 

43 

BATCH # 

0333050 

0333025 

0322329 

0322185 

of 57 
PARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE 

Total Alkalinity SD Lot-Sample #: COK180490-001 

103 J 103 mg/L 0.068 (0-20) SM18 2320 B 12/02/10 

Dilution Factor: 1 Analysis Time .. : 00:00 MS Run Number .. : 

NOTE(S): 

Calcul•lons are performed before rounding to avoid round-off errors In calculated results. 

J Method blank contamination. The associated method blank contains the ~get analyte at a reportable level. 

COK180490 44 

BATCH # 

0335025 

0336085 

of 57 
Project Description(s) 

Equitable Production Company 

Equitable Production Company 

For: 

Chris Kovitch 

TestAmerlca Pittsburgh 

301 Alpha Drive; RIDC Park 

Pittsburgh, PA 15238 

Melissa Deyo For Sally Hoffman 

Project Manager 

melissa.deyo@testamericainc.com 

Tuesday, January 4, 2011 

The test results in this report meet all NELAP requirements for analytes for which accreditation is required or 

available. Any exception to NELAP requirements are noted in this report. Persuant to NELAP, this report may not 

be reproduced, except in full, without the written approval of the laboratory. All questions regarding this test report 

should be directed to the TestAmerica Project manager who has signed this report. 

COK180490 45 

of 57 
As of 08/16/2010 

STATE Program Cert #I Lab ID 

Ark_ansas CWA, RCRA, SOIL 88-0686 

California* NELAP CWA, RCRA 01169CA 

Connecticut SDWA, CWA, RCRA, SOIL PH-0568 

Florida* NELAP CWA, RCRA E87672 

Georgia* SDWA,NELAP CWA, RCRA 956 

Illinois* NELAP SDWA, CWA, RCRA 200003 

Iowa SWIGS 374 

Kansas* NELAP SDWA, CWA, RCRA E-10187 

Kentucky SDWA 90029 

Kentucky UST UST 30 

Louisiana* NELAP CWA, RCRA 2031 

Maine SDWA, CWA NY0044 

Maryland SDWA 294 

Massachusetts SDWA, CWA M-NY044 

Michigan SDWA 9937 

Minnesota SDWA,CWA, RCRA 036-999-337 

New Hampshire* NELAP SDWA, CWA 233701 

New Jersey* NELAP,SDWA, CWA, RCRA, NY455 

New York* NELAP, AIR, SDWA, CWA, RCRA 10026 

North Dakota CWA, RCRA R-176 

Oklahoma CWA, RCRA 9421 

Oregon* CWA,RCRA NY200003 

Pennsylvania* NELAP CWA,RCRA 68-00281 

Tennessee SDWA 02970 

Texas* NELAP CWA, RCRA T1 0470441 2 -08-TX 

USDA FOREIGN SOIL PERMIT 

Virginia SDWA 

Washington* NELAP CWA,RCRA 

Wisconsin CWA, RCRA 

West Virginia CWA,RCRA 

*As required under the hdicated accrec:llation, the test results i1 this report meet all NELAP 

requirements for parame ters for which accreditation is required or avalable. Any exceptions to 

NELAP requirements are noted in this report. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

S-41579 

278 

C1677 

998310390 

252 

COK180490 46 Page 2 of t1 of 57 
field-pH), they were not analyzed immediately, but as soon as possible after laboratory receipt. 

I certify that this data package is in compliance with the terms and conditions of the contract, both technically 

and for completeness, for other than the conditions detailed within the body of this report. Release of the data 

contained in this sample data package and in the electronic data deliverables has been authorized by the 

Laboratory Manager or his/her designee, as verified by the following signature. 

Melissa Deyo For Sally Hoffman 

Project Manager 

Tuesday, January 4, 2011 

There are pertinent documents appended to this report, 2 pages, are included and are an integral part of this report. 

Reproduction of this analytical report is permitted only in its entirety. This report shall not be reproduced except in 

full without the written approval of the laboratory. 

TestArnerica Laboratories, Inc. certifies that the analytical results contained herein apply only to the samples tested 

as received by our Laboratory. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 47 
p

ce

ed and analyzed past holding time. 

Z3 The sample required a dilution, the surrogate spike concentration in the sample are reduced to a level where the 

recovery calculation does not provide useful information. 

NR Any inclusion of NR indicates that the project specific requirements do not require reporting estimated values below 

the laboratory reporting limit. 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 48 
U

OW BACK

590398 (RTK1402..01 

Water) Sampled: 11/17/10 11:30 

General Chemistry Parameters 

Recvd: 11/19/10 09:00 

Methylene Blue Active 0.134 H3 0.0250 0.0130 mg/L 1.00 11/19/10 16:30 JFR 10K2067 5540C 

Substances 

Total Kjek:lahl Nitrogen 8.52 008 2.00 1.50 mg/L 10.0 11/24/10 14:01 JME 10K2404 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 49 

351.2 
HURD FLOW BACK-590398 

HURD FLOW BACK-590398 

RTK1402-01 

RTK1537-01 

Water 

Water 

11/17/10 11 :30 

11/17/1011:30 

TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 50 

11/19/10 09:00 

11/23/10 09:15 

Page 6 of t1 of 57 
p

General Chemistry Parameter! 

Methylene Blue Active 0.134 H3 0.0250 0.0130 mg/L 1.00 11/19/10 16:30 JFR 10K2067 5540C 

Substances 

Total Kjeldahl Nitrogen 8.52 008 2.00 1.50 mgll 10.0 11/24/10 14:01 JME 10K2404 351.2 

TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 51 Page 7 obf1 57 
(

) Sampled: 11/17/10 11:30 

Non-Halogenated Volatile Organics 

Recvd: 11123/10 09:15 

Ethylene Glycol NO 010 1000 NR rngiL 100 11/24/10 20:36 GFD 10K2446 8015 

1, 4-Butanedio/ 198% 01 O,Z3 Surr Umits: (66-130%) 11124110 20:36 GFD 10K2446 8015 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 52 Page 8 of L1 of 57 
General Chemistry Parameters 

351 .2 10K2404 RTK1402-01 25.00 mL 25.00 mL 11/23/10 10:20 

5540C 10K2067 RTK1402-01 400.00 mL 400.00 mL 11/19/10 16:30 

SAMPLE EXTRACTION DATA 

WWol Extract 

Parameter Batch Lab Number Extracte Units Volume Units Date Prepared 

Non-Halogenated Volatile Organics 

8015 10K2446 RTK1537-01 0.50 mL 1.00 mL 11/24/10 06:26 

TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 53 

JME TKN Digestion 

JFR MBAS 

Lab 

Tech Extraction Method 

GFD 8015 Glycols 

Page 9 obJ:1 57 
Blank Analyzed: 11124/10 (Lab Number:10K2446-BLK1, Batch: 101<2446) 

Ethylene Glycol 10 NR rng/L NO 

Surrogate: 1,4-Butanediol mg!L 

LCS Analyzed: 11/24/10 (Lab Number:10K2446-BS1, Batch: 101<2446) 

Ethylene Glycol 20.0 10 NR rng/L 19.8 

Surrogate: 1,4-Butanediol mg!L 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 54 

109 

99 

109 

66-130 

50-150 

66-130 

Page 1 0 off11 0 57 
Blank Analyzed: 11/19/10 (Lab Number:10K2067-8LK1, Batch: 101<2067) 

Methylene Blue Active 0.0250 0.0130 mgiL ND 

Substances 

LCS Analyzed: 11/19/10 (Lab Number:10K2067-BS1, Batch: 101<2067) 

Methylene Blue Active 0.400 0.0250 0.0130 mg/L 0.380 

Substances 

General Chemistry Parameters 

Blank Analyzed: 11/24/10 (Lab Number:10K2404-BLK1, Batch: 101<2404) 

Total Kjeldahl Nitrogen 0.20 0.15 mg/L ND 

LCS Analyzed: 11/24/10 (Lab Number:10K2404-8S1, Batch: 101<2404) 

Total Kjeldahl Nitrogen 2.50 0.20 0.15 mg/L 2.46 

TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600 fax 716-691-7991 

www.testamericainc.com 

COK180490 55 

95 

98 

90-110 

90-110 
WORK L.OCATION: W5 TNLAmetlca NAhvflle 

ADDRESS; 2000 Fosler CnliehJOn Drive 

• NtshlfiJie TN 37204 

SNP.r 1 

t 

CJ...IENT ID: HURD FLOW BACK·590398 

S6MPLE COMMENT 

DATEmME 20101117 1130 MATRIX: I WATER 

METHOD; zo NONE 

EXTBACTION: 88 NO SAMPLE PERFORMED/ OCTYPE; Cl STANDARD TEST SET 

WQR!CCPROER L98HCIAO XX 

114--:::rt:f:Q!;!: zo NONE NONE WATER, o4Z5.1 •BAS TA Nash'lllle 

EXTRakiiQN: 88 NO SAMPLE P'R:EP'ARAiiON I QC T'r'P'E: 01 TEST SET 

WORKOROER L£18HC1A1 )()( 

Th8 tisted on lhls form are being sen11o yourlocBtiDn fi:lr the specified analysis. If you haw any ques!ions. please 

eon1act the F='mject Manager lsted above. PLEASE RETURN THE ORIGINAL SIGNED FORM WITH THE REPORT AT THE 

COMPLETION OF ANALYSIS. · 

IIi 

Thank You 

IJ 

testAmenca Pittsburgh 

Sample Receiving L 

BY: DATE: II b b C,) 7 c. " 1r r 1 ·--=-----

REcelvE:.oFORLAeev.· DATE:/1 - TIME: <21'vJ,) 

TesiAmerica Pittsbu.rgll 

COK1J0490 

printed on: Tlll.lre:d;,y. 1\jovenlber 18, 2010 01:04 Pr.t 

56 Page1 of 57 
. 

rt · WOR« LOCATION: 

ADDRESS: 10 Ma%!!!1Mxx! DI'!Ye 

SMP' 1 

AmherE! N"r 14221 

CLIENT JD: liURD fL. Oil B~CK-!1-!JOJ~l'. SAMPLE COt.I!MjiNI 

..,'5TI'tOD: ~ NONE NONE WAT!R.I01!1 l!th1'en& GIJr;ol T.A Bufralo 

t.IJA,JBI:X.: I WATER 

I 

I 

.r 

EXTRAC!10N: B8 .IK) SAMPLE. ~AAATION PERFORMED/ OCIYPE: D1 SiANOA~tl 'lEST a:-;-

WQBI('ORQER l.M."IC1A2 ~ XJt 

•I The sample(s} listed en ltds ro1:n are beil'lg se,liO your k)calic!fl lor the li1P&Cillltd analysis.. u !'OU Nwe anv q~.~estcn •. '!)leaSe conti!CIIhe ?.roject Managet listed above. PLEASE RETURN THE ORIGINAL SIGNED FORM WrTH THE REP~ .\T THE 

COMPLETION OF ANALYSIS. 't 

thank VDU 

TesiAmerice Pillsburgh Scl.mpl~ Receiving 

!t 

-----:-,c---------- DATE:...;I~~+-r----TIME:.L2:~ _ 

--!\-_.,..:;....._ ___ --ft- DATE: --=-~f-1:---TIME ~)~ _ :r 

iesiAIMf'lca. P1ltS.buryh 

COK180490 

Jl- ll -J~ prlnle\luu; Tllul:ldl:f, ~ovet•1ber "lB. 201{) 01:04PM 

57 

>agP.1 

•; 

., 

J 

li 

I 

., 

of 57 

-4· 

t 

COK180493 

ANALYTICAL REPORT 

Fonll 26R 

Lot I: COJ0.80493 

MaryanDa Babich 

Equitable Productior co. 

225 Borth Shore Dr.: .-e 

Pittsburgh, PA 15212-5861 

INC. 

Project Manager 

December 15, 2010 

301 Alpna Drive Pittsburgh, PA 15238 tel412.963.7058 fax412.963.2468 www.testamericainc.com 

1 of 14 
TestAmerica's St. Louis laboratory analyzed the metals. 

The sample was analyzed at a dilution for strontium due to the high concentration of the 

target analyte. The reporting limit has been adjusted accordingly. 

Radiological Chemistry: 

TestAmerica's St. Louis laboratory analyzed the gross alpha and beta. 

The gross Alpha Beta reporting limit was not met due to a reduction of sample size attributed to the sample's high residual mass. The analytical results are reported. 

COK180493 2 of 14 
n 

0 

~ 

1-' 

<Xl 

0 

~ 

\0 

VJ 

VJ 

0 

HI 

1-' 

~ 

~T~l-~.ftoc .. 

. ,.,.. ......... 

T~&l)ai!Qn._ft~ld ~!Cit.CO.-- ....... 

Chain of Custody Record 

Test!~merlcaiAboratory lacatloa:_-:=:-::::---==-:-:::::=:----:=~-:::----:=~------------- Replatory pnanm: C1 OW C:=:J NPDf.S I=:J RC:Ro\ c::J Other - ··· ---··--" ----

Test America THE LEAllP IN ti:HYIROIIMENTAL 11!8Tm0 

5o"'''le Spedflc S-1 

Sp«lal IIIICI'tRI .... ; 

.;l .. ~ .. 

TAL0018- I (04110) 
Gross Alpha/Beta by GFPC 

Trace Inductively Coupled Plasma (ICP) Metals 

SW846 9310 MOD SWB46 6010C 

Refereuces: 

SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical 

Methods", Third Edition, November 1986 and its updates. 

COK180493 4 of 14 
m'I"B(S): 

- Tbc ltlllytical resuhs of lhc llll1plcs lilled above arc praemcd on Che followin& pqes. 

- All cak:uladons are perfonnecl belbre roundln& to avoid round-off errors in calculated resulls. 

- ResuiCI no&cd as "ND" were not dcleaed 11 or above lhc Silled limic. 

- ThiJ report must not be reproduced, cxapt In CuD, wilbout !lie wrillal approval of lhe laboratory. 

- Resul11 for lbe followina )lii'IIIIXfelll arc 111:\'CI' l1iJIOlUd on a dry weight basis: color, conorivity, density, flubpoinr, ipillbility, layers, odor, 

palDt filler lesl, pH. porosity preaute, rcadivily, redox potelllial, specific aravll)', spot taas, &Oiidl. solubility, ~. Yillcolity, and wei&bt. 

COK180493 5 of 14 
=.P::.:ARAME::.:..:::..::T.:.;E=R:;._ __ RE=S:::.;UL=T=------ LIMIT __ ;;.;;ME=T.=.:H:.:.O::..:D=c.._ _____ ANALYSIS DATE ORDER # 

Prep Batch •••• : 0335204 

Strontium 94700 100 ug/L SWB-16 6010C 12/01-12/13/10 L98BQ1AA 

Dilution Factor: 20 Analysis Time .. : 13:47 MS Run# ....... : 0335105 

MDL •••••••••••• : 10.8 

Thorium 510 200 ug/L SW846 6010C 12/01-12/08/10 L98BQ1AD 

Dilution Factor: 1 .Analysis Time .. : 15:07 MS Run# ....... : 0335105 

MDL •••••••••••• : 35.6 

uranium ND 500 ug/L SW846 6010C 12/01-12/13/10 L9BHQ1AC 

Dilution Factor: 1 Analysis Time .• : 12:10 MS Run# ....... : 0335105 

MDL •••••••••••• : 23.5 

COK180493 6 of 14 
MB Lot

Sample I: FOLOl0000

204 Prep Batch 1 

 : 0335204 

Strontium ND 5.0 ug/L SW846 6010C 

Thorium ND 

Uranium ND 

BOTB(S): 

Dilution Factor: 1 

Analysis Time •. : 11:25 

200 ug/L 

Dilution Factor: 1 

Analysis Time .. : 14:17 

500 ug/L 

Dilution Factor: 1 

Analysis Time .. : 11:25 

Calculations arc pcrfonnc:d before rounding to IIVOid round-off errors in calwlatc:d n:sulrs. 

COK180493 7 

SW846 6010C SW846 6010C 

12/01-12/13/10 MAN7QlAA 

12/01-12/08/10 MAN7Q1AD 12/01-12/13/10 MAN7Q1AC 

of 14 
TS 

~ME=TH~O~D~-------- ANALYSIS DATE WORK ORDER # 

LCS Lot-Samplei: FOLOl0000-204 Prep Batch 1 ... : 0335204 Strontium 106 (BO - 120) SW846 6010C 12/01-12/13/10 MAN7Q1AB Dilution Factor: 1 Analysis Time •• : 11•32 

Uranium 102 (80 - 120) SW846 6010C 12/n1-12/13/1o MAN7Q1AF Dilution Factor: 1 Analysis Time .. : 11:32 

Thorium 102 (80 - 120) SW846 6010C 12/0l-12/08/10 MAN7Q1AG Dilution Factor: 1 Analysis Time .. : 14:23 

ROTB(S): 

Caleulations are performed before roundiD& to avoid round-off crTOI'Ii in calwlated resulls. 

COK180493 8 of 14 
MS Lot-Sample I: COK180450-001 Prep Batch t ... : 0335204 

Strontium 0.0 N (75 - 125) SW846 6010C 

0.0 N (75- 125) 0.0 (0-20) SW846 6010C 

Thorium 

Uranium 

BOTB(S): 

29 N 

78 

42 N 

52 N, * 

(75 -

(75 -

(75 -

(75 -

Dilution Factor: 500 

Analysis Time •. : 13:32 

MS Run# ..•.... : 0335105 

125) SW846 

125) 3.7 (0-20) SW846 

Dilution Factor: 50 

Analysis Time • . : 14:54 

MS Run fl. ...... : 0335105 

125) SW846 

125) 21 (0-20) SW846 

Dilution Factor: 50 

Analysis Time .. : 11:55 

MS Run 1 •••••.• : 0335105 

Calculations are performed before roundina to avoid round-off enon iD c:alaalaled results. 

N Spilced ~yre rcamry is ouaidc IIIIAICI comrollimils. 

• Relative pcrcem diffcn:nce (RPD) is outside Silled oonttol limit&. 

COK180493 9 

6010C 

6010C 

6010C 

6010C 

12/01-12/13/10 L977P1AJ 

12/01-12/13/10 L977P1AK 

12/01-12/08/10 L977PlAN 

12/01-12/08/10 L977P1AP 

12/01-12/13/10 L977P1AL 

12/01-12/13/10 L977P~ 

of 14 
aaault 

aROSS A/B BY GFPC SW846 ,310 MOD 

Groea Alpha 

Groaa Beta 

NOTB(S) 

49 

21 

Qual 

u 

u 

Data ara incogplate witho~t tha caee narrative . 

KDC ia determined by instrument performance only. 

Bold reaulta are greater than the MDC. 

Total 

Vr&Qart. 

(:Z o+/·) 

40 

16 

u Result ia leas than the aampla dataction limit. 

COK180493 

PZ'ap 

RL mdc: Data 

pCi/L Batcb • 0326115 

3 59 11/22/10 

4 25 11/22/10 

10 

ADalya1a 

Data Yld~ ll/23/lD 

11/23/10 

of 14 
To"al 

UD.coert. 

Par-ter ae.ul" ~1 12 (1+/-) 

BROSS A/8 BY 13J'PC Stf846 9310 ICOD 

Gross Alpha -0 . 63 u 0.41 

Gross Beta 0 . 99 u 0.67 

NOTB(S) 

nata are 1ncooaplete without tbe caaa narrative. 

MDC ie determined ueing inatrument performance only 

Bold result• are greater than the MDC. ~ Reault ia leaa than the aample detection liait. 

COK180493 

pCi/L 

IlL 

Batch 

3,00 

4 . 00 

11 

Lab BIUIPla ID 

Prep Analy•h 

1IDC 

Data Date 

• 0326115 YlcS' POJ::22000D-115B 

l.l ll/22/10 11/23/10 

1.0 ll/22/10 11/23/10 

of 14 
Par .. ete:r 

Spike -.ant ••11111t 

Toul 

'Dncert. 

(2 G+/-) \ Ylcl \ aec 

La!) s...,le JD 

QC Caatrol 

LiaiU 

GROSS A/8 BY OPPC SW846 9310 MOD pCi/L !1310 NOD POJt220000-115C 

Gross Alpha 49.4 53.4 

Gross Beta 66.8 66.3 

Ba~d> •• 0326115 

NOTB(Sl 

MDC ie deterained by inetrument perfo~c• only 

5.9 

5.7 

1.2 

l.l 

108 

99 

ualyde Date: 11/23/10 

Calculetione are perfo~d before rounding to avoid round-off error in calculeted reeulte 

COK180493 12 

(69 - 128) 

(74 - 128) 

of 14 
Spike PaZ"aaeter 

A~Dolmt 

GROSS A/8 BY' OI'PC SN8U 9310 MOD 

Gross Beta 26700 

Batch II : 

GROSS A/8 BY QFPC SW846 9310 MOD 

Gross Alpha 1!1800 

Batch #: 

NOTB(S) 

Spike 

•••\llt 

29900 

0326115 

32400 

0326115 

Da'a are incomplete without the case narrative . 

Total Total 

'D'Ilce"t. Spike SUIJile 'D'Ilce"t. 

12o +/·l Ylcl. •••~alt (2 0 +/-) 

pCi/L 9310 MOD 

2500 3920 610 

Analysis Date: 11/23/10 

pCi/L 9310 ICOD 

3800 17800 2500 

Analysis Date: 11/23/10 

Calculations are performed before rounding to avoid round -off errors in calculated results. 

COK180493 13 

0C SUIPle 

\TLD \RBC 

ID 

QC CODtrol 

t.imit8 

C01tl80t50-001 

97 (54-150) 

C01t180450-001 

74 (35-150) 

of 14 
••r-t•r 

GROSS A/8 BY GFPC 

Gross Alpha 

Gross Beta 

NOTE(S) 

SAIIPLB 

hlnllt 

SW8t6 9310 ICOD 

17800 

3920 

aatcb •• 

Total 

Vncart. 

(lcr+/-1 

2500 

610 

0326115 

Data are incomplete witbout the c••• narrative. 

DIIPLICATII ~ nd hll\llt 

pCi/L 9310 ICOD 

lUDO 

t7t0 

Total 0C: BIIIIPle ID 

'lhlaa><t. 

12 cr+/-1 'nd Pracieiou 

COitl80450-001 

2700 '1 

680 20 

ISalUplel 0326115 (Dupl icat11 l 

calculation• are perfo~4 before roundinv to avoid round-off error in calculated reaulta 

COK180493 14 

\RPD 

tRPD 

of 14 
ANAL YllCAL REPORT 

Ponl 26R. 

Lot I: COUB0503 

Maryanna Babich 

Equitable Production Co. 

225 North Shore Drive 

Pittsburgh. PA 15212-5861 

Chriatina M. Jtovitch 

Project Manager 

November 30. 2010 

301 Alpha Drive Pittsburgh, PA 15238 te14 12.963.7058 fax 412.963.2468 www.testamericainc.com 

COK180503 1 of 14 
TestAmerica

s St. Louis laboratory performed the metals analysis. 

The sample was analyzed at a dilution due to the presence of matrix interferences. The 

samples caused QC failure at a lesser dilution and were high in target analytes. The reporting limit has been adjusted for the dilution. 

The method blank had strontium detected at a concentration between the MDL and the 

reporting limit. The result was flagged with a "B, qualifier. Any sample associated with 

a method blank that had the same analyte detected had the result flagged with a "J" qualifier. 

Radiological Chemistry: 

TestAmerica•s St. Louis laboratory performed the radiological analysis. 

The gross alpha beta reporting limit was not met due to a reduction of sample size attributed to the sample's high residual mass. The analytical results are reported. 

COK180503 2 of 14 
() 

0 

~ 

1-' 

co 

0 

lJ1 

0 

w 

w 

0 

Hl 

1-' 

~ 

--'T~&~• "-----~- .. ,.,.,....ar,.~~- ................. 

Cbatn of Custody Record Test America TlfE LUOERIN E~AL TlliTWG 

MOIIIha 

S.aopleSpedtlc ,..., 

SpediJ ... Ia ua.. 

TALOOII-1 (04/JO) 
Gross Alpha/Beta by GFPC 

Trace Inductively Coupled Plasma (ICP) Metals 

References: 

SW846 9310 MOD 

SW846 6010C 

SW846 RTest Methods for Evaluating Solid waste, Physical/Chemical Methods", Third Edition, November 1986 and its updates. 

COK180503 4 of 14 
ROTB(S): 

• The -!Jtical rlllllls of lhl .. mptes lbllld lbove lie presenlld Dn lhe fOIIOwillg I'll"· 

• All calcullliDns .,.. perfDrmed WfDre 111111ding to m~kii'DIIIIIkllf .rnn In Cllculllild r.dls. 

• Resulll ~a "NO" - nD1 dlleclld a Dr _,.llle Slllld llml. 

• This rwpDit must IIIII b. nprDCiuced, excaptln full, wiiiiOd .._ wrilltn •prcMI vf lhiiiiiOniDry. 

• Resulh far lhl follvlrlng penme111$ are-reported Dill 11y 111119t 111511: color, wnosfvily, •nsiry, fllllllpDinl. igniltblllty, IIY«$. Odlr. 

palM fi .. lnl, pH, pDIOiily preaure. ,_.lvlty, ndDX polelllial, spedflc gnvily, spDtle'IU, sOlids, solulllllly, tllllpenllft, v'-hy, IIIII Wllgllt. 

COK180503 5 

ll/17 /10 1l: 30 

of 14 
PREPARATION- WORK 

~PARAME~~~T~E:R~----

~RE==SUL~T~----- LIMIT 

~UN~I~T~S~---

ME~T~H~O~D~--------- ANALYSIS DATE ORDER # 

Prep Batch 1 ... : 0326259 

Strontium 4130 J 

Thorium ND 

Uranium ND 

NOTB(S): 

COK180503 

50.0 ug/L 

Dilution Factor: 10 

MDL .. .. .. . ... .. : 5.4 

10000 ug/L 

Dilution Factor: so 

MDL •• • .••• • •••• : 1780 

5000 ug/L 

Diluti on Factor : 10 

MDL •• • ••• • •••• . : 235 

6 

SW846 6010C 11/22-11/25/10 L98L61AA 

Analysis Titne . . : 12 : 19 MS Run# ..•.... : 0326175 

SW846 6010C ll/22-11/29/10 L98L61AD 

Analysis Time . . : 14 : 08 ~s Run w . ... .. . : 0326175 

SW846 6010C 11/22-11/25/10 L98L61AC 

Analysis Time . . : 12:19 MS Run# ......• : 0326175 

of 14 
MB Lot-Saaple I: FOK220000-259 Prep Batch# ... : 0326259 

Strontium 1.6 B 5.0 ug/L SW846 6010C 

Thorium ND 

Uranium ND 

ROTB(S): 

Dilution Factor: 1 

Analysis Time .. : 12:47 

200 ug/L 

Dilution Factor: 1 

Analysis Time .. : 12:47 

500 ug/L 

Dilution Factor: 1 

Analysis Time .. : 10:42 

Calculltlons .,.. performed llefo,. rvundlng 10 avolll round-off errvn In celcullled resulls. 

B EstiiNIId mulL Rnullls less thin RL. 

COK180503 

SW846 6010C 

SW846 6010C 

7 

11/22-11/29/10 ~1AA 

11/22-11/29/10 MAEF31AD 

11/22-11/25/10 MAEF31AC 

of 14 
PARAMETER 

RECOVERY 

LIMITS 

;:..;M;;;;E.;;.TH;.;;O.;;.;D;;;._ _____ ANALYSIS DATE WORK ORDER # 

LCS Lot-Bamplel: FOK220000-259 Prep Batch 1 •.• : 0326259 

Strontium 103 (80 - 120) SW846 6010C 11/22-11/29/10 MAEF31AE 

Dilution Factor: 1 Analysis Ti~ .. : 12:53 

Uranium 102 (80 - 120) SW846 6010C 11/22-11/25/10 MAEF31AF 

Dilution Factor: 1 Analysis Time .. : 10:50 

Thorium 116 (80 - 120) SW846 6010C 11/22-11/29/10 MAEF31AG 

Dilution Factor: 1 Analysis Ti~e .. : 12:53 

ROTB(S): 

COK180503 8 of 14 
NS Lot-Sample 1: COK180474-001 Prep Batch# ..• : 0326259 

Strontium 24900 N (75 - 125) SW846 6010C 

35300 N (75 - 125) 7.6 (0-20) SW846 6010C 

Thorium 

Uranium 

NOTB(S): 

597 N 

555 N 

41 N 

55 N,* 

(75 -

(75 -

(75 -

(75 -

Dilution Factor: 500 

Analysis Time .. : 13:12 

MS Run 1 •. •.• •• : 0326175 

125) SW846 

125) 4.8 (0-20) SW846 

Dilution Factor: 50 

Analysis Time .. : 13:56 

MS Run II ••••••• : 0326175 

125) 

125) 28 (0-20) 

Dilution Pactor: 10 

Analysis Time.,: 12:04 

SW846 

SW846 

MS Run M . .. .. .. : 0326175 

C•lcullllklns 1re perfor,.d Wore rounding to IIVOicl rvund4ff ''""' In Clleullllld results. 

N Spiked .. ,_ .._.y is -• IWted conlrlll lillllts. 

• RelltiYt ..-- dllflnnce (RPO) Is OUISidt lllllld CMrDI limlll. • 

COK180503 9 

6010C 

6010C 

6010C 

6010C 

11/22-11/29/10 L98DQ1AF 

11/22-11/29/10 L98DQ1AG 

11/22-11/29/10 L98DQ1AK 

11/22-11/29/10 L98DQ1AL 

11/22-11/25/10 L98DQ1AH 

11/22-11/25/10 L98DQ1AJ 

of 14 
aeault: 

GROSS A/B BY GFPC SW846 9310 MOD 

Grose Alpha 

G~o•• Beta 

NOTB(S) 

80 

170 

QUal 

u 

Data are incomplete without tbe c••• narrative. 

MDC ia determined by inat~ent performance only. 

Bold result• are greater tban the MDC. 

Total 

IIDOert:. 

(2 rs+/·1 

uo 

7!1 

U Result is less than the aaaple detection limit. 

COK180503 

PritP 

RL lick: Date 

pCi/L Batch i 0326115 

3 220 11/22/10 

4 110 11/22/10 

10 

ualyah 

Data 

YlcS \ 

11/23/10 

11/23/10 

of 14 
Total 

Uacert. 

Par ... ter llaav1t Qllal (2 ,..,., 

GROSS A/B BY OFPC SWIU !1310 ICOD 

Grosa Alpha -0 . 63 u 0.41 

Groll& Beta 0.99 u 0.67 

MOTB(S) 

Data are incoaplete witbovt the caae narrative. 

MDC ie determined uaing instrument performance only sold reeulta are greater than the HOC, 

0 Reault ia lea& than the sample detection limit. 

COK180503 

pCi/L 

RL 

Batch 

3.00 

4.00 

11 

Le.b IU~Ple ID 

Prep AAalyah 

III)C Date U.te 

• 0326115 Yl6\ POJt:Z20000~115B 

1.1 11/22/10 11/23/10 

1.0 11/22/10 11/23/10 

of 14 
'l'ata1 LUI lulple m 

ODc•rt. QC Ccmtn1 Spika Aao\mt ltell\llt (2 rs+/-1 IG)C Par-ter ' T14 ' .. ., Lia!U 

GROSS A/8 BY GFPC SW846 9310 MOD pCi/L 9310 MOD l"Olt220000-115C 

Gross Alpha 49.4 53.4 5 . 9 1 . 2 108 (69 - 1281 

Gross Beta 66.8 66.3 5.7 1.1 99 (74 - 128) 

Batcll I• 0326115 Aaa1y•1• Date• 11/23/10 

NOTBCS) 

MDC 1• 4etar.Dine4 by in•truaent p•rformauce only Calculation• are performed before rounding to avoid round-off error in calculated re•ult• 

COK180503 12 of 14 
Par-tar Spike "-nnnt 

GROSS A/B BY GFPC SW846 9310 IIOD 

Gross Beta 26700 

Batch #: 

GROSS A/B BY GFPC SW846 9310 IIOD 

Gross Alpha 19800 

Batch #: 

ROTE (S) 

Spike 

Jlaault 

29900 

0326115 

.32400 

0326115 

Data are 1ncomplete w1thout the case narrative. 

Total Total 

'DIIcaz:t. SpUta 811115'1• thloart. 

(2o +/-) Yld. Ra•ult (2 0 +/-) 

pCi/L 9310 IIOD 

2500 3920 610 

And reb Date : 11/23/10 

pCi/L UlO JIOD 

3800 17800 2500 

Analysis Date: 11/23/10 

Calculations are performed before rounding to avoid round -off errors i n calculated results. 

COK180503 13 

oc eaple 

\YLI) \DC 

ID / 

QC Control 

Limita 

COitl80UO-OOl 

97 (54-150) 

C01tl80U0-001 

74 (35-150) 

of 14 
Par-car 

GROSS A/8 BY GPPC 

Gross Alpha 

Gross Beta 

NOTB(S) 

lAIII' .. 

Re•ult 

SWB46 9310 MOD 

17800 

:U20 

llatc:b I• 

Total 

Oneut. 

(2G •/-) 

2500 

no 

0326115 

D•ta are lnca.plete without the ca•• narrative. 

DVl'LlCAD 

\ Yld •••lllt 

pCi/L 9310 IIOD 

15600 

nto 

Total OC Suopla ID 

Vncert. 

(2 fl+/-) \ Yld Preci•lon 

CODB04S0-001 

2700 7 

680 20 

(Sample) 0326115 (Duplicate) 

Calculation• are perfo~d before roUDdiug to avoid round-off error lD calculated reaults 

COK180503 14 

UPD 

\RPD 

of 14 
each attached sheet as Form 26R, reference the Item number and Identify the date 

prepared. The date on attached sheets needs to match the date noted below. 

General Reference 287.54 

Date Prepared/Revised 2/24/11 

c. Physical Appearance 

Number of Solid or Liquid Phases of Separation 

Describe each phase of separation. --------------------l 

- 1 -
Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

c. Facility Contact Name 

Title 

Phone 

d. Volume of waste shipped to processing or 

785,025 0 cu yd gal 

Email Address 

.o lb 

a. waste permit 

WVR000521948 

processing or disposal facility being 

c. 

Address Line 1 

Address Line 1 Address City State ZIP 

Municipality 

(check one) 

Delaware 

d. Volume 

743,435 

waste shipped to processing or disposal facility In the previous year. 0 cu yd gal 0 lb 0 ton (check one) 

0 ton (check one) 

-2-
b. Facility Name 

c. 

d. 

a. 

c. 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Volume of waste shipped 

90,000 

Facility Name 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Email Address 

Energy 

Email Address 

D ton 

-2 -

georgem@shallenbergerconstruction.c 

om 

(check one} 

(check one} 
b. Facility Name 

c. 

d. 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

me of waste shipped to processing or 

Email Address 

facility in the previous year. 

4,200 D cu yd 181 gal D lb D ton (check one) 

a. Solid 

PA0095443 

b. Facility Name 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

c. Facility Contact Name 

Title 

Volume of waste 

echnologies 

Indiana 

D ton (check one) 

- 2 -
The area below (a.-c:l.) will accommodate the Identification of two facilities. Attach additional sheets If necessary. 

a. 

c. 

c. 

waste permit number(s) 

PA0095273 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Facility Name 

Title 

Phone 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Title 

Phone 

Name 

or disposal utilized. 

Indiana 

(check one) 

Tri County Waste Management 

Email Address 

D gal 0 ton (check one) 

- 2 -
The area below {a.-d.) will accommodate the Identification of two facilities. Attach additional sheets If necessary. 

a. Solid permit number{s} or a•&IIXJII'il' 

31-121-2-4037 

c. 

c. 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Tunnelton Liquids Company 

County 

karnold@triadhunter .com 

(check one) 

Email Address tlcbufalini@hotmail.com 

0 ton (check one) 

-2-
The area below (a.-d.) will accommodate the Identification of two facilities. Attach additional sheets If necessary. 

a. waste permit number(s) for processing or disposal 

47-085-05051 

Address Line 1 Address Line 1 Address City State ZIP 

Municipality 

c. Facility Contact Name 

Title 

County 

lty in the previous year. D lb D ton (check one) 

a. Solid waste permit number(s) for processing or 

9395 

Address Line 1 

Address Line 1 Address City State ZIP 

Municipality 

c. Facility Contact Name 

Title 

If "Yes", list the general permit number or approval number. 

Volume of waste beneficially used in the year. D cu yd D gal D lb 

-2-

Muskingum 

(check one) 

D ton (check one) 
Form Submitted: D Form26R 

0 Other (specify) 

Date Submitted: 

181 I certify the Information required In Section B-2, Chemical Analysis was supplied to the Department for the year 

2010 and has not changed. 

Form Submitted: 181 Form 26R 

0 Other (specify) 

Date Submitted: 

181 I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Department 

for the and has not changed. 

Form Submitted: 181 Form 26R 

0 Other (specify) 

Date Submitted: 

Name of Responsible Official Title Su erintendent Water Mana ement 

J. Michael Baran 

Date 2/24/2011 

- 3 -