MJn'IJOD BLAHK REPORT General Chemistry Client Lot
1 ...

: COK180501

MatrU: •••••••••

: WATER REPORTING :!:•REPARATION- PREP =-PARAME:.;:.:::..:..:=-T=-E=R:.;,_ ____ :..:RE=-5=-U:..:L::.:T=---._ **:L:::IM~I:...:T:___** .=UN::.:.I:..T:...:S:__ __ **:.:ME=TH::.O:..:D~-----** JINALYSIS DATE BATCH

# Nitrite as N ND Oil & Grease (HEM) ND Specific conductance
ND Su1fate Total Alkalinity Total Dissolved Solids Total. Recoverabl.e Phenolics Total Suspended Solids NOTB(S}:
0.22

B 2.3 B ND 0.0068

B ND Work Order #: MACXX1AA 0.050 mg/L Dilution Factor:

1 Analysis Time ..

: 14:34 Work Order #: MAALD1AA 5.0 mg/L Dilution Factor:

1 Analysis Time ..
: 10:35 Work Order #: MAK241AA 1.0 umhos/cm Dilution Factor:

1 Analysis Time ..

: 00:00 Work Order #: MACXL1AA 1.. 0 urg/L Dilution Factor:

1 Analysis Time ..

: 14:34 Work Order #: MANJJ1AA 5.0 urg/L Dilution Factor:

1 Analysis Time ..

: 00:00

MB Lot-Sample

#: COK200000-045 MCAWW 300.0A 11/18/10 MB Lot-Sample

#: COK190000-244 CFR136A 1664A HEM 11/19/10 MB Lot-Sample

#: COK290000-041 SM20 2510B 11/29/10 MB Lot-Sample

#: COK200000-043 MCAKW 300.0A 11/18/l.O MB Lot-Sample

#: COLOl0000-025 SM18 2320

B 12/02/10 0324045 0323244 0333041 0324043 0335025 Work Order #: MAAQV1AA

MB Lot-Sample

#: COK190000-271 10.0 mg/L Dilution Factor:

l Analysis Time .•

: 11:15 SM20 2540C 11/19-11/20/10 0323271 work Order #: MAGG01AA

MB Lot-Sample

#: COK230000-071 0.010 urg/L Dilution Factor:

1 Analysis Time ..

: 10:33 MCA1IW 420.4 11/23-11/24/10 0327071 Work Order #: MAAP91AA
MB Lot-Sample

#: C

· JK190000-267 4.0 mg/L Dilution Factor:

1 Analysis Time ..
: 06:15 SM20 2540D 1L/l9-11/20/10 0323267 Calculations
are performed before rounding

10 avoid round-off errors in calculated results. B Estimated result. Result
is less !han RL. COK180501

31

of 57LABORATORY CONTROL SAMPLB BVALUATIOB REPORT General Chemistry Lot-Sample

1 ...

: COK180501

Matrix •.•.....•

: WATER PARAMETER PERCENT RECOVERY Biochemical Oxygen Demand (BOD) Bromide Chloride Nitrate as N Nitrite as N Oil
& Grease Sulfate BOTB(S):
105 105 104 104 104 104 108 108 104 103 (HEM) 82 86 104 104 RECOVERY
RPD PREPARATIONLIMITS RPD LIMITS :..:MET=:.:.HO:;D:._ _____ ANALYSIS DATE PREP BATCH

# WO#:L99RA1AC-LCS/L99RA1AD-LCSD

LCS Lot-Sample#: COK190000-082 (85

- 115)
SM20 5210B (85

- 115) 0.24 (0-20) SM20 5210B 11/19-11/24/10 0323082 11/19-11/24/10 0323082 Dilution Factor:

1 Analysis Time ..

: 09: OS WO#:MACXR1AC-LCS/MACXR1AD-LCSD

LCS Lot-Sample#: COK200000-044 (90- 110) MCAWW 300.0A 11/18/:.o 0324044

. (90

- 110) 0.09 (0-20) MCAWW 300.0A 11/18/:

. 0 0324044 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MACXH1AC-LCS/MACXH1AD-LCSD

LCS Lot-Sample#: COK200000-040 (90

- 110) MCAWW 300. OA 11/18/:

. o 0324040 (90

- 110) 0.13 (0-20) MCAWW 300.0A 11/18/:.0 0324040 Dilution Factor

: 1 Analysis Time ..

: 14

: 13 WO#:MACXF1AC-LCS/MACXF1AD-LCSD

LCS Lot-Sample#: COK200000-039 (90- 110) MCAWWJOO.OA 11/18/:.0 0324039 (90- 110) 0.14 (0-20) MCAWW 300.0A 11/18/:.0 0324039 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MACXX1AC-LCS/MACXX1AD-LCSD

LCS Lot-Sample#: COK200000-045 (90

- 110) MCAWW 300. OA 11/18/:.0 0324045 (90

- 110) 0. 07 (0-20) MCAWW 300. OA 11/18/:.o 0324045 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MAALD1AC-LCS/MAALD1AD-LCSD

LCS Lot-Sample#: COK190000-244 (78

- 114) CFR136A 1664A HEM 11/19/:.0 0323244 (78

- 1H) 3.9 (0-18) CFRJ.36A 1664A HEM 11/1!:1/:.0 0323244 Dilution Factor:

1 Analysis Time ..

: 10:35 WO#:MACXLlAC-LCS/MACXLlAD-LCSD

LCS Lot-Sample#: COK200000-043 (90

- 110) MCAWW 300. OA 11/18/:.o 0324043 (90- 110) 0.17 (0-20) MCAWW 300.0A 11/18/:

. 0 0324043 **Dilut~n** Factor:

1 Analysis Time ..

: 14:13 C11CUiatlons lrt performecl before rouncling

10 1110id round-off emil'S in calcullled resuhs. COK180501

32

of 57LABORATORY COIITR.OL SAMPLE EVALUATION REPORT Client Lot ....

: COK180501 PERCENT PARAMETER RECOVERY pH

100 Acidity

99 Ammonia Nitrogen
92 Chemical Oxygen Demand (COD} Hardness, as CaC03 103 100 Specific Conductance 111 Total Alkalinity
91 Total Dissolved Solids
109 Total Recoverable Phenolics
100 COK180501

General Cb.emi.st:ry Matrix .•••...••

: WATER RECOVERY PREPARATION-
PREP LIMITS METHOD ANALYSIS j)ATE BATCH

# Work Order #: L985AlAA LCS Lot-Sample#: CoJK180000-329 (99

- 101} SM20 4500-H+B 11/18/10 0322329 Dilution Factor:

l Analysis Time ..
: 15:05 Work Order #: MAKRLlAC LCS Lot-Sample#: CI)K270000-042 (80

- 120) SM20 2310B (4a) ll./27 /10 0331042 Dilution Factor:

l Analysis Time ..
: 13:38 Work Order #: L999G1AC (90

- 110) MCAWW 350.1 LCS Lot-Sample#: COK190000-198 11/19-11/23/10 0323198 Dilution Factor:

1 Analysis Time ..

: 13:26 Work Order#: MAK8T1AC LCS Lot-Sample#: COK290000-068 (90

- 110) MCAWW 410.4 11/29/:

. o 0333068 Dilution Factor:

1 Analysis Time ..

: 13:14 Work Order #: MAKSOlAC LCS Lot-Sample#: C(IK290000-050 (90

- 110) SM2D 2340C 11/29/J.D 0333050 Dilution Factor:

1 Analysis Time ..
: 08:45 Work Order #: MAK241AC (80

- 120) SM20 251DB LCS Lot-Sample#: CCK290000-041 11/29/JO 0333041 Dilution Factor:

1 Analysis Time ..

: 00:00 Work Order #: MANJJ1AC (80

- 120) SM18 2320
B LCS Lot-Sample#: CCL010000-025 12/02/lO 0335025 Dilution Factor:

1 Analysis Time ..

: 00:00 Work Order #: MAAQV1AC LCS Lot-Sample#: COK190000-271 (80

- 120) SM20 2540C 11/19-11/20/10 0323271 Dilution Factor:

1 Analysis Time ..
: 11:15 Work Order #: MAGG01AC LCS Lot-Sample#: COK230000-071 (90

- 110} MCAWW 420.4 11/23-11/24/10 0327071 Dilution Factor:

1 Analysis Time ..
: 10

: 33 (Continued

on next page) 33

of 57LABORATORY CORTROL SAMPLE BVALtJAT.[QN' REPORT Genera1 Chemistry Client Lot

1 ...

: COK180501

Matrix .........

: WATER PERCENT RECOVERY PREPARATION-
PREP PARAMETER RECOVERY LIMITS **~ME~T~H~O~D___________** ANALYSIS DATE BATCH

# Total Suspended
Work Order #: MAAP91AC LCS Lot-Sample#:

C • )K190000-267 Solids

97
(80

- 120) SM20 25400 11/19-11/:20/10 0323267 Dilution Factor:

1 Analysis Time ..

: 06

: 15 ROTB(S): Calculatioos are performed before I'OWlding

10 avoid round-off errors in atk:ulalcd results. COK180501

34

of 57MATRIX SPIKE SAMPLE B'VALOATIOif REPORT Genera1 Chemistry Client Lot# ...

: COK180501

Matru: .••••.•••

: WATER Date **~led** ...

: 11/22/10 Date Received

••

: 11/22/10 PERCENT RECOVERY

RPD PREP.Al<ATION- PREP PARAMETER RECOVERY LIMITS RPD LIMITS **_ME~T~H~O~D** ___________ ANALY5IS DATE BATCH

# Ammonia Nitrogen

WO#: L96GV1A1-MS/L96GV1A2-MSD

MS **Lot-Sam~le**

#: COK170441-001 114 N . (90

- 110} 112 N (90

- 110) 1.4 (0-20) Dilution Factor:

1 Analysis Time

. . : 13:49 MCAWW 350.1 11/19-11/23/10 0323198 MCAWW 350.1 11/19-11/23/10 0323198 MS Run# .......

: 0323115 Chemical oxygen Demand (COD)

WO#: MAEP3lAH-MS/MAEP3LAJ-MSD

MS Lot-Sample

#: COK220467-001 92 100 (90

- 110) MCAWW 410.4 (90

- 110} 6.0 (0-20} MCAWW 410.4 Dilution Factor:

1 Analysis Time ..

: 13:17 MS Run# .....

. . : 0333032 11/29/10 11129no 0333068 0333068 Total Recoverable Phenolics

WO#: L98HL1AF-MS/L98HL1AG-MSD

MS Lot-Sample

#: COK180491-002 ROTB(S):
102 102 (90

- 110) MCAWW 420.4 (90

- 110} 0.19 (0-20} MCAWW 420.4 Dilution Factor:

1 Analysis Time ..

: 10:33 MS Run# ....

.
. . : 0327181 Calculalions are performed before rounding

to avoid round-ilff errors in calculaled results. N Spiked analyte recovery

is oullide stated COPITOllimits. COK180501

35 11/23-11/24/10 0327071 11/23-11/24/10 0327071 of 57

# Client Lot



# 1 ...

: COK180501 

# Date Sampled ...

: 11/18/10 

# DUPLICATE SAMPLE DUPLICATE BVALOATIOH REPORT 

# General Chemistry Work Order# ••.

: L979E-SMP L979E-DUP 

# Date Received

.•

: 11/18/10 

# Matrix .•••.••

: WATER RPD PREPARATION- PREP 

# PARAM RESULT **~R~ES~UL-=T~---** 

# UNITS Biochemical 

# Oxygen

RPD 

# LIMIT METHOD **l~YSIS** 

# DATE BATCH

# SD Lot-Sample



# #: COK180463-001 

# Demand (BOD) ND

ND 

# mg/L

0 Dilution Factor:

1 

# COK180501

{0-20) SM20 5210B Analysis Time ..

: 09:05 

# 11/19-11/24/10 0323082 MS Run Number
..
: 0323050 

# 36



# FEB 2 8 2011 DEP, SOUTHWEST 

# REGION OIL.& GAS

of 57Client Lot

1 ...

: COK180501 Date Sampled ••.

: 11/18/10 DUPLICATE PARAM RESULT RESULT Total Suspended Solids ND

ND COK180501
SAMPLB DOPLICATB EVALUATION REPORT Genera1 Chemistry Work Order

1 ...

: L990D-SMP L990D-DUP Date Received

••

: 11/19/10 Matrix ...••••

: WATER RPD PREPARATION- PREP UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH

# SD Lot-Sample

#: COK19042l-001 mg/L 0.0 (0-20) SM20 25400 11/19-11/20/10 0323267 Dilution Factor:

1 Analysis Time .•

: 06:15
MS Run Number
..

: 0323145 37

of 57Client Lot ••••

: COK18050l Date sampled •.•

: 11/16/10 DUPLICATE PARAM RESULT RESULT Total Dissolved Solids 259
215 COK180501
SAMPLE DUPLICATE BVALUM."IOIIJ REPORT General Chemistry Work Order

1 ...

: L9642-SMP L9642-DUP Date Received

..

: 11/17/10 Matrix .•..•••

: WATER RPD

" PREPARATION- PREP UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH

# SD Lot-Sample

#: COK170523-001 mg/L
19 (0-20) SM20 2540C 11/19-11/20/10 0323271 Dilution Factor:

1 Analysis Time

. . : 11:15
MS Run Number

. . : 0323149 38

of 57C1ient Lot

1 ..•

: COK180501 Date Samp1ed •••

: 11/17/10 DUPLICATE PARAM RESULT RESULT **~cidity** ND

ND COK180501
SAMPLE DUPLiCATE EVALUATION REPORT General Chemistry Work Order# ••.

: L98XT-SMP L98XT-DUP Date Received

•.

: 11/18/10 Matri::t ••.••••

: WATER RPD PREPARATIONUNITS RPD LIMIT METHOD ANALYSIS DATE SD Lot-Sample

#: COK1805.29-003 mg/L

0 (0-.20) SM20 2310B (4a) 11/27/10 Dilution Factor:

1 Analysis Time •.

: 13:38
MS Run Number

. . : 39

PREP BATCH

# 033104.2 0331019 of 57Client Lot# .••

: COK180501 Date Sampled •••

: 11/19/10 DUPLICATE PARAM RESULT RESULT Acidity ND

ND COK180501
SAMPLE DUPLICATE BVALOATIOB REPORT General Chemistry Work Order

1 ...

: MAEPJ-SMP MAEPJ-DUP Date Received

••

: 11/20/10 Matrix ....•..

: WATER RPD :?REPARATIONUNITS RPD LIMIT METHOD ;:WALYSIS DATE SD Lot-Sample

#: COK220465-001 mg/L

0 (0-20) SM20 23108 {4a) 11/27/10 Dilution Factor:

1 Analysis Time ..

: 13:38

MS Run Number
..

: 40

PREP BATCH

# 0331042 0331019 of 57C1ientLot1...:COK180501DateSamp1ed...:11/16/10DUPLICATEPARAMRESULTRESULTSpecificConductance523 528COK180501SAMPLEDOPL:ICATEEVALUATIOBREPORTGeneralChemistryWorkOrder#•••:L95MM-SMPL95MM-DUPDateReceived..:11/16/10Matrix.......:WATERRPD:?REPARATIONUNITSRPDLIMITMETHODANALYSISDATESDLot-Sample#:C•JK160529-001umhos/cm0.95(0-20)SM202510B11/29/10DilutionFactor:1AnalysisTime..:oo:ooMSRunNumber•.:41PREPBATCH#03330410333014of57Client Lot

t ...

: COK180501 Date Sampled ...

: 11/03/10 DUPLICATE PARAM RESULT RESULT Hardness, as CaC03 200 200 COK180501
SAMPLE DUPLICATE EVALUAT:IOH REPORT Genera1 Chemistry Work Order

I ...

: L9H9D-SMP L9H9D-DUP Date Received

..
: 11/04/10 Matrix .......

: WATER RPD !?REPARATION- PREP UNITS RPD LIMIT METHOD i\NALYSIS DATE BATCH

# SD Lot-Sample

#: COK04043l-004 mg/L 0.0 (0-20) SM20 2340C :Ll/29/10 0333050 Dilution Factor:
10 Analysis Time ..

: 08:45

)IS Run Number
..

: 0333025 42

of 57Client Lot

1 ...

: COK180501 Date Sampled ..•

: 11/17/10 DUPLICATE PARAM RESULT RESULT Hardness, as CaC03 36000 35000 pH 6.6
6.6 COK180501
SAMPLE DOPLICATB BVALtlATIOlf REPORT General Chemistry Work Order

1 ...

: L97SG-SMP L975G-DUP Date Received

••

: 11/17/10 Matrix •..••••

: WATER RPD PREPARATION- PREP UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH

# SD Lot-Sample

#: ::OK180438-001 mg/L 2.8 (0-20) SM20 2340C 11/29/10 0333050 Dilution Factor: 500 Analysis Time .•

: 08:45
MS RWl Number
..

: 0333025 SD Lot-Sample

#: <::OK180438 -001 0.0 (0-2.0) SM20 4500-H+B 11/18/10 0322329 Dilution Factor:

1 Analysis Time ..
: 15:07
MS RWl Num:ber
.•

: 0322185 43

of 57SAMPLE DUPLl:CATB KVALUATIOH REPORT General Chemistry Client Lot# ...

: COK180S01 Work Order

t ...

: L98HC-SMP L98HC-DUP Date Received

..
: 11/17/10 Matrix .......

: WATER Date Sampled ...

: 11/17/10 DUPLICATE

RPD PREPARATION- PREP PARAM RESULT RESULT UNITS RPD LIMIT METHOD **.~ALYSIS** DATE BATCH

# Total Alkalinity

SD Lot-Sample

#: CJK180490-00l 103

J 103 mg/L 0.068 (0-20) SM18 2320
B 12/02/10 0335025 Dilution Factor:

1 Analysis Time .•

: 00:00
MS Run Nulllber

. . : 0336085 NOTB'(S): Calculations are performed before roundiniiO avoid round-off arors in calculaud results. J Medtocl blauk conwnination. The aSIIOCillred method blaDit contains lhe larget analyte at a reponable level

. COK180501

44

of 57::::TestAmericaAnalyticalReportSDGNumber:COK180501ProjectDescription(s)EquitableProductionCompanyEquitableProductionCompanyFor:ChrisKovitchTestAmericaPittsburgh301AlphaDrive;RIDCParkPittsburgh,PA15238MelissaDeyoForSallyHoffmanProjectManagermelissa.deyo@testamericainc.comTuesday,November30,2010ThetestresultsinthisreportmeetallNELAPrequirementsforanalytesforwhichaccreditationisrequiredoravailable.AnyexceptiontoNELAPrequirementsarenotedinthisreport.PersuanttoNELAP,thisreportmaynotbereproduced,exceptinfull,withoutthewrittenapprovalofthelaboratory.AllquestionsregardingthistestreportshouldbedirectedtotheTestAmericaProjectmanagerwhohassignedthisreport.COK18050145::of57TestAmericaTestAmericaPittsburghSDGNumber:COK180501Received:11/19/10-11/23/10301AlphaDrive;RIDCPar1<Pittsburgh,PA15238Reported:11/30/1008:43Project:EquitableProductionCompanyProjectNumber:COK180501TestAmericaBuffaloCurrentCertificationsAsof08/16/2010STATEProgramCert#ILab/DArkansasCWA,RCRA,SOIL88-0686California*NELAPCWA,RCRA01169CAConnecticutSDWA,CWA,RCRA,SOILPH-0568Florida*NELAPCWA,RCRAE87672Georgia*SDWA,NELAPCWA,RCRA956Illinois*NELAPSDWA,CWA,RCRA200003IowaSWIGS374Kansas*NELAPSDWA,CWA,RCRAE-10187KentuckySDWA90029KentuckyUSTUST30Louisiana*NELAPCWA,RCRA2031MaineSDWA,CWANY0044MarylandSDWA294MassachusettsSDWA,CWAM-NY044MichiganSDWA9937MinnesotaSDWA,CWA,RCRA036-999-337NewHampshire*NELAPSDWA,CWA233701NewJersey*NELAP,SDWA,CWA,RCRA,NY455NewYork*NELAP,AIR,SDWA,CWA,RCRA·10026NorthDakotaCWA,RCRAR-176OklahomaCWA,RCRA9421Oregon*CWA,RCRANY200003Pennsylvania*NELAPCWA,RCRA68-00281TennesseeSDWA02970Texas*NELAPCWA,RCRAT104704412-08-TXUSDAFOREIGNSOILPERMITVirginiaSDWAWashington*NELAPCWA,RCRAWisconsinCWA,RCRAWestVirginiaCWA,RCRA*Asrequiredundertheindicatedaccreditation,thetestresultsi1thisreportmeetallNELAPrequrementsforparametersforwhichaccreditationisrequiredoravaiable.AnyexceptionstoNELAPrequirementsarenotedinthisreport.TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comS-41579278C1677998310390252COK18050146Page2of1.1of57

# TestAmerica 1HE- U!AQtt IN 91\'JAI)NMENtiiL

f £STING TestAmerica Pittsburgh

SDG Number

: COK180501

Received: 11/19/10-11/23/10 301 Alpha Drive; RIDC Park Pittsburgh

, PA 15238

Reported: 11/30/10 08

: 43 Project: Equitable Production Company Project Number: COK180501 CASE NARRATIVE According

to 40CFR Part 136.3, pH, Chlorine Residual, Dissolved Oxygen, Sulfite, and Temperature analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e

. g. field-pH)

, they were not analyzed immediately, but as soon as possible after laboratory receipt. I certify that this data package

is in compliance with the terms and conditions
of the contract, both technically and for completeness,

for other than the conditions detailed within the body of this report. Release
of the data contained

in this sample data package and in the electronic data deliverables has been authorized
by the Laboratory Manager
or his/her designee,
as verified by the following signature. Melissa Deyo For Sally Hoffman Project Manager Tuesday, November 30,2010 There are pertinent documents appended
to this report,

2 pages, are included and are an integral part of this report. Reproduction

of this analytical report
is permitted only in Its entirety. This report shall not be reproduced except
in full without the written approval
of the laboratory. TestAmerica Laboratories,
Inc

. certifies that the analytical results contained herein apply only to the samples tested as received by our Laboratory

. TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www

. testamericainc.com 

### COK180501

47

Page
3 of t.1 of 

### 57Test America TestAmerica Pittsburgh 301 Alpha Drive; RIDC Par1< Pittsburgh, PA 15238

SDG Number

: COK180501 Project: Equitable Production Company Project Number: COK180501 DATA QUALIFIERS AND DEFINITIONS DOS Dilution required due to high concentration

of target analyte(s) D10 Dilution required due to sample color H3 Sample was received and analyzed past holding time.

Received: Reported: 11/19/10-11/23/10 11/30/10 08:43 Z3 The sample required

a dilution, the surrogate spike concentration

in the sample are reduced
to a level where the recovery calculation does not provide useful information

. NR Any inclusion
of NR indicates that the project specific requirements

do not require reporting estimated values below the laboratory reporting limit. TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600
fax 716-691-7991 www.testamericainc.com COK180501

48

Page
4 of 1..1 of 57TestAmeri•caTestAmericaPittsburgh301AlphaDrive;RIDCParkPittsburgh,PA15238SampleDataSDGNumber:COK180501Project:EquitableProductionCompanyProjectNumber:COK180501ExecutiveSummary-DetectionsOilAnalyteResultQualifiersRLMDLUnitsFacDateAnalyzedClient10:HURDDRILLPIT-590398(RTK1396..01-Water)Sampled:11/17/1011:30GeneralChemlstrvParametersReceived:11/19/10-11/23/10Reported:11/30/1008:43LabTechBatchMethodRecvd:11/19/1009:00TotalKjeldahlNitrogen34.30082.001.50mg/L10.011/24/1014:08JME10K2404351.2TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comCOK18050149Page5of1..1of57TestAmericaTestAmericaPittsburgh301AlphaDrive;RIDCParkPittsburgh,PA15238SampleIdentificationHURDDRILLPIT-590398HURDDRILLPIT-590398SDGNumber:COK180501Project:EquitableProductionCompanyProjectNumber:COK180501LabNumberRTK1396-01RTK1536-01SampleSummaryClientMatrixWaterWaterDate/TimeSampled11/17/1011:3011/17/1011:30TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comCOK18050150Received:11/19/10-11/23/10Reported:11/30/1008:43Date/TimeReceived11119/1009:0011/23/1009:15SampleQualifiersPage6of1..1of57TestAmericaTestAmericaPittsburgh301AlphaDrive;RIDCParkPittsburgh,PA15238SampleDataSDGNumber:COK180501Project:EquitableProductionCompanyProjectNumber:COK180501AnalyticalReportAnalyteResultQualifiersRLMDLUnitsDllFacDateAnalyzedClientID:HURDDRILLPIT-590398(RTK1396-01-Water)Sampled:11/17/1011:30GeneralChemistrvParametersReceived:11/19/10-11/23/10Reported:11/30/1008:43LabTechBatchMethodRecvd:11/19/1009:00MethyleneBlueActiveNOH30.02500.0130mg/L1.0011/19/1016:30JFR10K20675540CSubstancesTotalKjeldahlNitrogen34.30082.001.50mg/L10.011/24/1014:08JME10K2404351.2TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comCOK18050151Page7of1...1ot57TestAmerica TestAmerica Pittsburgh 301 Alpha Drive; RIDC Park Pittsburgh, PA 15238 Sample Data SDG Number: COK180501 Project: Equitable Production Company Project Number: COK180501 Analytical Report Analyte
Result Qualifiers

RL MDL Units
Dll Date Fac Analyzed Client ID: HURD DRILL PIT -590398 (RTK1536-01 -Water) Sampled: 11/17/1011:30 Non-Halogenated Volatile Organics

Received

: Reported: Lab 11/19/10-11/23/10 11/30/10 08

: 43 Tech Batch Method Recvd: 11/23/10 09:15 Ethylene Glycol

NO 010 1000 NR mg!L 100 11/24/10 20

: 15 GFD 10K2446 8015 1,4-Butanedio/
303% D10,Z3 Surr Limits: (66-130016)
11124/10 20:15 GFD 10K2446 8015 TestAmerica Buffalo-
10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600
fax 716-691-7991 www

. testamericainc.com COK180501

52

Page
8 of L1 of 57TestAmerica"'HELEADS!INeJl\'IA.OMNI!N'IliLTestAmericaPittsburghSDGNumber:COK180501301AlphaDrive;RIDCPari<:Pittsburgh,PA15238Project:EquitableProductionCompanyProjectNumber:COK180501SAMPLEEXTRACTIONDATAWWolExtractParameterBatchLabNumberExtracteUnitsVolumeUnitsDatePreparedGeneralChemistryParameters351.210K2404RTK1396-0125.00mL25.00mL11/23/1010:205540C10K2067RTK1396-01400.00mL400.00mL11/19/1016:30SAMPLEEXTRACTIONDATAWWolExtractParameterBatchLabNumberExtracteUnitsVolumeUnitsDatePreparedNon-HalogenatedVolatileOrganics801510K2446RTK1536-010.50mL1.00mL11/24/1006:26TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comCOK18050153LabTechJMEJFRLabTechGFDReceived:11/19/10-11/23/10Reported:11/30/1008:43ExtractionMethodTKNDigestionMBASExtractionMethod8015GlycolsPage9of1.1ot57Test America TestAmerica Pittsburgh

SDG Number: COK180501

Received: 1111911 0-11 12311
0 301 Alpha Drive: RIDC Par11:

Reported: 11130110 08:43 Pittsburgh, PA 15238

Project: Equitable Production Company Project Number: COK180501 LABORATORY
QC DATA Source Spike

% % REC % RPD Data Analyte
Result Level
RL MDL Units Result REC Limits RPD Limit Qualifiers Non-Halogenated Volatile Organics Blank Analyzed: 11/24/10 (Lab Number:10K2446-BLK1, Batch: 101<2446) Ethylene Glycol

10
NR mgfl
NO Surrogate: 1,4-Butanedio/

mg!L LCS Analyzed: 11/24/10 (Lab Number:10K2446-BS1, Batch: 101<2446) Ethylene Glycol

20.0

10
NR mg/L 19.8 Surrogate:

1, 4-Butanediol

mg!L TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel 716-691-2600
fax 716-691-7991 www

. testamericainc.com COK180501

54

109 99 109 66-130 50-150 66-130 Page

1 0 off11 0 57TestAmericalHSLEJIOEfiiNENVIRONMENtALil;:$l1NGTestAmericaPittsburghSDGNumber:COK180501301AlphaDrive;RIDCParkPittsburgh,PA15238Project:EquitableProductionCompanyProjectNumber:COK180501LABORATORYQCDATAAnalyteSourceResultGeneralChemistryParametersSpikeLevelRLMDLBlankAnalyzed:11/19/10(LabNumber:10K2067-BLK1,Batch:101<2067)MethyleneBlueActiveSubstances0.02500.0130LCSAnalyzed:11/19/10(LabNumber:10K2067-BS1,Batch:101<2067)MethyleneBlueActiveSubstances0.4000.02500.0130Unitsmg/Lmg/LMatrixSpikeAnalyzed:11/19/10(LabNumber:10K2067-MS1,Batch:101<2067)QCSourceSample:RTK1391H11MethyleneBlueActiveSubstancesNDGeneralChemistryParameters0.1000.02500.0130BlankAnalyzed:11/24/10(LabNumber:10K2404-BLK1,Batch:101<2404)TotalKjeldahlNitrogen0.200.15LCSAnalyzed:11/24/10(LabNumber:10K2404-BS1,Batch:101<2404)TotalKjeldahlNitrogen2.500.200.15mg/Lmg/Lmg/L%ResultRECNO0.380950.105105ND2.4698TestAmericaBuffalo-10HazelwoodDriveAmherst,NY14228tel716-691-2600fax716-691-7991www.testamericainc.comCOK18050155Received:11/19/10-11/23/10Reported:11/30/1008:43%REC%RPDDataLimitsRPDLimitQualifiers90-11079-11790-110Page11off11057

# • 

# lll~f~~~~~~~~~IIJI **Jlr!~ll C0~1B0501**  

## INTER-COMPANY CHAIN OF CUSTODY COMMENTS: Prqec\ **M;ana~B"r:** Chris l(ovitcl• Prqec.t;
Form25R Report

, Type;

B1 Std Rep· CO only Cliant: 1424975. **Equitabl~** Pradur:tion Co. WORK·LOCA TION:

WS ADDRESS: .2.960 Faster CreighiDil Oriwe 

### ·I **Nastwi~**

TN 37:.!04

Date Received: Anat:(tica1 D11e Date: Report Du111 Date: 2010-11·17 2010-11-2111 2010.11·29 CLIENT ID: HURD DRILL PIT·59D3gll DATE/TIME SAMPLED; 20101117 1130 MATRIX:

I WATER j

- SAMP:._:; COMMENT **~:i;iTHQD:**

Zll IliON: NONE WATER. 351.2 TJ!;N TA. Na•hvllht EXTRACTION;

8.!1 NO SAMP!.!: PREPARATION PSRFORMED

I QC IV;;>E; 01 STANDARD TEST SET WOFU<OBQER LQSK11.t,O

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## zo NONE NONE WATER, 415.1 MBAS T,t.. **~shville** 

### EXIRJ\C:D!Z:!:

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I OC 

### T"YFS·
01 STA.N!)AR:J TEST SET WORKORDER L981<\ 1A1

**~** XX rhe sample(s}
lis led on this 

### form tue being senllo your location for the specified anelysis.

If you have any (!Uesuons, please contact Lhe **Projsc:~** Mar1agerlisled **Olb~;Jve.** PLEASE RETURN **T:~E** ORIGINA!. SIGNED FORM WITH THE REPOrtT AT THE COMPLETION
OF ANALYSIS. Thank You TestAmerir:a Pittsburgh **~ampfe** Receilo'ing

pr\ntect on: **Thnl"!i~l6** N•Jvcmber

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,,., rER-COMPANY CHAIN OF CUSTODY COIIII'MENTS: **Pro)~** M;arrager: Qlns Kowch **ProJ~:**

Form .2'6R Report **T~**

B1 std **~-** C

; ) **o~**

O&le Received: Arlalytlcal Due Date: Repar'! Du1 Da111

· .2010.11·17 7ZCIIO.H·29 2010-11-20 CliSit

I 14249'1'5

• Equl\abk· PmdueliGrl Ca. WORK LOCA710N;

IJ ADORESS:

10 Haelwoad Dr;W! • Amhe'st

NY 1-4228 **SM~**

' 1 I CI..I&.NT 10: liURD DRI;.L. PrT·90lt8 S.o.MPLE COr.AMENT

t.i!A'rRI)(

I EXTBACIIPN:

Be lifO SN.WLE PREPARATION **PERF=~MED**

I CC **TYP~;** 01 STANOARO TEST SET WATI;;R J ME!HOO:

%D NO,.E HONE. WA.TER,I01S l!.th.-fene **Gt-,~t** TA Bllffab **WORKOR~B** t98K11A2

**~** XX The !H.'ft'lp\e(s) listed on Ulis form are be"ng sent to your locallon fCJt the spec! (jed analysis. **If~** haw any queslioJ

&, plea sa Contact the Project Manager listed above. PlEASE RETURN n-tE ORIGINAL SIGNED FORM WrTH THE REPOR'" AT THE COMPlETION
OF ANALYSIS. 1: Tnank Vou • TestAmerica Pittsburgh Sample Receiving • RELINQUISHED
BV: **---+--~"5oo"'::.o-~~;;..,;t....._** _____ **DATE:_......_._f-~--** le:sW!Ierit'.o!l **Pittsbu~h** COK180501 :>'¥-____..,;;;....;lO;;=-rf-------

DATE:
TIME: **b~l,tl** d'iljprinled on: ThuP.Id:av, Ho..-nber 18, 4'010 01:28PM 57

**Pa~e**

1 of 57Test America THE LEADER
IN ENVIRONMENTAL TESTING ANALYTICAL REPORT Fonn 26R Lot #: COK180490 Maryamla Babich Equitable Production Co. 225 North Shore D.ri ve Pittsburgh,

PA 15212-5861 TESTAMERICA LABORAT·:lRIES, INC. Christi:c;:

M., KO\"'itch Proj
**~** ;': **Ma~** December

6, 2010 TestAmerlca Laboratories, Inc. 301 Alpha Drive Pittsburgh,
PA 15238 tel412.963.7058 fax412.963.2468 www.testamericalnc.com COK180490

1

of 57- .

. .
,. .

. **~** (.) 0 <

;
: **~** '1

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,- '. NELAC REPORTING: At the time of analysis the laboratory was in compliance with the current NELAC standards and held accreditation
for all analyses performed unless noted by a qualifier. The labs accreditation numbers are listed below. The format and contents
of the report meets all applicable NELAC standards except as noted
in the narrative and shall not be reproduced except
in full, without the written approval
of the laboratory

. The table below presents

a summary
of the certifications held by TestAmerica Pittsburgh. Our primary accreditation authority for the Non-potable water and Solid & Hazardous waste programs

is Pennsylvania DEP. A more detailed parameter
list is available upon request. Please ask your project manager for this information when required.

TestAmerlca X f-

· ----Califomia- NELAC Connecticut

-

- ww

X HW

X ww

X HW

X ww

X HW

X ww

X **~-------~N~ort~h-C~a-ro~l i-n-a·---------+**  **---- ~(#4~34~~)·------,------~~~-----~-·-----~~----** 

**--­ r--**  **----~P-e-nn-s-~~va--n~ia---N~E=L~A~C------**

**+---- -(~#0~2~~-04~~1~6~)---~-------~~-----** 

**-~ -------~-------**  HW

X ww

X 1- -----south caio-=l,....in_a _____

. __ **+- --(:-:-:#8""'oo=-:1-:4o~o:::-::2"')**  _____ **----~:.,- -----** 

**-i t------·---':-:------**  HW

X ww

X **--------~~-~~~~--**

**-- --**  **--- ----<S-T**  **~L~P)~-----~-----~~~--**

**-- -------~--**  **---** Utah- NELAC

HW ww HW

-- ww r- -------West_Vi_rg-in-ia -----

-- -· ---=-(#::-1'"4"c=:-2:-) ----+---

· - ---, **------- ---~w~,~--n-si~n----------** 
**;----~**

**99 ~80~2~7~8~00~**  **---+------~~~~------**
HW The codes utilized for program types are described below: HW Hazardous Waste certification VlfN Non-potable Water and/or Wastewater certification

X X X X **-----~- -----**  X X Laboratory has some form of certification under the specific program

. Many states certify laboratories
for specific parameters

or tests within
a category. The Information

In the table Indicates the lab is certified

In a general category
of testing. Please contact the laboratory

if parameter speclflc certification information

is required. Updated

: 0.5/19/10 N:\Reporting\NELAC NARRATIVE Pttsburgh_Updated 051910.doc COK180490

2

of 57Sample Receiving: CASE NARRATIVE Equitable Production Company Lot# COK180490 TestAmerica's Pittsburgh laboratory received samples on November
17, 2010. The coolers were received within the proper temperature range. GC/MS Volatiles: There were no problems associated with the analysis. Metals: The total and dissolved sample was analyzed

at a dilution for the ICP analytes, due to over range analytes and matrix interference. The total method blank had aluminum detected
at a concentration between the MDL and the reporting limit. The result was flagged with
a "B" qualifier. Any sample associated with
a method blank that had the same analyte detected had the result flagged with
a "J" qualifier. General Chemistry: The test for pH is a field parameter. The laboratory pH analysis was completed

at the request of the client. The sample was analyzed
at a dilution for various parameters. Results flagged with
a "G" qualifier indicate dilution due to matrix interference. The method blanks had analytes detected
at concentrations between the MDL and the reporting limit. The results were flagged with
a "B" qualifier. Any sample associated with
a method blank that had the same analyte detected had the result flagged with
a "J" qualifier. 8015: TestArnerica's Buffalo laboratory performed the 8015 analysis. Their report is included. TKNIMBAS: TestArnerica's Nashville laboratory performed the MBAS and TKN analyses. Their report is included. COK180490

3

of 57

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# Chain of Custody Record TettA...tca 

# Laboratorylo<atln: __________________________________ _ Rep
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# p........... c::J D'lll 

# CJ NPDES 

# c:::J RCRA 

# CJ Ol1ler ---------- 

# Test America

TH£ l-IN

**E~loi&MTAL** 

# TUTINO



# MoDIIoa SaiQio 

# Speclllc N- I s,odlll ........



# TAL 0018- t 

# (04110)METHODSSUMMARYPARAMETERpH(Electrometric)Acidity(Titrimetric)2310B(4a)Alkalinity,TotalBiochemicalOxygenDemand5210BBromideChemicalOxygenDemandChlorideConductivity2510BHARDNESS,TOTALCOK180490MercuryinLiquidWaste(ManualCold-Vapor)N-HexaneExtractableMaterial(1664A)NitrateasNNitriteasNNitrogen,AmmoniaSulfateTotalDissolvedSolidsSM2540C(SM20)TotalPhenolics420.4TotalSuspendedSolidsSM2540DTraceInductivelyCoupledPlasma(ICP)MetalsTraceInductivelyCoupledPlasma(ICP)MetalsVolatileOrganicsbyGC/MSReferences:ANALYTICALMETHODSM204500-H+BSM202310B(4a)SM182320BSM2052lOBMCAWW300.0AMCAWW410.4MCAWW300.OASM202510BSM202340CSW8467470ACFR136A1664AHMCAWW300.0AMCAWW300.0AMCAWW350.1MCAWW300.0ASM202540CMCAWW420.4SM202540DSW8466010BSW8466010BSW8468260BCFR136A"MethodsforOrganicChemicalAnalysisofMunicipalandIndustrialWastewater",40CFR,Part136,AppendixA,October26,1984andsubsequentrevisions.MCAWW"MethodsforChemicalAnalysisofWaterandWastes",EPA-600/4-79-020,March1983andsubsequentrevisions.SM18"StandardMethodsfortheExaminationofWaterandWastewater",18thEdition,1992.SM20"STANDARDMETHODSFORTHEEXAMINATIONOFWATERANDWASTEWATER",20THEDITION."PREPARATIONMETHODSM204500-HBSM182320BSM2052lOBMCAWW300.0AMCAWW410.4MCAWW300.OASM202510BSM202340CSW8467470AEPA1664AMCAWW300.0AMCAWW300.OAMCAWW350.1MCAWW300.0ASM202540CSM202540DSW8463005ASW8463010ASW8465030BSW846"TestMethodsforEvaluatingSolidWaste,Physical/ChemicalMethods",ThirdEdition,November1986anditsupdates.COK1804905of57SAMPLE SUMMAR.Y WO # SAMPLE# CLIENT SAMPLE ID L98HC L98MC NOTE (S): 001 002 HURD FLOW BACK-590398 TRIP BLANK COK180490 - The analytical results of the samples listed above are presented
on the following pages. - All calculations are performed before rounding
to avoid round-off errors In calculated results

. - Results noted as "ND" were not detected
at or above the stated limit. - This report must not be reproduced, except
In full, without the written approval of the laboratory

. -Results for the following parameters are never reported on a dry weight basis: color, corroslvity, density, flashpolnt. lgnltability, layers

, odor. paint filter test, pH, porosity pn!S$Ure, reactivity, redox potential, specific gravity, spot tests

, solids, solubility, temperature, viscosity, and weight

. COK180490

6
SAMPLED SAMP DATE TIME 11/17/10 11:30 11/17/10 of 57

# Equitable Production Co. Client Sample ID: HURD FLOW BACK-590398 Lot-Sample



# t ...

: COK180490-001 Date Sampled ...

: 11/17/10 Prep Date ......

: 11/30/10 Prep Batch



# t ...

: 0334067 Dilution Factor:

1 

# PARAMETER Benzene Toluene SURROGATE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 

# COK180490

GC/MS Volatiles Work Order



# t ...

: L98HC1AA Date Received

..
: 11/17/10 Analysis Date ..
: 11/30/10 Analysis Time ..
: 10:58 Method .........

: SW846 8260B REPORTING RESULT LIMIT ND

5.0 ND

5

. 0 PERCENT RECOVERY RECOVERY LIMITS 93

(62



# - 123) 108

(80



# - 120) 95

(75



# - 120) 101

(80



# - 120) 

# 7 Matrix .........

: WATER MS Runt .......

: UNITS MDL ug/L 0.99 ug/L 0.85



# of 57EquitableProductionCo.ClientSampleID:TRIPBLANKGC/MSVolatilesLot-Samplef...:COK180490-002WorkOrderf...:L98MC1AAMatrix.........:WATERDateSampled...:11/17/10DateReceived.. :11/17/10MSRunf.......:PrepDate......:11/30/10AnalysisDate..:11/30/10PrepBatchf...:0334067AnalysisTime..:07:28DilutionFactor:1Method.........:SW8468260BREPORTINGPARAMETERRESULTLIMITUNITSMDLBenzeneND5.0ug/L0.99TolueneND5.0ug/L0.85PERCENTRECOVERYSURROGATERECOVERYLIMITS1,2-Dichloroethane-d496(62-123)Toluene-d8113(80-120)4-Brornofluorobenzene99(75-120)Dibrornofluorornethane106(80-120)COK1804908of57Client Lot

f ...

: COK180490 MB Lot-Sample

1: COK300000-067 Analysis Date ..

: 11/30/10 Dilution Factor:

1 PARAMETER Benzene Toluene SURROGATE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane NOTE(S):

METHOD BLANK REPORT GC/MS Volatiles Work Order# •.•

: MAMC41AA Prep Date .••

• ••

: 11/30/10 Prep Batch# •••

: 0334067 REPORTING RESULT LIMIT ND

5.0 ND

5.0 PERCENT RECOVERY RECOVERY LIMITS 94

(62

- 123) 108

(80

- 120) 93

(75

- 120) 102

(80

- 120) Calculations
are performed before rounding

to avoid round-off errors In calculated results

. COK180490

9 Matrix .••.•••••

: WATER Analysis Time ••

: 06:20 UNITS METHOD ug/L SW846 8260B ug/L SW846 8260B

of 57LABORATORYCONTROLSAMPLEEVALUATIONREPORTGC/MSVolatilesClientLotf•••:COK180490WorkOrderf..•:MAMC41AC-LCSMAMC41AD-LCSDAnalysisDate••:11/30/10AnalysisTime..:07:51Matrix••••.••••:WATERLCSLot-Samplef:COK300000-067PrepDate••••••:11/30/10PrepBatchf•••:0334067DilutionFactor:1PARAMETER1,1-DichloroetheneTrichloroetheneChlorobenzeneBenzeneTolueneSURROGATE1,2-Dichloroethane-d4Toluene-dB4-BromofluorobenzeneDibromofluoromethaneNOTE(S):PERCENTRECOVERY929810110311011597101107110Calculationsareperformedbeforeroundingtoavoidround-offerrorsincalculatedresults.BoldprintdenotescontrolparametersCOK180490RECOVERYRPDLIMITSRPDLIMITSMETHOD(69-127)SW8468260B(69-127)6.6(0-20)SW8468260B(80-120)SW8468260B(80-120)2.6(0-20)SW8468260B(83-120)SW8468260B(83-120)3.8(0-20)SW8468260B(80-120)SW8468260B(80-120)3.9(0-20)SW8468260B(80-124)SW8468260B(80-124)2.8(0-20)SW8468260BPERCENTRECOVERYRECOVERYLIMITS88(62-123)87(62-123)104(80-120)102(80-120)92(75-120)91(75-120)97(80-120)97(80-120)10of57EquitableProductionCo.ClientSampleID:HURDFLOWBACK-590398TOTALMetalsLot-Samplet...:COK180490-001Matrix.......:WATERDateSampled...:11/17/10DateReceived..:11/17/10REPORTINGPREPARATION-WORKPARAMETER;:...:RE=S-=-U;:...:L::.cT=-------=.U::..:.N=IT::..:S:..____:.:M.:::E..::.T=H-=-O=D_____ANALYSISDATEORDER4tPrepBatcht...:0327129SilverNDAluminum297B,JArsenicNDBarium9920BerylliumNDBoron1510BCalcium373000CadmiumNDCobaltNDCOK18049050.0ug/LDilutionFactor:10MDL....•...•.••:6.82000ug/LDilutionFactor:10MDL..........•.:96.8100ug/LDilutionFactor:10MDL•...........:27.42000ug/LDilutionFactor:10MDL....•.•.....:6.240.0ug/LDilutionFactor:10MDL.....•......:2.32000ug/LDilutionFactor:10MDL..•.........:13.150000ug/LDilutionFactor:10MDL......••....:96.850.0ug/LDilutionFactor:10MDL............:1.3500ug/LDilutionFactor:10MDL........•...:4.0SW8466010BAnalysisTime••:SW8466010BAnalysisTime..:SW8466010BAnalysisTime..:SW8466010BAnalysisTime..:SW8466010BAnalysisTime..:SW8466010BAnalysisTime..:SW8466010BAnalysisTime•.:SW8466010BAnalysisTime..:SW8466010BAnalysisTime..:(Continuedonnextpage)1111/23-11/29/10L98HC1CL14:16MSRun11....•..:032707911/23-11/29/10L98HC1A314:16MSRunII•.....•:032707911/23-11/29/10L98HC1A414:16MSRunII..•....:032707911/23-11/29/10L98HC1A514:16MSRunII.••....:032707911/23-11/29/10L98HC1A614:16MSRunII.......:032707911/23-11/29/10L98HC1A714:16MSRunII..•...•:032707911/23-11/29/10L98HC1A914:16MSRunII....•..:032707911/23-11/29/10L98HC1A814:16MSRunII.......:032707911/23-11/29/10L98HC1CA14:16MSRun11....•..:0327079of57EquitableProductionCo.ClientSampleID:HURDFLOWBACK-590398TOTALMetal.sLot-Samplet...:COK180490-001Matrix.........:WATERREPORTINGPREPARATION-WORKPARAMETERRESULTLIMITUNITSMETHODANALYSISDATEORDER#ChromiumNO50.0ug/LSW8466010B11/23-11/29/10L98HC1CQDilutionFactor:10AnalysisTime..:14:16MSRunt.......:0327079MDL............:5.7CopperNO250ug/LSW8466010B11/23-11/29/10L98HC1CCDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL.•.•........:27.1Iron68001000ug/LSW8466010B11/23-11/29/10L98HC1CDDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL............:119Lithium3200500ug/LSW8466010B11/23-12/02/10L98HC1CEDilutionFactor:10AnalysisTime..:00:45MSRun#.......:0327079MDL..••.•......:27.8.Magnesium44300B50000ug/LSW8466010B11/23-11/29/10L98HC1CFDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL............:207Manganese646150ug/LSW8466010B11/23-11/29/10L98HC1CGDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL..•.........:6.8MolybdenumNO400ug/LSW8466010B11/23-11/29/10L98HC1CHDilutionFactor:10AnalysisTime..:14:16MSRun#.•.....:0327079MDL.••....•....:13.8Sodium157000050000ug/LSW8466010B11/23-11/29/10L98HC1CMDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL............:2150NickelNO400ug/LSW8466010B11/23-11/29/10L98HC1CJDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL..••........:15.6LeadNO30.0ug(LSW8466010B11/23-11/29/10L98HC1CRDilutionFactor:10AnalysisTime..:14:16MSRun#.......:0327079MDL............:12.6(Continuedonnextpage)COK18049012of57EquitableProductionCo.ClientSampleID:HURDFLOWBACK-590398TOTALMetalsLot-Samplet...:COK180490-001PARAMETERRESULTSeleniumNDStrontium117000Zinc66.2BPrepBatchf...:0330011MercuryNDNOTE(S):BEstimatedresult.ResultislessthanRL.REPORTINGLIMIT50.0UNITSug/LDilutionFactor:10MDL.....•......:30.41000ug/LDilutionFactor:20MDL...•........:1.9200ug/LDilutionFactor:10MDL........•...:24.60.20ug/LDilutionFactor:1MDL............:0.038METHODSW8466010BAnalysisTime••:14:16SW8466010BAnalysisTime..:11:10SW8466010BAnalysisTime.•:14:16SW8467470AAnalysisTime..:13:48JMethodblankcontamination.Theassociatedmethodblankcontainsthetargetanalyteatareportablelevel.COK18049013Matrix•••..•••.:WATERPREPARATION-WORKANALYSISDATEORDER#11/23-11/29/10L98HC1CKMSRunil.......:032707911/23-11/30/10L98HC1CNMSRun#...•...:032707911/23-11/29/10L98HC1CPMSRun41•...•..:032707911/26/10L98HC1AWMSRun#.......:0330003of57EquitableProductionCo.ClientSampleID:HURDFLOWBACK-590398Lot-Samplet...:COK180490-001DateSampled.••:11/17/10DISSOLVEDMetalsDateReceived••:11/17/10REPORTINGMatrix•.•••.•:WATERPREPARATION-WORK_PARAME______T_E_R_______R_E_S_U_L_T________L_I_M_I_T____________________ANALYSISDATEORDER#PrepBatcht...:0327127Iron32801000ug/LSW8466010B11/23-11/29/10L98HC1AXDilutionFactor:10AnalysisTime..:15:38MSRunf.......:0327078MDL••••••••••••:119COK18049014of57METHODBLANKREPORTTOTALMetalsClientLotf...:COK180490Matrix.........:WATERREPORTINGPREPARATION-WORK_________________________________ANALYSISDATEORDER#MBLot-Samplef:COK230000-129PrepBatchf...:0327129Aluminum30.1B200ug/LSW8466010B11/23-11/29/10MAFPD1ADArsenicNDBariumNDBerylliumNDBoronNDCadmiumNDCalciumNDChromiumNDCobaltNDCopperNDIronNDCOK180490DilutionFactor:1AnalysisTime..:13:5410.0ug/LDilutionFactor:1AnalysisTime..:13:54200ug/LDilutionFactor:1AnalysisTime..:13:544.0ug/LDilutionFactor:1AnalysisTime..:13:54200ug/LDilutionFactor:1AnalysisTime..:13:545.0ug/LDilutionFactor:1AnalysisTime..:13:545000ug/LDilutionFactor:1AnalysisTime..:13:545.0ug/LDilutionFactor:1AnalysisTime..:13:5450.0ug/LDilutionFactor:1AnalysisTime..:13:5425.0ug/LDilutionFactor:1AnalysisTime..:13:54100ug/L.DilutionFactor:1AnalysisTime..:13:54SW8466010BSW8466010BSW8466010BSW8466010BSW8466010BSW8466010BSW8466010BSW8466010BSW8466010BSW8466010B11/23-11/29/10MAFPD1AE11/23-11/29/10MAFPD1AF11/23-11/29/10MAFPD1AG11/23-11/29/10MAFPD1AH11/23-11/29/10MAFPD1AJ11/23-11/29/10MAFPD1AK11/23-11/29/10MAFPD1AA11/23-11/29/10MAFPD1AL11/23-11/29/10MAFPD1AM11/23-11/29/10MAFPD1AN....(Continuedonnextpage)FEB28201115DEP,SOUTHWESTREGIONOIL&GkSof57Client Lot



### t ...

: COK180490 PARAMETER RESULT Lead

ND Lithium

ND Magnesium

ND Manganese

ND Molybdenum

ND Nickel

ND Selenium

ND Silver

ND Sodium

ND Strontium

ND Zinc

ND 

### COK180490

METHOD BLANK REPORT TOTAL Metals REPORTING LIMIT UNITS 3.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 50.0 ug/L Dilution Factor:

1 Analysis Time ..

: 23:57 5000 ug/L Dilution Factor:

1 Analysis Time ••

: 13:54 15.0 ug/L Dilution Factor:

1 Analysis Time .•

: 13:54 40.0 ug/L Dilution Factor:

1 Analysis Time .•

: 13:54 40.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 5.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 5.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 5000 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 50.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 20.0 ug/L Dilution Factor:

1 Analysis Time ..

: 13:54 Matrix .........

: WATER PREPARATION- WORK **=ME=T~H~O~D~---------** ANALYSIS DATE ORDER



### # SW846 6010B 11/23-11/29/10 MAFPD1A2 SW846 6010B 11/23-12/01/10 MAFPD1AP SW846 6010B 11/23-11/29/10 MAFPD1AQ SW846 6010B 11/23-11/29/10 MAFPD1AR SW846 6010B 11/23-11/29/10 MAFPD1AT SW846 6010B 11/23-11/29/10 MAFPD1AU SW846 6010B 11/23-11/29/10 MAFPDlAV SW846 6010B 11/23-11/29/10 MAFPD1AW SW846 6010B 11/23-11/29/10 MAFPD1AX SW846 6010B 11/23-11/29/10 MAFPD1AO SW846 6010B 11/23-11/29/10 MAFPD1A1 (Continued

on next page) 

### 16



### of 57METHODBLANKREPORTTOTALMetalsClientLott...:COK180490Matrix••••••...:WATERREPORTINGPREPARATION-WORKPARAMETERRESULTLIMITANALYSISDATEORDER#MBLot-Samplef:COK260000-011PrepBatcht...:0330011MercuryND0.20ug/LSW8467470ADilutionFactor:1AnalysisTime..:13:28NOTE(S):Calculationsareperformedbeforeroundingtoavoidround-offerrorsincalculatedresults.8Estimatedresult.ResultIslessthanRL.COK1804901711/26/10MAKNK1AAof57METHOD BLANK REPORT DISSOLVED Metals Client Lot



### f ...

: 

### COK180490

Matrix •••••••••

: 

### WATER REPORTING PREPARATION- WORK **_P~ARAME~~~T=E~R______ ~RE~S~U=L~T**  

### ______

_ LIMIT **~UN~I~T~S~--- ~ME~TH~O~D~---------**  

### ANALYSIS DATE ORDER

# 

### MB Lot-Sample



### f: 

### COK230000-127 Prep Batch



### f ...

: 

### 0327127 Iron

ND
100 ug/L SW846 6010B 11/23-11/29/10 MAFN81AD Dilution Factor:

1 Analysis Time ..
: 15:16 NOTE(S): Calculations
are performed before rounding
to avoid round-off errors in calculated results. 

### COK180490

18



## of 57LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot

t ...

: COK180490

Matrix .........

: WATER PERCENT RECOVERY PREPARATIONPARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER

# LCS Lot-Samplef: COK230000-129 Prep Batch

t ...

: 0327129 Chromium

104
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlAC Dilution Factor:

1 Analysis Time .•

: 13:59 Aluminum

106
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A3 Dilution Factor:

1 Analysis Time ..

: 13:59 Arsenic

104
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A4 Dilution Factor:

1 Analysis Time ..

: 13:59 Barium

106
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A5 Dilution Factor:

1 Analysis Time •.

: 13:59 Beryllium

105
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A6 Dilution Factor:

1 Analysis Time ..

: 13:59 Boron

104
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A7 Dilution Factor:

1 Analysis Time ..

: 13:59 Cadmium

101
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A8 Dilution Factor:

1 Analysis Time ..

: 13:59 Calcium

104
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1A9 Dilution Factor:

1 Analysis Time ..

: 13:59 Cobalt

102
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlCA Dilution Factor:

1 Analysis Time ..

: 13:59 Copper

106
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlCC Dilution Factor:

1 Analysis Time ..

: 13:59 Iron

95
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlCD Dilution Factor:

1 Analysis Time .•

: 13:59 Lithium

104
(80

- 120) SW846 6010B 11/23-12/02/10 MAFPDlCE Dilution Factor:

1 Analysis Time ..

: 00:02 Magnesium

103
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlCF Dilution Factor:

1 Analysis Time ..

: 13:59 Manganese

102
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPDlCG Dilution Factor:

1 Analysis Time ..

: 13:59 (Continued

on next page) COK180490

19

of 57LABORATORY CONTROL SAMPLE EVALUATION REPORT TOTAL Metals Client Lot

t ••.

: COK180490

Matrix •••••.•••

: WATER PERCENT RECOVERY PREPARATIONPARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER

# Molybdenum

104
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CH Dilution Factor:

1 Analysis Time ..

: 13:59 Nickel

102
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CJ Dilution Factor:

1 Analysis Time ..

: 13:59 Selenium

103
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CK Dilution Factor:

1 Analysis Time .•

: 13:59 Silver

106
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CL Dilution Factor:

1 Analysis Time ..

: 13:59 Sodium

107
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CM Dilution Factor:

1 Analysis Time ..

: 13:59 Strontium

106
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CN Dilution Factor:

1 Analysis Time ..

: 13:59 Zinc

105
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CP Dilution Factor:

1 Analysis Time •.

: 13:59 Lead

102
(80

- 120) SW846 6010B 11/23-11/29/10 MAFPD1CQ Dilution Factor:

1 Analysis Time •.

: 13:59 LCS Lot-Samplet: COK260000-011 Prep Batch

t •..

: 0330011 Mercury

100
(80

- 120) SW846 7470A 11/26/10 MAKNK1AC Dilution Factor:

1 Analysis Time ..

: 13:29 NOTE (S): Calculations
ere performed before rounding
to avoid round-off errors In calculated results. COK180490

20

of 57LABORATORYCONTROLSAMPLEEVALUATIONREPORTClientLott...:COK180490PARAMETERPERCENTRECOVERYRECOVERYLIMITSDISSOLVEDMetalsMatrix•......••:WATERPREPARATIONMETHODANALYSISDATEWORKORDER#LCSLot-Samplef:COK230000-127PrepBatcht...:0327127Iron94(80-120)SW8466010B11/23-11/29/10MAFN81AEDilutionFactor:1AnalysisTime..:15:21NOTE(S):Calculationsareperformedbeforeroundingtoavoidround-offerrorsIncalculatedresults.COK18049021of57MATRIXSPIKESAMPLEEVALUATIONREPORTClientLot1...:COK180490DateSampled•••:11/16/10PERCENTRECOVERYTOTALMetalsDateReceived.•:11/17/10RPDMatrix••••.....:WATERPREPARATION-WORKPARAMETERRECOVERYLIMITSRPDLIMITSDATEORDER#MSLot-Sample1:COK170523-001PrepBatch1...:0330011Mercury101(75-125)SW8467470A103(75-125)2.0(0-20)SW8467470ADilutionFactor:1AnalysisTime.•:13:43MSRun#.•..•..:0330003NOTE(S):Calculationsareperformedbeforeroundingtoavoidround-offerrorsIncalculatedresults.COK1804902211/26/1011/26/10L96421DJL96421DKof57MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot

t ...

: COK180490

Matrix .........

: WATER Date Sampled ...

: 11/17/10 Date Received

..
: 11/18/10 PERCENT RECOVERY

RPD PREPARATION- WORK PARAMETER RECOVERY LIMITS RPD LIMITS **~ME~TH~O~D~---------** ANALYSIS DATE ORDER

# MS Lot-Sample

t: COK180494-017 Prep Batch

t ...

: 0327129 Aluminum
107 (75

- 125) SW846 6010B Arsenic Barium Beryllium Boron Cadmium Calcium COK180490

105 (75

- 125) 1.1 (0-20) SW846 6010B 105 103 106 104 106 105 105 104 103 102 103 103
(75 (75 (75 (75 (75 (7 5 (75 (75 (75 (75 (75 (75

- - - - - - - - - - - - Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .......

: 0327079 125) SW846 6010B 125) 1.3 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time .•

: 14:37 MS Run

II .••..•.

: 0327079 125) SW846 6010B 125) 1.1 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .......

: 0327079 125) SW846 6010B 125) 1.2 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II ....•..

: 0327079 125) SW846 6010B 125) 1.3 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .•••...

: 0327079 125) SW846 6010B 125) 1.0 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .......

: 0327079 125) SW846 6010B 125) 0.35 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II ..•....

: 0327079 (Continued

on next page) 23 11/23-11/29/10 L98LQ1AH 11/23-11/29/10 L98LQ1AJ 11/23-11/29/10 L98LQ1AL 11/23-11/29/10 L98LQ1AM 11/23-11/29/10 L98LQ1AP 11/23-11/29/10 L98LQ1AQ 11/23-11/29/10 L98LQ1AT 11/23-11/29/10 L98LQ1AU 11/23-11/29/10 L98LQ1AW 11/23-11/29/10 L98LQ1AX 11/23-11/29/10 L98LQ1A1 11/23-11/29/10 L98LQ1A2 11/23-11/29/10 L98LQ1A4 11/23-11/29/10 L98LQ1A5 of 57MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot
1 ...

: COK180490

Matrix .........

: WATER Date Sampled ...

: 11/17/10 Date Received

..
: 11/18/10 PARAMETER Chromium Cobalt Copper Iron Lead Lithium Magnesium COK180490 PERCENT RECOVERY 105 104 103 102 107 106 97 97 102 101 106 105 103 103 RECOVERY

RPD PREPARATION- WORK **ME~T~H~O~D~----------** ANALYSIS DATE ORDER

i LIMITS RPD LIMITS (75

- 125) SW846 6010B 11/23-11/29/10 L98LQ1AE (75

- 125) 1.1 (0-20) SW846 6010B 11/23-11/29/10 L98LQ1AF (75

- (75

- (75

- (75

- (75

- (75

- (75

- (75

- (7 5 - (75

- (75

- (75

- Dilution Factor:

1 Analysis Time .•

: 14:37 MS Run
# ..••..•

: 0327079 125) SW846 6010B 125) 1.3 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .......

: 0327079 125) SW846 6010B 125) 1.2 (0-20) SW846 601.0B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run
# .•.••.•

: 0327079 125) SW846 6010B 125) 0.30 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14

: 37 MS Run

II ..•....

: 0327079 125) SW846 6010B 125) 1.1 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run
# •.••.•.

: 0327079 125) SW846 6010B 125) 0.17 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 00:16 MS Run
# ......•

: 0327079 125) SW846 6010B 125) 0.32 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 14:37 MS Run

II .......

: 0327079 (Continued

on next page) 24 11/23-11/29/10 L98LQ1A7 11/23-11/29/10 L98LQ1A8 11/23-11/29/10 L98LQ1CA 11/23-11/29/10 L98LQ1CC 11/23-11/29/10 L98LQ1CE 11/23-11/29/10 L98LQ1CF 11/23-11/29/10 L98LQ1DH 11/23-11/29/10 L98LQ1DJ 11/23-12/02/10 L98LQ1CH 11/23-12/02/10 L98LQ1CJ 11/23-11/29/10 L98LQ1CL 11/23-11/29/10 L98LQ1CM of 57MATRIXSPIKESAMPLEEVALUATIONREPORTTOTALMetalsClientLotf...:COK180490Matrix.........:WATERDateSampled...:11/17/10DateReceived..:11/18/10PERCENTRECOVERYRPDPREPARATION-WORKPARAMETERRECOVERYLIMITSRPDLIMITSMETHODANALYSISDATEORDER#Manganese104(75-125)SW8466010B11/23-11/29/10L98LQ1CP103(75-125)0.99(0-20)SW8466010B11/23-11/29/10L98LQ1CQDilutionFactor:1AnalysisTime.•:14:37MS......•:0327079Molybdenum104(75-125)SW8466010B11/23-11/29/10L98LQ1CT104(75-125)0.27(0-20)SW8466010B11/23-11/29/10L98LQ1CUDilutionFactor:1AnalysisTime••:14:37MSRun#..•....:0327079Nickel103(75-125)SW8466010B11/23-11/29/10L98LQ1CW102(75-125)1.4(0-20)SW8466010B11/23-11/29/10L98LQ1CXDilutionFactor:1AnalysisTime..:14:37MSRun#..•••..:0327079Selenium104(75-125)SW8466010B11/23-11/29/10L98LQ1Cl103(75-125)1.2(0-20)SW8466010B11/23-11/29/10L98LQ1C2DilutionFactor:1AnalysisTime.•:14:37MSRun#.••.••.:0327079Silver108(75-125)SW8466010B11/23-11/29/10L98LQ1C4106(75-125)1.5(0-20)SW8466010B11/23-11/29/10L98LQ1C5DilutionFactor:1AnalysisTime..:14:37MSRun#..•••••:0327079Sodium107(75-125)SW8466010B11/23-11/29/10L98LQ1C7106(75-125)0.50(0-20)SW8466010B11/23-11/29/10L98LQ1C8DilutionFactor:1AnalysisTime..:14:37MSRun#.....•.:0327079Strontium105(75-125)SW8466010B11/23-11/29/10L98LQ1DA104(75-125)1.1(0-20)SW8466010B11/23-11/29/10L98LQ1DCDilutionFactor:1AnalysisTime..:14:37MSRun#.....•.:0327079(Continuedonnextpage)COK18049025of57MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot

t ...

: COK180490 Date Sampled ...

: 11/17/10 Date Received

..
: 11/18/10 PARAMETER Zinc NOTE (S): PERCENT RECOVERY 104 103 RECOVERY LIMITS RPD (75

- 125) (75

- 125) 1.1 RPD LIMITS (0-20) Dilution Factor:

1 Analysis Time ..

: 14:37 METHOD SW846 6010B SW846 6010B MS Run# .......

: 0327079 Calculations
are performed before rounding
to avoid round-off errors in calculated results

.
. COK180490

26 Matrix .........

: WATER PREPARATIONANALYSIS DATE 11/23-11/29/10 11/23-11/29/10 WORK ORDER

# L98LQ1DE L98LQ1DF of 57Client Lot

f ...

: COK180490 Date Sampled ••.

: 11/17/10 MATRIX SPIKE SAMPLE EVALUATION REPORT DISSOLVED Metals Date Received

•.

: 11/18/10 RPD Matrix ••.......

: WATER PARAMETER PERCENT RECOVERY RECOVERY LIMITS RPD LIMITS **ME~~TH~O~D~----------** PREPARATION- WORK ANALYSIS DATE ORDER

# MS Lot-Sample

f: COK180494-016 Prep Batch

f ...

: 0327127 Iron

94 (75

- 125) SW846 6010B 96 (75

- 125) 0.30 (0-20) SW846 6010B Dilution Factor:

1 Analysis Time ..

: 16:16 MS Run# .......

: 0327078 NOTE(S): Calculations
are performed before rounding
to avoid round-off erron in calculated results

. COK180490

27 11/23-11/29/10 L98LL1AH 11/23-11/29/10 L98LL1AJ of 57Equitable Production Co. Client Sample ID: HURD FLOW BACK-590398 General Chemistry Lot-Sample

f ...

: COK180490-001 Date Sampled •..

: 11/17/10 Work Order

f ...

: L98HC Date Received

.•

: 11/17/10 Matrix ••..•••••

: WATER PARAMETER pH Acidity Ammonia Nitrogen Biochemical Oxygen Demand (BOD) Bromide Chemical Oxygen Demand (COD) Chloride Hardness, as CaC03 Nitrate
as N Nitrite
as N COK180490 RESULT 7.4 ND 8.0 53.2 28.0 286 3490 1320 ND G ND G
RL UNITS Dilution Factor:

1 MDL ............

: 0.0 5.0 mg/L Dilution Factor:

1 MDL ............

: 5.0 0.50 mg/L Dilution Factor:

5 MDL ............

: 0.041 2.0 mg/L Dilution Factor:

1 MDL ............

: 0. 79 2.0 mg/L Dilution Factor:
10 MDL ............

: 0.42 10.0 mg/L Dilution Factor:

1 MDL ............

: 3.9 100 mg/L Dilution Factor: 100 MDL ............

: 19.5 50.0 mg/L Dilution Factor:
10 MDL ............

: 15.4 0.50 mg/L Dilution Factor:
10 MDL ............

: 0.14 0.50 mg/L Dilution Factor:
10 MDL ............

: 0.15 METHOD SM20 4500-H+B Analysis Time ..

: 15:13 SM20 2310B (4a) Analysis Time ..

: 13:38 MCAWW 350.1 Analysis Time ..

: 14:46 SM20 5210B Analysis Time ..

: 09:05 MCAWW 300.0A Analysis Time ..

: 20:10 MCAWW 410.4 Analysis Time ..

: 13:16 MCAWW 300. OA Analysis Time ..

: 20:31 SM20 2340C Analysis Time ..

: 08:45 MCAWW 300.0A Analysis Time ..

: 20:10 MCAWW 300.0A Analysis Time ..

: 20:10 (Continued

on next page) 28PREPARATIONANALYSIS DATE 11/18/10 PREP BATCH

# 0322329 MS Runt .......

: 0322185 11/27/10 0331042 MS Run

t .......

: 0331019 11/19-11/23/10 0323198 MS Run# .......

: 0323115 11/19-11/24/10 0323082 MS Runt .......

: 0323050 11/18/10 0324044 MS Runt .......

: 11/29/10 0333068 MS Run

t .......

: 0333032 11/18/10 0324040 MS Run

f .......

: 11/29/10 0333050 MS Runt .......

: 0333025 11/18/10 0324039 MS Run

II .•.....

: 11/18/10 0324045 MS Run# .......

: of 57Equitable Production Co. Client Sample ID: HURD FLOW BACK-590398 General Chemistry Lot-Sample

f ...

: COK180490-001 Work Order

1 ...

: L98HC Matrix •.••..••.

: WATER PARAMETER RESULT Oil & Grease (HEM) 13.1 Specific Conductance 12300 Sulfate Total Alkalinity Total Dissolved Solids Total Recoverable Phenolics Total Suspended Solids NOTE (S): RL Reporting Limit
126

J 103

J 6740 0.016

J 25.6

RL UNITS 4.7 mq/L Dilution Factor: 0.94 MDL .•..........

: 1.5 25.0 umhos/cm Dilution Factor: 25 MDL •.....••••.•

: 10.0 mq/L Dilution Factor:
10 MDL •........•..

: 2.1 5.0 mg/L Dilution Factor:

1 MDL ............

: 0.41 50.0 mg/L Dilution Factor:

5 MDL ............

: 50.0 0.010 mq/L Dilution Factor:

1 MDL ...

· ..•......

: 0. 0062 4.0 mg/L Dilution Factor:

1 MDL •...•...•...

: 2 . 0 G Elevated reporting limit. The reporting limit Is elevated due to matrix interference. PREPARATION- PREP METHOD ANALYSIS DATE BATCH

f CFR136A 1664A HEM 11/19/10 0323244 Analysis Time ..

: 10:35 SM20 2510B Analysis Time ..

: 00:00 MCAWW 300

. OA Analysis Time ..

: 20:10 SM18 2320
B Analysis Time ..

: 00:00 SM20 2540C Analysis Time ..

: 11

: 15 MCAWW 420.4 Analysis Time ..

: 10:33 SM20 25400 Analysis Time ..

: 06:15
MS Run

II .....•.

: 11/29/10 0333041 MS Run

II ....•.•

: 0333014 11/18/10 0324043 MS Run

t .......

: 12/02/10 0335025 MS Run

t .......

: 0336085 11/19-11/20/10 0323271 MS Run

II .......

: 0323149 11/23-11/24/10 0327071 MS Run# .......

: 0327181 11/19-11/20/10 0323267 MS Run# .......

: 0323145 J Method blank contamination. The associated method blank contains the target analyte
at a reportable level. COK180490

29

of 57Client Lot

t ...

: COK180490 PARAMETER Acidity Ammonia Nitrogen Biochemical Oxygen Demand (BOD) Bromide Chemical Oxygen Demand (COD) Chloride Hardness, as CaC03 Nitrate
as N COK180490 RESULT ND ND ND ND ND ND ND ND METHOD BLANK REPORT General Chemistry Matrix .........

: WATER REPORTING LIMIT UNITS Work Order #: MAKRL1AA 5.0 mg/L Dilution Factor:

1 Analysis Time ••

: 13:38 Work Order #: L999G1AAPREPARATIONMETHOD ANALYSIS DATE MB Lot-Sample

#: COK270000-042 SM20 2310B (4a) 11/27/10 MB Lot-Sample

#: COK190000-198 PREP BATCH

# 0331042 0.10 mg/L MCAWW 350.1 11/19-11/23/10 0323198 Dilution Factor:

1 Analysis Time ..

: 13:28 Work Order #: L99RA1AA
MB Lot-Sample

#: COK190000-082 2.0 mg/L SM20 5210B 11/19-11/24/10 0323082 Dilution Factor:

1 Analysis Time ..

: 09:05 Work Order #: MACXR1AA 0.20 mg/L Dilution Factor:

1 Analysis Time ..

: 14:34
MB Lot-Sample

#: COK200000-044 MCAWW 300.0A 11/18/10 Work Order #: MAK8T1AA
MB Lot-Sample

#: COK290000-068 10.0 mg/L Dilution Factor:

1 Analysis Time ..

: 13:14 Work Order #: MACXH1AA 1. 0 mg/L Dilution Factor:

1 Analysis Time ..

: 14:34 MCAWW 410.4 11/29/10 MB Lot-Sample

#: COK200000-040 MCAWW 300.0A 11/18/10 Work Order #: MAK501AA
MB Lot-Sample

#: COK290000-050 5.0 mg/L Dilution Factor:

1 Analysis Time

. . : 08:45 Work Order #: MACXF1AA 0.050 mg/L Dilution Factor:

1 Analysis Time ..

: 14

: 34 SM20 2340C 11/29/10 MB Lot-Sample

#: COK200000-039 MCAWW 300.0A 11/18/10 (Continued

on next page) 30

0324044 0333068 0324040 0333050 0324039 of 57METHOD BLANK REPORT General Chemistry Client Lot

f ...

: COK180490

Matrix •••••••••

: WATER REPORTING PREPARATION- PREP **.::.P.:..:ARAME==T~E=R'-'------** ::...:RE:::.S=-.U.::.;L:;..:T:..___ =L-=IM.:..:I::..:T:..___ ..::.UN::..:..::...IT::..:S::.__ __ **ME==-TH::.O.=.D~-----** ANALYSIS DATE BATCH

# Nitrite
as N ND Oil & Grease (HEM) ND Specific Conductance
ND Sulfate Total Alkalinity Total Dissolved Solids Total Recoverable Phenolics Total Suspended Solids NOTE (S): 0.22
B 2.3 B ND 0.0068

B ND Work Order #: MACXX1AA 0.050 mg/L Dilution Factor:

1 Analysis Time ..

: 14:34 Work Order #: MAALD1AA 5.0 mg/L Dilution Factor:

1 Analysis Time ..

: 10:35 Work Order #: MAK241AA 1.0 umhos/cm Dilution Factor:

1 Analysis Time ..

: 00:00 Work Order #: MACXL1AA 1.0 mg/L Dilution Factor:

1 Analysis Time ..

: 14:34 Work Order #: MANJJ1AA 5.0 mg/L Dilution Factor:

1 Analysis Time ..

: 00:00

MB Lot-Sample

#: COK200000-045 MCAWW 300.0A 11/18/10 MB Lot-Sample

#: COK190000-244 CFR136A 1664A HEM 11/19/10 MB Lot-Sample

#: COK290000-041 SM20 25108 11/29/10 MB Lot-Sample

#: COK200000-043 MCAWW 300.0A 11/18/10 MB Lot-Sample

#: COL010000-025 SM18 2320

B 12/02/10 0324045 0323244 0333041 0324043 0335025 Work Order #: MAAQV1AA
MB Lot-Sample

#: COK190000-271 10.0 mg/L Dilution Factor:

1 Analysis Time ..

: 11:15 SM20 2540C 11/19-11/20/10 0323271 Work Order #: MAGG01AA
MB Lot-Sample

#: COK230000-071 0.010 mq/L Dilution Factor:

1 Analysis Time •.

: 10:33 MCAWW 420.4 11/23-11/24/10 0327071 Work Order #: MAAP91AA
MB Lot-Sample

#: COK190000-267 4.0 mg/L Dilution Factor:

1 Analysis Time ..

: 06:15 SM20 2540D 11/19-11/20/10 0323267 Calculations
are performed before rounding
to avoid round-off errors in calculated results

. B Estimated result. Result
is less than RL. COK180490

31

of 57LABORATORY CONTROL SAMPLE EVALUATION REPORT General Chemistry Lot-Sample

f ...

: COK180490

Matrix .........

: WATER PERCENT RECOVERY
RPD PREPARATION- PREP PARAMETER RECOVERY LIMITS RPD LIMITS **~ME~TH_O~D** ____________ ANALYSIS DATE BATCH

# Biochemical Oxygen Demand (BOD) Bromide Chloride Nitrate
as N Nitrite
as N Oil & Grease Sulfate NOTE(S):
105 105 104 104 104 104 108 108 104 103 (HEM) 82 86 104 104 WO#:L99RA1AC-LCS/L99RA1AD-LCSD

LCS Lot-Sample#: COK190000-082 (85

- 115)
SM20 5210B (85

- 115) 0.24 (0-20) SM20 5210B 11/19-11/24/10 0323082 11/19-11/24/10 0323082 Dilution Factor:

1 Analysis Time •.

: 09:05 WO#:MACXR1AC-LCS/MACXR1AD-LCSD

LCS Lot-Sample#: COK200000-044 (90

- 110) MCAWW 300.0A 11/18/10 0324044 (90

- 110) 0.09 (0-20) MCAWW 300.0A 11/18/10 0324044 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MACXH1AC-LCS/MACXH1AD-LCSD

LCS Lot-Sample#: COK200000-040 (90

- 110) MCAWW 300.0A 11/18/10 0324040 (90

- 110) 0.13 (0-20) MCAWW 300.0A 11/18/10 0324040 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MACXF1AC-LCS/MACXF1AD-LCSD

LCS Lot-Sample#: COK200000-039 (90

- 110) MCAWW 300.0A 11/18/10 0324039 (90

- 110) 0.14 (0-20) MCAWW 300.0A 11/18/10 0324039 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MACXX1AC-LCS/MACXX1AD-LCSD

LCS Lot-Sample#: COK200000-045 (90

- 110) MCAWW 300.0A 11/18/10 0324045 (90

- **1~0)** 0.07 (0-20) MCAWW 300.0A 11/18/10 0324045 Dilution Factor:

1 Analysis Time ..

: 14:13 WO#:MAALD1AC-LCS/MAALD1AD-LCSD

LCS Lot-Sample#: COK190000-244 (78

- 114) CFR136A 1664A HEM 11/19/10 0323244 (78

- 114) 3.9 (0-18) CFR136A 1664A HEM 11/19/10 0323244 Dilution Factor:

1 Analysis Time ..

: 10:35 WO#:MACXL1AC-LCS/MACXL1AD-LCSD

LCS Lot-Sample#: COK200000-043 (90

- 110) MCAWW 300.0A 11/18/10 0324043 (90

- 110) 0.17 (0-20) MCAWW 300.0A 11/18/10 0324043 Dilution Factor:

1 Analysis Time ..

: 14:13 Calculations are performed before rounding

to avoid round-off errors In calculated results. COK180490

32

of 57LABORATORY CONTROL SAMPLE EVALUATION REPORT Client Lot

t ...

: COK180490 PERCENT PARAMETER RECOVERY pH

100 Acidity

99 Ammonia Nitrogen
92 Chemical Oxygen Demand (COD) Hardness, as CaC03 103 100 Specific Conductance 111 Total Alkalinity

91 Total Dissolved Solids
109 Total Recoverable Phenolics
100 COK180490

General Chemistry Matrix .........

: WATER RECOVERY LIMITS METHODPREPARATIONANALYSIS DATE PREP BATCH

# Work Order #: L985AlAA LCS Lot-Sample#: COK180000-329 (99

- 101) SM20 4500-H+B 11/18/10 0322329 Dilution Factor:

1 Analysis Time ..

: 15:05 Work Order #: MAKRLlAC LCS Lot-Sample#: COK270000-042 (80

- 120) SM20 2310B (4a) 11/27/10 0331042 Dilution Factor:

1 Analysis Time ..

: 13:38 Work Order #: L999GlAC (90

- 110) MCAWW 350.1 LCS Lot-Sample#: COK190000-198 11/19-11/23/10 0323198 Dilution Factor:

1 Analysis Time ..

: 13:26 Work Order #: MAK8TlAC LCS Lot-Sample#: COK290000-068 (90

- 110) MCAWW 410.4 11/29/10 0333068 Dilution Factor:

1 Analysis Time

. . : 13:14 Work Order #: MAK501AC LCS Lot-Sample#: COK290000-050 (90

- 110) SM20 2340C 11/29/10 0333050 Dilution Factor:

1 Analysis Time ••

: 08:45 Work Order #: MAK241AC ( 80

- 120) SM20 2510B LCS Lot-Sample#: COK290000-041 11/29/10 0333041 Dilution Factor:

1 Analysis Time ..

: 00:00 Work Order #: MANJJlAC (80

- 120) SM18 2320
B LCS Lot-Sample#: COLOl0000-025 12/02/10 0335025 Dilution Factor:

1 Analysis Time .•

: 00:00 Work Order #: MAAQVlAC LCS Lot-Sample#: COK190000-271 (80

- 120) SM20 2540C 11/19-11/20/10 0323271 Dilution Factor:

1 Analysis Time

. . : 11:15 Work Order #: MAGGOlAC LCS Lot-Sample#: COK230000-071 (90

- 110) MCAWW 420.4 11/23-11/24/10 0327071 Dilution Factor:

1 Analysis Time

. . : 10:33 (Continued

on next page) 33

of 57LABORATORY CONTROL SAMPLE EVALUATION REPORT Client Lot

t ...

: COK180490 PERCENT PARAMETER RECOVERY Total Suspended Solids

97 NOTE(S):
General Chemistry RECOVERY LIMITS **~ME~TH~O~D~----------** Matrix •...••.••

: WATER PREPARATIONANALYSIS DATE PREP BATCH

# Work Order #: MAAP91AC LCS Lot-Sample#: COK190000-267 (80

- 120) SM20 25400 11/19-11/20/10 0323267 Dilution Factor:

1 Analysis Time ..

: 06:15 Calculations are performed before rounding
to avoid I'OUJ1d.off errors
In calculated results. COK180490

34

of 57MATRIX SPIKE SAMPLE EVALUATION REPORT Client Lot

t ...

: COK180490 Date Sampled •..

: 11/22/10 PERCENT RECOVERY General Chemistry Date Received

••

: 11/22/10 RPD
Matrix .•.•.•.••

: WATER PREPARATION- PREP PARAMETER RECOVERY Ammonia Nitrogen 114N 112N _L_I_M_I_T_S ____ RPD LIMITS **~ME~T~H~O~D** ___________ ANALYSIS DATE BATCH

# WO#: L96GV1A1-MS/L96GV1A2-MSD

MS Lot-Sample

#: COK170441-001 Chemical Oxygen Demand (COD) 92 100 Total Recoverable Phenolics NOTE (S): 102 102 (90

- 110) MCAWW 350.1 11/19-11/23/10 0323198 (90

- 110) 1.4 (0-20) MCAWW 350.1 11/19-11/23/10 0323198 Dilution Factor:

1 Analysis Time •.

: 13:49 MS Run# •.•

• ...

: 0323115 WO#: MAEP31AH-MS/MAEP31AJ-MSD

MS Lot-Sample

#: COK220467-001 (90

- 110) (90

- 110) 6.0 MCAWW 410.4 (0-20) MCAWW 410.4 Dilution Factor:

1 Analysis Time ..

: 13:17 MS Run# •.•.•..

: 0333032 11/29/10 11/29/10 0333068 0333068 WO#: L98HL1AF-MS/L98HL1AG-MSD

MS Lot-Sample

#: COK180491-002 (90

- 110) MCAWW 420.4 (90

- 110) 0.19 (0-20) MCAWW 420.4 Dilution Factor:

1 Analysis Time ..

: 10:33 MS Run# .......

: 0327181 11/23-11/24/10 0327071 11/23-11/24/10 0327071 Calculations
are performed before rounding
to avoid round-off errors in calculated results. N Spiked analyte recovery

Is outside stated control limils. COK180490

35

of 57Client Lot

f ...

: COK180490 Date Sampled ...

: 11/18/10 DUPLICATE PARAM RESULT RESULT Biochemical Oxygen Demand (BOD) NO

NO COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

f ...

: L979E-SMP L979E-DUP Date Received

..
: 11/18/10 Matrix .......

: WATER RPD PREPARATION- PREP UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH

# SD Lot-Sample

#: COK180463-001 mg/L

0 (0-20) SM20 5210B 11/19-11/24/10 0323082 Dilution Factor:

1 Analysis Time ..

: 09:05
MS Run Number
..

: 0323050 36

of 57Client Lot

f ...

: COK180490 Date Sampled ...

: 11/18/10 DUPLICATE PARAM RESULT RESULT Total Suspended Solids ND

ND COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

f ...

: L990D-SMP L990D-DUP Date Received

..
: 11/19/10 RPD UNITS RPD LIMIT METHOD Matrix .......

: WATER PREPARATION- PREP ANALYSIS DATE BATCH

# SD Lot-Sample

#: COK190421-001 mg/L 0.0 (0-20) SM20 2540D 11/19-11/20/10 0323267 Dilution Factor:

1 Analysis Time ..

: 06:15

MS Run Number
..

: 0323145 37

of 57ClientLotf...:COK180490DateSampled...:11/16/10DUPLICATEPARAMRESULTRESULTTotalDissolvedSolids259215COK180490SAMPLEDUPLICATEEVALUATIONREPORTGeneralChemistryWorkOrderf...:L9642-SMPL9642-DUPDateReceived..:11/17/10Matrix.......:WATERRPDPREPARATION-PREPUNITSRPDLIMITMETHODANALYSISDATEBATCH#SDLot-Sample#:COK170523-001mg/L19(0-20)SM202540C11/19-11/20/100323271DilutionFactor:1AnalysisTime..:11:15MSRunNumber..:032314938of57Client Lot

f ...

: COK180490 Date **Sampled~··=** 11/17/10 DUPLICATE PARAM RESULT RESULT Acidity ND

ND COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

f ...

: L98XT-SMP L98XT-DUP Date Received

..
: 11/18/10 Matrix .......

: WATER RPD PREPARATIONUNITS RPD LIMIT METHOD ANALYSIS DATE SD Lot-Sample

i: COK180529-003 mg/L

0 (0-20) SM20 231GB (4a) 11/27/10 Dilution Factor:

1 Analysis Time •.

: 13:38
MS Run Number
..

: 39

PREP BATCH

# 0331042 0331019 of 57Client Lot

f ...

: COK180490 Date Sampled ...

: 11/19/10 DUPLICATE PARAM RESULT RESULT Acidity ND

ND COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

f ...

: MAEPJ-SMP MAEPJ-DUP Date Received

..
: 11/20/10 Matrix .......

: WATER RPD PREPARATIONUNITS RPD LIMIT METHOD ANALYSIS DATE SD Lot-Sample

#: COK220465-001 mg/L

0 (0-20) SM20 231GB (4a) 11/27/10 Dilution Factor:

1 Analysis Time ..

: 13:38
MS Run Number
..

: 40

PREP BATCH

# 0331042 0331019 of 57Client Lot

f ...

: COK180490 Date Sampled ...

: 11/16/10 PARAM RESULT DUPLICATE RESULT Specific Conductance 523 528 COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

f ...

: L95MM-SMP L95MM-DUP Date Received

..
: 11/16/10 Matrix .......

: WATER UNITS RPD umhos/cm 0.95 Dilution Factor:

1 RPD LIMIT METHOD SO Lot-Sample

#: (0-20) SM20 2510B Analysis Time ..

: 00:00 41PREPARATIONANALYSIS DATE COK160529-001 11/29/10 MS Run Number
..

: PREP BATCH

# 0333041 0333014 of 57Client Lot

t ...

: COK180490 Date Sampled ...

: 11/03/10 DUPLICATE PARAM RESULT RESULT Hardness, as CaC03 200 200 COK180490
SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Work Order

t ...

: L9H9D-SMP L9H9D-DUP Date Received

..
: 11/04/10 Matrix .......

: WATER RPD PREPARATIONUNITS RPD LIMIT METHOD ANALYSIS DATE SD Lot-Sample

#: COK040431-004 mg/L 0.0 (0-20) SM20 2340C 11/29/10 Dilution Factor:
10 Analysis Time ..

: 08:45

MS Run Number
..

: 42

PREP BATCH

# 0333050 0333025 of 57ClientLotf...:COK180490DateSampled...:11/17/10DUPLICATEPARAMRESULTRESULTHardness,asCaC033600035000pH6.66.6COK180490SAMPLEDUPLICATEEVALUATIONREPORTGeneralChemistryWorkOrderf...:L975G-SMPL975G-DUPDateReceived..:11/17/10Matrix.......:WATERRPDPREPARATIONUNITSRPDLIMITMETHODANALYSISDATESDLot-Sample#:COK180438-001mg/L2.8(0-20)SM202340C11/29/10DilutionFactor:500AnalysisTime..:08:45MSRunNumber..:SDLot-Sample#:COK180438-0010.0(0-2.0)SM204500-H+B11/18/10DilutionFactor:1AnalysisTime..:15:07MSRunNumber.•:43PREPBATCH#0333050033302503223290322185of57SAMPLE DUPLICATE EVALUATION REPORT General Chemistry Client Lot

f ...

: COK180490 Work Order

t ...

: L98HC-SMP L98HC-DUP Date Received
•.

: 11/17/10 Matrix •••...•

: WATER Date Sampled •••

: 11/17/10 DUPLICATE

RPD PREPARATIONPARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE Total Alkalinity

SD Lot-Sample

#: COK180490-001 103

J 103 mg/L 0.068 (0-20) SM18 2320
B 12/02/10 Dilution Factor:

1 Analysis Time ..

: 00:00

MS Run Number
..

: NOTE(S): Calcul•lons are performed before rounding
to avoid round-off errors In calculated results. J Method blank contamination. The associated method blank contains the **~get** analyte
at a reportable level

. COK180490

44

PREP BATCH

# 0335025 0336085 of 57Test America Analytical Report SDG Number: COK180490 Project Description(s) Equitable Production Company Equitable Production Company For: Chris Kovitch TestAmerlca Pittsburgh 301 Alpha Drive; RIDC Park Pittsburgh, PA 15238 Melissa Deyo For Sally Hoffman Project Manager melissa.deyo@testamericainc.com Tuesday, January
4, 2011 The test results
in this report meet all NELAP requirements
for analytes for which accreditation

is required or available

. Any exception
to NELAP requirements
are noted
in this report. Persuant
to NELAP, this report may not be reproduced, except
in full, without the written approval
of the laboratory

. All questions regarding this test report should be directed
to the TestAmerica Project manager who has signed this report. COK180490

45

:: of 57Test America THe **~1ft INYIRON~NfAL**  TI!SYING TestAmerica Pittsburgh

SDG Number: COK180490

Received: 11/19/10-11/23/10 301 Alpha Drive; RIDC Par1c:

Reported

: 01/04/1110:27 Pittsburgh, PA 15238

Project: Equitable Production Company Project Number: COK180490 TestAmerica Buffalo Current Certifications

As of 08/16/2010 STATE Program

Cert #I Lab ID Ark_ansas

CWA, RCRA, SOIL

88-0686 California*
NELAP CWA, RCRA
01169CA Connecticut
SDWA, CWA, RCRA, SOIL
PH-0568 Florida*
NELAP CWA, RCRA

E87672 Georgia* SDWA,NELAP CWA, RCRA

956 Illinois*
NELAP SDWA, CWA, RCRA

200003 Iowa

SWIGS

374 Kansas*
NELAP SDWA, CWA, RCRA
E-10187 Kentucky

SDWA

90029 Kentucky UST

UST

30 Louisiana*
NELAP CWA, RCRA

2031 Maine

SDWA, CWA

NY0044 Maryland

SDWA

294 Massachusetts

SDWA, CWA

M-NY044 Michigan

SDWA

9937 Minnesota SDWA,CWA, RCRA 036-999-337 New Hampshire* NELAP SDWA, CWA

233701 New Jersey* NELAP,SDWA, CWA, RCRA,

NY455 New York* NELAP, AIR, SDWA, CWA, RCRA

10026 North Dakota

CWA, RCRA

R-176 Oklahoma

CWA, RCRA

9421 Oregon* CWA,RCRA

NY200003 Pennsylvania*
NELAP CWA,RCRA

68-00281 Tennessee

SDWA

02970 Texas*
NELAP CWA, RCRA

T1 0470441

2 -08- TX USDA FOREIGN SOIL PERMIT Virginia

SDWA Washington*
NELAP CWA,RCRA Wisconsin

CWA, RCRA West Virginia CWA,RCRA *As required under the hdicated accrec:llation,
the test results

i1 this report meet all NELAP requirements

for parame ters for which accreditation

is required
or avalable. Any exceptions

to NELAP requirements
are noted
in this report. TestAmerica Buffalo-
10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com

S-41579 278 C1677 998310390 252 COK180490

46

Page
2 of t1 of 57Test America TestAmerica Pittsburgh 301 Alpha Drive; RIDC Park Pittsburgh, PA 15238

SDG Number

: COK180490

Recaived

: 11/19/10.11/23/10 Reported: 01/04/1110:27 Project: Equitable Production Company Project Number: COK180490 CASE NARRATIVE According

to 40CFR Part 136

. 3, pH, Chlorine Residual, Dissolved Oxygen, Sulfite, and Temperature analyses are to be performed immediately after aqueous sample collection

. When these parameters are not indicated as field (e.g. field-pH), they were not analyzed immediately, but as soon as possible after laboratory receipt. I certify that this data package

is in compliance with the terms and conditions

of the contract, both technically and for completeness,

for other than the conditions detailed within the body of this report. Release
of the data contained

in this sample data package and in the electronic data deliverables has been authorized
by the Laboratory Manager
or his/her designee,
as verified by the following signature. Melissa Deyo For Sally Hoffman Project Manager Tuesday, January
4, 2011 There are pertinent documents appended
to this report,

2 pages, are included and are an integral part of this report. Reproduction

of this analytical report
is permitted only in its entirety. This report shall not be reproduced except
in full without the written approval
of the laboratory. TestArnerica Laboratories,
Inc. certifies that the analytical results contained herein apply only to the samples tested as received by our Laboratory. TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com COK180490

47Test America 'fHI UlAOEit lN INYIIIIOIIMENTAL f!S'hNG TestAmerica Pittsburgh

SDG Number: COK180490

Received: 11/19/10-11/23110 301 Alpha Drive; RIDC Par1<:

Reported: 01/04/11 10:27 Pittsburgh, PA 15238

Project: Equitable Production Company Project Number: COK 180490 DATA QUAUFIERS AND DEFINmONS DOB Dilution required due to high concentration

of target analyte(s} D10 Dilution required due to sample color H3 Sample was received and analyzed past holding time. Z3 The sample required

a dilution, the surrogate spike concentration

in the sample are reduced
to a level where the recovery calculation does not provide useful information. NR Any inclusion
of NR indicates that the project specific requirements

do not require reporting estimated values below the laboratory reporting limit. TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com COK180490

48Test America - THI! LI!AO!R 11'1 biVIRONMI!NfAl fi!S!INC. TestAmerica Pittsburgh 301 Alpha Drive

; RIDC Park Pittsburgh, PA 15238 Sample Data SDG Number

: COK180490 Project: Equitable Production Company Project Number

: COK180490 Executive Summary

• Detections
on Analyte
Result Qualifiers

RL MDL Units Fac Date Analyzed Client 10: HURD FLOW BACK-590398 (RTK1402..01 -Water) Sampled: 11/17/10 11:30 General Chemistry Parameters

Received: 11/19/10-11/23/10 Reported

: 01/04/1110

: 27 Lab Tech Batch Method Recvd: 11/19/10 09:00 Methylene Blue Active 0.134

H3 0.0250

0

. 0130 mg/L 1.00 11/19/10 16:30 JFR 10K2067 5540C Substances Total Kjek:lahl Nitrogen
8.52 008 2.00 1.50 mg/L 10.0 11/24/10 14:01 JME 10K2404 TestAmerica Buffalo-
10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com COK180490

49

351.2Test America **'I'~** LEAOIR 1H DIVIAOJ!IMENfAL YES'IINC!i TestAmerica Pittsburgh 301 Alpha Drive; RIDC Park Pittsburgh

, PA 15238 Sample Identification HURD FLOW BACK-590398 HURD FLOW BACK-590398

SDG Number

: COK180490 Project: Equitable Production Company Project Number: COK180490 Lab Number RTK1402-01 RTK1537-01 Sample Summary Client Matrix Water Water Date/Time Sampled 11/17/10

11

: 30 11/17/1011:30 TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc

. com COK180490

50

Received

: 11/19/10-11123/10 Reported

: 01/04/1110

: 27 Date/Time Received 11/19/10 09:00 11/23/10 09:15 Sample Qualifiers Page
6 of t1 of 57Test America THE U!AOER IN JJIIVI"ONMENtAL TESTING TestAmerica Pittsburgh 301 Alpha Drive

; RIDC Park Pittsburgh, PA 15238 Sample Data SOG Number

: COK180490 Project: Equitable Production Company Project Number

: COK180490 Analytical Report Analyte
ResuH Qualifiers

RL MDL Units
Dll Date Fac Analyzed Client ID: HURD FLOW BACK-590398 (RTK1402..01 -Water) Sampled: 11/17/10 11:30 General Chemistry Parameter!

Received

: 11/19/10-11/23/1

0 Reported

: 01/04/1110

: 27 Lab Tech Batch Method Recvd: 11/19/10 09:00 Methylene Blue Active 0.134

H3 0.0250 0.0130 mg/L 1.00 11/19/10 16:30 JFR 10K2067 5540C Substances Total Kjeldahl Nitrogen
8.52 008 2.00 1.50 mgll

10

. 0 11/24/10 14:01 JME 10K2404 351.2 TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com COK180490

51

Page
7 obf1 57TestAmerica TestAmerica Pittsburgh 301 Alpha Drive; RJDC Park Pittsburgh, PA 15238 Sample Data SDG Number: COK180490 Project

: Equitable Production Company Project Number: COK180490 Analytical Report Analyte
Result Qualifiers

RL MDL Units
Dll Date Fac Analyzed Client ID: HURD FLOW BACK-590398 (RTK1537-G1- Water) Sampled: 11/17/10 11:30 Non-Halogenated Volatile Organics

Received

: 11/19/10-11/23110 Reported

: 01/04/1110

: 27 Lab Tech Batch Method Recvd: 11123/10 09:15 Ethylene Glycol

NO 010 1000 NR rngiL 100 11/24/10 20

: 36 GFD 10K2446 8015 1, 4-Butanedio/

198%
01 O , Z3 Surr Umits

: (66-130%)
11124110 20:36 GFD 10K2446 8015 TestAmerica Buffalo-
10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamer

i cainc.com COK180490

52

Page
8 of L1 of 57Test America T estAmerica Pittsburgh

SDG Number: COK180490 301 Alpha Drive; RIDC Pari<: Pittsburgh, PA 15238

Project: Equitable Production Company Project Number: COK 180490 SAMPLE EXTRACTION DATA WWol Extract Parameter

Batch Lab Number Extracte Units Volume Units Date Prepared General Chemistry Parameters 351

. 2 10K2404 RTK1402-01 25.00 mL 25.00 mL 11/23/10
10

: 20 5540C 10K2067 RTK1402-01 400.00 mL 400.00 mL 11/19/10
16

: 30 SAMPLE EXTRACTION DATA WWol Extract Parameter

Batch Lab Number Extracte Units Volume Units Date Prepared Non-Halogenated Volatile Organics 8015 10K2446 RTK1537-01
0.50 mL 1.00 mL 11/24/10 06:26 TestAmerica Buffalo -10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www.testamericainc.com COK180490

53
Received: 11119/10-11/23/10 Reported: 01/04/11
10

: 27 Lab Tech Extraction Method JME TKN Digestion JFR MBAS Lab Tech Extraction Method GFD 8015 Glycols Page
9 obJ:1 57Test America THE UAOU .. ENVIROtllloiENTAL fESYIHG T estAmerlca Pittsburgh

SDG Number: COK180490 301 Alpha Drive; RIDC Pari<: Pittsburgh, PA 15238

Project: Equitable Production Company Project Number: COK180490 LABORATORY
QC DATA

% Analyte Source Result Spike Level RL MDL Units Result REC Non-Haloaenat!d Volatile Oraanics Blank Analyzed: 11124/10 (Lab Number:10K2446-BLK1, Batch: 101<2446) Ethylene Glycol

10
NR rng/L
NO Surrogate: 1,4-Butanediol

mg!L LCS Analyzed: 11/24/10 (Lab Number:10K2446-BS1, Batch: 101<2446) Ethylene Glycol

20

. 0
10
NR rng/L 19.8 Surrogate

: 1,4-Butanediol

mg!L TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www

. testamericainc.com COK180490

54

109 99 109 Received

: 11/19/10-11/23/10 Reported: 01/04/1110

: 27 % REC % RPD Data Limits RPD Umlt Qualifiers 66-130 50-150 66-130 Page 1 0 off11 0 57Test America T estAmerica Pittsburgh 301 Alpha Drive; RIDC Park Pittsburgh, PA 15238 Source Spike SDG Number: COK180490 Project: Equitable Production Company Project Number: COK180490 LABORATORY
QC DATA

% Analyte
Result Level RL MDL Units Result REC General Chemistry Parameters Blank Analyzed: 11/19/10 (Lab Number:10K2067-8LK1, Batch: 101<2067) Methylene Blue Active

0.0250 0.0130 mgiL
ND Substances LCS Analyzed: 11/19/10 (Lab Number:10K2067-BS1, Batch: 101<2067) Methylene Blue Active

0

. 400 0.0250 0.0130 mg/L 0.380 Substances General Chemistry Parameters Blank Analyzed: 11/24/10 (Lab Number:10K2404-BLK1, Batch: 101<2404) Total Kjeldahl Nitrogen

0

. 20

0

. 15 mg/L
ND LCS Analyzed: 11/24/10 (Lab Number:10K2404-8S1, Batch: 101<2404) Total Kjeldahl Nitrogen

2

. 50 0.20

0

. 15 mg/L 2.46 TestAmerica Buffalo- 10 Hazelwood Drive Amherst, NY 14228 tel716-691-2600

fax 716-691-7991 www

. testamericainc.com COK180490

55

95 98 Received: 11/19/10-11/23/10 Reported: 01/04/11
10

: 27 % REC
% RPD Data Limits RPD Umlt Qualifiers 90-110 90-110...COK180490INTER-COMPANYCHAINOFCUSTODYCOMMENTS:iPru]edMan.'lger:ChrisKovltcllProjlld:Farm21JRR•pcrtT!fPe:B 1SldRep•COontyClientE.qul18bleProdvtr1ionCo.WORKL.OCATION:W5TNLAmetlcaNAhvflleADDRESS;2000FoslerCnliehJOnDrive•NtshlfiJieTN37204DaleReceived:DueDale:ReportDueDate:2010-11-172010·11·292010-1'1-29SNP.r1tCJ...IENTID:HURDFLOWBACK·590398S6MPLECOMMENTDATEmME201011171130MATRIX:IWATERMETHOD;zoNONEEXTBACTION:88NOSAMPLEPERFORMED/OCTYPE;ClSTANDARDTESTSETWQR!CCPROERL98HCIAOXX114--:::rt:f:Q!;!:zoNONENONEWATER,o4Z5.1•BASTANash'lllleEXTRakiiQN:88NOSAMPLEP'R:EP'ARAiiONIQCT'r'P'E:01TESTSETWORKOROERL£18HC1A1)()(Th8tistedonlhlsformarebeingsen11oyourlocBtiDnfi:lrthespecifiedanalysis.Ifyouhawanyques!ions.pleaseeon1acttheF='mjectManagerlstedabove.PLEASERETURNTHEORIGINALSIGNEDFORMWITHTHEREPORTATTHECOMPLETIONOFANALYSIS.·IIiThankYouIJtestAmencaPittsburghSampleReceivingLBY:DATE:IIbbC,)7c."1rr1·--=-----REcelvE:.oFORLAeev.·DATE:/1-TIME:<21'vJ,)TesiAmericaPittsbu.rgllCOK1J0490printedon:Tlll.lre:d;,y.1\jovenlber18,201001:04Pr.t56Page1of57COK18049D COMt.IENTS; Pl'flied t.II:'IOger:

C hrjs Ko\'ilcl• Project

:

Form 26R R8pcm TYDt:

81 Std Reo· C[J only .

**-- ---**  **·--~---**

,, •

I INTER-COMPANY CHAIN OF CUSTODY 0111fe Received: Analytical 0111!1 Cago: Repon. **D~** Date: 2D1l•11

- 1'1 201C-11-;nl ' rt · WOR« LOCATION: ADDRESS:

10 Ma%!!!1Mxx! DI'!Ye SMP'

1 AmherE!

N"r 14221 CLIENT JD: liURD fL. Oil **B~CK-!1-!JOJ~l'.** SAMPLE COt.I!MjiNI ..,'5TI'tOD:

**~** NONE NONE WAT!R.I01!1 l!th1'en& GIJr;ol T.A Bufralo t.IJA,JBI:X.:

I WATER

I I .r EXTRAC!10N:

B8 .IK) SAMPLE. **~AAATION** PERFORMED/ OCIYPE:

D1 **SiANOA~tl** 'lEST a:-;- WQBI('ORQER l.M."IC1A2

**~** XJt • I The sample(s} listed en ltds ro1:n are beil'lg se,liO your k)calic!fl lor the li1P&Cillltd analysis..

u !'OU Nwe anv **q~.~estcn**

• . '!)leaSe conti!CIIhe ?.roject Managet listed above

. PLEASE RETURN THE ORIGINAL SIGNED FORM WrTH THE **REP~** .\T THE COMPLETION
OF ANALYSIS.

't thank VDU TesiAmerice Pillsburgh **Scl.mpl~** Receiving

!t -----:-,c---------- **DATE:...;I~~+-r----TIME:.L2:~**

_ --!\-_.,..:;....._ ___ --ft- DATE

: **--=-~f-1:---TIME ~)~** 

_

:r iesiAIMf'lca. P1ltS.buryh COK180490

Jl- ll **-J~** prlnle\luu; Tllul:ldl:f

, **~ovet•1ber** "lB. 201{) 01:04PM 57

>agP.1

•; ., J li I ., of 57
.. -4· t

# Test America THE LEADER
IN ENVIRONMENTAL TESTING 

# COK180493 

# ANALYTICAL REPORT Fonll 26R 

# Lot 

# I: COJ0.80493 MaryanDa 

# Babich 

# Equitable Productior 

# co. 225 Borth Shore 

# Dr.: .-e Pittsburgh,

PA 15212-5861 

# INC. 

# Project Manager December 15, 2010 

# TestAmerlca Laboratories, Inc. 301 

# Alpna Drive 

# Pittsburgh,
PA 15238 tel412.963

. 7058 fax412.963.2468 www.testamericainc.com 

# 1



# of 

# 14Sample Receiving: CASE NARRATIVE Equitable Production Company Lot # COK180493 TestAmerica's Pittsburgh laboratory received one sample on November 17,2010. The coolers were received within the proper temperature range. Metals: TestAmerica's

St. Louis laboratory analyzed the metals. The sample was analyzed

at a dilution for strontium due to the high concentration

of the target analyte. The reporting limit has been adjusted accordingly. Radiological Chemistry: TestAmerica's

St. Louis laboratory analyzed the gross alpha and beta. The gross Alpha Beta reporting limit was not met due to a reduction of sample size attributed

to the sample's high residual mass. The analytical results are reported. COK180493

2

of 14

# n 0



# ~ 

# 1-' <Xl 

# 0

**~** 

# \0 

# VJ

VJ



# 0 HI 

# 1-'

**~** 

# . **~T~l-~**

**.ftoc** 

# .. , .,.. ......... **T~&l)ai!Qn._ft~ld ~!Cit.CO.--**  

# ....... 

# Chain of Custody Record

**Test!~merlcaiAboratory lacatloa:_-:=:-::::---==-:-:::::=:----:=~-:::----:=~-------------**  Replatory pnanm: 

# C1 OW 

# C:=:J NPDf.S 

# I=:J RC:Ro\ 

# c::J Other
- · · · --- ··-- " ---- 

# Test America

THE LEAllP IN ti:HYIROIIMENTAL 11!8Tm0



# 5o"'''le Spedflc 

# S-1 Sp«lal IIIICI'tRI
.... ;

.; l
..

**~** 

# . .



# TAL0018

- I (04110)PARAMETERGrossAlpha/BetabyGFPCMEmODSSUMMARYCOIG.804.93ANALYTICALMETHODTraceInductivelyCoupledPlasma(ICP)MetalsSW8469310MODSWB466010CRefereuces:PREPARATIONMETHODSW846"TestMethodsforEvaluatingSolidWaste,Physical/ChemicalMethods",ThirdEdition,November1986anditsupdates.COK1804934of14SAMPLE SUMMARY COIU80493

SAMPLED SAMP WO # SAMPLE# CLIENT SAMPLE ID

.:::D:;ATB==--- TIME L98HQ **00~** HURD FLOW BACK-590398

11/17/10 11:30 m'I"B(S): - Tbc ltlllytical resuhs of lhc llll1plcs lilled above arc praemcd on Che followin& pqes. - All cak:uladons are perfonnecl belbre roundln&
to avoid round-off errors in calculated resulls. - ResuiCI no&cd as "ND" were not dcleaed

11 or above lhc Silled limic

. - ThiJ report must not be reproduced, cxapt
In CuD, wilbout !lie wrillal approval of lhe laboratory. - Resul11 for lbe followina )lii'IIIIXfelll arc 111:\'CI' l1iJIOlUd on a dry weight basis: color, conorivity, density, flubpoinr, ipillbility, layers, odor, palDt filler lesl, pH. porosity preaute, rcadivily, redox potelllial, specific aravll)', spot taas, &Oiidl. solubility, **~.** Yillcolity, and wei&bt. COK180493

5

of 14EquitableProductioneo.ClientSamplem:HURDP'LOII'BAClt-590398Lot-sample1...:COK180493-001DateSampled•••:11/17/10"l''TALMetalsDateReceived••:11/17/10REPORTINGMatrix•....••:WATERPREPARATION-WORK=.P::.:ARAME::.:..:::..::T.:.;E=R:;.___RE=S:::.;UL=T=------LIMIT__;;.;;ME=T.=.:H:.:.O::..:D=c..______ANALYSISDATEORDER#PrepBatch••••:0335204Strontium94700100ug/LSWB-166010C12/01-12/13/10L98BQ1AADilutionFactor:20AnalysisTime..:13:47MSRun#.......:0335105MDL••••••••••••:10.8Thorium510200ug/LSW8466010C12/01-12/08/10L98BQ1ADDilutionFactor:1.AnalysisTime..:15:07MSRun#.......:0335105MDL••••••••••••:35.6uraniumND500ug/LSW8466010C12/01-12/13/10L9BHQ1ACDilutionFactor:1AnalysisTime.•:12:10MSRun#.......:0335105MDL••••••••••••:23.5COK1804936of14MBiBODBLMIKRBPORT"l''TALMetalsClientLot1...:COK180493Matrix•••••••..;WATERREPORTINGPREPARATION-WORK.::..PARAME::.==..::=..T:;.:E;;;.:R;.;;..___=.::RE=-S"-UL=T;;....____LIMIT.::..ON::.:ci=..T=.::S::;...___:..:ME=T:::::HO.::..D=-------ANAI..YSISDATEORDER#MBLot-SampleI:FOLOl0000-204PrepBatch1•••:0335204StrontiumND5.0ug/LSW8466010CThoriumNDUraniumNDBOTB(S):DilutionFactor:1AnalysisTime•.:11:25200ug/LDilutionFactor:1AnalysisTime..:14:17500ug/LDilutionFactor:1AnalysisTime..:11:25Calculationsarcpcrfonnc:dbeforeroundingtoIIVOidround-offerrorsincalwlatc:dn:sulrs.COK1804937SW8466010CSW8466010C12/01-12/13/10MAN7QlAA12/01-12/08/10MAN7Q1AD12/01-12/13/10MAN7Q1ACof14lABORATORY CONTROL SAMPLB BVALUAT:IOIII REPORT T01'AL Metals Client Lot
1 ...

: COK180493

Matrix ...••....

: WATER PERCENT RECOVERY PARAMETER RECOVERY LIMITS PREPARATION- **~ME=TH~O~D~--------** ANALYSIS DATE WORK ORDER

# LCS Lot-Samplei: FOLOl0000-204 Prep Batch

1 ...

: 0335204 Strontium

106
(BO

- 120) SW846 6010C 12/01-12/13/10 MAN7Q1AB Dilution Factor:

1 Analysis Time ••

: 11•32 Uranium

102
(80

- 120) SW846 6010C 12/n1-12/13/1o MAN7Q1AF Dilution Factor:

1 Analysis Time ..
: 11:32 Thorium

102
(80

- 120) SW846 6010C 12/0l-12/08/10 MAN7Q1AG Dilution Factor:

1 Analysis Time ..

: 14:23 ROTB(S): Caleulations
are performed before roundiD&

to avoid round-off crTOI'Ii in calwlated resulls. COK180493

8

of 14Client Lot

1 •••

: COK180493 Date Sampled .••

: 11/17/10 'l'OTAL Meta1s Date Received

••

: 11/17/10 RPD Matrix •.•••••••

: WATER PREPARATION- WORK PARAMETER PERCENT RECOVERY RECOVERY LIMITS RPD LIMITS :..:ME=:::TH=O:.D _____ ANALYSIS DATE ORDER# MS Lot-Sample

I: COK180450-001 Prep Batch

t ...

: 0335204 Strontium
0.0 N (75

- 125) SW846 6010C 0.0 N (75- 125) 0.0 (0-20) SW846 6010C Thorium Uranium BOTB(S):

29 N 78 42 N 52 N, * (75

- (75

- (75

- (75

- Dilution Factor

: 500 Analysis Time •.

: 13:32 MS Run# ..•....

: 0335105 125) SW846 125) 3.7 (0-20) SW846 Dilution Factor

: 50 Analysis Time

• . : 14:54 MS Run fl. ......

: 0335105 125) SW846 125) 21 (0-20) SW846 Dilution Factor

: 50 Analysis Time ..
: 11:55 MS Run

1 •••••.•

: 0335105 Calculations are performed before roundina

to avoid round-off enon iD c:alaalaled results. N Spilced **~yre** rcamry

is ouaidc IIIIAICI comrollimils

. • Relative pcrcem diffcn:nce (RPD)
is outside Silled oonttol limit&. COK180493

9 6010C 6010C 6010C 6010C 12/01-12/13/10 L977P1AJ 12/01-12/13/10 L977P1AK 12/01-12/08/10 L977PlAN 12/01-12/08/10 L977P1AP 12/01-12/13/10 L977P1AL 12/01-12/13/10 **L977P~** of 14Equitable Production Co. Client Samcle ID: HURD FLOW BACK-590398 Radiochemistry Lab Sample ID: COK180493

- 001 Work Order: Matrix

: L9BHO WATER aaault aROSS A/B BY GFPC SW846 ,310 MOD Groea Alpha Groaa Beta NOTB(S)

49 21 Qual u u Data ara incogplate **witho~t** tha caee narrative

. KDC ia determined

by instrument performance only. Bold reaulta are greater than the MDC. Total Vr&Qart. (:Z o+/·) 40 16 u Result ia leas than the aampla dataction limit. COK180493

Date Collected: 11/17/10 1130 Date Received: 11/17/10 1620 PZ'ap RL
mdc: Data pCi/L Batcb

• 0326115 3

59 11/22/10 4

25 11/22/10 10

ADalya1a Data **Yld~** ll/23/lD 11/23/10
of 14METHOD BLANK REPORT Raaiochemistry Clie;nt Lot ID: COK180493 Matrix: WATER

To"al UD.coert. Par-ter
ae.ul" **~1**

12 (1+/-) BROSS A/8 BY 13J'PC Stf846 9310 ICOD Gross Alpha

-0

. 63

u 0.41 Gross Beta

0

. 99

u 0.67 NOTB(S) nata are 1ncooaplete without tbe caaa narrative. MDC ie determined ueing inatrument performance only Bold result• are greater than the MDC. **~** Reault ia leaa than the aample detection liait. COK180493

pCi/L

IlL Batch 3,00 4

. 00 11

Lab BIUIPla ID Prep Analy•h 1IDC Data Date • 0326115 YlcS' POJ::22000D-115B l.l ll/22/10 11/23/10 1.0 ll/22/10 11/23/10 of 14Client Lot ID: Matrix: Par .. ete:r Laboratory Control Sample Report COK180493 WATER Spike -.ant ••11111t Radiocheulistry Toul 'Dncert. (2 G+/-)

\ Ylcl

\ aec La!) s...,le JD QC Caatrol LiaiU GROSS A/8 BY OPPC SW846 9310 MOD pCi/L !1310 NOD POJt220000-115C Gross Alpha
49.4 53.4 Gross Beta
66.8 66.3 **Ba~d>** •• 0326115 NOTB(Sl MDC ie deterained

by inetrument **perfo~c•** only
5.9 5.7
1.2 l.l

108 99 ualyde Date: 11/23/10 Calculetione
are **perfo~d** before rounding
to avoid round-off error in calculeted reeulte COK180493

12

(69

- 128) (74

- 128) of 14MATRIX SPIKE RBPORT Client Lot Id: Matrix: COK180450 WATER Spike PaZ"aaeter
**A~Dolmt** GROSS A/8 BY' OI'PC SN8U 9310 MOD Gross Beta
26700 Batch

II : GROSS A/8 BY QFPC SW846 9310 MOD Gross Alpha
1!1800 Batch #: NOTB(S)

Spike •••\llt 29900 0326115 32400 0326115 Da'a are incomplete without the case narrative

. Radiochemistry
Date Sampled: Date Received: Total

Total 'D'Ilce"t. Spike SUIJile 'D'Ilce"t. 12o +/·l Ylcl. **•••~alt**

(2 0 +/-) pCi/L 9310 MOD 2500 3920 610 Analysis Date: 11/23/10 pCi/L 9310 ICOD 3800 17800 2500 Analysis Date: 11/23/10 Calculations
are performed before rounding
to avoid round

- off errors in calculated results. COK180493

13 11/17/10 ll/17/10 0C SUIPle \TLD \RBC
ID QC CODtrol t.imit8 C01tl80t50-001 97 (54-150) C01t180450-001 74 (35-150) of 14DUPLICATE EVALUATION REPORT Client Lot ID

: Matrix: ••r-t•r GROSS A/8 BY GFPC Gross Alpha Gross Beta NOTE(S) COK180493 WATER SAIIPLB hlnllt SW8t6 9310 ICOD 17800 3920 aatcb •• Total Vncart. (lcr+/-1 2500 610 0326115 Data are incomplete witbout the c••• narrative. Radiochemistry DIIPLICATII **~** nd hll\llt pCi/L 9310 ICOD lUDO t7t0 Date Sampled: 11/11/10 Date Received: 11/11/10 Total

0C: BIIIIPle ID 'lhlaa><t. 12 cr+/-1 'nd Pracieiou COitl80450-001 2700

'1 680

20 ISalUplel 0326115 (Dupl icat11

l calculation• are **perfo~4** before roundinv
to avoid round-off error in calculated reaulta COK180493

14

\RPD tRPD of 14Test America THE LEADER
IN ENVIRONMeNTAL TESTING ANAL YllCAL REPORT Ponl 26R. Lot I: COUB0503 Maryanna Babich Equitable Production Co. 225 North Shore Drive Pittsburgh.

PA 15212-5861 Chriatina

M. Jtovitch Project Manager November 30. 2010 TestAmerica Laboratories, Inc. 301 Alpha Drive Pittsburgh,
PA 15238 te14 12.963

. 7058 fax 412.963.2468 www.testamericainc.com COK180503

1

of 14Sample Receiving: CASE NARRATIVE Equitable Production Company Lot # COK 180503 TestAmerica•s Pittsburgh laboratory received one sample on November 17,2010. The coolers were received within the proper temperature range. Metals: TestAmerica•s

St. Louis laboratory performed the metals analysis. The sample was analyzed

at a dilution due to the presence of matrix interferences. The samples caused QC failure at a lesser dilution and were high in target analytes. The reporting limit has been adjusted for the dilution. The method blank had strontium detected
at a concentration between the MDL and the reporting limit. The result was flagged with
a "B, qualifier. Any sample associated with a method blank that had the same analyte detected had the result flagged with
a "J" qualifier. Radiological Chemistry: TestAmerica•s

St. Louis laboratory performed the radiological analysis. The gross alpha beta reporting limit was not met due to a reduction of sample size attributed
to the sample's high residual mass. The analytical results are reported. COK180503

2

of 14

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# TALOOII-1 (04/JO)METHODS SUMMARY C01U80503 ANALYTICAL **~PARAME~~~T~BR~--------------------------------------- ~MET~H~O~D~-------**  Gross Alpha/Beta
by GFPC Trace Inductively Coupled Plasma (ICP) Metals References:

SW846 9310 MOD SW846 6010C PREPARATION METHOD SW846 RTest Methods for Evaluating Solid waste, Physical/Chemical Methods", Third Edition, November 1986 and its updates. COK180503

4

of 14SAMPLE SUMMAilY COIU80503 WO # SAMPLE# CLIENT SAMPLE ID L9BL6 001 HURD DRILL PIT-590398 ROTB(S): • The -!Jtical rlllllls of lhl .. mptes lbllld lbove lie presenlld Dn lhe fOIIOwillg I'll"· • All calcullliDns .,.. perfDrmed WfDre 111111ding
to **m~kii'DIIIIIkllf** .rnn In Cllculllild r.dls. • Resulll **~a** "NO"

- nD1 dlleclld

a Dr _,.llle Slllld llml. • This rwpDit must IIIII b. nprDCiuced, excaptln full, wiiiiOd .._ wrilltn •prcMI vf lhiiiiiOniDry. • Resulh far lhl follvlrlng penme111$ are- reported Dill 11y 111119t 111511: color, wnosfvily, •nsiry, fllllllpDinl. igniltblllty, IIY«$. Odlr. palM fi .. lnl, pH, pDIOiily preaure. ,_.lvlty, ndDX polelllial, spedflc gnvily, spDtle'IU, sOlids, solulllllly, tllllpenllft, v'-hy, IIIII Wllgllt. COK180503

5
SAMPLED SAMP ""DA::..::..::T=E __ TIME ll/17 /10 1l: 30 of 14Equitable Producticm Co. Client Sample ID: HURD DRILL PrT-590398 Lot-Sample

1 ..•

: COK180503-001 Date Sampled •••

: 11/17/10 TOTAL Metals Date Received

.•

: 11/17/10 Matrix .••••.•

: WATER REPORTING PREPARATION- WORK **~PARAME~~~T~E:R~---- ~RE==SUL~T~-----**  LIMIT **~UN~I~T~S~--- ME~T~H~O~D~---------**  ANALYSIS DATE ORDER

# Prep Batch

1 ...

: 0326259 Strontium 4130

J Thorium

ND Uranium

ND NOTB(S): COK180503

50.0 ug/L Dilution Factor

: 10 MDL .. .. ..

. ... ..

: 5.4 10000 ug/L Dilution Factor:
so MDL ••
• .•••

• ••••

: 1780 5000 ug/L Dilut

i on Factor

: 10 MDL ••
• •••

• ••••

. : 235
6 SW846 6010C 11/22-11/25/10 L98L61AA Analysis Titne

. . : 12

: 19 MS Run#
.. •....

: 0326175 SW846 6010C ll/22-11/29/10 L98L61AD Analysis Time

. . : 14

: 08 **~s** Run w
. . ..

. . . : 0326175 SW846 6010C 11/22-11/25/10 L98L61AC Analysis Time

. . : 12:19
MS Run# ......•

: 0326175 of 14TOTAL Metals Client Lot

1 •••

: COK180503

Matrix ...••••••

: WATER REPORTING PREPARATION- WORK =.P;:.;:ARAME='-=T:::..:E=R:.:.--- :.:R::E:.SU.:.:L:.T;;.... ___ =L;:IM;..:;I=.;T=--- **-=UN=IT:.:S~--** :..:ME=TH:::O.:;D:._ _____ ANALYSIS DATE ORDER

# MB Lot-Saaple

I: FOK220000-259 Prep Batch# ...

: 0326259 Strontium

1.6 B 5.0 ug/L SW846 6010C Thorium

ND Uranium

ND ROTB(S):
Dilution Factor:

1 Analysis Time ..
: 12:47 200 ug/L Dilution Factor:

1 Analysis Time ..
: 12:47 500 ug/L Dilution Factor:

1 Analysis Time ..
: 10:42 Calculltlons .,.. performed llefo,. rvundlng

10 avolll round-off errvn
In celcullled resulls. B EstiiNIId mulL Rnullls less thin RL. COK180503

SW846 6010C SW846 6010C 7 11/22-11/29/10 **~1AA** 11/22-11/29/10 MAEF31AD 11/22-11/25/10 MAEF31AC of 14Client Lot

t ...

: COK180503 PARAMETER PERCENT RECOVERY RECOVERY LIMITS 'l'Ol"AL Metals Matrix •.•.•...•

: WATER PRBPARATION- ;:..;M;;;;E.;;.TH;.;;O.;;.;D;;;._ _____ ANALYSIS DATE WORK ORDER

# LCS Lot-Bamplel: FOK220000-259 Prep Batch

1 •.•

: 0326259 Strontium

103
(80

- 120) SW846 6010C 11/22-11/29/10 MAEF31AE Dilution Factor:

1 Analysis **Ti~** ..

: 12:53 Uranium

102
(80

- 120) SW846 6010C 11/22-11/25/10 MAEF31AF Dilution Factor:

1 Analysis Time ..

: 10:50 Thorium

116
(80

- 120) SW846 6010C 11/22-11/29/10 MAEF31AG Dilution Factor:

1 Analysis **Ti~e** ..

: 12:53 ROTB(S): COK180503

8

of 14MTIUX SPID SAMPLB BVALUATIOR REPORT Client Lot

t ...

: COK180503 Date Sampled .••

: 11/17/10 PERCENT RECOVERY "l''TAL Metals Date Received

••

: 11/17/10 RPD Matrix ..••••...

: WATER PREPARATION- WORK PARAMETER RECOVERY LIMITS RPD LIMITS ;;.:ME=T;;.:;HO""'D;;._ _____ ANALYSIS DATE ORDER

# NS Lot-Sample

1: COK180474-001 Prep Batch# ..•

: 0326259 Strontium 24900
N (75

- 125) SW846 6010C 35300
N (75

- 125) 7.6 (0-20) SW846 6010C Thorium Uranium NOTB(S):
597 N 555 N 41 N 55 N,* (75

- (75
- (75

- (75

- Dilution Factor: 500 Analysis Time ..
: 13:12 MS Run

1 •. •.• ••

: 0326175 125) SW846 125) 4.8 (0-20) SW846 Dilution Factor:
50 Analysis Time ..
: 13:56 MS Run
II •••••••

: 0326175 125) 125) 28 (0-20) Dilution Pactor:
10 Analysis Time.,: 12:04 SW846 SW846 MS Run M

. .. .. ..
: 0326175 C•lcullllklns 1re perfor,.d Wore rounding
to IIVOicl rvund4ff ''""' In Clleullllld results. N Spiked .. ,_ .._.y

is -• IWted conlrlll lillllts. • RelltiYt ..-- dllflnnce (RPO)
Is OUISidt lllllld CMrDI limlll.

• COK180503

9 6010C 6010C 6010C 6010C 11/22-11/29/10 L98DQ1AF 11/22-11/29/10 L98DQ1AG 11/22-11/29/10 L98DQ1AK 11/22-11/29/10 L98DQ1AL 11/22-11/25/10 L98DQ1AH 11/22-11/25/10 L98DQ1AJ
of 14Equitable Production Co. Client Samole ID: HURD DRILL PIT-590398 Radiochemistry La.b Sample ID: COK180503-001 Work Order: Matrix: L98L6 WATER aeault: GROSS A/B BY GFPC SW846 9310 MOD Grose Alpha **G~o••** Beta NOTB(S)

80 170
QUal u Data are incomplete without tbe c••• narrative. MDC ia determined
by **inat~ent** performance only. Bold result• are greater tban the MDC. Total IIDOert:. (2 rs+/·1 uo 7!1 U Result is less than the aaaple detection limit. COK180503

Date Collected: 11/17/10 1130 Date Received

: 11/17/10 1620 PritP RL
lick: Date pCi/L Batch

i 0326115 3
220 11/22/10 4
110 11/22/10 10

ualyah Data YlcS

\ 11/23/10 11/23/10
of 14METHOD BLANE REPORT Radiochemistry Client Lot ID: COK180503 Matrix: WATER

Total Uacert. Par ... ter llaav1t Qllal

(2 ,..,., GROSS A/B BY OFPC SWIU !1310 ICOD Grosa Alpha

-0

. 63

u 0.41 Groll& Beta
0.99

u 0.67 MOTB(S) Data are incoaplete witbovt the caae narrative. MDC ie determined uaing instrument performance only sold reeulta are greater than the HOC, 0 Reault ia lea& than the sample detection limit. COK180503

pCi/L

RL Batch 3.00 4.00 11

Le.b **IU~Ple** ID Prep AAalyah III)C
Date U.te • 0326115 Yl6\ **POJt:Z20000~115B** 1.1 11/22/10 11/23/10 1.0 11/22/10 11/23/10 of 14Client Lot ID: Matrix: COK180503 WATER Laboratory Control Sample Report Radiochemistry 'l'ata1

LUI lulple m ODc•rt.

QC Ccmtn1 Spika Aao\mt ltell\llt

(2 rs+/-1 IG)C

' T14

' .. ., Lia!U Par-ter GROSS A/8 BY GFPC SW846 9310 MOD pCi/L 9310 MOD l"Olt220000-115C Gross Alpha
49.4 53.4

5

. 9

1

. 2

108 (69

- 1281 Gross Beta
66.8 66.3

5.7

1.1

99
(74

- 128) Batcll I• 0326115
Aaa1y•1• Date• 11/23/10 NOTBCS) MDC 1• 4etar.Dine4
by in•truaent p•rformauce only Calculation•
are performed before rounding
to avoid round-off error in calculated re•ult• COK180503

12

of 14MATRIX SPIKB RBPORT Client Lot Id: Matrix: COK180450 WATER Par-tar

Spike "-nnnt GROSS A/B BY GFPC SW846 9310 IIOD Gross Beta 26700 Batch #: GROSS A/B BY GFPC SW846 9310 IIOD Gross Alpha
19800 Batch #: ROTE (S)

Spike Jlaault 29900 0326115 .32400 0326115 Data are 1ncomplete w1thout the case narrative. Radiochemistry
Date Sampled: Date Received: Total

Total 'DIIcaz:t. SpUta 811115'1• thloart. (2o +/-) Yld. Ra•ult

(2 0 +/-) pCi/L 9310 IIOD 2500 3920 610 And reb Date

: 11/23/10 pCi/L UlO JIOD 3800 17800 2500 Analysis Date: 11/23/10 Calculations
are performed before rounding
to avoid round

- off errors

i n calculated results. COK180503

13 11/17/10 11/17/10 oc eaple \YLI) \DC
ID
/ QC Control Limita COitl80UO-OOl 97 (54-150) C01tl80U0-001 74 (35-150) of 14DUPLICATE EVALUATION RBPORT Client Lot ID: Matrix: Par-car GROSS A/8 BY GPPC Gross Alpha Gross Beta NOTB(S) COK180503 WATER lAIII' .. Re•ult SWB46 9310 MOD 17800 :U20 llatc:b I• Total Oneut. (2G •/-) 2500 no 0326115 D•ta are lnca.plete without the ca•• narrative. Radiochemilltry DVl'LlCAD \ Yld •••lllt pCi/L 9310 IIOD 15600 nto Date Sampled: 11/17/10 Date Received: 11/17/10 Total

OC Suopla ID Vncert. (2 fl+/-)

\ Yld Preci•lon CODB04S0-001 2700

7 680

20 (Sample) 0326115 (Duplicate) Calculation•
are **perfo~d** before roUDdiug
to avoid round-off error lD calculated reaults COK180503

14

UPD \RPD of 142540-PM·BWM0347
Rev. 1/2011 c **e!'!,'!~!l.!!..** COMMONWEALTH

OF PENNSYLVANIA DEPARTMENT
OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM 26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERATOR This form must be fully and accurately completed.
All required Information must be typed or legibly printed
In the spaces provided.

If additional space
Is necessary, Identify each attached sheet as Form 26R, reference the Item number and Identify the date prepared. The date on attached sheets needs to match the date noted below. General Reference 287.54 Date Prepared/Revised
2/24/11 c. Physical Appearance Number of Solid or Liquid Phases of Separation
Date Received

& General Notes Describe each phase of separation. -- ----- ---- ------

---l - 1 -2540-PM-BWM0347Rev.1/2011a.manthewaste,asspecifiedIntheInstructions,Isattached.AddressLine1AddressLine1AddressCityStateZIPMunicipalityc.FacilityContactNameTitlePhoned.Volumeofwasteshippedtoprocessingor785,0250cuydgalEmailAddress.olba.wastepermitWVR000521948processingordisposalfacilitybeingc.AddressLine1AddressLine1AddressCityStateZIPMunicipality(checkone)Delawared.Volume743,435wasteshippedtoprocessingordisposalfacilityInthepreviousyear.0cuydgal0lb0ton(checkone)0ton(checkone)-2-2540

· PM·BWM0347 Rev. 112011 b.
A schematic
of the as specified

In the Instructions,

Is attached. c.

If portions of the

are a confidentiality claim, as described

In the Instructions,

Is attached. b. Facility Name c. d. a. c. Address Line
1 Address Line
1 Address City State ZIP Municipality Volume of waste shipped 90,000 Facility Name Address Line
1 Address Line
1 Address City State ZIP Municipality

Email Address Energy Email Address D ton -2

-

No georgem@shallenbergerconstruction.c om (check one} (check one}2540-PM-BWM0347 Rev.1/2011 A detailed description the waste, as specified

In the Instructions,

Is attached. b.
A schematic
of as specified

In the Instructions,

Is attached. c.

If

are
the substantiation
for a confidentiality claim, as described

In the Instructions,

Is attached. b. Facility Name c. d. Address Line
1 Address Line

1 Address City State ZIP Municipality me of waste shipped to processing

or Email Address facility in the previous year. 4,200

D cu yd 181 gal D lb D ton (check one) a. Solid PA0095443 b. Facility Name Address Line
1 Address Line
1 Address City State ZIP Municipality c. Facility Contact Name Title Volume of waste echnologies Indiana D ton (check one) - 2 -

No No2540-PM-BWM0347 Rev.1/2011 a. the waste, as spec

i fied In the Instructions,

Is attached. b.

man
control processes as specified

In the Instructions,

Is attached. c.

are
the substantiation a confidentiality claim

, as described

In the Instructions

, Is attached. The area below (a.-c:l.) will accommodate
the Identification

of two facilities. Attach additional sheets

If necessary. a. c. c. waste permit number(s) PA0095273 Address Line
1 Address Line

1 Address City State ZIP Municipality Facility Name Title Phone Address Line
1 Address Line
1 Address City State ZIP Municipality Title Phone Name

or disposal utilized. Indiana (check one) Tri County Waste Management Email Address D gal

0 ton (check one) - 2 -

No2540-PM-BWM0347 Rev.1/2011 a.

pollution control processes pn;IUu'IOmly the waste, as specified

in the Instructions,

Is attached. A
the manufacturing and/or pollution control processes producing the waste, as specified

In the Instructions,

Is attached. c.

If portions Information
su are

for a confidentiality claim, as described

In the Instructions,

Is attached. The area below {a.-d.) will accommodate
the Identification

of two facilities. Attach additional sheets
If necessary. a. Solid permit number{s}

or a•&IIXJII

' il' 31-121-2-4037 c. c. Address Line
1 Address Line
1 Address City State ZIP Municipality Address Line
1 Address Line
1 Address City State ZIP Municipality Tunnelton Liquids Company County karnold@triadhunter
.com (check one) Email Address tlcbufalini@hotmail.com 0 ton (check one) -2-

N/A2540-PM-BWM0347Rev.1/2011c.asspecifiedIntheInstructions,Isattached.submittedareconfidential,thesubstantiationforaconfidentialityclaim,asdescribedIntheInstructions,Isattached.Theareabelow(a.-d.)willaccommodatetheIdentificationoftwofacilities.AttachadditionalsheetsIfnecessary.a.wastepermitnumber(s)forprocessingordisposal47-085-05051AddressLine1AddressLine1AddressCityStateZIPMunicipalityc.FacilityContactNameTitleCountyltyinthepreviousyear.DlbDton(checkone)a.Solidwastepermitnumber(s)forprocessingor9395AddressLine1AddressLine1AddressCityStateZIPMunicipalityc.FacilityContactNameTitleIf"Yes",listthegeneralpermitnumberorapprovalnumber.Volumeofwastebeneficiallyusedintheyear.DcuydDgalDlb-2-Muskingum(checkone)Dton(checkone)N/A2540.PM-BWM0347Rev.1/2011Icertify,underpenaltyoflaw,thatIhavepersonallyexaminedandamfamiliarwiththeInformationsubmittedInthisAnnualReportandallattacheddocumentsandthatbaseduponmyInquiryofthoseIndividualsImmediatelyresponsibleforobtainingtheInformation,IverifythatthesubmittedInformationIstrue,accurateandcompletetothebestofmyknowledge.IunderstandthatthesubmissionoffalseInformationhereinIsmadesubjecttothepenaltiesof18Pa.C.S.§4904,relatingtounswornfalsificationtoauthorities,whichIncludefineandImprisonment.Checkthefollowing,Ifapplicable:181IcertifytheInformationrequiredInSectionB-1,GeneralPropertieswassuppliedtotheDepartmentfortheyear2010andhasnotchanged.FormSubmitted:DForm26R0Other(specify)DateSubmitted:181IcertifytheInformationrequiredInSectionB-2,ChemicalAnalysiswassuppliedtotheDepartmentfortheyear2010andhasnotchanged.FormSubmitted:181Form26R0Other(specify)DateSubmitted:181IcertifytheInformationrequiredInSectionB-3,ProcessDescriptionandSchematic,wassuppliedtotheDepartmentfortheandhasnotchanged.FormSubmitted:181Form26R0Other(specify)DateSubmitted:NameofResponsibleOfficialTitleSuerintendentWaterManaementJ.MichaelBaranDate2/24/2011- 3 -