### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #1 7/7/2009 ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #2 7/7/2009 ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #3 7/8/2009 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/8/2006 60 1.00 15.5 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 1 9/9/2009 240 4.00 4.22 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 2 9/9/2009 240 4.00 4.9 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 3 9/10/2009 240 4.00 4.39 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 8/7/1997 120 2.00 6.7 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 8/7/1997 120 2.00 6.4 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 8/7/1997 120 2.00 6.4 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 12/5/2002 60 1.00 8.07 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 12/5/2002 60 1.00 7.84 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 12/5/2002 60 1.00 7.84 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #17/22/2009 240 4.00 9.18 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #27/23/2009 240 4.00 9.23 ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 7/23/2009 240 4.00 9.33 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/20/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/20/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/20/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #111/24/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #211/24/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #311/24/1998 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #111/22/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #211/22/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #311/22/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #411/22/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/1/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/1/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/1/1999 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #111/20/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #211/20/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #311/20/2001 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/2/2002 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/2/2002 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/2/2002 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2004 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2004 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2004 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/21/2005 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/21/2005 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/21/2005 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2006 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #112/19/2007 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #212/19/2007 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #312/19/2007 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #112/22/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #212/22/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #312/22/2009 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2010 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2010 FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2010 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/8/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/8/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/8/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #112/17/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #212/17/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #312/17/1999 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/31/2000 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/31/2000 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/31/2000 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2001 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2001 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/6/2001 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/9/2002 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/9/2002 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/9/2002 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #111/15/2002

Page 1 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #211/15/2002 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #311/15/2002 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #112/30/2003 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #212/30/2003 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #312/30/2003 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/4/2005 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/4/2005 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/4/2005 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2006 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2006 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/5/2006 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/25/2007 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/25/2007 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/25/2007 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/24/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/24/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/24/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/4/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/4/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/4/2008 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #111/20/2009 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #211/20/2009 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #311/20/2009 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/4/2010 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/4/2010 FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/4/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #13/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #13/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 6/2/2006 60 1.00 7.58 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 6/2/2006 60 1.00 7.99 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 6/2/2006 60 1.00 9.22 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 6/2/2006 60 1.00 9.84 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #5 6/2/2006 60 1.00 9.1 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #18/22/2006 64 1.07 10.36 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #28/22/2006 64 1.07 10.43 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #38/22/2006 64 1.07 10.3 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 39083 60 1.00 6.52 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 39083 60 1.00 6.96 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 39083 60 1.00 6.53 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/5/2007 60 1.00 7.73 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/5/2007 60 1.00 7.65 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/5/2007 60 1.00 7.25 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #111/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #211/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #311/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #112/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #212/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #312/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #412/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/2/2009 60 1.00 6.4 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/2/2009 60 1.00 7 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/3/2009 60 1.00 5.6 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #111/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #211/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #311/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/2/2010 GATempleInlandRome WF Biomass FB 1 7/27/2009 GATempleInlandRome WF Biomass FB 2 7/28/2009 GATempleInlandRome WF Biomass FB 3 7/28/2009 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #14/18/1994 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #24/18/1994 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #34/18/1994 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #15/22/1995 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 5/22/1995 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 5/22/1995 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #19/11/1997 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #29/11/1997 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #39/11/1997 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #17/12/2000 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #27/12/2000 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/12/2000 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #19/25/2003 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #29/25/2003

Page 2 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #39/25/2003 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #110/07/2004 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #210/07/2004 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #310/07/2004 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #14/11/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #24/11/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #34/11/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #14/12/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #24/12/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #34/12/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #44/12/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #54/12/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #64/13/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #74/13/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #84/13/2005 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #17/16/2007 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #27/17/2007 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/17/2007 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #18/23/2010 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #28/23/2010 HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #38/23/2010 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #14/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #24/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #34/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #17/28/2009 240 4.00 13.2 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #27/28/2009 240 4.00 13.8 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 7/29/2009 240 4.00 13 MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #112/20/2006 MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #212/20/2006 MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #312/20/2006 MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #1 8/1/2007 MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #2 8/1/2007 MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #3 8/1/2007 MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #1 8/1/2007 MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #2 8/1/2007 MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #3 8/1/2007 MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #1 8/1/2007 MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #2 8/1/2007 MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #3 8/1/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #18/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #28/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #38/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #17/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #27/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 7/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 6/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 6/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 6/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #18/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #28/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #38/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/5/2009 180 3.00 8.06 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/5/2009 180 3.00 7.25 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/5/2009 180 3.00 7.63 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #1 6/18/2008 60 1.00 9.7 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #2 6/18/2008 60 1.00 9.48 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #3 6/18/2008 60 1.00 9.43 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #13/22/2006 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #2 3/22/2006 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #3 3/22/2006 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/6/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/6/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/6/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/7/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/7/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/7/2005 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 8/4/2009 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 8/4/2009 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 8/5/2009 TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #1 1/13/2009 TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #2 1/13/2009 TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #3 1/13/2009 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #19/18/1996 120 2.00 10.7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #29/18/1996 120 2.00 10.6

Page 3 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #39/18/1996 120 2.00 9.4 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #111/10/2004 60 1.00 9.5 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #211/10/2004 60 1.00 9.3 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #311/10/2004 60 1.00 8.7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #18/11/2009 240 4.00 7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #28/11/2009 240 4.00 7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #38/12/2009 240 4.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #19/19/2007 60 1.00 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #29/19/2007 60 1.00 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #39/19/2007 60 1.00 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #18/20/2009 240 4.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #28/20/2009 240 4.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #38/21/2009 240 4.00 7 WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #17/11/2006 WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #27/11/2006 WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #3 7/11/2006 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2011 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2011 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2011 ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2006 ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2006 ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2006 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #18/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #28/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #38/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #111/21/1998 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #211/21/1998 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #311/21/1998 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #112/10/1999 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #212/10/1999 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #312/10/1999 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 11/9/2000 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 11/9/2000 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 11/9/2000 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/5/2001 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/5/2001 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/5/2001 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2002 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2002 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2002 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2003 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2003 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2003 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #19/29/2004 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #29/29/2004 ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #39/29/2004 CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 3/5/2008 CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 3/5/2008 CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 3/5/2008 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 37773 120 2.00 9.78 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 37773 120 2.00 9.55 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 37773 120 2.00 7.91 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #110/14/2004 60 1.00 8.82 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #210/14/2004 60 1.00 8.76 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #310/14/2004 60 1.00 9.06 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/15/2006 60 1.00 7.75 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/15/2006 60 1.00 8.13 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/15/2006 60 1.00 8.46 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/2006

Page 4 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/18/2007 60 1.00 7.35 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/18/2007 60 1.00 6.6 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/18/2007 60 1.00 7.51 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/11/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/12/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/12/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/27/2009 240 4.00 8.88 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/27/2009 240 4.00 8.21 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/27/2009 240 4.00 7.21 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/27/2009 GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #1 2/27/2008 GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #2 2/27/2008 GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #3 2/27/2008 IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/1/2008 IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/1/2008 IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/1/2008 IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #14/24/2003 60 1.00 8 IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #24/24/2003 60 1.00 8 IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #34/24/2003 60 1.00 8 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #15/31/2002 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/31/2002 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/31/2002 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #15/29/2007 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/29/2007 LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/29/2007 MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #110/21/2009 55.6 0.93 6.3 MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #210/21/2009 61.3 1.02 5.9 MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #310/21/2009 63.5 1.06 5.9 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #17/12/2006 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #27/12/2006 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/12/2006 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/22/2010 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/23/2010 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/23/2010 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/28/2010 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/29/2010 MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/30/2010 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/19/1993 90 1.50 7.1 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/19/1993 90 1.50 7.1 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/19/1993 90 1.50 7.5 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/16/1995 120 2.00 8.3 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/16/1995 120 2.00 7.1 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/16/1995 120 2.00 6.3 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/13/1997 125 2.08 3.6 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/13/1997 125 2.08 3.3 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/13/1997 125 2.08 3.1 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/1999 125 2.08 6.5 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/1999 125 2.08 6.3 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/1999 125 2.08 6.1 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/5/2003 125 2.08 8.7 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/5/2003 125 2.08 8.3 SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/5/2003 125 2.08 8.4 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #17/14/2009 180 3.00 9.74 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #27/14/2009 180 3.00 9.38 SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/14/2009 180 3.00 9.11 WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #18/29/2007 60 1.00 7 WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #28/29/2007 60 1.00 7 WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #38/29/2007 60 1.00 7 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #13/24/2005 120 2.00 7.8 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #2 3/24/2005 120 2.00 8.1 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #3 3/24/2005 120 2.00 8.4 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #43/24/2005 120 2.00 7.3 AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #18/17/2005 60 1.00 7 AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #28/17/2005 60 1.00 6.67 AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #38/17/2005 60 1.00 6.6 AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #18/16/2005 60 1.00 7.6 AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #28/16/2005 60 1.00 7.93

Page 5 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #38/16/2005 60 1.00 8 FLSmurfit-Stone 7PB Coal PC Sample #17/11/2007 60 1.00 7.05 FLSmurfit-Stone 7PB Coal PC Sample #27/11/2007 60 1.00 7.29 FLSmurfit-Stone 7PB Coal PC Sample #3 7/11/2007 60 1.00 7.41 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 6/3/2008 100 1.67 6.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #18/26/2009 240 4.00 5.58 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #28/26/2009 240 4.00 5.56 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #38/27/2009 240 4.00 5.66 IAIAStateUnivPowerPlant B1 Coal FB Sample #13/26/2008 62.5 1.04 4.3 IAIAStateUnivPowerPlant B1 Coal FB Sample #2 3/26/2008 62.5 1.04 3.9 IAIAStateUnivPowerPlant B1 Coal FB Sample #3 3/26/2008 62.5 1.04 4.4 IAIAStateUnivPowerPlant B2 Coal FB Sample #13/27/2008 62.5 1.04 4 IAIAStateUnivPowerPlant B2 Coal FB Sample #2 3/27/2008 62.5 1.04 3.9 IAIAStateUnivPowerPlant B2 Coal FB Sample #3 3/27/2008 62.5 1.04 3.7 IAUofNorthernIowa Boiler #3 Coal PC 4 10/6/2009 IAUofNorthernIowa Boiler #3 Coal PC 5 10/6/2009 IAUofNorthernIowa Boiler #3 Coal PC 6 10/7/2009 IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #19/26/2006 120 2.00 6.9 IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #29/26/2006 120 2.00 6.9 IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #39/26/2006 120 2.00 6 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #18/22/2007 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #28/22/2007 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #38/22/2007 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-1 8/4/2009 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-2 8/5/2009 ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-3 8/5/2009 ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #13/13/2007 ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #2 3/13/2007 ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #3 3/13/2007 INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #18/26/2009 INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #28/26/2009 INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #38/27/2009 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 6/28/2006 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 6/28/2006 INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 6/28/2006 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 6/28/2006 125 2.08 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 6/28/2006 125 2.08 INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 6/28/2006 125 2.08 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #110/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #210/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #310/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/2/2005 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/2/2005 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/2/2005 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/3/2005 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/3/2005 MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/3/2005 NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008 NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008 NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008 NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008 NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008 NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008 NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008 NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008 NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008 NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #13/21/2007 NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007 NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007 NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #13/21/2007 NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007 NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007 OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #18/21/2007 OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #28/21/2007 OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #38/21/2007 OHSmartPapersHoldingsLLC B010 Coal PC Sample #18/11/2005 120 2.00 7.9 OHSmartPapersHoldingsLLC B010 Coal PC Sample #28/11/2005 120 2.00 7.8 OHSmartPapersHoldingsLLC B010 Coal PC Sample #38/11/2005 120 2.00 7.8 OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #19/22/2005 OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #29/22/2005 OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #39/22/2005 OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #34/27/2005

Page 6 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #14/26/2006 OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #24/26/2006 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #110/24/2000 60 1.00 6 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #210/24/2000 60 1.00 6.1 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #310/24/2000 60 1.00 5.9 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/9/2002 60 1.00 6.1 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/9/2002 60 1.00 3.1 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/9/2002 60 1.00 5.8 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #110/19/2004 60 1.00 5.6 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #210/19/2004 60 1.00 5.9 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #310/19/2004 60 1.00 5.4 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #110/25/2006 60 1.00 3.2 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #210/25/2006 60 1.00 3.6 SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #310/25/2006 60 1.00 3.8 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #17/17/2007 60 1.00 12.4 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #27/17/2007 60 1.00 12.2 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #3 7/17/2007 60 1.00 11.9 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 8/5/2009 240 4.00 10.84 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 8/6/2009 240 4.00 10.25 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 240 4.00 10.31 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #18/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #28/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #38/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 6/29/2004 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 6/29/2004 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 11/9/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 11/9/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #111/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #211/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #311/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #311/11/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #17/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #27/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 7/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #17/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #27/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 7/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #19/30/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #29/30/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #39/30/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #18/14/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #28/14/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #38/14/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 6/21/2005 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 6/21/2005 TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 6/21/2005 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #17/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #27/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 7/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #19/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #29/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #39/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #18/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #28/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #38/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #13/10/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/10/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/10/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #15/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 5/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 5/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #17/29/1994 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #27/29/1994 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/29/1994 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 7/7/1998 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 7/7/1998 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/7/1998 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 6/6/2002 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 6/6/2002 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 6/6/2002 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #18/22/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #28/22/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #38/22/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 11/8/1994 75 1.25 7

Page 7 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 11/8/1994 75 1.25 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 11/8/1994 75 1.25 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #19/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #29/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #39/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #19/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #29/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #39/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Coal PC 1 8/26/2009 TNEastman_NO_CBIDATA Boiler 30 Coal PC 2 8/27/2009 TNEastman_NO_CBIDATA Boiler 30 Coal PC 3 8/27/2009 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #112/14/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #212/15/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #312/15/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #19/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #29/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #39/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #17/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #27/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 7/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #18/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #28/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #38/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 12/6/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 12/6/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 12/6/2006 125 2.08 7 VADukeEnergyNarrows Boiler #2 Coal PC Sample #110/12/2004 VADukeEnergyNarrows Boiler #2 Coal PC Sample #110/12/2004 VADukeEnergyNarrows Boiler #2 Coal PC Sample #210/12/2004 VADukeEnergyNarrows Boiler #2 Coal PC Sample #210/12/2004 VADukeEnergyNarrows Boiler #2 Coal PC Sample #310/12/2004 VADukeEnergyNarrows Boiler #2 Coal PC Sample #310/12/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #14/14/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #24/14/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #34/14/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #110/14/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #210/14/2004 VADukeEnergyNarrows Boiler #3 Coal PC Sample #310/14/2004 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 2/3/2004 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 2/3/2004 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 2/3/2004 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #15/24/2005 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/24/2005 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/24/2005 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #17/13/2006 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #27/13/2006 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 7/13/2006 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 5/1/2007 120 2.00 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/1/2007 120 2.00 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/1/2007 120 2.00 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 9/9/2008 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 9/9/2008 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 9/9/2008 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #13/30/2009 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 3/30/2009 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 3/30/2009 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 4/8/2009 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 4/8/2009 VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 4/8/2009 VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #1 4/4/2008 60 1.00 6.8 VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #2 4/4/2008 60 1.00 7.5 VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #3 4/4/2008 60 1.00 8.5 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #1 12/6/2007 60 1.00 7.07 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #2 12/6/2007 60 1.00 7.09 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #3 12/6/2007 60 1.00 6.98 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-1 9/17/2009 240 4.00 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-2 9/17/2009 240 4.00 VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-3 9/18/2009 240 4.00 VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #1 1/16/2007 60 1.00 6.64 VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #2 1/16/2007 60 1.00 6.96 VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #3 1/16/2007 60 1.00 6.74 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #110/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #210/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #310/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #19/24/1994 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #29/24/1994 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #39/24/1994 120 2.00

Page 8 of 9

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #17/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #27/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 11/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 11/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 11/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #17/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #27/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #18/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #28/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #38/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #18/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #28/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #38/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #18/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #28/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #38/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #19/21/2007 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #29/21/2007 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #39/21/2007 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #19/12/2007 60 1.00 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #29/12/2007 60 1.00 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #39/12/2007 60 1.00 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 1 9/22/2009 240 4.00 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 2 9/22/2009 240 4.00 WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 3 9/23/2009 240 4.00 WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00 WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00 WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00 WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #17/24/2007 60 1.00 WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #27/24/2007 60 1.00 WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #3 7/24/2007 60 1.00 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009 NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-1 8/19/2009 NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-2 8/19/2009 NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-3 8/19/2009 PABoeingRidleyPark 033 Heavy Liquid N/A M29-1 9/22/2009 PABoeingRidleyPark 033 Heavy Liquid N/A M29-2 9/23/2009 PABoeingRidleyPark 033 Heavy Liquid N/A M29-3 9/24/2009 SCMilliken-Dewey D30 Heavy Liquid N/A Sample #18/12/2009 180 3.00 3.83 SCMilliken-Dewey D30 Heavy Liquid N/A Sample #28/12/2009 180 3.00 4.02 SCMilliken-Dewey D30 Heavy Liquid N/A Sample #38/12/2009 180 3.00 3.96 ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #1 1/24/2001 ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #2 1/24/2001 ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #3 1/24/2001 SCGPChemRussellville FO Boiler Light Liquid N/A Sample #18/26/2009 120 2.00 8.06 SCGPChemRussellville FO Boiler Light Liquid N/A Sample #28/26/2009 120 2.00 7.26 SCGPChemRussellville FO Boiler Light Liquid N/A Sample #38/26/2009 120 2.00 7.31 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 1 11/17/2009 216 3.60 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 2 11/17/2009 216 3.60 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 3 11/18/2009 216 3.60 HITesoro SG1102 Non-Continental Liquid N/A Sample #1 10/9/2010 60 1.00 4.89 HITesoro SG1102 Non-Continental Liquid N/A Sample #2 10/9/2010 60 1.00 5.19 HITesoro SG1102 Non-Continental Liquid N/A Sample #3 10/9/2010 60 1.00 5.29 HITesoro SG1102 Non-Continental Liquid N/A Sample #112/13/2010 192 3.20 6.3 HITesoro SG1102 Non-Continental Liquid N/A Sample #212/13/2010 192 3.20 6.42 HITesoro SG1102 Non-Continental Liquid N/A Sample #312/13/2010 192 3.20 6.77 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #110/19/2009 240 4.00 4.5 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #210/19/2009 240 4.00 4.7 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #310/20/2009 240 4.00 4.8

Page 9 of 9

### Appendix C-2: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for New Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/8/2006 60 1.00 15.5 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 1 9/9/2009 240 4.00 4.22 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 2 9/9/2009 240 4.00 4.9 ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 3 9/10/2009 240 4.00 4.39 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #13/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/24/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #13/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/26/2005 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/10/2006 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 6/2/2006 60 1.00 7.58 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 6/2/2006 60 1.00 7.99 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 6/2/2006 60 1.00 9.22 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 6/2/2006 60 1.00 9.84 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #5 6/2/2006 60 1.00 9.1 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #18/22/2006 64 1.07 10.36 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #28/22/2006 64 1.07 10.43 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #38/22/2006 64 1.07 10.3 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 39083 60 1.00 6.52 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 39083 60 1.00 6.96 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 39083 60 1.00 6.53 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/5/2007 60 1.00 7.73 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/5/2007 60 1.00 7.65 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/5/2007 60 1.00 7.25 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #111/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #211/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #311/30/2007 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #112/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #212/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #312/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #412/11/2008 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/2/2009 60 1.00 6.4 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/2/2009 60 1.00 7 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/3/2009 60 1.00 5.6 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #111/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #211/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #311/30/2010 FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/2/2010 GATempleInlandRome WF Biomass FB 1 7/27/2009 204 3.40 5.1 GATempleInlandRome WF Biomass FB 2 7/28/2009 204 3.40 5 GATempleInlandRome WF Biomass FB 3 7/28/2009 204 3.40 5.2 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #14/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #24/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #34/30/2008 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #17/28/2009 240 4.00 13.2 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #27/28/2009 240 4.00 13.8 IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 7/29/2009 240 4.00 13 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #1 6/18/2008 60 1.00 9.7 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #2 6/18/2008 60 1.00 9.48 OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #3 6/18/2008 60 1.00 9.43 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 37773 120 2.00 9.78 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 37773 120 2.00 9.55 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 37773 120 2.00 7.91 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #110/14/2004 60 1.00 8.82 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #210/14/2004 60 1.00 8.76 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #310/14/2004 60 1.00 9.06 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/15/2006 60 1.00 7.75 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/15/2006 60 1.00 8.13 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/15/2006 60 1.00 8.46 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/18/2007 60 1.00 7.35 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/18/2007 60 1.00 6.6 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/18/2007 60 1.00 7.51 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #19/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #29/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #39/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/11/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/12/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/12/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/27/2009 240 4.00 8.88

Page 1 of 2

### Appendix C-2: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for New Sources (Recommended Option)

**Facility ID Combusor ID**  **Fuel Category Combustor Design**  **Test ID Test Date**  **Sample Time (min)** **Sample**

**Time (hrs) Stack Oxygen** 

**Concentration (%)**  GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #18/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/27/2009 240 4.00 8.21 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #28/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/27/2009 240 4.00 7.21 GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #38/27/2009 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #13/24/2005 120 2.00 7.8 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #2 3/24/2005 120 2.00 8.1 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #3 3/24/2005 120 2.00 8.4 WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #43/24/2005 120 2.00 7.3 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 6/3/2008 100 1.67 6.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #18/26/2009 240 4.00 5.58 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #28/26/2009 240 4.00 5.56 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #38/27/2009 240 4.00 5.66 IAUofNorthernIowa Boiler #3 Coal PC 4 10/6/2009 247 4.12 5.8 IAUofNorthernIowa Boiler #3 Coal PC 5 10/6/2009 249 4.15 5.3 IAUofNorthernIowa Boiler #3 Coal PC 6 10/7/2009 250 4.17 6 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #17/17/2007 60 1.00 12.4 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #27/17/2007 60 1.00 12.2 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #3 7/17/2007 60 1.00 11.9 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 8/5/2009 240 4.00 10.84 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 8/6/2009 240 4.00 10.25 TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 240 4.00 10.31 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009 191 3.18 16.6 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009 190 3.17 16.3 MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009 190 3.17 16 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 1 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 2 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 3 11/18/2009 216 3.60 5.3 HITesoro SG1102 Non-Continental Liquid N/A Sample #1 10/9/2010 60 1.00 4.89 HITesoro SG1102 Non-Continental Liquid N/A Sample #2 10/9/2010 60 1.00 5.19 HITesoro SG1102 Non-Continental Liquid N/A Sample #3 10/9/2010 60 1.00 5.29 HITesoro SG1102 Non-Continental Liquid N/A Sample #112/13/2010 192 3.20 6.3 HITesoro SG1102 Non-Continental Liquid N/A Sample #212/13/2010 192 3.20 6.42 HITesoro SG1102 Non-Continental Liquid N/A Sample #312/13/2010 192 3.20 6.77 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #110/19/2009 240 4.00 4.5 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #210/19/2009 240 4.00 4.7 WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #310/20/2009 240 4.00 4.8

Page 2 of 2

# Appendix C-3a: Summary of PM 3x RDL for Existing Sources (Recommended Option)

**Fuel Category Combustor Design**  **Average Sample Time (hrs) 3x RDL**  **( μg/dscm)**  **F d** 

## Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)** 

FB 1 3.00E+03 9,780 5.45 **2.48E-03** PC 2 1.50E+03 9,780 7.05 **1.38E-03** Stoker/Other 2 1.50E+03 9,780 7.46 **1.42E-03** Dutch Oven/Pile Burner 2 1.50E+03 9,420 8.67 **1.51E-03**

FB 2 1.50E+03 9,420 7.00 **1.32E-03** Fuel Cell 2 1.50E+03 9,420 13.33 **2.43E-03** Suspension Burner 1 3.00E+03 9,240 9.54 **3.18E-03** Suspension/Grate 1 3.00E+03 9,420 8.03 **2.86E-03** Wet Biomass Stoker/Other 2 1.50E+03 9,420 7.56 **1.38E-03** Dry Biomass Stoker/Other 2 1.50E+03 9,240 7.90 **1.39E-03** Heavy Liquid N/A 3 1.00E+03 9,190 3.94 **7.07E-04** Light Liquid N/A 3 1.00E+03 9,190 7.54 **8.96E-04**

Non-Continental Liquid N/A 2 1.50E+03 9,190 5.81 **1.19E-03** Process Gas N/A 4 7.50E+02 8,710 4.67 **5.25E-04**



# Appendix C-3b: Summary of PM 3x RDL for New Sources (Recommended Option)

**Fuel Category Combustor Design**  **Average Sample Time (hrs) 3x RDL**  **( μg/dscm)**  **F d** 

## Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)** 

FB 3 1.00E+03 9,780 6.58 **8.90E-04** PC 4 7.50E+02 9,780 5.70 **6.29E-04** Stoker/Other 3 1.00E+03 9,780 11.32 **1.33E-03** Dutch Oven/Pile Burner 3 1.00E+03 9,420 10.17 **1.14E-03**

FB 3 1.00E+03 9,420 5.10 **7.77E-04** Fuel Cell 4 7.50E+02 9,420 13.33 **1.21E-03** Suspension Burner 1 3.00E+03 9,240 9.54 **3.18E-03** Suspension/Grate 1 3.00E+03 9,420 8.03 **2.86E-03** Wet Biomass Stoker/Other 2 1.50E+03 9,420 8.27 **1.46E-03** Dry Biomass Stoker/Other 2 1.50E+03 9,240 7.90 **1.39E-03** Heavy Liquid N/A 3 1.00E+03 9,190 16.30 **2.59E-03** Light Liquid N/A 4 7.50E+02 9,190 4.63 **5.52E-04**

Non-Continental Liquid N/A 2 1.50E+03 9,190 5.81 **1.19E-03** Process Gas N/A 4 7.50E+02 8,710 4.67 **5.25E-04** Coal

Biomass

Coal

Biomass

Page 1 of 1

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  AKDoyonUtilities_AK 4 Solid Sample #18/17/2005 60 1.00 7 AKDoyonUtilities_AK 4 Solid Sample #28/17/2005 60 1.00 6.67 AKDoyonUtilities_AK 4 Solid Sample #38/17/2005 60 1.00 6.6 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #112/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #212/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #312/12/2007 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #17/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #27/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #37/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #37/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #37/11/2008 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #16/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #26/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #36/24/2009 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #16/14/2011 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #26/14/2011 ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Solid Sample #36/14/2011 ARPotlatchForestWarren Wellons Boiler Solid Sample #1 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Solid Sample #2 8/8/2006 60 1.00 15.5 ARPotlatchForestWarren Wellons Boiler Solid Sample #3 8/8/2006 60 1.00 16 ARPotlatchForestWarren Wellons Boiler Solid 1 9/9/2009 240 4.00 4.22 ARPotlatchForestWarren Wellons Boiler Solid 2 9/9/2009 240 4.00 4.9 ARPotlatchForestWarren Wellons Boiler Solid 3 9/10/2009 240 4.00 4.39 ARWeyerhaeuserDierksMill SN-32 Solid Sample #18/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Solid Sample #28/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Solid Sample #38/11/1997 60 1.00 9 ARWeyerhaeuserDierksMill SN-32 Solid Sample #111/21/1998 ARWeyerhaeuserDierksMill SN-32 Solid Sample #211/21/1998 ARWeyerhaeuserDierksMill SN-32 Solid Sample #311/21/1998 ARWeyerhaeuserDierksMill SN-32 Solid Sample #112/10/1999 ARWeyerhaeuserDierksMill SN-32 Solid Sample #212/10/1999 ARWeyerhaeuserDierksMill SN-32 Solid Sample #312/10/1999 ARWeyerhaeuserDierksMill SN-32 Solid Sample #111/9/2000 ARWeyerhaeuserDierksMill SN-32 Solid Sample #211/9/2000 ARWeyerhaeuserDierksMill SN-32 Solid Sample #311/9/2000 ARWeyerhaeuserDierksMill SN-32 Solid Sample #112/5/2001 ARWeyerhaeuserDierksMill SN-32 Solid Sample #212/5/2001 ARWeyerhaeuserDierksMill SN-32 Solid Sample #312/5/2001 ARWeyerhaeuserDierksMill SN-32 Solid Sample #112/4/2002 ARWeyerhaeuserDierksMill SN-32 Solid Sample #212/4/2002 ARWeyerhaeuserDierksMill SN-32 Solid Sample #312/4/2002 ARWeyerhaeuserDierksMill SN-32 Solid Sample #112/4/2003 ARWeyerhaeuserDierksMill SN-32 Solid Sample #212/4/2003 ARWeyerhaeuserDierksMill SN-32 Solid Sample #312/4/2003 ARWeyerhaeuserDierksMill SN-32 Solid Sample #19/29/2004 ARWeyerhaeuserDierksMill SN-32 Solid Sample #29/29/2004 ARWeyerhaeuserDierksMill SN-32 Solid Sample #39/29/2004 ARWeyerhaeuserDierksMill SN-45 Solid Sample #1 8/7/1997 120 2.00 6.7 ARWeyerhaeuserDierksMill SN-45 Solid Sample #2 8/7/1997 120 2.00 6.4 ARWeyerhaeuserDierksMill SN-45 Solid Sample #3 8/7/1997 120 2.00 6.4 ARWeyerhaeuserDierksMill SN-45 Solid Sample #112/5/2002 60 1.00 8.07 ARWeyerhaeuserDierksMill SN-45 Solid Sample #212/5/2002 60 1.00 7.84 ARWeyerhaeuserDierksMill SN-45 Solid Sample #312/5/2002 60 1.00 7.84 ARWeyerhaeuserDierksMill SN-45 Solid Sample #17/22/2009 240 4.00 9.18 ARWeyerhaeuserDierksMill SN-45 Solid Sample #27/23/2009 240 4.00 9.23 ARWeyerhaeuserDierksMill SN-45 Solid Sample #37/23/2009 240 4.00 9.33 CASierraPacificLincoln McBurney Boiler Solid Sample #1 3/5/2008 CASierraPacificLincoln McBurney Boiler Solid Sample #2 3/5/2008

Page 1 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  CASierraPacificLincoln McBurney Boiler Solid Sample #3 3/5/2008 CASierraPacificLincoln McBurney Boiler Solid Sample #13/11/2008 CASierraPacificLincoln McBurney Boiler Solid Sample #23/11/2008 CASierraPacificLincoln McBurney Boiler Solid Sample #33/11/2008 FLSmurfit-Stone 7PB Solid Sample #17/11/2007 60 1.00 7.05 FLSmurfit-Stone 7PB Solid Sample #27/11/2007 60 1.00 7.29 FLSmurfit-Stone 7PB Solid Sample #37/11/2007 60 1.00 7.41 FLUSSugarCorp Boiler No. 8 Solid Sample #13/24/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #23/24/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #33/24/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #13/26/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #23/26/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #33/26/2005 FLUSSugarCorp Boiler No. 8 Solid Sample #11/10/2006 FLUSSugarCorp Boiler No. 8 Solid Sample #21/10/2006 FLUSSugarCorp Boiler No. 8 Solid Sample #31/10/2006 FLUSSugarCorp Boiler No. 8 Solid Sample #1 6/2/2006 60 1.00 7.58 FLUSSugarCorp Boiler No. 8 Solid Sample #2 6/2/2006 60 1.00 7.99 FLUSSugarCorp Boiler No. 8 Solid Sample #3 6/2/2006 60 1.00 9.22 FLUSSugarCorp Boiler No. 8 Solid Sample #4 6/2/2006 60 1.00 9.84 FLUSSugarCorp Boiler No. 8 Solid Sample #5 6/2/2006 60 1.00 9.1 FLUSSugarCorp Boiler No. 8 Solid Sample #18/22/2006 64 1.07 10.36 FLUSSugarCorp Boiler No. 8 Solid Sample #28/22/2006 64 1.07 10.43 FLUSSugarCorp Boiler No. 8 Solid Sample #38/22/2006 64 1.07 10.3 FLUSSugarCorp Boiler No. 8 Solid Sample #1 39083 60 1.00 6.52 FLUSSugarCorp Boiler No. 8 Solid Sample #2 39083 60 1.00 6.96 FLUSSugarCorp Boiler No. 8 Solid Sample #4 39083 60 1.00 6.53 FLUSSugarCorp Boiler No. 8 Solid Sample #1 1/5/2007 60 1.00 7.73 FLUSSugarCorp Boiler No. 8 Solid Sample #2 1/5/2007 60 1.00 7.65 FLUSSugarCorp Boiler No. 8 Solid Sample #3 1/5/2007 60 1.00 7.25 FLUSSugarCorp Boiler No. 8 Solid Sample #111/30/2007 FLUSSugarCorp Boiler No. 8 Solid Sample #211/30/2007 FLUSSugarCorp Boiler No. 8 Solid Sample #311/30/2007 FLUSSugarCorp Boiler No. 8 Solid Sample #112/11/2008 FLUSSugarCorp Boiler No. 8 Solid Sample #212/11/2008 FLUSSugarCorp Boiler No. 8 Solid Sample #312/11/2008 FLUSSugarCorp Boiler No. 8 Solid Sample #412/11/2008 FLUSSugarCorp Boiler No. 8 Solid Sample #112/2/2009 60 1.00 6.4 FLUSSugarCorp Boiler No. 8 Solid Sample #212/2/2009 60 1.00 7 FLUSSugarCorp Boiler No. 8 Solid Sample #312/3/2009 60 1.00 5.6 FLUSSugarCorp Boiler No. 8 Solid Sample #111/30/2010 FLUSSugarCorp Boiler No. 8 Solid Sample #211/30/2010 FLUSSugarCorp Boiler No. 8 Solid Sample #311/30/2010 FLUSSugarCorp Boiler No. 8 Solid Sample #412/2/2010 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #16/19/2003 60 1.00 8.82 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #26/19/2003 60 1.00 8.76 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #36/19/2003 60 1.00 9.06 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #110/14/2004 120 2.00 9.78 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #210/14/2004 120 2.00 9.55 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #310/14/2004 120 2.00 7.91 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #16/15/2006 60 1.00 7.75 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #26/15/2006 60 1.00 8.13 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #36/15/2006 60 1.00 8.46 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #16/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #26/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #36/16/2006 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #19/18/2007 60 1.00 7.35 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #19/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #29/18/2007 60 1.00 6.6 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #29/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #39/18/2007 60 1.00 7.51 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #39/18/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #19/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #29/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #39/19/2007 GAGPMadisonPly 800 Wood Waste Boiler Solid 1 8/11/2009 GAGPMadisonPly 800 Wood Waste Boiler Solid 2 8/12/2009 GAGPMadisonPly 800 Wood Waste Boiler Solid 3 8/12/2009

Page 2 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #18/27/2009 240 4.00 8.88 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #18/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #28/27/2009 240 4.00 8.21 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #28/27/2009 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #38/27/2009 240 4.00 7.21 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #38/27/2009 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #1 2/7/2007 120 2.00 5.89 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #2 2/7/2007 120 2.00 6.8 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #3 2/7/2007 120 2.00 6.44 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #12/21/2008 120 2.00 10.71 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #22/21/2008 120 2.00 10.73 GAGPMonticelloPlywood EU700 - Wood Waste Boiler Solid Sample #32/21/2008 120 2.00 11.35 IAADMCornProcessingCR EU-502B Solid Sample #111/28/1994 IAADMCornProcessingCR EU-502B Solid Sample #211/28/1994 IAADMCornProcessingCR EU-502B Solid Sample #311/28/1994 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 6/3/2008 100 1.67 6.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #18/26/2009 240 4.00 5.58 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #28/26/2009 240 4.00 5.56 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #38/27/2009 240 4.00 5.66 IAIAStateUnivPowerPlant B1 Solid Sample #13/26/2008 62.5 1.04 4.3 IAIAStateUnivPowerPlant B1 Solid Sample #23/26/2008 62.5 1.04 3.9 IAIAStateUnivPowerPlant B1 Solid Sample #33/26/2008 62.5 1.04 4.4 IAIAStateUnivPowerPlant B2 Solid Sample #13/27/2008 62.5 1.04 4 IAIAStateUnivPowerPlant B2 Solid Sample #23/27/2008 62.5 1.04 3.9 IAIAStateUnivPowerPlant B2 Solid Sample #33/27/2008 62.5 1.04 3.7 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #1 5/8/2007 60 1.00 8.3 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #2 5/8/2007 60 1.00 7.9 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #3 5/8/2007 60 1.00 8.3 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #1 5/9/2007 60 1.00 8.3 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #2 5/9/2007 60 1.00 8.1 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #3 5/9/2007 60 1.00 8.3 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #15/10/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #25/10/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #35/10/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #18/14/2007 60 1.00 9.3 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #28/14/2007 60 1.00 9 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #38/14/2007 60 1.00 9 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #18/15/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #28/15/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #38/15/2007 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #110/15/2009 240 4.00 7 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #210/16/2009 240 4.00 6.8 IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #310/16/2009 240 4.00 6.9 IAUofIowa EP7 Boiler 11 Solid Sample #12/15/2006 IAUofIowa EP7 Boiler 11 Solid Sample #22/21/2006 IAUofIowa EP7 Boiler 11 Solid Sample #32/21/2006 IAUofIowa EP7 Boiler 11 Solid Sample #12/22/2006 IAUofIowa EP7 Boiler 11 Solid Sample #22/23/2006 IAUofIowa EP7 Boiler 11 Solid Sample #32/23/2006 IAUofIowa EP7 Boiler 11 Solid 1 8/4/2009 IAUofIowa EP7 Boiler 11 Solid 2 8/5/2009 IAUofIowa EP7 Boiler 11 Solid 3 8/5/2009 IAUofNorthernIowa Boiler #3 Solid 4 10/6/2009 240 4.00 5.8 IAUofNorthernIowa Boiler #3 Solid 5 10/6/2009 240 4.00 5.3 IAUofNorthernIowa Boiler #3 Solid 6 10/7/2009 240 4.00 6 IDAmalgamatedSugarCoTwinFalls S-B1 Solid Sample #19/26/2006 120 2.00 6.9 IDAmalgamatedSugarCoTwinFalls S-B1 Solid Sample #29/26/2006 120 2.00 6.9 IDAmalgamatedSugarCoTwinFalls S-B1 Solid Sample #39/26/2006 120 2.00 6 IDPotlatch PB-1 CE Solid Sample #14/30/2008 IDPotlatch PB-1 CE Solid Sample #24/30/2008 IDPotlatch PB-1 CE Solid Sample #34/30/2008 IDPotlatch PB-1 CE Solid Sample #17/28/2009 240 4.00 13.2 IDPotlatch PB-1 CE Solid Sample #27/28/2009 240 4.00 13.8 IDPotlatch PB-1 CE Solid Sample #37/29/2009 240 4.00 13 IDPotlatch PB-2 Riley Solid Sample #1 5/1/2008 IDPotlatch PB-2 Riley Solid Sample #2 5/1/2008

Page 3 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  IDPotlatch PB-2 Riley Solid Sample #3 5/1/2008 IDRileyCreekLumber HFB1 Solid Sample #14/24/2003 60 1.00 8 IDRileyCreekLumber HFB1 Solid Sample #24/24/2003 60 1.00 8 IDRileyCreekLumber HFB1 Solid Sample #34/24/2003 60 1.00 8 ILAbbottAbbottPark Unit 5AP Solid Sample #18/22/2007 ILAbbottAbbottPark Unit 5AP Solid Sample #28/22/2007 ILAbbottAbbottPark Unit 5AP Solid Sample #38/22/2007 ILAbbottAbbottPark Unit 5AP Solid OTM28-1 8/4/2009 ILAbbottAbbottPark Unit 5AP Solid OTM28-2 8/5/2009 ILAbbottAbbottPark Unit 5AP Solid OTM28-3 8/5/2009 ILPolyOne B1 Solid Sample #111/14/2006 ILPolyOne B1 Solid 1 9/9/2009 240 4.00 8.4 ILPolyOne B1 Solid 2 9/9/2009 240 4.00 8.1 ILPolyOne B1 Solid 3 9/10/2009 240 4.00 8.3 ILRockIslandArsenal NBN 12602 (Boiler #1) Solid Sample #13/13/2007 ILRockIslandArsenal NBN 12602 (Boiler #1) Solid Sample #23/13/2007 ILRockIslandArsenal NBN 12602 (Boiler #1) Solid Sample #33/13/2007 INPurdueUniverisity Boiler 5 Solid Sample #111/29/2006 64 1.07 INPurdueUniverisity Boiler 5 Solid Sample #211/29/2006 70 1.17 INPurdueUniverisity Boiler 5 Solid Sample #311/29/2006 75 1.25 INPurdueUniverisity Boiler 5 Solid M5-1 7/21/2009 240 4.00 4.4 INPurdueUniverisity Boiler 5 Solid M5-2 7/21/2009 240 4.00 4.4 INPurdueUniverisity Boiler 5 Solid M5-3 7/22/2009 240 4.00 4.3 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #1 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #2 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #3 4/7/2005 121 2.02 7 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #16/28/2006 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #26/28/2006 INSABICInnovativePlastics 01-001 BW1 Boiler Solid Sample #36/28/2006 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #1 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #2 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #3 4/7/2005 123 2.05 7 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #16/28/2006 125 2.08 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #26/28/2006 125 2.08 INSABICInnovativePlastics 01-001 BW2 Boiler Solid Sample #36/28/2006 125 2.08 LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #18/14/2007 LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #38/14/2007 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #15/31/2002 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #25/31/2002 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #35/31/2002 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #15/29/2007 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #25/29/2007 LAWeyerhaeuserDodson ES-017 WFB Solid Sample #35/29/2007 MENewPage-Rumford Cogen#6 Solid Sample #1 9/6/2007 MENewPage-Rumford Cogen#6 Solid Sample #2 9/6/2007 MENewPage-Rumford Cogen#6 Solid Sample #3 9/6/2007 MENewPage-Rumford Cogen#6 Solid 1 12/8/2009 240 4.00 7.5 MENewPage-Rumford Cogen#6 Solid 2 12/8/2009 240 4.00 7.6 MENewPage-Rumford Cogen#6 Solid 3 12/9/2009 240 4.00 7.7 MENewPage-Rumford Cogen#7 Solid Sample #1 9/6/2007 MENewPage-Rumford Cogen#7 Solid Sample #2 9/6/2007 MENewPage-Rumford Cogen#7 Solid Sample #3 9/6/2007 MENewPage-Rumford Cogen#7 Solid 1 12/8/2009 240 4.00 7.5 MENewPage-Rumford Cogen#7 Solid 2 12/8/2009 240 4.00 7.6 MENewPage-Rumford Cogen#7 Solid 3 12/9/2009 240 4.00 7.7 MESDWarren #21 Boiler Solid Sample #111/10/2006 MESDWarren #21 Boiler Solid Sample #211/10/2006 MESDWarren #21 Boiler Solid Sample #311/10/2006 MNAmericanCrystalCrookston Boiler 1 Solid Sample #110/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Solid Sample #210/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Solid Sample #310/31/2005 60 1.00 11.5 MNAmericanCrystalCrookston Boiler 1 Solid Sample #111/2/2005 MNAmericanCrystalCrookston Boiler 1 Solid Sample #211/2/2005 MNAmericanCrystalCrookston Boiler 1 Solid Sample #311/2/2005 MNAmericanCrystalCrookston Boiler 1 Solid Sample #111/3/2005 MNAmericanCrystalCrookston Boiler 1 Solid Sample #211/3/2005 MNAmericanCrystalCrookston Boiler 1 Solid Sample #311/3/2005 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #14/22/2008 60 1.00

Page 4 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #24/22/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #34/22/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #14/23/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #24/23/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #34/23/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #1 8/8/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #2 8/8/2008 60 1.00 MNAndersonCorpBayport Boiler 11 EU620 Solid Sample #3 8/8/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #14/22/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #24/22/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #34/22/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #14/23/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #24/23/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #34/23/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #1 8/8/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #2 8/8/2008 60 1.00 MNAndersonCorpBayport Boiler 12 EU621 Solid Sample #3 8/8/2008 60 1.00 MSGPNewAugusta AA-015 Power Boiler Solid Sample #17/12/2006 MSGPNewAugusta AA-015 Power Boiler Solid Sample #27/12/2006 MSGPNewAugusta AA-015 Power Boiler Solid Sample #37/12/2006 MSGPNewAugusta AA-015 Power Boiler Solid Sample #19/22/2010 MSGPNewAugusta AA-015 Power Boiler Solid Sample #29/23/2010 MSGPNewAugusta AA-015 Power Boiler Solid Sample #39/23/2010 MSGPNewAugusta AA-015 Power Boiler Solid Sample #19/28/2010 MSGPNewAugusta AA-015 Power Boiler Solid Sample #29/29/2010 MSGPNewAugusta AA-015 Power Boiler Solid Sample #39/30/2010 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #12/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #22/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #32/26/1993 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #18/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #28/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #38/23/1999 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #17/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #27/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #37/11/2003 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #16/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #26/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #36/28/2005 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #12/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #22/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #32/22/2006 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #18/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #28/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #38/31/2007 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #1 8/5/2009 180 3.00 8.06 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #2 8/5/2009 180 3.00 7.25 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #3 8/5/2009 180 3.00 7.63 OHSmartPapersHoldingsLLC B010 Solid Sample #18/11/2005 120 2.00 7.9 OHSmartPapersHoldingsLLC B010 Solid Sample #28/11/2005 120 2.00 7.8 OHSmartPapersHoldingsLLC B010 Solid Sample #38/11/2005 120 2.00 7.8 OHUofCincinnati B108 Solid Sample #34/27/2005 OHUofCincinnati B108 Solid Sample #14/26/2006 OHUofCincinnati B108 Solid Sample #24/26/2006 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #110/24/2000 60 1.00 6 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #210/24/2000 60 1.00 6.1 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #310/24/2000 60 1.00 5.9 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #110/9/2002 60 1.00 6.1 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #210/9/2002 60 1.00 3.1 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #310/9/2002 60 1.00 5.8 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #110/19/2004 60 1.00 5.6 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #210/19/2004 60 1.00 5.9 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #310/19/2004 60 1.00 5.4 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #110/25/2006 60 1.00 3.2 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #210/25/2006 60 1.00 3.6 SCInternationalPaperEastover No. 1 Power Boiler Solid Sample #310/25/2006 60 1.00 3.8 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #18/19/1993 90 1.50 7.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #28/19/1993 90 1.50 7.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #38/19/1993 90 1.50 7.5

Page 5 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #18/16/1995 120 2.00 8.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #28/16/1995 120 2.00 7.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #38/16/1995 120 2.00 6.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #18/13/1997 125 2.08 3.6 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #28/13/1997 125 2.08 3.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #38/13/1997 125 2.08 3.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #16/16/1999 125 2.08 6.5 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #26/16/1999 125 2.08 6.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #36/16/1999 125 2.08 6.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #1 6/5/2003 125 2.08 8.7 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #2 6/5/2003 125 2.08 8.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #3 6/5/2003 125 2.08 8.4 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #13/25/2004 125 2.08 7.5 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #23/25/2004 125 2.08 7.3 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #33/25/2004 125 2.08 6.8 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #13/15/2006 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #23/15/2006 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #33/15/2006 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #13/19/2008 125 2.08 10.1 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #23/19/2008 125 2.08 9.8 SCInternationalPaperEastover No. 2 Power Boiler Solid Sample #33/19/2008 125 2.08 10.1 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #11/26/2005 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #21/26/2005 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #31/26/2005 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #1 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #2 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #3 1/4/2007 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #17/14/2009 180 3.00 9.74 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #27/14/2009 180 3.00 9.38 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #37/14/2009 180 3.00 9.11 TNCargillMemphis Stoker Boiler 8001 Solid Sample #17/17/2007 60 1.00 12.4 TNCargillMemphis Stoker Boiler 8001 Solid Sample #27/17/2007 60 1.00 12.2 TNCargillMemphis Stoker Boiler 8001 Solid Sample #37/17/2007 60 1.00 11.9 TNCargillMemphis Stoker Boiler 8001 Solid 1 8/5/2009 240 4.00 10.84 TNCargillMemphis Stoker Boiler 8001 Solid 3 8/6/2009 240 4.00 10.25 TNCargillMemphis Stoker Boiler 8001 Solid 2 11/6/2009 240 4.00 10.31 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #18/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #28/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #38/20/1996 64 1.07 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #1 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #2 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #3 8/8/2000 64 1.07 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #26/29/2004 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #36/29/2004 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #111/9/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #211/9/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #111/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #211/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #311/10/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #311/11/2004 120 2.00 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #17/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #27/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 25 Solid Sample #37/24/2008 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #17/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #27/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #37/12/1993 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #19/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #29/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #39/25/1997 64 1.07 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #18/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #28/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #38/28/2001 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #1 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #2 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #3 3/9/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #13/10/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #23/10/2005 120 2.00 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #33/10/2005 120 2.00

Page 6 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  TNEastman_NO_CBIDATA Boiler 27 Solid Sample #15/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #25/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 27 Solid Sample #35/17/2005 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #111/8/1994 75 1.25 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #211/8/1994 75 1.25 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #311/8/1994 75 1.25 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #19/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #29/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #39/19/2002 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #19/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #29/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #39/19/2006 60 1.00 7 TNEastman_NO_CBIDATA Boiler 30 Solid 1 8/26/2009 TNEastman_NO_CBIDATA Boiler 30 Solid 2 8/27/2009 TNEastman_NO_CBIDATA Boiler 30 Solid 3 8/27/2009 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #1 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #2 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #3 8/4/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #112/14/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #212/15/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #312/15/1994 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #19/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #29/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #39/29/1998 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #17/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #27/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #37/25/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #18/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #28/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #38/14/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #112/6/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #212/6/2006 125 2.08 7 TNEastman_NO_CBIDATA Boiler 31 Solid Sample #312/6/2006 125 2.08 7 TXRGVSG Boiler No. 6 Solid Sample #11/13/2009 TXRGVSG Boiler No. 6 Solid Sample #21/13/2009 TXRGVSG Boiler No. 6 Solid Sample #31/13/2009 VAUniversityofVirginia 7103-1-01R Solid Sample #112/6/2007 60 1.00 7.07 VAUniversityofVirginia 7103-1-01R Solid Sample #212/6/2007 60 1.00 7.09 VAUniversityofVirginia 7103-1-01R Solid Sample #312/6/2007 60 1.00 6.98 VAUniversityofVirginia 7103-1-01R Solid M027-1 9/17/2009 240 4.00 VAUniversityofVirginia 7103-1-01R Solid M027-2 9/17/2009 240 4.00 VAUniversityofVirginia 7103-1-01R Solid M027-3 9/18/2009 240 4.00 VAUniversityofVirginia 7103-1-02R Solid Sample #11/16/2007 60 1.00 6.64 VAUniversityofVirginia 7103-1-02R Solid Sample #21/16/2007 60 1.00 6.96 VAUniversityofVirginia 7103-1-02R Solid Sample #31/16/2007 60 1.00 6.74 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #16/22/2006 60 1.00 6.3 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #26/22/2006 60 1.00 6.9 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #36/22/2006 60 1.00 7.4 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #18/12/2009 240 4.00 7 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #28/13/2009 240 4.00 7 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #38/13/2009 240 4.00 7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #19/18/1996 120 2.00 10.7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #29/18/1996 120 2.00 10.6 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #39/18/1996 120 2.00 9.4 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #111/10/2004 60 1.00 9.5 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #211/10/2004 60 1.00 9.3 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #311/10/2004 60 1.00 8.7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #18/11/2009 240 4.00 7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #28/11/2009 240 4.00 7 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #38/12/2009 240 4.00 7 WAWeyerhaeuserLongview No. 11 Hog Fuel Boiler Solid Sample #110/7/2008 WAWeyerhaeuserLongview No. 11 Hog Fuel Boiler Solid Sample #210/7/2008 WAWeyerhaeuserLongview No. 11 Hog Fuel Boiler Solid Sample #310/7/2008 WIDomtar2814 B11, S11 Solid Sample #18/29/2007 60 1.00 7 WIDomtar2814 B11, S11 Solid Sample #28/29/2007 60 1.00 7 WIDomtar2814 B11, S11 Solid Sample #38/29/2007 60 1.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #19/19/2007 60 1.00 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #29/19/2007 60 1.00

Page 7 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #39/19/2007 60 1.00 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #18/20/2009 240 4.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #28/20/2009 240 4.00 7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Solid Sample #38/21/2009 240 4.00 7 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #110/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #210/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #310/27/1992 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #19/24/1994 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #29/24/1994 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #39/24/1994 120 2.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #17/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #27/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #37/28/1998 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #111/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #211/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #311/9/1999 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 2/2/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #17/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #27/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #37/19/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #18/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #28/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #38/29/2000 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #18/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #28/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #38/28/2002 60 1.00 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #18/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #28/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #38/10/2004 60 1.00 6 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #19/21/2007 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #29/21/2007 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #39/21/2007 WINewPageBiron B24 Solid Sample #19/12/2007 60 1.00 WINewPageBiron B24 Solid Sample #29/12/2007 60 1.00 WINewPageBiron B24 Solid Sample #39/12/2007 60 1.00 WINewPageBiron B24 Solid 1 9/22/2009 240 4.00 WINewPageBiron B24 Solid 2 9/22/2009 240 4.00 WINewPageBiron B24 Solid 3 9/23/2009 240 4.00 WIThilmanyPapersNicoletMill B23 Solid Sample #12/22/2006 60 1.00 WIThilmanyPapersNicoletMill B23 Solid Sample #22/22/2006 60 1.00 WIThilmanyPapersNicoletMill B23 Solid Sample #32/22/2006 60 1.00 WIThilmanyPapersNicoletMill B23 Solid Sample #12/23/2006 WIThilmanyPapersNicoletMill B23 Solid Sample #22/23/2006 WIThilmanyPapersNicoletMill B23 Solid Sample #32/23/2006 WIThilmanyPapersNicoletMill B24 Solid Sample #12/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Solid Sample #22/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Solid Sample #32/22/2006 60 1.00 WIThilmanyPapersNicoletMill B24 Solid Sample #12/23/2006 WIThilmanyPapersNicoletMill B24 Solid Sample #22/23/2006 WIThilmanyPapersNicoletMill B24 Solid Sample #32/23/2006 WIWausau # 5 Power Boiler (B24) Solid Sample #17/24/2007 60 1.00 WIWausau # 5 Power Boiler (B24) Solid Sample #27/24/2007 60 1.00 WIWausau # 5 Power Boiler (B24) Solid Sample #37/24/2007 60 1.00 ALBP-Decatur24 AB-8301 Liquid Sample #11/24/2001 ALBP-Decatur24 AB-8301 Liquid Sample #21/24/2001 ALBP-Decatur24 AB-8301 Liquid Sample #31/24/2001 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #111/30/2004 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #211/30/2004 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #311/30/2004 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #111/14/2006 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #211/14/2006 SCCogenSouth B002 - Auxiliary Boiler #1 Liquid Sample #311/14/2006 SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #111/30/2004 SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #211/30/2004 SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #311/30/2004 SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #111/14/2006

Page 8 of 9

## Appendix C-4: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for Existing Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #211/14/2006 SCCogenSouth B003 - Auxiliary Boiler #2 Liquid Sample #311/14/2006 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #111/30/2004 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #211/30/2004 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #311/30/2004 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #111/14/2006 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #211/14/2006 SCCogenSouth B004 - Auxiliary Boiler #3 Liquid Sample #311/14/2006 SCGPChemRussellville FO Boiler Liquid Sample #18/26/2009 120 2.00 8.06 SCGPChemRussellville FO Boiler Liquid Sample #28/26/2009 120 2.00 7.26 SCGPChemRussellville FO Boiler Liquid Sample #38/26/2009 120 2.00 7.31 SCMilliken-Dewey D30 Liquid Sample #18/12/2009 180 3.00 SCMilliken-Dewey D30 Liquid Sample #28/12/2009 180 3.00 SCMilliken-Dewey D30 Liquid Sample #38/12/2009 180 3.00 SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Liquid PM2.5-1 7/23/2009 SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Liquid PM2.5-2 7/23/2009 SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Liquid PM2.5-3 7/23/2009 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 1 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 2 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 3 11/18/2009 216 3.60 5.3 WVMountainStateCarbonFollansbee S1 Process Gas Sample #110/19/2009 240 4.00 4.5 WVMountainStateCarbonFollansbee S1 Process Gas Sample #210/19/2009 240 4.00 4.7 WVMountainStateCarbonFollansbee S1 Process Gas Sample #310/20/2009 240 4.00 4.8

Page 9 of 9

## Appendix C-5: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL for New Sources (Alternative Option)

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Sample**  **Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 6/3/2008 100 1.67 6.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 6/3/2008 100 1.67 7.9 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #18/26/2009 240 4.00 5.58 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #28/26/2009 240 4.00 5.56 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #38/27/2009 240 4.00 5.66 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 1 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 2 11/17/2009 216 3.60 4.3 TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid 3 11/18/2009 216 3.60 5.3 WVMountainStateCarbonFollansbee S1 Process Gas Sample #110/19/2009 240 4.00 4.5 WVMountainStateCarbonFollansbee S1 Process Gas Sample #210/19/2009 240 4.00 4.7 WVMountainStateCarbonFollansbee S1 Process Gas Sample #310/20/2009 240 4.00 4.8

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# Appendix C-6a: Summary of PM 3x RDL for Existing Sources (Alternative Option)

**Fuel Category Average Sample Time (hrs)**  **3x RDL (** **μg/dscm) F** **d**

# Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)**  Solid 2 1.50E+03 9,780 7.54 **1.43E-03** Liquid 3 1.00E+03 9,190 6.09 **8.09E-04** Process Gas 4 7.50E+02 8,710 4.67 **5.25E-04**



# Appendix C-6b: Summary of PM 3x RDL for New Sources (Alternative Option)

**Fuel Category Average Sample Time (hrs)**  **3x RDL (** **μg/dscm) F** **d**

# Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)**  Solid 3 1.00E+03 9,780 6.58 **8.90E-04** Liquid 4 7.50E+02 9,190 4.63 **5.52E-04** Process Gas 4 7.50E+02 8,710 4.67 **5.25E-04**

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