**Non-Hg Metal**

**HA P**  **Source Sb**  **As Be**  **Cd Cr**  **Co Pb** 

**Total Runs Floor tile roller kilns**  15 15 15 15 15 15 15 **No. Set A**

**side** 0 0 9 0 0 0 0

**No. Use** 15 15 6 15 15 15 15

**No. BDL** 0 0 0 0 0 0 0

**No. A DL**  15 15 6 15 15 15 15 **% BDL** 0 0 0 0 0 0 0

**% A DL**  100 100 100 100 100 100 100

**Total Runs Wa** **ll tile roller kilns** 6 6 6 6 6 6 6 **No. Set A**

**side** 0 0 6 0 0 0 0

**No. Use** 6 6 0 6 6 6 6

**No. BDL** 0 0 0 0 0 0 0

**No. A DL**  6 6 0 6 6 6 6 **% BDL** 0 0 0 0 0 0

**% A DL**  100 100 100 100 100 100

**Total Runs Tile glaze lines**  9 9 9 9 9 9 9 **No. Set A**

**side** 0 7 9 4 0 0 0

**No. Use** 9 2 0 5 9 9 9

**No. BDL** 4 0 0 0 0 4 0

**No. A DL**  5 2 0 5 9 5 9 **% BDL** 44 0 0 0 44 0

**% A DL**  56 100 100 100 56 100

**Total Runs First-fire sanitary**  **ware tunnel kilns**  18 18 18 18 18 18 18

**No. Set A**

**side** 0 2 18 0 0 0 0

**No. Use** 18 16 0 18 18 18 18

**No. BDL** 0 0 0 0 0 0 0

**No. A DL**  18 16 0 18 18 18 18 **% BDL** 0 0 0 0 0 0

**% A DL**  100 100 100 100 100 100**Mn Ni**  **Se Total Non**  **Hg HA P**  **Metals**

7 15 15 142

0 0 0 9

7 15 15 133

0 0 0 0

7 15 15 133

0 0 0 0

100 100 100 100

4 6 6 58

0 0 0 6

4 6 6 52

0 0 0 0

4 6 6 52

0 0 0 0

100 100 100 100

6 9 9 87

0 0 4 24

6 9 5 63

0 0 0 8

6 9 5 55

0 0 0 13

100 100 100 87

16 18 18 178

0 0 1 21

16 18 17 157

0 0 0 0

16 18 17 157

0 0 0 0

100 100 100 100**Kiln No Run No** **Test Date Parent Company**  **Facility Name**

41 15/25/2010 Florim Ceramiche S.p.AFlorim USA 41 25/25/2010 Florim Ceramiche S.p.AFlorim USA 41 35/26/2010 Florim Ceramiche S.p.AFlorim USA 60, 61, 62 15/13-15/2010Dal-Tile Corp. Dal Italia 60, 61, 62 25/13-15/2010Dal-Tile Corp. Dal Italia 60, 61, 62 35/13-15/2010Dal-Tile Corp. Dal Italia 77 15/4-5/10 Monarch Ceramic Tile Monarch 77 25/4-5/10 Monarch Ceramic Tile Monarch 77 35/4-5/10 Monarch Ceramic Tile Monarch 36 1 12/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility 36 212/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility 36 312/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility 84 1 12/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility 84 212/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility 84 312/6-7/2010Marazzi Group S.p.A. Marazzi, Sunny vale Facility**City State** **Ma jor or A** **rea Kiln ID**  **AP CD Type**  **Laboratory** Clarksville TNMajor RK-1 DIFF ALS Laboratory Group Clarksville TNMajor RK-1 DIFF ALS Laboratory Group Clarksville TNMajor RK-1 DIFF ALS Laboratory Group Muskogee OKMajor RK-2, RK-3, RK-4 Wet ScrubberALS Laboratory Group Muskogee OKMajor RK-2, RK-3, RK-4 Wet ScrubberALS Laboratory Group Muskogee OKMajor RK-2, RK-3, RK-4 Wet ScrubberALS Laboratory Group Florence ALMajor RK-2L None ALS Laboratory Group Florence ALMajor RK-2L None ALS Laboratory Group Florence ALMajor RK-2L None ALS Laboratory Group Sunny vale TXMajor RK-4 None ALS Laboratory Group Sunny vale TXMajor RK-4 None ALS Laboratory Group Sunny vale TXMajor RK-4 None ALS Laboratory Group Sunny vale TXMajor RK-5U None ALS Laboratory Group Sunny vale TXMajor RK-5U None ALS Laboratory Group Sunny vale TXMajor RK-5U None ALS Laboratory Group**An alytical M** **ethod Lab Method Listed in PW**  **Me mo**  **Ty pe of** 

**Tile An** **timony Total**

**Blank Corrected ug An** **timony Fraction Status**  ICP-MS Method 29 ICP/MS or GFAAFloor 1.523 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.306 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.425 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.28 ADL_BDL ICP-MS Method 29 ICP/MS or GFAAFloor 1.465 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.289 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.226 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.412 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.398 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 2.96 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 1.736 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 2.382 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 0.546 BDL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 0.515 ADL_ADL ICP-MS Method 29 ICP/MS or GFAAFloor 0.588 ADL_ADL**An timony Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Ar senic Total Blank**  **Corrected ug Ar** **senic Fraction Status**  Use ADL 7.93 ADL_ADL Use ADL 17.9 BDL_ADL Use ADL 14.11 ADL_ADL Use ADL 11.6 ADL_ADL Use ADL 9.97 ADL_ADL Use ADL 9.47 ADL_ADL Use ADL 50.78 ADL_ADL Use ADL 44.76 ADL_ADL Use ADL 35.96 ADL_ADL Use ADL 125.9 ADL_ADL Use ADL 77.4 ADL_ADL Use ADL 97.7 ADL_ADL Use ADL 26.97 ADL_ADL Use ADL 48.85 ADL_ADL Use ADL 38.92 ADL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Ar senic Run Status** **Detection Limit Comments**  If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Beryllium Total Blank Corrected ug** **Beryllium Fraction Status**  Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.353 BDL_ADL Use ADL 0.389 BDL_ADL Use ADL 0.381 BDL_ADL Use ADL 0.499 BDL_ADL Use ADL 0.445 ADL_ADL Use ADL 0.467 BDL_ADL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL Use ADL 0.3 BDL_BDL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Beryllium Run**

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DL BDL Other DL BDL 0.08 Yes, Check DLMDL or Other DL Use / Set Aside Final **Cadmium Total Blank Corrected ug** **Cadmium Fraction Status**  Other DL Set Aside 1.552 ADL_ADL Other DL Set Aside 0.597 ADL_BDL Other DL Set Aside 0.897 ADL_BDL Other DL Set Aside 1.34 ADL_BDL Other DL Set Aside 1.1863 ADL_ADL Other DL Set Aside 1.38 ADL_BDL Use ADL 2.006 ADL_ADL Use ADL 4.232 ADL_ADL Use ADL 3.627 ADL_ADL Use ADL 19.022 ADL_ADL Use ADL 17.36 ADL_ADL Use ADL 23.65 ADL_BDL Other DL Set Aside 0.728 ADL_ADL Other DL Set Aside 0.688 ADL_BDL Other DL Set Aside 0.939 ADL_ADL

Total Runs 15 No. Set Aside 9 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Cadmium Run**

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADL DLL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Chromium Total Blank Corrected ug** **Chromium Fraction Status**  Use ADL 20.952 ADL_ADL Use ADL 17.502 ADL_ADL Use ADL 36.562 ADL_ADL Use ADL 172.252 ADL_ADL Use ADL 178.928 ADL_ADL Use ADL 211.042 ADL_ADL Use ADL 133.649 ADL_ADL Use ADL 107.719 ADL_ADL Use ADL 486.359 ADL_ADL Use ADL 114.15 ADL_ADL Use ADL 67.88 ADL_ADL Use ADL 114.82 ADL_ADL Use ADL 30.96 ADL_ADL Use ADL 46.1 ADL_ADL Use ADL 44.35 ADL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Chromium Run**

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Cobalt Total Blank Corrected ug**  **Cobalt Fraction Status**  Use ADL 0.51 ADL_ADL Use ADL 0.981 ADL_ADL Use ADL 0.846 ADL_ADL Use ADL 0.479 ADL_ADL Use ADL 0.553 ADL_BDL Use ADL 1.047 ADL_BDL Use ADL 1.264 ADL_ADL Use ADL 0.661 ADL_ADL Use ADL 4.426 ADL_ADL Use ADL 2.244 ADL_ADL Use ADL 2.099 ADL_ADL Use ADL 0.745 ADL_ADL Use ADL 0.461 BDL_ADL Use ADL 0.41 BDL_ADL Use ADL 0.466 BDL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Cobalt Run Status Detection Limit**  **Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL DLL Other DL ADL DLL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL DLL Other DL ADL DLL Other DL ADL DLL Other DL ADLMDL or Other DL Use / Set Aside Final **Lead Total Blank Corrected ug**  **Lead Fraction Status**  Use ADL 7.549 ADL_ADL Use ADL 6.76 ADL_ADL Use ADL 14.973 ADL_ADL Use ADL 129.416 ADL_ADL Use ADL 115.254 ADL_ADL Use ADL 84.252 ADL_ADL Use ADL 66.024 ADL_ADL Use ADL 57.754 ADL_ADL Use ADL 60.504 ADL_ADL Use ADL 240.2053 ADL_ADL Use ADL 84.5053 ADL_ADL Use ADL 287.6053 ADL_ADL Use ADL 22.0753 ADL_ADL Use ADL 25.8923 ADL_ADL Use ADL 25.7853 ADL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Lead Run Status Detection Limit**  **Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Ma nganese Total**  **Blank Corrected ug Ma** **nganese Fraction Status**  Use ADL 9.67 ADL_ADL Use ADL 34.02 Use ADL 31.19 Use ADL 14.66 Use ADL 33.99 Use ADL 126.47 Use ADL 28.954 Use ADL 26.641 Use ADL 60.791 ADL_ADL Use ADL 43.602 ADL_ADL Use ADL 106.312 Use ADL 30.792 ADL_ADL Use ADL 6.642 ADL_ADL Use ADL 3.212 ADL_ADL Use ADL 3.672 ADL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Ma nganese Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL

Other DL Other DL Other DL Other DL Other DL Other DL Other DL ADL Other DL ADL ADL Other DL ADL

Other DL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Nickel Total Blank Corrected ug**  **Nickel Fraction Status**  Use ADL 4.295 ADL_ADL 1.745 ADL_ADL 6.405 ADL_ADL 2.464 ADL_ADL 1.606 ADL_ADL 2.327 ADL_ADL 2.683 ADL_ADL 2.753 ADL_ADL Use ADL 181.683 ADL_ADL Use ADL 7.869 ADL_ADL 6.389 ADL_ADL Use ADL 3.899 ADL_ADL Use ADL 5.079 ADL_ADL Use ADL 2.379 ADL_ADL Use ADL 3.039 ADL_ADL

Total Runs 7 No. Set Aside 0 No. Use 7 No. BDL 0 No. ADL 7 % BDL 0 % ADL 100**Nickel Run Status Detection Limit**  **Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final **Selenium Total Blank Corrected ug** **Selenium Fraction Status**  Use ADL 40.62 ADL_ADL Use ADL 59.63 ADL_ADL Use ADL 78.63 ADL_ADL Use ADL 105.8 ADL_ADL Use ADL 92.7 ADL_ADL Use ADL 71.2 ADL_ADL Use ADL 398.22 ADL_ADL Use ADL 408.7 ADL_ADL Use ADL 328.95 ADL_ADL Use ADL 1753.9 ADL_ADL Use ADL 1132 ADL_ADL Use ADL 1677 ADL_ADL Use ADL 932.7 ADL_ADL Use ADL 1647.3 ADL_ADL Use ADL 1419.3 ADL_ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Selenium Run**

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL RDL (ug) Blank Corrected > RDL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADL ADL Other DL ADLMDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 15 No. Set Aside 0 No. Use 15 No. BDL 0 No. ADL 15 % BDL 0 % ADL 100**Kiln No Run No** **Test Date Parent Company**  **Facility Name**

64, 65, 68, 69 1 12/13-14/2010Mohawk Industries Dal-Tile El Paso Plant 64, 65, 68, 69 212/13-14/2010Mohawk Industries Dal-Tile El Paso Plant 64, 65, 68, 69 312/13-14/2010Mohawk Industries Dal-Tile El Paso Plant 70, 71, 74, 75 1 12/15-16/2010Mohawk Industries Dal-Tile El Paso Plant 70, 71, 74, 75 212/15-16/2010Mohawk Industries Dal-Tile El Paso Plant 70, 71, 74, 75 312/15-16/2010Mohawk Industries Dal-Tile El Paso Plant**City State** **Ma jor or A** **rea Kiln ID**  **AP CD Type**  El Paso TXMajor RK-1, RK-2, RK-5, RK-6 Bisque None El Paso TXMajor RK-1, RK-2, RK-5, RK-6 Bisque None El Paso TXMajor RK-1, RK-2, RK-5, RK-6 Bisque None El Paso TXMajor RK-7, RK-8, RK-11, RK-12 Glost None El Paso TXMajor RK-7, RK-8, RK-11, RK-12 Glost None El Paso TXMajor RK-7, RK-8, RK-11, RK-12 Glost None**Laboratory An** **alytical M ethod**  **Lab Method Listed in PW Me** **mo Ty** **pe of**

**Tile** ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA Wall**An timony Total** 

**Blank Corrected ug An** **timony Fraction Status**  **An timony Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL 0.86 ADL_ADL ADL Other DL ADL 0.741 ADL_ADL ADL Other DL ADL 0.674 ADL_ADL ADL Other DL ADL 0.481 ADL_ADL ADL Other DL ADL 0.372 BDL_ADL DLL Other DL ADL 0.388 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Ar senic Total Blank** 

**Corrected ug Ar** **senic Fraction Status**  **Ar senic Run Status** **Detection Limit Comments**  If DLL or ADL, ADL 36.22 ADL_ADL ADL Other DL ADL 11.59 ADL_ADL ADL Other DL ADL 27.91 ADL_ADL ADL Other DL ADL 8.61 ADL_ADL ADL Other DL ADL 7.48 ADL_ADL ADL Other DL ADL 8.22 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Beryllium Total**

**Blank Corrected ug Beryllium Fraction**  **Status Beryllium Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL 0.3 BDL_BDL BDL Other DL BDL 0.3 BDL_BDL BDL Other DL BDL 0.3 BDL_BDL BDL Other DL BDL 0.3 BDL_BDL BDL Other DL BDL 0.3 BDL_BDL BDL Other DL BDL 0.3 BDL_BDL BDL Other DL BDLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final 0.08 Yes, Check DL Other DL Set Aside 0.08 Yes, Check DL Other DL Set Aside 0.08 Yes, Check DL Other DL Set Aside 0.08 Yes, Check DL Other DL Set Aside 0.08 Yes, Check DL Other DL Set Aside 0.08 Yes, Check DL Other DL Set Aside

Total Runs 6 No. Set Aside 6 No. Use 0 No. BDL 0 No. ADL 0 % BDL #DIV/0! % ADL #DIV/0!**Cadmium Total**

**Blank Corrected ug Cadmium Fraction**  **Status Cadmium Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL 3.476 ADL_ADL ADL Other DL ADL 2.7 ADL_BDL DLL Other DL ADL 4.38 ADL_BDL DLL Other DL ADL 0.371 ADL_BDL DLL Other DL ADL 1.21 ADL_BDL DLL Other DL ADL 0.329 ADL_BDL DLL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Chromium Total**

**Blank Corrected ug Chromium Fraction**  **Status Chromium Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL 94.747 ADL_ADL ADL Other DL ADL 257.097 ADL_ADL ADL Other DL ADL 59.027 ADL_ADL ADL Other DL ADL 68.637 ADL_ADL ADL Other DL ADL 17.087 ADL_ADL ADL Other DL ADL 31.707 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Cobalt Total Blank**

**Corrected ug Cobalt Fraction**  **Status Cobalt Run Status** **Detection Limit Comments**  If DLL or ADL, ADL 1.655 ADL_ADL ADL Other DL ADL 0.912 ADL_ADL ADL Other DL ADL 0.884 ADL_ADL ADL Other DL ADL 0.729 ADL_ADL ADL Other DL ADL 0.672 BDL_ADL DLL Other DL ADL 0.368 BDL_ADL DLL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Lead Total Blank**

**Corrected ug Lead Fraction**  **Status Lead Run Status**  **Detection Limit Comments**  If DLL or ADL, ADL 10.6752 ADL_ADL ADL Other DL ADL 5.6852 ADL_ADL ADL Other DL ADL 12.2152 ADL_ADL ADL Other DL ADL 8.5052 ADL_ADL ADL Other DL ADL 7.8552 ADL_ADL ADL Other DL ADL 7.1842 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Ma nganese Total** 

**Blank Corrected ug Ma** **nganese Fraction Status**  **Ma nganese Run**  **Status Detection Limit** 

**Comments** If DLL or ADL, ADL 18.75 Other DL 13.39 ADL_ADL ADL Other DL ADL 14.05 ADL_ADL ADL Other DL ADL 12.87 ADL_ADL ADL Other DL ADL 31.36 Other DL 8.03 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final

Use ADL Use ADL Use ADL

Use ADL

Total Runs 4 No. Set Aside 0 No. Use 4 No. BDL 0 No. ADL 4 % BDL 0 % ADL 100**Nickel Total Blank**

**Corrected ug Nickel Fraction**  **Status Nickel Run Status** **Detection Limit Comments**  If DLL or ADL, ADL 16.235 ADL_ADL ADL Other DL ADL 42.315 ADL_ADL ADL Other DL ADL 25.585 ADL_ADL ADL Other DL ADL 34.385 ADL_ADL ADL Other DL ADL 4.725 ADL_ADL ADL Other DL ADL 8.995 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Selenium Total**

**Blank Corrected ug Selenium Fraction**  **Status Selenium Run** 

**Status Detection Limit** 

**Comments** If DLL or ADL, ADL 424.6 ADL_ADL ADL Other DL ADL 99.5 ADL_ADL ADL Other DL ADL 259.4 ADL_ADL ADL Other DL ADL 25.74 ADL_ADL ADL Other DL ADL 12.7 BDL_ADL DLL Other DL ADL 16.99 ADL_ADL ADL Other DL ADLRDL (ug) Blank Corrected > RDL MDL or Other DL Use / Set Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 6 No. Set Aside 0 No. Use 6 No. BDL 0 No. ADL 6 % BDL 0 % ADL 100**Glaze_No Run No**  **Test Date Parent_Co**  **Fac_Name City**  **Stat**

**e Maj_Area** **Glaze_ID APCD_Type**  **Laboratory Analytical**  **Method Lab Method Listed in PW**  **Memo Antimony** 

**Total Blank Corrected ug**  **Antimony**

**Fraction Status**  **Antimony Run**

**Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Arsenic Total Blank**  **Corrected ug Arsenic Run** 

**Status Arsenic Run** 

**Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Beryllium Total Blank**  **Corrected ug Beryllium** 

**Run Status Beryllium** 

**Run Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Cadmium Total Blank**  **Corrected ug Cadmium** 

**Run Status Cadmium** 

**Run Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Chromium Total Blank**  **Corrected ug Chromium** 

**Run Status Chromium** 

**Run Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Cobalt Total Blank**  **Corrected ug Cobalt Run** 

**Status Cobalt Run** 

**Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Lead Total Blank**  **Corrected ug Lead Run** 

**Status Lead Run** 

**Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Manganese Total Blank**  **Corrected ug Manganese** 

**Run Status Manganese** 

**Run Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Nickel Total Blank**  **Corrected ug Nickel Run** 

**Status Nickel Run** 

**Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL

114; 116; 117; 119 1 5/13-15/2010Dal-Tile Corp. Dal ItaliaMuskogee OKMajor GL 7 - 10Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.869 ADL_BDL DLL Other DL ADL Use ADL 1.2 BDL_ADL DLL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.271 ADL_BDL DLL Other DL ADL Use ADL 2.4 ADL_ADL ADL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.30 No Use BDL 1.333 ADL_ADL ADL Other DL ADL Use ADL 20.395 Other DL 1.811 ADL_ADL ADL Other DL ADL

114; 116; 117; 119 2 5/13-15/2010Dal-Tile Corp. Dal ItaliaMuskogee OKMajor GL 7 - 10Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.32 ADL_BDL DLL Other DL ADL Use ADL 1.2 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.1511 BDL_ADL DLL Other DL ADL Use ADL 2.0 ADL_ADL ADL Other DL ADL Use ADL 0.464 BDL_ADL DLL Other DL ADL Use ADL 1.38 ADL_ADL ADL Other DL ADL Use ADL 38.88 Other DL 6.594 ADL_ADL ADL Other DL ADL

114; 116; 117; 119 3 5/13-15/2010Dal-Tile Corp. Dal ItaliaMuskogee OKMajor GL 7 - 10Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.3 BDL_BDL BDL Other DL BDL 1.10 No Use BDL 1.2 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.15 BDL_BDL BDL Other DL BDL 0.03 Yes, Check DL Other DL Set Aside 1.0 BDL_ADL DLL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.30 No Use BDL 0.841 ADL_ADL ADL Other DL ADL Use ADL 1.15 ADL_ADL ADL Other DL ADL Use ADL 1.334 ADL_ADL ADL Other DL ADL

71 1 5/26/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-1 Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.3 BDL_BDL BDL Other DL BDL 1.10 No Use BDL 1.2 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.15 BDL_BDL BDL Other DL BDL 0.03 Yes, Check DL Other DL Set Aside 1.6 ADL_ADL ADL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.30 No Use BDL 1.347 ADL_ADL ADL Other DL ADL Use ADL 2.806 ADL_ADL ADL Other DL ADL Use ADL 0.428 ADL_ADL ADL Other DL ADL

71 2 5/26/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-1 Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.3 BDL_BDL BDL Other DL BDL 1.10 No Use BDL 1.2 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.15 BDL_BDL BDL Other DL BDL 0.03 Yes, Check DL Other DL Set Aside 1.2 ADL_ADL ADL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.30 No Use BDL 0.866 ADL_ADL ADL Other DL ADL Use ADL 19.02 Other DL 0.682 ADL_ADL ADL Other DL ADL

71 3 5/27/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-1 Baghouse/Fabric FilterALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.3 BDL_BDL BDL Other DL BDL 1.10 No Use BDL 1.2 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.1932 BDL_ADL DLL Other DL ADL Use ADL 0.4 ADL_ADL ADL Other DL ADL Use ADL 1.02 BDL_ADL DLL Other DL ADL Use ADL 0.554 BDL_ADL DLL Other DL ADL Use ADL 4.02 ADL_ADL ADL Other DL ADL Use ADL 4.922 ADL_ADL ADL Other DL ADL

73, 74, 75 1 5/24/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-3, 4, 5Wet Scrubber ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1.454 ADL_ADL ADL Other DL ADL Use ADL 1.9 ADL_ADL ADL Other DL ADL Use ADL 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.298 ADL_ADL ADL Other DL ADL Use ADL 152.4 ADL_ADL ADL Other DL ADL Use ADL 17.534 ADL_ADL ADL Other DL ADL Use ADL 17.11 ADL_ADL ADL Other DL ADL Use ADL 1292.62 ADL_ADL ADL Other DL ADL Use ADL 5.276 ADL_ADL ADL Other DL ADL

73, 74, 75 2 5/25/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-3, 4, 5Wet Scrubber ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 6.08 ADL_ADL ADL Other DL ADL Use ADL 3.0 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.15 BDL_BDL BDL Other DL BDL 0.03 Yes, Check DL Other DL Set Aside 343.2 ADL_ADL ADL Other DL ADL Use ADL 14.7 ADL_BDL DLL Other DL ADL Use ADL 5.11 ADL_ADL ADL Other DL ADL Use ADL 526.45 ADL_ADL ADL Other DL ADL Use ADL 9.892 ADL_ADL ADL Other DL ADL

73, 74, 75 3 5/25/2010Florim Ceramiche S.p.A Florim USA Clarksville TNMajor GL-3, 4, 5Wet Scrubber ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 0.757 ADL_BDL DLL Other DL ADL Use ADL 3.0 BDL_BDL BDL Other DL BDL 0.40 Yes, Check DL Other DL Set Aside 0.3 BDL_BDL BDL Other DL BDL 0.08 Yes, Check DL Other DL Set Aside 0.154 ADL_BDL DLL Other DL ADL Use ADL 149.1 ADL_ADL ADL Other DL ADL Use ADL 14.7 ADL_BDL DLL Other DL ADL Use ADL 3.56 ADL_ADL ADL Other DL ADL Use ADL 221.56 ADL_ADL ADL Other DL ADL Use ADL 7.158 ADL_ADL ADL Other DL ADL

Total Runs 9 Total Runs 9 Total Runs 9 Total Runs 9 Total Runs 9 Total Runs 9 Total Runs 9 Total Runs 6 No. Set Aside 0 No. Set Aside 7 No. Set Aside 9 No. Set Aside 4 No. Set Aside 0 No. Set Aside 0 No. Set Aside 0 No. Set Aside 0 No. Use 9 No. Use 2 No. Use 0 No. Use 5 No. Use 9 No. Use 9 No. Use 9 No. Use 6 No. BDL 4 No. BDL 0 No. BDL 0 No. BDL 0 No. BDL 0 No. BDL 4 No. BDL 0 No. BDL 0 No. ADL 5 No. ADL 2 No. ADL 0 No. ADL 5 No. ADL 9 No. ADL 5 No. ADL 9 No. ADL 6 % BDL 44 % BDL 0 % BDL #DIV/0! % BDL 0 % BDL 0 % BDL 44 % BDL 0 % BDL 0 % ADL 56 % ADL 100 % ADL #DIV/0! % ADL 100 % ADL 100 % ADL 56 % ADL 100 % ADL 100

09000064819365f1 Glazing Page 1 of 2 12/1/2014RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final **Selenium Total Blank**  **Corrected ug Selenium** 

**Run Status Selenium** 

**Run Status Detection** 

**Limit Comment**  If DLL or ADL,

ADL RDL (ug) Blank Corrected > RDL MDL or Other

DL Use / Set Aside Final

Use ADL 3.59 BDL_ADL DLL Other DL ADL Use ADL

Use ADL 3 BDL_BDL BDL Other DL BDL 0.80 Yes, Check DL Other DL Set Aside

Use ADL 3 BDL_BDL BDL Other DL BDL 0.80 Yes, Check DL Other DL Set Aside

Use ADL 3 BDL_BDL BDL Other DL BDL 0.80 Yes, Check DL Other DL Set Aside

Use ADL 3.06 BDL_ADL DLL Other DL ADL Use ADL

Use ADL 3 BDL_BDL BDL Other DL BDL 0.80 Yes, Check DL Other DL Set Aside

Use ADL 3.85 BDL_ADL DLL Other DL ADL Use ADL

Use ADL 3.02 BDL_ADL DLL Other DL ADL Use ADL

Use ADL 3.11 BDL_ADL DLL Other DL ADL Use ADL

Total Runs 9 Total Runs 9 No. Set Aside 0 No. Set Aside 4 No. Use 9 No. Use 5 No. BDL 0 No. BDL 0 No. ADL 9 No. ADL 5 % BDL 0 % BDL 0 % ADL 100 % ADL 100

09000064819365f1 Glazing Page 2 of 2 12/1/2014**RTI**

**Inventory Kiln ID**  **FA CID** **Test Date Run** **Company Plant Location**  **(City/State) AP** **CD Type** 19 & 20KOHL-TX8/23-24/20101Kohler Co.Brownwood, TXNone 19 & 20KOHL-TX8/23-24/20102Kohler Co.Brownwood, TXNone 19 & 20KOHL-TX8/23-24/20103Kohler Co.Brownwood, TXNone 33KOHL-WI8/3-4/20101Kohler Co.Kohler, WI None 33KOHL-WI8/3-4/20102Kohler Co.Kohler, WI None 33KOHL-WI8/3-4/20103Kohler Co.Kohler, WI None 2KOHL-SC8/10-11/20101Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20102Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20103Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20101Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20102Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20103Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20101Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20102Kohler Co.Spartanburg, SCNone 2KOHL-SC8/10-11/20103Kohler Co.Spartanburg, SCNone 7KOHL-SC8/12-13/20101Kohler Co.Spartanburg, SCNone 7KOHL-SC8/12-13/20102Kohler Co.Spartanburg, SCNone 7KOHL-SC8/12-13/20103Kohler Co.Spartanburg, SCNone**New-Source ID Laboratory**  **An alytical M** **ethod Lab Method Listed in PW**  **Me mo**  TK #6/12 POC stackALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #6/12 POC stackALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #6/12 POC stackALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #19 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #19 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #19 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 EE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 EE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 EE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 FE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 FE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #2 FE stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #8 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #8 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA TK #8 POC stack ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA**An timony** 

**Run Total Blank**  **Corrected ug An** **timony**

**Fraction Status**  **An timony** 

**Run Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL 0.695 ADL_ADL ADL Other DL ADL 0.378 ADL_ADL ADL Other DL ADL 0.307 ADL_ADL ADL Other DL ADL 0.209 ADL_ADL ADL Other DL ADL 0.619 ADL_ADL ADL Other DL ADL 5.15 ADL_ADL ADL Other DL ADL 0.382 ADL_ADL ADL Other DL ADL 0.376 ADL_ADL ADL Other DL ADL 3.107 ADL_ADL ADL Other DL ADL 1.647 ADL_ADL ADL Other DL ADL 0.337 ADL_ADL ADL Other DL ADL 0.3 ADL_ADL ADL Other DL ADL 1.788 ADL_ADL ADL Other DL ADL 0.295 BDL_ADL DLL Other DL ADL 0.242 BDL_ADL DLL Other DL ADL 0.364 BDL_ADL DLL Other DL ADL 0.277 BDL_ADL DLL Other DL ADL 0.282 BDL_ADL DLL Other DL ADLMDL or Other

DL Use / Set

Aside Final **Ar senic Run**  **Total Blank Corrected ug** **Ar senic** 

**Fraction Status**  **Ar senic Run** 

**Status Detection** 

**Limit Comment**  Use ADL 9.54 ADL_ADL ADL Other DL Use ADL 8.39 ADL_ADL ADL Other DL Use ADL 10.53 ADL_ADL ADL Other DL Use ADL 16.36 ADL_ADL ADL Other DL Use ADL 30.5 ADL_ADL ADL Other DL Use ADL 35.8 ADL_ADL ADL Other DL Use ADL 21.91 ADL_ADL ADL Other DL Use ADL 18.52 ADL_ADL ADL Other DL Use ADL 32.97 ADL_ADL ADL Other DL Use ADL 2.75 ADL_BDL DLL Other DL Use ADL 1.2 BDL_BDL BDL Other DL Use ADL 1.2 BDL_BDL BDL Other DL Use ADL 1.951 ADL_ADL ADL Other DL Use ADL 2.042 ADL_ADL ADL Other DL Use ADL 1.724 ADL_ADL ADL Other DL Use ADL 6.1 ADL_ADL ADL Other DL Use ADL 7.83 ADL_ADL ADL Other DL Use ADL 6.89 ADL_ADL ADL Other DL

Total Runs 18 No. Set Aside 0 No. Use 18 No. BDL 0 No. ADL 18 % BDL 0 % ADL 100If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL Use / Set

Aside Final **Beryllium Run Total**  **Blank Corrected ug**  ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 BDL 0.40 Yes, Check DLOther DL Set Aside 0.3 BDL 0.40 Yes, Check DLOther DL Set Aside 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3 ADL Use ADL 0.3

Total Runs 18 No. Set Aside 2 No. Use 16 No. BDL 0 No. ADL 16 % BDL 0 % ADL 100**Beryllium**

**Fraction Status**  **Beryllium**

**Run Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DL BDL_BDL BDL Other DL BDL 0.08 Yes, Check DLOther DLUse / Set

Aside Final **Cadmium Run Total**  **Blank Corrected ug** **Cadmium**

**Fraction Status**  **Cadmium**

**Run Status Detection** 

**Limit Comment** If DLL or ADL,

ADL Set Aside 0.34 ADL_BDL DLL Other DL ADL Set Aside 0.31 ADL_ADL ADL Other DL ADL Set Aside 0.86 ADL_BDL DLL Other DL ADL Set Aside 0.53 ADL_ADL ADL Other DL ADL Set Aside 0.85 ADL_ADL ADL Other DL ADL Set Aside 1.17 ADL_ADL ADL Other DL ADL Set Aside 479.27 ADL_ADL ADL Other DL ADL Set Aside 470.23 ADL_ADL ADL Other DL ADL Set Aside 494.23 ADL_ADL ADL Other DL ADL Set Aside 502.54 ADL_ADL ADL Other DL ADL Set Aside 483.94 ADL_ADL ADL Other DL ADL Set Aside 510.25 ADL_ADL ADL Other DL ADL Set Aside 483.20 ADL_ADL ADL Other DL ADL Set Aside 499.35 ADL_ADL ADL Other DL ADL Set Aside 513.38 ADL_ADL ADL Other DL ADL Set Aside 249.12 ADL_ADL ADL Other DL ADL Set Aside 1.35 ADL_ADL ADL Other DL ADL Set Aside 0.17 ADL_BDL DLL Other DL ADL

Total Runs 18 No. Set Aside 18 No. Use 0 No. BDL 0 No. ADL 0 % BDL #DIV/0! % ADL #DIV/0!RDL (ug)Blank Corrected > RDL MDL or Other

DL Use / Set

Aside Final **Chromium Run Total**  **Blank Corrected ug** **Chromium**

**Fraction Status**  Use ADL 10.29 ADL_ADL Use ADL 11.07 ADL_ADL Use ADL 11.10 ADL_ADL Use ADL 15.93 ADL_ADL Use ADL 20.85 ADL_ADL Use ADL 31.03 ADL_ADL Use ADL 37.60 ADL_ADL Use ADL 44.13 ADL_ADL Use ADL 40.28 ADL_ADL Use ADL 75.21 ADL_ADL Use ADL 11.59 ADL_ADL Use ADL 3.11 ADL_ADL Use ADL 11.03 ADL_ADL Use ADL 12.77 ADL_ADL Use ADL 5.76 ADL_ADL Use ADL 6.94 ADL_ADL Use ADL 6.00 ADL_ADL Use ADL 6.14 ADL_ADL

Total Runs 18 No. Set Aside 0 No. Use 18 No. BDL 0 No. ADL 18 % BDL 0 % ADL 100**Chromium**

**Run Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL Use / Set

Aside ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use

Total Runs No. Set Aside No. Use No. BDL No. ADL % BDL % ADLFinal **Cobalt Run Total Blank**  **Corrected ug Cobalt** 

**Fraction Status**  **Cobalt Run**

**Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug) ADL 0.63 ADL_ADLADL Other DL ADL ADL 1.27 BDL_ADLDLL Other DL ADL ADL 0.39 BDL_ADLDLL Other DL ADL ADL 0.77 ADL_ADLADL Other DL ADL ADL 0.72 ADL_ADLADL Other DL ADL ADL 0.88 ADL_ADLADL Other DL ADL ADL 2.13 ADL_ADLADL Other DL ADL ADL 1.82 ADL_ADLADL Other DL ADL ADL 1.03 ADL_ADLADL Other DL ADL ADL 3.14 ADL_ADLADL Other DL ADL ADL 0.63 ADL_ADLADL Other DL ADL ADL 0.39 BDL_ADLDLL Other DL ADL ADL 0.48 ADL_ADLADL Other DL ADL ADL 0.64 BDL_ADLDLL Other DL ADL ADL 0.34 BDL_ADLDLL Other DL ADL ADL 0.63 BDL_ADLDLL Other DL ADL ADL 0.38 BDL_ADLDLL Other DL ADL ADL 0.37 BDL_ADLDLL Other DL ADL

18 0 18 0 18 0 100Blank Corrected

> RDL MDL or Other

DL Use / Set

Aside Final **Lead Run Total Blank**  **Corrected ug Lead Fraction** 

**Status Lead Run** 

**Status** Use ADL 46.23 ADL_ADL ADL Use ADL 54.11 ADL_ADL ADL Use ADL 44.53 ADL_ADL ADL Use ADL 43.08 ADL_ADL ADL Use ADL 55.59 ADL_ADL ADL Use ADL 47.29 ADL_ADL ADL Use ADL 71.63 ADL_ADL ADL Use ADL 67.10 ADL_ADL ADL Use ADL 59.98 ADL_ADL ADL Use ADL 183.81 ADL_ADL ADL Use ADL 28.45 ADL_ADL ADL Use ADL 6.19 ADL_ADL ADL Use ADL 17.14 ADL_ADL ADL Use ADL 12.38 ADL_ADL ADL Use ADL 6.85 ADL_ADL ADL Use ADL 8.29 ADL_ADL ADL Use ADL 6.69 ADL_ADL ADL Use ADL 6.67 ADL_ADL ADL

Total Runs 18 No. Set Aside 0 No. Use 18 No. BDL 0 No. ADL 18 % BDL 0 % ADL 100**Detection**

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL Use / Set

Aside Final Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL Other DL ADL Use ADL

Total Runs 18 No. Set Aside 0 No. Use 18 No. BDL 0 No. ADL 18 % BDL 0 % ADL 100**Ma nganese** 

**Run Total Blank**  **Corrected ug Ma** **nganese**

**Fraction Status**  **Ma nganese** 

**Run Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL 2.20 ADL_ADL ADL Other DL ADL 265.29 Other DL 1.42 ADL_ADL ADL Other DL ADL 2.15 ADL_ADL ADL Other DL ADL 2.87 ADL_ADL ADL Other DL ADL 2.73 ADL_ADL ADL Other DL ADL 2.08 ADL_ADL ADL Other DL ADL 2.91 ADL_ADL ADL Other DL ADL 5.95 ADL_ADL ADL Other DL ADL 57.92 ADL_ADL ADL Other DL ADL 9.10 ADL_ADL ADL Other DL ADL 3.22 ADL_ADL ADL Other DL ADL 2.64 ADL_ADL ADL Other DL ADL 13.22 ADL_ADL ADL Other DL ADL 2.24 ADL_ADL ADL Other DL ADL 2.73 ADL_ADL ADL Other DL ADL 30.27 Other DL 1.21 ADL_ADL ADL Other DL ADLMDL or Other

DL Use / Set

Aside Final **Nickel Run Total Blank**  **Corrected ug Nickel** 

**Fraction Status**  **Nickel Run**

**Status Detection** 

**Limit Comment**  Use ADL 1.23 ADL_ADL ADL Other DL 1.92 ADL_ADL ADL Other DL Use ADL 0.92 ADL_ADL ADL Other DL Use ADL 9.92 ADL_ADL ADL Other DL Use ADL 4.78 ADL_ADL ADL Other DL Use ADL 6.08 ADL_ADL ADL Other DL Use ADL 6.40 ADL_ADL ADL Other DL Use ADL 7.27 ADL_ADL ADL Other DL Use ADL 4.33 ADL_ADL ADL Other DL Use ADL 37.78 ADL_ADL ADL Other DL Use ADL 7.37 ADL_ADL ADL Other DL Use ADL 2.10 ADL_ADL ADL Other DL Use ADL 2.01 ADL_ADL ADL Other DL Use ADL 3.67 ADL_ADL ADL Other DL Use ADL 1.08 ADL_ADL ADL Other DL Use ADL 1.32 ADL_ADL ADL Other DL 0.87 ADL_ADL ADL Other DL Use ADL 0.90 ADL_ADL ADL Other DL

Total Runs 16 No. Set Aside 0 No. Use 16 No. BDL 0 No. ADL 16 % BDL 0 % ADL 100If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL Use / Set

Aside Final **Selenium Run Total Blank**  **Corrected ug** ADL Use ADL 125.90 ADL Use ADL 117.40 ADL Use ADL 136.50 ADL Use ADL 22.33 ADL Use ADL 43.97 ADL Use ADL 42.20 ADL Use ADL 62.99 ADL Use ADL 50.76 ADL Use ADL 99.00 ADL Use ADL 11.10 ADL Use ADL 3.40 ADL Use ADL 3.00 ADL Use ADL 16.02 ADL Use ADL 14.60 ADL Use ADL 16.73 ADL Use ADL 99.30 ADL Use ADL 119.20 ADL Use ADL 100.90

Total Runs 18 No. Set Aside 0 No. Use 18 No. BDL 0 No. ADL 18 % BDL 0 % ADL 100**Selenium**

**Fraction Status**  **Selenium Run**

**Status Detection** 

**Limit Comment** If DLL or ADL,

ADL RDL (ug)Blank Corrected > RDL MDL or Other

DL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_BDL DLL Other DL ADL BDL_ADL DLL Other DL ADL BDL_BDL BDL Other DL BDL 0.80 Yes, Check DLOther DL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADL ADL_ADL ADL Other DL ADLUse / Set

Aside Final Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL Set Aside Use ADL Use ADL Use ADL Use ADL Use ADL Use ADL

Total Runs 18 No. Set Aside 1 No. Use 17 No. BDL 0 No. ADL 17 % BDL 0 % ADL 100**ICP/A ES or A**  **A ICP/MS or GFA** 

**A RDL (μg)**  **RDL (μg)** Antimony 1.20E+01 1.10E+00 Arsenic 1.90E+01 4.00E-01 Beryllium 1.10E-01 8.00E-02 Cadmium 1.50E+00 3.00E-02 Chromium 2.50E+00 3.00E-01 Cobalt 2.50E+00 3.00E-01 Lead 1.50E+01 3.00E-01 Manganese 7.00E-01 3.00E-01 Nickel 5.40E+00 5.40E+00 Selenium 2.70E+01 8.00E-01



### Westlin, P., and R. Merrill.Data and procedure for handling below detection level data in analyzing various pollutant emissions databases for MACT and RTR emissions limits

. Memorandum from Peter Westlin, SPPD, MPG and Ray mond Merrill, AQAD, MTG, to SPPD management and MACT rule writers. December 13, 2011. **Method 29 Non-Hg HA P M** **etals**