### Mr. Robert Hurt, Director Environmental Health & Safety Dal

- Tile Corporation P.O. Box 170130 7834 C.F. Hawn Freeway Dallas, T exas 75217

Re: Requirement to provide information according to Title 42 of the United States Code, Chapter 85, Subchapter I, Part A, S ection 7414 ( 42 U.S.C 7414)

Dear Mr. Hurt :

Pursuant to section 114 of the Clean Air Act (CAA), the U.S. Environmental Protection Agency (EPA) is requesting that you provide information on the following :

• S tartup and shutdown events at all of your clay ceramics manufacturing facilities, as described in Enclosure 1

.

• E missions of hydrogen fluoride (HF), hydrochloric acid (HCl), metals, dioxins/furans, and particulate matter (PM) from the kilns listed in Enclosure 2.

• E missions of metals and PM fro m th e glaze lines listed in Enclosure 2 that spray apply the glaze.

• E missions of dioxins/furans from the tile dryers and spray dryers listed in Enclosure 2

. We request that you send this information to us by July 16, 2010

.
Enclosure 3 provides additional i nformation on the pollutants to be tested and the requirements for conducting and reporting the emission tests.

Enclosure 4 contains a summary of our legal authority in section 114 of the CAA to obtain the information that is now being requested

. If you b elieve that providing any specific information to us would reveal a trade secret, please identify this information clearly in the test report (s) that you submit in response to this request

. Enclosure 4 describes the type of information that EPA may ask of you at a later time to prove that any information you have so2



### identified is truly confidential

. Any information determined to be a trade secret will be protected by 18 U.S.C. 1905

. If you do not claim as confidential any of the information you submit in response to this request, we can make the information available to the public without notifying you further (40 CFR Part 2.203, September 1, 1976)

. Because section 114 of the CAA does not allow emissions data to be claimed as confidential, the emissions data you provide to us can be made available to the public

. A detailed explanation of what we consider to be emissions data is contained in Enclosure 5. Please take note of Enclosure 5 when identifying any information in your submittal that you are claim ing as confidential.

We have contracted RTI International (RTI) (Contract No. EP

- D

- 06

- 118) to help us gather information about your industry

. As noted in Enclosure 6 , we have designated RTI to be our authorized representative

. Therefore, RTI has the same rights discussed above and in Enclosure 4 as EPA has

. This means that RTI will have access to all information you provide to

us

. As a designated representative of the Agency, RTI must, by law, also abide by the requirements of 42 U.S.C. 7414(c) in regar d to the confidentiality of what you claim to be trade
secrets.

Enclosure 7 summarizes our policies and procedures for handling trade secret information and describes how our contractor also is required to use the same procedures as we do

. Because our con tractors or other authorized representatives are required to follow the requirements in Enclosure 6 , your rights and any privileged information you submit to us will be protected

.

E ach facility subject to emissions testing should prepare a site

- specific te st plan prior to testing. A site

- specific test plan addresses the planning and quality assurance and quality control procedures and acceptance criteria for all of the testing, including the collection of process data. Please note that you do not have to submit a test plan to EPA for approval prior to testing. However, the EPA Electronic Reporting Tool (ERT) Version 3, in which EPA requires that data be reported, requires that a test plan be entered into the program prior to submitting test results. Encl osure 8 provides an example of the EPA ERT Version 3 test plan. Enclosure 9 provides guidance for developing a site

- specific test plan.

You are requested to notify your state air regulatory agency or designated permitting authority at least 21 days before the requested stack tests are scheduled to begin. Detailed instructions on how and where to submit the data are provided in Section 4.0 of Enclosure 3.

If you have questions regarding the need for this request or need clarification on the information we are requesting, please contact Jeffrey Telander with EPA’s Office of Air Quality Planning and Standards at 919

- 541

- 5427 (e

- mail: telander.jeff@epa.gov )

. Please return the requested information to Mr. Telander by July 16, 2010

.3



### The collection of the information requested in this letter is part of EPA’s effort to obtain the best information available to develop the standard

. Your help in providing this information is greatly appreciated.

Sincerely,

Peter Tsi rigotis Director, Sector Policies and Programs Division

Office of Air Quality Planning and Standards

9 Enclosures

Enclosure 1: Startup and shutdown s urvey Enclosure 2: Emissions sources to be t ested Enclosure 3: Summary of t est p rocedures, methods, a nd r eporting r equirements Enclosure 4: EPA’s information gathering a uthority Enclosure 5: Clarification of what EPA considers to be emissions data Enclosure 6: Summary of contractor’s authority as representative of EPA Enclosure 7: Procedures for safeguard ing CBI under the CAA Enclosure 8: Example EPA ERT Version 3 test plan Enclosure 9: Site

- specific test plan development guidance

cc: Eddie Terrill , Director, Air Quality Division

, Oklahoma Department of Environmental Quality (w/o enclosures) David Bryme r , Director, Air Quality Division

, Texas Commission on Environmental

Quality (w/o enclosures) T h om as Diggs, Associate Director for Air Programs

, U.S. Environmental Protection

Agency, Region VI (w/o enclosures)

### Enclosure 1

The questions below apply to startup and shutdown that resulted in exceedances of permit conditions at an affected source or portion of an affected source.

1. Please provide the following information for your facility:

A. Facility ID, consisting of the first four letters in the parent company name, followed by a number (e.g., ABCD

- 1, ABCD

- 2, etc.) ;
B. Facility name;

C. Address (including city, state, and zip code);

D. Mailing address (if different); and

E. Latitude and longitude coordinates of t he facility.

2. For each startup and shutdown event that occurred over the last 3 years, please provide the following information requested in A. through J

. A. Using the definitions provided below, indicate whether the event was a startup or shutdown. Startup : the setting in operation of an affected source or portion of an affected source for any purpose. Shutdown : the cessation of operation of an affected source or portion of an affected source for any purpose.

B. A description of the event, includ ing identification of the emissions source or sources associated with the startup or shutdown;

C. Whether any permit condition was exceeded and, if so, what permit condition was exceeded;

D. Whether the event was covered by any contingency plan for con trolling emissions during startup and shutdown events and, if so, whether the plan was followed; if the plan was not followed, why not;

E. The duration of the event;

F. The actions taken to minimize emissions during the event, including the use of any backup control systems;

G. Estimates or measurements, if any, of emissions during the event; if you did not have the ability to quantify emissions during the event, please explain why;

### Enclosure 1

H. Whether the emission profile of each unit was different during s tartup and shutdown than during normal operating conditions and, if so, how emissions we re different and why ; please pro vide any supporting information;

I. All performance test data collected during each period of startup and shutdown ; the test method us ed for each event; when the testing was conducted and why; the test conditions at the time of testing; and whether the tests were associated with a routine startup or shutdown; and

J. All monitoring data, including control system parameter monitoring, co llected during each period of startup and shutdown

. If this information is contained in periodic and immediate startup and shutdown reports (either stand

- alone or contained within the periodic excess emissions report) submitted to your permitting authorit y, you may submit copies of those reports instead.

3 . Please submit a copy of your startup and shutdown plan if you are required to develop one.

4 . Optional: Do you wish to recommend a standard that would apply during startup or shutdown? If so, plea se describe the type of event to which the standard would apply; the recommended standard (this could be an emission limitation, work practice, or operational standard) that would apply during the period; the basis for the recommended standard; why and how the standard would minimize emissions during the event; and how would compliance be determined and/or monitored.

### Enclosure 2

Kilns, Glaze Lines, Dryers, and Spray Dryers to be Tested No. EU ID EU Type Control Device Control/Stack ID Pollutants to Test a Dal Italia

– Muskogee, OK b 1 RK

- 3 Roller Kiln Wet Scrubber EPN

- 29 (combined stack) HF, HCl, metals, dioxins/fura ns, PM/PM 2.5 (filterable), PM 2.5 (condensable) 2 RK

- 4 Roller Kiln 3 GL

- 7 Glaze Line Fabric Filter EPN

- 21 (combined stack) PM/PM 2.5 (filterable), metals 4 GL

- 8 Glaze Line 5 GL

- 9 G laze Line 6 GL

- 10 Glaze Line 7 EPN

- 7 Tile Dryer None EPN

- 7 D ioxins/furans OR EPN

- 8 Tile Dryer None EPN

- 8 Dioxins/furans

OR EPN

- 9 Tile Dryer None EPN

- 9 Dioxins/furans

OR EPN

- 10 Tile Dryer None EPN

- 10 Dioxins/furans OR EPN

- 11 Tile Dryer None EPN

- 11 Dioxins/furans OR EPN

- 12 Tile Dryer None EPN

- 12 Dioxins/furans OR EPN

- 30 Tile Dryer None EPN

- 30 Dioxins/furans OR EPN

- 31 Tile Dryer None EPN

- 31 Dioxins/furans OR EPN

- 32 Tile Dryer None EPN

- 32 Dioxins/furans OR EPN

- 33 Tile Dryer None EPN

- 33 Dioxins/furan s 8 EPN

- 5 Spray Dryer Fabric Filter EPN

- 5 Dioxins/furans OR EPN

- 36 Spray Dryer Fabric Filter EPN

- 36 Dioxins/furans

### 2 No. EU ID EU Type Control Device Control/Stack ID Pollutants to Test a Dal

- Tile

– El Paso, TX c 1 RK

- 1 Roller Kiln None EPN

- 29 (combined stack) Metals, dioxins/furans, PM/PM 2.5 (filterable), PM 2.5 (cond ensable) 2 RK

- 2 Roller Kiln 3 RK

- 3 Roller Kiln 4 RK

- 4 Roller Kiln 5 RK

- 5 Roller Kiln 6 RK

- 6 Roller Kiln 7 RK

- 7 Roller Kiln 8 RK

- 8 Roller Kiln 9 RK

- 9 Roller Kiln 10 RK

- 10 Roller Kiln 11 RK

- 11 Roller Kiln 12 RK

- 12 Rol ler Kiln 13 DC

- 1 Tile Dryer None EPN

- 6 Dioxins/furans OR DC

- 2 Tile Dryer None EPN

- 5 Dioxins/furans

OR DC

- 3 Tile Dryer None EPN

- 15 Dioxins/furans

OR DC

- 4 Tile Dryer None EPN

- 14 Dioxins/furans

OR DC

- 5 Tile Dryer None EPN

- 2 0 Dioxins/furans

OR DC

- 6 Tile Dryer None EPN

- 24 Dioxins/furans 14 SD

- 1 S pray Dryer Wet Scrubber EPN

- 11 Dioxins/furans

a HF = hydrogen fluoride, HCl = hydrochloric acid, PM = particulate matter , PM 2.5 = PM with an aerodynamic diameter of up to 2. 5 micrometers

. Note: Metals analysis requires weighing the filter and reporting that value as PM filterable.
b The company has indicated it also plans to test RK

- 1 and 2 for HF and HCl using Method 320, to replace the currently available Method 26A data for those kilns, data which the company does not consider representative. However, EPA is not requiring such testing, becaus e RK

- 3 and 4 are considered representative of RK

- 1 and 2 (i.e., same raw materials, process equipment, emission control device, an d equipment size).

c Because t he glaze lines at the El Paso plant do not spray apply the glaze, they are not included in this table

.

### Enclosure 3

Summary of Test Procedures, Methods, and Reporting Requirements This document provides an overview of approved methods, target pollutant units of measure, and reporting requirements for ceramic tile industry emissions test ing

. Refer to Enclos ure 2 of the Section 114 letter you received for the specific sources and pollutants for which emissions data are requested

. This document is organized as follows:

1.0 Stack Testing Procedures and Methods 2.0 How to Report Data 3.0 How to Submit Data 4.0 Contact Information for Questions on Test Plan and Reporting 

## 1.0 Stack Testing Procedures and Methods

1. 1 How to Select Sample Location and Gas Composition Analysis Methods 

### U.S. EPA Method 1 of Appendix A of Part 60 must be used to select th e locations and number of traverse points for sampling. Please note that , for sources equipped with emission controls, you are required to sample only at the outlet of the control device. If any of the sources to be tested have multiple outlets or stacks , you must test all outlets/stacks simultaneously. For a complete copy of the method and guidance information, s ee http://www.epa.gov/ttn/emc/methods/method1.html

. Analysis of flue gas compo sition, including oxygen concentration, must be performed using U.S. EPA Methods 3A or 3B of Appendix A

- 2 of Part 60. See http://www.epa.gov/ttn/emc/methods/method3a.html for Method 3A or http://www.epa.gov/ttn/emc/methods/method3b.html for Method 3B information.

1 .2 Source Test Methods


### Table 1. 1 presents a summary of the recommended test methods for each pollutant

, alternat ive methods

, minimum number of tests runs required, minimum test run duration, and units of

measure

. For copies of the recommended U.S. EPA methods and additional information, please refer to EPA’s Emission Measurement Center website: http://www.epa.gov/ttn/emc/ . If you would like to use a method not on this list, please contact EPA for approval of an alternative method.

Please take note of the following requirements regarding the emission tests:

• E xtended test runs ( 4 hours per run) are required for the EPA Method 23 tests for dioxins and f urans and for the EPA Method 29 tests for metals

.
• A ll test s must be performed with the process and emission control devices operating under normal conditions.

### 2 Please provi de a complete copy of the emission test report (s) with all appendices, including a description of test methods and any deviations from the test methods or other anomalies that occurred with the process or control device operations during the test; run

- by

- r un emission data ; sample calculations ; field data sheets and notes; laboratory data ; and quality assurance and quality control activities performed. In addition to the emission test data, you should also report the following process information recorded a t the time of, and during, the emissions test : stack or exhaust gas flow rate (as determined using U

. S

. EPA Method 2 , 2F, or 2G ); production data, as indicated in Table 1.2 ; emission control devices in use during the test; and control device operating or monitoring parameters

, as indicated in Table 1.3

.

Table 1. 1. Summary of Ceramic Tile Source Test Methods and Alternative Methods

Pollutant Recommended Method Alternative Method Minimum No. of Test Runs and Duration Target Reported Units of Measure a
Kiln s HCl and HF U.S. EPA Method 26A U.S. EPA Method 320 Three 1

- hour runs kg /hr

, kg / Mg of product

, and ppmvd @ 7% O 2 PM 2.5 (filterable) U.S. EPA Other Test Method (OTM) 27 b None Three 1

- hour runs kg /hr

, kg / Mg of product

, and mg/dscm @ 7% O 2 PM 2.5 (condens able) U.S. EPA OTM 2 8 b None Three 1

- hour runs kg /hr , kg/Mg of product

, and mg/dscm @ 7% O 2 HAP m etals and PM (filterable) c U.S. EPA Method 29 None Three 4

- hour runs with a minimum sample volume of 3.4 m 3 kg /hr , kg / Mg of product

, and mg/dscm @ 7% O 2

Diox ins/furans U.S. EPA Method 23 None Three 4

- hour runs with a minimum sample volume of 3.4 m 3 kg /hr

, kg / Mg of product

, and ng/dscm @ 7% O 2

Flow rate U.S. EPA Method 2, 2F, or 2G None Simultaneous with each pollutant test run acm m and dsc m m

O 2 U.S. EPA Meth od 3A U.S. EPA Method 3B Simultaneous with each pollutant test run Volume % , dry

Moisture U.S. EPA Method 4 None Simultaneous with each pollutant test run Volume %

Glaze Lines
PM 2.5 (filterable) U.S. EPA Other Test Method (OTM) 27 b None Three 1

- hour ru ns kg /hr

, kg / Mg of product

, and mg/dscm @ 7% O 2 HAP m etals and PM (filterable) c U.S. EPA Method 29 None Three 4

- hour runs with a minimum sample volume of 3.4 m 3 kg /hr

, kg / Mg of product

, and mg/dscm @ 7% O 2

Flow rate U.S. EPA Method 2, 2F, or 2G None Simu ltaneous with each pollutant test run acm m and dsc m m

O 2 U.S. EPA Method 3A U.S. EPA Method 3B Simultaneous with each pollutant test run Volume % , dry

Moisture U.S. EPA Method 4 None Simultaneous with each pollutant test run Volume %

### 3 Pollutant Recommended Method Alternative Method Minimum No. of Test Runs and Duration Target Reported Units of Measure a
Tile Dryers /Spray Dr yers Dioxins/furans U.S. EPA Method 23 None Three 4

- hour runs with a minimum sample volume of 3.4 m 3 kg /hr

, kg / Mg of product

, and mg/dscm @ 7% O 2

Flow rate U.S. EPA Method 2, 2F, or 2G None Simultaneous with each pollutant test run acm m and dsc m m

O 2 U.S . EPA Method 3A U.S. EPA Method 3B Simultaneous with each pollutant test run Volume % , dry

Moisture U.S. EPA Method 4 None Simultaneous with each pollutant test run Volume %

a kg /hr = kilograms per hour; kg/Mg = kilograms per megagram; ppmvd = parts per million by volume, dry basis ;

m 3 = cubic meters; mg/dscm = milligrams per dry standard cubic meter; ng/dscm = nanograms p er dry standard cubic meter; acm m = actual cubic meters per minute; and dscm m = dry standard cubic meters per minute

. See Table 1.2 f or format of production data.
b A copy of the method can be found at: http://www.epa.gov/ttn/emc/prelim.html

c Includes antimony, arsenic, beryllium, cadmium, chromium, cobalt, lead, manganese, mercu ry, nickel, and selenium. In addition, weigh filter and report as PM filterable.

Table 1. 2. Production Data Requested a
Source Type Production Data Format Kiln Megagrams of fired tile produced per hour Glaze line Volume of glaze applied per hour Total solids content of glaze HAP metal content (weight percent) of each HAP metal included in glaze formulation Spray dryer Megagrams of spray

- dried material produced per hour Tile dryer Megagrams of green tile dried per hour

a For each hour of testing or e ach test run



### .

Table 1.3 . Control Device Monitoring Requirements

Control Device a Parameters to be Monitored During Test
Wet scrubber Pressure drop, liquid flow rate, sorbent type and feed rate
DIFF Sorbent type and injection rate
DLS/FF Sorbent type an d injection rate
Fabric filter No monitoring required

a DIFF = dry sorbent injection fabric filter; DLS/FF = dry lime scrubber / fabric filter.

.



## 2 .0 How to Report Data

The method for reporting the results of any testing and monitoring requests depend s on the type of tests and the type of methods used to complete the test requirements. This section discusses the requirements for reporting the data.

### 4 2 .1 Reporting S tack T est D ata 

### If you conducted a stack test using one of the methods listed in Table 2

. 1, shown below, you must report your data using the EPA Electronic Reporting Tool (ERT) Version 3. ERT is a Microsoft ® 

### Access database application. Two versions of the ERT application are available. If you are not a registered owner of Microsoft ® 

### Access , you can install the runtime version of the ERT Application. Both versions of the ERT are available at http://www.epa.gov/ttn/chief/ert/ert_tool.html . The ERT supports an Excel spreadsheet

a pplication (which is included in the files downloaded with the ERT) to document the collection of the field sampling data. After completing the ERT, you will also need to attach an electronic copy of the emission test report (PDF format preferred) to the Attachments module of the ERT.

Table 2 .1: List of Test Methods Supported by ERT
Test Methods Supported by ERT Methods 1 through 4 Method 29 Method 3A OTM 27 Method 23 OTM 28 Method 26A



### If you conducted a stack test using a method not currently sup ported by the ERT, you must report the results of this test in a Microsoft ® 

### Excel Emission Test Template. The Excel templates are specific to each pollutant and type of unit

, and they can be downloaded from the following

w ebsite : http://icr2010.rti.org

. Y ou must report the results of each test on the appropriately labeled worksheet corresponding to the specific tests requested at your facility

. If more than one

source at your facility was tested using methods not currently supported by the ERT, you must make a copy of the worksheet and update the source ID in order to distinguish between each separate test. After completing the worksheet, you must also submit an electronic copy of the emission test report (PDF format preferred).

2 .2 Required Fields fo r ERT Reporting


### Enclosure 8 provides an EPA ERT Version 3 example test plan and lists each field within the ERT and notes whether or not the field is required or optional.

2.3 Reporting Measured Values Below the Detection Level 

### Identify the status of mea sured values relative to detection levels on the spreadsheet or in the ERT using the following descriptions:

• BDL (below detection level)

– all analytical values used to calculate and report an in

stack emissions value are less than the laboratory’s report ed detection level(s);

• DLL (detection level limited)

– at least one but not all values used to calculate and report an in

- stack emissions value are less than the laboratory’s reported detection level(s); or

• ADL (above detection level)

– all analytical val ues used to calculate and report an in

stack emissions value are greater than the laboratory’s reported detection level(s).

### 5 For each reported emissions value, insert the appropriate flag (BDL, DLL, or ADL) in the Note s line of Excel emission t est spreadsh eet template or in the Comments line of the Electronic Reporting Tool (ERT).

When reporting and calculating individual test run data:

• For analytical data reported from the lab as “nondetect” or “below detection level;”

− Include a brief description of the procedures used to determine the analytical detection and in

- stack detection levels:

o In the Note s line of Excel emission t est spreadsheet template; or

o In the Comments line of Lab Data tab in the Run Data Details in the ERT

.

− Describe these procedures comple tely in a separate attachment including the measurements made, the standards used, and the statistical procedures applied.

− Calculate in

- stack emissions rate for any analytical measurement below detection level using the relevant detection level as the “rea l” value.

− Report the calculated emissions concentration or rate result:

o As a bracketed “less than” detection level value (e.g., [<0.0105]) in the Excel emission t est spreadsheet template and include the appropriate flag in the Note s line; or

o As a “real” va lue in the ERT with the appropriate flag in the Comments line.

− Report as “real” values (i.e., no brackets or < symbol) any analytical data measured above the detection level including any data between the analytical detection level and a laboratory

- specifi c reporting or quantification level (i.e., flag as ADL).

− Apply these reporting and calculation procedures to measurements made with Method 23 :

o Report data in the Excel emission t est spreadsheet template for each of the D/F congeners measured with Method 23 below the detection level as [< detection level]

. o Do not report emissions as zero as described in the method

.

• For pollutant measurements composed of multiple components or fractions (e.g., Hg and other metals sampling trains) when the result for the valu e for any component is measured below the analytical detection level :

− Calculate in

- stack emissions rate or concentrations as outlined above for each component or fraction;

− Sum the measured and detection level values as outlined above using the in

- stack

em issions rate or concentrations for all of the components or fractions; and

− Report the sum of all components or fractions:

o As a bracketed “less than” detection level value (e.g., [<0.0105]) in the Excel emission t est spreadsheet template and include the app ropriate flag in the Note s line; or

o As a “real” value in the ERT with the appropriate flag in the Comments line.

### 6 − Report also the individual component or fraction values for each run if the Excel emission t est spreadsheet template or ERT format allows; if n ot (i.e., the format allows reporting only a single sum value):

o For the Excel emission t est spreadsheet template, next to the sum reported as above report in the Notes line the appropriate flag along with the values for the measured or detection level valu e for each component or fraction as used in the calculations (e.g., 0.036, [<0.069], 1.239, [<0.945] for a fo ur fra ction sample)

. o For the ERT , next to the sum reported as above, report on the Comments line the appropriate flag and the measured or detection level value for each component or fraction as used in the calculations (e.g., 0.036, [<0.069], 1.239, [<0.945] for a four fraction sample)

.

• For measurements conducted using instrumental test methods (e.g., Method 3A) :

− Record gaseous concentration values as measured including negative values and flag as ADL; do not report as BDL

.

− Calculate and report in

- stack emissions rates using these measured values

.

− Include relevant information relative to calibration gas values or other technical qualifiers for measur ed values in Comments line in the ERT

.

• When reporting and calculating average emissions rate or concentration for a test when some results are reported as BDL :

− Sum all of the test run values including those indicated as BDL or DLL as “real” values

.

− Calcul ate the average emissions rate or concentration (e.g., divide the sum by 3 for a three

- run test)

.

− Report the average emissions rate or concentration average:

o As a bracketed “less than” detection level value (e.g., [<20.06]) in the Excel emission t est sprea dsheet template and include the appropriate flag in the Note s line

. o As a “real” value in the ERT and include the appropriate flag in the Comments line.



## 3 .0 How to Submit Data
You may submit your data in any of the ways listed below. However, in order to avoid duplicate data and keep all data for a particular facility together, we request that you submit all of the data requested from each of your facilit ies in the same way. To submit your data:



## • E

- mail an electronic copy of all requested files to telander.jeff@epa.gov

.



## • If the files are too large for your e

- mail system, you may upload the electronic files to a FTP site ; if you would like to use this option, send an email to rjmarinshaw@rti.org for instructions on how to access the site

.

### 7 

## • Mail a CD or DVD containing an electronic copy of all requested files to the EPA address below:

Jeffrey Telander U.S. EPA Mailroom (D243

- 02) U.S. Environmental Protection Agency Office of Air Quality Planning and Standards 109 T.W. Alexander Drive Research Triangle Park, NC 27711



## • If no electronic copy is available, mail a hard copy of all requested files to the aforementioned EPA address.



## • If the process data or other information you a re providing is considered confidential, please create a separate CD or DVD containing only the confidential portion of your data or prepare a copy of the hard copy materials containing only the pages that include the information you consider confidential. Clearly mark the disk and/or materials with the words “Confidential Business Information.” Send these confidential files under separate cover to the attention of Jeff Telander at the following address :

Roberto Morales, Document Control Officer U.S. EPA Mailroom (C404

- 02) U.S. Environmental Protection Agency Office of Air Quality Planning and Standards 109 T.W. Alexander Drive Research Triangle Park, NC 27711

For the security of your data, EPA recommends sending your confidential files to Mr. Morales v ia Registered U.S. Mail using return receipt requested, Federal Express, or other method for which someone must provide a signature upon receipt. Do not electronically transmit confidential business information (CBI) to EPA. E

- mail and facsimile are not se cure forms of communication and should never be used to transmit CBI.

### 8 

## 4 .0 Contact Information for Questions on Test Plan and Reporting

For questions on how to report data using the ERT, contact : Ron Myers (U.S. EPA) (919) 541

- 5407 myers.ron@epa.gov

OR

Barrett Parker (U.S. EPA) (919) 541

- 5635 p arker. b arrett@epa.gov
For questions on the test methods , contact : Peter Westlin (U.S. EPA) (919) 541

- 1058 westlin.peter@epa.gov

OR

Gary McAlister (U.S. EPA) (919) 541

- 1062 mcalister.gary@epa.gov
For questions on the ICR and on reporting mechanisms other than the ERT, contact :
Jeff Telander (U.S. EPA) (919) 541

- 5427 telander.jeff@epa.gov

For questions on uploading files to the FTP site, contact :

Richard Marinshaw RTI International (919) 316

- 3735 rjmarinshaw@rti.org* Section 114 requires public availability of all emission data and authorizes disclosure of confidential information in certain circumstances. See 40 FR 36902 - 36912 (September 1, 1976)

(Rev. 12/8/95) 

### Enclosure 4

EPA’s Information Gathering Authority Under Section 114 of the Clean Air Act

Under Section 114 of the Act (42 U.S.C. 7414), Congr ess has given the U.S. Environmental Protection Agency broad authority to secure information needed “for the purpose of (i) developing or assisting in the development of any implementation plan under Sec tion 100 or 111(d), any standard of performance under Section 111, or any emission standard under Section 112, (ii) determining whether any person is in violation of any such standard of any requirement of such a plan, or (iii) carrying out any provision of this Act.” Among other things, Section 114 authorizes EPA to make inspections, conduct tests, examine records, and require owners or operators of emission sources to submit information reasonably required for the purpose of developing such standards. In addition, the EPA Office of General Coun sel has interpreted Section 114 to include authority to photograph or require submission of photographs of pertinent equipment, emissions, or both.

Under Section 114, EPA is empowered to obtain information described by that section even if you consider it to be confidential. You may, however, re quest that EPA treat such information as confidential. Information obtained under Section 114 a nd covered by such a request will ordinarily be released to the public only if EPA determines that the information is not entitled to confidential treatment. * Procedures to be used for making confidentiality determinations, s ubstantive criteria to be used in su ch determinations, and special rules governing information obtained under Section 114 are set forth in 40 CFR Part 2 published in the Federal Register on September 1, 1976 (40 FR 36902).

Pursuant to §2.204(a) of EPA’s Freedom of Informati on Act (FOIA) regulation, in the event a request is received, or it is determined that a request is likely to be received, or EPA desires to determine whether business information in its possession is entitled to confidentia l treatment even though no request for release of the information has been received, please be advised that EPA will seek, at that time, the following information to support your claim as required by §2.204( e)(4) of EPA’s FOIA regulations:

1. Measures taken by your company to guard agains t undesired disclosure of the information to others;

2. The extent to which the information has been disclosed to others, and the precautions taken in connection therewith;

3. Pertinent confidentiality determinations, if any, by EPA or other Federal agencies, and a copy of any such determinations, or reference to it, if available; and

4. Whether your company asserts that disclosure of the information would be likely to result in substantial harmful effects on the business’ competitive positi on, and if so, what those harmful effects would be, why they should be viewed as substantial, and an expl anation of the causal relationship between disclosure and such harmful effects.

### Enclosure 5

### January 2002



# Summary of Procedures for Safeguarding Clean Air Act Confidential Business Information

1. Purpose

This memorandum describes U.S. Environm ental Protection Agency (EPA), Office of Air Quality Planning and Standard s (OAQPS) policy and procedures set forth for the handling of information claimed as Confidential Business Information (CBI), whether submitted voluntarily or obtained under Section 114 of the Clean Air Act (CAA), and governed by EPA regulations in 40 Code of Federal Regulations (CFR), Part 2, Subpart B, and other EPA regulations and policies.

2. Reference Documents:

a. Clean Air Act, as amended. b. 40 CFR, Chapter 1, Part 2, Subpart B - Confidentiality of Business Information. c. EPA Information Security Manual. d. Clean Air Act Confidential Business In formation Security Manual (January 2002).

3. Exception:

This document was prepared as a summary of data gathering a nd handling procedures used by the OAQPS of the EPA. Nothing in this document shall be construed as superseding or being in conflict with any applicable regulations , statutes, or policies to which EPA is subject.

4. Definition:

Confidential Business Information - Information claimed by the provider to be confidential. This information may be identifi ed with such titles as trade secret, secret, administrative secret, company secret, secret pr oprietary, privileged, admi nistrative confidential, company confidential, confidentia l proprietary, or proprietary. NOTE: These markings should not be confused with the classi fication markings of national secu rity information identified in Executive Order 11652.

### 5. Background

Section 114 (c) of the CAA, as amended, reads as follows:

“Any records, reports, or information obtained un der subsection (a) shall be available to the public, except that upon a showing satisfactory to the Administrator by any person that records, reports, or information, or partic ular part thereof (other than emission data), to which the Administrator has access under this section if made public, would divulge methods or processes entitled to protection as trade secrets of such person, the Admi nistrator shall consider such record, report, or information or particular portion thereof confidentia l in accordance with the purposes of Section 1905 of Title 18 of the United States Code, except that such record, report, or information may be disclosed to other officers, employees, or authorized representatives of the United States concerned with carrying out this Ac t or when relevant in any proceeding under this Act.”

The treatment of CBI by EPA, including data obtained under Section 114 of the CAA, is governed by 40 CFR Part 2. These regulations requi re EPA offices to include a notice with each request for information to inform the business of: (1) its right to assert a claim of confidentiality covering part or all of the information, (2) the me thod for asserting a claim, and (3) the effect of failure to assert a claim at time of submissi on. In addition, the regulations: (1) set forth procedures for the safeguarding of confidential information, (2) contain provisions for providing confidential information to authorize representati ves, (3) contain provisio ns for the release of information to the Congress, Comptroller Gene ral, other Federal agen cies, State and local governments, and Courts, (4) permit the disclosure of information within EPA to employees with an official need for the information, and (5) pr ohibit wrongful use of such information and cite penalties for wrongful disclosure. Further, th e regulations contain the Agency’s basic rule concerning the treatment of requests for info rmation under the Freedom of Information Act (FOIA) (5 U.S.C. 552).

6. Procedures:

a. Request for Information.

Each request for information made under the provisions of Section 114(a) is signed by the Division Director. The re quest includes standard enclosur e “EPA’s Information Gathering Authority under Section 114 of the Clean Air Act” which was designed to meet the requirement of 40 CFR Part 2 discussed above.

b. Receipt of CAA CBI.

Upon receipt of information for which conf idential treatment has been requested, the OAQPS Document Control Officer (DCO) logs in the material and a permanent file is established. If part of the material is claimed to be confid ential, that portion should be marked “Subject to Confidentiality Cl aim.” In compliance with Se ctions 2.204 and 2.208 of 40 CFR

Part 2, the Group Leader responsible fo r the requested information reviews the information to determine the validity of the confid entiality claim as prescribed by the sections. If the information is clearly not c onfidential, the Group Leader prepar es a letter for the signature of

### the responsible Division Director to notify the business of this finding. Information claimed as confidential is hand carried to the OAQPS CBI Office to be logged into the OAQPS CAA CBI tracking system and filed for safekeeping. The OAQPS CAA CBI tracking system provides a brief description of the material (submitter, subj ect, number of pages, etc.), identifies it with the correct project number or work assignment number , and lists those persons who are authorized to have access to the information. A record of pe rsonnel accessing the inform ation (Attachment A) is also kept on filed. By regula tion, confidential information must be so marked or designated by the originator. The EPA takes additional measures to ensure that the proprietary designation is uniformly indicated and immediately observable. All unmarked or undesignated information (except as noted below) may be authorized for public release.

c. Storage of CAA CBI.

Folders, documents, or material containi ng CAA CBI (as defined) shall be secured according to the instructions lis ted in the OAQPS Security Manual. In addition, the CBI storage area that has been identified sp ecifically for that purpose is equipped with a supplementary locking device. The storage area and files ar e under the direct control of the OAQPS DCO.

Access to the storage area is limited to th e DCO, Document Control Assistant, and the minimum number of persons required to effectively maintain normal business operations as directed by the Director, Pl anning, Resources, and Regional Management Staff (PRRMS).

Files may be issued upon confirmation that the requesting individua l is authorized to receive the information. All conf idential files must be returned no later than close of business on the same day. The intended user must sign th e CBI Control Record when checking out files.

Individuals signing out confiden tial files are re sponsible for their safekeeping. Files must never be left unattended. The information mu st not be disclosed to any non-authorized personnel.

Storage procedures for CAA CBI by an aut horized representative of EPA (see Section d. below) must be, at a minimum, as secure as those established for EPA offices within OAQPS. Whenever CBI is removed from the EPA files to be transmitted to an aut horized representative, a notation is made in the file’s control record and transfer log indicati ng what information was transmitted, the date, and the recipient. The author ized representative returns a signed receipt to the DCO.

d. Access to CAA CBI.

Only authorized EPA employees may open or distribute CAA CBI.

Only employees who require, have a need to know, and are authorized access to CAA CBI in the performance of their official du ties are permitted to review documents and, upon receiving a confidential document, must sign and date the form show n in Attachment A to certify their access to the document.

The Group Leader having primary res ponsibility for the CAA CBI provides a memorandum to the DCO designating those personne l authorized to access specific CBI. No

### person is automatically entitled to access based sole ly on grade, position, or security clearance. The names of persons granted access to CAA CBI are placed on the CAA CBI access list. The CAA CBI access list indicates the “specific” CBI each person is permitted to see. The access list is reviewed and updated periodically.

Companies under contract to perform work for the EPA may be designated authorized representatives of EPA. As au thorized representatives, contractors may be granted access to CAA CBI. The following condition s apply when it has been dete rmined that disclosure is necessary:
(1) The contractor designated as a repres entative and its employees (a) may use such confidential information only for the purpose of carrying out the wo rk required, (b) must refrain from disclosing the information to anyone othe r than EPA without havi ng received from EPA prior written approval of each affected business or of an EPA legal office, and (c) must return to EPA all copies of the information (and any abst racts or excerpts there from) upon request or whenever the information is no longer re quired for the perfor mance of the work.

(2) The authorized contractor designated as a representative must obtain a written confidentiality agreement from each of its employees who will ha ve access to the information. A copy of each employee agreement (Attachment B) must be furnished to EPA before access is permitted.

(3) The contractor designa ted as an authorized representative must agree that the conditions in the contract concerning the use and disclosure of CAA CBI are included for the benefit of, and shall be enforceable by, both EP A and any affected business having a proprietary interest in the information.

Information may be released to or accessed by EPA employ ees other than OAQPS employees only upon approval of the Director, PRRMS.

Requests for CAA CBI from other Federal agen cies, Congress, the Comptroller General, Courts, etc., are processed in accord ance with 40 CFR Part 2, Subpart B.

Requests under the FOIA are handled in accordance with 40 CFR Part 2, Subpart A. The FOIA Coordinator must be cons ulted prior to responding to any request for information if a claim of confidentiality has been asserted or if there is reason to believe that a claim might be made if the business kne w release was intended.

e. Use and Disclosure of CAA CBI.

The CAA CBI, as defined, may not be us ed in publications, supporting documentation, memoranda, etc., that become a part of the public domain, except as provided for in 40 CFR Part 2, Subpart B. The CAA CBI may not be summari zed without the approval of the Group Leader responsible for the CAA CBI. Any authorized re productions must be logg ed into the CAA CBI document tracking system and treated according to the same procedures applicable to the original confidential material. Documents, mate rials, or extracts of information generated by EPA which contain CAA CBI must be stamped “Subject to Confid entiality Claim” and a cover sheet must be attached to identify the material as CBI.5



### f. Handling of Other Information.

Reports, memoranda, documents, etc., prepared by EPA or its authorized representatives are not normally circulated outside EPA for co mment or review prior to publication except in such cases as described in section 6 above. Ho wever, because industrial-data-gathering visits, plant inspections, and source testing can involve inadvertent receipt of CAA CBI, it is the policy of OAQPS to protect all parties involved in the following manner:

(1) Prior to or at the inception of a plant inspection, data-gathering vi sit, or source test, EPA or its authorized represen tative discusses with a res ponsible industry official the information sought, how it is to be used, and how it is to be protected. A copy of this summary is usually provided to the indus try official being consulted.

(2) Following an inspection, visit, or test , a trip report is prep ared to include, as practicable, all information received by EPA or its authorized representati ve during the visit or test. The report may be prepared by either EPA or its authorized representative. The draft report is clearly identified with an att ached yellow cover sheet. A second c opy of the draft trip report is forwarded by EPA to the responsible industry o fficial for review. The responsible industry official is requested by cover lette r to review the report, clearly mark any information considered to be confidential, and return the edited copy to the responsible EPA employee within the time specified. The original draft is kept in the CBI file until the edited copy is returned by the business firm.

(3) When the reviewed copy is returned to EPA, informa tion designated confidential is placed in the CBI files as described above. The origin al draft of the trip repor t is edited to delete the confidential information and the trip report is authorized for release.

Attachments (2)

### ENCLOSURE 7 - ATTACHMENT A

EXAMPLE RECORD FO RM FOR CBI ACCESS

## CAA CONFIDENTIAL BUSINESS INFORMATION CONTROL RECORD

DATE RECEIVED: RESPONSIBLE GROUP: CONTROL NUMBER:

DOCUMENT AUTHOR: DATE OF DOCUMENT:

DESCRIPTION (PROVIDING ORGANIZATION, TITLE, SU BJECT, NUMBER OF COPI ES, NUMBER OF PAGES)

RETURN DATE: DESTRUCTION DATE: INITIALS:

EACH PERSON WHO IS GIVEN ACCESS TO THIS DOCUMENT MUST FILL IN THE INFORMATION BELOW.

SIGNATURE DATE SIGNATURE DATE 

## CHECK-OUT CHECK-IN

TIME TIME

C A A Form 1 (Re v

. 0 1 / 0 2 )

### ENCLOSURE 7 -- ATTACHMENT B

EXAMPLE AUTHORIZATION FORM FOR CBI ACCESSCAA CBI Security Manual (Appendix A)



### I. AUTHORIZATION FOR ACCESS TO CAA CBI FOR FEDERAL EMPLOYEES

FULL NAME POSITION

SSN OFFICE
It is the responsibility of each Authorizing Official* to ensure that the employees under his/her supervision who require access to CAA CBI: 1. Sign the Confidentiality Agreement for Federal Employees 2. Are fully informed regarding their security responsibilities for CAA CBI. 3. Obtain access only to that CAA CBI required to perform their official duties

SIGNATURE OF AUTHORIZING OFFICIAL* TELEPHONE NO. DATE

TITLE LOCATION



### II. CONFIDENTIALITY AGREEMENT FOR FEDERAL EMPLOYEES

I understand that, in accordance with my official dutie s, I will have access to certain Confidential Business Information submitted under the Clean Ai r Act (CAA) (42 U.S.C. 7401 et seq.)

I understand that, under 18 U.S.C. 1905 and 18 U.S.C 1924I am liable for a possible fine of up to $1,000 and/or imprisonment for up to one year, if I willfully disclose CAA Confidential Business Information to any person not authorized to receive it. Additionally, I understand that, I may be subject to disciplinary action for violation of this agreement with penalties ranging up to and including dismissal.

I am aware that, I may be subject to criminal penalties under 18 U.S.C. 1001 if I have made any statement of material facts knowing that such statement is fals e or if I willfully conceal any material fact.

I agree that, upon the termination of my duties, transfer or departure from the Environmental Protection Agency, I will return all materials containing CAA Confidential Business Information in my possession to the OAQPS CBI Office.

I certify that I have read and understand these procedur es and those outlined in the CAA CBI Security Manual.

SIGNATURE TELEPHONE NO. DATE



### III. THE UNDERSIGNED CERTIFIES THE ALL TRAINING AND TEST REQUIREMENTS HAVE BEEN MET BY THE EMPLOYEE.

SIGNATURE CBI MANAGER/DCO TELEPHONE NO. DATE



### IV. ANNUAL RE-CERTIFICATION : I certify that, in conjunction with my duties, I require access to CAA CBI. I am current with all CBI handling procedur es and security guidelines as outlined in the CCA CBI Security Manual.

Date Date Date Date Date Date

Initial Initial Initial Initial Initial Initial

Date Date Date Date Date Date

Initial Initial Inital Initial Initial Initial CAA CBI From 2 (Rev. 01/ 02) * Must be Division Director (or equivalent) or above. A-1Test Plan
Clay Ceramics - Tile - Kiln Emission Testing

Facility Information: Enter Facility Name Enter Physical Address

City Stat Zip Code

Contact: Person to contact for more detail

Phone: Enter contact's phone number

Fax: Enter contact's fax number

Email: Enter contact's email address Testing Company: Name of primary testing organization Enter US postal address

City Stat

e Zip Code

Contact: Field Test Leader

Phone: Enter contact's phone number

Fax: Enter contact's fax number

Email: Enter contact's email address

Air Permit Number: Enter your facility's Air Permit Number Permitted Source ID/Name:
Kiln Name Kiln ID

Permitted Maximum Process Rate: Process rate (Mg fired tile/hr) Max. Normal Operation Process Rate: Process rate (Mg fired tile/hr) Target Process Test Rate Process rate (Mg fired tile/h

1. What is the specific purpose for the proposed testing? The primary reason for performing this emissions test is to provide emissions data to develop emission standards for HAP.

3. Will the test results be used for other regulatory purposes (e.g., emission inventories, permit applications, etc.) beyond that stated above? If yes, explain.
List any secondary purposes that you will use the data from this emissions test to address. If known, list those pollutants that are of secondary interest.

5a. Please give a brief description of the source (including control equipment) and attach source or process flow diagram:
This description should describe the process and associated controls to differentiate this facility from, or document similarity with others of same SCC. An example is: The source is a tunnel kiln. Emissions are controlled by a dry sorbent injection fabric filter (DIFF).

5b. Control Devices: Industry NAICS: 327122

4a. Enter the process data to be documented during testing.

4b. Enter the process lab data to be documented during testing. AFS #: Enter AFS Number FRS #: Enter FRS ID

SCC / Description 30500850 Industrial Processes - Mineral Products - Ceramic Clay/Tile Manufacture - Firing - Natural Gas-fired Kiln

2. List all state and federal regulations that apply to the proposed testing:

Process Parameter Units Target Value Comments

Tile Produced Megagrams/hr 0 Provide estimated process rate for this test.

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7. Please provide the following information for each test parameter. 6. Please enter sampling location information. Control Device Name List all emissions control devices in order of process flow. Choose from drop down lists. If not on list, add description and provide detailed description in section 5a.

Target Parameter Test

Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location
% H2O Method 1 - 4 3 60 0 Outlet of Control Device Flowrate Method 1 - 4 3 60 0 Outlet of Control Device % H2O Method 1 - 4 3 240 0 Outlet of Control Device Flowrate Method 1 - 4 3 240 0 Outlet of Control Device O2 Method 3A O2 3 60 0 Outlet of Control Device
O2 Method 3A O2 3 240 0 Outlet of Control Device Hydrogen Chloride Method 26A 3 60 0 Outlet of Control Device Hydrogen Fluoride Method 26A 3 60 0 Outlet of Control Device Filterable PM2.5 OTM - 27/28 3 60 0 Outlet of Control Device Inorganic

(Aqueous) Condensible Part. OTM - 27/28 3 60 0 Outlet of Control Device

Organic

Condensible Particulate OTM - 27/28 3 60 0 Outlet of Control Device

Antimony Method 29 3 240 0 Outlet of Control Device Arsenic Method 29 3 240 0 Outlet of Control Device Beryllium Method 29 3 240 0 Outlet of Control Device Cadmium Method 29 3 240 0 Outlet of Control Device Chromium Method 29 3 240 0 Outlet of Control Device Cobalt Method 29 3 240 0 Outlet of Control Device Filterable

Particulate Method 29 3 240 0 Outlet of Control Device Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width
Outlet of Control Device 0 0 0 0 0 0 0 0

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Clay Ceramics - Tile - Kiln Emission Testing

Lead Method 29 3 240 0 Outlet of Control Device Manganese Method 29 3 240 0 Outlet of Control Device Mercury Method 29 3 240 0 Outlet of Control Device Nickel Method 29 3 240 0 Outlet of Control Device Selenium Method 29 3 240 0 Outlet of Control Device 2,3,7,8-TCDD Method 23 3 240 0 Outlet of Control Device 1,2,3,7,8-PeCDD Method 23 3 240 0 Outlet of Control Device 1,2,3,4,7,8-

HxCDD Method 23 3 240 0 Outlet of Control Device 1,2,3,6,7,8-

HxCDD Method 23 3 240 0 Outlet of Control Device Total TCDD Method 23 3 240 0 Outlet of Control Device Total TCDF Method 23 3 240 0 Outlet of Control Device Total PeCDD Method 23 3 240 0 Outlet of Control Device Total PeCDF Method 23 3 240 0 Outlet of Control Device Total HpCDD Method 23 3 240 0 Outlet of Control Device Total HpCDF Method 23 3 240 0 Outlet of Control Device Total HxCDD Method 23 3 240 0 Outlet of Control Device Total HxCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,7,8,9-

HxCDD Method 23 3 240 0 Outlet of Control Device 1,2,3,4,6,7,8-

HpCDD Method 23 3 240 0 Outlet of Control Device
OCDD Method 23 3 240 0 Outlet of Control Device 2,3,7,8-TCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,7,8-PeCDF Method 23 3 240 0 Outlet of Control Device 2,3,4,7,8-PeCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,4,7,8-HxCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,6,7,8-HxCDF Method 23 3 240 0 Outlet of Control Device 2,3,4,6,7,8-HxCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,7,8,9-HxCDF Method 23 3 240 0 Outlet of Control Device

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Clay Ceramics - Tile - Kiln Emission Testing

8. Describe below or attach complete documentation of all modifications and/or deviations to the applicable test methods. If alternative methods requested, attach documentation of request 7b. Please select the Emissions / Concentrations for each location.

1,2,3,4,6,7,8- HpCDF Method 23 3 240 0 Outlet of Control Device 1,2,3,4,7,8,9-

HpCDF Method 23 3 240 0 Outlet of Control Device OCDF Method 23 3 240 0 Outlet of Control Device Other TCDD Method 23 3 240 0 Outlet of Control Device Other PeCDD Method 23 3 240 0 Outlet of Control Device Other HxCDD Method 23 3 240 0 Outlet of Control Device Other HpCDD Method 23 3 240 0 Outlet of Control Device Other TCDF Method 23 3 240 0 Outlet of Control Device Other PeCDF Method 23 3 240 0 Outlet of Control Device Other HxCDF Method 23 3 240 0 Outlet of Control Device Other HpCDF Method 23 3 240 0 Outlet of Control Device Total Dioxins Method 23 3 240 0 Outlet of Control Device Total Furans Method 23 3 240 0 Outlet of Control Device Total TEQ Method 23 3 240 0 Outlet of Control Device

Test Method Emissions / Concentrations Corrected Analyte Corrected

Percent Location

Method 1 - 4 percent(%) 0 Outlet of Control Device Method 3A O2 percent(%) 0 Outlet of Control Device Method 26A grams/hr 0 Outlet of Control Device Method 26A ppm corrected O2 7 Outlet of Control Device OTM - 27/28 grams/hr 0 Outlet of Control Device OTM - 27/28 mg/dscm corrected O2 7 Outlet of Control Device Method 29 grams/hr 0 Outlet of Control Device Method 29 mg/dscm corrected O2 7 Outlet of Control Device Method 23 grams/hr 0 Outlet of Control Device Method 23 ng/dscm corrected O2 7 Outlet of Control Device

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Clay Ceramics - Tile - Kiln Emission Testing

8. Describe below or attach complete documentation of all modifications and/or deviations to the applicable test methods. If alternative methods requested, attach documentation of request

9. Does the proposed sampling location meet the minimum EPA Method 1 criteria for acceptable measurement sites? Please list below or attach the supporting documentation.
In this section, provide documentation about the compliance of the sampling location to Method 1 criteria AND if the site meets these requirements, change the check box to "Yes". If the sampling location does not meet Method 1 requirements, indicate the method used to make the sampling location representative of the emissions from the source.

10. Has absence of cyclonic flow been verified per EPA Method 1 (Section 2.4)? If no, absence of cyclonic flow must be verified prior to testing. If yes, please attach supporting documentation.
This field is for the documentation of the absence of cyclonic flow that is available at the time of the Test Plan generation. If this documentation is not available at this time, documentation is required during the performance of the emissions test. If cyclonic flow exists at the testing location, describe the procedures used to obtain representative samples. If there is an absence of cyclonic flow, check the "Yes" box.
11. Select the method that will determine the oxygen concentration : M3A-instrumental

13. Has all testing equipment been calibrated within the past year? If no, please explain. It is expected that the response to this question will be "Yes". This highlights the need to attach the documentation of the calibrations for all equipment used during the conduct of the emissions test. If all the equipment has been calibrated, check the "Yes" box.

17. What is the proposed test schedule? This field is primarily to advise the regulatory authority and facility the dates that emissions testing will be performed including any set up dates.

18. Additional comments: Yes No

Yes No

Yes No

Yes No

Yes No

14. Will all calibration gases be certified by EPA Traceability Protocol procedures? If No, describe certification procedure below.

15. Is a dilution system (via EPA Method 205) proposed? Yes No N/A

Yes No N/A 16. If applicable, list the expected calibration gas concentrations for all proposed instrumental test methods. Include as much information as is known at this time. 12. Do any of the proposed test methods require analysis of EPA audit samples? If yes, notify Regional Office at least 45 days prior to testing to allow for audit sample preparation and shipment.

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Name:
Title: Company: Sign Date: Name:
Title: Company: Sign Date: Permitted Facility Representative Testing Company Representative Date Date 19. Required Personal Protection Equipment: This field is primarily to advise the regulatory authority of the type of personal protective equipment that will be required for them to use to access the sampling location and any other locations that are associated with the performance of the test program. It will also serve to inform the facility of the source tester's knowledge of the required protective equipment that they will use during the source test program.

Tuesday, March 09, 2010 Page 6 of 6 Test Plan

### Enclosure 9

Site

- Specific Test Plan Development Guidance

This information collection request (ICR) provides specific additional instructions for each prescribed test method to ensure that the collected data will meet the objectives of the ICR. To ensure that all dat a submitted in fulfillment of this ICR are of sufficient and known quality, EPA believes it is highly advisable for each facility (subject to emissions testing under the ICR) to prepare a site

- specific test plan prior to testing. A site

- specific test plan addresses the planning and quality assurance and quality control procedures and acceptance criteria for all of the testing, including the collection of process and fuel data.

You may find guidance for developing such a site

- specific test plan at http://www.epa.gov/ttn/emc/guidlnd/gd

- 042.pdf . Such a test plan would provide a means for you to verify that the quality assurance protocols

, contained in the various test methods

, are met. You nee d not submit the test plan to EPA; however, much of the information in a complete site

specific test plan consists of data that are used for required fields in Version 3 of the EPA Electronic Reporting Tool (ERT) (see Enclosure 8).