Analytical Testing 

Consultants Inc. 

1630 Dale Earnhardt Blvd. 

Kannapolis, NC 28083

Boral Bricks 

Salisbury Plant Inlet & Outlet 

Augusta Plants 4 & 5 Inlets & Outlets 

Project # P-10124 

PO # P-10124

Analytical Report 

(0910-96)

EPA Method 26A

Hydrogen chloride, Hydrogen fluoride 

Chloride 

Enthalpy Analytical, Inc. 

Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 

2202 Ellis Road Durham, NC 27703 - 5518 
I certify that to the best of my knowledge all analytical data presented in this report: 

 Have been checked for completeness 

 Are accurate, error-free, and legible 

 Have been conducted in accordance with approved protocol, and that all deviations and analytical 

problems are summarized in the appropriate narrative(s) 

This analytical report was prepared in Portable Document Format (.PDF) and contains  pages. 

EA# 0910-96 Page 2 of 202
Summary of Results

EA# 0910-96 Page 3 of 202
Compound Sample ID / Catch Weight (ug)

Salisbury Inlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 44,722 49,144 61,452 

Hydrogen Chloride 2,911 3,890 5,514 

Salisbury Outlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 28.7 ND 30.1 ND 27.9 ND

Hydrogen Chloride 330 J 253 J 217 J

Augusta Plant 4 Inlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 11,071 35,672 41,007 

Hydrogen Chloride 601 3,000 2,995 

Augusta Plant 4 Outlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 1,522 1,808 2,325 

Hydrogen Chloride 988 1,100 1,278 

Augusta Plant 5 Inlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 19,206 49,828 57,084 

Hydrogen Chloride 617 2,259 2,887 

Augusta Plant 5 Outlet Acid Impingers

Run 1 Run 2 Run 3

Hydrogen Fluoride 2,259 2,092 2,121 

Hydrogen Chloride 329 J 283 J 312 J

Company

Analyst

Parameters

# Samples

Analytical Testing Consult.

EO

EPA Method 26A (H2SO4)

18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-10124

0910-96

P-10124

10/6/2010

0910-96 res 10/6/2010

EA# 0910-96 Page 4 of 202
Compound Sample ID / Catch Weight (ug)

Company

Analyst

Parameters

# Samples

Analytical Testing Consult.

EO

EPA Method 26A (H2SO4)

18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-10124

0910-96

P-10124

10/6/2010

Blanks

Acid Blank DI H2O blank

Hydrogen Fluoride 17.6 J 1.55 ND

Hydrogen Chloride 10.1 ND 11.9 J

0910-96 res 10/6/2010

EA# 0910-96 Page 5 of 202
Compound Sample ID / Catch Weight (ug)

Salisbury Inlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 382 202 J 17.8 ND

Salisbury Outlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 134,815 14.4 ND 6,408 

Augusta Plant 4 Inlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 227 J 18.2 ND 17.6 ND

Augusta Plant 4 Outlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 16.9 ND 18.7 ND 15.1 ND

Augusta Plant 5 Inlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 16.7 ND 15.7 ND 17.4 ND

Augusta Plant 5 Outlet Alkaline Impingers

Run 1 Run 2 Run 3

Chloride 13.8 ND 15.5 ND 16.1 ND

Blanks

Base Blank DI H2O blank

Chloride 34.2 J 11.5 J

Company

Analyst

Parameters

# Samples

Analytical Testing Consul

EO

EPA Method 26A (NaOH)

18 Runs, 1 Blank

Client #

Job #

PO #

Report Date

P-10124

0910-96

P-10124

10/6/2010

0910-96 res 10/6/2010

EA# 0910-96 Page 6 of 202
Results

EA# 0910-96 Page 7 of 202
MDL 0.0100 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Salisbury Run 1 In A 009-1001.D 009-1002.D HPLC53PG98.M 3.13 3.13 0.0 7.99 7.99 0.0 7.99 1.053 Salisbury Run 2 In A 012-1301.D 012-1302.D HPLC53PG98.M 3.13 3.13 0.0 7.99 7.97 0.1 7.98 1.053 Salisbury Run 3 In A 013-1401.D 013-1402.D HPLC53PG98.M 3.13 3.13 0.0 8.07 8.05 0.2 8.06 1.053 

Salisbury Run 1 Out A 014-1501.D 014-1502.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 Salisbury Run 2 Out A 015-1601.D 015-1602.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 Salisbury Run 3 Out A 016-1901.D 016-1902.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 

P4 Run 1 In A 026-3301.D 026-3302.D HPLC53PG98.M 3.12 3.12 0.0 3.84 3.86 0.3 3.85 1.053 P4 Run 2 In A 029-3601.D 029-3602.D HPLC53PG98.M 3.14 3.14 0.0 11.7 11.7 0.1 11.7 1.053 P4 Run 3 In A 030-3701.D 030-3702.D HPLC53PG98.M 3.14 3.14 0.0 11.0 10.9 0.1 10.9 1.053 

P4 Run 1 Out A 031-3801.D 031-3802.D HPLC53PG98.M 3.12 3.12 0.0 0.492 0.487 0.5 0.490 1.053 P4 Run 2 Out A 032-3901.D 032-3902.D HPLC53PG98.M 3.12 3.12 0.0 0.608 0.606 0.1 0.607 1.053 P4 Run 3 Out A 033-4001.D 033-4002.D HPLC53PG98.M 3.12 3.12 0.1 0.685 0.684 0.1 0.684 1.053 

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

0910-96 res 

EA# 0910-96 Page 8 of 202
MDL 0.0100 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

P5 Run 1 In A 040-4901.D 040-4902.D HPLC53PG98.M 3.13 3.13 0.0 6.19 6.24 0.4 6.21 1.053 P5 Run 2 In A 009-1001.D 009-1002.D HPLC53PG100.M 3.14 3.14 0.0 8.73 8.68 0.3 8.70 1.053 P5 Run 3 In A 010-1101.D 010-1102.D HPLC53PG100.M 3.14 3.17 1.0 11.0 11.1 0.5 11.0 1.053 

P5 Run 1 Out A 043-5201.D 043-5202.D HPLC53PG98.M 3.12 3.12 0.0 0.750 0.702 3.3 0.726 1.053 P5 Run 2 Out A 044-5701.D 044-5702.D HPLC53PG98.M 3.13 3.13 0.0 0.822 0.839 1.0 0.830 1.053 P5 Run 3 Out A 045-5801.D 045-5802.D HPLC53PG98.M 3.12 3.12 0.0 0.776 0.768 0.5 0.772 1.053 

Acid Blank 052-6701.D 052-6702.D HPLC53PG98.M 3.17 NA NA 0.0138 0.0100 15.9 0.0119 1.053 

DI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 

0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 

0910-96 res 

EA# 0910-96 Page 9 of 202
MDL 0.0100 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

MS Salisbury R1 In A 010-1101.D 010-1102.D HPLC53PG98.M 3.13 3.13 0.0 11.3 11.3 0.2 11.3 1.053 

S

N

Sp

MSD Salisbury R1 In A 011-1201.D 011-1202.D HPLC53PG98.M 3.13 3.13 0.0 10.7 10.7 0.2 10.7 1.053 

S

N

Sp

MS P4 R1 In A 027-3401.D 027-3402.D HPLC53PG98.M 3.13 3.13 0.0 6.94 6.95 0.0 6.94 1.053 

S

N

Sp

MSD P4 R1 In A 028-3501.D 028-3502.D HPLC53PG98.M 3.13 3.12 0.1 6.97 6.94 0.2 6.96 1.053 

S

N

Sp

HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 3.12 3.12 0.1 5.37 5.36 0.1 5.36 1.053 

S

Sp

HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 3.12 3.12 0.0 5.34 5.35 0.1 5.35 1.053 

S

Sp

0910-96 res 

EA# 0910-96 Page 10 of 202
MDL 0.0100 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 3.12 3.12 0.0 5.22 5.22 0.0 5.22 1.053 

S

Sp

HPLC53pg100 #LCS 007-0801.D 007-0802.D HPLC53PG100.M 3.12 3.13 0.0 5.27 5.29 0.1 5.28 1.053 

S

Sp

0910-96 res 

EA# 0910-96 Page 11 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Salisbury Run 1 In A 009-1001.D 009-1002.D HPLC53PG98.M 4.26 4.26 0.0 0.533 0.532 0.0 0.533 1.028 Salisbury Run 2 In A 012-1301.D 012-1302.D HPLC53PG98.M 4.26 4.26 0.0 0.650 0.644 0.5 0.647 1.028 Salisbury Run 3 In A 013-1401.D 013-1402.D HPLC53PG98.M 4.26 4.26 0.0 0.742 0.740 0.1 0.741 1.028 

Salisbury Run 1 Out A 014-1501.D 014-1502.D HPLC53PG98.M 4.25 4.26 0.0 0.120 0.115 2.2 0.118 1.028 Salisbury Run 2 Out A 015-1601.D 015-1602.D HPLC53PG98.M 4.25 4.25 0.0 0.0848 0.0869 1.2 0.0859 1.028 Salisbury Run 3 Out A 016-1901.D 016-1902.D HPLC53PG98.M 4.25 4.25 0.0 0.0825 0.0764 3.8 0.0794 1.028 

P4 Run 1 In A 026-3301.D 026-3302.D HPLC53PG98.M 4.26 4.26 0.0 0.218 0.210 1.7 0.214 1.028 P4 Run 2 In A 029-3601.D 029-3602.D HPLC53PG98.M 4.26 4.26 0.0 1.01 1.01 0.3 1.01 1.028 P4 Run 3 In A 030-3701.D 030-3702.D HPLC53PG98.M 4.26 4.26 0.0 0.815 0.823 0.5 0.819 1.028 

P4 Run 1 Out A 031-3801.D 031-3802.D HPLC53PG98.M 4.26 4.26 0.0 0.325 0.327 0.3 0.326 1.028 P4 Run 2 Out A 032-3901.D 032-3902.D HPLC53PG98.M 4.26 4.26 0.0 0.378 0.378 0.1 0.378 1.028 P4 Run 3 Out A 033-4001.D 033-4002.D HPLC53PG98.M 4.26 4.26 0.0 0.386 0.385 0.2 0.385 1.028 

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

0910-96 res 

EA# 0910-96 Page 12 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

P5 Run 1 In A 040-4901.D 040-4902.D HPLC53PG98.M 4.26 4.26 0.0 0.206 0.203 0.6 0.205 1.028 P5 Run 2 In A 041-5001.D 041-5002.D HPLC53PG98.M 4.27 4.27 0.0 0.806 0.812 0.4 0.809 1.028 P5 Run 3 In A 042-5101.D 042-5102.D HPLC53PG98.M 4.27 4.27 0.0 1.15 1.14 0.3 1.14 1.028 

P5 Run 1 Out A 043-5201.D 043-5202.D HPLC53PG98.M 4.26 4.26 0.0 0.121 0.0953 12.0 0.108 1.028 P5 Run 2 Out A 044-5701.D 044-5702.D HPLC53PG98.M 4.26 4.26 0.0 0.115 0.115 0.2 0.115 1.028 P5 Run 3 Out A 045-5801.D 045-5802.D HPLC53PG98.M 4.26 4.26 0.0 0.114 0.118 2.0 0.116 1.028 

Acid Blank 052-6701.D 052-6702.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 

DI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M 4.29 4.29 0.0 0.113 0.0436 44.3 0.0783 1.028 

0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 

0910-96 res 

EA# 0910-96 Page 13 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

MS Salisbury R1 In A 010-1101.D 010-1102.D HPLC53PG98.M 4.25 4.25 0.0 3.65 3.65 0.0 3.65 1.028 

S

N

Sp

MSD Salisbury R1 In A 011-1201.D 011-1202.D HPLC53PG98.M 4.26 4.26 0.0 3.45 3.45 0.1 3.45 1.028 

S

N

Sp

MS P4 R1 In A 027-3401.D 027-3402.D HPLC53PG98.M 4.26 4.26 0.0 3.05 3.06 0.1 3.06 1.028 

S

N

Sp

MSD P4 R1 In A 028-3501.D 028-3502.D HPLC53PG98.M 4.26 4.26 0.0 3.07 3.08 0.0 3.07 1.028 

S

N

Sp

HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 4.26 4.26 0.1 5.00 5.01 0.1 5.01 1.028 

S

Sp

HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 4.26 4.26 0.0 5.01 5.01 0.0 5.01 1.028 

S

Sp

0910-96 res 

EA# 0910-96 Page 14 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Convers

Facto

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consultants

EOEPA Method 26A (H2SO4)18 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 4.26 4.27 0.0 4.88 4.87 0.1 4.87 1.028 

S

Sp

HPLC53pg100 #LCS 007-0801.D 007-0802.D HPLC53PG100.M 4.25 4.25 0.0 4.92 4.92 0.1 4.92 1.028 

S

Sp

0910-96 res 

EA# 0910-96 Page 15 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Aliquo

Facto

Salisbury Run 1 In B 017-2001.D 017-2002.D HPLC53PG98CL.M 4.23 4.23 0.0 0.224 0.219 1.1 0.222 1 Salisbury Run 2 In B 018-2101.D 018-2102.D HPLC53PG98CL.M 4.23 4.23 0.0 0.0797 0.0760 2.3 0.0779 1 Salisbury Run 3 In B 019-2201.D 019-2202.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

Salisbury Run 1 Out B 023-2601.D 023-2602.D HPLC53PG98CL.M 4.15 4.15 0.0 7.48 7.39 0.6 7.44 1 Salisbury Run 2 Out B 021-2401.D 021-2402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 Salisbury Run 3 Out B 022-2501.D 022-2502.D HPLC53PG98CL.M 4.24 4.24 0.0 2.42 2.36 1.2 2.39 1 

P4 Run 1 In B 034-4301.D 034-4302.D HPLC53PG98CL.M 4.23 NA NA 0.171 0.00695 92.2 0.0889 1 P4 Run 2 In B 035-4401.D 035-4402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P4 Run 3 In B 036-4501.D 036-4502.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

P4 Run 1 Out B 037-4601.D 037-4602.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P4 Run 2 Out B 038-4701.D 038-4702.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P4 Run 3 Out B 039-4801.D 039-4802.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consul

EOEPA Method 26A (NaOH)18 Runs, 1 Blank

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

0910-96 res 

EA# 0910-96 Page 16 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Aliquo

Facto

Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consul

EOEPA Method 26A (NaOH)18 Runs, 1 Blank

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

P5 Run 1 In B 046-5901.D 046-5902.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P5 Run 2 In B 047-6001.D 047-6002.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P5 Run 3 In B 048-6101.D 048-6102.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

P5 Run 1 Out B 049-6201.D 049-6202.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P5 Run 2 Out B 050-6301.D 050-6302.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 P5 Run 3 Out B 051-6401.D 051-6402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

Base Blank 053-6801.D 053-6802.D HPLC53PG98CL.M 4.24 4.24 0.0 0.0235 0.0231 0.9 0.0233 1 

DI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M 4.29 4.29 0.0 0.113 0.0436 44.3 0.0783 1 

0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 

0910-96 res 

EA# 0910-96 Page 17 of 202
MDL 0.00695 (ug/mL) Lower Curve Limit 0.200 (ug/mL)

LOQ 0.200 (ug/mL) Upper Curve Limit 15.0 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Aliquo

Facto

Chloride

Company

Analyst

Parameters

# Samples

Analytical Testing Consul

EOEPA Method 26A (NaOH)18 Runs, 1 Blank

Client #

Job #

PO #

Report Date

P-101240910-96P-1012410/6/2010

HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 4.26 4.26 0.1 5.00 5.01 0.1 5.01 1 

Sp

Spik

HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 4.26 4.26 0.0 5.01 5.01 0.0 5.01 1 

Sp

Spik

HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 4.26 4.27 0.0 4.88 4.87 0.1 4.87 1 

Sp

Spik

0910-96 res 

EA# 0910-96 Page 18 of 202
Narrative Summary

EA# 0910-96 Page 19 of 202
Enthalpy Analytical Narrative Summary 

Company Analytical Testing 

Consultants Inc.

Client # P-10124

Analyst EO Job # 0910-96 

Parameters EPA Method 26A PO # P-10124 

# Samples 18 Runs, 3 Blanks Report Date October 6, 2010 

Custody David Eckard received the samples on 9/24/10 after being relinquished 

by Analytical Testing Consultants Inc. The samples were received at 

15.9C and in good condition. Samples Plant 5 Inlet and Outlet Runs 

2 and 3 were received in glass. Prior to, during, and after analysis, the 

samples were kept under lock with access only to authorized personnel 

by Enthalpy Analytical, Inc. 

Analysis The samples were analyzed for hydrogen chloride (HCl), hydrogen 

fluoride (HF), and chloride using the analytical procedures in EPA 

Method 26A, Determination of Hydrogen Halide and Halogen 

Emissions from Stationary Sources Isokinetic Method (40 CFR Part 60, 

Appendix A). 

With the exceptions noted above, all samples and standards were 

prepared, stored, and analyzed using high-density polyethylene 

containers. 

The Metrohm 861, High Performance Liquid Chromatograph "Mr 

Burns" (S/N 1861004003180) was equipped with a Metrohm 861 

Conductivity Detector and a Metrosep A Supp 5 - 110/4.0mm column 

(S/N # 7908297), for these analyses. 

Calibration The calibration curves are included in the Calibration Curve 

Chromatograms section of this report and referenced in the Analysis 

Method column on the Detailed Results page. 

For each calibration curve used, the first page of the curve contains all 

method specific parameters (i.e., curve type, origin, weight, etc.) used to 

quantify the samples. The calibration curve section also includes a table 

with the Retention Time (RetTime), Level (Lvl), Amount 

(corresponding units), Area, Response Factor (Amt/Area) and the 

analyte Name. The calibration table is used to identify (by retention 

time) and quantify each target compound. 

Chromatographic 

Conditions 

The acquisition method Metrohm.M is included in the Calibration 

Curve Chromatograms section of this report. 

EA# 0910-96 Page 20 of 202
Enthalpy Analytical Narrative Summary 

(continued) 

QC Notes Fluoride was not identified above the MDL in the analyses of the lab 

reagent blanks and client DI H2O blank. Fluoride was detected below 

the LOQ in the acid blank. 

Chloride was not identified above the MDL in the analyses of the lab 

reagent blanks and client acid blank. Chloride was detected below the 

LOQ in the client base blank and DI H2O blank. 

Matrix spike and matrix spike duplicates (MS and MSD) were prepared 

using aliquots of the samples Salibury R1-In A and P4 R1 In A. The 

recovery values were 111%, 91.3%, 103%, and 105% for HF. The 

recovery values were 104%, 97.3%, 94.7%, and 95.4% for HCl. 

Laboratory Control Samples (LCS) were prepared and analyzed with 

the samples. The recovery values ranged from 104% to 107 for HF and 

97.5% to 100% for HCL. 

The samples were analyzed within the four-week holding time specified 

by the method. 

Reporting Notes The results presented in this report are representative of the samples as 

provided to the laboratory. 

The H2SO4 matrix samples were analyzed for Cl- and F- but are 

reported as HCl and HF. The results were converted using an acid 

conversion factor of 1.028 for HCl and 1.053 for HF. 

Enthalpy Analytical, Inc. is accredited to perform EPA Method 26A for 

compliance purposes by the National Environmental Laboratory 

Accreditation Conference (NELAC) through the Louisiana 

Environmental Laboratory Accreditation Program (LELAP), certificate 

number 04010. 

EA# 0910-96 Page 21 of 202
General Reporting Notes 

The following are general reporting notes that are applicable to all Enthalpy Analytical, Inc. data 

reports, unless specifically noted otherwise.

 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot 

determine the presence of the analyte of interest reliably. 

 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot 

quantitate the analyte of interest within the criteria of the method. 

 The acronym ND following a value indicates a non-detect or analytical result below the MDL. 

 The letter J following a value indicates an analytical result between the MDL and the LOQ. A J flag 

indicates that the laboratory can positively identify the analyte of interest as present, but the value 

should be considered an estimate. 

 The letter E following a value indicates an analytical result exceeding 100% of the highest calibration 

point. The associated value should be considered as an estimate. 

 The acronym DF represents Dilution Factor. This number represents dilution of the sample during the 

preparation and/or analysis process. The analytical result taken from a laboratory instrument is 

multiplied by the DF to determine the final undiluted sample results. 

 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual sample is 

spiked with a known amount of analyte so that a percent recovery value can be determined. This shows 

what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample 

matrix interferes with the analysis of the analyte(s). 

 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same 

manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality 

by showing the consistency of results gained by performing the same steps multiple times. 

 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares an 

additional aliquot of sample for testing and the results of the duplicate analysis are compared to the 

initial result. The result should have a difference value of within 10% of the initial result (if the results 

of the original analysis are greater than the LOQ). 

 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an 

additional aliquot at a different dilution factor (usually double the initial factor). This analysis helps 

confirm that no additional compound is present and coeluting or sharing absorbance with the analyte of 

interest, as they would have a different response/absorbance than the analyte of interest. 

 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample 

matrix, prepared and analyzed by the laboratory using the same reagents, spiking standards and 

procedures used for the client samples. The LCS is used to assess the control of the laboratory’s 

analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. 

The extras (randomly chosen) are labeled with the associated project number and kept in-house at the 

appropriate temperature conditions. When the project samples are received for analysis, the LCSs are 

analyzed to confirm that the analyte could be recovered from the media, separate from the samples 

which were used on the project and which may have been affected by source matrix, sample collection 

and/or sample transport. 

EA# 0910-96 Page 22 of 202
General Reporting Notes 

(continued) 

 Significant Figures: Where the reported value is much greater than unity (1.00) in the units expressed, 

the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a 

value of 10,456.45 ug catch is rounded to 10,456 ug. There are five significant digits displayed, but no 

confidence should be placed on more than two significant digits. 

 Manual Integration: The data systems used for processing will flag manually integrated peaks with 

an “M”. There are several reasons a peak may be manually integrated. These reasons will be identified 

by the following two letter designations. The peak was not integrated by the software “NI”, the peak 

was integrated incorrectly by the software “II” or the wrong peak was integrated by the software 

“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the 

compound name. 

EA# 0910-96 Page 23 of 202
Sample Custody

EA# 0910-96 Page 24 of 202
EA# 0910-96 Page 25 of 202
EA# 0910-96 Page 26 of 202
EA# 0910-96 Page 27 of 202
EA# 0910-96 Page 28 of 202
EA# 0910-96 Page 29 of 202
EA# 0910-96 Page 30 of 202
Sample 

Chromatograms

EA# 0910-96 Page 31 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 10

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 9:27:01 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1001.D) 2.253 3.125 - Fluoride 3.513 4.257 - Chloride 5.431

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BV 467.71011 1.70755e-2 7.98639 Fluoride 

 4.257 BB 17.94451 2.96828e-2 5.32643e-1 Chloride 

Totals : 8.51904

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1001.D

Sample Name: Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:25 AM IGG Page 1 of 1

EA# 0910-96 Page 32 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 10

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 9:39:20 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1002.D) 2.254 3.125 - Fluoride 3.514 4.257 - Chloride 5.433

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BV 467.69397 1.70755e-2 7.98612 Fluoride 

 4.257 BB 17.93629 2.96844e-2 5.32427e-1 Chloride 

Totals : 8.51854

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1002.D

Sample Name: Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:33 AM IGG Page 1 of 1

EA# 0910-96 Page 33 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 13

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 10:40:59 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1301.D) 2.253 3.126 - Fluoride 3.512 4.257 - Chloride 5.425

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.126 BV 467.74438 1.70755e-2 7.98698 Fluoride 

 4.257 BB 22.41548 2.90028e-2 6.50111e-1 Chloride 

Totals : 8.63709

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1301.D

Sample Name: Salisbury R2 In A *20 0910-96

Instrument 1 10/4/2010 9:31:25 AM IGG Page 1 of 1

EA# 0910-96 Page 34 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 13

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 10:53:19 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1302.D) 2.255 3.126 - Fluoride 3.512 4.257 - Chloride 5.426

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.126 BV 466.99976 1.70755e-2 7.97425 Fluoride 

 4.257 BB 22.18078 2.90316e-2 6.43944e-1 Chloride 

Totals : 8.61819

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1302.D

Sample Name: Salisbury R2 In A *20 0910-96

Instrument 1 10/4/2010 9:31:33 AM IGG Page 1 of 1

EA# 0910-96 Page 35 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 14

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 11:05:39 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1401.D) 2.256 3.126 - Fluoride 3.508 4.257 - Chloride 5.405

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.126 BV 472.81418 1.70757e-2 8.07365 Fluoride 

 4.257 BB 25.90080 2.86355e-2 7.41682e-1 Chloride 

Totals : 8.81534

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1401.D

Sample Name: Salisbury R3 In A *20 0910-96

Instrument 1 10/4/2010 9:31:41 AM IGG Page 1 of 1

EA# 0910-96 Page 36 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 14

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 11:17:58 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1402.D) 2.253 3.125 - Fluoride 3.507 4.257 - Chloride 5.405

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BV 471.29227 1.70757e-2 8.04764 Fluoride 

 4.257 BB 25.83895 2.86411e-2 7.40057e-1 Chloride 

Totals : 8.78769

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1402.D

Sample Name: Salisbury R3 In A *20 0910-96

Instrument 1 10/4/2010 9:31:49 AM IGG Page 1 of 1

EA# 0910-96 Page 37 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 15

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 11:30:18 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1501.D) 2.255 3.342 3.506 4.254 - Chloride 4.635 5.655 7.160

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.254 BV 3.17554 3.78526e-2 1.20202e-1 Chloride 

Totals : 1.20202e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1501.D

Sample Name: Salisbury R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:31:57 AM IGG Page 1 of 1

EA# 0910-96 Page 38 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 15

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 11:42:38 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1502.D) 2.256 3.343 3.508 4.255 - Chloride 4.632 5.492 7.160

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.255 BV 3.03742 3.78526e-2 1.14974e-1 Chloride 

Totals : 1.14974e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1502.D

Sample Name: Salisbury R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:05 AM IGG Page 1 of 1

EA# 0910-96 Page 39 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 16

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 11:54:58 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1601.D) 2.253 3.336 3.504 4.250 - Chloride 4.626 5.491 7.158

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.250 BV 2.24146 3.78526e-2 8.48451e-2 Chloride 

Totals : 8.48451e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1601.D

Sample Name: Salisbury R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:13 AM IGG Page 1 of 1

EA# 0910-96 Page 40 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 16

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 12:07:18 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1602.D) 2.256 3.339 3.506 4.250 - Chloride 4.629 5.491 7.158

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.250 BV 2.29672 3.78526e-2 8.69365e-2 Chloride 

Totals : 8.69365e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1602.D

Sample Name: Salisbury R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:22 AM IGG Page 1 of 1

EA# 0910-96 Page 41 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 19

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:08:57 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1901.D) 2.254 3.340 3.507 4.250 - Chloride 4.652 5.671 7.177

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.250 BV 2.17866 3.78526e-2 8.24680e-2 Chloride 

Totals : 8.24680e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1901.D

Sample Name: Salisbury R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:30 AM IGG Page 1 of 1

EA# 0910-96 Page 42 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 19

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:21:17 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1902.D) 2.256 3.342 3.507 4.250 - Chloride 4.644 5.484 7.174

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.250 BV 2.01728 3.78526e-2 7.63593e-2 Chloride 

Totals : 7.63593e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1902.D

Sample Name: Salisbury R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:38 AM IGG Page 1 of 1

EA# 0910-96 Page 43 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 20

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:33:04 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2001.D) 2.245 3.467 4.233 - Chloride 4.909 6.997 9.847

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.233 VB 6.20973 3.61257e-2 2.24331e-1 Chloride 

Totals : 2.24331e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2001.D

Sample Name: Salisbury R1 In B *10 0910-96

Instrument 1 10/4/2010 9:33:09 AM IGG Page 1 of 1

EA# 0910-96 Page 44 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 20

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:50:22 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2002.D) 2.244 3.460 4.233 - Chloride 4.908 6.996 9.847

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.233 VB 6.02410 3.64293e-2 2.19454e-1 Chloride 

Totals : 2.19454e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2002.D

Sample Name: Salisbury R1 In B *10 0910-96

Instrument 1 10/4/2010 9:33:19 AM IGG Page 1 of 1

EA# 0910-96 Page 45 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 21

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:07:41 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2101.D) 2.246 3.071 3.322 4.225 - Chloride 4.901 5.420 6.985 9.814

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.225 BV 2.10500 3.78526e-2 7.96796e-2 Chloride 

Totals : 7.96796e-2

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2101.D

Sample Name: Salisbury R2 In B *10 0910-96

Instrument 1 10/4/2010 9:33:27 AM IGG Page 1 of 1

EA# 0910-96 Page 46 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 21

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:24:59 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2102.D) 2.247 3.072 3.326 4.225 - Chloride 4.900 5.418 6.982 9.813

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.225 BV 2.00891 3.78526e-2 7.60425e-2 Chloride 

Totals : 7.60425e-2

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2102.D

Sample Name: Salisbury R2 In B *10 0910-96

Instrument 1 10/4/2010 9:33:37 AM IGG Page 1 of 1

EA# 0910-96 Page 47 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 22

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:42:16 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2201.D) 2.247 3.076 3.344 4.906 6.986 9.827

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2201.D

Sample Name: Salisbury R3 In B *10 0910-96

Instrument 1 10/4/2010 9:33:45 AM IGG Page 1 of 2

EA# 0910-96 Page 48 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 22

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:59:34 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2202.D) 2.249 3.077 3.346 4.907 6.985 9.826

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2202.D

Sample Name: Salisbury R3 In B *10 0910-96

Instrument 1 10/4/2010 9:33:53 AM IGG Page 1 of 2

EA# 0910-96 Page 49 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 26

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:00:41 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2601.D) 2.217 4.152 - Chloride 4.777 5.446

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.152 BV 282.51471 2.64899e-2 7.48380 Chloride 

Totals : 7.48380

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2601.D

Sample Name: Salisbury R1 Out B *100 0910-96

Instrument 1 10/4/2010 9:35:28 AM IGG Page 1 of 1

EA# 0910-96 Page 50 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 26

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:17:59 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2602.D) 2.214 4.154 - Chloride 4.780 5.444

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.154 BV 278.87683 2.64928e-2 7.38822 Chloride 

Totals : 7.38822

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2602.D

Sample Name: Salisbury R1 Out B *100 0910-96

Instrument 1 10/4/2010 9:35:37 AM IGG Page 1 of 1

EA# 0910-96 Page 51 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 24

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 3:51:29 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2401.D) 2.249 3.341 4.911 7.003 9.833

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2401.D

Sample Name: Salisbury R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:34:32 AM IGG Page 1 of 2

EA# 0910-96 Page 52 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 24

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:08:47 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2402.D) 2.249 3.344 4.912 6.999 9.840

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2402.D

Sample Name: Salisbury R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:34:54 AM IGG Page 1 of 2

EA# 0910-96 Page 53 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 25

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:26:05 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2501.D) 2.248 3.369 4.236 - Chloride 4.913 6.997 9.847

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.236 BB 89.76620 2.69549e-2 2.41964 Chloride 

Totals : 2.41964

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2501.D

Sample Name: Salisbury R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:35:06 AM IGG Page 1 of 1

EA# 0910-96 Page 54 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 25

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:43:22 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2502.D) 2.252 3.372 4.238 - Chloride 4.916 6.998 9.846

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.238 BB 87.67069 2.69712e-2 2.36459 Chloride 

Totals : 2.36459

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2502.D

Sample Name: Salisbury R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:35:19 AM IGG Page 1 of 1

EA# 0910-96 Page 55 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 33

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:23:39 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3301.D) 2.254 3.121 - Fluoride 4.261 - Chloride 5.476 7.148

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:41 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 BB 225.06882 1.70529e-2 3.83808 Fluoride 

 4.261 BV 5.95215 3.65521e-2 2.17564e-1 Chloride 

Totals : 4.05564

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3301.D

Sample Name: P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:36:45 AM IGG Page 1 of 1

EA# 0910-96 Page 56 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 33

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:35:58 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D) 2.267 3.121 - Fluoride 4.261 - Chloride 5.475 7.147

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 BB 226.27061 1.70532e-2 3.85863 Fluoride 

 4.261 BV 5.67176 3.70602e-2 2.10197e-1 Chloride 

Totals : 4.06882

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D

Sample Name: P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:36:58 AM IGG Page 1 of 1

EA# 0910-96 Page 57 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 36

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:37:38 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3601.D) 2.256 3.137 - Fluoride 4.263 - Chloride 5.483 7.154

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.137 BB 685.05603 1.70822e-2 11.70224 Fluoride 

 4.263 BB 36.18887 2.79640e-2 1.01198 Chloride 

Totals : 12.71423

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3601.D

Sample Name: P4 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:37:37 AM IGG Page 1 of 1

EA# 0910-96 Page 58 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 36

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:49:58 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3602.D) 2.256 3.137 - Fluoride 4.261 - Chloride 5.481 7.148

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.137 BB 686.89960 1.70822e-2 11.73376 Fluoride 

 4.261 BB 35.98354 2.79736e-2 1.00659 Chloride 

Totals : 12.74035

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3602.D

Sample Name: P4 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:37:45 AM IGG Page 1 of 1

EA# 0910-96 Page 59 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 37

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:02:17 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3701.D) 2.252 3.135 - Fluoride 4.261 - Chloride 5.461

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.135 BB 641.72162 1.70812e-2 10.96138 Fluoride 

 4.261 BB 28.69785 2.84053e-2 8.15170e-1 Chloride 

Totals : 11.77655

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3701.D

Sample Name: P4 R3 In A *10 0910-96

Instrument 1 10/4/2010 9:37:54 AM IGG Page 1 of 1

EA# 0910-96 Page 60 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 37

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:14:37 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3702.D) 2.255 3.135 - Fluoride 4.261 - Chloride 5.461

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.135 BB 640.17627 1.70812e-2 10.93496 Fluoride 

 4.261 BB 28.99791 2.83832e-2 8.23054e-1 Chloride 

Totals : 11.75801

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3702.D

Sample Name: P4 R3 In A *10 0910-96

Instrument 1 10/4/2010 9:38:02 AM IGG Page 1 of 1

EA# 0910-96 Page 61 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 38

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:26:57 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3801.D) 2.254 3.118 - Fluoride 4.259 - Chloride 5.466

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.118 BB 29.37646 1.67627e-2 4.92430e-1 Fluoride 

 4.259 BB 10.03031 3.23729e-2 3.24710e-1 Chloride 

Totals : 8.17140e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3801.D

Sample Name: P4 R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:10 AM IGG Page 1 of 1

EA# 0910-96 Page 62 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 38

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:39:16 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3802.D) 2.252 3.117 - Fluoride 4.258 - Chloride 5.465

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.117 BB 29.06601 1.67592e-2 4.87122e-1 Fluoride 

 4.258 BB 10.10172 3.23298e-2 3.26587e-1 Chloride 

Totals : 8.13709e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3802.D

Sample Name: P4 R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:18 AM IGG Page 1 of 1

EA# 0910-96 Page 63 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 39

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:51:37 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3901.D) 2.255 3.119 - Fluoride 4.260 - Chloride 5.480

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.119 BB 36.11133 1.68250e-2 6.07572e-1 Fluoride 

 4.260 BB 12.06006 3.13464e-2 3.78039e-1 Chloride 

Totals : 9.85611e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3901.D

Sample Name: P4 R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:26 AM IGG Page 1 of 1

EA# 0910-96 Page 64 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 39

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:03:56 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3902.D) 2.256 3.120 - Fluoride 4.260 - Chloride 5.479

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.120 BB 36.00581 1.68242e-2 6.05768e-1 Fluoride 

 4.260 BB 12.07534 3.13399e-2 3.78440e-1 Chloride 

Totals : 9.84209e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3902.D

Sample Name: P4 R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:34 AM IGG Page 1 of 1

EA# 0910-96 Page 65 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 40

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:16:16 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4001.D) 2.253 3.117 - Fluoride 4.259 - Chloride 5.460

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.117 BB 40.65833 1.68553e-2 6.85310e-1 Fluoride 

 4.259 BB 12.36708 3.12204e-2 3.86105e-1 Chloride 

Totals : 1.07142

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4001.D

Sample Name: P4 R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:42 AM IGG Page 1 of 1

EA# 0910-96 Page 66 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 40

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:28:36 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4002.D) 2.255 3.119 - Fluoride 4.261 - Chloride 5.462

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.119 BB 40.55775 1.68547e-2 6.83590e-1 Fluoride 

 4.261 BB 12.31650 3.12407e-2 3.84776e-1 Chloride 

Totals : 1.06837

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4002.D

Sample Name: P4 R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:52 AM IGG Page 1 of 1

EA# 0910-96 Page 67 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 43

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 12:29:43 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4301.D) 2.247 3.312 4.234 - Chloride 4.899 5.448 6.166 6.975 8.374 9.814

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.234 BV 4.51100 3.78526e-2 1.70753e-1 Chloride 

Totals : 1.70753e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4301.D

Sample Name: P4 R1 In B *10 0910-96

Instrument 1 10/4/2010 9:39:49 AM IGG Page 1 of 1

EA# 0910-96 Page 68 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 43

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 12:47:01 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4302.D) 2.250 3.315 4.901 5.449 9.807

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4302.D

Sample Name: P4 R1 In B *10 0910-96

Instrument 1 10/4/2010 9:39:57 AM IGG Page 1 of 2

EA# 0910-96 Page 69 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 44

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:04:23 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4401.D) 2.250 3.080 3.494 4.914 9.859

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4401.D

Sample Name: P4 R2 In B *10 0910-96

Instrument 1 10/4/2010 9:40:05 AM IGG Page 1 of 2

EA# 0910-96 Page 70 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 44

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:21:41 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4402.D) 2.249 3.080 3.494 4.914 9.861

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4402.D

Sample Name: P4 R2 In B *10 0910-96

Instrument 1 10/4/2010 9:40:14 AM IGG Page 1 of 2

EA# 0910-96 Page 71 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 45

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:38:59 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D) 2.252 3.081 3.307 3.483 4.914 9.854

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D

Sample Name: P4 R3 In B *10 0910-96

Instrument 1 10/4/2010 9:40:23 AM IGG Page 1 of 2

EA# 0910-96 Page 72 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 45

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 1:56:17 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4502.D) 2.253 3.083 3.308 3.484 4.915 9.846

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4502.D

Sample Name: P4 R3 In B *10 0910-96

Instrument 1 10/4/2010 9:40:32 AM IGG Page 1 of 2

EA# 0910-96 Page 73 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 46

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:13:36 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4601.D) 2.244 4.896 5.428 7.004 9.807

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4601.D

Sample Name: P4 R1 Out B *10 0910-96

Instrument 1 10/4/2010 9:40:41 AM IGG Page 1 of 2

EA# 0910-96 Page 74 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 46

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:30:53 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4602.D) 2.246 4.896 5.426 7.002 9.807

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4602.D

Sample Name: P4 R1 Out B *10 0910-96

Instrument 1 10/4/2010 9:56:49 AM IGG Page 1 of 2

EA# 0910-96 Page 75 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 47

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 2:48:12 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4701.D) 2.249 3.484 4.903 5.433 9.821

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4701.D

Sample Name: P4 R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:00 AM IGG Page 1 of 2

EA# 0910-96 Page 76 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 47

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 3:05:30 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4702.D) 2.246 3.483 4.903 5.431 9.819

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4702.D

Sample Name: P4 R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:16 AM IGG Page 1 of 2

EA# 0910-96 Page 77 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 48

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 3:22:48 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4801.D) 2.248 3.488 4.911 7.022 9.853

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4801.D

Sample Name: P4 R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:26 AM IGG Page 1 of 2

EA# 0910-96 Page 78 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 48

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 3:40:05 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4802.D) 2.249 3.489 4.912 7.024 9.853

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4802.D

Sample Name: P4 R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:37 AM IGG Page 1 of 2

EA# 0910-96 Page 79 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 49

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 3:57:55 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4901.D) 2.256 3.126 - Fluoride 4.262 - Chloride 5.488 7.130

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:17 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.126 BB 362.59586 1.70694e-2 6.18931 Fluoride 

 4.262 BB 5.50164 3.73938e-2 2.05727e-1 Chloride 

Totals : 6.39504

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4901.D

Sample Name: P5 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:58:22 AM IGG Page 1 of 1

EA# 0910-96 Page 80 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 49

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:10:15 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4902.D)

 Area: 5.41333

 2.312

 3.127 - Fluoride

 4.262 - Chloride

 5.481 7.127

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.127 VB 365.51782 1.70697e-2 6.23926 Fluoride 

 4.262 MM 5.41333 3.75752e-2 2.03407e-1 Chloride 

Totals : 6.44267

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4902.D

Sample Name: P5 R1 In A *10 0910-96

Instrument 1 10/4/2010 10:44:22 AM IGG Page 1 of 1

EA# 0910-96 Page 81 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 50

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:22:35 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5001.D) 2.265 3.151 - Fluoride 3.511 4.265 - Chloride 5.483 7.056

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.151 BV 937.34271 1.70860e-2 16.01546 Fluoride 

 4.265 VB 28.33126 2.84328e-2 8.05538e-1 Chloride 

Totals : 16.82100

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5001.D

Sample Name: P5 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:58:45 AM IGG Page 1 of 1

EA# 0910-96 Page 82 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 50

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:34:54 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5002.D) 2.258 3.150 - Fluoride 3.510 4.265 - Chloride 5.481 7.059

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.150 VV 935.54138 1.70860e-2 15.98466 Fluoride 

 4.265 VB 28.56014 2.84155e-2 8.11552e-1 Chloride 

Totals : 16.79621

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5002.D

Sample Name: P5 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:58:54 AM IGG Page 1 of 1

EA# 0910-96 Page 83 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 51

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:47:14 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5101.D)

 Area: 1155.26

 Area: 41.2572

 2.260

 3.158 - Fluoride

 4.265 - Chloride

 5.476 5.710 7.178

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.158 MM 1155.25562 1.70880e-2 19.74100 Fluoride 

 4.265 MM 41.25723 2.77563e-2 1.14515 Chloride 

Totals : 20.88615

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5101.D

Sample Name: P5 R3 In A *10 0910-96

Instrument 1 10/4/2010 10:46:25 AM IGG Page 1 of 1

EA# 0910-96 Page 84 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 51

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 4:59:35 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5102.D)

 Area: 40.9828

 2.261

 4.265 - Chloride

 5.474 5.710

 7.175

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.265 MM 40.98282 2.77662e-2 1.13794 Chloride 

Totals : 1.13794

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5102.D

Sample Name: P5 R3 In A *10 0910-96

Instrument 1 10/4/2010 10:48:06 AM IGG Page 1 of 1

EA# 0910-96 Page 85 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 10

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 5:39:47 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1001.D) 2.264 3.138 - Fluoride 3.501 4.252 - Chloride 5.396 6.903

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.138 BV 508.88586 1.71526e-2 8.72872 Fluoride 

 4.252 BB 14.43764 3.07776e-2 4.44356e-1 Chloride 

Totals : 9.17308

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1001.D

Sample Name: P5 R2 In A *20 0910-96

Instrument 1 10/5/2010 9:22:14 AM IGG Page 1 of 1

EA# 0910-96 Page 86 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 10

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 5:52:07 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1002.D) 2.261 3.137 - Fluoride 3.503 4.251 - Chloride 5.393 6.899

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.137 BV 506.10544 1.71527e-2 8.68108 Fluoride 

 4.251 BB 15.14480 3.05917e-2 4.63306e-1 Chloride 

Totals : 9.14439

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1002.D

Sample Name: P5 R2 In A *20 0910-96

Instrument 1 10/5/2010 9:22:22 AM IGG Page 1 of 1

EA# 0910-96 Page 87 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 11

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 6:04:27 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1101.D) 2.262 3.142 - Fluoride 4.251 - Chloride 5.398 6.977

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.142 BB 639.42731 1.71486e-2 10.96531 Fluoride 

 4.251 BB 23.24886 2.92691e-2 6.80473e-1 Chloride 

Totals : 11.64579

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1101.D

Sample Name: P5 R3 In A *20 0910-96

Instrument 1 10/5/2010 9:22:29 AM IGG Page 1 of 1

EA# 0910-96 Page 88 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 11

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 6:16:46 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1102.D) 2.265 3.174 - Fluoride 4.287 - Chloride 5.437 7.019

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.174 BB 645.62323 1.71485e-2 11.07147 Fluoride 

 4.287 BB 23.89014 2.92027e-2 6.97657e-1 Chloride 

Totals : 11.76913

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1102.D

Sample Name: P5 R3 In A *20 0910-96

Instrument 1 10/5/2010 9:22:41 AM IGG Page 1 of 1

EA# 0910-96 Page 89 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 52

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:11:54 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5201.D) 2.256 3.121 - Fluoride 3.315 4.260 - Chloride 4.588 5.477 7.099

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 BV 44.45597 1.68759e-2 7.50236e-1 Fluoride 

 4.260 BV 3.20624 3.78526e-2 1.21364e-1 Chloride 

Totals : 8.71600e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5201.D

Sample Name: P5 R1 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:05 AM IGG Page 1 of 1

EA# 0910-96 Page 90 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 52

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:24:14 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5202.D) 2.258 3.122 - Fluoride 3.323 4.258 - Chloride 4.939 5.479 7.100

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.122 BV 41.62362 1.68609e-2 7.01813e-1 Fluoride 

 4.258 BV 2.51682 3.78526e-2 9.52680e-2 Chloride 

Totals : 7.97081e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5202.D

Sample Name: P5 R1 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:14 AM IGG Page 1 of 1

EA# 0910-96 Page 91 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 57

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:15:12 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5701.D) 2.259 3.125 - Fluoride 3.321 4.262 - Chloride 4.947 5.495 7.181

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BV 48.65992 1.68950e-2 8.22109e-1 Fluoride 

 4.262 BV 3.04968 3.78526e-2 1.15438e-1 Chloride 

Totals : 9.37547e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5701.D

Sample Name: P5 R2 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:25 AM IGG Page 1 of 1

EA# 0910-96 Page 92 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 57

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:27:32 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5702.D) 2.260 3.125 - Fluoride 3.320 4.262 - Chloride 4.647 5.487 7.179

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BV 49.63752 1.68990e-2 8.38823e-1 Fluoride 

 4.262 BV 3.03725 3.78526e-2 1.14967e-1 Chloride 

Totals : 9.53790e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5702.D

Sample Name: P5 R2 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:35 AM IGG Page 1 of 1

EA# 0910-96 Page 93 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 58

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:39:51 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5801.D) 2.256 3.123 - Fluoride 3.316 4.260 - Chloride 4.940 5.482 7.149

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BV 45.96114 1.68832e-2 7.75969e-1 Fluoride 

 4.260 BV 3.00710 3.78526e-2 1.13826e-1 Chloride 

Totals : 8.89795e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5801.D

Sample Name: P5 R3 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:48 AM IGG Page 1 of 1

EA# 0910-96 Page 94 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 58

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:52:11 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:58:17 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5802.D) 2.259 3.123 - Fluoride 3.322 4.260 - Chloride 4.941 5.483 7.148

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:58:25 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BV 45.52016 1.68811e-2 7.68430e-1 Fluoride 

 4.260 BV 3.13018 3.78526e-2 1.18485e-1 Chloride 

Totals : 8.86915e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5802.D

Sample Name: P5 R3 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:57 AM IGG Page 1 of 1

EA# 0910-96 Page 95 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 59

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:03:59 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5901.D) 2.251 3.084 3.486 4.917 7.017 9.866

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5901.D

Sample Name: P5 R1 In B *10 0910-96

Instrument 1 10/4/2010 10:01:40 AM IGG Page 1 of 2

EA# 0910-96 Page 96 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 59

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:21:17 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5902.D) 2.250 3.085 3.483 4.918 7.020 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5902.D

Sample Name: P5 R1 In B *10 0910-96

Instrument 1 10/4/2010 10:01:51 AM IGG Page 1 of 2

EA# 0910-96 Page 97 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 60

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:38:36 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6001.D) 2.253 3.089 3.483 4.922 7.025 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6001.D

Sample Name: P5 R2 In B *10 0910-96

Instrument 1 10/4/2010 10:02:01 AM IGG Page 1 of 2

EA# 0910-96 Page 98 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 60

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:55:53 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6002.D) 2.254 3.092 3.483 4.923 7.024 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6002.D

Sample Name: P5 R2 In B *10 0910-96

Instrument 1 10/4/2010 10:02:10 AM IGG Page 1 of 2

EA# 0910-96 Page 99 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 61

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:13:11 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6101.D) 2.251 3.085 3.474 4.918 7.016 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6101.D

Sample Name: P5 R3 In B *10 0910-96

Instrument 1 10/4/2010 10:02:21 AM IGG Page 1 of 2

EA# 0910-96 Page 100 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 61

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:30:29 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6102.D) 2.255 3.087 3.476 4.921 7.017 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6102.D

Sample Name: P5 R3 In B *10 0910-96

Instrument 1 10/4/2010 10:02:32 AM IGG Page 1 of 2

EA# 0910-96 Page 101 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 62

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:47:47 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6201.D) 2.247 3.472 4.900 7.013 9.820

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6201.D

Sample Name: P5 R1 out B *10 0910-96

Instrument 1 10/4/2010 10:02:42 AM IGG Page 1 of 2

EA# 0910-96 Page 102 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 62

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:05:05 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6202.D) 2.244 3.471 4.898 7.011 9.820

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6202.D

Sample Name: P5 R1 out B *10 0910-96

Instrument 1 10/4/2010 10:02:51 AM IGG Page 1 of 2

EA# 0910-96 Page 103 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 63

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:22:23 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6301.D) 2.259 3.502 4.936 7.037 9.913

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6301.D

Sample Name: P5 R2 Out B *10 0910-96

Instrument 1 10/4/2010 10:03:06 AM IGG Page 1 of 2

EA# 0910-96 Page 104 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 63

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:39:41 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6302.D) 2.259 3.503 4.948 7.049 9.927

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6302.D

Sample Name: P5 R2 Out B *10 0910-96

Instrument 1 10/4/2010 10:03:15 AM IGG Page 1 of 2

EA# 0910-96 Page 105 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 64

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 10:56:59 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6401.D) 2.252 3.343 4.922 7.033 9.881

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6401.D

Sample Name: P5 R3 out B *10 0910-96

Instrument 1 10/4/2010 10:03:26 AM IGG Page 1 of 2

EA# 0910-96 Page 106 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 64

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:14:17 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6402.D) 2.254 3.344 4.923 7.031 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6402.D

Sample Name: P5 R3 out B *10 0910-96

Instrument 1 10/4/2010 10:03:35 AM IGG Page 1 of 2

EA# 0910-96 Page 107 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 67

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 12:21:26 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6701.D) 2.258 3.168 - Fluoride 4.708 5.483 8.558

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.168 BB 8.45559e-1 1.62975e-2 1.37805e-2 Fluoride 

 4.156 - - - Chloride 

Totals : 1.37805e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6701.D

Sample Name: Acid Blank *10 0910-96

Instrument 1 10/4/2010 10:03:59 AM IGG Page 1 of 1

EA# 0910-96 Page 108 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 67

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 12:33:46 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6702.D) 2.261 4.705 5.479 5.751

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6702.D

Sample Name: Acid Blank *10 0910-96

Instrument 1 10/4/2010 10:04:30 AM IGG Page 1 of 2

EA# 0910-96 Page 109 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 68

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 12:45:35 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6801.D) 2.272 3.495 4.237 - Chloride 5.599 9.700

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.237 BB 6.20201e-1 3.78526e-2 2.34762e-2 Chloride 

Totals : 2.34762e-2

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6801.D

Sample Name: Base Blank *10 0910-96

Instrument 1 10/4/2010 10:04:49 AM IGG Page 1 of 1

EA# 0910-96 Page 110 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 68

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 1:02:52 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M

Last changed : 10/4/2010 9:33:01 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6802.D) 2.268 3.496 4.238 - Chloride 5.596 9.701

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:32:52 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 4.238 BB 6.09262e-1 3.78526e-2 2.30621e-2 Chloride 

Totals : 2.30621e-2

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6802.D

Sample Name: Base Blank *10 0910-96

Instrument 1 10/4/2010 10:04:58 AM IGG Page 1 of 1

EA# 0910-96 Page 111 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 69

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 1:20:42 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6901.D) 3.539 4.286 - Chloride 9.799

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.286 VB 2.98664 3.78526e-2 1.13052e-1 Chloride 

Totals : 1.13052e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6901.D

Sample Name: DI H2O blank 0910-96

Instrument 1 10/4/2010 10:05:32 AM IGG Page 1 of 1

EA# 0910-96 Page 112 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 69

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 1:33:02 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6902.D) 2.185 2.472 3.541 4.288 - Chloride 9.810

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.288 VB 1.15224 3.78526e-2 4.36153e-2 Chloride 

Totals : 4.36153e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6902.D

Sample Name: DI H2O blank 0910-96

Instrument 1 10/4/2010 10:05:41 AM IGG Page 1 of 1

EA# 0910-96 Page 113 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 9

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 9:02:21 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0901.D) 2.269 5.499 9.879

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0901.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:28 AM IGG Page 1 of 2

EA# 0910-96 Page 114 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 9

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 9:14:41 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0902.D) 2.269 5.498 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0902.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:37 AM IGG Page 1 of 2

EA# 0910-96 Page 115 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 32

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:58:59 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3201.D) 2.271 5.499 9.893

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3201.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:54 AM IGG Page 1 of 2

EA# 0910-96 Page 116 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 32

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:11:19 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3202.D) 2.269 5.497 9.887

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3202.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:30:03 AM IGG Page 1 of 2

EA# 0910-96 Page 117 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 56

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 6:50:32 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5601.D) 2.275 5.501 9.907

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5601.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 10:07:32 AM IGG Page 1 of 2

EA# 0910-96 Page 118 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 56

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:02:52 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5602.D) 2.273 5.498 9.894

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 - - - Fluoride 

 4.156 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5602.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 10:07:41 AM IGG Page 1 of 2

EA# 0910-96 Page 119 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 9

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 5:15:07 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0901.D) 2.275 5.443

 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.149 - - - Fluoride 

 4.153 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0901.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/5/2010 9:21:57 AM IGG Page 1 of 2

EA# 0910-96 Page 120 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 9

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 5:27:28 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0902.D) 2.277 5.445

 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.149 - - - Fluoride 

 4.153 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0902.D

Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/5/2010 9:22:05 AM IGG Page 1 of 2

EA# 0910-96 Page 121 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 11

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 9:51:40 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1101.D) 2.255 3.132 - Fluoride 3.512 4.254 - Chloride 5.444 5.988 6.253 7.005 8.480

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.132 BV 663.60602 1.70817e-2 11.33552 Fluoride 

 4.254 VB 136.56146 2.67214e-2 3.64911 Chloride 

Totals : 14.98464

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1101.D

Sample Name: MS Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:40 AM IGG Page 1 of 1

EA# 0910-96 Page 122 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 11

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 10:04:00 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1102.D) 2.252 3.131 - Fluoride 3.510 4.253 - Chloride 5.443 5.988 6.253 7.005 8.479

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.131 BV 661.14001 1.70817e-2 11.29336 Fluoride 

 4.253 VB 136.65158 2.67211e-2 3.65148 Chloride 

Totals : 14.94484

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1102.D

Sample Name: MS Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:49 AM IGG Page 1 of 1

EA# 0910-96 Page 123 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 12

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 10:16:20 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1201.D) 2.255 3.131 - Fluoride 3.511 4.255 - Chloride 5.435 5.993 6.250 7.003 8.478

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.131 BV 626.82330 1.70808e-2 10.70667 Fluoride 

 4.255 VB 129.13361 2.67472e-2 3.45396 Chloride 

Totals : 14.16063

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1201.D

Sample Name: MSD Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:31:01 AM IGG Page 1 of 1

EA# 0910-96 Page 124 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 12

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 10:28:39 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1202.D) 2.256 3.132 - Fluoride 3.513 4.256 - Chloride 5.436 5.994 6.251 7.004 8.480

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:29:44 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.132 BV 629.07855 1.70809e-2 10.74523 Fluoride 

 4.256 VB 128.93863 2.67479e-2 3.44883 Chloride 

Totals : 14.19406

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1202.D

Sample Name: MSD Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:31:16 AM IGG Page 1 of 1

EA# 0910-96 Page 125 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 34

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 8:48:18 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3401.D) 2.265 3.125 - Fluoride 4.259 - Chloride 5.474 5.985 6.313 7.081 8.490

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 406.57947 1.70724e-2 6.94127 Fluoride 

 4.259 BB 113.87910 2.68106e-2 3.05317 Chloride 

Totals : 9.99444

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3401.D

Sample Name: MS P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:06 AM IGG Page 1 of 1

EA# 0910-96 Page 126 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 34

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:00:38 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3402.D) 2.255 3.125 - Fluoride 4.260 - Chloride 5.475 5.984 6.314 7.082 8.489

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 406.89011 1.70724e-2 6.94659 Fluoride 

 4.260 BB 114.10727 2.68095e-2 3.05916 Chloride 

Totals : 10.00575

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3402.D

Sample Name: MS P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:14 AM IGG Page 1 of 1

EA# 0910-96 Page 127 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 35

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:12:58 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3501.D) 2.256 3.126 - Fluoride 4.260 - Chloride 5.474 5.981 6.311 7.078 8.488

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.126 BB 408.43451 1.70725e-2 6.97299 Fluoride 

 4.260 BB 114.63012 2.68071e-2 3.07290 Chloride 

Totals : 10.04589

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3501.D

Sample Name: MSD P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:22 AM IGG Page 1 of 1

EA# 0910-96 Page 128 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 35

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 9:25:18 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:36:41 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3502.D) 2.253 3.124 - Fluoride 4.259 - Chloride 5.472 5.980 6.310 7.076 8.488

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.124 BB 406.71420 1.70724e-2 6.94358 Fluoride 

 4.259 BB 114.74656 2.68066e-2 3.07596 Chloride 

Totals : 10.01954

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3502.D

Sample Name: MSD P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:30 AM IGG Page 1 of 1

EA# 0910-96 Page 129 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 8:37:42 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0801.D) 2.270 3.118 - Fluoride 4.258 - Chloride 5.498 6.106 6.911 8.438 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.118 BB 314.60535 1.70653e-2 5.36884 Fluoride 

 4.258 BB 188.15720 2.65985e-2 5.00471 Chloride 

Totals : 10.37355

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0801.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:28:54 AM IGG Page 1 of 1

EA# 0910-96 Page 130 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 8:50:01 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0802.D) 2.267 3.115 - Fluoride 4.255 - Chloride 5.494 6.101 6.906 8.435 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.115 BB 313.83789 1.70652e-2 5.35572 Fluoride 

 4.255 BB 188.36598 2.65982e-2 5.01019 Chloride 

Totals : 10.36591

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0802.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:03 AM IGG Page 1 of 1

EA# 0910-96 Page 131 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 31

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:34:20 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3101.D) 2.268 3.116 - Fluoride 4.256 - Chloride 5.493 6.099 6.907 8.432 9.887

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.116 BB 313.15643 1.70652e-2 5.34407 Fluoride 

 4.256 BB 188.40083 2.65981e-2 5.01111 Chloride 

Totals : 10.35518

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3101.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:11 AM IGG Page 1 of 1

EA# 0910-96 Page 132 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 31

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 7:46:39 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3102.D) 2.271 3.117 - Fluoride 4.257 - Chloride 5.497 6.103 6.910 8.433 9.879

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.117 BB 313.53778 1.70652e-2 5.35059 Fluoride 

 4.257 BB 188.47112 2.65980e-2 5.01295 Chloride 

Totals : 10.36354

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3102.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:20 AM IGG Page 1 of 1

EA# 0910-96 Page 133 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 55

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 6:25:53 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5501.D) 2.272 3.121 - Fluoride 4.263 - Chloride 5.498 6.113 6.920 8.440 9.894

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 BB 305.91211 1.70644e-2 5.22022 Fluoride 

 4.263 BB 183.26718 2.66072e-2 4.87623 Chloride 

Totals : 10.09645

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5501.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 10:07:13 AM IGG Page 1 of 1

EA# 0910-96 Page 134 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 55

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 6:38:13 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5502.D) 2.275 3.122 - Fluoride 4.265 - Chloride 5.501 6.118 6.925 8.442 9.900

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.122 BB 305.85730 1.70644e-2 5.21928 Fluoride 

 4.265 BB 183.06128 2.66076e-2 4.87082 Chloride 

Totals : 10.09010

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5502.D

Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 10:07:23 AM IGG Page 1 of 1

EA# 0910-96 Page 135 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 4:50:29 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0801.D) 2.278 3.124 - Fluoride 4.249 - Chloride 5.448 6.054 6.834 8.415

 9.881

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.124 BB 307.02579 1.71654e-2 5.27021 Fluoride 

 4.249 BB 181.57738 2.71138e-2 4.92325 Chloride 

Totals : 10.19346

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0801.D

Sample Name: HPLC53pg100 #LCS

Instrument 1 10/5/2010 9:21:31 AM IGG Page 1 of 1

EA# 0910-96 Page 136 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 5:02:47 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0802.D) 2.277 3.125 - Fluoride 4.249 - Chloride 5.444 6.051 6.831 8.414

 9.886

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 307.89706 1.71653e-2 5.28514 Fluoride 

 4.249 BB 181.32318 2.71142e-2 4.91644 Chloride 

Totals : 10.20157

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0802.D

Sample Name: HPLC53pg100 #LCS

Instrument 1 10/5/2010 9:21:38 AM IGG Page 1 of 1

EA# 0910-96 Page 137 of 202
Calibration 

Curve Chromatograms

EA# 0910-96 Page 138 of 202
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : 10/4/2010 9:26:06 AM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.000 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.000 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Connected

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 3.147 1 1 2.00000e-1 11.23373 1.78035e-2 Fluoride 

 2 1.00000 61.93819 1.61451e-2 

 3 5.00000 309.42168 1.61592e-2 

 4 10.00000 593.11342 1.68602e-2 

 5 15.00000 852.09720 1.76036e-2 

 4.156 1 1 2.00000e-1 5.55649 3.59939e-2 Chloride 

 2 1.00000 34.57356 2.89238e-2 

 3 5.00000 185.83790 2.69052e-2 

 4 10.00000 378.92274 2.63906e-2 

 5 15.00000 570.98003 2.62706e-2 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Instrument 1 10/4/2010 9:27:53 AM IGG Page 1 of 2

EA# 0910-96 Page 139 of 202
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 10

Area

0

100

200

300

400

500

600

700

800

1

2

3

4

5

Fluoride at exp. RT: 3.147

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99937

Residual Std. Dev.: 18.29678

Formula: y = mx + b

 m: 58.49156

 b: 5.73482e-1 

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.2

 Level 3 : 0.04

 Level 4 : 0.02

 Level 5 : 0.013333

Amount[ug/mL]

0 10

Area

0

100

200

300

400

500

1

2

3

4

5

Chloride at exp. RT: 4.156

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99996

Residual Std. Dev.: 2.00920

Formula: y = mx + b

 m: 38.06134

 b: -2.32861

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.2

 Level 3 : 0.04

 Level 4 : 0.02

 Level 5 : 0.013333

=====================================================================

Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Instrument 1 10/4/2010 9:27:53 AM IGG Page 2 of 2

EA# 0910-96 Page 140 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 6:10:43 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0201.D) 2.216 2.984 - Fluoride 4.161 - Chloride 5.508 7.086

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.984 VB 11.43427 1.62975e-2 1.86350e-1 Fluoride 

 4.161 BB 5.52259 3.73516e-2 2.06278e-1 Chloride 

Totals : 3.92628e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0201.D

Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:21:47 AM IGG Page 1 of 1

EA# 0910-96 Page 141 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 6:23:04 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0202.D)

 Area: 10.9018

 Area: 5.51022

 2.980 - Fluoride

 4.156 - Chloride

 5.489

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.980 MM 10.90178 1.62975e-2 1.77672e-1 Fluoride 

 4.156 MM 5.51022 3.73765e-2 2.05952e-1 Chloride 

Totals : 3.83625e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0202.D

Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:06 AM IGG Page 1 of 1

EA# 0910-96 Page 142 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 70

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 1:45:22 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7001.D) 2.220 2.990 - Fluoride 4.158 - Chloride 5.469 7.035

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.990 VB 11.61392 1.62975e-2 1.89278e-1 Fluoride 

 4.158 BB 5.54815 3.73006e-2 2.06949e-1 Chloride 

Totals : 3.96227e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7001.D

Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:15 AM IGG Page 1 of 1

EA# 0910-96 Page 143 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 70

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 1:57:42 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7002.D)

 Area: 10.9849

 Area: 5.64502

 2.990 - Fluoride

 4.155 - Chloride

 5.455

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.990 MM 10.98494 1.62975e-2 1.79028e-1 Fluoride 

 4.155 MM 5.64502 3.71113e-2 2.09494e-1 Chloride 

Totals : 3.88522e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7002.D

Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:29 AM IGG Page 1 of 1

EA# 0910-96 Page 144 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 6:35:23 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0301.D) 2.260 3.106 - Fluoride 4.265 - Chloride 5.507 6.148 6.992 8.426 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.106 VB 62.57794 1.69398e-2 1.06006 Fluoride 

 4.265 BB 34.83099 2.80299e-2 9.76308e-1 Chloride 

Totals : 2.03637

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0301.D

Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:22:59 AM IGG Page 1 of 1

EA# 0910-96 Page 145 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 6:47:44 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0302.D) 2.268 3.105 - Fluoride 4.262 - Chloride 5.512 6.141 6.981 8.425 9.860

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.105 BB 60.57874 1.69346e-2 1.02588 Fluoride 

 4.262 BB 33.81343 2.80827e-2 9.49573e-1 Chloride 

Totals : 1.97545

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0302.D

Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:23:48 AM IGG Page 1 of 1

EA# 0910-96 Page 146 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 71

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 2:10:01 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7101.D) 2.270 3.116 - Fluoride 4.267 - Chloride 5.483 6.119 6.950 8.450 9.913

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.116 VB 63.31603 1.69416e-2 1.07268 Fluoride 

 4.267 BB 35.34018 2.80046e-2 9.89686e-1 Chloride 

Totals : 2.06236

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7101.D

Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:23:56 AM IGG Page 1 of 1

EA# 0910-96 Page 147 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 71

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 2:22:21 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7102.D) 2.275 3.115 - Fluoride 4.267 - Chloride 5.493 6.122 6.950 8.450 9.913

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.115 BB 61.28004 1.69365e-2 1.03787 Fluoride 

 4.267 BB 34.30963 2.80566e-2 9.62610e-1 Chloride 

Totals : 2.00048

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7102.D

Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:24:05 AM IGG Page 1 of 1

EA# 0910-96 Page 148 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 6:59:03 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0401.D) 2.265 3.112 - Fluoride 4.257 - Chloride 5.506 6.118 6.930 8.421 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.112 BB 308.75937 1.70647e-2 5.26889 Fluoride 

 4.257 BB 185.12665 2.66039e-2 4.92508 Chloride 

Totals : 10.19398

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0401.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:15 AM IGG Page 1 of 1

EA# 0910-96 Page 149 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 7:11:22 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0402.D) 2.266 3.113 - Fluoride 4.257 - Chloride 5.505 6.116 6.927 8.424 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.113 BB 308.33966 1.70647e-2 5.26172 Fluoride 

 4.257 BB 185.05852 2.66040e-2 4.92329 Chloride 

Totals : 10.18501

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0402.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:23 AM IGG Page 1 of 1

EA# 0910-96 Page 150 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 72

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 2:34:41 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7201.D) 2.277 3.124 - Fluoride 4.263 - Chloride 5.494 6.107 6.908 8.444 9.920

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.124 BB 309.26727 1.70648e-2 5.27758 Fluoride 

 4.263 BB 186.31842 2.66017e-2 4.95640 Chloride 

Totals : 10.23397

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7201.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:36 AM IGG Page 1 of 1

EA# 0910-96 Page 151 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 72

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 2:47:01 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7202.D) 2.277 3.125 - Fluoride 4.266 - Chloride 5.498 6.110 6.913 8.452 9.926

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 311.32043 1.70650e-2 5.31268 Fluoride 

 4.266 BB 186.84802 2.66008e-2 4.97031 Chloride 

Totals : 10.28299

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7202.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:44 AM IGG Page 1 of 1

EA# 0910-96 Page 152 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 7:23:42 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0501.D) 2.267 3.125 - Fluoride 4.256 - Chloride 5.501 6.110 6.899 8.423 9.866

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 592.99884 1.70799e-2 10.12839 Fluoride 

 4.256 BB 377.41034 2.64355e-2 9.97703 Chloride 

Totals : 20.10542

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0501.D

Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:24:57 AM IGG Page 1 of 1

EA# 0910-96 Page 153 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 7:36:02 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0502.D) 2.263 3.123 - Fluoride 4.254 - Chloride 5.495 6.102 6.891 8.422 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BB 591.84839 1.70799e-2 10.10872 Fluoride 

 4.254 BB 377.41174 2.64355e-2 9.97706 Chloride 

Totals : 20.08578

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0502.D

Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:05 AM IGG Page 1 of 1

EA# 0910-96 Page 154 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 73

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 2:59:21 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7301.D) 2.274 3.135 - Fluoride 4.263 - Chloride 5.491 5.968 6.100 6.882 8.443 9.919

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.135 BB 594.09766 1.70800e-2 10.14718 Fluoride 

 4.263 BB 380.40378 2.64342e-2 10.05567 Chloride 

Totals : 20.20285

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7301.D

Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:21 AM IGG Page 1 of 1

EA# 0910-96 Page 155 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 73

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 3:11:41 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:21:17 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7302.D) 2.276 3.135 - Fluoride 4.264 - Chloride 5.494 5.970 6.103 6.884 8.444 9.920

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.135 BB 593.50879 1.70800e-2 10.13711 Fluoride 

 4.264 BB 380.46509 2.64342e-2 10.05728 Chloride 

Totals : 20.19439

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7302.D

Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:29 AM IGG Page 1 of 1

EA# 0910-96 Page 156 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 7:48:22 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0601.D) 2.266 3.134 - Fluoride 4.255 - Chloride 5.966 6.102 6.873 8.425 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.134 BB 847.65564 1.70849e-2 14.48213 Fluoride 

 4.255 BB 568.12811 2.63811e-2 14.98783 Chloride 

Totals : 29.46995

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0601.D

Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:29 AM IGG Page 1 of 1

EA# 0910-96 Page 157 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 8:00:42 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0602.D) 2.265 3.134 - Fluoride 4.254 - Chloride 5.963 6.098 6.868 8.423 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.134 BB 850.78156 1.70850e-2 14.53557 Fluoride 

 4.254 BB 567.44427 2.63812e-2 14.96986 Chloride 

Totals : 29.50543

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0602.D

Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:37 AM IGG Page 1 of 1

EA# 0910-96 Page 158 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 74

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 3:24:00 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7401.D) 2.276 3.147 - Fluoride 4.266 - Chloride 5.495 5.951 6.105 6.873 8.443 9.920

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.147 BB 856.55316 1.70850e-2 14.63424 Fluoride 

 4.266 BB 574.05273 2.63800e-2 15.14349 Chloride 

Totals : 29.77773

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7401.D

Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:45 AM IGG Page 1 of 1

EA# 0910-96 Page 159 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 74

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/3/2010 3:36:20 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7402.D) 2.276 3.148 - Fluoride 4.268 - Chloride 5.495 5.952 6.106 6.873 8.447 9.921

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.148 BB 853.39844 1.70850e-2 14.58031 Fluoride 

 4.268 BB 574.29498 2.63799e-2 15.14985 Chloride 

Totals : 29.73016

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7402.D

Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:54 AM IGG Page 1 of 1

EA# 0910-96 Page 160 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 8:13:01 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0701.D) 2.266 3.105 - Fluoride 4.255 - Chloride 5.494 6.106 6.931 8.434 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.105 BB 75.83907 1.69672e-2 1.28678 Fluoride 

 4.255 BB 89.04053 2.69605e-2 2.40058 Chloride 

Totals : 3.68735

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0701.D

Sample Name: HPLC53pg98 #SS

Instrument 1 10/4/2010 9:28:12 AM IGG Page 1 of 1

EA# 0910-96 Page 161 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/1/2010 8:25:21 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:26:06 AM by IGG

 (modified after loading)

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0702.D) 2.270 3.109 - Fluoride 4.259 - Chloride 5.499 6.109 6.933 8.441 9.879

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:26:06 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.109 BB 75.80476 1.69671e-2 1.28619 Fluoride 

 4.259 BB 89.01553 2.69607e-2 2.39992 Chloride 

Totals : 3.68611

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0702.D

Sample Name: HPLC53pg98 #SS

Instrument 1 10/4/2010 9:28:20 AM IGG Page 1 of 1

EA# 0910-96 Page 162 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 12:19:37 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1701.D) 2.267 3.115 - Fluoride 4.253 - Chloride 5.486 6.092 6.899 8.430 9.879

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.115 BB 305.79456 1.70644e-2 5.21821 Fluoride 

 4.253 BB 183.50085 2.66068e-2 4.88237 Chloride 

Totals : 10.10057

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1701.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:05:55 AM IGG Page 1 of 1

EA# 0910-96 Page 163 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 12:31:57 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1702.D) 2.267 3.115 - Fluoride 4.254 - Chloride 5.492 6.096 6.903 8.432 9.873

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.115 BB 305.05637 1.70643e-2 5.20559 Fluoride 

 4.254 BB 182.77678 2.66081e-2 4.86334 Chloride 

Totals : 10.06893

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1702.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:04 AM IGG Page 1 of 1

EA# 0910-96 Page 164 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 29

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 6:45:00 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2901.D) 2.271 3.117 - Fluoride 4.257 - Chloride 5.495 6.100 6.907 8.436 9.893

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.117 BB 305.44266 1.70644e-2 5.21219 Fluoride 

 4.257 BB 183.08054 2.66076e-2 4.87132 Chloride 

Totals : 10.08352

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2901.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:14 AM IGG Page 1 of 1

EA# 0910-96 Page 165 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 29

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 6:57:20 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2902.D) 2.269 3.116 - Fluoride 4.257 - Chloride 5.495 6.099 6.907 8.436 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.116 BB 304.76215 1.70643e-2 5.20056 Fluoride 

 4.257 BB 182.93237 2.66078e-2 4.86743 Chloride 

Totals : 10.06799

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2902.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:23 AM IGG Page 1 of 1

EA# 0910-96 Page 166 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 41

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:40:56 AM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4101.D) 2.280 3.129 - Fluoride 4.268 - Chloride 5.500 6.113 6.919 8.441 9.901

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.129 BB 305.45007 1.70644e-2 5.21232 Fluoride 

 4.268 BB 183.04117 2.66076e-2 4.87029 Chloride 

Totals : 10.08261

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4101.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:07:50 AM IGG Page 1 of 1

EA# 0910-96 Page 167 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 41

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:53:15 AM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4102.D) 2.271 3.119 - Fluoride 4.259 - Chloride 5.495 6.101 6.908 8.437 9.886

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.119 BB 304.57260 1.70643e-2 5.19732 Fluoride 

 4.259 BB 182.35486 2.66089e-2 4.85226 Chloride 

Totals : 10.04957

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4102.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:00 AM IGG Page 1 of 1

EA# 0910-96 Page 168 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 53

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:36:34 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5301.D) 2.273 3.121 - Fluoride 4.260 - Chloride 5.491 6.104 6.910 8.436 9.900

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.121 BB 306.69925 1.70645e-2 5.23367 Fluoride 

 4.260 BB 183.57710 2.66066e-2 4.88437 Chloride 

Totals : 10.11805

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5301.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:09 AM IGG Page 1 of 1

EA# 0910-96 Page 169 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 53

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 5:48:53 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5302.D) 2.272 3.120 - Fluoride 4.261 - Chloride 5.496 6.107 6.914 8.436 9.900

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.120 BB 305.72400 1.70644e-2 5.21700 Fluoride 

 4.261 BB 182.98579 2.66077e-2 4.86884 Chloride 

Totals : 10.08584

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5302.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:18 AM IGG Page 1 of 1

EA# 0910-96 Page 170 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 65

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:32:07 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6501.D) 2.277 3.123 - Fluoride 4.263 - Chloride 5.494 6.111 6.913 8.444 9.907

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BB 310.41275 1.70649e-2 5.29716 Fluoride 

 4.263 BB 185.78922 2.66027e-2 4.94249 Chloride 

Totals : 10.23965

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6501.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:09:36 AM IGG Page 1 of 1

EA# 0910-96 Page 171 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 65

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/2/2010 11:44:27 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Last changed : 10/4/2010 9:39:38 AM by IGG

2 4 6 8 10 12 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6502.D) 2.297 3.122 - Fluoride 4.263 - Chloride 5.493 6.111 6.914 8.443 9.913

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/4/2010 9:36:48 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.122 VB 310.73752 1.70649e-2 5.30271 Fluoride 

 4.263 BB 186.29073 2.66018e-2 4.95567 Chloride 

Totals : 10.25838

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6502.D

Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:09:47 AM IGG Page 1 of 1

EA# 0910-96 Page 172 of 202
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : 10/5/2010 9:18:49 AM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.000 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.000 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Connected

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 3.149 1 1 2.00000e-1 9.95712 2.00861e-2 Fluoride 

 2 1.00000 61.11817 1.63617e-2 

 3 5.00000 308.63791 1.62002e-2 

 4 10.00000 589.09669 1.69751e-2 

 5 15.00000 849.33438 1.76609e-2 

 4.153 1 1 2.00000e-1 5.66901 3.52795e-2 Chloride 

 2 1.00000 33.68365 2.96880e-2 

 3 5.00000 182.27121 2.74317e-2 

 4 10.00000 369.59518 2.70566e-2 

 5 15.00000 562.35474 2.66736e-2 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Instrument 1 10/5/2010 9:20:49 AM IGG Page 1 of 2

EA# 0910-96 Page 173 of 202
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 10

Area

0

100

200

300

400

500

600

700

800

1

2

3

4

5

Fluoride at exp. RT: 3.149

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99933

Residual Std. Dev.: 18.30415

Formula: y = mx + b

 m: 58.36617

 b: -5.76052e-1 

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.2

 Level 3 : 0.04

 Level 4 : 0.02

 Level 5 : 0.013333

Amount[ug/mL]

0 10

Area

0

100

200

300

400

500

1

2

3

4

5

Chloride at exp. RT: 4.153

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99993

Residual Std. Dev.: 3.24460

Formula: y = mx + b

 m: 37.31718

 b: -2.14447

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.2

 Level 3 : 0.04

 Level 4 : 0.02

 Level 5 : 0.013333

=====================================================================

Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Instrument 1 10/5/2010 9:20:49 AM IGG Page 2 of 2

EA# 0910-96 Page 174 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 2:22:30 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0201.D)

 Area: 9.55972

 2.225

 2.990 - Fluoride

 4.157 - Chloride

 5.462

 7.014

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.990 MM 9.55972 1.80226e-2 1.72291e-1 Fluoride 

 4.157 BB 5.61364 3.70342e-2 2.07896e-1 Chloride 

Totals : 3.80187e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0201.D

Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:41 AM IGG Page 1 of 1

EA# 0910-96 Page 175 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 2:34:50 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0202.D)

 Area: 5.87644

 2.221

 2.985 - Fluoride

 4.150 - Chloride

 5.441

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.985 VB 10.01584 1.80226e-2 1.80511e-1 Fluoride 

 4.150 MM 5.87644 3.65764e-2 2.14939e-1 Chloride 

Totals : 3.95450e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0202.D

Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:55 AM IGG Page 1 of 1

EA# 0910-96 Page 176 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 14

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 7:38:19 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1401.D)

 Area: 10.0541 2.991 - Fluoride

 4.154 - Chloride

 5.445

 6.985

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.991 MM 10.05413 1.80226e-2 1.81201e-1 Fluoride 

 4.154 BB 5.65120 3.69661e-2 2.08903e-1 Chloride 

Totals : 3.90104e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1401.D

Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:17:10 AM IGG Page 1 of 1

EA# 0910-96 Page 177 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 14

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 7:50:38 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1402.D)

 Area: 5.53477

 2.221

 2.989 - Fluoride

 4.153 - Chloride

 5.436

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.989 VB 10.19880 1.80226e-2 1.83809e-1 Fluoride 

 4.153 MM 5.53477 3.71800e-2 2.05783e-1 Chloride 

Totals : 3.89592e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1402.D

Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:25 AM IGG Page 1 of 1

EA# 0910-96 Page 178 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 2:47:11 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0301.D) 2.270 3.114 - Fluoride 4.258 - Chloride 5.461 6.095 6.913 8.401

 9.860

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.114 VB 62.22894 1.72918e-2 1.07605 Fluoride 

 4.258 BB 34.35212 2.84702e-2 9.78010e-1 Chloride 

Totals : 2.05406

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0301.D

Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:19 AM IGG Page 1 of 1

EA# 0910-96 Page 179 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 2:59:30 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0302.D) 2.277 3.115 - Fluoride 4.257 - Chloride 5.467 6.093 6.907 8.405

 9.867

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.115 BB 59.91656 1.72979e-2 1.03643 Fluoride 

 4.257 BB 32.97707 2.85399e-2 9.41163e-1 Chloride 

Totals : 1.97760

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0302.D

Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:28 AM IGG Page 1 of 1

EA# 0910-96 Page 180 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 15

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 8:02:58 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1501.D) 2.270 3.118 - Fluoride 4.267 - Chloride 5.468 6.116 6.941 8.415

 9.887

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.118 VB 62.23907 1.72918e-2 1.07622 Fluoride 

 4.267 BB 34.30110 2.84726e-2 9.76643e-1 Chloride 

Totals : 2.05287

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1501.D

Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:37 AM IGG Page 1 of 1

EA# 0910-96 Page 181 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 15

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 8:15:17 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1502.D) 2.280 3.119 - Fluoride 4.268 - Chloride 5.478 6.120 6.942 8.415

 9.886

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.119 BB 60.08810 1.72975e-2 1.03937 Fluoride 

 4.268 BB 33.10430 2.85332e-2 9.44572e-1 Chloride 

Totals : 1.98394

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1502.D

Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:46 AM IGG Page 1 of 1

EA# 0910-96 Page 182 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 3:11:49 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0401.D) 2.276 3.123 - Fluoride 4.252 - Chloride 5.461 6.071 6.857 8.400

 9.873

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BB 308.96735 1.71652e-2 5.30347 Fluoride 

 4.252 BB 182.23886 2.71126e-2 4.94098 Chloride 

Totals : 10.24445

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0401.D

Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:17:53 AM IGG Page 1 of 1

EA# 0910-96 Page 183 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 3:24:10 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0402.D) 2.275 3.123 - Fluoride 4.251 - Chloride 5.455 6.064 6.848 8.404

 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.123 BB 308.16321 1.71652e-2 5.28970 Fluoride 

 4.251 BB 182.15358 2.71128e-2 4.93869 Chloride 

Totals : 10.22839

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0402.D

Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:01 AM IGG Page 1 of 1

EA# 0910-96 Page 184 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 16

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 8:27:38 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1601.D) 2.278 3.127 - Fluoride 4.264 - Chloride 5.476 6.102 6.898 8.406

 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.127 BB 309.30249 1.71651e-2 5.30921 Fluoride 

 4.264 BB 182.42313 2.71123e-2 4.94591 Chloride 

Totals : 10.25513

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1601.D

Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:09 AM IGG Page 1 of 1

EA# 0910-96 Page 185 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 16

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 8:39:57 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1602.D) 2.276 3.125 - Fluoride 4.262 - Chloride 5.475 6.103 6.900 8.403

 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.125 BB 308.11859 1.71652e-2 5.28893 Fluoride 

 4.262 BB 182.26926 2.71126e-2 4.94179 Chloride 

Totals : 10.23072

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1602.D

Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:16 AM IGG Page 1 of 1

EA# 0910-96 Page 186 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 3:36:29 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:16:05 AM by IGG

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0501.D) 2.277 3.135 - Fluoride 4.251 - Chloride 5.454 5.937 6.063 6.826 8.407

 9.873

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.135 BB 587.12793 1.71500e-2 10.06926 Fluoride 

 4.251 BB 369.45987 2.69528e-2 9.95800 Chloride 

Totals : 20.02725

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0501.D

Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:18:24 AM IGG Page 1 of 1

EA# 0910-96 Page 187 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 3:48:49 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0502.D) 2.283 3.149 - Fluoride 4.265 - Chloride 5.465 5.950 6.073 6.837 8.421

 9.894

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.149 BB 590.64954 1.71499e-2 10.12959 Fluoride 

 4.265 BB 369.45181 2.69529e-2 9.95778 Chloride 

Totals : 20.08737

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0502.D

Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:18:52 AM IGG Page 1 of 1

EA# 0910-96 Page 188 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 8:52:17 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1701.D) 2.295 3.154 - Fluoride 4.280 - Chloride 5.491 5.991 6.117 6.894 8.421

 9.899

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.154 BB 587.89532 1.71500e-2 10.08241 Fluoride 

 4.280 BB 369.70758 2.69527e-2 9.96463 Chloride 

Totals : 20.04704

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1701.D

Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:19:17 AM IGG Page 1 of 1

EA# 0910-96 Page 189 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 9:04:37 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1702.D) 2.277 3.138 - Fluoride 4.265 - Chloride 5.478 5.979 6.105 6.884 8.403

 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.138 BB 590.71399 1.71499e-2 10.13070 Fluoride 

 4.265 BB 369.76144 2.69527e-2 9.96608 Chloride 

Totals : 20.09677

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1702.D

Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:19:28 AM IGG Page 1 of 1

EA# 0910-96 Page 190 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 4:01:09 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0601.D) 2.274 3.144 - Fluoride 4.250 - Chloride 5.444 5.910 6.055 6.803 8.407

 9.881

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.144 BB 849.68134 1.71448e-2 14.56764 Fluoride 

 4.250 BB 562.55444 2.68995e-2 15.13241 Chloride 

Totals : 29.70005

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0601.D

Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:38 AM IGG Page 1 of 1

EA# 0910-96 Page 191 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 4:13:29 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0602.D) 2.276 3.145 - Fluoride 4.250 - Chloride 5.443 5.909 6.054 6.801 8.407

 9.873

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.145 BB 847.86249 1.71449e-2 14.53648 Fluoride 

 4.250 BB 562.09290 2.68995e-2 15.12004 Chloride 

Totals : 29.65652

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0602.D

Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:46 AM IGG Page 1 of 1

EA# 0910-96 Page 192 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 18

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 9:16:57 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1801.D) 2.276 3.148 - Fluoride 4.265 - Chloride 5.475 5.953 6.103 6.867 8.403

 9.893

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.148 BB 851.27545 1.71448e-2 14.59495 Fluoride 

 4.265 BB 562.78735 2.68994e-2 15.13865 Chloride 

Totals : 29.73360

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1801.D

Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:54 AM IGG Page 1 of 1

EA# 0910-96 Page 193 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 18

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 9:29:17 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1802.D) 2.276 3.146 - Fluoride 4.263 - Chloride 5.474 5.952 6.101 6.866 8.395

 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.146 BB 848.51825 1.71448e-2 14.54771 Fluoride 

 4.263 BB 561.98425 2.68996e-2 15.11713 Chloride 

Totals : 29.66484

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1802.D

Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:20:02 AM IGG Page 1 of 1

EA# 0910-96 Page 194 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 4:38:08 PM Inj : 2

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0702.D) 2.276 3.117 - Fluoride 4.251 - Chloride 5.446 6.053 6.851 8.419

 9.874

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:21:11 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.117 BB 76.75529 1.72618e-2 1.32493 Fluoride 

 4.251 BB 90.33049 2.74335e-2 2.47808 Chloride 

Totals : 3.80301

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0702.D

Sample Name: HPLC53pg100 #SS

Instrument 1 10/5/2010 9:21:23 AM IGG Page 1 of 1

EA# 0910-96 Page 195 of 202
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Mr_Burns Location : -

Injection Date : 10/4/2010 4:25:48 PM Inj : 1

Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M

Last changed : 4/1/2010 4:15:36 PM

Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Last changed : 10/5/2010 9:18:49 AM by IGG

 (modified after loading)

2 4 6 8 min

uS/cm

0

20

40

60

80

100

120

140

160

180

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0701.D) 2.278 3.119 - Fluoride 4.253 - Chloride 5.450 6.059 6.858 8.419

 9.880

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : 10/5/2010 9:18:49 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [uS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 3.119 BB 76.93913 1.72615e-2 1.32808 Fluoride 

 4.253 BB 90.24962 2.74341e-2 2.47591 Chloride 

Totals : 3.80400

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0701.D

Sample Name: HPLC53pg100 #SS

Instrument 1 10/5/2010 9:21:08 AM IGG Page 1 of 1

EA# 0910-96 Page 196 of 202
 Method Information

 Method: U:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

 Modified: 1/13/2010 at 7:06:26 AM

=========================================================================

 ANALOG DIGITAL CONVERTER

=========================================================================

 Signal 1

 ---------------------

Description: ADC1 A, Metrohm

Source: Signal

Unit: mAU

Units/Volt: 100.000

Peakwidth (Data Rate): 0.027 Min (10.00 Hz)

Stop Time: No Limit

Data Storage: All

Start Signal Source: External Device Will Start 35900

Timed Event Table:

 <no events>

 method: U:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Modified on: 1/13/2010 at 7:06:26 AM

Smithers 1/18/2010 7:20:57 AM mgb Page 1 of 1

EA# 0910-96 Page 197 of 202
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 127 DI Rinse METROHM 4 Sample 

 

 2 Vial 1 HPLC53pg98 #1 METROHM 2 Sample 

 3 Vial 2 HPLC53pg98 #2 METROHM 2 Sample 

 4 Vial 3 HPLC53pg98 #3 METROHM 2 Sample 

 5 Vial 4 HPLC53pg98 #4 METROHM 2 Sample 

 6 Vial 5 HPLC53pg98 #5 METROHM 2 Sample 

 7 Vial 6 HPLC53pg98 #SS METROHM 2 Sample 

 8 Vial 7 HPLC53pg98 #LCS METROHM 2 Sample 

 9 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample 

 10 Vial 9 Salisbury R1 In A *20 0910-96 METROHM 2 Sample 

 11 Vial 10 MS Salisbury R1 In A *20 0910-96 METROHM 2 Sample 

 12 Vial 11 MSD Salisbury R1 In A *20 0910-96 METROHM 2 Sample 

 13 Vial 12 Salisbury R2 In A *20 0910-96 METROHM 2 Sample 

 14 Vial 13 Salisbury R3 In A *20 0910-96 METROHM 2 Sample 

 15 Vial 14 Salisbury R1 Out A *10 0910-96 METROHM 2 Sample 

 16 Vial 15 Salisbury R2 Out A *10 0910-96 METROHM 2 Sample 

 17 Vial 100 HPLC53pg98 #3 METROHM 2 Sample 

 18 Vial 101 HPLC53pg98 #4 METROHM 2 Sample 

 19 Vial 16 Salisbury R3 Out A *10 0910-96 METROHM 2 Sample 

 20 Vial 17 Salisbury R1 In B *10 0910-96 METROHM 2 Sample 

 21 Vial 18 Salisbury R2 In B *10 0910-96 METROHM 2 Sample 

 22 Vial 19 Salisbury R3 In B *10 0910-96 METROHM 2 Sample 

 23 Vial 20 Salisbury R1 B Out *10 0910-96 METROHM 2 Sample 

 24 Vial 21 Salisbury R2 Out B *10 0910-96 METROHM 2 Sample 

 25 Vial 22 Salisbury R3 Out B *10 0910-96 METROHM 2 Sample 

 26 Vial 23 Salisbury R1 Out B *100 0910-96 METROHM 2 Sample 

 27 Vial 24 Salisbury R2 out B *100 0910-96 METROHM 2 Sample 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 1 of 3

EA# 0910-96 Page 198 of 202
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 28 Vial 25 Salisbury R3 Out B *100 0910-96 METROHM 2 Sample 

 

 29 Vial 100 HPLC53pg98 #3 METROHM 2 Sample 

 30 Vial 101 HPLC53pg98 #4 METROHM 2 Sample 

 31 Vial 7 HPLC53pg98 #LCS METROHM 2 Sample 

 32 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample 

 33 Vial 26 P4 R1 In A *10 0910-96 METROHM 2 Sample 

 34 Vial 27 MS P4 R1 In A *10 0910-96 METROHM 2 Sample 

 35 Vial 28 MSD P4 R1 In A *10 0910-96 METROHM 2 Sample 

 36 Vial 29 P4 R2 In A *10 0910-96 METROHM 2 Sample 

 37 Vial 30 P4 R3 In A *10 0910-96 METROHM 2 Sample 

 38 Vial 31 P4 R1 Out A *10 0910-96 METROHM 2 Sample 

 39 Vial 32 P4 R2 Out A *10 0910-96 METROHM 2 Sample 

 40 Vial 33 P4 R3 Out A *10 0910-96 METROHM 2 Sample 

 41 Vial 110 HPLC53pg98 #3 METROHM 2 Sample 

 42 Vial 111 HPLC53pg98 #4 METROHM 2 Sample 

 43 Vial 34 P4 R1 In B *10 0910-96 METROHM 2 Sample 

 44 Vial 35 P4 R2 In B *10 0910-96 METROHM 2 Sample 

 45 Vial 36 P4 R3 In B *10 0910-96 METROHM 2 Sample 

 46 Vial 37 P4 R1 Out B *10 0910-96 METROHM 2 Sample 

 47 Vial 38 P4 R2 Out B *10 0910-96 METROHM 2 Sample 

 48 Vial 39 P4 R3 Out B *10 0910-96 METROHM 2 Sample 

 49 Vial 40 P5 R1 In A *10 0910-96 METROHM 2 Sample 

 50 Vial 41 P5 R2 In A *10 0910-96 METROHM 2 Sample 

 51 Vial 42 P5 R3 In A *10 0910-96 METROHM 2 Sample 

 52 Vial 43 P5 R1 Out A *10 0910-96 METROHM 2 Sample 

 53 Vial 110 HPLC53pg98 #3 METROHM 2 Sample 

 54 Vial 111 HPLC53pg98 #4 METROHM 2 Sample 

 55 Vial 102 HPLC53pg98 #LCS METROHM 2 Sample 

 56 Vial 103 0.01N H2SO4/NaOH RB METROHM 2 Sample 

 57 Vial 44 P5 R2 Out A *10 0910-96 METROHM 2 Sample 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 2 of 3

EA# 0910-96 Page 199 of 202
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 58 Vial 45 P5 R3 Out A *10 0910-96 METROHM 2 Sample 

 

 59 Vial 46 P5 R1 In B *10 0910-96 METROHM 2 Sample 

 60 Vial 47 P5 R2 In B *10 0910-96 METROHM 2 Sample 

 61 Vial 48 P5 R3 In B *10 0910-96 METROHM 2 Sample 

 62 Vial 49 P5 R1 out B *10 0910-96 METROHM 2 Sample 

 63 Vial 50 P5 R2 Out B *10 0910-96 METROHM 2 Sample 

 64 Vial 51 P5 R3 out B *10 0910-96 METROHM 2 Sample 

 65 Vial 120 HPLC53pg98 #3 METROHM 2 Sample 

 66 Vial 121 HPLC53pg98 #4 METROHM 2 Sample 

 67 Vial 52 Acid Blank *10 0910-96 METROHM 2 Sample 

 68 Vial 53 Base Blank *10 0910-96 METROHM 2 Sample 

 69 Vial 54 DI H2O blank 0910-96 METROHM 2 Sample 

 70 Vial 1 HPLC53pg98 #1 METROHM 2 Sample 

 71 Vial 2 HPLC53pg98 #2 METROHM 2 Sample 

 72 Vial 3 HPLC53pg98 #3 METROHM 2 Sample 

 73 Vial 4 HPLC53pg98 #4 METROHM 2 Sample 

 74 Vial 5 HPLC53pg98 #5 METROHM 2 Sample 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 3 of 3

EA# 0910-96 Page 200 of 202
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 127 DI Rinse METROHM 4 Sample 

 

 2 Vial 1 HPLC53pg100 #1 METROHM 2 Sample 

 3 Vial 2 HPLC53pg100 #2 METROHM 2 Sample 

 4 Vial 3 HPLC53pg100 #3 METROHM 2 Sample 

 5 Vial 4 HPLC53pg100 #4 METROHM 2 Sample 

 6 Vial 5 HPLC53pg100 #5 METROHM 2 Sample 

 7 Vial 6 HPLC53pg100 #SS METROHM 2 Sample 

 8 Vial 7 HPLC53pg100 #LCS METROHM 2 Sample 

 9 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample 

 10 Vial 9 P5 R2 In A *20 0910-96 METROHM 2 Sample 

 11 Vial 10 P5 R3 In A *20 0910-96 METROHM 2 Sample 

 12 Vial 11 R1 C4 *10 1010-10 METROHM 2 Sample 

 13 Vial 12 R2 C4 *10 1010-10 METROHM 2 Sample 

 14 Vial 1 HPLC53pg100 #1 METROHM 2 Sample 

 15 Vial 2 HPLC53pg100 #2 METROHM 2 Sample 

 16 Vial 3 HPLC53pg100 #3 METROHM 2 Sample 

 17 Vial 4 HPLC53pg100 #4 METROHM 2 Sample 

 18 Vial 5 HPLC53pg100 #5 METROHM 2 Sample 

Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG100.S

Instrument 1 10/5/2010 9:25:03 AM IGG Page 1 of 1

EA# 0910-96 Page 201 of 202
This Is The Last Page

Of This Report.

EA# 0910-96 Page 202 of 202