# Analytical Testing Consultants Inc.

1630 Dale Earnhardt Blvd. Kannapolis, NC 28083



# Boral Bricks Salisbury Plant Inlet & Outlet Augusta Plants 4 & 5 Inlets & Outlets

Project # P-10124 PO # P-10124



# Analytical Report (0910-96)

EPA Method 26A
Hydrogen chloride, Hydrogen fluoride Chloride



# Enthalpy Analytical, Inc.

Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 2202 Ellis Road Durham, NC 27703 - 5518

### I certify that to the best of my knowledge a ll analytical data presented in this report:

 Have been checked for completeness

 Are accurate, error-free, and legible

 Have been conducted in accordance with approved prot ocol, and that all deviations and analytical problems are summarized in the appropriate narrative(s)

This analytical report was prepared in Portable Document Format (.PDF) and contains  pages.

# Summary of Results

### Compound Sample ID / Catch Weight (ug)

Salisbury Inlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 44,722 49,144 61,452 Hydrogen Chloride 2,911 3,890 5,514

Salisbury Outlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 28.7 ND 30.1 ND 27.9 ND Hydrogen Chloride 330 J 253 J 217 J

Augusta Plant 4 Inlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 11,071 35,672 41,007 Hydrogen Chloride 601 3,000 2,995

Augusta Plant 4 Outlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 1,522 1,808 2,325 Hydrogen Chloride 988 1,100 1,278

Augusta Plant 5 Inlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 19,206 49,828 57,084 Hydrogen Chloride 617 2,259 2,887

Augusta Plant 5 Outlet Acid Impingers Run 1 Run 2 Run 3 Hydrogen Fluoride 2,259 2,092 2,121 Hydrogen Chloride 329 J 283 J 312 J Company

Analyst Parameters # Samples Analytical Testing Consult. EO EPA Method 26A (H2SO4) 18 Runs, 2 Blanks Client # Job # PO # Report Date P-10124 0910-96 P-10124 10/6/2010

0910-96 res 10/6/2010

### Compound Sample ID / Catch Weight (ug) Company

Analyst Parameters # Samples Analytical Testing Consult. EO EPA Method 26A (H2SO4) 18 Runs, 2 Blanks Client # Job # PO # Report Date P-10124 0910-96 P-10124 10/6/2010



### Blanks Acid Blank DI H2O blank Hydrogen Fluoride 17.6 J 1.55 ND Hydrogen Chloride 10.1 ND 11.9 J

0910-96 res 10/6/2010

### Compound Sample ID / Catch Weight (ug)

Salisbury Inlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 382 202 J 17.8 ND

Salisbury Outlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 134,815 14.4 ND 6,408

Augusta Plant 4 Inlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 227 J 18.2 ND 17.6 ND

Augusta Plant 4 Outlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 16.9 ND 18.7 ND 15.1 ND

Augusta Plant 5 Inlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 16.7 ND 15.7 ND 17.4 ND

Augusta Plant 5 Outlet Alkaline Impingers Run 1 Run 2 Run 3 Chloride 13.8 ND 15.5 ND 16.1 ND

Blanks Base Blank DI H2O blank Chloride 34.2 J 11.5 J Company

Analyst Parameters # Samples Analytical Testing Consul EO EPA Method 26A (NaOH) 18 Runs, 1 Blank Client # Job # PO # Report Date P-10124 0910-96 P-10124 10/6/2010

0910-96 res 10/6/2010

# ResultsMDL 0.0100 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualSalisbury Run 1 In A 009-1001.D 009-1002.D HPLC53PG98.M 3.13 3.13 0.0 7.99 7.99 0.0 7.99 1.053 20 266 44,722Salisbury Run 2 In A 012-1301.D 012-1302.D HPLC53PG98.M 3.13 3.13 0.0 7.99 7.97 0.1 7.98 1.053 20 292 49,144Salisbury Run 3 In A 013-1401.D 013-1402.D HPLC53PG98.M 3.13 3.13 0.0 8.07 8.05 0.2 8.06 1.053 20 362 61,452Salisbury Run 1 Out A 014-1501.D 014-1502.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 10 273 28.7 NDSalisbury Run 2 Out A 015-1601.D 015-1602.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 10 286 30.1 NDSalisbury Run 3 Out A 016-1901.D 016-1902.D HPLC53PG98.M NA NA NA 0.01000 0.01000 0.0 0.01000 1.053 10 265 27.9 NDP4 Run 1 In A 026-3301.D 026-3302.D HPLC53PG98.M 3.12 3.12 0.0 3.84 3.86 0.3 3.85 1.053 10 273 11,071P4 Run 2 In A 029-3601.D 029-3602.D HPLC53PG98.M 3.14 3.14 0.0 11.7 11.7 0.1 11.7 1.053 10 289 35,672P4 Run 3 In A 030-3701.D 030-3702.D HPLC53PG98.M 3.14 3.14 0.0 11.0 10.9 0.1 10.9 1.053 10 356 41,007P4 Run 1 Out A 031-3801.D 031-3802.D HPLC53PG98.M 3.12 3.12 0.0 0.492 0.487 0.5 0.490 1.053 10 295 1,522P4 Run 2 Out A 032-3901.D 032-3902.D HPLC53PG98.M 3.12 3.12 0.0 0.608 0.606 0.1 0.607 1.053 10 283 1,808P4 Run 3 Out A 033-4001.D 033-4002.D HPLC53PG98.M 3.12 3.12 0.1 0.685 0.684 0.1 0.684 1.053 10 323 2,325Hydrogen Fluoride as FluorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/20100910-96 res10/6/2010MDL 0.0100 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Fluoride as FluorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010P5 Run 1 In A 040-4901.D 040-4902.D HPLC53PG98.M 3.13 3.13 0.0 6.19 6.24 0.4 6.21 1.053 10 294 19,206P5 Run 2 In A 009-1001.D 009-1002.D HPLC53PG100.M 3.14 3.14 0.0 8.73 8.68 0.3 8.70 1.053 20 272 49,828P5 Run 3 In A 010-1101.D 010-1102.D HPLC53PG100.M 3.14 3.17 1.0 11.0 11.1 0.5 11.0 1.053 20 246 57,084P5 Run 1 Out A 043-5201.D 043-5202.D HPLC53PG98.M 3.12 3.12 0.0 0.750 0.702 3.3 0.726 1.053 10 296 2,259P5 Run 2 Out A 044-5701.D 044-5702.D HPLC53PG98.M 3.13 3.13 0.0 0.822 0.839 1.0 0.830 1.053 10 239 2,092P5 Run 3 Out A 045-5801.D 045-5802.D HPLC53PG98.M 3.12 3.12 0.0 0.776 0.768 0.5 0.772 1.053 10 261 2,121Acid Blank 052-6701.D 052-6702.D HPLC53PG98.M 3.17 NA NA 0.0138 0.0100 15.9 0.0119 1.053 10 141 17.6 JDI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 1 147 1.55 ND0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 1 1.00 0.0105 ND0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 1 1.00 0.0105 ND0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 1 1.00 0.0105 ND0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.0100 0.0100 0.0 0.0100 1.053 1 1.00 0.0105 ND0910-96 res10/6/2010MDL 0.0100 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Fluoride as FluorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010MS Salisbury R1 In A 010-1101.D 010-1102.D HPLC53PG98.M 3.13 3.13 0.0 11.3 11.3 0.2 11.3 1.053 1 10.0 119Spike Amount (ug) 31.6Native Amount (ug) 84.1Spike Recovery (%) 111%MSD Salisbury R1 In A 011-1201.D 011-1202.D HPLC53PG98.M 3.13 3.13 0.0 10.7 10.7 0.2 10.7 1.053 1 10.0 113Spike Amount (ug) 31.6Native Amount (ug) 84.1Spike Recovery (%) 91.3%MS P4 R1 In A 027-3401.D 027-3402.D HPLC53PG98.M 3.13 3.13 0.0 6.94 6.95 0.0 6.94 1.053 1 10.0 73.1Spike Amount (ug) 31.6Native Amount (ug) 40.5Spike Recovery (%) 103%MSD P4 R1 In A 028-3501.D 028-3502.D HPLC53PG98.M 3.13 3.12 0.1 6.97 6.94 0.2 6.96 1.053 1 10.0 73.3Spike Amount (ug) 31.6Native Amount (ug) 40.5Spike Recovery (%) 104%HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 3.12 3.12 0.1 5.37 5.36 0.1 5.36 1.053 1 10.0 56.5Spike Amount (ug) 52.7Spike Recovery (%) 107%HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 3.12 3.12 0.0 5.34 5.35 0.1 5.35 1.053 1 10.0 56.3Spike Amount (ug) 52.7Spike Recovery (%) 107%0910-96 res10/6/2010MDL 0.0100 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Fluoride as FluorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 3.12 3.12 0.0 5.22 5.22 0.0 5.22 1.053 1 10.0 55.0Spike Amount (ug) 52.7Spike Recovery (%) 104%HPLC53pg100 #LCS 007-0801.D 007-0802.D HPLC53PG100.M 3.12 3.13 0.0 5.27 5.29 0.1 5.28 1.053 1 10.0 55.6Spike Amount (ug) 52.7Spike Recovery (%) 106%0910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualSalisbury Run 1 In A 009-1001.D 009-1002.D HPLC53PG98.M 4.26 4.26 0.0 0.533 0.532 0.0 0.533 1.028 20 266 2,911Salisbury Run 2 In A 012-1301.D 012-1302.D HPLC53PG98.M 4.26 4.26 0.0 0.650 0.644 0.5 0.647 1.028 20 292 3,890Salisbury Run 3 In A 013-1401.D 013-1402.D HPLC53PG98.M 4.26 4.26 0.0 0.742 0.740 0.1 0.741 1.028 20 362 5,514Salisbury Run 1 Out A 014-1501.D 014-1502.D HPLC53PG98.M 4.25 4.26 0.0 0.120 0.115 2.2 0.118 1.028 10 273 330 JSalisbury Run 2 Out A 015-1601.D 015-1602.D HPLC53PG98.M 4.25 4.25 0.0 0.0848 0.0869 1.2 0.0859 1.028 10 286 253 JSalisbury Run 3 Out A 016-1901.D 016-1902.D HPLC53PG98.M 4.25 4.25 0.0 0.0825 0.0764 3.8 0.0794 1.028 10 265 217 JP4 Run 1 In A 026-3301.D 026-3302.D HPLC53PG98.M 4.26 4.26 0.0 0.218 0.210 1.7 0.214 1.028 10 273 601P4 Run 2 In A 029-3601.D 029-3602.D HPLC53PG98.M 4.26 4.26 0.0 1.01 1.01 0.3 1.01 1.028 10 289 3,000P4 Run 3 In A 030-3701.D 030-3702.D HPLC53PG98.M 4.26 4.26 0.0 0.815 0.823 0.5 0.819 1.028 10 356 2,995P4 Run 1 Out A 031-3801.D 031-3802.D HPLC53PG98.M 4.26 4.26 0.0 0.325 0.327 0.3 0.326 1.028 10 295 988P4 Run 2 Out A 032-3901.D 032-3902.D HPLC53PG98.M 4.26 4.26 0.0 0.378 0.378 0.1 0.378 1.028 10 283 1,100P4 Run 3 Out A 033-4001.D 033-4002.D HPLC53PG98.M 4.26 4.26 0.0 0.386 0.385 0.2 0.385 1.028 10 323 1,278Hydrogen Chloride as ChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/20100910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Chloride as ChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010P5 Run 1 In A 040-4901.D 040-4902.D HPLC53PG98.M 4.26 4.26 0.0 0.206 0.203 0.6 0.205 1.028 10 294 617P5 Run 2 In A 041-5001.D 041-5002.D HPLC53PG98.M 4.27 4.27 0.0 0.806 0.812 0.4 0.809 1.028 10 272 2,259P5 Run 3 In A 042-5101.D 042-5102.D HPLC53PG98.M 4.27 4.27 0.0 1.15 1.14 0.3 1.14 1.028 10 246 2,887P5 Run 1 Out A 043-5201.D 043-5202.D HPLC53PG98.M 4.26 4.26 0.0 0.121 0.0953 12.0 0.108 1.028 10 296 329 JP5 Run 2 Out A 044-5701.D 044-5702.D HPLC53PG98.M 4.26 4.26 0.0 0.115 0.115 0.2 0.115 1.028 10 239 283 JP5 Run 3 Out A 045-5801.D 045-5802.D HPLC53PG98.M 4.26 4.26 0.0 0.114 0.118 2.0 0.116 1.028 10 261 312 JAcid Blank 052-6701.D 052-6702.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 10 141 10.1 NDDI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M 4.29 4.29 0.0 0.113 0.0436 44.3 0.0783 1.028 1 147 11.9 J0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 1 1.00 0.00714 ND0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 1 1.00 0.00714 ND0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 1 1.00 0.00714 ND0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.00695 0.00695 0.0 0.00695 1.028 1 1.00 0.00714 ND0910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Chloride as ChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010MS Salisbury R1 In A 010-1101.D 010-1102.D HPLC53PG98.M 4.25 4.25 0.0 3.65 3.65 0.0 3.65 1.028 1 10.0 37.5Spike Amount (ug) 30.8Native Amount (ug) 5.47Spike Recovery (%) 104%MSD Salisbury R1 In A 011-1201.D 011-1202.D HPLC53PG98.M 4.26 4.26 0.0 3.45 3.45 0.1 3.45 1.028 1 10.0 35.5Spike Amount (ug) 30.8Native Amount (ug) 5.47Spike Recovery (%) 97.3%MS P4 R1 In A 027-3401.D 027-3402.D HPLC53PG98.M 4.26 4.26 0.0 3.05 3.06 0.1 3.06 1.028 1 10.0 31.4Spike Amount (ug) 30.8Native Amount (ug) 2.20Spike Recovery (%) 94.7%MSD P4 R1 In A 028-3501.D 028-3502.D HPLC53PG98.M 4.26 4.26 0.0 3.07 3.08 0.0 3.07 1.028 1 10.0 31.6Spike Amount (ug) 30.8Native Amount (ug) 2.20Spike Recovery (%) 95.4%HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 4.26 4.26 0.1 5.00 5.01 0.1 5.01 1.028 1 10.0 51.5Spike Amount (ug) 51.4Spike Recovery (%) 100%HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 4.26 4.26 0.0 5.01 5.01 0.0 5.01 1.028 1 10.0 51.5Spike Amount (ug) 51.4Spike Recovery (%) 100%0910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AcidConversionFactorDFVol(mL)CatchWeight(ug)QualHydrogen Chloride as ChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsultantsEOEPA Method 26A (H2SO4)18 Runs, 2 BlanksClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 4.26 4.27 0.0 4.88 4.87 0.1 4.87 1.028 1 10.0 50.1Spike Amount (ug) 51.4Spike Recovery (%) 97.5%HPLC53pg100 #LCS 007-0801.D 007-0802.D HPLC53PG100.M 4.25 4.25 0.0 4.92 4.92 0.1 4.92 1.028 1 10.0 50.6Spike Amount (ug) 51.4Spike Recovery (%) 98.4%0910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AliquotFactorDFVol(mL)CatchWeight(ug)QualSalisbury Run 1 In B 017-2001.D 017-2002.D HPLC53PG98CL.M 4.23 4.23 0.0 0.224 0.219 1.1 0.222 1 10 172 382Salisbury Run 2 In B 018-2101.D 018-2102.D HPLC53PG98CL.M 4.23 4.23 0.0 0.0797 0.0760 2.3 0.0779 1 10 260 202 JSalisbury Run 3 In B 019-2201.D 019-2202.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 257 17.8 NDSalisbury Run 1 Out B 023-2601.D 023-2602.D HPLC53PG98CL.M 4.15 4.15 0.0 7.48 7.39 0.6 7.44 1 100 181 134,815Salisbury Run 2 Out B 021-2401.D 021-2402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 207 14.4 NDSalisbury Run 3 Out B 022-2501.D 022-2502.D HPLC53PG98CL.M 4.24 4.24 0.0 2.42 2.36 1.2 2.39 1 10 268 6,408P4 Run 1 In B 034-4301.D 034-4302.D HPLC53PG98CL.M 4.23 NA NA 0.171 0.00695 92.2 0.0889 1 10 255 227 JP4 Run 2 In B 035-4401.D 035-4402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 262 18.2 NDP4 Run 3 In B 036-4501.D 036-4502.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 254 17.6 NDP4 Run 1 Out B 037-4601.D 037-4602.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 244 16.9 NDP4 Run 2 Out B 038-4701.D 038-4702.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 269 18.7 NDP4 Run 3 Out B 039-4801.D 039-4802.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 217 15.1 NDChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsulEOEPA Method 26A (NaOH)18 Runs, 1 BlankClient #Job #PO #Report DateP-101240910-96P-1012410/6/20100910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AliquotFactorDFVol(mL)CatchWeight(ug)QualChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsulEOEPA Method 26A (NaOH)18 Runs, 1 BlankClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010P5 Run 1 In B 046-5901.D 046-5902.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 241 16.7 NDP5 Run 2 In B 047-6001.D 047-6002.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 226 15.7 NDP5 Run 3 In B 048-6101.D 048-6102.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 250 17.4 NDP5 Run 1 Out B 049-6201.D 049-6202.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 199 13.8 NDP5 Run 2 Out B 050-6301.D 050-6302.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 224 15.5 NDP5 Run 3 Out B 051-6401.D 051-6402.D HPLC53PG98CL.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 10 231 16.1 NDBase Blank 053-6801.D 053-6802.D HPLC53PG98CL.M 4.24 4.24 0.0 0.0235 0.0231 0.9 0.0233 1 10 147 34.2 JDI H2O blank 054-6901.D 054-6902.D HPLC53PG98.M 4.29 4.29 0.0 0.113 0.0436 44.3 0.0783 1 1 147 11.5 J0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 1 1.00 0.00695 ND0.01N H2SO4/NaOH RB 008-3201.D 008-3202.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 1 1.00 0.00695 ND0.01N H2SO4/NaOH RB 103-5601.D 103-5602.D HPLC53PG98.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 1 1.00 0.00695 ND0.01N H2SO4/NaOH RB 008-0901.D 008-0902.D HPLC53PG100.M NA NA NA 0.00695 0.00695 0.0 0.00695 1 1 1.00 0.00695 ND0910-96 res10/6/2010MDL 0.00695 (ug/mL)Lower Curve Limit 0.200 (ug/mL)LOQ 0.200 (ug/mL)Upper Curve Limit 15.0 (ug/mL)CompoundSampleIDLab ID# 1Lab ID# 2AnalysisMethodRetTime(min)RetTime(min)% DiffRetConc# 1(ug/mL)Conc# 2(ug/mL)% DiffConcAvgConc(ug/mL)AliquotFactorDFVol(mL)CatchWeight(ug)QualChlorideCompanyAnalystParameters# SamplesAnalytical Testing ConsulEOEPA Method 26A (NaOH)18 Runs, 1 BlankClient #Job #PO #Report DateP-101240910-96P-1012410/6/2010HPLC53pg98 #LCS 007-0801.D 007-0802.D HPLC53PG98.M 4.26 4.26 0.1 5.00 5.01 0.1 5.01 1 1 10.0 50.1Spike Amount (ug) 50.0Spike Recovery (%) 100%HPLC53pg98 #LCS 007-3101.D 007-3102.D HPLC53PG98.M 4.26 4.26 0.0 5.01 5.01 0.0 5.01 1 1 10.0 50.1Spike Amount (ug) 50.0Spike Recovery (%) 100%HPLC53pg98 #LCS 102-5501.D 102-5502.D HPLC53PG98.M 4.26 4.27 0.0 4.88 4.87 0.1 4.87 1 1 10.0 48.7Spike Amount (ug) 50.0Spike Recovery (%) 97.5%0910-96 res10/6/2010

# Narrative Summary

# Enthalpy Analytical Narrative Summary

Company 

### Analytical Testing Consultants Inc. Client # 

### P-10124

Analyst 

### EO Job # 

### 0910-96
Parameters 

### EPA Method 26A PO # 

### P-10124

# Samples 

### 18 Runs, 3 Blanks Report Date 

### October 6, 2010

Custody David Eckard received the samples on 9/24/10 after being relinquished by Analytical Testing Consultants Inc. The samples were received at 15.9  C and in good condition. Samples Plant 5 Inlet and Outlet Runs 2 and 3 were received in glass. Prior to, during, and after analysis, the samples were kept under lock with access only to authorized personnel by Enthalpy Analytical, Inc.

Analysis The samples were analyzed for hydrogen chloride (HCl), hydrogen fluoride (HF), and chloride using the analytical procedures in EPA Method 26A, Determination of Hydrogen Halide and Halogen Emissions from Stationary Sources Isokinetic Method (40 CFR Part 60, Appendix A).
With the exceptions noted above, all samples and standards were prepared, stored, and analyzed using high-density polyethylene containers.

The Metrohm 861, High Performance Liquid Chromatograph "Mr Burns" (S/N 1861004003180) was equipped with a Metrohm 861 Conductivity Detector and a Metrosep A Supp 5 - 110/4.0mm column (S/N # 7908297), for these analyses.

Calibration The calibration curves are included in the Calibration Curve Chromatograms section of this report and referenced in the Analysis Method column on the Detailed Results page.
For each calibration curve used, the first page of the curve contains all method specific parameters (i.e., curve type, origin, weight, etc.) used to quantify the samples. The calibration curve section also includes a table with the Retention Time (RetTime), Level (Lvl), Amount (corresponding units), Area, Response Factor (Amt/Area) and the analyte Name. The calibration table is used to identify (by retention time) and quantify each target compound.
Chromatographic Conditions The acquisition method Metrohm.M is included in the Calibration Curve Chromatograms section of this report.

# Enthalpy Analytical Narrative Summary (continued)

QC Notes Fluoride was not identified above the MDL in the analyses of the lab reagent blanks and client DI H2O blank. Fluoride was detected below the LOQ in the acid blank.

Chloride was not identified above the MDL in the analyses of the lab reagent blanks and client acid blank. Chloride was detected below the LOQ in the client base blank and DI H2O blank.

Matrix spike and matrix spike duplicates (MS and MSD) were prepared using aliquots of the samples Salibury R1-In A and P4 R1 In A . The recovery values were 111%, 91.3%, 103%, and 105% for HF. The recovery values were 104%, 97.3%, 94.7%, and 95.4% for HCl.

Laboratory Control Samples (LCS) were prepared and analyzed with the samples. The recovery values ranged from 104% to 107 for HF and 97.5% to 100% for HCL.

The samples were analyzed within the four-week holding time specified by the method.

Reporting Notes The results presented in this report are representative of the samples as provided to the laboratory.

The H 2 

### SO 4 

### matrix samples were analyzed for Cl- and F- but are reported as HCl and HF. The results were converted using an acid conversion factor of 1.028 for HCl and 1.053 for HF.

Enthalpy Analytical, Inc. is accredited to perform EPA Method 26A for compliance purposes by the National Environmental Laboratory Accreditation Conference (NELAC) through the Louisiana Environmental Laboratory Accreditation Program (LELAP), certificate number 04010.

# General Reporting Notes

The following are general reporting notes that are a pplicable to all Enthalpy Analytical, Inc. data reports, unless specifically noted otherwise.

 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot determine the presence of the analyte of interest reliably.

 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot quantitate the analyte of interest within the criteria of the method.

 The acronym ND following a value indicates a non-detect or analytical result below the MDL.

 The letter J following a value indicates an analytical r esult between the MDL and the LOQ. A J flag indicates that the laboratory can positively identify th e analyte of interest as present, but the value should be considered an estimate.

 The letter E following a value indicates an analytical r esult exceeding 100% of the highest calibration point. The associated value should be considered as an estimate.

 The acronym DF represents Dilution Factor. This number represents dilution of the sample during the preparation and/or analysis process. The analyti cal result taken from a laboratory instrument is multiplied by the DF to determine the final undiluted sample results.

 The addition of MS to the Sample ID represents a Matrix Sp ike. An aliquot of an actual sample is spiked with a known amount of analyte so that a per cent recovery value can be determined. This shows what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the analyte(s).

 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality by showing the consistency of results gained by performing the same steps multiple times.

 The addition of LD to the Sample ID represents a Laborat ory Duplicate. The analyst prepares an additional aliquot of sample for testing and the resu lts of the duplicate analysis are compared to the initial result. The result should have a difference value of within 10% of the initial result (if the results of the original analysis are greater than the LOQ).

 The addition of AD to the Sample ID represents an Alte rnate Dilution. The analyst prepares an additional aliquot at a different dilution factor (usu ally double the initial factor). This analysis helps confirm that no additional compound is present and coel uting or sharing absorbance with the analyte of interest, as they would have a different res ponse/absorbance than the analyte of interest.

 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample matrix, prepared and analyzed by the laborator y using the same reagents, spiking standards and procedures used for the client samples. The LCS is used to assess the control of the laboratory’s analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. The extras (randomly chosen) are labeled with the asso ciated project number and kept in-house at the appropriate temperature conditions. When the project samples are received for analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media, separate from the samples which were used on the project and which may have been affected by source matrix, sample collection and/or sample transport.

# General Reporting Notes

(continued)

 Significant Figures : Where the reported value is much greater than unity (1.00) in the units expressed, the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. Ther e are five significant digits displayed, but no confidence should be placed on more than two significant digits.

 Manual Integration : The data systems used for processing w ill flag manually integrated peaks with an “M”. There are several reasons a peak may be manually integrated. These reasons will be identified by the following two letter designations. The peak was not integrated by the software “NI” , the peak

was integrated incorrectly by the software “II” or the wrong peak was integrated by the software “WP” . These codes will accompany the analyst’s ma nual integration stamp placed next to the compound name.

# Sample Custody

# Sample Chromatograms===================================================================== Acq. Operator : EO Seq. Line : 10 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 9:27:01 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1001.D)2.2533.125 - Fluoride3.5134.257 - Chloride5.431

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BV 467.71011 1.70755e-2 7.98639 Fluoride 4.257 BB 17.94451 2.96828e-2 5.32643e-1 Chloride

Totals : 8.51904

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1001.D Sample Name: Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:25 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 10 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 9:39:20 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1002.D)2.2543.125 - Fluoride3.5144.257 - Chloride5.433

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BV 467.69397 1.70755e-2 7.98612 Fluoride 4.257 BB 17.93629 2.96844e-2 5.32427e-1 Chloride

Totals : 8.51854

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\009-1002.D Sample Name: Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:33 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 13 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 10:40:59 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1301.D)2.2533.126 - Fluoride3.5124.257 - Chloride5.425

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.126 BV 467.74438 1.70755e-2 7.98698 Fluoride 4.257 BB 22.41548 2.90028e-2 6.50111e-1 Chloride

Totals : 8.63709

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1301.D Sample Name: Salisbury R2 In A *20 0910-96

Instrument 1 10/4/2010 9:31:25 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 13 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 10:53:19 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1302.D)2.2553.126 - Fluoride3.5124.257 - Chloride5.426

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.126 BV 466.99976 1.70755e-2 7.97425 Fluoride 4.257 BB 22.18078 2.90316e-2 6.43944e-1 Chloride

Totals : 8.61819

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\012-1302.D Sample Name: Salisbury R2 In A *20 0910-96

Instrument 1 10/4/2010 9:31:33 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 14 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 11:05:39 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1401.D)2.2563.126 - Fluoride3.5084.257 - Chloride5.405

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.126 BV 472.81418 1.70757e-2 8.07365 Fluoride 4.257 BB 25.90080 2.86355e-2 7.41682e-1 Chloride

Totals : 8.81534

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1401.D Sample Name: Salisbury R3 In A *20 0910-96

Instrument 1 10/4/2010 9:31:41 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 14 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 11:17:58 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1402.D)2.2533.125 - Fluoride3.5074.257 - Chloride5.405

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BV 471.29227 1.70757e-2 8.04764 Fluoride 4.257 BB 25.83895 2.86411e-2 7.40057e-1 Chloride

Totals : 8.78769

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\013-1402.D Sample Name: Salisbury R3 In A *20 0910-96

Instrument 1 10/4/2010 9:31:49 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 15 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 11:30:18 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1501.D)2.2553.3423.5064.254 - Chloride4.6355.6557.160

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.254 BV 3.17554 3.78526e-2 1.20202e-1 Chloride

Totals : 1.20202e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1501.D Sample Name: Salisbury R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:31:57 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 15 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 11:42:38 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1502.D)2.2563.3433.5084.255 - Chloride4.6325.4927.160

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.255 BV 3.03742 3.78526e-2 1.14974e-1 Chloride

Totals : 1.14974e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\014-1502.D Sample Name: Salisbury R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:05 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 16 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 11:54:58 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1601.D)2.2533.3363.5044.250 - Chloride4.6265.4917.158

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.250 BV 2.24146 3.78526e-2 8.48451e-2 Chloride

Totals : 8.48451e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1601.D Sample Name: Salisbury R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:13 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 16 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 12:07:18 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1602.D)2.2563.3393.5064.250 - Chloride4.6295.4917.158

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.250 BV 2.29672 3.78526e-2 8.69365e-2 Chloride

Totals : 8.69365e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\015-1602.D Sample Name: Salisbury R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:22 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 19 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:08:57 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1901.D)2.2543.3403.5074.250 - Chloride4.6525.6717.177

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.250 BV 2.17866 3.78526e-2 8.24680e-2 Chloride

Totals : 8.24680e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1901.D Sample Name: Salisbury R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:30 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 19 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:21:17 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1902.D)2.2563.3423.5074.250 - Chloride4.6445.4847.174

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.250 BV 2.01728 3.78526e-2 7.63593e-2 Chloride

Totals : 7.63593e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\016-1902.D Sample Name: Salisbury R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:32:38 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 20 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:33:04 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2001.D)2.2453.4674.233 - Chloride4.9096.9979.847

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.233 VB 6.20973 3.61257e-2 2.24331e-1 Chloride

Totals : 2.24331e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2001.D Sample Name: Salisbury R1 In B *10 0910-96

Instrument 1 10/4/2010 9:33:09 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 20 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:50:22 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2002.D)2.2443.4604.233 - Chloride4.9086.9969.847

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.233 VB 6.02410 3.64293e-2 2.19454e-1 Chloride

Totals : 2.19454e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\017-2002.D Sample Name: Salisbury R1 In B *10 0910-96

Instrument 1 10/4/2010 9:33:19 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 21 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:07:41 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2101.D)2.2463.0713.3224.225 - Chloride4.9015.4206.9859.814

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.225 BV 2.10500 3.78526e-2 7.96796e-2 Chloride

Totals : 7.96796e-2

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2101.D Sample Name: Salisbury R2 In B *10 0910-96

Instrument 1 10/4/2010 9:33:27 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 21 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:24:59 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2102.D)2.2473.0723.3264.225 - Chloride4.9005.4186.9829.813

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.225 BV 2.00891 3.78526e-2 7.60425e-2 Chloride

Totals : 7.60425e-2

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\018-2102.D Sample Name: Salisbury R2 In B *10 0910-96

Instrument 1 10/4/2010 9:33:37 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 22 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:42:16 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2201.D)2.2473.0763.3444.9066.9869.827

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2201.D Sample Name: Salisbury R3 In B *10 0910-96

Instrument 1 10/4/2010 9:33:45 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 22 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:59:34 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2202.D)2.2493.0773.3464.9076.9859.826

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\019-2202.D Sample Name: Salisbury R3 In B *10 0910-96

Instrument 1 10/4/2010 9:33:53 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 26 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:00:41 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2601.D)2.2174.152 - Chloride4.7775.446

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.152 BV 282.51471 2.64899e-2 7.48380 Chloride

Totals : 7.48380

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2601.D Sample Name: Salisbury R1 Out B *100 0910-96

Instrument 1 10/4/2010 9:35:28 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 26 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:17:59 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2602.D)2.2144.154 - Chloride4.7805.444

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.154 BV 278.87683 2.64928e-2 7.38822 Chloride

Totals : 7.38822

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\023-2602.D Sample Name: Salisbury R1 Out B *100 0910-96

Instrument 1 10/4/2010 9:35:37 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 24 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 3:51:29 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2401.D)2.2493.3414.9117.0039.833

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2401.D Sample Name: Salisbury R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:34:32 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 24 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:08:47 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2402.D)2.2493.3444.9126.9999.840

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\021-2402.D Sample Name: Salisbury R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:34:54 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 25 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:26:05 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2501.D)2.2483.3694.236 - Chloride4.9136.9979.847

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.236 BB 89.76620 2.69549e-2 2.41964 Chloride

Totals : 2.41964

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2501.D Sample Name: Salisbury R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:35:06 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 25 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:43:22 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2502.D)2.2523.3724.238 - Chloride4.9166.9989.846

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.238 BB 87.67069 2.69712e-2 2.36459 Chloride

Totals : 2.36459

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\022-2502.D Sample Name: Salisbury R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:35:19 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 33 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:23:39 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3301.D)2.2543.121 - Fluoride4.261 - Chloride5.4767.148

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:41 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 BB 225.06882 1.70529e-2 3.83808 Fluoride 4.261 BV 5.95215 3.65521e-2 2.17564e-1 Chloride

Totals : 4.05564

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3301.D Sample Name: P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:36:45 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 33 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:35:58 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D)2.2673.121 - Fluoride4.261 - Chloride5.4757.147

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 BB 226.27061 1.70532e-2 3.85863 Fluoride 4.261 BV 5.67176 3.70602e-2 2.10197e-1 Chloride

Totals : 4.06882

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\026-3302.D Sample Name: P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:36:58 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 36 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:37:38 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3601.D)2.2563.137 - Fluoride4.263 - Chloride5.4837.154

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.137 BB 685.05603 1.70822e-2 11.70224 Fluoride 4.263 BB 36.18887 2.79640e-2 1.01198 Chloride

Totals : 12.71423

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3601.D Sample Name: P4 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:37:37 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 36 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:49:58 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3602.D)2.2563.137 - Fluoride4.261 - Chloride5.4817.148

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.137 BB 686.89960 1.70822e-2 11.73376 Fluoride 4.261 BB 35.98354 2.79736e-2 1.00659 Chloride

Totals : 12.74035

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\029-3602.D Sample Name: P4 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:37:45 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 37 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:02:17 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3701.D)2.2523.135 - Fluoride4.261 - Chloride5.461

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.135 BB 641.72162 1.70812e-2 10.96138 Fluoride 4.261 BB 28.69785 2.84053e-2 8.15170e-1 Chloride

Totals : 11.77655

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3701.D Sample Name: P4 R3 In A *10 0910-96

Instrument 1 10/4/2010 9:37:54 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 37 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:14:37 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3702.D)2.2553.135 - Fluoride4.261 - Chloride5.461

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.135 BB 640.17627 1.70812e-2 10.93496 Fluoride 4.261 BB 28.99791 2.83832e-2 8.23054e-1 Chloride

Totals : 11.75801

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\030-3702.D Sample Name: P4 R3 In A *10 0910-96

Instrument 1 10/4/2010 9:38:02 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 38 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:26:57 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3801.D)2.2543.118 - Fluoride4.259 - Chloride5.466

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.118 BB 29.37646 1.67627e-2 4.92430e-1 Fluoride 4.259 BB 10.03031 3.23729e-2 3.24710e-1 Chloride

Totals : 8.17140e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3801.D Sample Name: P4 R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:10 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 38 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:39:16 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3802.D)2.2523.117 - Fluoride4.258 - Chloride5.465

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.117 BB 29.06601 1.67592e-2 4.87122e-1 Fluoride 4.258 BB 10.10172 3.23298e-2 3.26587e-1 Chloride

Totals : 8.13709e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\031-3802.D Sample Name: P4 R1 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:18 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 39 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:51:37 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3901.D)2.2553.119 - Fluoride4.260 - Chloride5.480

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.119 BB 36.11133 1.68250e-2 6.07572e-1 Fluoride 4.260 BB 12.06006 3.13464e-2 3.78039e-1 Chloride

Totals : 9.85611e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3901.D Sample Name: P4 R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:26 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 39 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:03:56 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3902.D)2.2563.120 - Fluoride4.260 - Chloride5.479

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.120 BB 36.00581 1.68242e-2 6.05768e-1 Fluoride 4.260 BB 12.07534 3.13399e-2 3.78440e-1 Chloride

Totals : 9.84209e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\032-3902.D Sample Name: P4 R2 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:34 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 40 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:16:16 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4001.D)2.2533.117 - Fluoride4.259 - Chloride5.460

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.117 BB 40.65833 1.68553e-2 6.85310e-1 Fluoride 4.259 BB 12.36708 3.12204e-2 3.86105e-1 Chloride

Totals : 1.07142

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4001.D Sample Name: P4 R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:42 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 40 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:28:36 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4002.D)2.2553.119 - Fluoride4.261 - Chloride5.462

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.119 BB 40.55775 1.68547e-2 6.83590e-1 Fluoride 4.261 BB 12.31650 3.12407e-2 3.84776e-1 Chloride

Totals : 1.06837

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\033-4002.D Sample Name: P4 R3 Out A *10 0910-96

Instrument 1 10/4/2010 9:38:52 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 43 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 12:29:43 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4301.D)2.2473.3124.234 - Chloride4.8995.4486.1666.9758.3749.814

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.234 BV 4.51100 3.78526e-2 1.70753e-1 Chloride

Totals : 1.70753e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4301.D Sample Name: P4 R1 In B *10 0910-96

Instrument 1 10/4/2010 9:39:49 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 43 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 12:47:01 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4302.D)2.2503.3154.9015.4499.807

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\034-4302.D Sample Name: P4 R1 In B *10 0910-96

Instrument 1 10/4/2010 9:39:57 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 44 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:04:23 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4401.D)2.2503.0803.4944.9149.859

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4401.D Sample Name: P4 R2 In B *10 0910-96

Instrument 1 10/4/2010 9:40:05 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 44 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:21:41 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4402.D)2.2493.0803.4944.9149.861

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\035-4402.D Sample Name: P4 R2 In B *10 0910-96

Instrument 1 10/4/2010 9:40:14 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 45 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:38:59 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D)2.2523.0813.3073.4834.9149.854

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4501.D Sample Name: P4 R3 In B *10 0910-96

Instrument 1 10/4/2010 9:40:23 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 45 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 1:56:17 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4502.D)2.2533.0833.3083.4844.9159.846

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\036-4502.D Sample Name: P4 R3 In B *10 0910-96

Instrument 1 10/4/2010 9:40:32 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 46 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:13:36 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4601.D)2.2444.8965.4287.0049.807

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4601.D Sample Name: P4 R1 Out B *10 0910-96

Instrument 1 10/4/2010 9:40:41 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 46 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:30:53 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4602.D)2.2464.8965.4267.0029.807

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\037-4602.D Sample Name: P4 R1 Out B *10 0910-96

Instrument 1 10/4/2010 9:56:49 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 47 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 2:48:12 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4701.D)2.2493.4844.9035.4339.821

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4701.D Sample Name: P4 R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:00 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 47 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 3:05:30 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4702.D)2.2463.4834.9035.4319.819

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\038-4702.D Sample Name: P4 R2 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:16 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 48 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 3:22:48 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4801.D)2.2483.4884.9117.0229.853

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4801.D Sample Name: P4 R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:26 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 48 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 3:40:05 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4802.D)2.2493.4894.9127.0249.853

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\039-4802.D Sample Name: P4 R3 Out B *10 0910-96

Instrument 1 10/4/2010 9:57:37 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 49 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 3:57:55 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4901.D)2.2563.126 - Fluoride4.262 - Chloride5.4887.130

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:17 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.126 BB 362.59586 1.70694e-2 6.18931 Fluoride 4.262 BB 5.50164 3.73938e-2 2.05727e-1 Chloride

Totals : 6.39504

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4901.D Sample Name: P5 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:58:22 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 49 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:10:15 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4902.D)

A

r ea

: 5.

4 1 33

32.3123.127 - Fluoride4.262 - Chloride5.4817.127

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.127 VB 365.51782 1.70697e-2 6.23926 Fluoride 4.262 MM 5.41333 3.75752e-2 2.03407e-1 Chloride

Totals : 6.44267

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\040-4902.D Sample Name: P5 R1 In A *10 0910-96

Instrument 1 10/4/2010 10:44:22 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 50 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:22:35 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5001.D)2.2653.151 - Fluoride3.5114.265 - Chloride5.4837.056

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.151 BV 937.34271 1.70860e-2 16.01546 Fluoride 4.265 VB 28.33126 2.84328e-2 8.05538e-1 Chloride

Totals : 16.82100

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5001.D Sample Name: P5 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:58:45 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 50 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:34:54 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5002.D)2.2583.150 - Fluoride3.5104.265 - Chloride5.4817.059

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.150 VV 935.54138 1.70860e-2 15.98466 Fluoride 4.265 VB 28.56014 2.84155e-2 8.11552e-1 Chloride

Totals : 16.79621

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\041-5002.D Sample Name: P5 R2 In A *10 0910-96

Instrument 1 10/4/2010 9:58:54 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 51 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:47:14 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5101.D)

A

r ea

: 11

5 5 .2

6

A r ea

: 41 .

2 57

22.2603.158 - Fluoride4.265 - Chloride5.4765.7107.178

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.158 MM 1155.25562 1.70880e-2 19.74100 Fluoride 4.265 MM 41.25723 2.77563e-2 1.14515 Chloride

Totals : 20.88615

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5101.D Sample Name: P5 R3 In A *10 0910-96

Instrument 1 10/4/2010 10:46:25 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 51 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 4:59:35 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5102.D)

A

r ea

: 40

. 9 82

82.2614.265 - Chloride5.4745.7107.175

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.265 MM 40.98282 2.77662e-2 1.13794 Chloride

Totals : 1.13794

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\042-5102.D Sample Name: P5 R3 In A *10 0910-96

Instrument 1 10/4/2010 10:48:06 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 10 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 5:39:47 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1001.D)2.2643.138 - Fluoride3.5014.252 - Chloride5.3966.903

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.138 BV 508.88586 1.71526e-2 8.72872 Fluoride 4.252 BB 14.43764 3.07776e-2 4.44356e-1 Chloride

Totals : 9.17308

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1001.D Sample Name: P5 R2 In A *20 0910-96

Instrument 1 10/5/2010 9:22:14 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 10 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 5:52:07 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1002.D)2.2613.137 - Fluoride3.5034.251 - Chloride5.3936.899

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.137 BV 506.10544 1.71527e-2 8.68108 Fluoride 4.251 BB 15.14480 3.05917e-2 4.63306e-1 Chloride

Totals : 9.14439

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\009-1002.D Sample Name: P5 R2 In A *20 0910-96

Instrument 1 10/5/2010 9:22:22 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 11 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 6:04:27 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1101.D)2.2623.142 - Fluoride4.251 - Chloride5.3986.977

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.142 BB 639.42731 1.71486e-2 10.96531 Fluoride 4.251 BB 23.24886 2.92691e-2 6.80473e-1 Chloride

Totals : 11.64579

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1101.D Sample Name: P5 R3 In A *20 0910-96

Instrument 1 10/5/2010 9:22:29 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 11 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 6:16:46 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1102.D)2.2653.174 - Fluoride4.287 - Chloride5.4377.019

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.174 BB 645.62323 1.71485e-2 11.07147 Fluoride 4.287 BB 23.89014 2.92027e-2 6.97657e-1 Chloride

Totals : 11.76913

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\010-1102.D Sample Name: P5 R3 In A *20 0910-96

Instrument 1 10/5/2010 9:22:41 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 52 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:11:54 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5201.D)2.2563.121 - Fluoride3.3154.260 - Chloride4.5885.4777.099

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 BV 44.45597 1.68759e-2 7.50236e-1 Fluoride 4.260 BV 3.20624 3.78526e-2 1.21364e-1 Chloride

Totals : 8.71600e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5201.D Sample Name: P5 R1 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:05 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 52 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:24:14 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5202.D)2.2583.122 - Fluoride3.3234.258 - Chloride4.9395.4797.100

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.122 BV 41.62362 1.68609e-2 7.01813e-1 Fluoride 4.258 BV 2.51682 3.78526e-2 9.52680e-2 Chloride

Totals : 7.97081e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\043-5202.D Sample Name: P5 R1 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:14 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 57 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:15:12 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5701.D)2.2593.125 - Fluoride3.3214.262 - Chloride4.9475.4957.181

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BV 48.65992 1.68950e-2 8.22109e-1 Fluoride 4.262 BV 3.04968 3.78526e-2 1.15438e-1 Chloride

Totals : 9.37547e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5701.D Sample Name: P5 R2 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:25 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 57 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:27:32 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5702.D)2.2603.125 - Fluoride3.3204.262 - Chloride4.6475.4877.179

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BV 49.63752 1.68990e-2 8.38823e-1 Fluoride 4.262 BV 3.03725 3.78526e-2 1.14967e-1 Chloride

Totals : 9.53790e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\044-5702.D Sample Name: P5 R2 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:35 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 58 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:39:51 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5801.D)2.2563.123 - Fluoride3.3164.260 - Chloride4.9405.4827.149

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BV 45.96114 1.68832e-2 7.75969e-1 Fluoride 4.260 BV 3.00710 3.78526e-2 1.13826e-1 Chloride

Totals : 8.89795e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5801.D Sample Name: P5 R3 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:48 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 58 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:52:11 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:58:17 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5802.D)2.2593.123 - Fluoride3.3224.260 - Chloride4.9415.4837.148

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:58:25 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BV 45.52016 1.68811e-2 7.68430e-1 Fluoride 4.260 BV 3.13018 3.78526e-2 1.18485e-1 Chloride

Totals : 8.86915e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\045-5802.D Sample Name: P5 R3 Out A *10 0910-96

Instrument 1 10/4/2010 10:00:57 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 59 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:03:59 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5901.D)2.2513.0843.4864.9177.0179.866

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5901.D Sample Name: P5 R1 In B *10 0910-96

Instrument 1 10/4/2010 10:01:40 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 59 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:21:17 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5902.D)2.2503.0853.4834.9187.0209.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\046-5902.D Sample Name: P5 R1 In B *10 0910-96

Instrument 1 10/4/2010 10:01:51 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 60 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:38:36 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6001.D)2.2533.0893.4834.9227.0259.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6001.D Sample Name: P5 R2 In B *10 0910-96

Instrument 1 10/4/2010 10:02:01 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 60 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:55:53 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6002.D)2.2543.0923.4834.9237.0249.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\047-6002.D Sample Name: P5 R2 In B *10 0910-96

Instrument 1 10/4/2010 10:02:10 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 61 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:13:11 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6101.D)2.2513.0853.4744.9187.0169.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6101.D Sample Name: P5 R3 In B *10 0910-96

Instrument 1 10/4/2010 10:02:21 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 61 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:30:29 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6102.D)2.2553.0873.4764.9217.0179.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\048-6102.D Sample Name: P5 R3 In B *10 0910-96

Instrument 1 10/4/2010 10:02:32 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 62 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:47:47 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6201.D)2.2473.4724.9007.0139.820

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6201.D Sample Name: P5 R1 out B *10 0910-96

Instrument 1 10/4/2010 10:02:42 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 62 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:05:05 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6202.D)2.2443.4714.8987.0119.820

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\049-6202.D Sample Name: P5 R1 out B *10 0910-96

Instrument 1 10/4/2010 10:02:51 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 63 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:22:23 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6301.D)2.2593.5024.9367.0379.913

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6301.D Sample Name: P5 R2 Out B *10 0910-96

Instrument 1 10/4/2010 10:03:06 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 63 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:39:41 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6302.D)2.2593.5034.9487.0499.927

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\050-6302.D Sample Name: P5 R2 Out B *10 0910-96

Instrument 1 10/4/2010 10:03:15 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 64 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 10:56:59 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6401.D)2.2523.3434.9227.0339.881

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6401.D Sample Name: P5 R3 out B *10 0910-96

Instrument 1 10/4/2010 10:03:26 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 64 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:14:17 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6402.D)2.2543.3444.9237.0319.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\051-6402.D Sample Name: P5 R3 out B *10 0910-96

Instrument 1 10/4/2010 10:03:35 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 67 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 12:21:26 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6701.D)2.2583.168 - Fluoride4.7085.4838.558

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.168 BB 8.45559e-1 1.62975e-2 1.37805e-2 Fluoride 4.156 - - - Chloride

Totals : 1.37805e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6701.D Sample Name: Acid Blank *10 0910-96

Instrument 1 10/4/2010 10:03:59 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 67 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 12:33:46 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6702.D)2.2614.7055.4795.751

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\052-6702.D Sample Name: Acid Blank *10 0910-96

Instrument 1 10/4/2010 10:04:30 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 68 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 12:45:35 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6801.D)2.2723.4954.237 - Chloride5.5999.700

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.237 BB 6.20201e-1 3.78526e-2 2.34762e-2 Chloride

Totals : 2.34762e-2

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6801.D Sample Name: Base Blank *10 0910-96

Instrument 1 10/4/2010 10:04:49 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 68 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 1:02:52 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98CL.M Last changed : 10/4/2010 9:33:01 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6802.D)2.2683.4964.238 - Chloride5.5969.701

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:32:52 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
4.238 BB 6.09262e-1 3.78526e-2 2.30621e-2 Chloride

Totals : 2.30621e-2

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\053-6802.D Sample Name: Base Blank *10 0910-96

Instrument 1 10/4/2010 10:04:58 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 69 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 1:20:42 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6901.D)3.5394.286 - Chloride9.799

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.286 VB 2.98664 3.78526e-2 1.13052e-1 Chloride

Totals : 1.13052e-1

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6901.D Sample Name: DI H2O blank 0910-96

Instrument 1 10/4/2010 10:05:32 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 69 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 1:33:02 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6902.D)2.1852.4723.5414.288 - Chloride9.810

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.288 VB 1.15224 3.78526e-2 4.36153e-2 Chloride

Totals : 4.36153e-2

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\054-6902.D Sample Name: DI H2O blank 0910-96

Instrument 1 10/4/2010 10:05:41 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 9 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 9:02:21 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0901.D)2.2695.4999.879

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0901.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:28 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 9 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 9:14:41 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0902.D)2.2695.4989.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-0902.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:37 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 32 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:58:59 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3201.D)2.2715.4999.893

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3201.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:29:54 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 32 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:11:19 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3202.D)2.2695.4979.887

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\008-3202.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 9:30:03 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 56 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 6:50:32 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5601.D)2.2755.5019.907

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5601.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 10:07:32 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 56 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:02:52 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5602.D)2.2735.4989.894

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 - - - Fluoride 4.156 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

===================================================================== Area Percent Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\103-5602.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/4/2010 10:07:41 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 9 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 5:15:07 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0901.D)2.2755.4439.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.149 - - - Fluoride 4.153 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0901.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/5/2010 9:21:57 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 9 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 5:27:28 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0902.D)2.2775.4459.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.149 - - - Fluoride 4.153 - - - Chloride

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

===================================================================== Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\008-0902.D Sample Name: 0.01N H2SO4/NaOH RB

Instrument 1 10/5/2010 9:22:05 AM IGG Page 1 of 2===================================================================== Acq. Operator : EO Seq. Line : 11 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 9:51:40 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1101.D)2.2553.132 - Fluoride3.5124.254 - Chloride5.4445.9886.2537.0058.480

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.132 BV 663.60602 1.70817e-2 11.33552 Fluoride 4.254 VB 136.56146 2.67214e-2 3.64911 Chloride

Totals : 14.98464

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1101.D Sample Name: MS Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:40 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 11 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 10:04:00 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1102.D)2.2523.131 - Fluoride3.5104.253 - Chloride5.4435.9886.2537.0058.479

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.131 BV 661.14001 1.70817e-2 11.29336 Fluoride 4.253 VB 136.65158 2.67211e-2 3.65148 Chloride

Totals : 14.94484

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\010-1102.D Sample Name: MS Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:30:49 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 12 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 10:16:20 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1201.D)2.2553.131 - Fluoride3.5114.255 - Chloride5.4355.9936.2507.0038.478

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.131 BV 626.82330 1.70808e-2 10.70667 Fluoride 4.255 VB 129.13361 2.67472e-2 3.45396 Chloride

Totals : 14.16063

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1201.D Sample Name: MSD Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:31:01 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 12 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 10:28:39 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1202.D)2.2563.132 - Fluoride3.5134.256 - Chloride5.4365.9946.2517.0048.480

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:29:44 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.132 BV 629.07855 1.70809e-2 10.74523 Fluoride 4.256 VB 128.93863 2.67479e-2 3.44883 Chloride

Totals : 14.19406

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\011-1202.D Sample Name: MSD Salisbury R1 In A *20 0910-96

Instrument 1 10/4/2010 9:31:16 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 34 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 8:48:18 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3401.D)2.2653.125 - Fluoride4.259 - Chloride5.4745.9856.3137.0818.490

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 406.57947 1.70724e-2 6.94127 Fluoride 4.259 BB 113.87910 2.68106e-2 3.05317 Chloride

Totals : 9.99444

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3401.D Sample Name: MS P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:06 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 34 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:00:38 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3402.D)2.2553.125 - Fluoride4.260 - Chloride5.4755.9846.3147.0828.489

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 406.89011 1.70724e-2 6.94659 Fluoride 4.260 BB 114.10727 2.68095e-2 3.05916 Chloride

Totals : 10.00575

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\027-3402.D Sample Name: MS P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:14 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 35 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:12:58 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3501.D)2.2563.126 - Fluoride4.260 - Chloride5.4745.9816.3117.0788.488

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.126 BB 408.43451 1.70725e-2 6.97299 Fluoride 4.260 BB 114.63012 2.68071e-2 3.07290 Chloride

Totals : 10.04589

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3501.D Sample Name: MSD P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:22 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 35 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 9:25:18 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:36:41 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3502.D)2.2533.124 - Fluoride4.259 - Chloride5.4725.9806.3107.0768.488

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.124 BB 406.71420 1.70724e-2 6.94358 Fluoride 4.259 BB 114.74656 2.68066e-2 3.07596 Chloride

Totals : 10.01954

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\028-3502.D Sample Name: MSD P4 R1 In A *10 0910-96

Instrument 1 10/4/2010 9:37:30 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 8 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 8:37:42 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0801.D)2.2703.118 - Fluoride4.258 - Chloride5.4986.1066.9118.4389.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.118 BB 314.60535 1.70653e-2 5.36884 Fluoride 4.258 BB 188.15720 2.65985e-2 5.00471 Chloride

Totals : 10.37355

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0801.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:28:54 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 8 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 8:50:01 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0802.D)2.2673.115 - Fluoride4.255 - Chloride5.4946.1016.9068.4359.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.115 BB 313.83789 1.70652e-2 5.35572 Fluoride 4.255 BB 188.36598 2.65982e-2 5.01019 Chloride

Totals : 10.36591

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-0802.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:03 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 31 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:34:20 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3101.D)2.2683.116 - Fluoride4.256 - Chloride5.4936.0996.9078.4329.887

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.116 BB 313.15643 1.70652e-2 5.34407 Fluoride 4.256 BB 188.40083 2.65981e-2 5.01111 Chloride

Totals : 10.35518

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3101.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:11 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 31 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 7:46:39 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3102.D)2.2713.117 - Fluoride4.257 - Chloride5.4976.1036.9108.4339.879

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.117 BB 313.53778 1.70652e-2 5.35059 Fluoride 4.257 BB 188.47112 2.65980e-2 5.01295 Chloride

Totals : 10.36354

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\007-3102.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 9:29:20 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 55 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 6:25:53 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5501.D)2.2723.121 - Fluoride4.263 - Chloride5.4986.1136.9208.4409.894

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 BB 305.91211 1.70644e-2 5.22022 Fluoride 4.263 BB 183.26718 2.66072e-2 4.87623 Chloride

Totals : 10.09645

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5501.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 10:07:13 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 55 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 6:38:13 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5502.D)2.2753.122 - Fluoride4.265 - Chloride5.5016.1186.9258.4429.900

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.122 BB 305.85730 1.70644e-2 5.21928 Fluoride 4.265 BB 183.06128 2.66076e-2 4.87082 Chloride

Totals : 10.09010

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\102-5502.D Sample Name: HPLC53pg98 #LCS

Instrument 1 10/4/2010 10:07:23 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 8 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 4:50:29 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0801.D)2.2783.124 - Fluoride4.249 - Chloride5.4486.0546.8348.4159.881

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.124 BB 307.02579 1.71654e-2 5.27021 Fluoride 4.249 BB 181.57738 2.71138e-2 4.92325 Chloride

Totals : 10.19346

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0801.D Sample Name: HPLC53pg100 #LCS

Instrument 1 10/5/2010 9:21:31 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 8 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 5:02:47 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0802.D)2.2773.125 - Fluoride4.249 - Chloride5.4446.0516.8318.4149.886

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 307.89706 1.71653e-2 5.28514 Fluoride 4.249 BB 181.32318 2.71142e-2 4.91644 Chloride

Totals : 10.20157

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\007-0802.D Sample Name: HPLC53pg100 #LCS

Instrument 1 10/5/2010 9:21:38 AM IGG Page 1 of 1

# Calibration Curve Chromatograms===================================================================== Calibration Table

=====================================================================

Calib. Data Modified : 10/4/2010 9:26:06 AM

Calculate : External Standard Based on : Peak Area

Rel. Reference Window : 10.000 % Abs. Reference Window : 0.000 min Rel. Non-ref. Window : 10.000 % Abs. Non-ref. Window : 0.000 min Use Multiplier & Dilution Factor with ISTDs Uncalibrated Peaks : not reported Partial Calibration : Yes, identified peaks are recalibrated Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear Origin : Connected Weight : Linear (Amnt)

Recalibration Settings: Average Response : Average all calibrations Average Retention Time: Floating Average New 75%

Calibration Report Options : Printout of recalibrations within a sequence: Calibration Table after Recalibration Normal Report after Recalibration If the sequence is done with bracketing: Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name [min] Sig [ug/mL] -------|--|--|----------|----------|----------|---|--|---------------
3.147 1 1 2.00000e-1 11.23373 1.78035e-2 Fluoride
2 1.00000 61.93819 1.61451e-2
3 5.00000 309.42168 1.61592e-2
4 10.00000 593.11342 1.68602e-2
5 15.00000 852.09720 1.76036e-2 4.156 1 1 2.00000e-1 5.55649 3.59939e-2 Chloride
2 1.00000 34.57356 2.89238e-2
3 5.00000 185.83790 2.69052e-2
4 10.00000 378.92274 2.63906e-2
5 15.00000 570.98003 2.62706e-2

===================================================================== Peak Sum Table

=====================================================================

***No Entries in table***

===================================================================== Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Instrument 1 10/4/2010 9:27:53 AM IGG Page 1 of 2===================================================================== Calibration Curves

=====================================================================

Amount[ug/mL] 0 10 Area

0 100 200 300 400 500 600 700 800

1 2 3 4 5 Fluoride at exp. RT: 3.147 ADC1 A, ADC1 CHANNEL A Correlation: 0.99937 Residual Std. Dev.: 18.29678 Formula: y = mx + b
m: 58.49156 b: 5.73482e-1

x: Amount y: Area Calibration Level Weights:
Level 1 : 1 Level 2 : 0.2 Level 3 : 0.04 Level 4 : 0.02 Level 5 : 0.013333

Amount[ug/mL] 0 10 Area

0 100 200 300 400 500

1 2 3 4 5 Chloride at exp. RT: 4.156 ADC1 A, ADC1 CHANNEL A Correlation: 0.99996 Residual Std. Dev.: 2.00920 Formula: y = mx + b
m: 38.06134 b: -2.32861

x: Amount y: Area Calibration Level Weights:
Level 1 : 1 Level 2 : 0.2 Level 3 : 0.04 Level 4 : 0.02 Level 5 : 0.013333

===================================================================== Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M

Instrument 1 10/4/2010 9:27:53 AM IGG Page 2 of 2===================================================================== Acq. Operator : EO Seq. Line : 2 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 6:10:43 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0201.D)2.2162.984 - Fluoride4.161 - Chloride5.5087.086

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.984 VB 11.43427 1.62975e-2 1.86350e-1 Fluoride 4.161 BB 5.52259 3.73516e-2 2.06278e-1 Chloride

Totals : 3.92628e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0201.D Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:21:47 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 2 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 6:23:04 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0202.D)

A

r ea

: 10

. 9 01

8

A r ea

: 5.

5 1 02

22.980 - Fluoride4.156 - Chloride5.489

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.980 MM 10.90178 1.62975e-2 1.77672e-1 Fluoride 4.156 MM 5.51022 3.73765e-2 2.05952e-1 Chloride

Totals : 3.83625e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-0202.D Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:06 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 70 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 1:45:22 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7001.D)2.2202.990 - Fluoride4.158 - Chloride5.4697.035

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.990 VB 11.61392 1.62975e-2 1.89278e-1 Fluoride 4.158 BB 5.54815 3.73006e-2 2.06949e-1 Chloride

Totals : 3.96227e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7001.D Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:15 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 70 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 1:57:42 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7002.D)

A

r ea

: 10

. 9 84

9

A r ea

: 5.

6 4 50

22.990 - Fluoride4.155 - Chloride5.455

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.990 MM 10.98494 1.62975e-2 1.79028e-1 Fluoride 4.155 MM 5.64502 3.71113e-2 2.09494e-1 Chloride

Totals : 3.88522e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\001-7002.D Sample Name: HPLC53pg98 #1

Instrument 1 10/4/2010 9:22:29 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 3 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 6:35:23 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0301.D)2.2603.106 - Fluoride4.265 - Chloride5.5076.1486.9928.4269.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.106 VB 62.57794 1.69398e-2 1.06006 Fluoride 4.265 BB 34.83099 2.80299e-2 9.76308e-1 Chloride

Totals : 2.03637

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0301.D Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:22:59 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 3 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 6:47:44 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0302.D)2.2683.105 - Fluoride4.262 - Chloride5.5126.1416.9818.4259.860

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.105 BB 60.57874 1.69346e-2 1.02588 Fluoride 4.262 BB 33.81343 2.80827e-2 9.49573e-1 Chloride

Totals : 1.97545

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-0302.D Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:23:48 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 71 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 2:10:01 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7101.D)2.2703.116 - Fluoride4.267 - Chloride5.4836.1196.9508.4509.913

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.116 VB 63.31603 1.69416e-2 1.07268 Fluoride 4.267 BB 35.34018 2.80046e-2 9.89686e-1 Chloride

Totals : 2.06236

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7101.D Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:23:56 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 71 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 2:22:21 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7102.D)2.2753.115 - Fluoride4.267 - Chloride5.4936.1226.9508.4509.913

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.115 BB 61.28004 1.69365e-2 1.03787 Fluoride 4.267 BB 34.30963 2.80566e-2 9.62610e-1 Chloride

Totals : 2.00048

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\002-7102.D Sample Name: HPLC53pg98 #2

Instrument 1 10/4/2010 9:24:05 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 4 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 6:59:03 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0401.D)2.2653.112 - Fluoride4.257 - Chloride5.5066.1186.9308.4219.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.112 BB 308.75937 1.70647e-2 5.26889 Fluoride 4.257 BB 185.12665 2.66039e-2 4.92508 Chloride

Totals : 10.19398

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0401.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:15 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 4 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 7:11:22 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0402.D)2.2663.113 - Fluoride4.257 - Chloride5.5056.1166.9278.4249.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.113 BB 308.33966 1.70647e-2 5.26172 Fluoride 4.257 BB 185.05852 2.66040e-2 4.92329 Chloride

Totals : 10.18501

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-0402.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:23 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 72 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 2:34:41 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7201.D)2.2773.124 - Fluoride4.263 - Chloride5.4946.1076.9088.4449.920

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.124 BB 309.26727 1.70648e-2 5.27758 Fluoride 4.263 BB 186.31842 2.66017e-2 4.95640 Chloride

Totals : 10.23397

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7201.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:36 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 72 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 2:47:01 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7202.D)2.2773.125 - Fluoride4.266 - Chloride5.4986.1106.9138.4529.926

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 311.32043 1.70650e-2 5.31268 Fluoride 4.266 BB 186.84802 2.66008e-2 4.97031 Chloride

Totals : 10.28299

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\003-7202.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 9:24:44 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 5 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 7:23:42 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0501.D)2.2673.125 - Fluoride4.256 - Chloride5.5016.1106.8998.4239.866

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 592.99884 1.70799e-2 10.12839 Fluoride 4.256 BB 377.41034 2.64355e-2 9.97703 Chloride

Totals : 20.10542

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0501.D Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:24:57 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 5 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 7:36:02 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0502.D)2.2633.123 - Fluoride4.254 - Chloride5.4956.1026.8918.4229.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BB 591.84839 1.70799e-2 10.10872 Fluoride 4.254 BB 377.41174 2.64355e-2 9.97706 Chloride

Totals : 20.08578

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-0502.D Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:05 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 73 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 2:59:21 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7301.D)2.2743.135 - Fluoride4.263 - Chloride5.4915.9686.1006.8828.4439.919

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.135 BB 594.09766 1.70800e-2 10.14718 Fluoride 4.263 BB 380.40378 2.64342e-2 10.05567 Chloride

Totals : 20.20285

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7301.D Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:21 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 73 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 3:11:41 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:21:17 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7302.D)2.2763.135 - Fluoride4.264 - Chloride5.4945.9706.1036.8848.4449.920

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Monday, October 04, 2010 9:21:13 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.135 BB 593.50879 1.70800e-2 10.13711 Fluoride 4.264 BB 380.46509 2.64342e-2 10.05728 Chloride

Totals : 20.19439

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\004-7302.D Sample Name: HPLC53pg98 #4

Instrument 1 10/4/2010 9:25:29 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 6 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 7:48:22 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0601.D)2.2663.134 - Fluoride4.255 - Chloride5.9666.1026.8738.4259.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.134 BB 847.65564 1.70849e-2 14.48213 Fluoride 4.255 BB 568.12811 2.63811e-2 14.98783 Chloride

Totals : 29.46995

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0601.D Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:29 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 6 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 8:00:42 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0602.D)2.2653.134 - Fluoride4.254 - Chloride5.9636.0986.8688.4239.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.134 BB 850.78156 1.70850e-2 14.53557 Fluoride 4.254 BB 567.44427 2.63812e-2 14.96986 Chloride

Totals : 29.50543

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-0602.D Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:37 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 74 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 3:24:00 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7401.D)2.2763.147 - Fluoride4.266 - Chloride5.4955.9516.1056.8738.4439.920

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.147 BB 856.55316 1.70850e-2 14.63424 Fluoride 4.266 BB 574.05273 2.63800e-2 15.14349 Chloride

Totals : 29.77773

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7401.D Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:45 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 74 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/3/2010 3:36:20 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7402.D)2.2763.148 - Fluoride4.268 - Chloride5.4955.9526.1066.8738.4479.921

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.148 BB 853.39844 1.70850e-2 14.58031 Fluoride 4.268 BB 574.29498 2.63799e-2 15.14985 Chloride

Totals : 29.73016

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\005-7402.D Sample Name: HPLC53pg98 #5

Instrument 1 10/4/2010 9:26:54 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 7 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 8:13:01 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0701.D)2.2663.105 - Fluoride4.255 - Chloride5.4946.1066.9318.4349.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.105 BB 75.83907 1.69672e-2 1.28678 Fluoride 4.255 BB 89.04053 2.69605e-2 2.40058 Chloride

Totals : 3.68735

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0701.D Sample Name: HPLC53pg98 #SS

Instrument 1 10/4/2010 9:28:12 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 7 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/1/2010 8:25:21 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:26:06 AM by IGG (modified after loading)

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0702.D)2.2703.109 - Fluoride4.259 - Chloride5.4996.1096.9338.4419.879

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:26:06 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.109 BB 75.80476 1.69671e-2 1.28619 Fluoride 4.259 BB 89.01553 2.69607e-2 2.39992 Chloride

Totals : 3.68611

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\006-0702.D Sample Name: HPLC53pg98 #SS

Instrument 1 10/4/2010 9:28:20 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 17 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 12:19:37 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1701.D)2.2673.115 - Fluoride4.253 - Chloride5.4866.0926.8998.4309.879

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.115 BB 305.79456 1.70644e-2 5.21821 Fluoride 4.253 BB 183.50085 2.66068e-2 4.88237 Chloride

Totals : 10.10057

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1701.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:05:55 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 17 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 12:31:57 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1702.D)2.2673.115 - Fluoride4.254 - Chloride5.4926.0966.9038.4329.873

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.115 BB 305.05637 1.70643e-2 5.20559 Fluoride 4.254 BB 182.77678 2.66081e-2 4.86334 Chloride

Totals : 10.06893

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-1702.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:04 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 29 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 6:45:00 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2901.D)2.2713.117 - Fluoride4.257 - Chloride5.4956.1006.9078.4369.893

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.117 BB 305.44266 1.70644e-2 5.21219 Fluoride 4.257 BB 183.08054 2.66076e-2 4.87132 Chloride

Totals : 10.08352

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2901.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:14 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 29 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 6:57:20 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2902.D)2.2693.116 - Fluoride4.257 - Chloride5.4956.0996.9078.4369.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.116 BB 304.76215 1.70643e-2 5.20056 Fluoride 4.257 BB 182.93237 2.66078e-2 4.86743 Chloride

Totals : 10.06799

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\100-2902.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:06:23 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 41 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:40:56 AM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4101.D)2.2803.129 - Fluoride4.268 - Chloride5.5006.1136.9198.4419.901

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.129 BB 305.45007 1.70644e-2 5.21232 Fluoride 4.268 BB 183.04117 2.66076e-2 4.87029 Chloride

Totals : 10.08261

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4101.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:07:50 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 41 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:53:15 AM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4102.D)2.2713.119 - Fluoride4.259 - Chloride5.4956.1016.9088.4379.886

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.119 BB 304.57260 1.70643e-2 5.19732 Fluoride 4.259 BB 182.35486 2.66089e-2 4.85226 Chloride

Totals : 10.04957

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-4102.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:00 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 53 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:36:34 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5301.D)2.2733.121 - Fluoride4.260 - Chloride5.4916.1046.9108.4369.900

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.121 BB 306.69925 1.70645e-2 5.23367 Fluoride 4.260 BB 183.57710 2.66066e-2 4.88437 Chloride

Totals : 10.11805

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5301.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:09 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 53 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 5:48:53 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5302.D)2.2723.120 - Fluoride4.261 - Chloride5.4966.1076.9148.4369.900

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.120 BB 305.72400 1.70644e-2 5.21700 Fluoride 4.261 BB 182.98579 2.66077e-2 4.86884 Chloride

Totals : 10.08584

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\110-5302.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:08:18 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 65 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:32:07 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6501.D)2.2773.123 - Fluoride4.263 - Chloride5.4946.1116.9138.4449.907

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BB 310.41275 1.70649e-2 5.29716 Fluoride 4.263 BB 185.78922 2.66027e-2 4.94249 Chloride

Totals : 10.23965

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6501.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:09:36 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 65 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/2/2010 11:44:27 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG98.M Last changed : 10/4/2010 9:39:38 AM by IGG

min 2 4 6 8 10 12 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6502.D)2.2973.122 - Fluoride4.263 - Chloride5.4936.1116.9148.4439.913

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/4/2010 9:36:48 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.122 VB 310.73752 1.70649e-2 5.30271 Fluoride 4.263 BB 186.29073 2.66018e-2 4.95567 Chloride

Totals : 10.25838

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG98\120-6502.D Sample Name: HPLC53pg98 #3

Instrument 1 10/4/2010 10:09:47 AM IGG Page 1 of 1===================================================================== Calibration Table

=====================================================================

Calib. Data Modified : 10/5/2010 9:18:49 AM

Calculate : External Standard Based on : Peak Area

Rel. Reference Window : 10.000 % Abs. Reference Window : 0.000 min Rel. Non-ref. Window : 10.000 % Abs. Non-ref. Window : 0.000 min Use Multiplier & Dilution Factor with ISTDs Uncalibrated Peaks : not reported Partial Calibration : Yes, identified peaks are recalibrated Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear Origin : Connected Weight : Linear (Amnt)

Recalibration Settings: Average Response : Average all calibrations Average Retention Time: Floating Average New 75%

Calibration Report Options : Printout of recalibrations within a sequence: Calibration Table after Recalibration Normal Report after Recalibration If the sequence is done with bracketing: Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name [min] Sig [ug/mL] -------|--|--|----------|----------|----------|---|--|---------------
3.149 1 1 2.00000e-1 9.95712 2.00861e-2 Fluoride
2 1.00000 61.11817 1.63617e-2
3 5.00000 308.63791 1.62002e-2
4 10.00000 589.09669 1.69751e-2
5 15.00000 849.33438 1.76609e-2 4.153 1 1 2.00000e-1 5.66901 3.52795e-2 Chloride
2 1.00000 33.68365 2.96880e-2
3 5.00000 182.27121 2.74317e-2
4 10.00000 369.59518 2.70566e-2
5 15.00000 562.35474 2.66736e-2

===================================================================== Peak Sum Table

=====================================================================

***No Entries in table***

===================================================================== Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Instrument 1 10/5/2010 9:20:49 AM IGG Page 1 of 2===================================================================== Calibration Curves

=====================================================================

Amount[ug/mL] 0 10 Area

0 100 200 300 400 500 600 700 800

1 2 3 4 5 Fluoride at exp. RT: 3.149 ADC1 A, ADC1 CHANNEL A Correlation: 0.99933 Residual Std. Dev.: 18.30415 Formula: y = mx + b
m: 58.36617 b: -5.76052e-1

x: Amount y: Area Calibration Level Weights:
Level 1 : 1 Level 2 : 0.2 Level 3 : 0.04 Level 4 : 0.02 Level 5 : 0.013333

Amount[ug/mL] 0 10 Area

0 100 200 300 400 500

1 2 3 4 5 Chloride at exp. RT: 4.153 ADC1 A, ADC1 CHANNEL A Correlation: 0.99993 Residual Std. Dev.: 3.24460 Formula: y = mx + b
m: 37.31718 b: -2.14447

x: Amount y: Area Calibration Level Weights:
Level 1 : 1 Level 2 : 0.2 Level 3 : 0.04 Level 4 : 0.02 Level 5 : 0.013333

===================================================================== Method U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M

Instrument 1 10/5/2010 9:20:49 AM IGG Page 2 of 2===================================================================== Acq. Operator : EO Seq. Line : 2 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 2:22:30 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0201.D)

A

r ea

: 9.

5 5 97

22.2252.990 - Fluoride4.157 - Chloride5.4627.014

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.990 MM 9.55972 1.80226e-2 1.72291e-1 Fluoride 4.157 BB 5.61364 3.70342e-2 2.07896e-1 Chloride

Totals : 3.80187e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0201.D Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:41 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 2 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 2:34:50 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0202.D)

A

r ea

: 5.

8 7 64

42.2212.985 - Fluoride4.150 - Chloride5.441

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.985 VB 10.01584 1.80226e-2 1.80511e-1 Fluoride 4.150 MM 5.87644 3.65764e-2 2.14939e-1 Chloride

Totals : 3.95450e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-0202.D Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:55 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 14 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 7:38:19 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1401.D)

A

r ea

: 10

. 0 54

12.991 - Fluoride4.154 - Chloride5.4456.985

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.991 MM 10.05413 1.80226e-2 1.81201e-1 Fluoride 4.154 BB 5.65120 3.69661e-2 2.08903e-1 Chloride

Totals : 3.90104e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1401.D Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:17:10 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 14 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 7:50:38 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1402.D)

A

r ea

: 5.

5 3 47

72.2212.989 - Fluoride4.153 - Chloride5.436

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
2.989 VB 10.19880 1.80226e-2 1.83809e-1 Fluoride 4.153 MM 5.53477 3.71800e-2 2.05783e-1 Chloride

Totals : 3.89592e-1

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\001-1402.D Sample Name: HPLC53pg100 #1

Instrument 1 10/5/2010 9:16:25 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 3 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 2:47:11 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0301.D)2.2703.114 - Fluoride4.258 - Chloride5.4616.0956.9138.4019.860

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.114 VB 62.22894 1.72918e-2 1.07605 Fluoride 4.258 BB 34.35212 2.84702e-2 9.78010e-1 Chloride

Totals : 2.05406

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0301.D Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:19 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 3 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 2:59:30 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0302.D)2.2773.115 - Fluoride4.257 - Chloride5.4676.0936.9078.4059.867

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.115 BB 59.91656 1.72979e-2 1.03643 Fluoride 4.257 BB 32.97707 2.85399e-2 9.41163e-1 Chloride

Totals : 1.97760

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-0302.D Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:28 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 15 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 8:02:58 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1501.D)2.2703.118 - Fluoride4.267 - Chloride5.4686.1166.9418.4159.887

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.118 VB 62.23907 1.72918e-2 1.07622 Fluoride 4.267 BB 34.30110 2.84726e-2 9.76643e-1 Chloride

Totals : 2.05287

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1501.D Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:37 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 15 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 8:15:17 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1502.D)2.2803.119 - Fluoride4.268 - Chloride5.4786.1206.9428.4159.886

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.119 BB 60.08810 1.72975e-2 1.03937 Fluoride 4.268 BB 33.10430 2.85332e-2 9.44572e-1 Chloride

Totals : 1.98394

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\002-1502.D Sample Name: HPLC53pg100 #2

Instrument 1 10/5/2010 9:17:46 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 4 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 3:11:49 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0401.D)2.2763.123 - Fluoride4.252 - Chloride5.4616.0716.8578.4009.873

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BB 308.96735 1.71652e-2 5.30347 Fluoride 4.252 BB 182.23886 2.71126e-2 4.94098 Chloride

Totals : 10.24445

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0401.D Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:17:53 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 4 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 3:24:10 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0402.D)2.2753.123 - Fluoride4.251 - Chloride5.4556.0646.8488.4049.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.123 BB 308.16321 1.71652e-2 5.28970 Fluoride 4.251 BB 182.15358 2.71128e-2 4.93869 Chloride

Totals : 10.22839

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-0402.D Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:01 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 16 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 8:27:38 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1601.D)2.2783.127 - Fluoride4.264 - Chloride5.4766.1026.8988.4069.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.127 BB 309.30249 1.71651e-2 5.30921 Fluoride 4.264 BB 182.42313 2.71123e-2 4.94591 Chloride

Totals : 10.25513

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1601.D Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:09 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 16 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 8:39:57 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1602.D)2.2763.125 - Fluoride4.262 - Chloride5.4756.1036.9008.4039.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.125 BB 308.11859 1.71652e-2 5.28893 Fluoride 4.262 BB 182.26926 2.71126e-2 4.94179 Chloride

Totals : 10.23072

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\003-1602.D Sample Name: HPLC53pg100 #3

Instrument 1 10/5/2010 9:18:16 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 5 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 3:36:29 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:16:05 AM by IGG

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0501.D)2.2773.135 - Fluoride4.251 - Chloride5.4545.9376.0636.8268.4079.873

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : Tuesday, October 05, 2010 9:15:59 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.135 BB 587.12793 1.71500e-2 10.06926 Fluoride 4.251 BB 369.45987 2.69528e-2 9.95800 Chloride

Totals : 20.02725

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0501.D Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:18:24 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 5 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 3:48:49 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0502.D)2.2833.149 - Fluoride4.265 - Chloride5.4655.9506.0736.8378.4219.894

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.149 BB 590.64954 1.71499e-2 10.12959 Fluoride 4.265 BB 369.45181 2.69529e-2 9.95778 Chloride

Totals : 20.08737

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-0502.D Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:18:52 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 17 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 8:52:17 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1701.D)2.2953.154 - Fluoride4.280 - Chloride5.4915.9916.1176.8948.4219.899

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.154 BB 587.89532 1.71500e-2 10.08241 Fluoride 4.280 BB 369.70758 2.69527e-2 9.96463 Chloride

Totals : 20.04704

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1701.D Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:19:17 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 17 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 9:04:37 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1702.D)2.2773.138 - Fluoride4.265 - Chloride5.4785.9796.1056.8848.4039.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.138 BB 590.71399 1.71499e-2 10.13070 Fluoride 4.265 BB 369.76144 2.69527e-2 9.96608 Chloride

Totals : 20.09677

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\004-1702.D Sample Name: HPLC53pg100 #4

Instrument 1 10/5/2010 9:19:28 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 6 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 4:01:09 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0601.D)2.2743.144 - Fluoride4.250 - Chloride5.4445.9106.0556.8038.4079.881

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.144 BB 849.68134 1.71448e-2 14.56764 Fluoride 4.250 BB 562.55444 2.68995e-2 15.13241 Chloride

Totals : 29.70005

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0601.D Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:38 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 6 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 4:13:29 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0602.D)2.2763.145 - Fluoride4.250 - Chloride5.4435.9096.0546.8018.4079.873

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.145 BB 847.86249 1.71449e-2 14.53648 Fluoride 4.250 BB 562.09290 2.68995e-2 15.12004 Chloride

Totals : 29.65652

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-0602.D Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:46 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 18 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 9:16:57 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1801.D)2.2763.148 - Fluoride4.265 - Chloride5.4755.9536.1036.8678.4039.893

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.148 BB 851.27545 1.71448e-2 14.59495 Fluoride 4.265 BB 562.78735 2.68994e-2 15.13865 Chloride

Totals : 29.73360

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1801.D Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:19:54 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 18 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 9:29:17 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1802.D)2.2763.146 - Fluoride4.263 - Chloride5.4745.9526.1016.8668.3959.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.146 BB 848.51825 1.71448e-2 14.54771 Fluoride 4.263 BB 561.98425 2.68996e-2 15.11713 Chloride

Totals : 29.66484

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\005-1802.D Sample Name: HPLC53pg100 #5

Instrument 1 10/5/2010 9:20:02 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 7 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 4:38:08 PM Inj : 2 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0702.D)2.2763.117 - Fluoride4.251 - Chloride5.4466.0536.8518.4199.874

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:21:11 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.117 BB 76.75529 1.72618e-2 1.32493 Fluoride 4.251 BB 90.33049 2.74335e-2 2.47808 Chloride

Totals : 3.80301

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0702.D Sample Name: HPLC53pg100 #SS

Instrument 1 10/5/2010 9:21:23 AM IGG Page 1 of 1===================================================================== Acq. Operator : EO Seq. Line : 7 Acq. Instrument : Mr_Burns Location : - Injection Date : 10/4/2010 4:25:48 PM Inj : 1 Acq. Method : C:\HPLC2010Q3\MR BURNS\METHODS\METROHM.M Last changed : 4/1/2010 4:15:36 PM Analysis Method : U:\HPLC2010Q3\MR BURNS\METHODS\HPLC53PG100.M Last changed : 10/5/2010 9:18:49 AM by IGG (modified after loading)

min 2 4 6 8 uS/cm

0 20 40 60 80 100 120 140 160 180 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0701.D)2.2783.119 - Fluoride4.253 - Chloride5.4506.0596.8588.4199.880

===================================================================== External Standard Report

=====================================================================

Sorted By : Signal Calib. Data Modified : 10/5/2010 9:18:49 AM Multiplier : 1.0000 Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name [min] [uS/cm*s] [ug/mL] -------|------|----------|----------|----------|--|------------------
3.119 BB 76.93913 1.72615e-2 1.32808 Fluoride 4.253 BB 90.24962 2.74341e-2 2.47591 Chloride

Totals : 3.80400

===================================================================== *** End of Report *** Data File U:\HPLC2010Q4\MR BURNS\DATA\OCT\HPLC53PG100\006-0701.D Sample Name: HPLC53pg100 #SS

Instrument 1 10/5/2010 9:21:08 AM IGG Page 1 of 1Method Information

Method: U:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M Modified: 1/13/2010 at 7:06:26 AM

========================================================================= ANALOG DIGITAL CONVERTER

========================================================================= Signal 1

--------------------- Description: ADC1 A, Metrohm Source: Signal Unit: mAU Units/Volt: 100.000 Peakwidth (Data Rate): 0.027 Min (10.00 Hz) Stop Time: No Limit Data Storage: All

Start Signal Source: External Device Will Start 35900

Timed Event Table:
<no events> method: U:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M Modified on: 1/13/2010 at 7:06:26 AM

Smithers 1/18/2010 7:20:57 AM mgb Page 1 of 1Sequence Table:

Method and Injection Info Part:

Line Location SampleName Method Inj SampleType InjVolume DataFile AutoBalance LimsID

==== ======== ==================== ==================== ======== ========== =========

1 Vial 127 DI Rinse METROHM 4 Sample

2 Vial 1 HPLC53pg98 #1 METROHM 2 Sample

3 Vial 2 HPLC53pg98 #2 METROHM 2 Sample

4 Vial 3 HPLC53pg98 #3 METROHM 2 Sample

5 Vial 4 HPLC53pg98 #4 METROHM 2 Sample

6 Vial 5 HPLC53pg98 #5 METROHM 2 Sample

7 Vial 6 HPLC53pg98 #SS METROHM 2 Sample

8 Vial 7 HPLC53pg98 #LCS METROHM 2 Sample

9 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample

10 Vial 9 Salisbury R1 In A *20 0910-96 METROHM 2 Sample

11 Vial 10 MS Salisbury R1 In A *20 0910-96 METROHM 2 Sample

12 Vial 11 MSD Salisbury R1 In A *20 0910-96 METROHM 2 Sample

13 Vial 12 Salisbury R2 In A *20 0910-96 METROHM 2 Sample

14 Vial 13 Salisbury R3 In A *20 0910-96 METROHM 2 Sample

15 Vial 14 Salisbury R1 Out A *10 0910-96 METROHM 2 Sample

16 Vial 15 Salisbury R2 Out A *10 0910-96 METROHM 2 Sample

17 Vial 100 HPLC53pg98 #3 METROHM 2 Sample

18 Vial 101 HPLC53pg98 #4 METROHM 2 Sample

19 Vial 16 Salisbury R3 Out A *10 0910-96 METROHM 2 Sample

20 Vial 17 Salisbury R1 In B *10 0910-96 METROHM 2 Sample

21 Vial 18 Salisbury R2 In B *10 0910-96 METROHM 2 Sample

22 Vial 19 Salisbury R3 In B *10 0910-96 METROHM 2 Sample

23 Vial 20 Salisbury R1 B Out *10 0910-96 METROHM 2 Sample

24 Vial 21 Salisbury R2 Out B *10 0910-96 METROHM 2 Sample

25 Vial 22 Salisbury R3 Out B *10 0910-96 METROHM 2 Sample

26 Vial 23 Salisbury R1 Out B *100 0910-96 METROHM 2 Sample

27 Vial 24 Salisbury R2 out B *100 0910-96 METROHM 2 Sample Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 1 of 3Line Location SampleName Method Inj SampleType InjVolume DataFile AutoBalance LimsID

==== ======== ==================== ==================== ======== ========== =========

28 Vial 25 Salisbury R3 Out B *100 0910-96 METROHM 2 Sample

29 Vial 100 HPLC53pg98 #3 METROHM 2 Sample

30 Vial 101 HPLC53pg98 #4 METROHM 2 Sample

31 Vial 7 HPLC53pg98 #LCS METROHM 2 Sample

32 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample

33 Vial 26 P4 R1 In A *10 0910-96 METROHM 2 Sample

34 Vial 27 MS P4 R1 In A *10 0910-96 METROHM 2 Sample

35 Vial 28 MSD P4 R1 In A *10 0910-96 METROHM 2 Sample

36 Vial 29 P4 R2 In A *10 0910-96 METROHM 2 Sample

37 Vial 30 P4 R3 In A *10 0910-96 METROHM 2 Sample

38 Vial 31 P4 R1 Out A *10 0910-96 METROHM 2 Sample

39 Vial 32 P4 R2 Out A *10 0910-96 METROHM 2 Sample

40 Vial 33 P4 R3 Out A *10 0910-96 METROHM 2 Sample

41 Vial 110 HPLC53pg98 #3 METROHM 2 Sample

42 Vial 111 HPLC53pg98 #4 METROHM 2 Sample

43 Vial 34 P4 R1 In B *10 0910-96 METROHM 2 Sample

44 Vial 35 P4 R2 In B *10 0910-96 METROHM 2 Sample

45 Vial 36 P4 R3 In B *10 0910-96 METROHM 2 Sample

46 Vial 37 P4 R1 Out B *10 0910-96 METROHM 2 Sample

47 Vial 38 P4 R2 Out B *10 0910-96 METROHM 2 Sample

48 Vial 39 P4 R3 Out B *10 0910-96 METROHM 2 Sample

49 Vial 40 P5 R1 In A *10 0910-96 METROHM 2 Sample

50 Vial 41 P5 R2 In A *10 0910-96 METROHM 2 Sample

51 Vial 42 P5 R3 In A *10 0910-96 METROHM 2 Sample

52 Vial 43 P5 R1 Out A *10 0910-96 METROHM 2 Sample

53 Vial 110 HPLC53pg98 #3 METROHM 2 Sample

54 Vial 111 HPLC53pg98 #4 METROHM 2 Sample

55 Vial 102 HPLC53pg98 #LCS METROHM 2 Sample

56 Vial 103 0.01N H2SO4/NaOH RB METROHM 2 Sample

57 Vial 44 P5 R2 Out A *10 0910-96 METROHM 2 Sample Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 2 of 3Line Location SampleName Method Inj SampleType InjVolume DataFile AutoBalance LimsID

==== ======== ==================== ==================== ======== ========== =========

58 Vial 45 P5 R3 Out A *10 0910-96 METROHM 2 Sample

59 Vial 46 P5 R1 In B *10 0910-96 METROHM 2 Sample

60 Vial 47 P5 R2 In B *10 0910-96 METROHM 2 Sample

61 Vial 48 P5 R3 In B *10 0910-96 METROHM 2 Sample

62 Vial 49 P5 R1 out B *10 0910-96 METROHM 2 Sample

63 Vial 50 P5 R2 Out B *10 0910-96 METROHM 2 Sample

64 Vial 51 P5 R3 out B *10 0910-96 METROHM 2 Sample

65 Vial 120 HPLC53pg98 #3 METROHM 2 Sample

66 Vial 121 HPLC53pg98 #4 METROHM 2 Sample

67 Vial 52 Acid Blank *10 0910-96 METROHM 2 Sample

68 Vial 53 Base Blank *10 0910-96 METROHM 2 Sample

69 Vial 54 DI H2O blank 0910-96 METROHM 2 Sample

70 Vial 1 HPLC53pg98 #1 METROHM 2 Sample

71 Vial 2 HPLC53pg98 #2 METROHM 2 Sample

72 Vial 3 HPLC53pg98 #3 METROHM 2 Sample

73 Vial 4 HPLC53pg98 #4 METROHM 2 Sample

74 Vial 5 HPLC53pg98 #5 METROHM 2 Sample Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG98.S

Instrument 1 10/4/2010 12:16:32 PM IGG Page 3 of 3Sequence Table:

Method and Injection Info Part:

Line Location SampleName Method Inj SampleType InjVolume DataFile AutoBalance LimsID

==== ======== ==================== ==================== ======== ========== =========

1 Vial 127 DI Rinse METROHM 4 Sample

2 Vial 1 HPLC53pg100 #1 METROHM 2 Sample

3 Vial 2 HPLC53pg100 #2 METROHM 2 Sample

4 Vial 3 HPLC53pg100 #3 METROHM 2 Sample

5 Vial 4 HPLC53pg100 #4 METROHM 2 Sample

6 Vial 5 HPLC53pg100 #5 METROHM 2 Sample

7 Vial 6 HPLC53pg100 #SS METROHM 2 Sample

8 Vial 7 HPLC53pg100 #LCS METROHM 2 Sample

9 Vial 8 0.01N H2SO4/NaOH RB METROHM 2 Sample

10 Vial 9 P5 R2 In A *20 0910-96 METROHM 2 Sample

11 Vial 10 P5 R3 In A *20 0910-96 METROHM 2 Sample

12 Vial 11 R1 C4 *10 1010-10 METROHM 2 Sample

13 Vial 12 R2 C4 *10 1010-10 METROHM 2 Sample

14 Vial 1 HPLC53pg100 #1 METROHM 2 Sample

15 Vial 2 HPLC53pg100 #2 METROHM 2 Sample

16 Vial 3 HPLC53pg100 #3 METROHM 2 Sample

17 Vial 4 HPLC53pg100 #4 METROHM 2 Sample

18 Vial 5 HPLC53pg100 #5 METROHM 2 Sample Sequence: U:\HPLC2010Q4\MR BURNS\SEQUENCE\HPLC53PG100.S

Instrument 1 10/5/2010 9:25:03 AM IGG Page 1 of 1

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