6 1



# Sampl e Receip t Documentatio

n

i i



### VES01920 9

## Sampl e Traceabilat y Lis t KDU ^§Ab

SE6 3 9 ^1 ^ SLPff e SUZ . B7_ ^ BtfWe ^2-12-Slft O 

### ©I p^ I p SZl- L$26 0 

## .ECO M

Site, o f Proqram : Veoli aE S Tec

h Sample Date : f^/fa , /2/tf/o ? Projec tLocation : Sauget , I L P.O . if

: Type of Program : CP T Dat e Shipped : /a.fiUfa'} Laboratory : TestAmerica , Inc . Knoxville , TN Projects ; 60133216 Progra m Office : Syracus e N Y Shipper/

' ' ' Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , TN Progra m Contact : Jef f Gorma n FedE x AirBil l #

: Ite m Sampl e I D Cod e Sampl e Matri x Sampl e Descriptio

n Analltica l Parameter

s | Specia l Instruction

s 1 HBTU-U4-IVI23A-R 1 Liqui d Hig

h Btu , Uni t4 , Ru n 1 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 . HBTU-U4-M23A-R 2 Liqui d Hig

h Btu, Uni

t4 , Ru n 2 Physica l Parameter

s & Cl , Tota

l Chlorin e 3 HBTU-U4-M23A-R 3 Liqui d Hig

h Btu , Uni t4 , Ru n 3 Physica l Parameter

s & Cl , Tota

l Chlorin e 4 1 5 L.BTU-II4-M23A-R 1 Liqui d Lo

w Btu , Uni t4 Ru n 1 Physica l Parameter

s & Cl , Tota

l Chlorin e 6 LBTU-U4-M23A-R 2 Liqui d Lo

w Btu , Uni tA Ru n 2 Physica l Parameter

s & Cl , Tota

l Chlorin e 7 LBTU-U4-W123A-R3 Liqui d Lo

w Btu , Uni t4 Ru n 3 Physica l Parameter

s a Cl , Tota

l Chlorin e 8 • i 9 SF-U4-W123A-R 1 Liqui d Specialit

y Feeder , Uni t4 , Ru n 1 Physica

l Parameter

s & Cl , Tota

l Chlorin e 1 0 SI--U4-IVI23A-R 2 Liqui d Specilait

y Feeder , Uni t4 , Ru n 2 Physica

l Parameter

s & Cl , Tota

l Chlorin e 1 1 SF-U4-M23A-R 3 Liqui d Specialit

y Feeder , Uni t4 , Ru n 3 Physica

l Parameter

s & Cl , Tota

l Chlorin e 1 2 

### | 1 3 CS-U4-M23A-R 1 Soli d Containerize d Solids , Uni

t4 , Ru n 1 Physica

l Parameter

s 8 . Cl , Tota l Chlorin e 1 4 CS-U4-W123A-R2 Soli d Containerize d Solids , Uni

t4 , Ru n 2 Physica

l Parameter

s & Cl , Tota

l Chlorin e 1 5 CS-U4-M23A-R 3 Soli d Containerize d Solids , Uni

t4 , Ru n 3 Physica

l Parameter

s & Cl , Tota

l Chlorin e 1 6 1 1 7 BS-U4-M23A-R 1 Soli d Bul

kSolids , Uni

t4 , Ru n 1 Physica l Parameter

s & Cl , Tota

l Chlorin e 1 8 BS-U4-M23A-R 2 Soli d Bul

kSolids , Uni

t4 , Ru n 2 Physica l Parameter

s & Cl , Tota

l Chlorin e 1 9 BS-U4-M23A-R 3 Soli d Bul

kSolids , Uni

t4 , Ru n 3 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 0 1 Fiel d Notes / Comment

s 1 • Physica l Parameter

s = Tota l chlorides, hea

tconten taas h content

. 2 . C l Pag e 1 o

f _ 2 Relinquishe

d B y (print) : Date ; Signature : / Time : Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d B y (print) : Date : Signature : Time : Receive d b y La b (print) : Date ; Signature ; Time ; Receive d By (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Analvtlca l Laborator

y Destination : TestAmeric

aInc . 5815 Middlebroo

kPik e Knoxville , T N 3792

1 Attn : Mr . Kevi n Woodcoc

k865-291-300

0 <3

> r o 

### VES01921 0I AECO M 

## Sampl e Traceafoifit

y Lis t! Sit e o f Program : Veoli aE S Tec h Sample Date : - |2.IW/o« > Projec tLocation : Sauget , I L P.O . #

: Type of Program : CP T Dat e Shipped: ' 'fT./lU'/o^ ' Laboratory : TestAmerica , Inc . Knoxville , T N Project* : 60133216 Shippe r/ Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , T N Progra m Office : Syracus e N Y Shippe r/

Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , T N Progra m Contact : Jef f Gorma n FedEx Ai rBill # : Ite m Sampl e I D Cod e Sampl e Matri x Liqui d Sampl i Hig h Btu , Uni t4. i Descriptio

n Analitlca l Parameter

s | Specia l Instruction

s 2 1 HBTU-U4-M26-R 1 . Sampl e Matri x Liqui d Sampl i Hig h Btu , Uni t4. *u n 1 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 2 HBTU-U4-IVI26A-R 2 . Liqui d Higl

i Btu , Uni t4 , Ru n 2 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 3 HBTU-U4-WI26A-R 3 . Liqui d Hig

h Btu , Uni t4 , Ru n 3 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 4 I 2 5 LBTU-U4-M26A-R 1 • Liqui d Lo

w Btu , Uni t4 Ru n 1 Physica l Parameter

s a Cl , Tota

l Chlorin e 2 6 LBTU-U4-M26A-R 2 - Liqui d Lo

w Btu , Uni t4 Ru n 2 Physica l Parameter

s & Cl , Tota

l Chlorin e 2 7 LBTU-U4-WI26A-R 3 - Liqui d Lo

w Btu , Uni t4 Ru n 3 Physica l Parameter

s a Cl , Tota

l Chlorin e 2 8 I 2 9 SF-U4-M26A-R 1 • Liqui d Specialit

y Feeder , Uni t4 , Ru n 1 Physica

l Parameter

s aCl , Tota

l Chlorin e 3 0 SF-U4-M26A-R 2 • Liqui d Specilait

y Feeder , Uni t4 , Ru n 2 Physica

l Parameter

s & Cl , Tota

l Chlorin e 3 1 SF-U4-M26A-R 3 ' Liqui d Specialit

y Feeder , Uni t4 , Ru n 3 Physica

l Parameter

s aCl , Tota

l Chlorin e 3 2 I 3 3 CS-U4-IVI26A-R 1 Soli d Containerize d Solids , Unit.4

, Ru n 1 Physica

l Parameter

s & Cl , Tota

l Chlorin e 3 4 • CS-U4-M26A-R 2 Soli d Containerize d Solids , Uni

t4 , Ru n 2 Physica

l Parameter

s aCl , Tota

l Chlorin e 3 5 CS-U4-WI26A-R 3 Soli d Containerize d Solids , Uni

t4, Ru n 3 Physica

l Parameter

s aCl , Tota

l Chlorin e 3 6 | 3 7 BS-U4-M26A-R I Soli d Bul

kSolids , Uni

t4 , Ru n 1 Physica l Parameter

s & Cl , Tota

l Clilorin e 3 8 BS-U4-M26A-R 2 Soli d Bul

kSolids , Uni

t4 , Ru n 2 Physica l Parameter

s aCl , Tota

l Chlorin e 3 9 BS-U4-M26A-R 3 Soli d Bul

kSolids , Uni

t4 , Ru n 3 Physica l Parameter

s & Cl , Tota

l Chlorin e 4 0 • 1 Fiel d Notes / Comment

s 1 . Physica l Parameter

s = Tota l chlorides, hea

tconten t& as h content

. 2 . C l Page 2 o f 2 Relinquishe

d B y (print) : Date : Signature : , Time : Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d B y (print) ; Date : Signature : Time : Receive d b y La b (print) : Date : Signature : Time : Receive d B y (print) : Date : /Signature ^ ^ Time : Receive d B y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Analytica l Laborator

y Destination : Receive d B y (print) : Date : /Signature ^ ^ Time : Receive d B y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Tes tAmeric aInc . 581 5 Middlebroo

kPik e Knoxville , T N 37921 Attn : Mr . Kevi n Woodcoc

k865-291-300

0TESTAMERIC A KNOXVILL ESAMPL ERECEIPT/CONDITIO NUPO NRECEIP T ANOMAL Y CHECKLIS T Lo t Number : V\ c \V.^PHf) M Revie w Items Ye s < N o N A I f No , whatwa

s the problem ? Comments/Action s Take n 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : • 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 1 . D o sample containe rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

— I • l aD o no tmatc h CO C D 1 b Incomplet

e information 0 l c Markin g smeare

d • I d Labe l tor

n d i e N o labe

l O l f CO C no

treceived • l g Other : 2 . I s th e coole rtemperatur

e withi n limits ? (

> freezing temp, o f wate rt o 6"C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6"C ) 

## J j • 2aTem p Blan k= 2 . I s th e coole rtemperatur

e withi n limits ? (

> freezing temp, o f wate rt o 6"C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6"C ) 

## J j D 2 b Coole rTemp = 2 . I s th e coole rtemperatur

e withi n limits ? (

> freezing temp, o f wate rt o 6"C;NC , 1668, 1613B : 0-4"C ; VOST : 10°C;MA:2-6"C ) 

## J j 3 . Wer

e sample s received wit

h correc tchemica

l preservativ

e (excluding Encore) ? I— 

## J 0 3 aSample preservativ e = 3 . Wer

e sample s received wit

h correc tchemica

l preservativ

e (excluding Encore) ? I— 

## J 0 3 aSample preservativ e = 4 . Wer e custod y seal s present/intac

ton coole rand/o

r containers ? 

## j 0 d 4aNo tpresen t 0 4b No tintac

t 0 4 c Other : 4 . Wer e custod y seal s present/intac

ton coole rand/o

r containers ? 

## j 0 d 4aNo tpresen t 0 4b No tintac

t 0 4 c Other : - 4 . Wer e custod y seal s present/intac

ton coole rand/o

r containers ? 

## j 0 d 4aNo tpresen t 0 4b No tintac

t 0 4 c Other : 5 . Wer e al l ofth e sample

s listed on th

e CO C received ? 

# 1 0 5aSample s received-noto

n CO C • 5 b Sample

s no treceived-on CO C 5 . Wer e al l ofth e sample

s listed on th

e CO C received ? 

# 1 0 5aSample s received-noto

n CO C • 5 b Sample

s no treceived-on CO C 6 . Wer e al l o f th e sampl e container

s received intact

? 

# J ( • 6 aLeakin g • 6b Broken 6 . Wer e al l o f th e sampl e container

s received intact

? 

# J ( • 6 aLeakin g • 6b Broken 7 . Wer e VO A sample

s received withou

theadspace ? 

## 4- 

## J • 7 aHeadspac e (VO A only ) 8 . Wer e sample s received i n appropriat e containers ? 

## •J 

## I • 8aImprope rcontainer 9. Di d yo u chec

k fo rresidua

l chlorine , i f

necessary ? i 

## j • 9aCoul d no tb e determine

d du e t o matri x interferenc

e 9. Di d yo u chec

k fo rresidua

l chlorine , i f

necessary ? i 

## j • 9aCoul d no tb e determine

d du e t o matri x interferenc

e 10 . Wer e sample s received within holdin g time ? / • 10 aHoldin g tim

e expire d U . Forra

d samples , wa

s sampl e activit y info , provided ? 0 Incomplet e information 12 . Fo r1613

B wate rsample s i s pH<9 ? i 

# J I f no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 12 . Fo r1613

B wate rsample s i s pH<9 ? i 

# J I f no , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid ? 13. Ar e th

e shipping container

s intact? 

# T

- i - • 13aLeakin g

• 13 b Other : 13. Ar e th

e shipping container

s intact? 

# T

- i - • 13aLeakin g

• 13 b Other : 13. Ar e th

e shipping container

s intact? 

# T

- i - • 13aLeakin g

• 13 b Other : 14 . Wa s CO C relinquished ? (Signed/Dated/Timed ) • v Q 14 aNo trelinquishe

d 15. Ar e tests/parameter s listed fo reac

h sample ? 

# H

• 15 aIncomplet

e information 16 . I s th e matri x ofth e sample

s noted ? 

## i 0 15 n Incomplet

e information 17. I s th e date/tim

e o f sampl e collectio n noted ? 

### •/ 0 15 aIncomplet

e information 18 . I s th e clientan

d projec tname/ #identified ? 

## u • 15aIncomplet e information 19. Wa s th e sample ridentifie d o n th

e COC ? 

## J Ouote# : 

### fif''31 , P M Instructions : ^V—f^4— JX- , . ,-„ Date : QA026R21.doc , 09040 9

•J> . 

### VES01921 26 5



# We t Chemistry

VES01921 36 6



# Sampl e Summar

y

VES01921 46 7

AECOM , In c Clien t Sampl e ID : HBTU-U4-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L210404-00 1 Wor k Orde r #... : LRE3 3 Matri x: WAST E Dat e Sampled . . . : 12/16/0 9 Dat e Received.. : 12/19/0 9

PARAMETER RESUL T R L UNIT S Ash . Conten t
Gros s Calorifi c Valu e
Tota l Chlorin e 670 0 20 0 mg/kg Dilutio nFactor : 1 858 0 180 0 BTU/l b

Dilutio nFactor : 1 644 0 24 4 nig/k g

Dilutio nFactor : 1.2 2 _METHO D AST M D482-0O a MDL : 5 1 AST M D240-0 2
MD L : 1 3 0 KNO X WC-001 6 MD L : 7 3 PREPARATION - PRE P ANALYSI S DAT E BATCH # 01/11-01/13/1 0 001120 8
01/12/1 0 001204 8

01/11-01/15/1 0 001104 4



### VES01921 56 8

AECOM , In c Clien t Sampl e ID : HBTtI-U4-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L210404-00 2 Wor k Orde r #.. . Dat e Sample d : 12/17/0 9 Dat e Received. .
PARAMETER RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 373 0 20 0 mg/kg Dilutio nFactor : 1 859 0 180 0 BTU/l b

Dilutio nFactor : 1 254 0 25 8 mg/kg

Dilutio nFactor : 1.2 S LRE3 4 12/19/0 9 Matri x: WAST E

_METHO

D AST M D482-O0 a MDL : 5 1 AST M D240-0 2 MDI J : 13 0 KNO X WC-001 6 MD L : 7 7 PREPARATION - PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01921 66 9

AECOM , In c Clien t Sampl e ID : HBTU-U4-M23A-R 3

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-00 3 Wor k Orde r #.. . : LRE3 5 Matri x: WAST E Dat e Sampled . .. : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 308 0 20 0 mg/kg AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 851 0 180 0 BTU/11 ) AST M D240-0 2 01/12/1 0 001204 8 VaLu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 234 0 31 8 mg/kg KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.5 3 MD L : 9 5



### VES01921 77 0

AECOM , In c Clien t Sampl e ID : LBTU-U4-M23A-R 1

Genera l Chemistry Lot-Sampl e #... : H9L210404-00 4 Wor k Orde r #... : LRE3 6 Matri x: WAST E Dat e Sampled... : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH ft As hConten t 256 0 20 0 mg/k g AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor ; 1 MD L : 5 1 Gros s Calorifi c 22 6 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Vala e Dilutio nFactor : 1 MD L - . 13 0 Tota l Chlorin e 128 0 21 4 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 7 MD L : S 4 NOT E (S) : , R L Repellin

g Limi t B Estimate

dresult . Result i

s les s tha nRL .



### VES01921 87 1

AECOM , m c Clien t Sampl e ID : LBTU-U4-M23A-R 2

Genera l Chemistr y Lot-Sampl e #.. . Dat e Sampled.. .
PARAMETE R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e : H9L210404-00 5 : 12/17/0 9 Wor k Orde r #. . Dat e Received .
RESUL T RL UNIT S 273 0 20 0 mg/k g

Dilutio nFactor : 1 15 4 B 180 0 BTU/l b

Dilutio nFactor : 1 137 0 21 G mg/k g

Dilutio nFactor : 1.0 B . : LRE3 7 Matri x: WAST E : 12/19/0 9 PREPARATION - PRE P METHO D ANALYSI S DAT E BATCH # AST M D482-O0 a 01/11-01/13/l O 001120 8 MDL : 5 1 AST M D240-0 2 01/12/1 0 001204 8

MD L : 1 3 0 KNO X WC-001 6 01/11-01/15/1 0 001104 4 MD L : 6 5 NOTB(S ) : R L Reportin

g Limi t B Est'unsie

d result . Resul ti s les s tha n RL .



### VES01921 97 2

AECOM , In c Clien t Sampl e ID : LBTU-U4-M23A-R 3

Genera l Chemistry Lo t -Sampl e # . . . : H9L210404-00 6 Wor k Orde r #... : LRE3 8 Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE

R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH S As hConten t 335 0 20 0 mg/k g fiSTM

D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c 24 6 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e . Dilutio nFactor : 1 MDL : 13 0 Tota l Chlorin e 167 0 21 6 mg/kg KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 8 MDL : 6 5 NOT E (S ) : R L Reportin

g Limit B Estimate

d result . Resul ti s les s tha n RL .



### VES01922 07 3

AECOM , In c Clien t Sampl e ID : SF-U4-M23A-R 1

Genera l Chemistr y Lot-Sampl e # : H9L210404-00 7 Wor k Orde r ft...: LRE4 C Matri x: WAST E Dat e Sampled . .. : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 160 0 20 0 mg/k g AST M D482-00 a 01/11-01/13/1 0 001120 3 Dilutio nFactor : 1 MDL : 5 1 Gros s Calorifi c 939 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 1 3 0 Tota l Chlorin e 124 0 25 2 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.2 6 MD L : 7 6



### VES01922 17 4

' AECOM , In c Clien t Sampl e ID : SF-TT4-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L210404-00 8 Wor k Orde r : LRE4 D Matri x: WAST E Dat e Sampled . .. : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H ft As hConten t 289 0 20 0 mg/kg AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : S i Gros s Calorifi c 991 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 222 0 26 6 mg/k g KNO XWC-001 6 Ol/ll-Ol/15/l O 001104 4 Dilutio nFactor : 1.3 3 MD L i 8 0



### VES01922 27 5

AECOM , In c Clien t Sampl e ID : SF-U4-M23A-R 3

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-00 9 Wor k Orde r #... : LRE4 F Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 192 0 20 0 mg/k g AST M D482-00 a 01/11-01/13/1 0 001120 B Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 977 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MDL : 13 0 Tota L Chlorin e 144 0 25 8 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.2 9 MD L : 7 7



### VES01922 37 6

AECOM , In c Clien t Sampl e ID : CS-U4-M23A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L210404-01 0 Wor k Orde r #.. . : LRE4 G Matri x: SOLI D Dat e Sampled... : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 69900 0 20 0 mg/kg AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : l MDL : s i Gros s Calorifi c N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L . : 13 0 • Tota l Chlorin e 22 4 20 4 mg/kg KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 2 MDL . : 6 1



### VES01922 47 7

AECOM , In c Clien t Sampl e ID : CS-U4-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L210404-Oi l Wor k Orde r #.. . : LRE4 H Matri x: SOLI D Dat e Sampled . . . : 12/17/0 9 Dat e Received . . : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T RL ; UNIT S METHO D ANALYSI S DAT E BATCH g As hConten t 74600 0 20 0 mg/kg AST M D482-O0 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e N D 20 8 mg/k g KNO

X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor ; 1.0 4 MD L : 6 2



### VES01922 57 8

AECOM , In c Clien t Sampl e ID : CS-U4-M23A-R 3

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-01 2 Wor k Orde r #.. . : LRE4 J Matri x: SOLI D Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T Ri o UNIT S METHO D ANALYSI S DAT S BATC H # As hConten t 73700 0 20 0 mg/kg AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MDL : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MDL : 1 3 0 Tota l Chlorin e 14 6 B 20 0 mg/kg KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MD L : 6 0 NOTECS ) : RL Repottin

g Limit B Estimate

d result . Resul ti s les s tha n RL .



### VES01922 67 9

AECOM , In c Clien t Sampl e ID : BS-U4-M23A-R 1

Genera l Chemistr y Lot-Sampl e #- - - : H9L210404-01 3 . Wor k Orde r #.. . Dat e Sampled-.. : 12/16/0 9 Dat e Received. .
PARAMETER As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R L UNIT S 72500 0 20 0 mg/k g

Dilutio nFactor : 1 21 5 B 180 0 BTU/l b

Dilutio nFactor : 1 65 0 20 8 mg/k g

Dilutio nFactor : 1.0 4 LRE4 K 12/19/0 9 Matrix . SOLI D

_METHO

D AST M D482-O0 a MD L : 5 1 AST M D5865-0 0
MD L : 13 0 KNO X WC-001 6 MD L : 6 2 PREPARATION - PRE P ANALYSI S DAT E BATCH # 01/05-01/07/1 0 000527 4 01/13/1 0 001302 8
01/07-01/14/1 0 000703 6 NOTE(S ) : RL Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .



### VES01922 78 0

AECOM , In c Clien t Sampl e ID : BS-U4-M23A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L210404-01 4 Wor k Orde r : LRE4 L Matri x: SOLI D Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 77600 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 19 8 B 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 VaLn e Dilutio nFactor : 1 MDL : 13 0 Tota l Chlorin e 51 7 20 0 mg/kg KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MDL : 6 0 NOTB(S ) : R L Rearin g Limi

t B Estimate

d result . Resul ti s les s tha n RL .



### VES01922 88 1

AECOM , In c Clien t Sampl e ID : BS-U4-M23A-R 3

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-01 5 Wor k Orde r #... : LRE4 M Matri x: SOLI D Dat e Sampled . .. : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 79400 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 22 9 20 2 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 1 • MD L : 6 1



### VES01922 98 2

AECOM , In c Clien t Sampl e ID : HBTU-U4-M26A-R 1

Genera l Chemistr y L o t - Sampl e #-.. : H9L210404-01 6 Wor k Orde r #.. . : LRE4 N Matri x: WAST E Dat e Sampled . .. : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S . METHO D ANALYSI S DAT E BATCH # As hConten t 1320 0 20 0 mg/k g AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 900 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1250 0 119 0 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 5.9 4 MD L : 36 0



### VES01923 08 3

AECOM , In c Clien t Sampl e ID : HBTU-U4-M26A-R 2

Genera l Chemistr y Lot-Sampl e #... : H9L210404-01 7 Wor k Orde r #.. . : LRE4 P Matri x... : WAST E Dat e Sampled... : 12/17/0 9 Dat e Received.. : .12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 317 0 20 0 mg/k g AST M D482-O0 a Ol/ll-Ol/13/l O 001120 8 Dilutio nFactor : 1 HD L : S I Gros s Calorifi c 864 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MDL... , : 13 0 Tota l Chlorin e 247 0 27 0 mg/k g KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.3 5 MD L : 8 1



### VES01923 18 4

Lot-Sampl e #. . Dat e Sampled. . PARAMETE R AECOM , In c Clien t Sampl e ZD : HBTU-U4-M26A-R 3

Genera l Chemistr y H9L210404-01 8 Wor k Orde r #.. . 12/18/0 9 Dat e Received. . RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 329 0 20 0 mg/kg Dilutio nFactor : 1 866 0 180 0 BTU/l b

Dilutio nFactor : 1 231 0 24 0 mg/kg

Dilutio nFactor : 1. 2 LRE4 Q 12/19/0 9 Matri x: WAST E

_METHO

D AST M D482-00 a MD L : 5 1 AST M D240-0 2
MD L : 1 3 0 KNO X WC-001 6 MD L : 7 2 PREPARATION - PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01923 28 5

AECOM , In c Clien t Sampl e ID : LBTU-U4-M 2 6A-R 1

Genera l Cheinistr y Lot-Sampl e #... : H9L210404-01 9 Wor k Orde r #... : LRE4 R Dat e Sample d : 12/16/0 9 Dat e Received.. : 12/19/0 9 Matri x- . WAST E

PARAMETE R RESUL T R L UNIT S Ash . Conten t
Gros s Calorifi c Vala e
Tota l Chlorin e 266 0 20 0 mg/k g Dilutio nFactor : 1 , 25 8 B 180 0 BT0/l b

Dilutio nFactor : 1 125 0 21 2 mg/k g

Dilutio nFactor : 1.0 6 _METHO D AST M D482-O0 a MDL : 5 1 ASTM D240-0 2
MD L : 13 0 KNO X WC-001 6 MD L : 6 4 PREPARATION - PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4 NOTE(S) : R L Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .



### VES01923 38 6

AECOM , In c Clien t Sampl e ID : LBTO-U4-M26A-R 2

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-02 0 Wor k Orde r #.. . : LRE4 T Matri x: WAST E Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 277 0 20 0 mg/k g AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 25 1 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 131 0 21 0 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 5 MDL : 6 3 NOTE(S ) : R L Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .

i

I



### VES01923 48 7

AECOM , In c Clien t Sampl e ID : L_rU-U4-M26A-R 3

Genera l Chemistr y Lot-Sampl e #... : H9L210404-02 1 Wor k Orde r #... : LRE4 V Matri x: WAST E Dat e Sample d : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 415 0 20 0 mg/k g AST M D482-O0 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 18 9 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1S2 0 20 8 mg/k g KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 4 MD L : 6 2 NOTE(S ) : RL Reportin

g Limi t B Estimaie

d result . Resul ti s les s tha n RL .



### VES01923 58 8

AECOM , In c Clien t Sampl e ID : SF-U4-M26A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L210404-02 2 Wor k Orde r #.. . LRE4 W Matri x: WAST E Dat e Sampled .
PARAMETE R 12/15/0 9

RESUL T Dat e Received.. : 12/19/0 9

R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 148 0 20 0 mg/k g Dilutio nFactor : 1 1010 0 180 0 BTU/l b

Dilutio nFactor : 1 112 0 2S 0 mg/k g

Dilutio nFactor : 1. 3 METHO D AST M D482-00 a

. MD L : 5 1 ASTM D240-0 2

MD L : 13 0 KNO X WC-001 6 MD L : 7 8 PREPARATION - PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/19/1 0 001104 4



### VES01923 68 9

AECOM , In c Clien t Sampl e ID : SF-U4-M26A-R 2

Genera l Chemistr y lot-Sampl e #.. . : H9L210404-02 3 Wor k Orde r : LRE4 XMatri x: WASTE Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 457 0 20 0 mg/k g ASTM D482-O0 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MDL : 5 1 Gros s Calorifi c 943 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 361 0 25 2 mg/k g KNO X WC-001 6 01/11-01/19/1 0 001104 4 Dilutio nFactor : 1.2 6 MD L : 7 6



### VES01923 79 0

Lot-Sampl e #. . Dat e Sampled . .
PARAMETE R AECOM , In c Clien t Sampl e ID : SF-D4-M26A-R 3

Genera l Chemistr y H9L210404-02 4 Wor k Orde r #... : LRE4 0 Matri x: WAST E 12/18/0 9

RESUL T Dat e Received .

R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 182 0 20 0 mg/k g Dilutio nFactor ; 1 982 0 180 0 BTU/l b

Dilutio nFactor : 1 140 0 25 2 rag/kg

Dilutio nFactor : 1.2 6 12/19/0 9

METHO D AST M D482-00 a MD L : 5 1 ASTM D240-0 2
MDL : 13 0 KNO X WC-001 6 MDL : 7 6 PREPARATION - PRE P ANALYSI S DAT E BATCH # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01923 89 1

AECOM , In c Clien t Sampl e ID : CS-U4-M26A-R 1

Genera l Chemistr y Lot-Sampl e #... : H9L210404-02 5 Wor k Orde r #... : LRE4 3 Dat e Sampled . . . : 12/16/0 9 Dat e Received.. : 12/19/0 9

PARAMETE R As hConten t Matrxx . SOLI D

RESUL T RL UNIT S METHO D PREPARATION - PRE P

ANALYSI S DAT E BATCH # 78500 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MDL -.5 1 Gros s Calorifi c Valu e N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e N D 20 8 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 4 MDL : 6 2



### VES01923 99 2

AECOM , In c Clien t Sampl e ID : CS-04-M26A-R 2

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-02 6 Wor k Orde r : LRE4 4 Matri x: SOLI D Dat e SSampled . . . : 12/17/0 9 Dat e Received... - 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 85700 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e N D 21 2 mg/kg KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 5 MD L : 6 4



### VES01924 09 3

AECOM , In c Clien t Sampl e ID : CS-tT4-M26A-R 3

Genera l Chemistr y L o t - Sampl e #... : H9L210404-02 7 Wor k Orde r : LRE4 5 Matri x: SOLI D Dat e Sample d : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H ff As hConten t 74400 0 20 0 mg/k g AST M D482-00 a 01/0S-01/07/1 O 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 Vala e Dilutio nFactor : 1 MDL : 13 0 Tota l Chlorin e N D 20 8 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 4 MDL : 6 2



### VES01924 19 4

AECOM , In c Clien t Sampl e XD : BS-U4-M26A-R 1

Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-02 8 Wor k Orde r #.. . : LRE4 6 Matri x: SOLI D Dat e Sampled... : 12/16/0 9 Dat e Received. . : 12/19/0 9 PREPARATION - PRE P PARAMETE R RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH j ? A s hConten t 80800 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 20 0 B 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MDL : 13 0 Tota l Chlorin e 43 3 20 2 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 1 MD L : 6 1 NOTE(S ) : R L Reportin

g Limit B Estimate

d result . Resul ti s les s tha n RL .



### VES01924 29 5

AECOM , In c Clien t Sampl e ID : BS-U4-M26A-R 2

Genexa l Chemistr y Lot-Sampl e #.. . : H9L210404-02 9 Wor k Orde r #... : LRE4 7 Matri x: SOLI D Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 80100 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MDL : 5 1 Gros s Calorifi c 19 6 B 180 0 BTU/l bASTM D5865-0 0 01/13/1 0 001302 8 "Valu e Dilutio nFactor : 1 MDL : 13 0 Tota l Chlorin e 97 6 21 6 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 8 MD L : 5 5 KOTB(S ) : RL Repinin

g Limi t B Estimate

d result . Resul ti s les s lin n RL .



### VES01924 39 6

AECOM , In c Clien t Sampl e ID : BS-U4-M26A-R 3

Genera l Chemistr y Lot-Sampl e #... : H9L210404-03 0 Wor k Orde r #...- . LRE4 8 Matri x: SOLI D Dat e Sample d : 12/18/0 9 Dat e Received.. ; 12/19/0 9 PREPARATION - PRE P PARAMETER RESUL T R L UNIT S METHO D ANALYSI S DAT E BATCH # As hConten t 79700 0 20 0 mg/k g AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MDL : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 61 0 20 0 mg/k g KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MD L : S O



### VES01924 49 7



# Q C Summar

y

VES01924 59 8

METHO D BLAN KEEPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: SOLI D REPORTIN

G PREPARATION - PRE P PARAMETERRESUL T LIMI T UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t Wor k Orde r # : LRVT31A A M B Lot-Sampl e # : HOA050000-27 4 N D 20 0 mg/k g ASTM

D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 Tota l Chlorin e Wor k Orde r LRW7S1A A M B Lot-Sampl e # : HOA070000-03 6 N D 20 0 mg/kg KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 NOT E |S ) : Calculation

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



### VES01924 69 9

METHO D BLAN KEEPOR T Genera l Chemistr y Clien t Lo t # . . . : H9L21040 4 Matri x: WAST E REPORTIN

G PREPARATION - PRE P PARAMETE RRESUL T LIMI T UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t Wor k Orde r # : LR2KQ1A A M B Lot-Sampl e # : HQA110000-20 8 N D 20 0 mg/kg AST M D482-00 a Ol/U-01/13/1 0 001120 8 Dilutio nFactor : 1 Tota l Chlorin e Work Orde r # : LR2CJ1A A M B Lot-Sampl e # : HQA110000-04 4 N D 20 0 mg/kg KNO XWC-001 5 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1 NOTB ( S ) : Calculaiion

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01924 710 0

LABORATOR

YCONTRO

L SAMPL E EVALUATIO N REPOR T Genera l Chemistr y Lot-Sairrpl e # . . H9L21040 4 Matrix .
PARAMETER As hConten t PERCENT

RECOVER

Y 10 1 10 1 RECOVER Y LIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E : SOLI D

PRE P BATC H # WO#:LRVT31AC-LCS/LRVT31AD-LCS D LC S Lot-Sample# : H0A050OO0-27 4 (9 0 - 110 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 (9 0 - 110 ) 0.1 2 (0-10 ) ASTM D482-O0 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

10 0 W0#:LR4DC1AA-LCS/LR4DC1AC-LCS D LC S Lot-Sample# : H0A130OO0-02 8

(9 8 - 102 ) AST M D58S5-0 0 (9 8 - 102 ) 0.0 6 (0-2.0 ) AST M D5865-0 0 Dilutio nFactor : 1 01/13/1 0 01/13/1 0 001302 8

001302 8

NOTE(S) : Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01924 810 1

LABORATOR

YCONTROL SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e #.. . : H9L21040 4 Matri x: SOLI D

SPIK E MEASURE

D PERCN T PREPARATION - PRE P PARAMETER AMOUN T AMOUN

T UNIT S RECVR YRPD METHO

D ANALYSI S DAT E BATCH # As hConten t WO#:LRVT31AC-LCS/LRVT31AD-LCS D LC S Lot-SampleS : H0A05OO00-27 4

400 0 405 0 mg/kg 10 1 AST M D482-O0 a 01/05-01/07/1 0 000527 4 400 0 406 0 mg/kg 10 1 0.1 2 ASTM D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 Gros s Calorifi c WO#:LR4DC1AA-LCS/LR4DC1AC-LCS D LC S Lot-Sample# : HOA130000-02 8 Valu e 1140 0 1140 0 BTU/l b10 0 AST M D5865-0 0 01/13/1 0 001302 8 1140 0 1140 0 BTU/l b10 0 0.0 6 AST M D5865-0 0 01/13/1 0 001302 8 Dilutio nFactor : 1 NOTECS ) : ' Calculaiion

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



### VES01924 910 2

LaBORATOR

YCONTROL SAMPL E EVALUATIO N REPOR T Genera l C_emistr y Clien t Lo t # : H9L21040 4 Matrix . . : SOLI D PERCENT RECOVER YPREPARATION - PRE P PARAMETER RECOVER YLIMIT S METHO D __ _ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LRW761A C LC S Lot-SampleS : HOA070000-03 6 10 1 (8 0 - 120 ) KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 5 NOTE(S ) : Cslculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01925 010 3

LABORATOR

YCONTRO L SAMPL E DAT A REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: SOLI D

SPIK E MEASURED PERCNT PREPARATION - PRE P PARAMETER AMOUN T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LRW761A C LC S Lot-Sample* : HOA070000-03 6 1000 0 1010 0 mg/k g 10 1 KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 5 NOTE(S ) : Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01925 110 4

LABORATOR

YCOHTRO

L SAMPL E EVALUATIO N REPORT Genera l Cnemistr y Lot-Sampl e #... : H9L21040 4 Matrxx .
PARAMETER As hConten t PERCEN T RECOVER

Y 9 8 10 1 RECOVER Y LIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E : WAST E

PRE P BATC H # W0#:LR2KQ1AC-LCS/LR2KQ1AD-LCS D LC S Lot-Sample?* : H0A110OO0-2O 6 (9 0 - 110 ) AST M D482-00 a 0l/ll-0l/l3/l 0 001120 8 (9 0 - 110 ) 2. 4 (0-10 ) AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 Gros s Calorifi c Valu e io o

10 0 WO#:LR2981AA-LCS/LR2981AC-LCS D LC S Lot-Samples : H0A120O00-04 8

(9 8 - 102 ) (9 8 - 102 ) 0.0 2 (0-2.0 ) Dilutio nFactor : 1 AST M D24O-0 2 AST M D240-0 2 01/12/1 0 01/12/1 0 001204 8

001204 8

NOTE(S ) Calculation

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### VES01925 210 5

LABORATOR

YCONTROL SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e #.. . : H9L21040 4 Matri x: WAST E

SPIK E MEASURE

D PERCN T PREPARATION - PRE P PARAMETE R AMOUN T AMOUN

T UNIT S RECVR YRPD METHO

D ANALYSI S DAT E BATC H # As hConten t W0#:LR2KQ1AC-LCS/LR2KQ1AD-LCS D LC S Lot-Sample# : HOA110000-20 8

40O 0 393 0 mg/k g 9 8 AST M D482-00 a 01/11-01/13/1 0 001120 8 400 0 403 0 mg/kg 10 1 2. 4 AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 Gros s Calorifi c WO#:LR2981AA-LCS/LR2981AC-LCS D LC S Lot-Sample# : HOA120000-04 8 Vala e 2060 0 2050 0 BTU/l b10 0 AST M D240-0 2 01/12/1 0 001204 8 2060 0 2050 0 BTU/l b10 0 0.0 2 AST M D240-0 2 01/12/1 0 001204 8 Dilutio nFactor : 1 NOTE(S ) : Calculaiion

s ar e performe

d befor e roundin g i o avoi d round-of

f error s i n calculate

d results .



### VES01925 310 6

LABORATOR

YCONTROL SAMPL E EVALUATIO N REPORT Genera l Chemistr y Clien t Lo t #-.. : H9L21040 4 Matri xt WAST E PERCENT RECOVER YPREPARATION - PRE P PARAMETE R RECOVER YLIMIT S METHO D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LR2CJ1A C LC S Lot-Sample* : HOA110000-04 4 10 4 (8 0 - 120 ) KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : S NOTE(S ) : . Caloularion

s ar e perfomie

d befor e roundin g l o avoi d round-of

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### VES01925 410 7

LABORATOR

YCONTRO L SAMPL E DAT A REPORT Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: WAST E

SPIK E MEASURE

D PERCNT PREPARATION - PRE P PARAMETER AMOUN T AMOUN

T UNIT S RECVRYMETHO D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LR2CJ1A C LC S Lot-Sample# : HOA110000-04 4

1000 0 1040 0 mg/k g 10 4 KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 5 NOTE(S ) : — Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01925 510 8

MATRI XSPIK E SAMPL E EVALUATIO N REPORT

Clien t Lo t # . . . Dat e Sampled. . : H9L21040 4 : 12/18/0 9 Genera l Chemistr y
Dat e Received.. : 12/19/0 9

PARAMETER Tota l Chlorin e

10 7 10 6 PERCENT RECOVER Y RECOVER

YLIMIT S RPD RPD LIMIT S METHO

D Matri x: WAST E

PREPARATION ANALYSI S DAT E PRE P

BATC H # WO# : LRE351AG-MS/LRE351AH-MS D M S Lot-Sampl e # : H9L210404-00 3 (8 0 - 120 ) KNOX'WC-001 6 01/11-01/15/1 0 001104 4 (8 0 - 120 ) 2. 5 (0-10 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 8. 3 NOT E (S ) : Calculation

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



### VES01925 610 9

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: WAST E Dat e Sampled . .. : 12/18/0 9 Dat e Received.. : 12/19/0 9

SAMPL E SPIK E MEASR D PERCNT PREPARATION - PRE P PARAMETE R AMOUN T AM T AMOUN

T UNIT S RECVR YRPD METHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e W0# : LRE351AG-MS/LRE351AH-MS D M S Lot-Sampl e # : H9L21O404-O0 3 234 0 1560 0 2010 0 mg/kg 10 7 KNO X WC-001 6 01/11-01/15/1 0 001104 4 234 0 1620 0 1960 0 mg/kg 10 6 2. 5 KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFacto r -.8. 3 « NOT E IS)

: Calculation

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I



### VES01925 711 0

MATRI XSPIK E SAMPL E EVALUATIO N EEPOR T Genera l Chemistr y Clien t Lo t #.. . Dat e Sampled.. . : H9L21040 4 : 12/18/0 9 Dat e Received. . 2.2/19/0 9

PARAMETE R Tota l Chlorin e

9 7 10 0 PERCENT RECOVER Y RECOVER

YLIMIT S RP

D RPD LIMIT S METHO

D Matri x: SOLI D

PREPARATION ANALYSI S DAT E PRE P

BATC H # W0# : LRE4J1AG-MS/LRE4J1AH-MS D M S Lot-Sampl e # : H9L210404-01 2 (8 0 - 120 ) KNO XWC-001 6 01/07-01/14/1 0 000703 6 (8 0 - 120 ) 3. 4 (0-10 ) KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 4 . 9 S NOTE(S ) : Calculaiion

s ar e performe

d befor e roundin g l o avoi d round-of

f error s i n calculate

d results .



### VES01925 811 1

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l _emistr y Clien t Lo t #. . , Dat e Sampled . . H9L21040 4 12/18/0 9 Dat e Received.. : 12/19/0 9 Matrix . SOLI D

SAMPL E SPIK E PARAMETE R AMODN T AM T Tota l Chlorin e

14 6 992 0 14 6 1000 0 MEASR D AMOUN T UNIT S PERCNT

RECVR YRPD METHO

D PREPARATION - PRE P

ANALYSI S DAT E BATC H WO# : LRE4J1AG-MS/LRE4J1AH-MS D M S Lot-Sampl e # : H9L210404-01 2 982 0 mg/k g 9 7 KNO X WC-001 6 01/07-01/14/1 0 000703 6 1020 0 mg/k g 10 0 3. 4 KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.9 6 NOT E (S) : Calculation

s ar e performe

d befor e roundin

s t o avoi d round-of

f error s i n calculaie

d results .



### VES01925 911 2

SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l <_ien_str y Clien t Lo t #... : H9L21040 4 Wor k Orde r #.... - LRE35-SM P Matri x: WAST E LRE35-DU P Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 DUPLICAT E RPD PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RP D LIMI T METHO D ANALYSI S DAT E BATC H # Gros s Calorifi c SD Lot-Sampl e # : H9L210404-00 3 Valu e 851 0 8S2 0 BTU/l b1. 3 (0-10 ) ASTM D240-0 2 01/12/1 0 001204 8 Dilutio nFactor : 1 .As hConten t S D Lot-Sampl e # : H9L210404-00 3 308 0 305 0 mg/kg 1. 1 (0-10 ) ASTM D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e # : H9L210404-00 3 234 0 235 0 mg/k g 0.1 3 (0-10 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.S 9



### VES01926 011 3

SAMPL E DUPLICAT E EVALUATIO N REPORT Genera l Chemistr y Clien t Lo t #..- : H9L21040 4 Wor k Orde r # . . . : LRE4J-SM P Matri x: SOLI D LRE4J-DU P Dat e Sampled... : 12/18/0 9 Dat e Received . . : 12/19/0 9 DUPLICAT E RPD PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RPD LIMI T METHO D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L210404-01 2 Valu e N

D N

D BTU/l b0 (0-10 ) AST M D58S5-0 0 01/13/1 0 001302 8 Dilutio nFactor : 1 As hConten t S D Lot-Sampl e # : H9L210404-01 2

73700 0 74100 0 mg/kg 0.5 6 (0-10 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor- . 1 Tota l Chlorin e S D Lot-Sampl e #: • H9L210404-01 2

14 6 B 14 9 B mg/kg 1. 9 (0-10 ) KNO X WC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 NOT E (S ) : ; ' Calculation

s ar e performe

d befor e roundin

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d result . Resul ti s les s tha n RL .



### VES01926 111 4

SAMPL E DDPLICAT E EVALUATIO N REPOR T Genera l Cherrristr y Clien t Lo t #... : H9L21040 4 Wor k Orde r # . . . : LRE4P-SM P Matri x: WAST E LRE4P-DU P Dat e Sample d : 12/17/0 9 Dat e Received.. : 12/19/0 9 DUPLICAT E RPD PREPARATION - PRE P PARA M RESUL T RESUL T UNIT S RP D LIMI T METHO D ANALYSI S DAT E BATC H # Tota l Chlorin e S D Lot-Sampl e # : H9L210404-01 7 247 0 253 0 mg/kg 2. 5 (0-10 ) KNO X WC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.3 5



### VES01926 211 7

Clien t Lo t #... : H9L21040 4 Dat e Sampled . 12/18/0 9 SAMPL E DDPLICAT E EVALUATIO N REPOR T Genera l C_emistr y Wor k Orde r #... : LRE48-SM P LRE48-DU P . Dat e Received.. : 12/19/0 9 Matrix . SOLI D

PARA M RESUL T Tota l Chlorin e SI O DUPLICAT E

RESUL T UNIT S RPD RP D LIMI T METHOD . 24 5 mg/kg 8 5

Dilutio nFactor : 1 PREPARATION - PRE P ANALYSI S DAT E BATC H # SD Lot-Sampl e # : H9L210404-03 0 (0-10 ) KNO

X WC-001 6 01/07-01/14/1 0 000703 6

### VES01926 4

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### VES01926 5T R I For mR| Envirofact s | U S EP A Pag e 2 of 6

NAM E STREE T CIT Y COUNT

Y STAT E ZI

PCODE VEOLI A E S TECHNICA

L SOLUTION

S LL C 7 MOBIL

E AV E SAUGE T ST CLAI R I L 62201106

9
BI A Triba l Code Trib

e N O DAT A N O DAT A Mailin g Informatio

n NAM E STREE T CIT Y STAT

E ilPCOD E VEOLI A E S TECHNICA

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S LL C 7 MOBIL

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L 62201-106

9 PROVINC

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Y (NO N - US 1 N O DAT A N

O DAT A 4. 2 Facilit

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Y YE S N

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t NAM E PHON

E DENNI S WARCHO

L 618271280

4 4. 5 NAIC

S Codes NAIC S COD E PRIMARYlNAIC S CODE DESCRIPTIO

N 56221 1 YE S Hazardou s Wast e Treatmen

tan d Disposa

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s |OUN S NUMBER | 5 , Paren tCompan

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A ENVIRONMENTA

L SERVICES Paren tCompan

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: 14596812

4 PAR TII . CHEMICA L - SPECIFI C INFORMATIO N

DOCUMENT

CONTROL

NUMBER:

131321162725

8 Section 1 . Toxi

c Chemica

l Identit y 1. 1 CA S Number

: N45 8 1. 2 Toxi c Chemica

l o rChemica

l Categor y Name: MERCUR

Y COMPOUNDS 1 . 3 Generi

c Chemica

l Name: N

A 1. 4 Distributio

n o f Eac h Membe ro f Ih e Dioxi n an d Dioxi n lik e Compound

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http://oaspub.epa.gov/enviro/tri_forr ^ 12/15/201 4 

### VES01926 6T R I For mR I Envirofact s IU S EP A Pag e 3 o f 6

2. 1 Supplie

rProvide d Generi c Chemica

l Name : N

A Section 3 . Activitie

s an d Use s o f th e Toxic Chemica

l 3 . 1 Manufactur

e th e Toxi c Chemical : Produce : YE S Import : N O On-Sll

e Use/Processina : N

O Sale/Distribution : N

O BvDroducI

: N O ImDurltv

: YE S

3. 2 Proces s th e Toxi c Chemical : Reactant : N O Formulatio

n Component

: N O Articl e Component

; N O Reoackaaina ; N

O ImDuritv

; N O

3. 3 Otherwis

e Us e th e Toxi c Chemical : Chemica l Processin

g Aid : N O Manufacturfn

aAid : N O Ancillar

y o rOlhe rUse : YE S

Section 4. Maximu

m Amoun

to f th e Toxic Chemica

l Onsit e Durin g th e Calenda

rYea r Maximu m Chemica

l Amount : 0 t o 9 9 Section 6

. Quantit y o f th e Toxi c Chemica

l Enterin g eac h Environmenta

l Mediu m Onsit e 5 . 1 Fugitiv

e o rNon-Poin

tAi rEmission

s N A TOTA L RELEAS E (Dervear l UNI T OF MEASUR

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s 6. 2 Stac ko rPoin tAi rEmission

s N A TOTA

L RELEAS E (pe

rvear l UNI T OF MEASUR

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s t o Receivin

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s o rWate rBodie s N A STREAM/WATE RBOD Y NAM E TOTA L RELEAS E (Dervear l UNI T OF MEASUR

E BASI S O F ESTIMAT

E f * FRO M STORMWATE

R YE S N A 6.4, 1 Undergroun

d Injectio n Onsit e t o Class I Wells

, N A TOTAL RELEAS E (oe ryear ) UNI T OF MEASUR

EBASI S OF ESTIMAT

E YE S 6.4. 2 Undergroun

d Injectio n Onsit e t o Clas s ll- V Wells. N A TOTA L RELEAS E (pe r vear ) UNI T OF MEASUR

E BASI S O F ESTIMAT

E YE S 5. 5 Disposa

l t o Lan d Onsit e 6.5.1 A RCR A Subtitl e C Landfill

s N A TOTAL RELEAS E (pe rvear ) UNI T O F MEASUR

EBASI S OF ESTIMAT

E YE S

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s http://oaspub.epa.gov/enviro/tri_formr^_partone_v2.get_thisone?rpt_jear=2013&dcn_nu.. , 12/15/201 4 

### VES01926 7T R I For mR| Envirofact s | U S EP A

N & TOTA

L RELEAS E (pe

rvear )UNI T O F MEASUR

EBASI S OF ESTIMAT

E YE S 5.5. 2 Lan d Treatment/ARplicatjor

tFarmin g N A TOTAL RELEAS E (De r vear )UNI T OF MEASUR

E BASI S O F ESTIMAT

E YE S 5.5.3 A RCR A Subtitl e C Surfac

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s NA . TOTAL RELEAS E (De r vear t UNI T OF MEASUR

E BASI S OF ESTIMAT

E YE S 5.5.3 B Othe rSurfac e Impoundment

s N A TOTAL RELEAS E (pe r vear ) UNI T OF MEASUR

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E YE S 5.6, 4 Othe rDisposa

l N A [TOTA

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E BASI S OF ESTIMAT

E N O 0 Pound s 0 - Othe

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s Section 6

. Transfer

s o f th e Toxi c Chemica

l i n Waste s t o Off-Sit e Locations 6. 1 Discharge

s t o Publicl y Owne d Treatmen

tWork s (POTWs

) 1 - NAME : ADDRESS : CITY : STATE : COUNTY : ZI

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E BASI S OF ESTIMAT

E N O DAT A N O DAT A 6. 2 Transfer

s t o othe rOff-Sit e Location

s 1 RCR A Number

: ILD984S9346

1 Paren

tComDan

v Controlled : N

O Name : MILA

M RECYCLING & DISPOSA L Address : I5

5 AN D ILLINOI

S 20 3 N Citv : EAS T ST LOUI

S Stale : I L County : S T CLAI R Zi D Code : 6220

1 Countr y Cod e (No n - US) : Province :

OFFSIT E AMOUN

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2 RCR A Number

: MID00072483

1 Paren tCompan

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O Name : MICHIGA

N DISPOSA

L Address : 4935019 4 SERVICE DR

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### VES01926 8 Pag e 4 o f

6T R I For mRIEnvirofact s IU S EP A Pag e 5 o f 6

Cilv : BELLEVILL

E State : M l Countv : WAYN

E Zi

D Code : 4811 1 Countr y Cod e (No n - US) : Province :

OFFSITE AMOUN

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s onl y
3 RCR A Number

: WID00396714

8 Paren tCompan

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A E S TECHNICA

L SOLUTION

S LL C Address : W124N945 1 BOUNDAR

Y R D City : MENOMONE

E FALLS Slate : W I Countv : WAUKESH

A Zi D Code ; 5305

1 Countr v Cod e (No n - US) : Province :

OFFSIT E AMOUN TSEQUENC E TOTA L TRANSFER S (pe rvear ) UNI TO F MEASUR E BASI S O F ESTIMAT E W AST E MANAGEMEN TTYP E 1 168 2 Pound

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1 Paren

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y Estimate : Equa

l t o o rgreate rtha n 0 % bu tles s tha n o requa l t o 50 % http://oaspub.epa.gov/enviro/tri_f o 12/15/201 4 

### VES01926 9T R I For mR| Envirofact s | U S EP A Pag e 6 o f 6

7A.3a. Wast

e Slream : WASTEWATE R 7A.3b.WASTE TREATMENT METHODIS ) SEQUENC E 1 H04 0 - Incineratio

n - therma

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l t o o rgreate rtha n 0 % bu tles s tha n o requa l t o 50 % 7A.4a . Wast

e Slream : GASEOU S 7A.4 b WAST E TREATMENT METHODIS ) SEQUENC E 1 H04 0 - Incineratio

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e Treatmen

tEfficienc

y Estimate: Equa

l t o o rgreate rtha n 0 % bu tles s tha n o requa l t o 50 % Section 7B . On-Sit

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http://oaspub.epa.gov/enviro/tri_formrjpartone_v2.get_thisone?ipt_year=2013&dcn_nu.. . 12/15/201 4 

### VES01927 0

# VES019271.pd fJosep h M . Kellmeye

r P314.552,616

6 F 314.552.716

6 jkellmeyer@thompsoncoburn.cor n



### Decembe r

26,201 3 Georg e T . Czernia k Director , Ai r

an dRadiatio n Division , Regio n 5 Unite dStat e Environmenta l Protectio n Agenc y 7 7 Wes t Jackso n Boulevar d Chicago , Illinoi s 6060 4 Re : Reques t

T o Provid e Informatio n Pursuan t t o th e Clea n Ai r

Ac t Date dDecembe r

10,201 3 Dea r Mr . Czerniak : A s yo u know , thi s firmrepresent s Veoli aE S Technica l Solutions , L.L.C . ("Veolia") . O n o r abou t Decembe r

12,2013 , Veoli areceive dth e above-reference dInformatio n Requests , acop y o f whic hi s enclose da s Ex . A . Th e Infonnatio n Request s see k informatio n unde r

Sectio n 114(a ) o f th e Clea n Ai r

Ac t an drequir e Veoli at o respon dwtthi n 1 4 day s o f receipt . Upo n receivin g th e requests , Veoli aworke ddiligentl y t o compil e an dproduc e th e requeste ddat aan dformulat e response s t o th e Agency' s inquirie s b y th e deadline . Veolia' s narrativ e respons e an daccompanyin g dat aar e enclose dwit hthi s cove r lette r an dare bein g produce dsubjec t t o an dunde r

th e followin g objections : 1 . Veoli aobject s t o th e Informatio n Request s t o th e exten t tha t an y instructio n o r reques t i s overl y broad , vagu e o r ambiguous , o r

otherwis e no t

i n accordanc e wit h applicabl e law . 2 . Veoli aobject s t o th e Informatio n Request s t o th e exten t an y instructio n o r

reques t i s differen t

i n whol e o r

i n part frominformatio n Veolia' s competitor s ar e require d t o provid e t o th e Agency . T o th e exten t suc hdifference s exist , Veoli ai s place dat adisadvantag e tha t

violate s it s equa l protectio n an ddu e proces s rights . 3 . Veoli aobject s t o th e Informatio n Request s t o th e exten t an y instructio n o r

reques t arbitraril y an dcapriciousl y request s informatio n whic hi s irrelevan t o r informatio n that

ha s alread y bee n collecte db y th e Agenc y albei t i n adifferen t fashio n o r

usin g adifferen t

method . 4 . Veoli aobject s t o th e Informatio n Request s an dreserve s it s righ t t o withhol d informatio n t o th e exten t an y reques t

seek s informatio n o r

material s protecte db y Thompso n Cobu m LL P | Attorney s at La w| On e U S Ban k Plaz a | St . Louis , Missour i 6310 1 P 314.552.600 0 | F 314.552.700 0 | www.thompsoncoburn.co m Chicag o * St

. Loui s • Souther

n Illinoi s * Washington , D.C , 

### THOMPSO N COBURN l l p



### VES01927 1Decembe r 26,201 3 Pag e 2 th e attorney-clien t privilege , th e wor k

produc t doctrin e o r

an y othe r

applicabl e privileges . Whil e Veoli asubmit s it s respons e subjec t t o th e foregoin g genera l objection s an dqualifications , Veolia , nevertheless , ha s attempte dt o provid e th e requeste dinformatio n i n goo dfait han dha s expende dsignifican t

tim e an dresource s i n doin g so . Veoli areserve s th e righ t t o provid e additiona l informatio n i n th e futur e and/o r t o furthe r

amen d o r supplemen t

it s response . I f

yo u hav e an y question s o r concern s regardin g thi s matter , pleas e contac t th e undersigned . Ver y trul y yours , Thompso n Cobu mLL P

JMK /

Enclosure sUNITE D STATE S ENVIRONMENTA LPROTECTIO NAGENC Y REGION S I NTH EMATTE ROF : Veoli aEnvironmenta l Service s "WT Mobfl e Aveuii e •'

• * - —,„,„„..,.,.„„,„,, , , „.,.„.,.,„„.,., . Sauget , Illinoi s 6220 1 ATTENTION : Dou g Harri s Genera l Manage r

Reaoes t t o Provid e Informatio n Pursuan t t o th e Clea n Ai r

Ac t Th e U.S , Envirorimenta l Protectio n Agenc y i s requirin g Veoli aEnvironmenta l Service s (Veoli ao r

j'ou ) to submi t

certai n informatio n abou t you r facilit y at

# 7 Mobil e Avenue , Sauget , Illinois . Appendi x A provide s th e instruction s neede dto answe r thi s informatio n request , mclud^'mstraction s fo r electroni c submissions . Appendi x B specifie s th e ir&nnatio n tha t yo u mus t submi t Yo u mus t

sen dthi s informatio n t o u s withi n 1 4 calendar day s afte r

yo u receiv e thi s reques t W e ar e issum g thi s formatio n reques t under sectio n 114(a ) o f

th e Clea n Ai r

Ac t (the Act) , 4 2 U.S.C . § 7414(a) . Sectio n 114(a ) authorize s th e Adrninistrato r o f EP Ato requir e th e submissio n o f

information.

- Th e Administcato r ha s delegate dthi s authorit y t o th e Directo r o f the Ai r an dRadiatio n Division , Regio n 5 , Veoli aown s an doperate s hazardou s waste ineinerator s a t th e Sauget , Blinoi s facility . W e are requestin g thi s informatio n t o determin e whether you r emissio n sourc e i s complyin g wit h th e Hazardou s Wast e Combusto r MACT .



### VES01927 3Veoli amus t sen dal l requiredinformatio n to : Attn : Complianc e Tracker , AE-17 J A i r Enforcemen t

an dComplianc e Assuranc e Branc h U.S . Environmenta l Protection . Agenc y Regio n 5 "^7 '~^B £1^3^n'B6vSiCvwSL " v TM~~- v -••-•- , "-'TM~•• ; Chicago , Hlinoi s 6060 4 Veoli amus t

submi t al l require dinfonnatio n unde r a n authorize dsignatur e wit hth e followin g certification : I certify unde r

penalt y o f

la w that I hav e examine dan da mfanrilia r with'th e infonnatio n i nth e enclose ddocuments , mcludin g al l attachments . Base do n m y inquir y o f

thos e individual s wit hprimar y responsibilit y fo r obtainin g th e information , I certif

y tha t th e statement s an dinformatio n are , t o th e bes t o f m y knowledg e an dbehef, tru e an dcomplete . I a maware tha t there are significan t penaltie s fo r

knowingl y submittin g fals e statement s an dinformation , mcludin g th e possibilit y o f

fines o r imprisonmen t

pursuan t

t o Sectio n 113(c)(2 ) ofth e Clea n Ai r Ac t an d1 8 U.S.C . § § 100 1 an d1341 . A s explaine dmor e full y i n Appendi x C , yo u ma y asser t aclai mo f

busines s rarifidentiality unde r

4 0 C.F.R . Par t

2 , Subpart

B fo r an y part ofth e informatio n yo u submi t to us . Informatio n subjec t to abusines s confidentialit y clai mi s availabl e t o m e publi c onl y t o th e extent , an db y mean s o f th e procedures , se

t fort hat 4 0 C.F.R . Par t

2 , Subpart

B . J f yo u do no t assert abusines s confidentialit y clai mwhe n yo u submi t th e Mormation , EP Ama y mak e thi s informatio n availabl e t o the publi c withou t furthe r notice . Yo u shoul db e aware , moreover , tha t pursuan t t o Sectio n 114(c ) ofth e CA Aan d4 0 C.F.R . § 2.301(a ) an d(f) , emission s data , standard s an dlimitation s ar e no t entitle dto confidentia l treatmen t an dshal l b e mad e availabl e to th e publi c notwiliistandin g an y assertio n o f abusines s confidentialit y claim . Appendi x C provide s additiona l informatio n regardin g th e meanin g an dscop e o f 1h e term"emission s data, "



### VES01927 4Thi s informatio n reques t i s no t subjectt o th e Paperwor k Reductio n Act , 4 4 U.S.C . § 350 1 etseq., becaus e i t

seek s collectio n o f

informatio n fro mspecifi c mdividual s o r entitie s as par

t o f a n adnnnistrativ e actio n o r investigation . We'mayuse'anym^ ^ civi l o r crimina l action . Failur e to compl y full y wit hthi s informatio n reques t ma y subjec t

Veoli at o a n enforcemen t

actio n unde r

Sectio n 11 3 ofth e CAA , 4 2 U.S.C . § 7413 . Y o u shoul ddirec t

an y question s about

thi s informatio n Reques t t o Shanno n Downe y a

t (312 ) 353-215 1 an ddownev.shannon@epa.go v o r Eleano r Kan e at (312 ) 353-484 0 an d kane.eleanor©,epa.gov .

Dat e

i•
3



### VES01927 5Appendi x A Whe n providin g th e mformatio n requeste di nAppendi x B , us e th e foUowin g instruction s an d definitions .

_Instnictiori s 1 . Provid e aseparat e ri^rrativ e respons e to eac hquestio n an dsubpart o f aquestio n se

t fort h i nAppendi x B . 2 . Preced e eac hanswer wit hfh e number

o f th e questio n to whic hi t correspond s an didentify th e person(s ) wh o provide dinformatio n use do r considere di n respondin g t o tha t question , a s wel l as eac hperso n consulte di n th e preparatio n o f that response . 3 . Indicat e o n eac hdocument produced , or

i n som e othe r

reasonabl e manner , th e numbe r o f th e questio n to whic hi t corresponds . 4 . .Whe n arespons e i s provide di n th e for mo f anumber , specif

y th e unit s o f

measure . 5 . Wher e informatio n o r document s necessary fo r arespOM e ar e neither

i n you r possessio n no r availabl e t o you , indicat e i n you r respons e wh y th e irifoinratio n o r document s ar e no t availabl e o r

i n you r possession , an didentif y an y sourc e that

eithe r possesse s or

i s likel y t o posses s th e document s o r information . 6 . I f informatio n no t

know n o r

no t availabl e to yo u a s o f

th e date o f

submissio n later become s know n o r

availabl e t o you , yo u mus t supplemen t

you r response . Moreover , shoul dyo u fin da

t an y time afte r

th e submissio n o f

you r respons e tha

t an y portio n ofth e submitte dirArmatio n i s fals e o r incorrect , yo u mus t

notif y EP Aas soo n a s possible . Electroni c Submission s T o ai di n ou r

electroni c recordkeepin g efforts , w e reques t tha t yo u provid e al l document s responsiv e t o tins Lnfotmatio n reques t i n a n electroni c forma t

accordin g t o paragraph s 1 throug h 6, below . Thes e submission s ar e i n lie u o f

har dcopy . 1 . Provid e al l responsiv e document s i nPortabl e Documen t Forma t (PDF ) o r

simila r format , unles s otherwis e requeste di n specifi c questions . I f th e PDF s ar e scanne dimages , perfor mat

leas t Optica l Characte r

Recognitio n (OCR ) fo r "imag e ove r

text " t o allo w th e documen t

to b e searchable . 2 . Whe n specifi c question s reques t dat ai n electroni c spreadshee t form , provid e th e dat aan d correspondin g informatio n i n editabl e Exce l o r Lotu s format , an dno t

i n imag e format , i f Exce l o r Lotu s format s are no t

available , the n th e forma t shoul dallo w fo r

dat at o b e use d i ncalculation s b y astandar dspreadsheet progra msuc ha s Exce l o r Lotus .3 . Provid e submissio n o n physica l medi asuc ha s compac t

dis k o r flas hdrive . 4 . Provid e atabl e o f content s fo r

eac hcompac t

disk-o r flas hdriv e containin g electroni c document s submitte ds o that eac hdocumen t

ca n b e accuratel y identifie di n relatio n t o 'ryOWT-espOnse-.to ^ organized

by question number. I n addition , eac hcompac t dis k o r flas hdriv e shoul db e -labele dappropriatel y (e.g, , Compan y Name , Dis k 1 o f 4 fo r Informatio n Reques t Response , Dat e o f

Response) . 5 . Document s claime da s confidentia l busines s informatio n (CBI ) mus t b e submitte do n separate disks/drive s apar t fro mth e non-confidentia l information . Thi s wil l facilitat e appropriat e record s managemen t an dappropriat e handlin g an dprotectio n ofth e CBI . Pleas e follow th e instruction s i nAppendi x C fo r designatin g informatio n as CBI . 6 . Certify that

th e attache dfiles hav e bee n scanne dfo r viruse s an dindicat e wha t progra m wa s used , Definition s A l l term s use di nthi s informatio n reques t hav e thei r

orrdinar y meanin g unles s suc hterm s are define dinth e CAA , 4 2 U.S.C . § § 740 1 et seq., o r the Nationa l Emissio n Standard s fo r Hazardou s Ai r

Pollutant s fo r

Hazardou s Wast e Combustor s a t 4 0 C.R RPart

63 , Subpar t

EEE . 1 . Th e term s "document " an d"documents " shal l mea n an y objec t that records , stores , o r present s information , an dinclude s writings , memoranda , records , o r informatio n o f

any kind , forma l o r

informal , whethe r

wholl y o r

partiall y handwritte n o r typed , whethe r

i n compute r

format , memory , o r

storag e device , o r

i nhardcopy , includin g an y for mo r forma t o f these . I f

i ncompute r

forma t o r memory , eac hsuc hdocumen t shal l b e provide d i ntranslatio n t o afor museabl e an dreadabl e b y EPA , wit hal l necessary documentatio n an dsupport . Al l document s i nhar dcop y shoul dals o includ e attachment s t o o r enclosure s wit han y documents . 2 . Th e term s "relat e to " o r "pertai n to " (o r

an y for mthereof

) shal l mea n constituting , reflecting , representing , supporting , conttaalcting , referrin g to, stating , describing , recording , noting , embodying , containing , mmtioning , studying , analyzing , discussing , evaluatin g o r

relevan t to ,Appendi x B Veoli amus t

submi t tb e foUowin g informatio n withi n 1 4 days , pursuan t t o Sectio n 114(a) ofth e CAA , 4 2 U.S.C . § 7414(a) . ^Question s refe r t o th e faciht y locate da t # 7 Mobil e Avenue , Sauget , Illinois . 1 . Provid e th e 1-minute averag e feedrate s (fjounds/rnmute ) fo r a U metal s (includin g bu t no t .limite dt o mercury , cadmium , lead , arsenic , beryUium , an dchromium ) fo r Incinerator s 2 , 3 , an d4 i n a n Excel-compatibl e forma t fro mJun e 1,201 0 to th e present . 2 . Provid e th e calculate d12-hou r rollin g averag e fo r

al l meta l feedrate s (pomds/minute ) fo r Incinerator s 2,3 , an d4 i n a n Excel-compatibl e forma t fromJun e 1,201 0 to th e present . Provid e adetaile ddescriptio n o f ho w th e 12-hou r

rollin g average s wer e calculate d includin g al l assumptions . D o no t includ e instance s wher e metal s wer e no t fe dt o th e incinerato r

as part ofth e average .Appendi x C Confidentia l Busines s an dPersona l Privac y Informatio n

Assertio n Requirement s Yo u ma y assert

abusines s confidentialit y clai mcoverin g an y part s o f the informatio n requeste d ' Emissio n dat aprovide dunde r Sectio n 11 4 ofth e CAA , 4 2 U.S.C . § 7414 , i s no t entitle dt

o confidentia l treatmen t

unde r 4 0 C.F.R . Par t

2 . "Emissio n data " means , wit hreferenc e t o an y sourc e o f emission s o f

an y substanc e int o th e air : Informatio n necessary t o determin e th e identity , amount , frequency , concentratio n o r othe r characteristic s (to th e extent relate dt o ai r

quality ) o f

an y emissio n whic h ha s bee n emitte db y th e sourc e (o r o f an y pollutan t

resultin g fro man y emissio n b y th e source) , o r

any combinatio n ofth e foregoing ; Informatio n necessary t o determin e th e identity , amount , frequency , concentratio n o r other characteristic s (to the exten t relate dt o ai r

quality ) ofth e emission s which , unde r a n applicabl e standardo i limitation , th e sourc e wa s authorize dt o emi t (mcludin g t o the exten t necessar y fo r suc hpurposes , adescriptio n o f th e manner an drat e o f

operatio n o f

th e source) ; an d Agenera l descriptio n ofth e locatio n and/o r natur e o f

th e sourc e t o Ih e extent necessary to identif

y th e sourc e an dt o distinguis hi t fro mothe r

source s (mcluding , to th e exten t necessar y fo r suc hpurposes , adescriptio n o f th e device , installation , o r

operatio n constitutin g th e source) . 4 0 C.FJ L§ 2.301(aX2Xi)(A) , (B ) an d(C) . T o mak e aconfidentialit y claim , submi t th e requeste dinformatio n an dindicat e that yo u ar e makin g aclai mo f

confidentiality . An y document fo r whic hyo u mak e aclai mo f confidentialit y shoul db e marke db y attachin g acove r sheet stampe do r

type dwit hacaptio n o r other suitabl e for mo f notic e t o indicat e th e inten t to clai mconfidentiality . Th e stampe do r type dcaptio n o r othe r suitabl e for mo f

notic e shoul demplo y languag e suc has "trad e secret " o r "proprietary " o r "compan y confidential " an dindicat e adate , i f any , whe n th e informatio n shoul dn o longe r b e treate da s confidential . Informatio n covere db y suc haclai mwil l b e disclose db y EP A onl y t o th e exten t

pennitte dan db y mean s ofth e procedure s se t fort ha t Sectio n 114(c ) o f

th e CA A an d 4 0 C.F. RPar t

2 . Allegedl y confidentia l portions o f otherwis e non-confidentia l document s shoul db e clearl y identified . EP A wil l constru e th e failur e to furnis haconfidentialit y clai mwit h you r respons e t o th e Reques t t o Provid e Informatio n a s awaive r o f that claim , an dth e informatio n ma y b e mad e availabl e to th e pubh c withou t furthe r notic e t o you .Determinin g Whetherthe Informatio n i s Entitle d t o Confidentia l Treatmen t A l l confidentialit y claim s ar e subjec t t o EP Averificatio n an dmus t b e mad e i n accordanc e wit h 4 0 C.F.R . § 2.208 , whic hprovide s i npart that yo u mus t

satisfactoril y sho w tha t yo u hav e take n reasonabl e measure s t o protec t th e confidentialit y ofth e informatio n an dthat yo u inten dt o

, continu e t o d o so ? ibirt ^ legitimat e mean s withou t you r consen t an dthat disclosur e ofth e informatio n i s likel y to caus e substantia l har mt o you r business' s competitiv e position . Pursuan t t o 4 0 CF.R . Par t

2 , Subpar

t B , EP Ama y at

any tim e sen dyo u aletter askin g that

yo u support you r confidentia l busines s informatio n (CBI ) claim . I f yo u receiv e suc haletter , yo u mus t respon dwithi n th e number o f day s specifie db y EPA . Failur e to submi t you r comment s withi n tha t

tim e woul db e regarde da s awaive r o f you r confidentialit y clai mo r claims , an dEP A ma y release th e mformation . Ifyo u receiv e suc haletter , EP Awil l as k yo u to specif

y whic h portion s o f

th e informatio n yo u conside r confidentia l b y page , paragraph , an d sentence. An y informatio n no t

specificall y identifie da s subjec t to aconfidentialit y clai mma y b e disclose dto th e requesto r

withou t furthe r notic e t o you . Fo r

eac hite morclas s o f

informatio n that

yo u identify a s bein g CBI , EP Awil l as k that yo u answe r

th e followin g questions , givin g a s muc h detai l a s possible : 1 . Fo r

wha t perio do f

time d o yo u reques t

that th e informatio n b e maintaine das confidential , e.g. , unti l acertai n date , unti l th e occurrenc e o f aspecia l event , o r permanently ? I f

th e occurrenc e o f

aspecifi c even t

wil l eliminat e th e nee dfo r confidentiality , pleas e specif y that even t 2 . Monnatio n submitte dt o EP Abecome s stal e ove r time. Wh y shoul dth e infonnatio n yo u clai ma s confidentia l b e protecte dfo r th e tim e perio dspecifie di n you r answer t o questio n numbe r

1 ? 3 . Wha t

measure s hav e yo u take n t o protec t th e informatio n claime da s confidential ? Hav e yo u disclose dth e informatio n to anyon e othe r tha n agovernmenta l bod y o r someon e wh o i s boun db y a n agreemen t no t to disclos e th e infonnatio n further ? I f so , wh y shoul dth e infonnatio n stil l b e considere dconfidential ? 4 . I s Ih e irdbrmatio n containe di n an y publicl y availabl e databases , promotiona l publications , annua l report s o r articles ? I s ther e an y mean s b y whic hamembe r o f th e publi c coul dobtai n acces s t o th e information ? I s th e informatio n o f alan d that yo u woul dcustomaril y no t releas e t o th e public ? 5 . Ha s any governmental bod y mad e adeterminatio n a s t o confidentialit y ofth e information ? I f

so , pleas e attac hacop y ofth e determination . 6 . Fo r

eac hcategory o f

informatio n claime da s confidential , explain with specificit

y wh y releas e ofth e informatio n i s likel y t o caus e substantial har mt o 2you r competitiv e position . Explai n th e specifi c natur e o f thos e harmfu l effects , wh y they shoul db e viewe da s substantial an dth e causa l relationshi p betwee n disclosur e an dsuc hharmfu l effects . Ho w coul dyou r competitor s mak e us e o f thi s informatio n t o you r detriment ? 7. ; ©o-youassertf e basis ? Pleas e explai n th e reaso n fo r you r assertion . I f

yo u asser

t tha t th e informatio n i s voluntaril y submitte dinformation , explai n whethe r an dwh y disclosur e o f

m e .informatio n woul dten dt o lesse n th e availabiht y t o EP Ao f simila r informatio n i n th e future . 8 . Is there an y other informatio n yo u dee mrelevan t t o EPA' s determinatio n regardin g you r

clai mo f busines s confidentiality ? I f yo u receiv e areques t

fo r asubstantiatio n lette r

fromth e EP Ay» ubea r th e burde n o f substantiatin g you rconfidentialit y claim . Conclusor y allegation s wil l b e give n littl e o r n o weigh t i n th e detenrnnation . I n substantiatin g you r CB I claim(s) , yo u mus t bracke t al l tex t s o claime dan dmar k

i t "CBI. " Infonnatio n s o designate dwil l b e disclose db y EP Aonl y t o th e exten t allowe db y andb y mean s o f th e procedure s se

tfort hi n 4 0 C.F.R . Part 2 , Subpar t

B , I f yo u fai l t o clai mth e infonnatio n as confidential , i t ma y b e mad e availabl e t o th e publi c withou t furthe r notic e t o you . Persona l Privac y Infonnatio n Pleas e segregate an y personnel , medica l an dsimila r files fro myou r

response s an dinclud e tha t irjformatio n o n aseparat e sheets ) marke da s "Persona l Privac y Infonnation, " Disclosur e o f suc h informatio n t o th e general publi c ma y constitut e a n invasio n o f privacy .CERTIFICAT E O F MAILIN G LLorett aShaffer , certif y that I sent aReques t

t o Provid e Informatio n Pursuan t t o th e Clea n Ai r

Ac t b y Certifie dMai l Retur n Receip t Requested , to : Dou g Harri s Genera l Manage r Veoli aEnvironmenta l Service s # 7 Mobil e Avenu e Sauget , Dlinoi s 6220 1 I als o certif

y that I sen t acop y o f

th e Reques t

t o Provid e Informatio n Pursuan t to th e Clea n A i r Ac t b y Firs t Clas s Mai l to: Ra y Pilapi LManage r Complianc e an dSystem s Managemen t Sectio n Burea u o f

Ai r Illinoi s Environmenta l Protectio n Agenc y 102 1 Nort hGran dAvenu e Springfield , Illinoi s 6270 2

Certifie dMai l Receip t

Numto : 7* 0 

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# VES019283.pd f

### Comment s b y Michae l Fuch s o n behal f o

fVeoli a E S Technica l Solutions . L.LC . o n the Draf

t Titl e V Permi t an d th e Statement o f Basi s Date

d Octobe r 201 4 I , Michae l Fuchs , bein g ove r th e ag e o f

1 8 an do f

soun dmind , state an ddepos e unde r oat h
a s follows : 1 . I a maProjec t

Manage r

i n th e Measurement s Grou p i n UR S Corporation' s Austin , Texa s office . I primaril y manag e project s relate dt o th e treatmen t o f hazardou s wast e (primaril y combustion) ; emission s measurement s includin g sourc e testing ; an dregulator y complianc e (RCRA , TSCA , an dHW C MACT ) fo r hazardou s wast e combustio n facilities , I prepar e tes t plan s an dqualit y assuranc e projec t plan s (QAPPs) ; supervis e tria l burn s an drelate dprojects ; an dprepar e report s an d regulator y filings . Man y o f th e tes t program s includ e th e us e o f continuou s emissio n monitorin g system s (CEMS) . UR S ha s bee n workin g wit hVeolia' s Sauge t facilit y i n meetin g regulator y requirement s o f th e HW C MACT . I hav e attache dm y curriculu mvita e heret o a s Attachmen t 1 an dincorporat e i t

herein . 2 . I hav e reviewe dportion s o f th e Draf t

Titl e V Permi t

an dth e Statemen t

o f Basi s fo r DRAF T Ai r

Pollutio n Contro l Titl e V Permi t t o Operat e No . V-IL-1716300103-2014-1 0 date dOctobe r 201 4 issue dt o Veoli aE S Technica l Solutions , L.L.C . ("Veolia" ) i n Sauget , IL . I focuse di n particula r o n th e portion s o f th e Draf t

Permi t an dStatemen t

relatin g t o th e Coope r Enviromnenta l Services , L L C Xact TM 64 0 Multi-Meta l Continuou s Emission s Monitorin g System . 3 . I hav e almos t

4 0 year s o f

experienc e i n conductin g ai r pollutio n emissio n measurement s an dassessin g th e performanc e o f ai r pollutio n measuremen t technologie s a

t numerou s combustio n sources . Throug hproject s I hav e performe d
a t UR S ove r

th e years , I a mfamilia r wit hth e measuremen t o f metal s emission s an d -1
-



### VES01928 3wit hCEM S technology . 4 , Du e t o m y familiarit y wit hmetal s emission s measuremen t an dCEM S technology , Veoli arequeste dthat

I revie w th e Statemen t ofBasis . I a mfamilia r wit hth e basi c fundamental s ofth e multi-metal s CEM S Xact TM 64 0 devic e reference di n th e Statemen t

ofBasis . Th e Xact TM multi-metal s CEM S wa s develope db y Coope r Environmenta l Services , LLC . A s state db y EP A i n th e Statemen t ofBasis , th e Xact TM multi-metal s CEM S ha dbee n markete db y Pal l Corporation , bu t no w Coope r Environmenta l Services , LL C hold s th e exclusiv e manufactur e an d marketin g right s fo r

th e XactTM . Th e Xact TM multi-metal s CEM S use s X-ra y Fluorescenc e fo r

th e measuremen t

o f metal s collecte do n filte r tape . 5 , USEPA' s Statemen t o f Basi s provide s tha t

"multi-metal s CEM S .. . hav e bee n demonstrate dt o b e reliabl e fo r measurin g metal s emission s fro mahazardou s wast e combusto r

" , an d"ha s monitore dside-by-sid e evaluation s o f multi-metal s CEM S wit hEP A Metho d29, " Statemen t ofBasi s at

Sectio n 5.3.4 . Th e Statemen t o f Basi s als o state s "U S EP A recentl y evaluate dat severa l facilitie s acommercia l versio n o f

amulti-metal s CEM S (th e Xact TM multi-metal s CEMS) " althoug hn o citatio n i s give n fo r

arepor t o f thi s testing . 6 , I n USEPA' s website , at http://www.epa.gov/ttnemc01/monitor.htm l unde r Metal s an dMercur y Emission s Monitoring , EP A state s "I n 199 6 Performanc e Specificatio n 1 0 (PS10 ) wa s propose di n conjunctio n wit hth e origina l Hazardou s Wast e Combusto r

NESHAP , bu t

becaus e th e measuremen t technolog y ha dno t bee n full y develope dan ddemonstrated , th e specificatio n wa s no t promulgated. " P S 1 0 remain s a s apropose dmethodology . Therefore , USEP A shoul didentif y i n it s respons e t o comment s wha t th e Statemen t

ofBasi s mean s tha t

"multi-metal s



### VES01928 4CEM S .. . hav e bee n demonstrate dt o b e reliabl e fo r measurin g metal s emission s fro mahazardou s wast e combusto r " . Sinc e th e accurac y o f th e Xact TM multi-metal s CEM S ha s no t

bee n demonstrate dagains t EP AMetho d2 9 wit hsample s collecte d directl y fro masourc e b y bot hth e Xact TM an db y EP AMetho d29 , a s i s th e preferre d approac hi n th e propose dP S 10 , an dsinc e th e HW C MAC T require s that Metho d 2 9 b e use dt o demonstrat e complianc e wit hth e emissio n standard s fo r metals , th e accurac y o f

th e Xact TM multi-metal s CEM S ha s no t bee n demonstrated . E P Aals o state s i n th e Statemen t ofBasi s that

"El i Lill y Compan y receive d approva l fro mth e EP At o us e thi s instrumen t (i.e. , th e multi-metal s CEM S develope db y Coope r Environmenta l Services ) a s aCEM S a s a n alternativ e i n lie u o f paramete r

monitorin g o n ahazardou s wast e incinerator" , an dtha t th e "U S Arm y ha s successfull y installe dan devaluate don e o f thes e CEM S o n ahazardou s wast e incinerator . Thes e studie s resulte di n severa l monitorin g method s an dperformanc e standard s fo r

th e x-ra y technology . Thes e document s ma y b e foun dunde r th e Otlie r Method s sectio n o f

thi s we b site. " Th e Othe r Tes t Method s liste do n EPA' s websit e tha t

pertai n t o multi-metal s CEM S include :

• Othe r

Tes t Metho d1 6 (OT M 16 ) - Specification s fo r X-Ra y Fluorescenc e Base dMulti-Metal s CEM S a t Stationar y Sources ;

• Othe r

Tes t Metho d1 7 (OT M 17 ) - Determinatio n o f Meta l Concentratio n i n CES ' Xact TM CEM S Stillin g Chambe r Usin g Filter s an dSoli dSorbent s wit h X-Ra y Fluorescenc e Analysis ;

• Othe r

Tes t Metho d1 8 (OT M 18 ) - Performanc e Specification s fo r a Quantitativ e Referenc e Aeroso l Generator ;

• Othe r

Tes t Metho d1 9 (OT M 19 ) - Determinatio n o f Meta l Concentration s i n Emission s fro mStationar y Source s (Instrumenta l Analyze r Procedure) ;• Othe r Tes t Metho d2 0 (OT M 20 ) - Qualit y Assuranc e Requirement s fo r X-Ra y Fluorescenc e Base dMulti-Metal s CEM S a t Stationar y Sources ; an d

• Othe r

Tes t Metho d2 1 (OT M 21 ) - Standar dOperatin g Procedur e fo r Generatin g aQuantitativ e Multi-Metal s Referenc e Aeroso l wit hCE S QAG . 8 . Thes e method s wer e prepare db y Coope r Environmenta l Services , LLC . Whil e thes e method s wer e ostensibl y produce dusin g th e cumulativ e knowledg e garnere d b y Coope r

Environmenta l Service s o n th e operatin g requirement s an dnuance s o f th e Xact TM multi-metal s CEMS , OTM s 16-2 1 wer e prepare dspecificall y for , an d i nsuppor t

of , th e Alternativ e Monitorin g Petitio n fo r th e us e o f

th e Xact TM t o monito r metal s emission s o n th e hazardou s wast e incinerato r a t El i Lilly' s Tippecano e Laboratorie s manufacturin g facilit y nea r Lafayette , Indiana . Th e Xact TM multi-metal s CEM S wa s primaril y t o sho w ther e wer e no , t o ver y low , concentration s o f

metal s emission s fro mEl i Lilly' s incinerator . Thi s technicall y i s differen t

tha n measurin g a n actual , an dvarying , concentratio n o f metals . Th e H W C MAC T state s that Metho d2 9 (4 0 CF R60 , Appendi x A , Metho d29 ) mus t b e use dt o demonstrat e complianc e wit hth e emissio n standard s fo r mercury ; th e semivolatil e metal s cadmiu man dlead ; an dth e lo w volatilit y metal s arsenic , berylliu man dchromium . Despit e thi s mandate , o n th e El i Lill y incinerator , Coope r Environmenta l Services , LLC' s OTM s di dno t us e Metho d2 9 t o demonstrat e th e accurac y ofth e Xact TM multi-metal s CEMS . 9 . Th e significanc e o f Coope r Environmenta l Services , LLC' s failur e t o utiliz e Metho d2 9 i s demonstrate db y comparin g propose dPerformanc e Specificatio n 10 , whic hwa s discusse dearlier , t o OT M 16 . 10 . O n EPA' s website , OT M 1 6 i s title dSpecifications forX-Ray Fluorescence Based Multi-Metals CEMS at Stationary Sources; while , th e cop y o f OT M 1 6



### VES01928 6downloade dfro mEPA' s websit e bear s th e titl e Performance Specification YY: Specifications forX-Ray Fluorescence Based Multi-Metals CEMS at Stationary Sources, Performanc e specification s (PS ) promulgate db y EP Ainclud e a requiremen t

t o demonstrat e th e Relativ e Accurac y (RA ) o f th e monitorin g syste m usin g a n EPA-approve dan dvalidate dtes t method , terme daReferenc e Metho d (RM) . I n P S 10 , th e preferre d(o r primary ) metho dfo r

measuremen t

o f R Ai s agains t a n EPA-approve dtes t metho d(i.e. , Metho d29) . Thi s i s consisten t wit h ever y performanc e specificatio n promulgate db y EPA . I n comparison , Performanc e Specificatio n Y Y (OT M 16 ) doe s no t includ e arequiremen t fo r RA , P S Y Y include s Relative Bias Criteria-Accuracy and Precision an dLinearity Test Criteria - Accuracy and Precision. A s cite di n th e propose dP S 10 , th e R M t o b e use dt o evaluat e th e R A o f th e multi-metal s CEM S i s 4 0 CF R60 , Appendi x A , Metho d29 , an d"th e R A o f th e CEMS , relativ e t o th e RM , mus t b e n o greate r

tha n 2 0 percen t

o f th e mea n valu e o f

th e R M tes t

dat ai n term s o f

unit s ofth e emissio n standar dfo r

eac hmetal , o r

1 0 percen t

o f th e applicabl e standard , whicheve r i s greater" . EP AMetho d2 9 wa s adraft metho dwhe n P S 1 0 wa s proposed . Propose d P S 1 0 doe s howeve r

stat e that

a n alternativ e procedur e t o determin e RA , calle d tota l syste mcalibration , wa s t o b e develope dan dadde da s a n appendi x t o P S 10 . Thi s alternativ e procedur e ha s apparentl y no t ye t bee n develope db y EPA . I t ca n howeve r

b e state dthat

OT M 1 6 fail s t o compl y wit hth e HW C MACT , at 4 0 CF R 63.1208(b)(2) , (3) , an d(4 ) whic hstate s tha t Metho d2 9 mus t

b e use dt o demonstrat e complianc e wit hth e emissio n standard s fo r mercury , cadmiu man d lead , an darsenic , berylliu man dchromium .Th e HW C MAC T state s that Metho d2 9 (4 0 CF R60 , Appendi x A , Metho d29 ) mus t b e use dt o demonstrat e complianc e wit hth e emissio n standard s fo r mercury ; th e semivolatil e metal s cadmiu man dlead ; an dth e lo w volatilit y metal s arsenic , berylliu man dchromium . Metho d2 9 include s anumbe r o f requirement s to addres s potentiall y critica l aspect s o f th e measuremen t

o f metal s emission s fro m stationar y source s tha t ar e no t include di n th e operatio n o f th e Xact TM multi-metal s CEMS . Thi s coul dpotentiall y lea dt o th e Xact TM multi-metal s CEM S providin g inaccurat e and/o r

inconsisten t

results .

• A requiremen t

o f Metho d2 9 i s that

th e sampl e b e collecte disokineticall y a t multipl e point s acros s th e stac k t o ensur e that

arepresentativ e sampl e o f th e stac k ga s i s collected , includin g bot haeroso l an dgas-phas e constituents . Fo r th e result s o f

Metho d29 , an dal l isokineti c samplin g methods , t o b e acceptable , th e samplin g mus t

b e withi n 10 % o f

isokineti c (i.e. , 100±10%) . Thi s requiremen t

i s rigorousl y enforced . I f th e samplin g i s no t

withi n 10 % o f

th e isokineti c samplin g rat e the n tha t sampl e wil l no t

b e accepte db y regulator y agencies . P S Y Y state s i n Sectio n 1.3. 2 "you r multi-metal s CEM S shoul d sampl e fromth e sourc e a t aflo w rat e whic hi s withi n 1 0 percen t o f tru e isokinetic" . However , operatin g dat afo r installe dan devaluate dXactTM CEM S d o no t repor t th e isokineti c samplin g rate . A s state di nth e Statemen t ofBasi s at 5.3.4 , "Th e proces s begin s whe n a n isokineti c sub-sampl e o f stac k ga s i s take n fro mth e stillin g chambe r an ddraw n throug hachemically-reactiv e filte r tape. " Th e stillin g chambe r

i s acomponen t

o f th e sampl e acquisitio n system , an di s a vesse l int o whic hsampl e ga s i s draw n fro mth e source . Thi s shoul dno t b e confuse da s withdrawin g a n isokineti c sampl e fro mth e sourc e itsel f a s require d b y Metho d29 . P S 1 0 doe s no t requir e sampl e b e draw n fromth e stac k isokinetically , bu t

i t doe s requir e tha t

th e R Ao f

th e multi-metal s CEM S b e compare dt o Metho d29 , an dsampl e ga s fo r Metho d2 9 mus t

b e draw n fromth e sourc e isokinetically .• Followin g collectio n o f th e Metho d2 9 sample , th e entir e samplin g trai n i s rinse d(wit hreagent s specifie di n th e method) , an dal l ofth e component s recovere dfro mth e samplin g trai n (fro mth e nozzl e t o th e impinger s use dt o collec t gas-phas e metals ) ar e analyze dfo r metal s i n alaborator y (usin g method s specifie di n Metho d29) . Result s fo r Metho d2 9 ar e specifi c t o individua l metals , an dinclud e result s fo r al l component s recovere dan d analyzed . I n comparison , whil e differen t sampl e collectio n configuration s are foun dfo r

application s o f

th e Xact TM multi-metal s CEMS , th e sampl e acquisitio n system s alway s includ e atranspor t line , an dma y includ e astillin g chamber , wate r trap , and/o r

dryin g chamber . Non e ofth e component s fro mth e sampl e acquisitio n syste mar e recovere do r analyze dfo r

inclusio n i n th e result s fo r th e Xact TM multi-metal s CEMS . Thi s differenc e betwee n Metho d2 9 an dth e Xact TM multi-metal s CEM S i s potentiall y critica l t o th e accurac y o f th e result s o f

th e Xact TM multi-metal s CEMS . Specificall y fo r mercury , experienc e ha s show n that mercur y ma y condens e an dthe n re-vaporiz e i n th e sampl e acquisitio n system , dependin g o n conditions . Thi s phenomeno n coul doccu r fo r othe r metals , dependin g o n th e configuratio n an dcondition s o f th e sampl e acquisitio n system , an di f experienced , th e Xact TM multi-metal s CEM S wil l no t b e quantifyin g asampl e representativ e o f th e sourc e (i.e. , th e stac k gas) , an d potentially , inaccurat e dat awil l b e collected . Du e t o th e desig n an doperatio n o f th e ai r pollutio n contro l systems , th e moistur e conten t o f stac k gase s fro mVeolia' s incinerator s i s variabl e an dconsiderabl y highe r tha n mos t

incinerators , typicall y fro m3 0 t o 45% . Whil e Coope r Environmenta l Service s ha s assure dEP Athat th e Xact TM ca n operat e reliabl y a t moistur e content s abov e 40 % (se e Statemen t ofBasi s footnot e 58) , n o studie s supportin g Coope r

Environmenta l Services ' assuranc e are cited . Concentratio n o f moistur e i n th e stac k

ga s fromVeolia' s incinerator s coul dhav e anegativ e impac t upo n th e operatio n o f multi-metal s CEM S (i.e. , it s reliability) , an dth e CEM S abilit y t o produc e vali dmetal s dat ai n th e stac k ga s fromthos e incinerators . T o m yknowledge , th e Xact 1 " multi-metal s CEM S ha s no t bee n operate do n a n incinerato r havin g th e concentratio n o f moistur e i n th e stac k

ga s fro mVeolia' s incinerators , an dthu s ha s no t

bee n demonstrate dan dprove n t o b e reliabl e fo r measurin g actua l emission s o f

metal s a

t th e stac k

ga s moistur e concentration s tha t woul db e experience da

t Veolia . 13 . A j ourna l articl e authore db y Ha y et al (K . Jame s Hay , Bruc e E . Johnsen , Pau l R . Ginochi o & Joh n A . Coope r (2006 ) Relativ e Accurac y Testin g o f a n X-Ra y Fluorescence-Base dMercur y Monito r at Coal-Fire dBoilers , Journa l ofth e Ai r an d Wast e Managemen t

Association , 56:5,657-665 , DOI : 10 , 1080/10473289.2006.10464471 ) present s th e result s o f relativ e accurac y testin g o f th e Xact TM multi-metal s CEMS . Whil e relativ e accurac y (RA ) testin g o f th e Xact TM multi-metal s CEM S wa s performed , R A wa s no t demonstrate dfo r

sample s collecte ddirectl y fro mth e sourc e (i.e. , stack ) a s woul db e require dfo r othe r performanc e specifications , includin g th e propose dP S 10 . An dR Awa s measure d betwee n th e Xact TM multi-metal s CEM S an dMetho d2 9 onl y fo r mercur y an d arsenic . Result s ar e no t reporte dfo r

th e othe r

metal s regulate db y th e HW C MACT , beryllium , cadmium , chromium , an dlead . Sampl e wa s draw n fro mth e sourc e throug hasampl e acquisitio n syste mincludin g atranspor t line , wate r

trap , an ddryin g chamber . Compresse dai r wa s injecte dint o th e sampl e acquisitio n syste mupstrea mofth e dryin g chamber . Followin g th e dryin g chamber , aportio n ofth e sampl e ga s wa s draw n int o th e Xact TM multi-metal s CEMS , an dth e remainde r ofth e sampl e ga s wa s collecte di n paire d(i.e. , two ) Metho d2 9 samplin g trains . Relativ e accurac y testin g performe di n thi s manne r i s ameasur e o f

th e relativ e accurac y ofth e analytica l portio n o f th e Xact TM multi-metal s CEM S t o Metho d29 , -8
-



### VES01929 0bu t i s no t ameasur e o f

th e relativ e accurac y o f th e whol e o f

th e Xac t

multi-metal s CEMS , including , bu t no t limite dto , th e samplin g an danalytica l components , agains t Metho d2 9 als o measure di n th e sourc e (i.e. , stac k gas ) a s require db y othe r performanc e specifications , includin g propose dP S 10 . 14 . Evonik s Deguss aCorporatio n purchase dth e Tippecano e facilit y i n 2010 , an dn o longe r use s amulti-metal s CEM S o n th e incinerato r at th e Tippecano e facility . Th e multi-metal s CEM S i s n o longe r i n operatio n fo r

functiona l an deconomi c reasons . 15 . Footnot e 6 0 i n th e Statemen t ofBasi s states , "EP Aunderstand s that th e U.S . Departmen t

o f Defens e ha s purchase dthre e Xact TM unit s fo r us e a t arm y munition s incinerators. " Denni s Warcho l wit hVeoli arelate dt o m e i n 201 3 tha t h e ha d spoke n wit hDou g Barth , th e Busines s Developmen t Manage r

wit hPall . Bart h suggeste dVeoli acontac t Larr y Well s wit hth e U.S . Arm y at th e Tooel e Arm y Depo t (TEAD ) t o obtai n additiona l informatio n o n ho w th e Xact TM unit s hav e bee n utilized . Base dupo n Barth' s recommendation , I contacte dWell s o n Januar y 29 , 2013 . Well s relate dtha t TEA D ha dtw o Xact TM multi-metal s CEM S wit hon e installe do n eac hofth e tw o incinerator s at TEAD . O f

th e tw o incinerator s a t TEAD , on e i s auni t

use dfo r

testin g an dth e othe r

i s use dfo r

production . Th e uni t use dfo r testin g onl y operate s periodically , whil e th e productio n uni t operate s mor e often . Well s sai dthat

whil e ther e i s aXact TM multi-metal s CEM S a t th e tes t unit , h e wa s no t awar e tha t

i t ha deve r

bee n operated . Well s the n introduce dhi s colleague , Jo e Peterson , wh o i s involve di n th e operation/monitorin g o f th e productio n furnac e at

TEAD . Peterso n remembere dthat th e Xact TM multi-metal s CEM S wa s installe do n th e productio n furnac e an dcalibrate dwhe n i t wa s acquire d(h e though t aroun d2007) , an dtha t testin g ofth e productio n furnac e wa s performe dshortl y

-9
-



### VES01929 1thereafte r that allowe dcompariso n o f measurement s performe db y th e multi-metal s CEM S t o a n EP Areferenc e method . H e remembere dthat th e Xact TM multi-metal s CEM S wa s operate dfo r abou t 1 5 t o 2 0 day s befor e i t failed . Peterso n sai dthat th e Xact TM multi-metal s CEM S ha s no t operate dsinc e i t

failed . Base do n th e phon e conversation s wit hbot hWell s an dPeterson , bot hofth e Xact TM multi-metal s CEM S ar e stil l a

t TEAD , bu t

are no t i n operation . 16 . Th e Thir dXact TM multi-metal s CEM S reference da t footnot e 6 0 i s a

t th e Cran e Nava l Surfac e Warfar e Cente r i n Crane , IN , an dI understan dthat th e instrumenta l monitorin g syste mha s bee n set up . However , th e CEM S i s no t connecte dto , o r drawin g sampl e ga s from , th e stac k o f th e uni t a s par t o f norma l operation s an d therefor e i t

i s no t trul y installed . Additionally , munition s incinerator s are no t commercia l hazardou s wast e incinerators . Munition s incinerator s d o no t trea t th e broa drang e o f

waste s treate di n acommercia l incinerato r and , unlik e Veolia , th e stac k emission s fro mmunition s incinerator s d o no t hav e th e sam e hig hmoistur e content , I nclosing , m y assessmen t o f th e Xact TM multi-metal s CEM S i s that i t ha s no t bee n demonstrate dt o operat e reliabl y o r produc e accurat e dat awhe n compare dagains t a n EPA-approve dtes t

method . Further , Coope r Environmenta l Service s i s th e onl y vendo r that purport s t o hav e develope dacommerciall y availabl e multi-metal s CEMS . I t i s simpl y unprecedente dfo r

EP At o endors e th e us e o f aspecifi c vendo r

o f a n instrument , monitorin g equipment , o r othe r suc hsyste mi n amandate dregulator y o r enforcemen t circumstanc e o r

fo r us e i n lea u o f

aperformanc e test . Further , t o m y knowledge , n o multi-metal s CEM S i s i n us e a s aparametri c o r i n an y othe r

capacit y o n acommercia l hazardou s wast e incinerator . -10
-FURTHE RAFFIAN T SAYET H NOT .

Michae l Fuch s SWOR NAN D SUBSCRIBE D Befor e m e thi s 

## /Sd&y o f Decembe r

2014 .

Notar y Publi c M y Commissio n Expires : .Vl-CJL./i- ' 

# j0W&\ , ^ORIND A MADSE N I fsfc^ l Notar

y Public, Stat

e o f Texa s VS5 £?3& ? M V Commission Expire s J!4)it y February is , 201 6'•

" Pi s j ee l Managemen t v Ai r Regulator s Complianc e {Federa l an dStale , RCRA . TH C A , an dI IW

C MAC ! ) v ' Sourc e Lmissioti s letting : I .S , I-P A 4 0 C F RFa n 6 0 an d75 , SW- X Id, an dA S I' M Samplin g Method s •> ' 1 ria l Bur n Plans , Cornpreheiis hc Performanc e les t(CP! } Plans , Confirmator y Perfonnanc e I'es i (CfP' l I Plan s an d Qualit y Assuranc e Pro j ee l Plan s

vTria l Burn , CPT . an d CI T 1' Reportin g v I IW C MAC T Regulator y Piling s HS . Chemistry . Souihwes t Texa s Stat e Cnhersit y (no w Texa s Stat e University) , 197 3 I lazardtHi. s Wast e Operation s k, hmergene y Respons e (IIAZWOPP.R ) HA/WOPF K

Refresher . Annuall y Basi c Piu s Refresher . Anniml h personne l a

t TOCDF . > Projec t

Manager , TOCD FPreparatio n o f AM Rani l MPM ' Sorben t Traps , 2006 , 2007 , 2008,200 9 Tooele , UT . UR S prepare s th

e AM R13-bed . spiked ) an dMP M (2-bed . unspiked ) sorbent trap s lo r

TOCDF . Th e AM R an dMP' M sorben t

trap s ar e shippe dt

o TOCD Fweekly . • Projec t

Manager , TOCD FQuarterl y Calibratio n o f Appendi x K

Mete r Boxes , 2006 , 2007 , 2008 , 200 9 Tooele , UT . CR S performe dthe quarterl y calibration s o f the Appendi x K

meter boxe s as require db y Appendi x M r Michae l Fuch s i s aPrincipa l Projec t Manage i i n th

e Measurement s (irou p i n I IRS ' Austi n office , an dha s o \er Ts y ca n o f

experienc e doin g e

n \ironmenia l consulting . Oscrih c past 25 + years , h

e has focuse do n th

e pennittin g o f hazardou s waste combustio n unit s includin g RCR A an dI SC A incinerators , R ( R A B11
- (Boile r

an dIndustria l furnace ) units , an dunit s subjec t t o the Au/mw/ / f 'nn ,\sii»i Sitiih/tifiis fur

I!tizai\hiii\ iir

I'ullunims imm I

laTunlniis U\i\h' t ',;/«/t«s/Mr. s t i e. . th

e //IP C ,t/J ( '/') . M i I uch s began hi s ca i eer perfumin g sourc e testin g an dnow manage s project s lo r bot hindustria l an dgovernmen t client s whil e continuin g l o pro \id e hands-o n participation . Mr . fuch s primaril y manage s project s relate dt o di e treatment

o f hazardou s wast

e (primaril y combustion) ; emission s measurement s includin g sourc e testing : an dregulatory complianc e (RCRA . I S t \ . an d11\

\C MA< ' I I fo r hazardou s waste combustio n facilities , I l e activel y participate s i nthos e project s preparin g tes t

plan s an dOAPPs : super s isin g tria l bunts , t PIs . andrelate d projects ; an dpreparin g report s an dregulator } filings . Mr . I uch s manage s th e tria l burns , CPTs , an drelate dproject s ani l the de\elopmenl , installation , an dannua l RA' I A s ofth e mercur y monitorin u syste ma t "PCX'DP .

• Projec t

Manager , I OCD I Alternativ e Monitorin g Reques t (AMR ) Mercu n Monitorin u o f th e MPT . 2t!0o . Tooele . I T . \ n \M ROc- 1 ( re d andprepare dlo r

th e MP Fa t TOCD F(a

n incinerator ) t

o pio \id e HW C MA C I " complianc e dat alo r

th e mercui y standard , '

I h e AM Ri s base do n Appendi x K . \IR S develope dth

e samplin g ani l analytica l procedures , procure dal l .system s fo r samplin g andannl

y sis . transferre dthe samplin g an danalysi s procedure s t o FO t DF . andtraine dpeisonne i a t K K'DF , SOP s were ptcpare dfo r integia ) procedures ,
• ProjectManager , TOCD FRAT Aofth e AM RMercur y Monitorin g System , Annuall y 200 6 - 201.2 , Tooele , UT . A RAT A(Relativ e Accurac y Tes t Audit ) ofth e AM Rmercuiy ' complianc e monitorin g syste mo f the MP F(I.e. , a

n incinerato r

a t TOCDF ) i s performe dannuall y i n accordanc e wit hEP A Performanc e Specificatio n (PS ) 12A , Th e RAT Awa s initiall y performe di n 200 6 usin g EP A .Metho d2 9 as the referenc e method . Sinc e 2006 , the referenc e metho duse di n th e RATA s has ; been FP A Metho d30 B withOhi o Lume x o n site analysis .
• Projec t

Manager , TOCD F Mercur y Proces s Monitorin g fo r Mercur y fro m th e MPF , 2006 , Tooele , UT . Mercui y Proces s Monitorin g (MPM ) ofth e MP F wa s performe dusin g a n adaptatio n o f

Appendi x K

wit hon sit e analyst s usin g a n Ohi o Lumex . anal

y zer , UR S develope dthe samplin g an danalytica l procedures , transferre dth

e samplin g an danalysi s procedure s t o TOCDF , an dtraine d



### VES019293 a• Projec tManager , Veoli aHW GMAC T CPT , 2(106 , Port . Arthur , TX . UR S performe dan dreporte dth e HW C MAC T CP T o f

Veolia' s incinerato r

in Port Arthur , TX . Veoli ause s aproprietar y proces s to contro l mercur y emissions , 'fh e mercui y standardwa s no t demonstrate di n the initia l performanc e ofth e CPT . Th e proprietary proces s wa s optimized , includin g testing . Testin g fo r mercur y durin g Ih

e optimizatio n phas e wa s performe dusin g Appendi x K

wit ho n site analysi s usin g an Ohi o Etirne x mercury analyzer . Th e mercur y standardwa s successfull y demonstrate ddurin g th e optimizatio n test s (usin g Appendi x K ) an dth e subsequen t

CP T (usin g EP A.Metho d29) .
• Projec t

Manager , EG&G , TOCD FMP Fan dLIC 2 Mustar dATBs , Januar y 2007 , Tooele , UT . Th e TOCD F Meta l Part s Furnac e (MPF ) exhaus t ga s wa s simultaneousl y sample db v U.S , EP A Melho d5/SW-84 6 Metho d 0050 : U.S . BP A Metho d29 : SW-84 6 Metho d0023A ; SW-84 6 Metho d001 0 fo r Semivolatiles ; SW-84 6 Metlio d 001 0 fo r Tota l Organi c Emission s (GRAV/TCO) : SW-84 6 Metlio d0040 : SW-84 6 Metho d00 3 I ; an dCEM S fo r CC K NO, , SOan dTFIC . Th e same testin g wa s performe don th e Liqui dIncinerato r {F.1C2 ) exhaus t

ga s followin g th e completio n ofth e MP FATB . Mr . Fuch s serve da s the Projec t Manage r

fo r thes e tria l burn s an dprovide don sit e supervisio n o f

ih e performanc e ofth e tria l burns , Mr , Fuch s wa s responsibl e fo r providin g dail y samplin g dat a an dupdate s fo r

the performanc e ofth e tria l burns . H e als o manage dan dparticipate di n th e preparatio n ofth e Samplin g ami Analytica l Report s andQA/Q C Report s fo r th e MP Fan dLIC 2 Mustar dATBs . • Projec tManager , EG&G , TOCD FMP FSecondar y Wast e Demonstratio n Tes t(SWDT) , Marc h 2006 , Tooele , UT . 'Fh e 'I'OCD FMP Fexhaus t wa s simultaneousl y sample dby U.S . EP A M C I I K K I5/SW-84 6 Metho d 0050 ; U.S . EP A Metho d29 ; SW-84 6 Metho d0023A : SW-84 6 Metho d001 0 fo r semivolatiles ; SW-84 6 Metho d 001 0 fo r Tota l Organi c Emissions ; SW-84 6 Metho d0040 ; SW-84 6 Metho d00 3 I : an dCEM S fo r CCE , NO, . SCF . an dTHC , Mr . Fuch s serve das ih e Projec t Manage r

fo r th e SWD T an dprovide don-sit e supervisio n ofth e performanc e ofth e test . Mr . Fuch s wa s responsibl e fo r providin g dail y samplin g dat aan dupdate s fo r the performanc e ofth e test . H e als o manage d.an dparticipate di n th e preparatio n ofth e Samplin g an dAnalytica l Report s an dQA/QC 1 Report s fo r the SWDT ,
• Project : Manager , Veoli aEnvironmenta l Services , CPT , RCR APeriodi c Testing , ari dTSC A Ris k Burn , April-Jul y 2006 , Por t Arthur , TX . Mr . Fuch s serve da s th e Projec t Manage r

fo r ih e test s - an initia l test , mini

burns , and

* afinal test . Durin g th e Apri l 200 6 CP T fo r

the Interi mStandard s ofth e HW C MACT , RCR APeriodi c Testing , an dTSC A ris k burn , ih e incinerato r

exhaus l wa s simultaneousl y sample db y U.S . KP AMetho d5/26A . U.S . BP AMetho d29 . SW-84 6 Metho d001 0 fo r semivolatil e POH C andorganics , SW-84 6 Metho d0023 A fo r dioxins/furans . SW-84 6 Metho d001 0 fo r PCBs . SW-8J 6 Metho d003 0 fo r volatil e organics , SW-84 6 Metho d 0061 . fo r CrfVI) , an dCEM S fo r NO , an dTHC . Mr . Fuch s worke dclosel y wit hVeolia . an dwa s th e primar y autho r ofth e les t

plan an dQAPP , Mr . Fuch s provide don-sit e supervisio n ofth e perfomianc e o f tli e tests , H e manage d an dparticipate di nthe preparatio n ofth e fina l report s an dpreparatio n ofth e Notificatio n o f Compliance .
• Projec t

Manager , EncrSo l Technologies , Plasm aEnerg y Pyrolysi s Sysfe m(PEPS ) Testing , Augus t 2006 , Springfield , VA . Manage dth e projec t involvin g testin g th

e PEP S t o determin e it s suitabilit y fo r processin g secondar y waste fro mchemica l demilitarizatio n sites . Th e PEP S exhaus t wa s simultaneousl y sample db y ICS . EP AMetho d5...SW-84 6 Metho d0050 . U.S . EPA , Metho d29 , SW-84 6 Metho d0010 . an dSW-84 6 Metho d0031 . • On-site Projec t

Manager/Tes t

Supervisor , Wast e Contro l Specialists , Octobe r2004, Andrews,.TX . Serve das On-Sit e Projec t

Manage r

an dTes t

Superviso r

fo r evaluatio n ofth e (Jeomel t proces s operate db y Wast e Contro l Specialist s wa s performe db y simultaneousl y samplin g the exhaus l b y U.S . EP A Metho d5/26A ; U.S . EP A Metho d 29 ; CAR D Metho d42 8 fo r dioxins/furan s an dPCBs ; SW-84 6 Metho d001 0 fo r semivolatil e organics ; SW-84 6 Metho d003 0 fo r

volatil e organics ; andCEM S lo r Oj , CCK . CO , NO, , SO, , an dTHC . Mr , Fuch s als o manage dan d participate di n tli e preparatio n ofth e report . • Projec t

Manager , EG&G , TOCD FLIC 2 V X ATB , Februar y 2004 , Tooele , UT . Th e TOCD FLIC 2 exhaus t wa s simultaneousl y sample db y U.S . EP A Metho d5/SW-84 6 Metho d0050 ; U.S . EP A Metho d29 ; SW-84 6 Metho d0023A ; SW-84 6 Metho d001 0 fo r semivolatil e organics ; SW-84 6 Metho d001 0 fo r lot aI Organi c Emissions ; SW-84 6 Metho d0040 ; SW-84 6 Metlio d00 3 I for volatil e organics ; an dCEM S fo r CO? , NO, , SO: , an d THC . Mr . Fuch s serve da s the Projec t Manage r

fo r thi s tria l bu man dprovide don-sit e supervisio n ofth e performanc e ofth e tria l bum . Mr , Fuch s wa s responsibl e fo r providin g dail y samplin g dataan dupdate s fo r th e performanc e ofth e tria l burns . He . manage dan dparticipate di n th e preparatio n ofth e Samplin g an dAnalytica l Report fo r th e EIC 2 V X A'FB .



### VES019293 b• Projec t Manager , Veoli aEnvironmenta l Services , Confirmator y Performanc e Test , 2011 , Sauget , IL . Mr . Fuch s serve das th

e Projec t Manage r

fo r th e Confirmator y Performanc e Test s (CfPTs ) require db y th e HW C M ACT . I

n thes e test s the incinerato r exhaus t wa s sample dby U.S . EP A Metho d002 3 Afo r dioxins/furans . Mr . Fuch s worke dclosel y wit hVeolia , an dwa s th e primar y autho r

ofth e tes t

plan an dQAPP , an dh e manage dand participate di n the preparatio n ofth e final report s an dpreparatio n ofth e Notificatio n o f Compliance . • Projec t

Manager , Veoli aEnvironmenta l Services , CP T an dRCR APeriodi c Testing , Decembe r 2011 , Por t Arthur , TX , Mr . Fuch s serve das th e Projec t Manage r

fo r th e CPT ' fo r

th e Fina l Replacemen t Standard s o f

the I IW C MAC T an dthe RCR APeriodi c Testing . I n thes e test s the incinerato r exhaus t wa s simultaneousl y sample d b y U.S . EP A Metho d5/26A , U.S . EP A Metho d29 , SW-84 6 Metho d0023 A fo r dioxins/furans , SW-84 6 Metho d 006 1 fo r Cr(VT) . an dCEM S fo r NO , an dTFIC . Mr , Fuch s worke dclosel y wit hVeolia , an dwa s the primai y autho r ofth e tes t

pla n an dQAPP . Mr . Fuch s provide don-sit e supervisio n ofth e performanc e ofth e tests . Fi e manage d an dparticipate din . th

e preparatio n ofth e final report s an dpreparatio n o f tli e Notificatio n o f

Compliance .



# UR S Piige 3 

### VES019293 C

# VES019294.pd fUNITE D STATE S ENVIRONMENTA LPROTECTIO NAGENC Y REGIO N 5 7 7 WES TJACKSO N BOULEVAR D CHICAGO , I L 60604-359 0 

# [SE P2 7 

# 2013 ] REPL

Y T O TH E ATTENTIO

N OF : Dougla s Harris , Genera l Manage r Veoli aE S Technica l Solutions , L.L.C . 7 Mobil e Avenu e Sauget , Illinoi s 6220 1 Re : Veoli aE S Technica l Solutions , L.L.C.' s Comprehensiv e Performanc e Tes t Plan s fo r Incinerator s 2 , 3 , an d4 Dea r Mr . Harris : Veoli aE S Technica l Solutions , L.L.C . (Veolia ) submitte dit s Comprehensiv e Performanc e Tes t (CPT ) plan s an dQualit y Assuranc e Projec t Pla n (QAPP ) fo r

Incinerator s 2,3 , an d4 at it s Sauget , Illinoi s facilit y t o th e U.S . Environmenta l Protectio n Agenc y o n Septembe r 5 , 2012 . Veoli ai s requhe dt o conduc t aCP T pursuan t

t o th e Clea n Ai r

Ac t (CAA ) Nationa l Emissio n Standard s fo r

Hazardou s Ai r

Pollutant s fro mHazardou s Wast e Combustors , 4 0 C.F.R . Par t 63 , Subpar t EE E(HW C MACT) . Prio r t o commencin g th e CPT , Veoli amus t submi t acomplet e C P T pla n fo r

eac hincinerato r

t o EP Afo r

revie w an dapprova l o r inten t t o deny , a s require db y 4 0 C.F.R . § 63.1207(e) . Th e HW C MAC T list s specifi c informatio n tha t hazardou s wast e combustor s mus t

provid e i n thei r

CP T plans . EP Adiscovere dtha t Veolia' s Septembe r

5,201 2 C P T plan s wer e missin g require dinformation , s o o n Ma y 13,201 3 EP Anotifie dVeoli ao f it s inten t t o den y th e approva l o f it s Septembe r

5 , 201 2 CP T plan s an dprovide dsignifican t comments . I n respons e t o EPA' s notic e an dcomments , numerou s email s an dconversations , an d a n inclusio n o f

amodifie d26 A testin g metho dt o establis hHCI /CI 2 (tota l chlorine ) operatin g paramete r

limits , Veoli asubmitte drevise dCP T plan s o n Septembe r 26 , 2013 . EP Afind s tha t th e revise dCP T plan s an dQAP Pare complete , a s require db y th e HW C MACT . Therefore , EP A approve s Veolia' s Septembe r 26,201 3 revise dCP T plan s an dQAPP , fo r Incinerator s 2 , 3 , an d4 . EPA' s approva l ofth e Septembe r 26 , 201 3 tes t

plan s i s solel y fo r

th e purpos e o f

conductin g a C P T consisten t

wit hth e HW C MACT . I f Veoli aintend s t o rel y o n th e performanc e tes t t o establis hamercur y syste mremova l efficienc y fo r Veolia' s RCR Apermit , Veoli ashoul dconsul t wit hth e appropriat e RCR Apermittin g authorit y befor e finalizin g it s CP T plans . E P Awoul dals o lik e t o clarif y that th e Agency' s approva l o f thi s CP T pla n o r

lac k o f commen t o n ancillar y reference s i n th e CP T plan , suc ha s Veolia' s Feedrat e Analysi s Plan , descriptio n o f it s fee dstreams , o r

extrapolatio n methods , shoul dno t b e deeme dt o b e approva l o f suc hancillar y references . Furthermore , EP Awoul dlik e Veoli at o b e awar e tha t "demonstrat e compliance, " a s use di n th e CP T plan , relate s t o stac k emission s correspondin g t o fee drate s use ddurin g th e CPT . I t doe s no t

guarante e o r

confir mpas t

o r futur e complianc e wit hth e HW C MACT . EP Abelieve s th e result s o f

th e CP T ca n demonstrat e complianc e at th e tim e ofth e CP T du e t o th e rigorou s
Recycled/Recyclabl e • Printe d wit h Vegetabl

e Oi l Base d Ink s o n 100 % Recycle

d Pape r(100 % Post-Consumer

)wast e fee dsamplin g conducte dprio r t o an ddurin g th e test . However , base dupo n a n EP A investigatio n o f

Veolia' s Sauge t

facility , i t

i s apparen t

tha t thi s typ e o f

comprehensiv e wast e strea msamplin g i s no t don e o n aday-to-da y basi s at Veolia . I f yo u hav e an y question s regardin g thi s response , pleas e contac t Shanno n Downe y at

(312 ) 353
- 215 1 o r Eleano r Kan e at (312 ) 353-4840 , o f

m y staff . Sincerely ,

Sar aBrenema n Chie f A i r Enforcemen t

an dComplianc e Assuranc e Branc h

2



### VES01929 5

# VES019296.pd f

### Pre-draf t permi t discussio n Veoli a Renewa l Permi t Septembe r30,201 4 

### Nam e Compan y Phon e emai l Davi d Ogule i EP A 312-353-098 7 ogulei.david@epa.go v Jan e Woolum s EP A 312-886-672 0 woolums.jane@epa.go v Geneviev e Damic o EP A 312-353-476 1 d a m ico.genevieve@epa.go v Andre a Morga n EP A 312-353-605 8 morgan.andrea@epa.go v

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VES01929 6

# VES019297.pd fi ; UNITE D STATE S ENVIRONMENTA LPROTECTIO NAGENC Y REGIO N5 I NTH E MATTE ROF : Veoli aEnvironmenta l Service s #7 Mobile'Avenue" " , ;; , , v ,...,_,,„ : ,.,, , ,., j . Sauget , Illinoi s 6220 1 ATTENTION : Dou g Harri s Genera l Manage r

Reques t t o Provid e Informatio n Pursuan t t o th e Clea n Ai r

Ac t Th e U.S . Environmenta l Protectio n Agenc y i s requirin g Veoli aEnvironmenta l Service s (Veoli ao r

you ) t o submi t

certai n informatio n abou t you r faciht y at

# 7 Mobil e Avenue , Sauget , Illinois . Appendi x A provide s th e instruction s neede dto answe r thi s informatio n request , includin g instruction s fo r electroni c submissions . Appendi x B specifie s th e infonnatio n that you . ; mus t submit . Yo u mus t

sen dthi s informatio n t o u s withi n 1 4 calenda r day s afte r

yo u receiv e thi s reques t W e are issuin g thi s informatio n reques t unde r sectio n 114(a ) o f

th e Clea n Ai r

Ac t (the Act) , 4 2 U.S.C . § 7414(a) . Sectio n 114(a ) authorize s th e Administrato r o f EP At o requir e th e submissio n o f

information.

- Th e Arljninistrato r ha s delegate dthi s authorit y t o th e Directo r o f th e Ai r an dRadiatio n Division , Regio n 5 . Veoli aown s an doperate s hazardou s wast e incinerator s at th e Sauget , Illinoi s facility . W e ar e requestin g thi s informatio n t o determin e whethe r you r emissio n sourc e i s complyin g wit h th e Hazardou s Wast e Combusto r MACT .



### VES01929 7Veoli amus t sen dal l require dmformatio n to : Attn : Complianc e Tracker , AE-17 J A i r Enforcemen t

an dComplianc e Assuranc e Branc h U.S . Environmenta l Protectio n Agenc y Regio n 5 7 7 WestTacksb n Boulevard : • • - .

- Chicago , Illinoi s 6060 4 Veoli amus t

submi t al l require dinformatio n unde r a n authorize dsignatur e wit hth e followin g certification : I certify unde r

penalt y o f

la w that I hav e examine dan da mfamilia r wit hth e infonnatio n i n th e enclose ddocuments , includin g al l attachments . Base do n m y inquir y o f

thos e individual s wit hprimar y responsibilit y fo r obt^nin g th e information , I certify that th e statement s an dinformatio n are , t o th e bes t o f m y knowledg e an dbelief , tru e an dcomplete . I a mawar e tha t ther e are significan t penaltie s fo r

knowingl y submittin g fals e statement s an dinformation , includin g th e possibilit y o f

fines o r imprisonmen t

pursuan t

t o Sectio n 113(c)(2 ) ofth e Clea n A i r Ac t an d1 8 U.S.C . § § 100 1 an d1341 . A s explaine dmor e full y i n Appendi x C , yo u ma y assert aclai mo f

busines s confidentialit y unde r

4 0 C.F.R . Par t

2 , Subpar t

B fo r an y par t ofth e informatio n you - submi t t o us . Informatio n subjec t t o abusines s confidentialit y clai mi s availabl e t o th e publi c onl y t o th e extent , an db y mean s o f th e procedures , set

fort hat 4 0 C.F.R . Par t

2 , Subpar t

B . I f yo u d o no t assert abusines s confidentialit y clai mwhe n yo u submi t th e information , EP Ama y mak e thi s iriformatio n availabl e t o th e publi c withou t furthe r notice . Yo u shoul db e aware , moreover , that pursuan t t o Sectio n 114(c ) ofth e CA Aan d4 0 C.F.R , § 2.301(a ) an d(f) , emission s data , standard s an dlimitation s ar e no t entitle dt o confidentia l treatmen t an dshal l b e mad e availabl e to th e publi c not^mstandin g an y assertio n o f abusines s confidentialit y claim . Appendi x C provide s additiona l informatio n regardin g tb e meanin g an dscop e ofth e ter m"emission s data. "Thi s iiiforrnatio n reques t i s no t subjec t t o th e Paperwor k

Reductio n Act , 4 4 U.S.C . § 350 1 et seq., becaus e i t

seek s collectio n o f

infonnatio n fro mspecifi c individual s o r entitie s a s par t

o f a n administrativ e actio n o r investigation . W e may/us e an y inforrnatim ^ t o thi s reques t i na n administrative , civi l o r crimina l action . Failur e t o compl y full y wit hthi s informatio n reques t ma y subjec t

Veoli at o a n enforcemen t

actio n unde r

Sectio n 11 3 o f

th e CAA , 4 2 U.S.C . § 7413 . Y o u shoul ddirec t

an y question s abou t

thi s informatio n Reques t t o Shanno n Downe y at (312 ) 353-215 1 an ddownev.shannon@epa.go v o r Eleano r Kan e at (312 ) 353-484 0 an d kane,eleanor(5),epa.gov .

Dat e A i r an dRadiatio n Divisio n