'~ 

J 

Compliance 

Anaheim 

March 

Test Results 

Plating, Inc. 

29, .1993 

Chemical Data Management 

11750 Dublin Blvd. 

Suite 201 

Dublin, California 
SOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 

21865 East Copley Drive, Diamond Bar, CA 91765 

PERMIT TO OPERATE 

CONTINUATION OF PERMIT TO OPERATE 

NOTICE 

049391 

A/N2S0329 

Page 2 

IN ACCORDANCE WITH RULE 206, THIS PERMIT TO OPERATE OR COPY SHALL BE POSTED ON OR 

WITHIN 8 METERS OF THE EQUIPMENT. 

THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE 

ALLOWED BY DMSION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR 

THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICT. THIS PERMIT CANNOT BE 

CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR 

STATUTES OF OTHER GOVERNMENT AGENCIES. 

ORIGINAL 

EXECUTIVE OFFICER 

~/l-h By Dorris M. Bailey /rgc 

3/09/1992 
y SOUTH COAST AIR QUAUlY MANAGEMENT DISTRICT 

21865 East Copley Drive, Diamond Bar, CA 91765 

PERMIT TO OPERATE 

D49391 

A/N250329 

Page 1 

This initial permit must be renewed ANNUALLY unless the equipment is moved, or changes ownership. 

If the billing for annual renewal fee (Rule 301.£) is not received by the expiration date, contact the District. 

Legal Owner 

or Operator: ANAHEIM PLATING INC 

928 E SOUTH ST 

ANAHEIM, CA 92805 

ATTN: DIEGO BARRIGA 

Equipment Location: 928 E SOUTH ST, ANAHEIM, CA 92805 

Equipment Description: 

ID 086444 

TANK NO.8, COPPER PLATING, 4'-0" W. X 9'_0" L. X 4'-0" D., WITH 6 VOLTS AND 2000 AMPERES 

RECTIFIER, UNHEATED. 

Conditions: 

1. OPERATION OF THIS EQUIPMENT SHALL BE CONDUCI'ED IN ACCORDANCE 

WITH ALL DATA AND SPECIFICATIONS SUBMITTED WITH THE APPUCATION 

UNDER WHICH THIS PERMIT IS ISSUED UNLESS OTHERWISE NOTED BELOW. 

2. THIS EQUIPMENT SHALL BE PROPERLY MAINTAINED AND KEPT IN GOOD 

OPERATING CONDmON AT ALL TIMES. 

3. THIS EQUIPMENT SHALL NOT BE OPERATED UNLESS IT IS VENTED ONLY 

TO AN AIR POLLUTION CONTROL EQUIPMENT WHICH HAS BEEN ISSUED A 

PERMIT TO OPERATE BY THE EXECUTIVE OFFICER. 

4. THE WEIGHT CONCENTRATION OF THE CHEMICALS SHALL NOT EXCEED THE 

FOLLOWING SPECIFIED AMOUNT: 

COPPER SULFATE- 20% 

SULFURIC ACID- 10% 

ONLY THE CHEMICALS SPECIFIED ABOVE SHALL BE USED IN THIS 

EQUIPMENT. 

5. THE OPERATOR SHALL RECORD THE CONCENTRATION OF THE CHEMICALS IN 

THE TANK DURING REPLENISHMENT. THE RECORDS SHALL BE MAINTAINED 

FOR A PERIOD OF TWO YEARS AND MADE AVAILABLE TO DISTRICT 

PERSONNEL UPON REQUEST. 

ORIGINAL 
SOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 

21865 East Copley Drive. Diamond Bar. CA 91765 

PERMIT TO OPERATE 

CONTINUATION OF PERMIT TO OPERATE 

NOTICE 

Page 2 

IN ACCORDANCE WITH RULE 206, THIS PERMIT TO OPERATE OR COpy SHALL BE POSTED ON OR 

WITHIN 8 METERS OF THE EQUIPMENT. 

THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE 

ALLOWED BY DIVISION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR 

THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICI'. THIS PERMIT CANNOT BE 

CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR 

STATUTES OF OTHER GOVERNMENT AGENCIES. 

ORIGINAL 

EXECUTIVE OFFICER 

tft11.w..; 

By Dorris 

I), 

M. Bailey 

~ 

/rgc 

3/09/1992 
\ 

SOUTH COAST AIR QUALIlY MANAGEMENT DISTRICT 

21865 East Copley Drive, Diamond Bar, CA 91765 

PERMIT TO OPERATE 

rennUNO. 

D49390 

A/N250328 

Page 1 

This initial permit must be renewed ANNUALLY unless the equipment is moved, or changes ownership. 

U the billing for annual renewal fee (Rule 3OlJ) is not received by the expiration date, contact the District. 

Legal Owner 

or Operator: ANAHEIM PLATING INC 

928 E SOUTH ST 

ANAHEIM, CA 92805 

AnN: DIEGO BARRIGA 

Equipment Location: 928 E SOUTH ST, ANAHEIM, CA 92805 

Equipment Description: 

ID 086444 

TANK NO.7, COPPER PLATING, 4'-0" W. X 7'-6" L. X 4'-0· D., WITH 6 VOLTS AND 2000 AMPERES 

RECI'IFIER, UNHEATED. 

Conditions: 

L OPERATION OF THIS EQUIPMENT SHALL BE CONDUCI'ED IN ACCORDANCE 

WITH ALL DATA AND SPECIFICATIONS SUBMITTED WITH TIlE APPUCATION 

UNDER WHICH THIS PERMIT IS ISSUED UNLESS OTHERWISE NOTED BELOW. 

2. THIS EQUIPMENT SHALL BE PROPERLY MAINTAINED AND KEPT IN GOOD 

OPERATING CONDITION AT ALL TIMES. 

3. TIllS EQUIPMENT SHALL NOT BE OPERATED UNLESS IT IS VENTED ONLY 

TO AN AIR POLLUTION CONTROL EQUIPMENT WHICH HAS BEEN ISSUED A 

PERMIT TO OPERATE BY THE EXECUTIVE OFFICER. 

4. THE WEIGHT CONCENTRATION OF THE CHEMICALS SHALL NOT EXCEED THE 

FOLLOWING SPECIFIED AMOUNT: 

COPPER SULFATE- 20% 

SULFURIC ACID- 10% 

ONLY THE CHEMICALS SPECIFIED ABOVE SHALL BE USED IN THIS 

EQUIPMENT. 

5. THE OPERATOR SHALL RECORD THE CONCENTRATION OF THE CHEMICALS IN 

THE TANK DURING REPLENISHMENT. THE RECORDS SHALL BE MAINTAINED 

FOR A PERIOD OF TWO YEARS AND MADE AVAILABLE TO DISTRICT 

PERSONNEL UPON REQUEST. 

ORIGINAL 
SOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 

21865 East Copley Dnve, Diamond Bar, CA 91765 

PERMIT TO CONSTRUCT/OPERATE 

C~NTlNUATlONOFPERMIT TO CONSTRUCf/OPERATE 

NOTICE 

PennilNo. 

D70356 

A/N278389 

IN ACCORDANCE WITH RULE 206, TIllS PERMIT TO OPERATE OR COPY SHALL BE POSTED ON OR 

WITHIN 8 METERS OF THE EQUIPMENT. 

THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE 

ALLOWED BY DMSION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR 

THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICf. THIS PERMIT CANNOT BE 

CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR 

STATUTES OF OTHER GOVERNMENT AGENCIES. 

ORIGINAL 

EXECUTIVE OFFICER 

By Dorris M. Bailey /rgc 

2/25/1993 
EXECUTIVE SUMMARY 

Anaheim Plating. Inc. of Anaheim, California is'required by permit 

conditions to conduct a source compliance lest. The results are to be 

reported to the South Coast Air Quality Management District 

(SCAQMD) located in Diamond Bar. The company has one decorativ e 

chrome plating lank with process gases wh ich ex haust first through a 

sin gle scrubber and th en through a 20 inch diameter stack. The 

emISSIOn point is approx imate ly 25 feet hi g h. 

The test is being conduc ted by Che mi cal Dara Ma nagement Systems 

of Dublin , Californi a. The test methods be ing used are based on those 

developed under the direction of the California A ir Resources B oard 

(CARB) and are referred to as CARB Method 425. The SCAQMD 

slightly modified the procedure in method 205. 1. It is the modi fied 

SCAQM D version which we wi ll be usin g. 

The enclosed samplin g protocol provides a detec tion leve l of less 

than .001 mg/amp-hr for hexava lent c hromiu_m. Anahe im Plating. 

Inc. is permitted to emit 0.03 mg/amp hr. 

The foll owin g lest results were obtained: 

To tal Chrome Hex Chrome 

(amp hr (amp hr) 

Tesl # 1 0.00247 1 0.000302 

Test #2 0 .00 1555 0.000283 

Two tests were run , each lasting 5 hours. Anaheim Plating performs 

its operations using 50 amps per hour or less. At Ihis rale, using the 

highest emissions rate per amp hour, the emissions of hex avalent 

chromium would be 0.0151 mg/amp hour. This is well below the 

pe rmitted level of 0.0378 

Between tests, a was h down was performed as described in 

conditi ons #6 and #8. During the lests, pe ri od ic monitoring of the 

static differenlial pressure ga uges mou nted on the scrubber housin g 

showed that th e diffe rential pressure did not exceed 4.5 inches of 

water across th e scrubbed (conditi ons #9 and #10). Smoke te sts 

showed that the fume hood captured all vapors emitted from the 

chrome tank surface. 

Anaheim Pl ating. Inc. Apri l 11. 1993 Page 1 
Results Test run #1 

Anaheim Platin 3.29.93 Test #t 

Diameter 0.238 inches Ms 28.60 Y 1.00 

An 0.0003 1 sq It Pbar 30.04 inches Hg Tstd 528 .00 Rankin 

Bws 0.02 Pq 0.45 inches HQ As 5.24 sq It 

Cp 0.84 coefficient Ps 30.07 inches Hg Ds 31.00 inches 

Kp 85 .49 constan t Pstd 29.92 inches Hg Ts(avg) 530.63 Rankin 

Mel 29 .00 • 300 .00 minutes Pv(avg) 0.48 

Tm(ave) 537.49 Rankin 

Amperage 250 Vm 213 .92 cu ft CRtotal 0.000 180 mg 

Vm(s td) 211.22 cu It CRhex 0.000022 mg 

Vo 42 .24 cu fVhr CRtperamphr 0.002471 mg/amp-hour 

I 98.8722 Om 43 .59 cu fVhf CRhperamphr 0.000302 mg/amp-hour 

. Vs 39.21 ft/sec 

Ostd 724 .872 cu fVhr 

Vratia 17 .159.12 

Page 1 
SOURCE TEST PLAN SUMMARY 

Company Information 

Company Name Anaheim Plating, Inc. 

Contact Gabriel Barriga 

Address 928 East South Street 

City, State Anaheim, CA 

Phone (714) 776-3597 

Source Information 

Type of Unit single tank, single stack 

Purpose Chrome plating of car wheel rims 

Testing Firm Information 

Company Name Chemical Data Management Systems 

Contact Ed Lewis - Address 11750 Dublin Blvd. 

City--, State Dublin, Ca 94568 

Phone (510) 551-7310 

Testing Information 

Procedure Used 

St ac k D escnp ° to IOn 

Stack Height 

Stack Diameter 

Sampling Ports 

Samplin2 Platform 

SCAQMD Method 205.1, Determination of 

hexavalent chromium and total chromium 

emissions from chrome plating and 

anodizing equipment using a wet 

impingement train. 

25 feet 

20 inch Diameter inches 

2 sampling ports located 90 degrees apart 

which comply with the modified 8 and 2 

rule (2 and 0.5 minimum) 

Roof Access 

Anaheim Plating, Inc. April 11. 1993 Page 2 
Sampling point locations 

T raverse P OlD . t S - d ou bl e por t s oca t d t e a 90° ang es 

Point Number % of Diameter Inches From Edge 

1 2.1 1 

2 6.7 1.3 

3 11.8 2.3 

4 17.7 3.5 

5 25.0 5.0 

6 35.6 7.12 

7 64.4 12.9 

8 75.0 15.0 

9 82.3 16.5 

10 88.2 17.6 

1 1 93.3 18.5 

12 97.9 19.0 

Anaheim Plating. Inc. April 11. 1993 Page 3 
Stack Gas Co nditi ons for run #1 

Stack Temperature ambient 

Expected Pitot Head 0.1 inches of H2O , -

Gas Velocity 39.21 ft/sec 

Stack Area (3. I 4 )(20/2) 2(1 / 144) ; 2.18 ft2 

Volume Flow Rate 724,872 cu ft/hour 

Wa ter Vapor 2% 

Oxygen 20.9% 

Carbon Dioxide 0.0% 

Barometric Press ure 30.04 

Molecular Weight Air 29.0 

Nozz le Diameter/Area 0.0.235 inches ; 0.000301 ft2 

Sample Volume 213.92 ft 3 

Appli ed Ampera ge 50 

Time at Each Point 12.5 minutes 

Total Sample Time 300 minutes ; 5.0 hr 

Total Charge per Run 250 

Process Cycle 100% 

Detection Limit 0.0002 8 

mg/amp-hr , 

Anaheim Plating, Inc. April II, 1993 Page 4 
Stack Gas Co nditions (estimate s) for run #2 

Stack Temperature ambient 

Expected PiLOt Head 0.1 inches of H2O 

Gas Velocit y 36.3 7 ft/sec 

Stack Area (3 . 14)(20!2)' (I1144) = 2.18 ft' 

Volume Flow Rate 680,396 cu ft/hour 

Water Vapor 2% 

Oxygen 20.9% 

Carbon Dioxide 0.0% 

Ba rometr ic Pressure 30.04 

Molec ular Weigh t Air 29.0 

Nozz le Diameter/Area 0.0.235 inches = 0.000301 ft' 

Sample Volume 191.23 ft3 

Applied Amperage 500 

Time at Each Point 12 .5 minutes 

Total Sample Time 300 minutes - 5.0 hr 

Total Charge per Run 2,500 

Process Cycle 100% 

Detection Limit 0.0000 I 

mg / amp - hr 

Anaheim Plating , Inc . April 11. 1993 Page 5 
Source Test Constituent and Methods 

Contaminant Sampling Method Analytical Method 

Total chromium SCAQMD Method 205.1 AA 

Hexavalent chromium SCAQMD Method 205.1 Ion 

Detection Limit Calculation 

see attached calculation sheet 

Detection Limit Test #1 = 0.00028 mg/amp-hr 

Detection Limit Test #2 = 0.00001 mg/amp-hr 

Exceptions 

Graphite Furnace 

chromatography 

Approved SCAQMD method 205.1 sampling methods will be followed 

with the following exceptions: 

1 ) Filter unit will be placed between the second and third 

impingers. The third impinger is fitted with a thermo coupler for 

continuous monitoring of sample gases to insure that the 

temperature stays below the dew point. With the filter unit in this 

position contamination of the thermo coupler is avoided. 

Anaheim Plating, Inc. April 11, 1993 Page 6 
Stack Test Protocol 

Following is the protocol that was used for chrome stack testing at 

Anaheim Plating. The protocol is based on the SCAQMD method 205.1 

The procedure is used to provide engineering data to the operators 

and to provide compliance data to the District. For this test two 

sample trains are run. The propose of the test is to show compliance 

with permit conditions. 

Tank Process Conditions 

1. Parts in the tank are typical of what are run on a regular basis. 

2. Tank temperature is to be consistent with normal plating 

practices. 

3. Typical amperage will be applied to the tank during one test 

run. During the other test, the amp~rage will ~ be increased to the 

maximum amperage which can be safely applied. 

Test Protocol: 

1. The purpose of this test is to determine the emISSions of 

hexavalent and total chromium per amp-hour of plating based on 

specific plating tank process conditions. 

2. The test method is based on the SCAQMD Method 205.1. 

3. SCAQMD Methods are' used to determine stack gas velocity, dry 

molecular weight, and moisture content. 

4. Isokinetic sampling is used. Air flow is calculated from 

pressure drops measured using a Dwyer Microtector Portable 

Electronic Point Gage and a 5/16" standard Pitot tube of appropriate 

length. 

5. The sample train (see attached drawing) components are made 

of glass or Teflon and a Teflon fiber filter. Neither the probe or the 

filter are heated since duct temperatures are near ambient. 

Anaheim Plating, Inc. April II, 1993 Page 7 
6. Two sets of three impingers are used. For each set the first two 

impingers contain 100 milliliters each of 0.02N NaHC03. The third 

impinger is empty, except for a thermocouple. 

7. An 11 centimeter diameter Teflon fiber filter In an appropriate 

filter holder follows the second impinger. 

8. A drying column is used to dry the air after it leaves the third 

ImpInger. 

9. Flow through the impingers is measured using a Dwyer Series 

RM Flowmeter. Flow is created using a Dayton Speedaire Oil-less 

Vacuum Pump. Volume is measured using a Rockwell Test Meter S275. Temperature is measured using Ashcroft Bi-Metal Dial 

Thermometers. Barometric readings are obtained from the weather 

service of the local airport. 

1 a. After collecting the samples, each sample train is capped and 

transported to the laboratory. No field cleaning of the train is done. 

The laboratory that is' used is West Coast AnalYtical of Santa Fe 

Springs (714-776-3597.). They are approved by various South Coast 

regulatory agencies and have received state certification under the 

new state certification plan. Their resume is available upon request. 

11. Train rinse is performed using a.OlN NaHC03. The filter is acid 

digested. 

12. Determination of hexavalent chromium is done colorimetrically. 

Minimum detection level is 2 parts per billion (2 ppb). 

13. Total chromium will be determined by digesting the sample in 

concentrated nitric acid followed by the Ie method described in 

§3.7.2 of method 205.1. Minimum detection level is 0.01 parts per 

billion. 

Anaheim Plating. Inc. April 11. 1993 Page 8 
QA / QC 

1. The sample train is rinsed at the laboratory with nltnc acid, 

filled with the appropriate solutions, capped or I sealed and 

transported to the test site. 

2. Blanks and spike samples are prepared by the laboratory, 

transported to the site and returned to the laboratory for analysis. 

3. Samples are analyzed within 48 hours of arrival at the 

laboratory. 

4. Components of the sample train that require calibration are 

returned to the supplier/manufacturer: 

Yearly or, 

If they are inconsistent with other readings or 

If error is suspected 

5. All test equipment is identifi~ble by serial number. 

6. Chain of custody forms are initiated at the test site. The forms 

follow the sample train from the job site, to the lab, through the lab 

and are attached to the lab results. 

Attachments: 

Results Test 1 

Results Test 2 

Stack Test Equations 

Laboratory Results 

Field Data Notes 

Facility Location Drawing 

Sample Train Drawing 

Schematic flow diagrahm 

Detection limit calculations 

Permit to construct/operate 

Scrubber description 

Copy of Chain of Custody 

Air Meter Calibration 

Form ST-2 

Anaheim Plating. Inc. April II. 1993 Page 9 
Results Test run #1 

Pv Ts am Tmi Tmo Meter 

Start 110.78 

1 0.50 13.60 43.74 74 70.00 119.80 

2 0.70 22.60 52.56 88 78.00 129.40 

3 0.60 22.60 48.66 88.00 68.00 140.80 

~ 0.60 21.70 48.59 90.00 68.00 150.90 

5 0.60 20.40 48.48 89.00 70.00 161.20 

6 0.40 24.80 39.88 88.00 70.00 169.40 

7 0.50 19.70 44.20 82.00 66.00 178.40 

8 0.60 19.30 48.39 80.00 64.00 187.80 

9 0.80 19.20 55.87 80.00 64.00 199.70 

10 0.50 19.60 44.20 82.00 64.00 208.60 

11 0.50 20.10 44.23 83.00 66.00 217.90 

12 0.50 21.40 44.33 88.00 66.00 227.10 

13 0.40 21.70 39.67 87.00 69.00 235.30 

14 0.50 21.2 44.32 84.00 69.00 244.60 

15 0.40 19.70 39.54 85.00 69.00 252.90 

16 0.50 23.30 44.48 83.00 72.00 261.00 

17 0.60 23.90 48.77 93.00 72.00 272.00 

18 0.40 26.00 39.96 97.00 73.00 280.40 

19 0.30 26.40 34.63 95.00 t 75.00 287.70 

20 0.30 25.50 34.58 . 90.00 75.00 294.70 - 21 0.40 21.40 39.65 80.00 70.00 302.40 

22 0.40 22.70 39.74 81.00 70.00 310.50 

23 0.30 19.70 34.24 80.00 69.00 317.60 

24 0.30 18.50 34.17 78.00 66.00 324.70 

Page 2 
Results Test run #2 

Anaheim Plating 3.29.93 Test #2 

Diameter 0.238 Inches Ms 28.60 Y 1.00 

An 0.00031 sq ft Pbar 30.04 inches Hg Tstd 528.00 Rankin 

Bws 0.02 iPg 0.45 Inches Hg As 5.24 sq ft 

Cp- 0.84 coefficient Ps 30.07 inches Kg Os 31.00 inches 

Kp 85.49 constant Pstd 29.92 inches Hg Ts(avg) 524.39 Rankin 

Md 29.00 " 300.00 minutes Pv(avg) 0.42 

Tm(avg) 527.10 Rankin 

Amperage 2500 Vm 191.23 cu ft CRtota! 0.001100 ffiR 

Vm(std) 192.54 cu ft CRhex 0.000200 mg 

Vo 38.51 cu ftlhr CRtperamphr 0.001555 mg/amp-hour 

I 96.0174 Om 40.44 cu ftlhr CRh~eramphr 0.000283 mg/amp-hour 

. Vs 36.37 ft/sec 

Ostd 680,396 cu ftlhr 

Vratlo 17,669.30 

Page 1 
Results Test run #2 

Pv Ts am Tmi Tmo Meter 

Start 332.57 

1 0.20 18.60 27.90 78 61.00 338.40 

2 0.30 16.,90 34.08 70 60.00 345.40 

3 0.30 18.50 34.17 71.00 61,.00 352.60 

4 0.40 19.40 39.52 73.00 60.00 360.80 

5 0.40 18.60 39.46 73.00 61.00 368.90 

6 0.40 17.70 39.40 72.00 60.00 377.10 

7 0.30 15.90 34.02 70.00 58.00 384.30 

8 0.30 16.40 34.05 72.00 58.00 390.90 

9 0.30 15.40 33.99 72.00 58.00 398.50 

10 0.40 16.50 39.32 72.00 58.00 406.60 

11 0.40 17.20 39.37 77.00 58.00 414.80 

12 0.40 17.40 39.38 78.00 58.00 423.10 

13 0.40 18.00 39.42 70.00 58.00 431.40 

14 0.40 18.9 39.48 76.00 58.00 439.50 

15 0.40 19.10 39.50 86.00 60.00 448.80 

16 0.50 19.70 44.20 80.00 60.00 457.50 

17 0.50 19.00 44.15 80.00 61.00 466.70 

18 0.50 18.80 44.14 80.00 62.00 475.80 

19 0.60 19.70 48.42 78.00 ~ 62.00 486.10 

20 0.60 18.10 48.29 . 76.00 61.00 496.00 . 21 0.60 18.10 48.29 77.00 60.00 506.20 

22 0.50 18.00 44.08 75.00 60.00 515.50 

23 0.50 17.90 44.07 74.00 59.00 524.60 

24 0.50 18.00 44.08 76.00 60.00 523.80 

Page 2 
Stack Test Equations 

Amperage = Amperage applied to tanks 

AN = Cross sectional area of. nozzle 

As = Cross sectional area of stack 

Bws = Water vapor in the gas stream 

Crhex = Hex chrome collected 

Crhperamphr= Crhex * VRatio * 60/ (Amperage * 9) 

Crtotal = Total chrome collected 

Crtotalperamphr= Crtotal * VRatio * 60/ (Amperage * 9) 

Cp = Pitot tube coefficient = 0.84 

TS(AVg) V (Id)P sid 1 00 I = Isokinetic Variation = m 5 

Tsld Vs9AnPs 60(1- Bws) 

K - P' be 8549 ft [(Ibllb-mole)(in.HG)f

12 

p - 1tot tu constant . - (0)(. ) sec R lD.H20 

Md = Molecular weight of stack gas, dry basis = 29.0 

Ms = Molecular weight of stack gas, wet basis 

Ms = Md (l- Bws) + 18.0Bws 

P = Velocity head of stack -gas, mm H20 

P bar = Barometric pressure at measurement site 

P 8 = Stack static pressure 

P 

P s = Absolute stack gas pressure = P bar + _8-

13.6 

P sid = Standard absolute pressure (29.92 in. Hg) 

ts = Stack temperature ·CCF) 

Ts = Absolute Stack temperature °K(OR) 

Ts =460 +t, 

Tsld = Standard Absolute temperature 293°K(528°R) 

9 = Total sampling time 

3,600 = Conversion Factor, seconds to hours 

18.0 = Molecular weight of water 

Y = Dry gas meter calibration factor 

V m = Meterstartreading - Meterfmishreading 

V = Sample gas volume = V Y (Pbar)(Tsld ) m(sld) m (PSld )( T m(aV8») 

V 0 = V m(sId) * (60 / 9) 

VRatio = QsId / V 0 

Vs = Average stack gas velocity, m/sec (ft/sec)= KpCp(-.jllp L8 
Q51d = Average stack gas dry volumetric rate = 3600(I-Bws )V,A,(/"" ')( P.) 

5(11\18) )lpild 

Qm = An (3600)(85. 49)(Cp) T;;:a::) 

Calculator: . 

Qm =' 1" STD' PV' STO' PS' STD' 79.87 * ((T * 1. 8 + 492) * PV I (PS * 28.6))A. S 
April 5, 1993 

CHEMICAL DATA MANAGEMENT SYSTEMS 

11750 Dublin Blvd. 

suite 201 

Dublin, CA 94568 

Attn: Ed Lewis 

JOB NO. 23630 

LABORATORY REPORT 

Samples Received: Three (3) Impinger Trains 

Date Received: 3-30-93 

Purchase Order No: Anaheim Plating 

The samples were analyzed as follows: 

Samples Analyzed Analysis 

Three (3) samples Total Chromium 

by SCAQMD 205.1 ~. 

Three (3) samples Hexavalent Chromium by 

SCAQMD 205.1 

WEST COAST 

ANALYTICAL 

SERVICE, INC. 

ANAL mCAL CHEMISTS 

D 

Results 

Data Sheet 

Data Sheet 

Page 1 of 4 

W~ Michael Shelton 

Technical Director 

J 

J 

J 

I 

I 

I D.~on, Ph.D. 

President 

This report is to be reproduced in its entirety. 

9840AlburtisAvenue • Santa Fe Springs. California 90670 • 310/948-2225 • FAX310/948-5850 
WEST COAST ANALYTICAL SERVICE, INC. 

CHEMICAL DATA MANAGEMENT SYSTEMS 

Mr. Ed Lewis 

LABORATORY REPORT 

Job # 23630 

AprilS, 1993 

Total Chromium in Impinger Train 

Quantitative Analysis Report 

Inductively Coupled Plasma-Mass Spectrometry 

Sample ID 

Blank Train 

Train #1 

Train #3 

Detection Limit 

Date Analyzed: 4/1/93 

Sample: Batch QC 

Matrix: Impinger 

ppb (ug/L) 

ND<0.6 

4.4 

0.7 

0.6 

Volume (L) 

0.235 

0.253 

0.258 

Total 

Micrograms 

ND<O.l 

1.1 

0.18 

Total Micrograms 

Sample 

Chromium 8.3 

Spike 

Cone 

ug 

142.9 

MS 

--------

170 

MSD 

% % 

Recovery Recovery -------- -------- --------

113.2 163 108.3 

Date Analyzed: 3/30/93 

Page 2 of 4 

===========~============ 

% 

RPD -------

4.2 
WEST COAST ANALYTICAL SERVICE, INC. 

CHEMICAL DATA MANAGEMENT SYSTEMS 

Mr. Ed Lewis 

LABORATORY REPORT · 

Job # 23630 

AprilS, 1993 

Hexavalent Chromium by SCAQMD 205.1 

sample Total Micrograms 

Sample Train #1 

Sample Train #3 

Blank Train 

Detection Limit 

Date Analyzed: 3/31/93 

0.20 

0.022 

NO 

0.002 

Matrix Spike/Matrix Spike Duplicate 

Sample:Train #3 

units :ppb (ug/L) 

Sample Amount MS % Rec 

Analyte Result Spiked Result MS -- Hexavalent 

Chromium 0.084 1 1.08 100 

QC Limits 

RPD 

Analyte Warning Control 

Recovery Summary 

'. 

MSD % Rec 

Result MSD 

1.1 102 

% Recovery 

Warning Control 

RPD 

2 

==================================================================== 

Hexavalent 

Chromium 9 13 86 108 

Page 3 of 4 

============~============= 

74 117 
WEST COAST ANALYTICAL SERVICE, INC. 

CHEMICAL DATA MANAGEMENT SYSTEMS 

Mr. Ed Lewis 

LABORATORY REPORT' 

sample 

Sample Train #1 

Sample Train #3 

Blank Train 

Date Analyzed: 4/1/93 

Moisture From Silica (g) 

grams 

2.0 

4.0 

0.0 

~. 

Job # 23630 

April 5, 1993 

Page 4 of 4 

============~============ 
f 

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Time Distance Pv 

Start 

1 12· ') I O'L 

2 7..~.() 1-3 ().-:... 

3 ~7. C; 2·~ (.~ 

4 [b./) 3>.~ fl.t.L 

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3.,2,57 

l?10 ~.o/' 3.2.!>. U. 338,l.} {. .0 78 

3'+.67 1-V 3'4--5.5 ~+(,q. :/.0 70 

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Vacuum Test Start 

Vacuum Test Finish 

s: / : ,)Tes~ T.eam LL! 5..L !~~ 

:. // ".) ~ 'f ! ,"" r ~O () 

Page 1 

Air Ice 

11·6 fr.& 

I Z· "!> 5·0 I~ ,~ ~.L...-

,,, .b s·] 

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·0 4,Y. 

'7~ t. '6 / " !' J ;- V s17 -/ $,( 

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-; .(),/ ". , , " 

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Time Distance 

Start !,6 ~" ... ~\ 

1 I~'C- /" 

2 ~ ,;.:- , \'S 

3 ~-r.~ 7.::-

4 SD -::-c-- -' ... 5 1··b"2.~ C".D 

6 ie:- ,.'''-

7 9:1·.s- , ") . ?": . 

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19 "A7·j I ); 

20 IOu I"~/> 

21 /12. r 1/, .. . 

22 I.: ":. () Ili 

23 17, 7.5 r~ . \ . 

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Company AN;- ~!"" ?I\ 

Date 'l/2'" 

Stack \ . . . , , " .' 

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• ·1 

\ 

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Pv Ts am Meter Calc'd 

'. o "-1 0 '-t 

(' 5 /1. L trf-'z ny }I'L~ 

0·7 7?b_ <::~ s~ III \ ~t.J ~ 

f). Co "2'2.. b 48.h,b 10/ 14-, ..n 

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0.::, "2.S. C 2,4 .60 ;i.,: 1-qlt-.'-j 

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0.3 177 3'1".24 [1.1/ 7J11. {P 

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I 

~. Test # I 

f .\ . \ .• Vacuum Test Start 

'l \. i'v Vacuum Test Finish .... \\ 

Meter Actual 

IIO.1J.6 

110,. ~ 

171 tr 

LLfa-~ 

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118 1 ,2 

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Page 1 

Vacuum Tmi Tmo Air Ice 

M tl v\ 

IDol'! 7~ 7{) 2(·L J{·5 

Z-UJ 6b ~ 212. 11-" 

"20.C- gg c..~ '2'2·0 I~.~ 

2" .0 90 bR ..,.., g --~ . , "2 • 0;., 

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CITt O£_ .. COAPoIWIOH YNII 

AHAHt.. f'V.1lHC fACUlY I!ln 

In 

[ 

CI1Y or _ ... TRAIlER 

c::J . t 

FliCNT O£ _ , 

-----~S1RttT-----

v"'""'" ,," ~ 

(NOT 10 SC>o.[) 

--------------- - ._._----------

L-JG 

SC>o.£ 

('[[11 

ANAHEIM PLA TlNG, INC. 

928 E. SOUTH ST. 

ANAHEIM. CA 

t 

DR. BY: G.P. T. 

DATE: 01-18-93 

REV. NO: 

OATE: 

BUILDING HEIGHTS 

AIR PERMIT 

CHEMICAL DATA MANACEMENT SYSTEMS 

11750 DUBLIN BL VO .• S lE ?~, ouBLIN. Clio 9~568 (510) 55~ - noo 
" , -' -....,... 

--------_._----

w 

z 

::I 

~ a:: 

w 

a. 

o 

a:: 

a. 

CHROIlAE TANK 

OUTSIDE STORAGE 

rRONT or eUllOINC 

"- ........ _ ..... __ .. _._-_._--

'0,--"," 

:.':·::::{l;li" 

~il:'\~i· ":.::: 

Duel WORK 

COPPER TANK 

NICKEL TANK 

EJ 

(FEET) 

...... '-'0-.0- ... _ ...... 1.11750 DU~LIN BlVD .• STE 7.01 DuBliN C':A Q4""'R '''In\ ..... 'o·nnf , 

I ANAHEIM PLATING, INC. I 

928 E. SOUTH ST. 

I~ ANAHEIM, CA 

! DR. BY: CPT. I REV. NO: J F" ACIU TY SI TE PLAN DATE: 01-18-93 I DATE: I AIR PERMIT 

I CHEMICAL DATA MANA CEMENT SYSTEMS , 
PILOT 

TUBE 

THERMOCOUPLE 

PROBE 

STACK 

TYPE S WALL 

PITOT TUBE 

FIGURE #1 

SAMPLE TRAIN - #2 

THERMOCOUPLE 

---' ........ _----

THERMOCOUPLE 

F"IL TER HOLDER 

BY-PASS 

VALVE 

ICE BATH 

JMPINGERS 

~ __ VACUUM 

LINE 

THERMOCOUPLE 

READOUT 

VACUUM GAUGE 

08-12-91 

MAIN VALVE 

AIR TIGHT PUMP 

CONFIDENTIAL 

DATE LTR DESCRIPTION 

C.D.M.S. T & M PRODUCTS 11750 DUBLIN BLVD .• STE 201 DUBLIN. CA 9456R 
SCHEMATIC FLOW DIAGRAM - ANAHEIM PLATING, INC. 

Sample platform 

14" from emission point to sample port 

., Do 

-Sample ports 

Stack diameter = 20" 72" from 90° bend to emission point 

56" from 90° bend to sample port 

- Scrubber fan "-_________ --1 7,000 cfm 

-

'scafolding 

Scrubber 

Anaheim Plating, Inc. (roof) 

Scrubber platform 
Detection Limit Calc 

Detection Limit Calculation 

Anaheim Plating, Inc. 

3 / 11 / 93 

24.00 

12.50 minutes 

300.00 minutes 

33.13 ft/sec 

20.00 

2.18 sq ft 

260,070.50 cu fUhr 

0.238 inch 

0.000309 sq ft 

184.14 cu ft 

500.00 amp 

2,500.00 amp 

1.00 

0.00001 mg 

0.07 mg 

0.00003 mg/amp·hr 

Number of Points 

Time Per Point 

Length of Test 

Stack Velocity (33.13 fUsee is BAAQMD minimum) 

Stack Diameter 

Stack Area 

Stack Flow Rate 

Nozzle Diameter 

Nozzle Area 

Sample Volume 

Applied Amperage 

Total Charge Per Run 

Process Cycle 

Detection Limit Calculations 

Detection limit per Sample (sample size 1 liter) 

Minimum detectable per test 

Detection limit in mg/amp-hour 

Page 1 
Detection Limit Calc 

Detection Limit Calculation 

Anaheim Plating, Inc. 

3 / 11 / 93 

24.00 

12.50 minutes 

300.00 minutes 

33. 13 ftlsec 

20.00 

2.18 sq ft 

260,070.50 cu fVhr 

0.238 inch 

0.000309 sq ft 

184 .14 cu ft 

50.00 amp 

250.00 amp 

1. 00 

0.00001 mg 

0.07 mg 

0.00028 mg/amp- hr 

Number of Points 

Time Per Point 

Length of Test 

Stack Velocity (33.13 fUsee is BAAQMD minimum) 

Stack Diameter· 

Stack Area 

Stack Flow Rate 

Nozzle Diameter 

Nozzle Area 

Sample Volume 

Applied Amperage 

Total Charge Per Run 

Process Cycle 

Detection Limit Calculations 

Detection limit per Sample (sample size 1 liter) 

Minimum detectable per test 

Detection limit in mg/amp-hour 

Page 1 
Nozzle Capacities 

T= 40 Kp= 85.49 Cp:;. 0.84 

Pbar= 29.92 Pg= 0.3 Ps= 29.9420588 

Ws 28.60 /" - Diameter i.- 0.175 ( 0.235 " ) 0.375 

Area - Sq Ft - ,..,. 0.000167 0.000301 0.0007-67 

p\/ 

0.1 11.08 19.97 50.86 

0.2 15.66 28.25 71.93 

0.3 19.18 34.60 88.09 

0.4 22.15 39.95 101. 72 

0.5 24.77 44.66 113.73 

0.6 27.13 48.93 124.58 

0.7 29.31 52.85 134.56 

0.8 31.33 56.49 143.86 

0.9 33.23 59.92 152.58 

1 35.03 63.16 160.84 

1.1 36.74 66.24 168.69 

1.2 38.37 69.19 176.19 

1.3 39.94 72.02 183.38 

1.4 41.44 74.73 190.30 

1.5 42.90 77.36 196.98 

1.6 44.31 79.8-9 203.44 - 1.7 45.67 82.35 209.70 

1.8 46.99 84.74 215.78 

1.9 48.28 87.06 221.70 

2 49.53 89.32 227.46 . 

2.1 50.76 91.53 233.07 

2.2 51.95 93.68 238.56 

2.3 53.12 95.79 243.92 

2.4 54.26 97.85 249.17 

2.5 55.38 99.87 254.30 

2.6 56.48 101.85 259.34 

2.7 57.55 103.79 264.28 

2.8 58.61 105.69 269.13 

2.9 59.65 107.56 273.89 

3 60.67 109.40 278.58 

3.1 61.67 111.21 283.18 

3.2 62.66 112.99 287.71 

3.3 63.63 114.74 292.17 

3.4 64.59 116.46 296.57 

3.5 65.53 118.17 300.90 

3.6 66.46 119.84 305.16 

3.7 67.37 121.49 309.37 

3.8 68.28 123.13 313.53 

3.9 69.17 124.73 317.63 

4 70.05 126.32 321.67 

Page 1 
SOUTH COAST AlA QUAUTY MANAGEMCM UISTRIGT 

21865 east Copfay DrIve, CAaITlOfld Bar, CA 91766 

PERMIT TO CONSTRUCT IOPERATE 

~ ANAHBJM PlATING INC 

ATJ'N: DIEGO BARRIGA 

928 E SOO1H ST 

ANAH.EIM. CA ~ 

f.4ujlptyllt DuatpIIon: 

AIR. 

1. 

1. 

mON CONTROL SYS'I'E!M CONSJS1"INO OF: 

SCRUBBER.. DUAIJ.. MODEL PWm. VJ!R.1'IC'AL TYPB, "-$ W. X S-UY' L U'-6- H.. EQUJPPIID 

W1TH.A MIST eLIMINATOR. AND A 1/2 H. P. PBED PUMP. 

iaxHAUST S\'STEM: 'MTJ{ 20 JU'. BtoWER. VP.NTINO THE DECX>RATIVE CHROME PLA'X»rG 

TM"K, 

: OPERAnON OF·fHJS I!QUlPltIONT SHAU. B8 (nNDUCTED IN ACCORDANCE WrrH AlL DATA 

AND SPEClPICATIONS SUBMl'I'IT'.D \\ITR THE APPLICAnOM UNDER WHICH THIS PeRMlT IS 

ISSUED UNLP.SS O1'1fERWlSE N01'ED' BELOW. 

2, . THIS EQUJPMENr SHALL Be PROPEIU. Y MAINTAINED AND KePI' IN 0000 OPERA1'lNQ 

! CONDmON AT ALL TIMeS. 

THJS SYSTEM SHAll. BE IN PUU. u~ WHENEVI!Jt THB D!!CORATIVE CHROMJ:! PIA TlNG 

TANK Vf!NTEO TO IT IS IN OPBRAI10N. 

11m CHaOME PLATlNG TANKSUBdIC'r TO RULE 1169 AT nos PACJurY SIiALL.BE 

EOUIPPED WInf A NON-REsE1TABE. TOTALJ2'lNO. AMPERB-HOUR METER THAT MEA.'URES 

THE PLATING CURRDrr INTeGRAtED OVER TIME. 

mE TOTAL AMPERB-HOVRS Of Tim PLATING CUllRENT APPLIED TO THE Cf{R.OMS 

PLATING TANK AT THIS FACILITY SHALL NOT EXCEBD 638,:302AMPERB-H0t1RS IN ANY ONE 

YE.Alt. 

nm <»'ERA TOR SfiALL PEIlRlltM A I MINUTE WASHDOWN AT LEAST.EVf..RY 8 HOURS OF 

OPERATION. 

OJlIGINAL 

I 
. , ( '" 

, 

A FLOWMtiTER SHALL BE JNSTA48>AND NAlNTAlNED TO JNOICAtt IN ~~UONS PER 

MJNU1E THE PLOWRATe OP'1lHBWA1'1!R SUPPLYING T8B MESH PADS DUlUNG 

WASHDOWN. THE SCALE OH11I!! JILOWMBTER SHALL NOT EXCIUID POUR TlMBS "nmUMrr 

SPBCIPJED IN CONDmON 8. 

&. THB PLOWJlATE OF THE WATER OOIUNG WASHDOWN SHALL NOT DS LESS T1L\N S 

OALtONS Pml MINUTE. 

p. A GAGS SHAl.L BB INS'I'ALLIJD MNDMAINTAINBD TO INDICATE IN INCHeS OPWAT£R nm 

STATlCP'RES#IORE ~ACROSS 11fI!SClUJBBBR.11mSCALB ON 'l1mOAGE 

SFIAU. NO'I' BXCBBD POVlt 'iUd!s THE UMrJ" SPBafIB'D 1N OONDmoN 10. 

lO. THE TOTAL STAnC PIteSStJRB OlJIfDENrt.\LACROSS niBSCRUBBBR SHALL NOT BXCBED 

45lNOf OPWATBR DURING OPmtA11ON. 

1L THE EXHAUST Sl'ACKSHALL DISCHARGE IN AN UPWARD DIRBl.'l10N AT A HEIGHI' OP2S 

FEIn' ABOVE GROUND. 

12. 11fE HBXAVAJ..EMT CHROMIUM BMISSlONS SHA1.L NOTaCE£D 0.0378 MILLlGltAMS PER 

HOUR. 

13. nmOWNek Q1l OPBItATOR OFTHB EOUIPMBNT SHALt. CONOUCI' A SOURa TSSrTO 

DEMONS11tATE ~\\Il11I CONDrnON 12~ THEPOUOWJNO CONDmONS: 

A. A SMOKE TP..S1I'SHAlL DB CONI>UCI'ED mOR TO nm ACTUAL SOURCE TEST 

TO DEMONSnlATB NO JrUOUl1YE J!MJSSIONS WIlL OCCUR DURlNG OPf!RADON. 

B. 11m SOURCE 'l"EST SHALL BE CONDUCT£D Wl11DN 30 CAL£NDAR DAYS 

API'BR JNmAL START-OP. 

e. THB SOUKCS1BST SHAU. DBJ'l!RMINS AT A MINIMUM -JlIE TOTAl" 

CHROtttIUM ANJl ma ilimiAV~CHaOMIUM EJdS!DONS TO THB ATMOSPHERE PROM 

THB Alit: fOlLtmO!UtbNftoL.8OVII"NJ!N1' VENI1NG THE DBCORATM! arROME PLATlMG 

TANK. nOiH&XAvAlJeNtCHROMIUM EMISSlONS SHALL Hal EXCEED THB TOTAL 

CHROMJUM .BMJSSlO1l1S. 

D. nm~TI1SI' SHAU.B£CONDUc:nm WHO.BTlmTANK VENI'El> TO nus~JS. 

~ 

~GATLOWLOADANDMAXJMlJMLOAD. nmWGHP.ST 

iNIssJolu LESS OPTHE lOAD SHAU. BE USJ!t) IN DEMONSTRATING 

~wniJ coliDmoN' 12. 

E. DUllIHG iHSnJST. 'I11E OUAN11TY OPWATER AND CHRONIC ACID ADDED 

TO 11HE TANIC.~£~1tON OP CRR.OMlCACID. TImFLOWRATES OP11IS WA'l'EIt 

SUPPL¥lNG THE MSsHi'PADS DUIUNG WASHDOWNS. AND 'tHE TarA!. PRBSSUltB DROP 

ACItOSi-.TiaJdR 'POU.JU'nON CONTaOLS'M'EM SHALL BE MONITORBJ> AND REPOR.TED IN 

'.l'H1i souRCE TE'rtltPiORT. 

ORIGINAL 
SOUTH GOA~r NR OUAUlY MANAGEMENt DISTHIGT 

21 M5 Ellsl (ju~lh=!y Drive, DIamond Bar, CA 91 (65 

PERMIT TO CONSTKUCI'/OPERATE 

....

;" ., 

F. 1HB (.:OMP.UAKCB!UNft' OI"THB 'lOXIa DANCH SHAU BE NOItm:D OF THE 

DA'IE AND TIME OPTRE"TBST AT l..DSI' to CAL.mlDAil DA'YS PRIOR TO nIB 'J'BST. Oil 

WlTHJN A TlNBAGRlmD UPON BYTHECOMPLlANCI! UNJT. 

O. THE SOt1Jlal TI!S'i S1MLL COMPLY wmr THEATrACIIED DlSTRlcr 

"GUIDELINES FOR coNSTRucnON OPSAMPUNG AND 1BTING PACRmm ..... PURsUANT TO 

DISTJUCT RVlJ! 217. 

H. 1111 souaca 11!ST SffIUL B8 OONDUCTED IN ACUl1lDANCB WITH TRIl 'IWI' 

MI!THODS OUTLlNBD 1N1Bin:mnwcrRULB 1169. 

I. 'I'HS SOURCE 'f" SJMU. BE PBRPORNED BY AN INDEPENPBNT QUALIFIED TESTING J.ABORATORY PURSUA'MTTO DlBI'RIcr 1t1.JLE 304-

J. 't'HE SOtJllCE T.l!Sr REPORT SHAU.INCWDS RPSULTS OF THE SMOJCE TEST. 

THE SOURCE TEST, TH£ 0P'BIlIlI'ING PARAMETERS OtmJNED IN CONDmON 12 (E). AND 

AlL JTEMS US'J'Sl) ON THE ATMCIISD CRI!(1CUST (POR.M ST.1). 'mE REPOltT SHALL BE 

SUBMlTI1!D TOTRE COMI'UAHcBUNIT OP11IB TOXICS BRANCH NOT lATER THAN 60 

CALENDAR DA~ AM'U. 11m SOtIkCB'l1!STDA'IB. A COPY OF 'llIB SOURCB msr IlBPORT 

SHAll. DB 0Pr AND BS MAJ)B"AVA.D.ABLE UPON DJSTRICl'REQUEST. 

:14. WHENBVJDt THE PLA11NU ~.IN.oPBRA"l1ON. THE OPBllATOR SHAU. PRBPARE AN.O 

MAlNTAJHJd!OjRDS"3'O ~TE(x)MPLIANCB WIl'H CONDmONS 5, c;, AND 8. AU. 

RECORDS SBAU DS RETAINED POll AT Ll!AST1WO YEAU AND MADE AVAIJ.ABt..E TO 

DfSTRICI' PBRSONNEL meN REQUEST. 

0JlIG1NAL 
SOUTH COAST AIR QIJALIl'( MANAGOdFNT DISTRtCT 

21 Ul).':i £331 Copley Olive, Diamond Bar, CA 91765 

PEKMIT TO CONSTRUCf/OPERATE [ ~~~~~.. ~~~~~~~~

NOTtCS 

IN ACCOIlDANCB WI1li RtJLB 2G6, THIS PDMlTTO OPERATE OR (.X)PY SHALL BE. PaS l'ED UN OR 

wmaN 8 MBTBJtS OFTHI! P.t.RJ1lPMJ!NT. 

THIS PERMIT DOeS PlOI' AU'I'HQIIntE DIE EMISSION OF AIR CONTAMIHAIfl'S IN PXCBSS OF THOSE 

ALLOWED BY DMSlON 26 OPTlIEimALnt AND SAP2TY CODa OJf1lJESTAT£ 0,.. CAUPORNlA OR. 

THB RULBS QP1HBAlIlQUAUtY~J>fSTIUcr. mJS PERMlTCAJtl1'4'OT lm 

C'ONSJDBIU!D AS~ION TO VIOLA'T8 BXISTING LAws, ORJ)INANCI?S, REGULATIONS OR 

STA1'lJTaS OF 0'l'HBR- OOVEllNMEHr AGSNaBS. 

ORIGINAL 

j 
( 

• 

Sp&oifioation Sh'6~' 

Hat-Pro/DuA.H Propotl&.l No. 1,13.B891..008 . H 

HEXMASTER 

r:H!lOHIC ACID SCRU~BER SYSTeM 

The exh .. utlC gu 3crubbtlr .hall be peckod-b.d t:.yp_ .... ith high·.ffichncy mitt 

ellmin4::or.. It shall be do.lgn"d for 1lIu.x!IIlWJI co!'laatLon o rtllaov41 officL .. ney ot 

4ir contAtO.inants arhing from Chi procoss b .. t::ha . Scrubber exhaust sh.U comply 

'.11th Maximum Avail.able Cont:rol Technology (MAeT) IIIm111sion stllndard!l tor ('.hro!llic 

acid. 

Scrubb&rs shall be conetrucccd from Typo I. Gr.e.da I, high. impact polyvinyl 

chlo=ide (PVC) conforming to ASTH 0-17 84, C.l1 14JJD except 'Where cQrrQcion 

rull1ta.ncl ot;" TY'P~ 1 PVC 1,; bAccl'lr suited to the appUc,f,tlon. 

Tho .crubber bottol'll ah.e.l1 be f4bricl'I.t.,d f["olll 1/2" (minimum) PVC, 

PAcking .hall be r",ndoa..c!Wlp .. d, high-.ffioiu\oy type. It shell b o hbricatod 

ero::! polypropylan. or och.r c: rrollio:\·r~sl~clt.ne mat.ri. .. l , 

High.eftieienyy mist: ol1c.in,u:.orl> 6hdl be provided ~o c041ue~ and elicin4t4 

ent:rained dropls.cs:. Thay lOhdl be 1nt:egr~1 t:o t:h •• crubb.r dnd £dbt lC41.~d erol); 

polypropylene. E11m1nato rs ahall be 1nstalhd .... ithin removable cart:ridg .. to 

fAc1l1t:4te mslntenanelil . CAnr!d~ea shall be .oeeh4nlc.ally sealed to pravent by· 

pel.1n5 ~ing 4n inter looking traok sy&tem. 

SprAY noz:zhB shall b~ 

qUAnclry and arraneem~nt 

open-orifica, non·clogsin& type ~nd of iuff1ciant 

cn ensure o!Idcquuce al~trlbut.ion of \.:d,shdo\o"n solution. 

Aecess doors shall he provi ded for 3prllY nozzle and mi~t eliminatur main· 

tonance. Furr.i.llh tI"oIInsporont vio\J ports to allow tor l.n3peet:lon of mililt 

climinators and sprs:; n07.z1o!l. 

Dlfferentie.l pr",~urCl galiSIHI for monitoring prouure drop dcros~ chs packing 

and mist .lim10AtOrS ahall he p~ vldQd . 

Flo\.1 IUltHJI for indicatin!,;/ adjUMt:ing '.Ju:hdovn r..eel; shAll be provi(jed. 

Equipment t o r LutOe:l4cle. control of v,,,hdovtl o f the 6crubbar c_n b. providad . 

Tho pacKas. ghall include Slohnoi(j v,a,lvali and timoril. Hcnud l "'p.::rat.ion eholl 

be lI ccompllAhed by U!lC o f H· ()· A I!vitc:hos mountod On thl8 face ot the enclo.u1.'~. 

A PLC ~n .I!. HEMA 4 6nclo6ur~ 15 provided. ' Tho anclosur(! Gh",ll bi ,.,Lred 1n ~Hn .. 11y, 'hrroin ... l blocks .... ill b4 pr ovided f o r ex':ornd connection", 
Sp.c1f~oation Sheets 

HBe-Pro/Duall P~opoaAl No. 413·8894.008·M 

Page 2 

HeAostar 

1. Type - FU303·53HH 

? . t':a.ra.r.1 t!y - 7. 000 C FH 

3. ~re'fute Drop· 4.5 Q v.g. 

4. MaceriAl of Con.cruct.loll - Type 1 PVC: 

5. Firat Seage Packing Type - ~l Tr1-Pack 

6. Y1r.t Stage \JAllhdown - 4.84 gallons for 1 mlnute once every 8 houro. 

7. Second SC4$6 Co~l~seins Pa6 TyP& • Hono·f11&mRnt. 

8. Seoond Stage Coalesoing Qashdown - 4.84 gau,ona for 1 mInute once ovor:y 9 

hours 

9. Thi~d Stale Mist Rlim1n4t:or Typo • Mono·fila~ent 

10. th1r4 Sr~8. W&~hdown • 4.84 ~lM fur 1 mlnuce on~c a month 

11. FloWMetor Type. Dwyer Ser1as KM 

12. nagnahe11c Gauge Type - Dwyer Saries 2000 

o 
Meter Designation 

ROCKWELL MODEL 5-275 

Rated Capac,ly cfh 

CVM and GT meters-max. mdex rate 

Diaphragm meters- 2" H20 Dill.rate 

~;:~:; 

::,::;: >- 101 

~'!f; ~ 

t~~'l'':­ ..t\~·:"z 

t~"'w .t.*.~ 

~~~ 99' 

~;-24 . .. ~ ... ~ 

FLOW RATE 

(AIR) 

.25 CFM 

.5 CFM 

.75 CFM 

1.0 CFM 

2 . 

.:.~..;.~'. 

30 

MINERS & PISANI, INC. 

2010 Farallon Drive 

SAN LEANDRO. CA 94577 

(415) 352-9040 

TEST MEDIUM - ATMOSPHERIC AIR 

40 50 60 70 

FLOW RATE - PERCENT DF RATED CAPACITY 

PERCENT PERCENT PERCENT RATED 

CAPACITY ACCURACY PROOF 

100.2 .. - .. .. _--

100.1 --- - .. ..... _ .. --.--. 

99.8 

99.8 .. ,---

-

Manufacturer's Number 

6848207 

Cartridge Number 

DIFFERENTIAL (inches H2O) 

Tested on air 

Customer: __ CHEMI ___ C_AL __ D_A_T_A ___________ _ Date Tested: ...... ?,/?6I93 ................................ .. 

Customer P.O. No.: _______________ ED LEWIS _ R.H. 

Tested by: ......... . 

Customer Meter No. _______________ _ Test Location: .. 
SOUTH COAST AIR QUALI1Y MANAGEMENT DISTRICT 

TECHNICAL SERVICES DIVISION 

SOURCE TESTING & MONITORING BRANCH 

• 

. INFORMATION REQUEST FORM (ST-2) FOR 

PROTOCOL/REPORT REVIEW 

This form is to be completed by the processing engineer requesting an evaluation of a Source Test 

Protocol or Source Test Repprt. Please check off appropriate items and provide the corresponding 

requested information. The sampling and analytical methods will be reviewed for .ruJ!y. those gaseous and 

particulate constituents identified. 

Constituents AJlowable(1) Rule # NSPS Sampling Identify 

to be Limits or 40CFR60 Location any other 

Measured Conc. Mass Permit Identify Requirements 

(ppm) Flow Cond.# Subpart 

Rate 

Ob/hr) 

Example: 

[x] CO 500 Reg ·IX J Exhaust Stack 

CO BOO Condo 12 Before CO Boiler 

CO 2000 407 (a) (1) Exhaust Stack 

[x] NOx 125 476(a) (1) Exhaust Stack @ 3% 02 

asN02 

[ J CO 

[ ] CO2 

[ ] 02 

[ ) S02 

. 

(1) " allowable limit is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark 

with an asterisk (*). 
) 

Constituents 

to be 

Measured 

[ ] S03 

( ] SOx as 

S02 

[ ) H2S 

[ ] Total 

(Reduced) 

Sulfur 

Compounds 

asS02 

[ ] NH3 

(Free) 

[ ] NH3 

(Free) 

Combined 

[ ] NOx 

[ ] NOxas 

N02 

[ J TGNMO 

AJlowable(1) 

Limits 

Conc. Mass 

(ppm) Row 

Rate 

(Ibjhr) 

TECHNICAL SERVICES DIVISION 

SOURCE TESTING & MONITORING BRANCH 

INFORMATION REQUEST FORM GST·2) FOR 

PROTOCOL/REPORT REVIEW 

Rule # NSPS Sampling 

or 40CFR6Q Location 

Permit Identify 

Cond.# Subpart 

.-

" 

Identify 

any other 

Requirements 

0 

0 

0 

0 

0 

0 

0 

0 

0 

I 

~ 

0 

I 

~ 

0 

0 

I 

~ 

0 

(1) If allowable limit Is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark 

with an asterisk (*). 

Page 2 of 4 
Constituents 

to be 

Measured 

( ] 

Organics 

Speciated 

(Identity) 

[ ] Part. 

Maner 

Oiquid) 

& solid) 

[ ] Part 

Maner 

(solid) 

[ ] PM·10 

[ 1 Part. J 

Size 

Distribution 

( ] lead 

[ ] HeN 

List other 

Compounds: 

[XChromium 

Hex. & Tot ~l 

Allowable(1) 

Limits 

Conc. Mass 

(ppm) Row 

Rate 

Qb/hr) 

. 

0.03 

mg/am 

TECHNICAL SERVICES DMSION 

SOURCE TESTING & MONITORING BRANCH 

INFORMATION REQUEST FORM (ST·2) FOR 

PROTOCOL/REPORT REvIEW 

Rule # NSPS Sampling 

or 40CFR60 location 

Permit Identify 

Cond.# Subpart 

Permit Exhaust stack 

Cond.f12 na 

t?-hr 

Identity 

any other 

Requirements 

0 

0 

I 

0 

I 

0 

I 

! 

0 

0 

I 

I 

0 

0 

na 

0 

0 

0 

I 

(1) If allowable limit Is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark 

with an asterisk (-). 

Page 3 of 4 
Constituents Allowable(l) 

to be Umit~ 

Measured Conc. Mass 

(ppm) Flow 

Rate 

Qb/ hr) 

[ 1 

[ 1 

[ 1 

( 1 

[ 1 

[ 1 

[ 1 

[ 1 

[ 1 

[ 1 

TECHNICAL SERVICES DIVISION 

SOURCE TESTING & MONITORING BRANCH 

INFORMATION REQUEST FORM (ST·2) FOR 

PROTOCOL/REPORT REVIEW 

Aule # NSPS Sampling 

or 40CFR60 Location · 

Permit Identity 

Cond.# Subpart 

. • 

Identity 

any other 

Requirements 

(1) 11 allowable limit is specified by rule or permit In mass flow rate only, please convert to approximate ppm levels and mark 

with an asterisk (*). 

Page 4 of 4 
III Plating a nd Polishing Process Informatio n 

A. Electroplating Tanks: Please provide the infonnation below for each tank in whi ch an 

elec troplating fi nish containing HAP listed in Table I is applied. 

·DO NOT inelude chromium eleclroplatillg and anodizing ranks 

regulated under 40 CFR 63, subpart N. 

TABLE 2. SUMMARY OF ELECTROPLATING TANK INFORMATION' 

Tan k Maximum Recti fie r Tlink 

Do ),ou 

usc 

Finish Tank surface operating operating Type of emission covers on 

Tank Iype volume dimensions amperage hours bath control your 

10' appliedl (cal) (fl x fI) (amps) (hr/yea r) :I~ it atio ll J mcth od4 tanks?5 

"' NiD· / NiD 260 4'x 3' 500 2,040 nOlle TKE Yes 

~ biNi-} Nil 380 5.5'x 3 1.000 1,550 AA TKE Yes 

.. Cd· I Cd 450 6':c J' 1.000 800 Ed "otle No 

~ A.g-I AJ! 210 4' x 2.5' 360 880 /lOll e none No 

Ag-2 Ag 210 4'x 1.5' 360 640 IfOnc 1IOlle No 

l/,f)- I MO /1.00 10' t $' 1'5"00 20'10 Aff t.'r'" e ,ho",'" !Vo 

#.0-2 N, P lZO· . 5 ' / 0 • ;;-OLJ ZOYO 04,4- flo ... .e N. 

At,P-J Ii/ f) 1'2.oQ / 0 

, 

. 5' 15 0 0 ZO'1 0 ,404 " .". ". 

< #,D-t 1I, D /2. 0 0 I )" 

Eo-< / .. 1 oo 2o'-{o A.+ It '' I1'''~ "'0 

< (JI.<. - / 12" I '2."0 ' -' l.d oD 0 20'70 

~ 1 0 )( > jVor>J~ no",. '" 

tv. -2 e", ' S' 20"'/.0 /200 / 0 • 2,0 0 0 ftJloJi! IID"'~ ". ~ t,,- 3 eLl { 1.0. / 0 ')( ~J 20e o z,,~o #J .~ f? "o,,~ ,,0 

0 

~ 

! For example. if you operate three industrial nickel plating tanks, you can number them InNi I, InNi2, and InNi3. 

For e.'(umple, Black nickel = BINi; Brass::: Bs; Cadmium"" Cd; Copper = CUi Gold ::: Au; Lead :: Pb; Nickel. Dccomtivc 

= NiD; Nicke l. Industrial '" Nil; Silver ::: Ag; Ti n/Lead = SnPb; Tin·Nickc l :c: SoNi; Zinc::: Zn; ZinclNickei = ZnNi. DO 

NOT include chromillm electroplating and allodizillg tanks reglliated III/der 40 CFR 63, subpart N. 

J Please fill in: Air agi tation = AA; Educlor (pump mixing) = Ed; Mechanical mix ing ::: MM: No agit:ltion z None; or 

Other (Specify) '" Other. 

~ Only controls applied to each specific tank. for example: polypropylene balls'" PB: wetting agent fume suppressant = 

\V AFS; foam blanket '" FB: Merlin covcr '" Me; tank enclosure'" TKE. Do not include control dev ices installed on the 

ventilation or e;"(haust system. 

S Indicate use of covers. If you replied Merli n covcr (MC) or tank enclosure (TKE) above, indicate "yes" here also. 

OMB 2186.01 7 
Please make blank copies of this table for use as work sheets and/or for additional room. 

B. Electroless Plating Tanks: Please provide the following infonnation for each tank in which an 

electro less plating, anodizing or other finish containing HAP listed in Table I is applied. 

.!! 

t 

a 

, .. '. 

-< 

~ 

< 

~'. 

:~. 

~. 

0 

>c 

TABLE 3. SUMMARY OF ELECTROLESS PLATING, ANODIZING, 

AND OTHER FINISHING TANK INFORMATION 

Finish Tank Tank surface Type of 

Tank type volume dimensions bath Tank emission 

Inl appUed2 (gal) (ft x ft) agitation) control metboct 

ENi-l ENi 300 4'x3' air None 

ENi-2 EN; 300 4'x3' air MlST-E 

Do you use 

covers on 

your tanks?! 

Yes 

No 

I For exampJe. if you operate three electroJess nickel plating tanks, they could be numbered ENi I, ENi2, and ENi3. 

2 For example; Alodine Treatment = Ad, Black Oxide = BIOx, Bright Dip = BrD, Cadmium Strip = CdStr, Chromate 

Conversion = ChCv; Electroless Nickel = ENi; Lacquering = Lq, Magnesium Treatment = Mg, Sodium Dichromate Treat = 

NaDiCr, Sulfuric Acid Aluminum Anodize = SuAn, Sulfuric Acid Strip Anodize = SuStrAn. 

3 Please fill in Air Agitation = AA, Eductor (pump mixing) = Ed, Mechanical Mixing = MM. or No Agitation = None. 

4 Indicate only controls applied to each specific tank. such as: polypropylene balls = PB; wetting agent fume suppressant = 

WAFS; foam blanket = FB; Merlin cover = MC; tank enclosure = TKE. Mist eliminators = MIST-E. 

Do not include control devices installed on exhaust system. 

S Indicate use of covers. If you replied Merlin cover (MC) or tank enclosure (TKE) above, indicate "yes" here also. 

Please make blank copies of this table for use as work sheets and/or for additional room. 

OMB2186.01 8 
c. Thermal Spraying: Please provide the following information for each thermal or metal 

spraying operation in which any material containing HAP listed in Table 1 is applied. 

TABLE 4. SUMMARY OF INFORMATION ON THERMAL SPRAYING 

Is line operated 

Thermal Thermal in booth or Is operation 

spraying spraying enclosure? Type of booth ventilated? 

line ID 1 process type2 (yes/no) or enclosure 3 (yes/no) 

J FIS-J FIS Yes Partial No 

HVOF-J HVOF Yes Complete Yes 

,'. 

, . 

. . . . 

. ~ , ~", 

... =; < 

" 

= ~ 

0 

~ 

I 

" 

I For each thennal spraymg process lme, mdlcate the name or ID number. 

For example, flame spraying = FIS; electric arc spraying = EAS; plasma arc spraying = PAS; high-velocity oxy-fuel = 

HVOF; detonation gun = DO; Other = (specify). 

J Indicate if booth or enclosure is partial (i.e., open on one or more sides) or if enclosure is complete (enclosed on all sides). 

Please make blank copies o/this table/or use as work sheets and/or/or additional room. 

OMB2186.01 9 
D. Finished ProductslMaterials: Please provide the following information for products or 

materials that have been plated, polished, or finished at your facility in the reporting year from 

Table 1. For each product, also indicate the base metal or base material that is finished and the 

ID number corresponding to the tanks from Tables 2 or 3, or thermal spraying operation from 

Table 4, that are used to finish the product. If the specific types of different products or materials 

are too numerous, you may use general descriptors of the products/materials. 

~ 

~ ~ 

~ 

~ < 

= 

== 

~ 

~. 

TABLE 5. SUMMARY OF INFORMATION ON FINISHED MATERIALS, 

SUBSTRATES, AND PRODUCTS 

ID No's for tanks or 

General type of product or Base metal or thermal spraying 

substrate finished material lines 

Faucets, plumbin1!!1xlUres steel InNi-I,InNi-2 

Pump housin1!s, blades, other pump parts steel ENi-2, ENi-2 

Light flXlUres steel, aluminum NiD-I, NiD-2 

Tractor parts steel InNi-I,InNi-2 

Machine rollers, military hardware steel Cd-I, Cd-2 

Electrical connectors copper A1i!-I, A1!-2 

*~"./t: r; 'Co ,f, I"1t S I!/ I"".,,, ~"'" Cu 1-7" 

PI/) 1-"1 

Please make blank copies of this table for use as work sheets and/or for additional room. 

OMB 2186.01 10 
IV. HAP·Containing Plating and Polishing Material Data 

Please provide the following infonnation for each HAP-containing plating or polishing material used in 

the Reporting Year that is a source of HAP emissions reported in Table I. If records for the full Reporting Year 

are not readily available, provide HAP-containing material information for a typical quarter in the Reporting Year 

and check 0 that data are for one quarter of the Reporting Year. For each material, either submit speciated HAP 

content data from the Material Safety Data Sheet [MSDS] or provide the speciated HAP content in Columns. 4 

and 5 of this table. DO NOT report chromium material data from chromium electroplating operations regulated 

under 40 CFR 63, subpart N. Reporting Year: £oo~ 

~ 

t 

~ 

< E-c 

~ 

~ 0 

;>4 

Data are for Full Reporting Year: 0 Data are for One Quarter ~ 

(Check the BOX that is applicable) 

TABLE 6. HAP·CONTAINING MATERIAL DATA 

Manufacturer 

Material name or supplier Amount HAP 

or lOt name used2 Units3 (From Table 1) 

Nickel anodes Acme 2.150 Ibs nickel 

Nickel sulfate Acme 628 Ibs nickel 

Cadmium anodes Industrial Chem 2.8/0 Ibs cadmium compound 

Potassium silver cyanide Industrial Chem 246 Ibs cyanide compounds 

Potassium cyanide Industrial Chem 1.227 Ibs cyanide compounds 

#u .. ltll cJ.lo~. Je. If,les IIfS- Its IJ,ck~1 

ICo,"-"- S"lnk. ~,I~J }200 ILs COl!Jd' ..... , I 7 

I Indicate the generic name, trade name, or product name for any material that contains one or more HAP. 

2 Indicate the total amount used during the reporting year. 

LinelD 

No's." 

InNi-l. InNl-2 

ENi-2. ENi-2 

Cd-I. Cd-2 

Ag-I. Ag-2 

Ag-I. Ag-2 

#.1> (1-'1) 

CIA.. -(.1- :1) 

J For example, gallons (ga1), pounds (lbs). 

4 Use the same ID No's for all plating and polishing tanks listed in Tables 2 & 3, and thermal spraying lines in Table 4. 

Please make blank copies of this table for use as work sheets and/or for additional room.. 

OMB2186.0I 11 
V. Ventilation System and Emission Control System Information 

A. Ventilation Systems: For each ventilation system that exhausts one or more of the tanks listed 

in Tables 2 or 3, or thermal spraying operation listed in Table 4, please provide the following 

infonnation, if available. 

TABLE 7. LOCAL VENTILATION SYSTEM DESIGN AND OPERATING DATA 

Tank and Type of 

Ventilation thermal sprar Exhaust flow Exhaust duct Hood emission 

system ml line ID No's. rate (acfm)3 diameter (int locations control6 

~ V-I InNi-l,lnNi-2 6,600 18 side none 

~ V-2 EN-2 3,000 9 centerline MPME 

~ V-5 CD-2 4.500 12 side WS 

11-1 AI, ° CI-'1) 7, ~() C> zll UI1ljc,J,,~ c'" (1-1) ~1',AlE" . -< ~ ~ 

, 

" 

.. 

.-

:: , <.0, ,E-c 

< =:, '" : 

=f, ;;J, 

0':,' 

> 

I Indicate the name or Identlficatlon number for each mdependent ventdatlon system. 

2 List the ID No's. from Tables 2 and 3 for all tanks or the thermal spray line ill No's from Table 4 for aU tanks and thermal 

. spraying operations that are exhausted by the ventilation system. ' 

3 Indicate the exhaust flow rate through the entire system in units of actual cubic feet per minute. 

4 Provide the diameter of the duct in inches at the inlet to the control device or at the exhaust point. 

S For ventilation systems that exhaust tanks, indicate if the tank exhaust hood is located on the centerlines or sides of the tanks. 

6 Identify the type of emission control system installed on the ventilation system. For example, composite mesh pad = CMP; 

mesh pad mist eliminator = MPME; packed bed scrubber = PBS; high efficiency particulate air filter = HEPA; wet scrubber 

(other than packed bed) = WS; chevron-blade mist eliminator = CBME. 

Please make blank copies of this table for use as work sheets and/or for additional room. 

OMB 2186.01 . 12 
B. Surfactant or Wetting Agent Fume Suppressant: For each tank listed in Tables 2 or 3 in 

which a foam blanket, surfactant or wetting agent fume suppressant, or combination foam 

blanket/surfactant or wetting agent is used, please provide the following infonnation and submit 

the MSDS for each surfactant or wetting agent used. 

TABLE 8. SURFACTANT OR WETTING AGENT FUME SUPPRESSANTS 

Annual cost Bath 

Surfactant Amount used of surfactant surface 

Tank or wetting Manufacturerl in reportin§ or wetting tension 

IDI agent name supplier year (units) agent ($) (dynes/em)] 

NiI-l FS-250 Electrochem l4gallons $1,840 45 ~ 

t NiI-2 FS-250 Electrochem l4 gallons $1,840 45 

~ AgCN-l No Foam Ind. Chem 8 gallons $160 NA 

'. 

~ 

< .. 

~ . 

. . 

== 

~ 

0 

> 

I List the ID No's. from Tables 2 and 3 for all tanks in which the surfactant or wetting agent is used. 

2 Indicate the amount used during the reporting year and units (e.g., gallons, pounds). 

3 If you monitor or periodically measure the bath surface tension, indicate the surface tension in units of dynes per 

centimeter. 

Please make blank copies of this table for use as work sheets antVor for additional room. 

OMB 2186.01 13 
lob 

C. Air Pollution Control Devices (APCD): For each ventilation system listed in Table 7 that is 

exhausted to an emission or air pollution control device, please provide the following 

information 

TABLE 9. AIR POLLUTION CONTROL DEVICE (APCD) INFORMATION 

Control Basis for 

VentUation efficiency control 

system Inl APCDTypeZ (%)3 efficiency· 

~ V-2 Sure Control. Inc.. mesh pad mist elimin 90 Manufocturer 

~ 

~ V-5 Whirlwind. Inc .• wet scrubber 85 Per/lest 

.. V .. 1 DlAc..I '/ t1\tS" 'P,J ,.,.,s). eh"",,,,,~.,,, 'I'." /'4 ... f 1i-(1 

~ 

~ 

.~. 

~ 

I Indicate the ventilation system ID No or name from Table 7. 

2 List the. type of air pollution control device. For example. composite mesh pad = CMP; mesh pad mist eliminator = 

MPME; packed bed scrubber = PBS; high efficiency particulate air filter = HEP A; wet scrubber (other than packed bed) = 

WS; chevron-blade mist eliminator = CBME. 

l Indicate the control efficiency or percent reduction in percent. 

4 Identify the basis for the control efficiency. For example, manufacturer's guarantee, performance test, other (please 

specify). 

Please make blank copies of this table for use as work sheets and/or for additional room. 

OMB 2186.01 14 
VI. Pollution Prevention· 

A. Steps used to minimize drag-out%: 

o Surfactants ot Drip time 0 Air blow down 0 Other: 

B. Describe any other pollution prevention measures (e.g., drain board between tanks angled to 

drain dragout back to the previous bath) or housekeeping activities that reduce air or water 

pollution, or solid waste. 

done 

C. Provide costs and cost basis (e.g., cost of developing and implementing work practices or cost 

of substituting a non-HAP plating finish for a HAP-containing plating finish) of work practices 

or pollution prevention (P2) measures currently being used: 

d<Jyt~ 

D. Provide costs and cost basis for P2 measures evaluated but not implemented and reason(s) why 

they were not implemented: 

~ svJ,s.}, I-.JI-~$ t;~ C~("QoMl""" Ih fl..so Ci-Cb.,. ... I-'JC CJ.~4. 

LJ~<Jc.« .J' 

I 

I Pollution prevention means any practice that reduces or eliminates the creation of pollutants through 

increased efficiency in the use of raw materials, energy, water, or other resources. Examples include 

substituting a hazardous material with a non-hazardous material, or a process change that eliminates 

the use of a hazardous material. 

2 Oragout refers to residual plating or finishing bath solution that remains on parts or workpieces after 

they are removed from the tank. 

OMB 2186.01 15 
OMB2186.01 

Attachment I 

List of Most Common Hazardous Air Pollutants (HAPs) 

Reported Emitted from Plating and Polishing Facilities 

in SIC Code 3471 

CAS Chemical Name Number 

7782505 Chlorine 

50000 Fonnaldehyde 

7647010 Hydrochloric acid 

7664393 Hydrogen Fluoride 

67561 Methanol 

7723140 Phosphorus 

108883 Toluene 

1330207 Xylenes 

Cadmium Compounds 

Cobalt Compounds 

Chromium Compounds 

Cyanide Compounds 

Glycol Ethers 

Lead Compounds 

Manganese Compounds 

Nickel Compounds 

16 
Attachment 2 

Complete List of Hazardous Air Pollutants (HAPs) 

CAS No. Chemical Dame CAS No. Chemical name 

75070 Acetaldehyde 106467 1 ,4-Dichlorobenzene(p) 

60355 Acetamide 91941 3,3-Dichlorobenzidene 

75058 Acetonitrile 111444 Dichloroethyl ether (Bis(2-chloroethyl)ether) 

98862 Acetophenone 542756 1,3-Dichloropropene 

53963 2-Acetylaminofluorine 62737 Dicblorvos 

107028 Acrolein 111422 Diethanolamine 

79061 Acrylamide 121697 N,N-Diethyl aniline (N,N-Dimethylaniline) 

79107 Acrylic acid 64675 Dietbyl sulfate 

107131 Acrylonitrile 119904 3,3-Dimethoxybenzidine 

107051 Allyl chloride 60117 Dimethyl aminoazobenzene 

92671 4-Aminobiphenyl 119937 3,3'-Dimethyl benzidine 

62533 Aniline 79447 Dimethyl carbamoyl chloride 

90040 o-Anisidine 57147 I,I-Dimethyl hydrazine 

1332214 Asbestos 68122 Dimethyl formamide 

71432 Benzene (including benzene from gasoline) 131113 Dimethyl phthalate 

92875 Benzidine 77781 Dimethyl sulfate 

98077 Benzotrichloride 534521 4,6-Dinitro-o-cresol, and salts 

100447 Benzyl chloride 51285 2,4-Dinitrophenol 

92524 Biphenyl 121142 2,4-Dinitrotoluene 

117817 Bis(2-ethylhexyl)phthalate (DEHP) 123911 1,4-Dioxane (1,4-Diethyleneoxide) 

542881 Bis( chloromethyl)ether 122667 1,2-Diphenylhydrazine 

75252 Bromofonn 106898 Epichlorohydrin (I-Chloro106990 1,3-Butadiene 2,3-epoxypropane) 

156627 Calcium cyanamide . 106887 1,2-Epoxybutane 

133062 Caplan 140885 Ethyl acrylate 

63252 Carbaryl 100414 Ethyl benzene 

75150 Carbon disulfide 51796 Ethyl carbamate (Urethane) 

56235 Carbon tetrachloride 75003 Ethyl chloride (Chloroethane) 

463581 Carbonyl sulfide 106934 Ethylene dibromide (Dibromoethane) 

120809 Catechol 107062 Ethylene dichloride (I ,2-Dichloroethane) 

133904 Chloramben 107211 Ethylene glycol 57749 Chlordane 151564 Ethylene imine (Aziridine) 

7782505 Chlorine 75218 Ethylene oxide 

79118 Chloroacetic acid 96457 Ethylene thiourea 

532274 2-Chloroacetophenone 75343 Ethy lidene dichloride (l, 1-Dichloroethane) 

108907 Chlorobenzene 50000 Fonnaldehyde 510156 Chlorobenzilate 76448 Heptachlor 67663 Chlorofonn 118741 Hexachlorobenzene 

107302 Chloromethyl methyl ether 87683 Hexachlorobutadiene 

126998 Chloroprene 77474 Hexachlorocyclopentadiene 1319773 CresolsiCresylic acid (isomers and mixture) 67721 Hexachloroethane 

95487 o-Cresol 822060 Hexamethylene-I,6-diisocyanate 108394 m-Cresol 680319 Hexamethylphosphoramide 106445 p-Cresol 110543 Hexane 

98828 Cumene 302012 Hydrazine 94757 2,4-D, salts and esters 7647010 Hydrochloric acid 

3547044 DDE 7664393 Hydrogen fluoride (Hydrofluoric acid) 334883 Diazomethane 123319 Hydroquinone 132649 Dibenzofurans 78591 Isophorone 96128 1.4-Dibromo-3-chloropropane 58899 Lindane (all isomers) 84742 Dibutylphthalate 108316 Maleic anhydride 

OMS 2186.01 17 
CAS No. 

67561 

72435 

74839 

74873 

71556 

78933 

60344 

101688 

101779 

91203 

98953 

92933 

100027 

79469 

684935 

62759 

59892 

56382 

82688 

87865 

108952 

106503 

75445 

7803512 

7723140 

85449 

1336363 

1120714 

57578 

123386 

114261 

78875 

OMB 2186.01 

List of Hazardous Air Pollutants (continued) 

Chemical name 

Methanol 

Methoxychlor 

Methyl bromide (Bromomethane) 

Methyl chloride (Chloromethane) 

Methyl ch1orofonn (1,1 , I-Trichloroethane) 

Methyl ethyl ketone (2-Butanone) 

Methyl hydrazine 

Methylene diphenyl diisocyanate (MOl) 

4,4'-Methylenedianiline 

Naphthalene 

Nitrobenzene 

4-Nitrobiphenyl 

4-N itrophenol 

2-Nitropropane 

N-Nitroso-N-methylurea 

N-Nitrosodimethylamine 

N-Nitrosomorpholine 

Parathion 

Pentachloronitrobenzene (Quintobenzene) 

Pentachlorophenol 

Phenol 

p-Phenylenediamine 

Phosgene 

Phosphine 

Phosphorus 

Phthalic anhydride 

Polychlorinated biphenyls (Aroclors) 

1,3-Propane sultone 

beta-Propiolactone 

Propionaldehyde 

Propoxur (Baygon) 

Propylene dichloride (l,2-Dichloropropane) 

18 

CAS No. 

74884 

108101 

624839 

80626 

1634044 

101144 

75092 

75569 

75558 

91225 

106514 

100425 

96093 

1746016 

79345 

127184 

7550450 

108883 

95807 

584849 

95534 

8001352 

120821 

79005 

79016 

95954 

88062 

121448 

1582098 

540841 

108054 

593602 

75014 

75354 

1330207 

95476 

108383 

106423 

Chemical name 

Methyl iodide (Iodomethane) 

Methyl isobutyl ketone (Hexone) 

Methyl isocyanate 

Methyl methacrylate 

Methyl tert butyl ether 

4,4-Methylene bis(2-chloroaniline) 

Methylene chloride (Dichloromethane) 

Propylene oxide 

1,2-Propylenimine (2-Methyl aziridine) 

Quinoline 

Quinone 

Styrene 

Styrene oxide 

2,3,7,8-Tetrachlorodibenzo-p-dioxin 

1,1,2,2-Tetrachloroethane 

Tetrachloroethylene (Perchloroethylene) 

Titanium tetrachloride 

Toluene 

2,4-Toluene diamine 

2,4-Toluene diisocyanate 

0-Toluidine 

Toxaphene (chlorinated camphene) 

1,2,4-Trichlorobenzene 

1, I ,2-Trichloroethane 

Trichloroethylene 

2,4,5-Trichlorophenol 

2,4,6-Trichlorophenol 

Triethy lamine 

Trifluralin 

2,2,4-Trimethylpentane 

Vinyl acetate 

Vinyl bromide 

Vinyl chloride 

Vinylidene chloride (l,I-Dichloroethylene) 

Xylenes (isomers and mixture) 

o-Xylenes 

m-Xylenes 

p-Xylenes 
[W] ~.&JmATIONAL 

TECHNOLOGY 

CORPORATION 

ANALYSIS RECauJEST AND 

CHAIN OF CUSTODY RECORD * 

Reference Document Nu. 334 a 2 a 

Page 1 of_ < 

< 

Project Name/No. 1 

Sample Team Members 2 

Aw\k.~ .~~ ___ . Samples Shipment Date 7 ~L"" ____ . __ 

t.'l.. I '>L Lab Destination 8 WI1f.~ kp;...1 .A<AM=-::-.'_-

Bill to:~_.c..Q~~\5> __ . _____ . __________ ~ 

._ i170 Qu~,.~ j~\~~.. ~ 

D",bj.V\ J LA '1,+/5 h ~ 

Profit Center No. 3 Lab Contact _9 _b~olO.l~~ ____ _ ---------~---- ~ 

Project Manager~ ____ . ________ Project Contact/Phone ~ --_ .. _-._--- Report to:'~_ . .tiL_~~_. __ _ Purchase Order No.~ __ . _____ . __ ~.___ ___ Carrier/Waybill No._'

_

3__ _._d __ .... __ .•. ~J.~.:_~1-7JCh - .. - . - --_ .. --. .. II 

9 

11 Required Report Date._ ....... _ ... __ . _ ------ _1f'h'.';~'h'I:::t=~IiIiiI"h'l . - - -.- - ... .. -

i 

r 

t 

Sample 14 Sample 15 Data/Time fa Containerf?~. .-1, I HI Pre- 19 Requested Testing 20 Condition on 21 Disposal 22 

Number Db ..... -i .. ~i ... I/Tvpe Collected Tvpe ........... servatiVa '-.-..... " ..... "- Record N.CI. 

/ I:;~ 10:""" CAV-C: ?f1.;t '"Z'I.S" 

~~I - ~~ N~ltl 4- 1"" f '~jAt}f ~.",~ { 

, ~ ~;,I ,__ ;4 A c;.".~,..? h.l C If"'" · · 

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/ (~~wR1 ~~ 4~~~~ ~~i~~ CI" .. ~ N..(.~\ ~ '. \.~ 1- ~. I . r 

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/\? .. t,4\ { .. #~ U ~<- ,;..~ , ~ , 'v , \fV)\'1~ ... ~-...... -"I.>_ (' ~ 

k "'- .1"L.~~\ . / }J l ' \ 

;. - - .' ~. .- . '" . ; 

r . . 

Special Instructions: 23 

Possible Hazard Identification: 24 Sample Disposal: 25 7 Non-hazard ..J Flammable -J Skin Irritant -J Poison B .-J Unknown ~ Return to Client '-J Disposal.by. Lab .J Archive - (mos.) 

Turnaround Time Required: 26 I QC Level: 27 

Normal..J Rush ~ I.i-J II..-J 1I1.W.. ... ... 'c,. (I :',): UlCI.. .. o;J .... CI..II.I.. l;:, .... CI..lly ••.. - .. -

1. Relinquished bY!.J ~~ate:~j~_ .. ___ ._ 1. Received ~~ I Date: yir.lt~ -- - (S'gnature/Affillatoon) It .L~:. Time: (Sillnatw- '-~ _ ~ Time: 

2. Relinquished by Date: -.. --.- _ .. .- --+-- 2. Received )~w, ~iJ~..k Date: 

(SIgnature/ A/f,ltauon) Time: ._ . .... -", .AU."...· r It [6 Time: '~~~~~}:M~ 3. Relinquished by Date: 3. Received by I C t- Date: 

(Sognature/ Affiliauon) Time: ---... _ .. _----- . - ... -~ .. _---_.- (Signature/ A/f,bation) Time: 

Comments: 29 p.(;~ ~"('1 ~ cJ~~~I~ V(. #23630 

e l c..I I bt~{~ 
CAS No. 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

o 

List of Hazardous Air Pollutants (continued) 

Chemical name 

Antimony Compounds 

Arsenic Compounds (inorganic including arsine) 

Beryllium Compounds 

Cadmium Compounds 

Chromium Compounds 

Cobalt Compounds 

Coke Oven Emissions 

Cyanide Compounds' 

Glycol ethers . 

Lead Compounds 

Manganese Compounds 

Mercury Compounds 

Fine mineral fibers3 

Nickel Compounds 

Polycylic Organic Matter" 

Radionuclides (including radon)! 

Selenium Compounds 

NOTE: For aU listings above which contain the word "compounds" and for glycol ethers, the following applies: 

Unless otherwise specified, these listings are defined as including any unique chemical substance that contains the named 

chemical (i.e., antimony, arsenic, etc.) as part of that chemical's infrastructure. 

'X'CN where X = H' or any other group where a formal dissociation may occur. For example KCN or 

Ca(CN)2. 

2Includes mono- and di-ethers of ethylene glycol, diethylene glycol, and triethylene glycol 

R-(OCH2CH2),,-OR' where 

n = 1,2, or 3 

R ::: alkyl or aryl groups 

R' = R, H, or groups which, when removed, yield glycol ethers with the structure: 

R-(OCH2CH),,-OH. Polymers are excluded from the glycol category. 

3lncludes mineral fiber emissions from facilities manufacturing or processing glass, rock, or slag fibers (or 

other mineral derived fibers) of average diameter I micrometer or less. 

4lncludes organic compounds with more than one benzene ring, and which have a boiling point greater than or 

equal to 100°C. 

sA type of atom which spontaneously undergoes radioactive decay. 

OMB 2186.01 19 
Marinshaw, Richard 

From: 

Sent: 

To: 

Marinshaw, Richard 

Friday, August 04, 2006 11 :47 AM 

'ecrdarrel@aol.com' 

Subject: Plating and Polishing Survey Response for Anaheim Plating 

Darrel Lewis 

Anaheim Plating & Polishing, Inc. 

Mr. Lewis, 

Page 1 of 1 

The response to the survey for the Plating and Polishing Source Category from Anaheim Plating & Polishing. Inc., 

included an emission test report, dated March 29. 1993. In the appendices to the test report is a diagram of the 

sampling train used for the emission test. That diagram is marked "Confidential.· It appears to be a standard 

sampling train schematic of the kind you find in any emission test report. Can you tell us whether or not that diagram 

is really meant to be confidential? 

Thank you, 

Rick Marinshaw 

Richard J. Marinshaw. P.E. 

RTI International 

3040 Cornwallis Road 

PO Box 12194 

Research Triangle Park, NC 27709-2194 

(919) 316-3735 

8/412006 
• -0- -

Marlnshaw, Richard 

From: Ecrdarrel@aol.com 

Sent: Sunday, August 06,20062:58 PM 

To: Marinshaw, Richard 

Subject: Re: Plating and Polishing Survey Response for Anaheim Plating 

Mr. Marinshaw 

No this document is not confidential, the Engineering Firm that did the test marked it Confidential, but this 

information has been given to several of the local administrating agencies and is not classified by Anaheim Plating 

& Polishing as confidential. 

Darrel Lewis 

Environmental Compliance, Anaheim Plating 

Sn12006