Dry Scrubber Blue Goose Combustion Data Septem ber 2011 Fyrite

Location : Dry

Scrubber Date 9/26/12 Time:

run O2 CO2

1 18 3 2 18 3 3 18 3
Avg 18 3

Molecular wt

1 29.2 2 29.2 3 29.2

AVG 29.2

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien &Gere

Page 1Test ID: 9-26-12-POM-ABF Run#3 

### Value 0

0 0

150.00 200.00 0.0021 0.0001 0.0000 200.00 200.00 0.002025

200.00 325.00 0.0024 0.0023

1180.00 1000.00 0.0004 0 0.00040



### Value 2.7000 2.0250 4.7250 Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)

Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #3** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/26/2012

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml)Test ID: 9-26-12-POM-ABF Run#3



### Value 0.6647 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 3.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.2 28.69486886 0.045100995 538.8 651.4 29.7 61 1.55 1.044 29.7 128 1.23 83.389 85.2 29.92 0.25 0.00034088462



### Value 84.9436553 41.57291 64.9 3.05484 20.3 0.957145 0.045101 0.045053 100.8354 I = % Isokinetic variation 

### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moisture Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute average temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg) Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/26/2012**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficientTest ID: 9-26-12-POM-ABF Run#3 LIMS ID#: 2012010670



### Value 2.7000 0.0027 2.025 0.002025 84.9436553 29.7 38.48 8.23 Green Carbon Baked tons/hr 0.045100995 74291.71118 4457502.6709 95983.53762 Acfm 77800.59543 Scfm 0.0009 Emission Rate of Total MCEM gr/dscf 0.31 7.49 0.2341 5.62 **0.55**

**0.038 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.028 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.066 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 8:45 AM End time: 11:06 AM

Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/26/2012**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d

## Value 4 0.004 84.9436553 29.7 38.48 8.23 Green Carbon produced tons/hr 0.045100995 73745.4486 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 4424726.916 0.0007 Particulate gr/dscf **0.46 Particulate lb/hr** 

**0.056 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Emission Calculations Test #3 9/26/2012** 

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions