**'~** J



## Compliance
Anaheim March Test Results Plating, Inc.

29, .1993

Chemical Data Management 11750 Dublin Blvd. Suite 201 Dublin, CaliforniaSOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 21865 East Copley Drive, Diamond Bar, CA 91765 

## PERMIT TO OPERATE

CONTINUATION OF PERMIT TO OPERATE

NOTICE 049391 A/N2S0329 Page 2

IN ACCORDANCE WITH RULE 206, THIS PERMIT TO OPERATE OR COPY SHALL BE POSTED ON OR WITHIN 8 METERS OF THE EQUIPMENT. THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE ALLOWED BY DMSION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICT. THIS PERMIT CANNOT BE CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR STATUTES OF OTHER GOVERNMENT AGENCIES.



## ORIGINAL EXECUTIVE OFFICER

# ~/l-h By Dorris M. Bailey/rgc 

### 3/09/1992

## y SOUTH COAST AIR QUAUlY MANAGEMENT DISTRICT 21865 East Copley Drive, Diamond Bar, CA 91765 

## PERMIT TO OPERATE D49391 A/N250329 Page 1
This initial permit must be renewed ANNUALLY unless the equipment is moved, or changes ownership. If the billing for annual renewal fee (Rule 301.£) is not received by the expiration date, contact the District.

Legal Owner or Operator: ANAHEIM PLATING INC 928 E SOUTH ST ANAHEIM, CA 92805 ATTN: DIEGO BARRIGA Equipment Location: 928 E SOUTH ST, ANAHEIM, CA 92805
Equipment Description: ID 086444

TANK NO.8, COPPER PLATING, 4'-0" W. X 9'_0" L. X 4'-0" D., WITH 6 VOLTS AND 2000 AMPERES RECTIFIER, UNHEATED.

Conditions:

1. OPERATION OF THIS EQUIPMENT SHALL BE CONDUCI'ED IN ACCORDANCE WITH ALL DATA AND SPECIFICATIONS SUBMITTED WITH THE APPUCATION UNDER WHICH THIS PERMIT IS ISSUED UNLESS OTHERWISE NOTED BELOW. 2. THIS EQUIPMENT SHALL BE PROPERLY MAINTAINED AND KEPT IN GOOD OPERATING CONDmON AT ALL TIMES. 3. THIS EQUIPMENT SHALL NOT BE OPERATED UNLESS IT IS VENTED ONLY TO AN AIR POLLUTION CONTROL EQUIPMENT WHICH HAS BEEN ISSUED A PERMIT TO OPERATE BY THE EXECUTIVE OFFICER. 4. THE WEIGHT CONCENTRATION OF THE CHEMICALS SHALL NOT EXCEED THE FOLLOWING SPECIFIED AMOUNT: COPPER SULFATE- 20% SULFURIC ACID- 10% ONLY THE CHEMICALS SPECIFIED ABOVE SHALL BE USED IN THIS EQUIPMENT. 5. THE OPERATOR SHALL RECORD THE CONCENTRATION OF THE CHEMICALS IN THE TANK DURING REPLENISHMENT. THE RECORDS SHALL BE MAINTAINED FOR A PERIOD OF TWO YEARS AND MADE AVAILABLE TO DISTRICT PERSONNEL UPON REQUEST.



## ORIGINALSOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 21865 East Copley Drive. Diamond Bar. CA 91765 

## PERMIT TO OPERATE

CONTINUATION OF PERMIT TO OPERATE

NOTICE Page 2

IN ACCORDANCE WITH RULE 206, THIS PERMIT TO OPERATE OR COpy SHALL BE POSTED ON OR WITHIN 8 METERS OF THE EQUIPMENT. THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE ALLOWED BY DIVISION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICI'. THIS PERMIT CANNOT BE CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR STATUTES OF OTHER GOVERNMENT AGENCIES.



## ORIGINAL EXECUTIVE OFFICER 

# tft11.w..; I),

# ~ By Dorris M. Bailey/rgc 3/09/1992\ SOUTH COAST AIR QUALIlY MANAGEMENT DISTRICT 21865 East Copley Drive, Diamond Bar, CA 91765 

## PERMIT TO OPERATE rennUNO. D49390 A/N250328 Page 1
This 

### initial permit 

### must be 

### renewed ANNUALLY 

### unless the equipment is moved, or changes 

### ownership. U the 

### billing for annual renewal fee (Rule 3OlJ) is 

### not received by 

### the expiration date, contact the District.

Legal Owner or Operator: ANAHEIM PLATING INC 928 E SOUTH ST ANAHEIM, CA 92805 AnN: DIEGO BARRIGA Equipment Location: 928 E SOUTH ST, ANAHEIM, CA 92805 Equipment Description: ID 086444

TANK NO.7, COPPER PLATING, 4'-0" W. X 7'-6" L. X 4'-0· D., WITH 6 VOLTS AND 2000 AMPERES RECI'IFIER, UNHEATED.

Conditions:

L OPERATION OF THIS EQUIPMENT SHALL BE CONDUCI'ED IN ACCORDANCE WITH ALL DATA AND SPECIFICATIONS SUBMITTED WITH TIlE APPUCATION UNDER WHICH THIS PERMIT IS ISSUED UNLESS OTHERWISE NOTED BELOW. 2. THIS EQUIPMENT SHALL BE PROPERLY MAINTAINED AND KEPT IN GOOD OPERATING CONDITION AT ALL TIMES. 3. TIllS EQUIPMENT SHALL NOT BE OPERATED UNLESS IT IS VENTED ONLY TO AN AIR POLLUTION CONTROL EQUIPMENT WHICH HAS BEEN ISSUED A PERMIT TO OPERATE BY THE EXECUTIVE OFFICER. 4. THE WEIGHT CONCENTRATION OF THE CHEMICALS SHALL NOT EXCEED THE FOLLOWING SPECIFIED AMOUNT: COPPER SULFATE- 20% SULFURIC ACID- 10% ONLY THE CHEMICALS SPECIFIED ABOVE SHALL BE USED IN THIS EQUIPMENT. 5. THE OPERATOR SHALL RECORD THE CONCENTRATION OF THE CHEMICALS IN THE TANK DURING REPLENISHMENT. THE RECORDS SHALL BE MAINTAINED FOR A PERIOD OF TWO YEARS AND MADE AVAILABLE TO DISTRICT PERSONNEL UPON REQUEST.



## ORIGINALSOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 21865 East Copley Dnve, Diamond Bar, CA 91765 

## PERMIT TO CONSTRUCT/OPERATE**C~NTlNUATlONOFPERMIT** TO CONSTRUCf/OPERATE

NOTICE PennilNo. D70356 A/N278389

IN ACCORDANCE WITH RULE 206, TIllS PERMIT TO OPERATE OR COPY SHALL BE POSTED ON OR WITHIN 8 METERS OF THE EQUIPMENT. THIS PERMIT DOES NOT AUTHORIZE THE EMISSION OF AIR CONTAMINANTS IN EXCESS OF THOSE ALLOWED BY DMSION 26 OF THE HEALTH AND SAFETY CODE OF THE STATE OF CALIFORNIA OR THE RULES OF THE AIR QUALITY MANAGEMENT DISTRICf. THIS PERMIT CANNOT BE CONSIDERED AS PERMISSION TO VIOLATE EXISTING LAWS, ORDINANCES, REGULATIONS OR STATUTES OF OTHER GOVERNMENT AGENCIES.



## ORIGINAL EXECUTIVE OFFICER



### By Dorris 

### M. Bailey /rgc 

### 2/25/1993

### EXECUTIVE SUMMARY

Anaheim Platin g. I nc. 

### of A nah ei m , Ca l ifornia i s're quired 

### b y perm it co nditi o ns to co ndu ct a so u rce co mpli ance lest. Th e re sult s are to be 

### r

epo rted to 

### th e So uth Co as t Air Qualit y Management Di s tri c t (SCAQ MD) loc ated in Diamo nd Bar. The co mpany has o ne decorativ e c hro me plating 

### lank with process gases wh ic h ex haus t fir s t thr o ug h a 

### s in g le sc rubb er and th e n throug h a 20 in c h diameter s t ack. Th e e mI SSIO n point i s approx im ate ly 25 f eet hi g h

. The t es t is bei ng co ndu c te d 

### b y Che mi c al Dara Ma nageme nt Sys t e ms o f Dub lin , Calif o rni a. The t es t metho ds be in g use d ar e ba se d on tho se deve l o ped und e r th e directi o n o f th e Ca lifo rnia A ir Re so urces B oard 

### (CA RB ) and are referred to as CA RB Me th od 425. Th e SCAQMD s l ig h tly modifi e d th e proc e dure in m eth od 205. 1. It i s th e modi fied 

### SCAQM D ve rsi o n 

### which we wi ll b e u s in g. The enclosed s amplin g protoco l pro vides a detec ti o n lev e l o f less 

### than

. 001 mg/a mp - hr for hexava lent c hro miu

_ m. Anahe im Platin g. In c. is perm itte d to e mit 0.03 mg/a mp hr. Th e foll o win g les t r es ults were o btain e d : 

### T o ta l C hrome Hex C hrome (amp hr (a mp hr ) T es l # 1 0.00247 1 0.000302 Test #2 0

. 00 1 555 0.000283 Two t es ts were run , e ac h las ting 5 hou r s . A nah e im Platin g perform s its ope ration s us in g 50 amp s pe r hour or less. At Ihi s rale , us in g th e highe s t e mi ss io ns rat e per amp ho ur , th e e mi ss ions of hex ava lent c hro mium would be 0.0 151 mg/amp hour. Thi s is we ll be low th e 

### p e rmitte d leve l of 0.0378 Be twee n te s t s, a was h dow n w as pe rf o rm e d as de sc ribed in co nditi o ns #6 and #8. Durin g the les ts , pe ri od ic mo nitorin g of th e s tatic differe nlial pre ss ure ga uges mou nted o n t he sc rubb er ho us in g s howe d that th e diff e r e ntial press ure did not e xceed 4.5 in c hes of water across th e sc rubbed (con diti o ns #9 and # 10). Smoke te s ts s howed that the fume hood ca ptured all vapo rs e mitte d from the c hro me tank s urf ace.

Anaheim Pl ating. Inc. Apri l 11. 1993 Page 1Results Test run #1
Anaheim P latin 

### 3

. 29.93 T es t # t Diameter 

### 0.238 inches Ms 

### 28.60 Y 

### 1.00 A n 

### 0

. 0003 1 sq 

### It Pbar 

### 30.04 in c hes Hg T s t d 

### 528

. 00 R ankin Bws 

### 0

. 02 Pq 

### 0.45 inch es HQ As 

### 5 .24 sq 

### It Cp 

### 0.84 coeff icie nt 

### Ps 30.07 in ches Hg 

### Ds 3 1

. 00 in ches Kp 

### 85

. 49 co nstan t Pstd 

### 29.92 inches Hg Ts( avg) 

### 5 30.63 Ranki n Mel 

### 29

. 00 

# • 300 .0 0 minut es Pv(av g) 

### 0.48 Tm( ave) 

### 537

. 49 Rankin Amperage 

### 250 V m 

### 2 13 .92 cu 

### ft CRtotal 

### 0

. 000 1 80 mg Vm(s td ) 

### 2 11.22 cu 

### It CRh ex 

### 0.000022 mg Vo 

### 42

. 24 c u fVhr CRtperamphr 

### 0

. 002471 mg /a mp - h o ur I 

### 98.8722 Om 

### 43

. 59 cu 

### fVhf CRhperamphr 

### 0

. 000302 mg /a mp-hour

. Vs 

### 39.2 1 ft/sec

Ostd 

### 724 .872 c u fVhr Vratia 

### 17

. 1 59.12

Page 1

### SOURCE TEST PLAN SUMMARY Company Information Company Name Anaheim Plating, Inc. Contact Gabriel Barriga Address 928 East South Street City, State Anaheim, CA Phone (714) 776-3597 Source Information Type of Unit single tank, single stack Purpose Chrome plating of car wheel rims Testing Firm Information Company Name Chemical Data Management Systems Contact Ed Lewis 

# - Address 11750 Dublin Blvd. City--, State Dublin, Ca 94568 Phone (510) 551-7310 Testing Information Procedure Used



### St k 

### D ° 

### to ac escnp IOn Stack Height Stack Diameter Sampling Ports Samplin2 Platform SCAQMD Method 205.1, Determination of hexavalent chromium and total chromium emissions from chrome plating and anodizing equipment using a wet impingement train.

25 feet 20 inch Diameter inches 2 sampling ports located 90 degrees apart which comply with the modified 8 and 2 rule (2 and 0.5 minimum) Roof Access

Anaheim Plating, Inc. April 11. 1993 Page 2

### Sampling point locations

T raverse P

. t OlD S 

# - d bl ou e t 

### por s t d t 90° 

### oca e 

## a ang es Point Number % 

### of Diameter Inches From Edge 1 

### 2.1 1 2 6.7 1.3 3 11.8 2.3 4 

### 17.7 3.5 5 25.0 5.0 6 35.6 7.12 7 64.4 12.9 8 75.0 15.0 9 82.3 16.5 10 88.2 17.6 1 1 93.3 18.5 12 97.9 19.0

Anaheim Plating. Inc. April 11. 1993 Page 3

### Stac k Gas Co nditi o n s for run # 1 Stac k Temperature 

### ambient Ex pe c ted Pitot H ead 0.1 in c hes of H2 

### O ,

- 

### Gas Ve loc ity 39.21 ft/sec Stack Area 

### (3. I 4 )(20/2) 

### 2(1 / 144) ; 

### 2.18 ft 2 

### Vo lume F low Ra te 

### 724,872 cu ft/ho ur Wa ter 

### Vapor 2% Oxyge n 20.9% Carbon Dioxide 0.0 % Barometric Pre ss ure 

### 30.04 Mo le c ul ar Weight Ai r 29.0 Nozz le D i ameter/ Area 

### 0.0.235 in ches ; 

### 0.000301 ft 2 

### Sa mple Vo lum e 2 1 3.92 ft 3 

### App li ed A mp era ge 50 Time 

### at Each Poi nt 12.5 

### minutes Total Sa mple 

### Time 300 minutes ; 

### 5.0 hr Tota l 

### C harge per Ru n 250 Process Cyc le 1 00% De t ect ion L imit 

### 0.0002 8 m g/a mp-hr

,

Anaheim Plating, Inc. April II, 1993 Page 4

### S tack Gas Co ndition s (es timate s) for run 

### #2 

### S tack Temperature ambient 

### Expected PiLOt Head 0

. 1 inc he s of H2 

### O Ga s Ve loc it y 3 6 .3 7 ft / sec Stack Ar e a 

### (3

. 14)(20!2) ' (I1144) = 

### 2.18 ft ' Vo lu me Flow Rate 

### 6 80,396 cu ft /hour Water 

### Vapor 2 % Oxygen 20.9% Carbon Dioxide 0.0 % Ba r o metr ic Press ure 

### 30.04 Mo lec ular Weigh t Air 29.0 Nozz le Diameter/Area 0.0.235 inches = 

### 0.00030 1 ft' Samp le Volu m e 

### 191.23 ft 3 

### Applied Amperage 500 Time at 

### Eac h Point 

### 12

. 5 minute s 

### To tal Sa mple Time 300 minutes - 5

.0 hr Total Charge per Run 2,500 Process Cyc le 100 % Detection 

### Limit 

### 0.0000 I mg / amp - hr

A na hei m Plati ng , Inc . A p ril 11. 19 93 P age 5

### Source Test Constituent and Methods Contaminant Sampling Method Analytical Method Total chromium SCAQMD Method 205.1 AA Hexavalent chromium SCAQMD Method 205.1 Ion Detection Limit Calculation

see attached calculation sheet Detection Limit Test #1 

# = 0.00028 mg/amp-hr Detection Limit Test #2 = 

### 0.00001 mg/amp-hr Exceptions Graphite Furnace chromatography

Approved SCAQMD method 205.1 sampling methods will be followed with the following exceptions: 1 ) Filter unit will be placed between the second and third impingers. The third impinger is fitted with a thermo coupler for continuous monitoring of sample gases to insure that the temperature stays below the dew point. With the filter unit in this position contamination of the thermo coupler is avoided.

Anaheim Plating, Inc. April 11, 1993 Page 6

### Stack Test Protocol Following is the protocol that was used for chrome stack testing at Anaheim Plating. The protocol is based on the SCAQMD method 205.1 The procedure is used to provide engineering data to the operators and to provide compliance data to the District. For this test two sample trains are run. The propose of the test is to show compliance with permit conditions. Tank Process Conditions 1. Parts in the tank are typical of what are run on a regular basis. 2. Tank temperature is to be consistent with normal plating practices. 3. Typical amperage will be applied to the tank during one test run. During the other test, the**amp~rage** 

### will**~**

### be increased to the maximum amperage which can be safely applied. Test Protocol: 1. The purpose of this test is to determine the emISSions of hexavalent and total chromium per amp-hour of plating based on specific plating tank process conditions. 2. The test method is based on the SCAQMD Method 205.1. 3. SCAQMD Methods are' used to determine stack gas velocity, dry molecular weight, and moisture content. 4. Isokinetic sampling is used. Air flow is calculated from pressure drops measured using a Dwyer Microtector Portable Electronic Point Gage and a 5/16" standard Pitot tube of appropriate length. 5. The sample train (see attached drawing) components are made of glass or Teflon and a Teflon fiber filter. Neither the probe or the filter are heated since duct temperatures are near ambient.

Anaheim Plating, Inc. April II, 1993 Page 7

### 6. Two sets of three impingers are used. For each set the first two impingers contain 100 milliliters each of 0.02N NaHC03. The third impinger is empty, except for a thermocouple. 7. An 11 centimeter diameter Teflon fiber filter In 

### an appropriate filter holder follows the second impinger. 8. A drying column is used to dry the air after it leaves the third ImpInger. 9. Flow through the impingers is measured using a Dwyer Series RM Flowmeter. Flow is created using a Dayton Speedaire Oil-less Vacuum Pump. Volume is measured using a Rockwell Test Meter S275. Temperature is measured using Ashcroft Bi-Metal Dial Thermometers. Barometric readings are obtained from the weather service of the local airport. 1a. After collecting the samples, each sample train is capped and transported to the laboratory. No field cleaning of the train is done. The laboratory that is' used is West Coast AnalYtical of Santa Fe Springs (714-776-3597.). They are approved by various South Coast regulatory agencies and have received state certification under the new state certification plan. Their resume is available upon request. 11. Train rinse is performed using a.OlN NaHC03. The filter is acid digested. 12. Determination of hexavalent chromium is done colorimetrically. Minimum detection level is 2 parts per billion (2 ppb). 13. Total chromium will be determined by digesting the sample in concentrated nitric acid followed by the 

# Ie method described in §3.7.2 of method 205.1. Minimum detection level is 0.01 parts per billion.

Anaheim Plating. Inc. April 11. 1993 Page 8

### QA / QC 

### 1. The sample train is rinsed at the laboratory with nltnc acid, filled with the appropriate solutions, capped or I 

### sealed and transported to the test site. 2. Blanks and spike samples are prepared by the laboratory, transported to the site and returned to the laboratory for analysis. 3. Samples are analyzed within 48 hours of arrival at the laboratory. 4. Components of the sample train that require calibration are returned to the supplier/manufacturer: Yearly or, If 

### they are inconsistent with other readings or If 

### error is suspected 5. All test equipment is**identifi~ble** 

### by serial number. 6. Chain of custody forms are initiated at the test site. The forms follow the sample train from the job site, to the lab, through the lab and are attached to the lab results.
Attachments: Results Test 1 Results Test 2 Stack Test Equations Laboratory Results Field Data Notes Facility Location Drawing Sample Train Drawing Schematic flow diagrahm Detection limit calculations Permit to construct/operate Scrubber description Copy of Chain of Custody Air Meter Calibration Form ST-2

Anaheim Plating. Inc. April II. 1993 Page 9Results Test run #1

Pv Ts am Tmi Tmo Meter Start 

### 110.78 1 

### 0.50 13.60 43.74 74 70.00 119.80 2 0.70 22.60 52.56 88 78.00 129.40 3 0.60 22.60 48.66 88.00 68.00 140.80**~** 

### 0.60 21.70 48.59 90.00 68.00 150.90 5 0.60 20.40 48.48 89.00 70.00 161.20 6 0.40 24.80 39.88 88.00 70.00 169.40 7 0.50 19.70 44.20 82.00 66.00 178.40 8 0.60 19.30 48.39 80.00 64.00 187.80 9 0.80 19.20 55.87 80.00 64.00 199.70 10 0.50 19.60 44.20 82.00 64.00 208.60 11 0.50 20.10 44.23 83.00 66.00 217.90 12 0.50 21.40 44.33 88.00 66.00 227.10 13 0.40 21.70 39.67 87.00 69.00 235.30 14 0.50 21.2 44.32 84.00 69.00 244.60 15 0.40 19.70 39.54 85.00 69.00 252.90 16 0.50 23.30 44.48 83.00 72.00 261.00 17 0.60 23.90 48.77 93.00 72.00 272.00 18 0.40 26.00 39.96 97.00 73.00 280.40 19 0.30 26.40 34.63 95.00 t 

### 75.00 287.70 20 0.30 25.50 34.58 

## . 90.00 75.00 294.70 

# - 21 0.40 21.40 39.65 80.00 70.00 302.40 22 0.40 22.70 39.74 81.00 70.00 310.50 23 0.30 19.70 34.24 80.00 69.00 317.60 24 0.30 18.50 34.17 78.00 66.00 324.70

Page 2Results Test run #2
Anaheim Plating 3.29.93 Test #2 Diameter 0.238 Inches 

### Ms 28.60 

### Y 1.00 An 0.00031 sq 

### ft Pbar 30.04 inches Hg Tstd 528.00 Rankin Bws 0.02 

## iPg 0.45 Inches Hg As 5.24 sq 

### ft Cp- 0.84 coefficient Ps 30.07 inches Kg 

### Os 31.00 inches Kp 85.49 constant Pstd 29.92 inches Hg Ts(avg) 524.39 Rankin Md 29.00 

# " 300.00 minutes Pv(avg) 0.42 Tm(avg) 527.10 Rankin Amperage 2500 Vm 191.23 cu ft CRtota! 0.001100 

### ffiR Vm(std) 192.54 cu ft CRhex 0.000200 mg Vo 38.51 cu ftlhr CRtperamphr 0.001555 mg/amp-hour 

### I 96.0174 Om 40.44 cu ftlhr**CRh~eramphr** 0.000283 mg/amp-hour

. Vs 36.37 ft/sec

Ostd 680,396 cu ftlhr Vratlo 17,669.30

Page 1

### Results Test run 

### #2



### Pv Ts am Tmi Tmo 

### Meter Start 332.57 1 0.20 18.60 27.90 78 61.00 338.40 2 0.30 16.,90 34.08 70 60.00 345.40 3 0.30 18.50 34.17 71.00 61,.00 352.60 4 0.40 19.40 39.52 73.00 60.00 360.80 5 0.40 18.60 39.46 73.00 61.00 368.90 6 0.40 17.70 39.40 72.00 60.00 377.10 7 0.30 15.90 34.02 70.00 58.00 384.30 8 0.30 16.40 34.05 72.00 58.00 390.90 9 0.30 15.40 33.99 72.00 58.00 398.50 10 0.40 16.50 39.32 72.00 58.00 406.60 11 0.40 17.20 39.37 77.00 58.00 414.80 12 0.40 17.40 39.38 78.00 58.00 423.10 13 0.40 18.00 39.42 70.00 58.00 431.40 14 0.40 18.9 39.48 76.00 58.00 439.50 15 0.40 19.10 39.50 86.00 60.00 448.80 16 0.50 19.70 44.20 80.00 60.00 457.50 17 0.50 19.00 44.15 80.00 61.00 466.70 18 0.50 18.80 44.14 80.00 62.00 475.80 19 0.60 19.70 48.42 78.00**~** 

### 62.00 486.10 20 0.60 18.10 48.29 

# . 76.00 61.00 496.00 

# . 21 0.60 18.10 48.29 77.00 60.00 506.20 22 0.50 18.00 44.08 75.00 60.00 515.50 23 0.50 17.90 44.07 74.00 59.00 524.60 24 0.50 18.00 44.08 76.00 60.00 523.80

Page 2

## Stack Test Equations Amperage = Amperage applied to tanks AN = Cross sectional area of. nozzle As 

# =Cross sectional area of stack Bws 

### = Water vapor in 

### the gas stream Crhex = 

### Hex chrome collected Crhperamphr= Crhex 

# * VRatio 

# *60/ (Amperage 

# * 9) Crtotal 

# = Total chrome collected Crtotalperamphr= Crtotal 

# * VRatio 

# * 60/ (Amperage 

# * 9) Cp 

### = Pitot tube 

### coefficient = 0.84 TS(AVg)

### V (Id)P sid 

### 1 00 I = Isokinetic Variation = m 5 

### TsldVs

### 9A n

### Ps 

### 60(1- 

### Bws) K - P' be 

### 8549 ft [(Ibllb-mole)(in.HG)f12



### p - 1tot tu constant . - 

# (0)(. ) sec 

### R 

### lD.H 2

### 0 

### Md = Molecular weight of stack gas, dry 

### basis = 29.0 Ms = Molecular weight of stack gas, wet basis Ms = 

### M d 

### (l- Bws) 

## + 18.0Bws P 

### = Velocity head of stack -gas, mm 

### H20 Pbar = Barometric pressure at measurement site P8 

### = Stack static pressure P 

### Ps 

### = Absolute stack gas pressure = Pbar 

## + _8- 

### 13.6 P sid 

### = Standard absolute pressure (29.92 in. Hg) ts = Stack temperature ·CCF) Ts 

### = Absolute Stack temperature °K(OR) Ts =460 +t, Tsld = Standard Absolute temperature 293°K(528°R) 9 = Total sampling time 3,600 = Conversion Factor, seconds to hours 18.0 = Molecular weight of water Y 

### = Dry gas meter calibration factor Vm 

### = Meterstartreading

- Meterfmishreading V = Sample gas volume = V 

### Y (Pbar)(Tsld )

m(sld) m 

### (PSld )( 

### T m( aV

# 8») V 0 

# = V m(sId) 

# * (60 / 9) VRatio = QsId / 

### V 0 

### Vs = Average stack gas velocity, m/sec (ft/sec)= KpCp(-.jllp

# L8Q51d 

### = Average stack gas dry 

### volumetric rate 

### = 

### 3600(I-B ws 

### )V,A,(/"" ')( 

### P.) 5(11\18) 

# )lpild 

### Q

### m= 

### An (3600)(85. 49)(C p ) 

# T;;:a::)
Calculator:

. 

### Qm =' 1" 

### STD' PV' 

### STO' PS' 

### STD' 79.87 

# * ((T 

# * 1. 8 

## + 492) 

# * PV 

## I (PS 

# *28.6))A. 

## S

### April 5, 1993

CHEMICAL DATA MANAGEMENT SYSTEMS 11750 Dublin Blvd. suite 201 Dublin, CA 94568 Attn: Ed Lewis JOB NO. 23630
LABORATORY REPORT Samples Received: Three (3) Impinger Trains Date Received: 3-30-93 Purchase Order No: Anaheim Plating The samples were analyzed as follows: Samples Analyzed Analysis Three (3) 

### samples Total Chromium by SCAQMD 205.1**~.** 

### Three (3) samples Hexavalent Chromium by SCAQMD 205.1 

# WEST COAST 

# ANALYTICAL SERVICE, INC. ANALmCAL CHEMISTS

D



### Results Data Sheet
Data Sheet

Page 1 of 

### 4

# W~ Michael Shelton Technical Director J J J 

## I I I

# D.~on, Ph.D. President This report is to be reproduced in its entirety. 9840AlburtisAvenue • Santa Fe Springs. California 90670 • 310/948-2225 • FAX310/948-5850

### WEST COAST ANALYTICAL SERVICE, INC. CHEMICAL DATA MANAGEMENT SYSTEMS Mr. Ed Lewis
LABORATORY REPORT Job # 23630 AprilS, 1993

Total Chromium in Impinger Train Quantitative Analysis Report Inductively Coupled Plasma-Mass Spectrometry Sample ID Blank Train Train #1 Train #3 Detection Limit Date Analyzed: 4/1/93

Sample: Batch QC Matrix: Impinger ppb (ug/L) ND<0.6 4.4 

### 0.7 0.6 Volume (L) 0.235 0.253 0.258 Total Micrograms ND<O.l 1.1 

### 0.18

Total Micrograms Sample

Chromium 8.3 Spike Cone

ug 142.9 MS



# -------- 170 MSD % % 

### Recovery Recovery



# -------- 

# -------- -------- 113.2 163 108.3 Date Analyzed: 3/30/93

Page 2 of 4

# ===========~============ % 

### RPD



# ------- 4.2

### WEST COAST ANALYTICAL SERVICE, INC. CHEMICAL DATA MANAGEMENT SYSTEMS Mr. Ed Lewis
LABORATORY REPORT · Job 

### # 23630 

### AprilS, 1993



### Hexavalent Chromium by 

### SCAQMD 205.1 

### sample Total Micrograms Sample Train #1 Sample Train #3 

### Blank Train Detection Limit Date Analyzed: 3/31/93 0.20 0.022 

### NO 0.002



### Matrix Spike/Matrix Spike Duplicate Sample:Train #3 

### units :ppb (ug/L) Sample Amount MS % Rec Analyte Result Spiked Result MS



# - - Hexavalent Chromium 0.084 1 1.08 100


### QC Limits RPD Analyte Warning Control Recovery Summary

'. 

### MSD % Rec Result 

### MSD
1.1 102



### % Recovery Warning Control 

### RPD

2

==================================================================== 

### Hexavalent Chromium 9 

### 13 86 108



### Page 3 of 4

## ============~============= 74 117

### WEST COAST ANALYTICAL SERVICE, INC. CHEMICAL DATA MANAGEMENT SYSTEMS Mr. Ed 

### Lewis
LABORATORY REPORT'

sample Sample Train #1 Sample Train 

### #3 Blank Train Date Analyzed: 4/1/93 Moisture From Silica (g) 

### grams

2.0 4.0 0.0**~.** 

### Job # 23630 April 5, 

### 1993

Page 4 of 4

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## ._._---------- L-JG SC>o.£ ('[[11 

### ANAHEIM PLA TlNG, INC. 928 E. SOUTH ST. ANAHEIM. CA 

# t

DR. BY: G.P. T. DATE: 01-18-93 REV. NO: OATE: BUILDING HEIGHTS AIR PERMIT CHEMICAL DATA MANACEMENT SYSTEMS 11750 DUBLIN BLVO .• S lE**?~,** ouBLIN. Clio**9~568** (510)**55~** - noo" , 

# -' -....,...



# --------_._---- w z ::I**~** a:: w a. o a:: a. CHROIlAE TANK

OUTSIDE STORAGE

rRONT or eUllOINC


### "-

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# _._-_._-- '0,--"," 

## :.':·::::{l;li"

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NICKEL TANK 

# EJ

(FEET)

...... '-'0-.0-

... _ ...... 1.11750**DU~LIN** BlVD .• STE 7.01 DuBliN C':A Q4""'R '''In\

..... 'o·nnf , 

# I ANAHEIM PLATING, INC. I 928 E. SOUTH ST.

# I~ ANAHEIM, CA 

### ! DR. BY: CPT. I REV. NO: 

### J F" ACIU TY SI TE PLAN DATE: 01-18-93 I DATE: I AIR PERMIT I CHEMICAL DATA MANA CEMENT SYSTEMS

,PILOT TUBE THERMOCOUPLE
PROBE

STACK TYPE S WALL PITOT TUBE



## FIGURE #1 

## SAMPLE TRAIN
- #2 THERMOCOUPLE 

### ---'

........ 

## _----

THERMOCOUPLE F"ILTER HOLDER

BY-PASS VALVE ICE BATH JMPINGERS**~**__ VACUUM LINE

THERMOCOUPLE READOUT VACUUM GAUGE

08-12-91 MAIN VALVE AIR TIGHT PUMP CONFIDENTIAL

DATE LTR DESCRIPTION C.D.M.S. T 

## & M PRODUCTS 11750 DUBLIN BLVD .• STE 201 DUBLIN. CA 9456R

## SCHEMATIC FLOW DIAGRAM - ANAHEIM PLATING, INC.

Sample platform 14" from emission point to sample port

., Do 

### -Sample ports Stack diameter 

# =20" 72" from 

### 90° bend to emission point



### 56" from 

### 90° bend to sample port



# - Scrubber fan "- _________ --1 

### 7,000 cfm



# -

'scafolding Scrubber Anaheim Plating, Inc. (roof)

Scrubber platformDetection Limi t Calc



### Det e ction Limit Ca l c ul ation Anaheim Plating , Inc

. 3 / 11 / 93

24.00 12.50 minutes 300.00 minutes

33.13 ft/sec 20.00

2.18 

### sq ft 260,070.50 cu fUhr 0.238 i nc h 0

. 000309 

### sq ft 184.14 cu 

### ft 500.00 amp 2,500

. 00 amp 1.00

0.00001 mg 0.07 mg 0.00003 mg / amp · hr N u mber of Points Time Per Poin t Length of Tes t Stack Velocity (33.13 fUsee i s BAAQM D minimum) Stack Diameter S tack Area Stack Flow Rate Nozzle Diameter Nozzle Area Samp le Vo l ume Applied Amperage To tal Charge Pe r Run Process Cycle Detectio n Limit Calculatio ns Detection limi t per Sample (samp le s ize 1 lite r ) M i n i mum detectable per test Detection limit in mg/amp-hou r

Page 1Detection Limit Calc



### Detection Limit Calculation Anaheim Plating, Inc. 

### 3 / 11 / 93

24.00 1 2.50 minu tes 300.00 minutes

33. 13 ftlsec 20.00

2.18 sq ft 260,070.50 cu fV hr 0.238 inch 0.000309 sq ft 18 4

. 14 c u ft

50.00 amp 250.00 amp 1. 00

0.0000 1 mg 0.07 mg 0.00028 mg/ amp- hr N umbe r of Points Time Per Point Length of Tes t Stack Ve locity (33.13 fUsee is BAAQMD minimum) Stack Diameter · Stack Area S t

ack Flow Rate Nozzle Diamete r N ozzle A r ea Samp le Vo l ume Applied Amperage Total Charge Pe r Run Process Cyc le Detection Limit Calc ulat io ns D etection l im it per Samp le (sample size 1 liter) Minimum detec t able p e r test Detection limi t in mg /amp-hour

Page 1Nozzle Capacities
T= 

### 40 Kp= 

### 85.49 Cp:;. 

### 0.84 Pbar= 

### 29.92 Pg= 

### 0.3 Ps= 

### 29.9420588 Ws 

### 28.60 /" 

# - " Diameter i.- 

### 0.175 ( 0.235 

### ) 0.375 Area
- Sq Ft
- 

# ,..,. 0.000167 0.000301 0.0007-67 p\/ 

### 0.1 11.08 19.97 50.86 0.2 15.66 28.25 71.93 0.3 19.18 34.60 88.09 0.4 22.15 39.95 101.72 0.5 24.77 44.66 113.73 0.6 27.13 48.93 124.58 0.7 29.31 52.85 134.56 0.8 31.33 56.49 143.86 0.9 33.23 59.92 152.58 1 35.03 63.16 160.84 1.1 36.74 66.24 168.69 1.2 38.37 69.19 176.19 1.3 39.94 72.02 183.38 1.4 41.44 74.73 190.30 1.5 42.90 77.36 196.98 1.6 44.31 79.8-9 203.44


# - 1.7 45.67 82.35 209.70 1.8 46.99 84.74 215.78 1.9 48.28 87.06 221.70

2 49.53 89.32 227.46



### . 2.1 50.76 91.53 233.07 2.2 51.95 93.68 238.56 2.3 53.12 95.79 243.92 2.4 54.26 97.85 249.17 2.5 55.38 99.87 254.30 2.6 56.48 101.85 259.34 2.7 57.55 103.79 264.28 2.8 58.61 105.69 269.13 2.9 59.65 107.56 273.89

3 60.67 109.40 278.58 3.1 61.67 111.21 283.18 3.2 62.66 112.99 287.71 3.3 63.63 114.74 292.17 3.4 64.59 116.46 296.57 3.5 65.53 118.17 300.90 3.6 66.46 119.84 305.16 3.7 67.37 121.49 309.37 3.8 68.28 123.13 313.53 3.9 69.17 124.73 317.63

4 70.05 126.32 321.67
Page 1SOUTH COAST AlA QUAUTY MANAGEMCM UISTRIGT 21865 

## east Copfay DrIve, CAaITlOfld 

### Bar, CA 91766 

## PERMIT TO CONSTRUCT IOPERATE**~** ANAHBJM PlATING INC ATJ'N: DIEGO BARRIGA 

### 928 E SOO1H ST ANAH.EIM. CA**~**

f.4ujlptyllt DuatpIIon: AIR. 1.

1. mON CONTROL SYS'I'E!M CONSJS1"INO OF: SCRUBBER.. DUAIJ.. MODEL 

### PWm. VJ!R.1'IC'AL TYPB, "-$ W. X S-UY' L U'-6- 

### H.. EQUJPPIID 

### W1TH.A MIST eLIMINATOR. AND A 1/2 H. P. PBED PUMP. iaxHAUST S\'STEM: 'MTJ{ 20 JU'. BtoWER. VP.NTINO THE DECX>RATIVE CHROME PLA'X»rG TM"K,

: OPERAnON OF·fHJS I!QUlPltIONT SHAU. B8 (nNDUCTED IN ACCORDANCE WrrH AlL DATA AND SPEClPICATIONS SUBMl'I'IT'.D 

### \\ITR THE APPLICAnOM UNDER WHICH THIS PeRMlT IS ISSUED UNLP.SS O1'1fERWlSE N01'ED' BELOW. 2,

. THIS EQUJPMENr SHALL Be PROPEIU. Y MAINTAINED AND KePI' IN 0000 OPERA1'lNQ 

## ! CONDmON AT ALL TIMeS.

THJS SYSTEM SHAll. BE IN PUU.**u~** WHENEVI!Jt THB D!!CORATIVE CHROMJ:! 

### PIA TlNG TANK Vf!NTEO TO IT IS IN OPBRAI10N. 11m CHaOME PLATlNG TANKSUBdIC'r TO RULE 1169 AT 

## nos PACJurY SIiALL.BE EOUIPPED WInf A NON-REsE1TABE. TOTALJ2'lNO. AMPERB-HOUR METER THAT MEA.'URES THE PLATING CURRDrr INTeGRAtED OVER TIME. mE TOTAL AMPERB-HOVRS Of 

### Tim PLATING CUllRENT APPLIED TO THE Cf{R.OMS PLATING TANK AT THIS FACILITY SHALL NOT EXCEBD 638,:302AMPERB-H0t1RS IN ANY ONE YE.Alt. 

## nm <»'ERATOR SfiALL PEIlRlltM A I MINUTE WASHDOWN AT LEAST.EVf..RY 8 

### HOURS OF OPERATION. 

## OJlIGINAL 

# I. , 

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# .---.

A FLOWMtiTER SHALL BE JNSTA48>AND NAlNTAlNED TO JNOICAtt IN**~~UONS** PER MJNU1E THE PLOWRATe OP'1lHBWA1'1!R SUPPLYING T8B MESH PADS DUlUNG WASHDOWN. THE SCALE OH11I!! JILOWMBTER SHALL NOT EXCIUID POUR TlMBS "nmUMrr SPBCIPJED IN CONDmON 8. &. THB PLOWJlATE OF THE WATER OOIUNG WASHDOWN SHALL NOT DS LESS T1L\N S OALtONS 

### PmlMINUTE. p. A GAGS SHAl.L BB 

### INS'I'ALLIJD MNDMAINTAINBD TO INDICATE IN INCHeS OPWAT£R 

## nm STATlCP'RES#IORE**~ACROSS** 11fI!SClUJBBBR.11mSCALB ON 'l1mOAGE SFIAU. NO'I' BXCBBD POVlt 

### 'iUd!s THE UMrJ" SPBafIB'D 1N OONDmoN 10. lO. THE TOTAL STAnC PIteSStJRB OlJIfDENrt.\LACROSS niBSCRUBBBR SHALL NOT BXCBED 

### 45lNOf OPWATBR DURING OPmtA11ON. 1L THE EXHAUST Sl'ACKSHALL DISCHARGE IN AN UPWARD DIRBl.'l10N AT A HEIGHI' OP2S 

### FEIn'ABOVE GROUND. 12. 11fE HBXAVAJ..EMT CHROMIUM BMISSlONS SHA1.L NOTaCE£D 0.0378 MILLlGltAMS PER HOUR. 13. nmOWNek Q1l OPBItATOR OFTHB EOUIPMBNT SHALt. CONOUCI' A SOURaTSSrTO DEMONS11tATE**~\\Il11I** CONDrnON**12~** THEPOUOWJNO CONDmONS: A. A SMOKE TP..S1I'SHAlL DB CONI>UCI'ED mOR TO nmACTUAL SOURCE TEST TO DEMONSnlATB NO JrUOUl1YE J!MJSSIONS WIlL OCCUR DURlNG OPf!RADON. B. 11mSOURCE 'l"EST SHALL BE CONDUCT£D Wl11DN 30 CAL£NDAR DAYS API'BR 

### JNmAL START-OP. 

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### TOTAl" CHROtttIUM 

### ANJl 

# ma**ilimiAV~CHaOMIUM** EJdS!DONS TO THB ATMOSPHERE PROM THB 

### Alit: fOlLtmO!UtbNftoL.8OVII"NJ!N1' VENI1NG THE DBCORATM! arROME PLATlMG TANK. 

## nOiH&XAvAlJeNtCHROMIUM EMISSlONS SHALL Hal EXCEED THB TOTAL 

### CHROMJUM .BMJSSlO1l1S. D.**nm~TI1SI'** SHAU.B£CONDUc:nm WHO.BTlmTANK VENI'El> TO**nus~JS. ~GATLOWLOADANDMAXJMlJMLOAD.**  nmWGHP.ST**~** 

### iNIssJolu LESS OPTHE lOAD SHAU. BE USJ!t) IN DEMONSTRATING**~wniJ** 

## coliDmoN' 12. E. DUllIHG 

## iHSnJST. 'I11E OUAN11TY OPWATER AND CHRONIC ACID ADDED TO 11HE**TANIC.~£~1tON** OP CRR.OMlCACID. TImFLOWRATES OP11IS WA'l'EIt 

### SUPPL¥lNG THE MSsHi'PADS DUIUNG WASHDOWNS. AND 'tHE TarA!. PRBSSUltB DROP ACItOSi-.TiaJdR 'POU.JU'nON CONTaOLS'M'EM SHALL BE MONITORBJ> AND REPOR.TED IN 

## '.l'H1i 

## souRCE TE'rtltPiORT.

ORIGINAL

# --

....

# -
...

# _-----. SOUTH**GOA~r** NR 

### OUAUlY MANAGEMENt DISTHIGT 21 M5 Ellsl**(ju~lh=!y** Drive, DIamond Bar, CA 91 (65 

### PERMIT TO CONSTKUCI'/OPERATE

.....* ;" ., 

### ..
F. 1HB (.:OMP.UAKCB!UNft' OI"THB 

### 'lOXIa DANCH SHAU BE NOItm:D OF THE DA'IE AND TIME OPTRE"TBST AT l..DSI' 

### to CAL.mlDAil DA'YS PRIOR TO nIB 'J'BST. Oil WlTHJN A TlNBAGRlmD UPON BYTHECOMPLlANCI! 

### UNJT. O. THE SOt1Jlal

### TI!S'i S1MLL COMPLY 

## wmr THEATrACIIED DlSTRlcr "GUIDELINES FOR 

## coNSTRucnON OPSAMPUNG AND 1BTING PACRmm

..... PURsUANT TO DISTJUCT RVlJ! 217. 

### H. 1111 

## souaca 11!ST SffIUL B8 OONDUCTED IN ACUl1lDANCB WITH TRIl 

### 'IWI' MI!THODS 

### OUTLlNBD 1N1Bin:mnwcrRULB 1169. 

### I. 'I'HS 

### SOURCE 

# 'f" SJMU. 

### BE PBRPORNED BY AN INDEPENPBNT QUALIFIED 

### TESTING J.ABORATORY 

### PURSUA'MTTO DlBI'RIcr 1t1.JLE 304- J. 

### 't'HE SOtJllCE 

### T.l!Sr REPORT SHAU.INCWDS RPSULTS OF THE SMOJCE TEST. THE SOURCE TEST, TH£ 0P'BIlIlI'ING 

### PARAMETERS OtmJNED IN CONDmON 12 (E). 

### AND AlL JTEMS US'J'Sl) ON THE ATMCIISD CRI!(1CUST (POR.M ST.1). 

### 'mE REPOltT SHALL BE 

### SUBMlTI1!D 

### TOTRE COMI'UAHcBUNIT OP11IB TOXICS BRANCH NOT lATER THAN 60 CALENDAR**DA~** 

### AM'U. 11m SOtIkCB'l1!STDA'IB. 

### A COPY OF 'llIB SOURCB 

## msr IlBPORT 

### SHAll. DB 

### 0PrAND BS MAJ)B"AVA.D.ABLE UPON DJSTRICl'REQUEST.
:14. 

### WHENBVJDt THE PLA11NU**~.IN.oPBRA"l1ON.** THE OPBllATOR SHAU. PRBPARE 

### AN.O MAlNTAJHJd!OjRDS"3'O**~TE(x)MPLIANCB** WIl'H CONDmONS 5, 

### c;, AND 8. AU. 

### RECORDS SBAUDS RETAINED 

### POll AT Ll!AST1WO YEAU AND MADE AVAIJ.ABt..E TO DfSTRICI' PBRSONNEL meN REQUEST.



### 0JlIG1NAL

# .- SOUTH COAST AIR QIJALIl'( MANAGOdFNT DISTRtCT 21 Ul).':i £331 Copley Olive, Diamond 

### Bar, CA 91765 

### PEKMIT TO CONSTRUCf/OPERATE 

# [**~~~~~.. ~~~~~~~~~** 

NOTtCS IN ACCOIlDANCB WI1li RtJLB 2G6, THIS PDMlTTO OPERATE OR (.X)PY SHALL BE. PaS l'ED UN OR 

### wmaN 8 MBTBJtS OFTHI! 

### P.t.RJ1lPMJ!NT. THIS PERMIT 

### DOeS PlOI' AU'I'HQIIntE 

### DIE EMISSION OF AIR CONTAMIHAIfl'S IN PXCBSS OF THOSE 

### ALLOWED BY DMSlON 26 

## OPTlIEimALnt AND SAP2TY CODa OJf1lJESTAT£ 0,.. CAUPORNlA OR. THB RULBS**QP1HBAlIlQUAUtY~J>fSTIUcr.** mJS 

### PERMlTCAJtl1'4'OT lm C'ONSJDBIU!D**AS~ION** TO VIOLA'T8 BXISTING LAws, ORJ)INANCI?S, REGULATIONS OR STA1'lJTaS OF 0'l'HBR- OOVEllNMEHrAGSNaBS.



## ORIGINAL j j 

### j j j j j j j j j j j j j j j j j j j j j j jj j

j j j

jj j

j j

### ( 

## • Sp&oifioation**Sh'6~'** Hat-Pro/DuA.H Propotl&.l No. 1,13.B891..008

. H

HEXMASTER 

### r: H!l O HIC ACID**SCRU~BER** 

### SYSTeM The exh

..utlC gu 3crubbtlr .hall be peckod-b.d t:.yp_
.... ith high·.ffichncy mitt ellmin4::or.. It shall be do.lgn"d for 1lIu.x!IIlWJI co !'laatLon o rtllaov41 officL

.. ney 

### ot 4ir contAtO.inants arhing from Chi procoss b

.. t::ha

. Scrubber exhaust sh.U comply '.11th Maximum Avail.able Cont:rol Technology (MAeT) IIIm111sion stllndard!l tor ('

.hro!llic acid. Scrubb&rs shall be conetrucccd from Typo I. Gr.e.da I, high. impact polyvinyl chlo=ide (PVC) conforming to ASTH 0-17 8 4, C.l1 14JJD except 'Where cQrrQcion rull1ta.ncl ot;"**TY'P~** 1 PVC 1,; bAccl'lr suited to the appUc,f,tlon. Tho .crubber bottol'll ah.e.l1 be f4bricl'I.t.,d f["olll 1/2" (minimum) PVC, PAcking .hall be r",ndoa..c!Wlp

.. d, high-.ffioiu\oy type. It shell b o hbricatod ero::! polypropylan. or och.r**c: rrollio:\·r~sl~clt.ne**  mat.ri.

..l , High.eftieienyy mist: ol1c.in,u:.orl> 6hdl be provided**~o c041ue~**  and elicin4t4 ent:rained dropls.cs:. Thay lOhdl be**1nt:egr~1** t:o t:h ••crubb.r dnd**£dbt lC41.~d**  erol); polypropylene. E11m1nato rs ahall be 1nstalhd

.... ithin removable cart:ridg

.. to fAc1l1t:4te mslnt enanelil

.**CAnr!d~ea** shall be .oeeh4nlc .ally sealed to pravent by· pel.1n5**~ing** 4n inter looking traok sy&tem. SprAY noz:zhB shall**b~** qUAnclry and**arraneem~nt** op en-orifica, non·clogsin& type**~nd** of iuff1ciant cn ensure o!Idcquuce**al~trlbut.ion** of \.:d,shdo\o"n solution. Aecess doors shall he prov i ded for 3prllY nozzle and**mi~t** elimin atur main· tonance. Furr.i.llh tI"oIInsporont vio\J ports to allow 

### tor l.n3peet:lon of mililt climinators and sprs:; n07.z1o!l. Dlfferentie.l**pr",~urCl** galiSIHI for monitoring pr ouure drop**dcros~** 

### chs packing and mist .lim10AtOrS ahall h e**p~ vldQd** **.** Flo\.1 IUltHJI for indicatin!,; / adjUMt:ing '.Ju:hdovn r..eel; shAll be provi(jed. Equipment t o r LutOe:l4cle. control of v,,,hdovtl o f the 6crubbar c_n b

. providad

. Tho pacKas. ghall include Slohnoi(j v,a,lvali and timoril. Hcnu d l "'p.::rat.ion eholl be lI cc om pllAhed by U!lC o f H · ()· A I!vitc:ho s mo untod On thl8 face 

### ot the**enclo.u1.'~.** A PLC**~n** .I!. HEMA 4**6nclo6ur~** 15 provid ed. ' Tho anclosur(! Gh",ll bi ,.,Lred**1n ~H**  n .. 11y, 'hrroin

... l blocks

.... ill b 4 pr ovided f o r ex':ornd connection",**Sp.c1f~oation** 

### Sheets HBe-Pro/Duall**P~opoaAl** No. 413·8894.008·M 

### Page 2



### HeAostar

1. Type

- FU303·53HH ? . t':a.ra.r.1 t!y

- 7. 000 CFH 

### 3.**~re'fute** 

### Drop· 4.5 Q 

### v.g. 4. MaceriAl of Con.cruct.loll

- Type 1 PVC: 

### 5. Firat Seage Packing Type

-**~l** 

### Tr1-Pack 6. 

### Y1r.t Stage \JAllhdown

- 4.84 

### gallons for 

### 1 mlnute 

### once every 8 houro. 

### 7. Second SC4$6**Co~l~seins** 

### Pa6 

### TyP& • Hono·f11&mRnt. 8. Seoond Stage Coalesoing Qashdown

- 4.84 gau,ona for 1 mInute once ovor:y 9 hours 

### 9.**Thi~d** 

### Stale Mist Rlim1n4t:or Typo •**Mono·fila~ent** 

### 10. th1r4

### Sr~8.**W&~hdown** • 4.84

### ~lM fur 1 

### mlnuce**on~c** a month 

### 11. FloWMetor Type. Dwyer Ser1as KM 12. nagnahe11c 

### Gauge 

### Type

- Dwyer Saries 2000 

# oMeter Designation ROCKWELL MODEL 5-275
Rated Capac,ly cfh CVM and GT meters-max. mdex rate Diaphragm meters- 2" H20 Dill.rate**~;:~:;** ::,::;: >- 101**~'!f; ~** **t~~'l'':­ ..t\~·:"z** 

### t~"'w**.t.*.~****~~~** 99'**~;-24** .



## ..**~** 

### ...**~**

FLOW RATE (AIR)
.25 CFM .5 CFM 

### .75 CFM 1.0 CFM 2 .**.:.~..;.~'.** 30 MINERS & PISANI, INC.

2010 Farallon Drive SAN LEANDRO. CA 94577 (415) 352-9040

TEST MEDIUM
- ATMOSPHERIC AIR

40 50 60 70

FLOW RATE
- PERCENT DF RATED CAPACITY
PERCENT PERCENT PERCENT RATED CAPACITY ACCURACY PROOF
100.2

.. 

### - .. ..

### _-- 100.1



### --- - .. ....._ .. 

### -

## - .--. 99.8 99.8

.. 

### ,---



## - Manufacturer's Number 6848207

Cartridge Number

DIFFERENTIAL (inches H2O) Tested on air

Customer:

__ CHEMI

___ C_AL

__ D_A_T_A

___________ _ Date Tested:

...... 

### ?,/?6I93

................................ .. ED LEWIS Customer P.O. No.:

_______________ _ R.H. Tested by:

......... . Customer Meter No.

_______________ _ Test Location:

..

### SOUTH COAST AIR QUALI1Y MANAGEMENT DISTRICT 

### TECHNICAL SERVICES DIVISION SOURCE TESTING & 

### MONITORING BRANCH •



### . INFORMATION REQUEST FORM (ST-2) 

### FOR PROTOCOL/REPORT REVIEW This form is to be completed by the processing engineer requesting an evaluation of a Source Test Protocol or Source Test Repprt. Please check off appropriate items and provide the corresponding requested information. The sampling and analytical methods will be reviewed for .ruJ!y. 

### those gaseous and particulate constituents identified.
Constituents AJlowable(1) Rule # NSPS Sampling Identify to be Limits or 40CFR60 Location any other Measured Conc. Mass Permit Identify Requirements (ppm) Flow Cond.# Subpart Rate Ob/hr) Example: [x] CO 

### 500 Reg ·IX 

### J 

### Exhaust Stack CO 

### BOO 

### Condo 12 Before CO Boiler CO 

### 2000 407 (a) (1) Exhaust Stack [x] NOx 

### 125 476(a) (1) Exhaust Stack 

### @ 3% 02 asN02 

## [ J CO

[ ] CO2

[ ] 02

[ ) S02



## .

(1) " allowable limit is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark with an asterisk (*).) Constituents to be Measured

[ ] S03

( ] SOx as S02

[ ) H2 S

[ ] Total

(Reduced) Sulfur Compounds asS02 [ ] NH3 (Free) 

### [ ] NH3 (Free) Combined [ ] NOx


### [ ] NOxas N02 [ 

## J TGNMO AJlowable(1) Limits Conc. Mass (ppm) Row Rate (Ibjhr) 

### TECHNICAL SERVICES DIVISION SOURCE TESTING & 

### MONITORING BRANCH INFORMATION REQUEST FORM GST·2) FOR PROTOCOL/REPORT REVIEW
Rule # NSPS Sampling

or 40CFR6Q Location Permit Identify Cond.# Subpart



# .-

" Identify any other Requirements

0

0 0

0

0 0 0 0 0 I**~** 0 

# I**~** 0 0 I**~**

0

(1) If allowable limit Is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark with an asterisk (*). 

### Page 2 of 4Constituents to be Measured

( ] Organics Speciated (Identity) [ ] 

### Part. Maner Oiquid) & solid) [ ] Part Maner (solid)
[ ] PM·10

[ 1 Part. J Size Distribution
( ] lead

[ ] 

### HeN

List other Compounds: 

### [XChromium Hex. & 

### Tot**~l** Allowable(1) Limits Conc. Mass (ppm) Row Rate Qb/hr)



## .

0.03 mg/am 

### TECHNICAL SERVICES DMSION 

### SOURCE TESTING & 

### MONITORING BRANCH 

### INFORMATION REQUEST FORM (ST·2) FOR PROTOCOL/REPORT REvIEW
Rule # NSPS Sampling

or 40CFR60 location Permit Identify Cond.# Subpart



### Permit Exhaust stack



### Cond.f12 na t?-hr Identity any other Requirements

0 0 I

# I

0 0 I 

## !
0 0 I 

# I

0 0



### na

0 0 0 I (1) If allowable limit Is specified by rule or permit in mass flow rate only, please convert to approximate ppm levels and mark with an asterisk (-). 

### Page 3 of4Const ituents Allowabl e (l) to be**Umit~** Measured Conc. Mass (ppm ) Flow Rate Qb/ hr) [ 

### 1

[ 

### 1
[ 

### 1

( 

### 1

[ 

### 1

[ 

### 1

[ 

### 1

[ 

### 1

[ 

### 1

[ 

### 1 TECHNICAL SERVICES DIVISION SOURCE TESTING & 

### MONITORING BRANCH INFORMATIO N REQUEST FORM (ST·2) FOR PROTOCOL/REPORT REVIEW
Aule # 

### NSPS Sampl i ng

or 40CFR60 Location · Permit Identity Cond.# Subpart



### • 

# . Identity any other Requirements

(1) 11 allowab le limit is specified 

### by rule or permit In mass flow rate only, please convert to approximate ppm levels and mark with 

### an asterisk (*)
. 

### Page 4 of 4

### III Plati n g a nd Po li s hin g Process I nformatio n A

. Elect r oplatin g Tank s : Pl ease p rovi de th e in fo nn ation be low for eac h tank in w hi c h an e lec tro p lat in g fi ni sh con tain ing HAP li sted in Tab le I is ap p lied

. 

### ·DO NOT inelude chromium eleclroplatillg and anodizing ranks regula ted under 40 CFR 63, 

### subpart 

### N. TABLE 2. S UMMARY OF EL EC TROPL ATI N G TANK INFORMATION '

Ta n k Maxi m um Rec ti fie r Tlink Do ), ou 

### usc Fi n is h Ta n k surface ope r atin g op er atin g T ype of e m is sion cov er s on Ta nk Iype vo lu m e dim e ns io n s ampera ge hou r s bat h co ntrol 

### your

10' a ppli ed l (cal) (fl 

### x fI) ( a mps) (h r/yea r)**:I~ it** **atio ll** **J** mc th od 4 t a n ks ?5 

# "' Ni D · / NiD 260 4'x 3' 500 2,040 n O lle TKE Yes

# ~ bi Ni-} Nil 380 5.5'x 3 1.000 1, 550 AA TKE Yes Cd· I C d 450 6':c J' 1.000 800 Ed "otle 

### No 

# ..**~** A.g-I A J! 2 10 4'x 2.5' 360 880 /l Oll e none 

### No Ag-2 Ag 210 4'x 1.5' 360 640 IfOnc 1IOlle 

### No l/,f)
- I 

## MO /1.00 10' t 

### $' 1'5"00 20'10 

### Aff 

# t.'r'" e ,ho",'" 

### !Vo 

## #.0-2 N, P lZO· 

## . 5 ' / 0 • ;;-OLJ ZOYO 

### 04,4- flo

... .e N. 

## At,P

-J 

# Ii/ f) 1'2.oQ / 0 

# ,

. 5' 1 5 0 0 ZO'1 0 ,404 

# "

# .". ". 

# < #,D-t 

## 1I , D /2. 0 0 I )" 1**oo** 2o'-{o 

### A.+

## It**'' I1'''~**  Eo-< / 

# .. "'0 

# < (JI.<

.- / 

## 12" I '2."0 

## ' 

## -' l.d oD 0 20'70

### ~ 1 0 )( 

## >**jVor>J~** 

### n o",. 

# '" 

# tv.
-2 

# e", ' S' 20"'/.0 /20 0 / 0 • 2,0 0 0 ftJloJi!**IID"'~** 

# ".

# ~ t,,- 3 

# eLl { 1.0. / 0 ')(**~J** 20e o**z,,~o #J** **.~ f?** **"o,,~** 

# ,,0 

# 0**~**

! For example. i f you ope rat e three indu s trial nickel p lat ing tanks , you ca n numbe r them InNi I , InNi2 , and InNi3. For e.'(umple, Black nickel = BIN i ; Brass::: B s; Cadmium"" Cd; Coppe r = CUi Gold ::: Au; Lea d :: Pb; Nicke l. Dccomtivc
= N iD ; Nicke l. In dus tri a l '" N il ; Si lve r ::: Ag; Ti n/Lead = SnP b; Tin ·N ickc l :c: SoN i ; Zinc::: Zn ; ZinclNickei = ZnNi. DO NOT include c hr o millm electroplating and allodizillg tanks reg ll iat ed III/d e r 40 CFR 63, s ubpart N. J Please fill in: Ai r agi t ation = AA; Educlo r (pum p mixi ng) = Ed; Mecha nical mix in g ::: MM: No ag it :ltion z None; or Other (Specify) '" Other.**~** Only controls applied to each spec ific tank. for example: polypropy lene balls'" PB: wetting agent fume s uppre ssant = \VA FS; foam blanket '" FB: Merli n covcr '" Me; tank enclosure'" TKE. Do not inclu de contro l dev ices ins talled on the vent il atio n or e ;"( hau s t system. S Indica t e use ofcovers. If you rep lied Mer li n covcr (MC) or tank enclosure (TKE) above, indicate "yes" here also.

OMB 2186

.01 

### 7

### Please make blank copies of this table for use as work sheets and/or for additional room. 

### B. Electroless Plating Tanks: Please provide the following infonnation for each tank in which an electroless plating, anodizing or other finish containing HAP listed in Table I is applied.

.!! 

## t 

# a

, ..'.



# -<**~** 

# <**~'.**

### :~.**~.** 

# 0 

# >c TABLE 3. SUMMARY OF ELECTROLESS PLATING, ANODIZING, AND OTHER FINISHING TANK INFORMATION Finish Tank Tank surface Type of Tank type volume dimensions bath Tank emission

Inl appUed2 

### (gal) (ft x ft) agitation) control metboct ENi-l ENi 300 4'x3' air None ENi-2 EN; 300 4'x3' air MlST-E 

### Do you use covers on your tanks?! Yes No

I For exampJe. ifyou operate three electroJess nickel plating tanks, they could be numbered ENi I, ENi2, and ENi3. 2 For example; Alodine Treatment = Ad, Black Oxide = BIOx, Bright Dip = BrD, Cadmium Strip = CdStr, Chromate Conversion = ChCv; Electroless Nickel 

## =ENi; Lacquering = Lq, Magnesium Treatment = Mg, Sodium Dichromate Treat = NaDiCr, Sulfuric Acid Aluminum Anodize = SuAn, Sulfuric Acid Strip Anodize = SuStrAn. 3 Please fill in Air Agitation = AA, Eductor (pump mixing) = Ed, Mechanical Mixing = MM. or No Agitation = None. 4 Indicate only controls applied to each specific 

### tank. such as: polypropylene balls = PB; wetting agent fume suppressant = WAFS; foam blanket = FB; Merlin cover 

## =MC; tank enclosure 

## =TKE. Mist eliminators 

## =MIST-E. Do not include control devices installed on exhaust system. S Indicate use ofcovers. Ifyou replied Merlin cover (MC) or tank enclosure (TKE) above, indicate "yes" here also. 

### Please make blank copies of this table for use as work sheets and/or for additional room.

OMB2186.01 

### 8

# c. Thermal Spraying: Please provide the following information for each thermal or metal spraying operation in which any material 

### containing HAP listed in Table 1 is applied. 

### TABLE 4. SUMMARY OF INFORMATION ON THERMAL SPRAYING Is line operated Thermal Thermal in booth or Is 

### operation spraying spraying enclosure? Type of booth ventilated? line ID 1 

### process type2 

### (yes/no) or enclosure 3 

### (yes/no) 

# J FIS-J FIS Yes Partial No HVOF-J HVOF Yes Complete Yes

,'.

, .

. . . 

### .

.

### ~ ,**~",**



### ... 

# < 

# =;

" 

# =**~** 

# 0**~**

I

"

I For each thennal spraymg process lme, mdlcate the name or ID number. For example, flame spraying 

## =FIS; electric arc spraying 

### =EAS; plasma arc spraying 

### =PAS; high-velocity oxy-fuel 

### = HVOF; detonation gun 

### =DO; Other 

### =(specify). J Indicate if booth or enclosure is partial (i.e., open on one or more sides) or ifenclosure is complete (enclosed on all sides). 

### Please make blank copies o/this table/or use as work sheets and/or/or additional room.

OMB2186.01 9

### D. Finished ProductslMaterials: Please provide the following information for products or materials that have been plated, polished, or finished at your facility in the reporting year from Table 1. For each product, also indicate the base metal or base material that is finished and the ID number corresponding to the tanks from Tables 2 or 3, or thermal spraying operation from Table 4, that are used to finish the product. 

### Ifthe specific types of different products or materials are too numerous, you may use general descriptors of the products/materials.**~**

## ~**~**

# ~

# ~ 

# < 

# = ==**~**

# ~. TABLE 5. SUMMARY OF INFORMATION ON FINISHED MATERIALS, SUBSTRATES, AND PRODUCTS ID No's for tanks or General type of product or Base metal or thermal spraying substrate finished material lines Faucets, plumbin1!!1xlUres steel InNi-I,InNi-2 Pump housin1!s, blades, otherpump parts steel ENi-2, ENi-2 Light flXlUres steel, aluminum NiD-I, NiD-2 Tractorparts steel InNi-I,InNi-2 Machine rollers, military hardware steel Cd-I, Cd-2 Electrical connectors copper A1i!-I, A1!-2

## *~"./t: 

# r; 'Co 

## ,f,I"1t S 

## I!/ 

# I"".,,,**~"'"** Cu 1-7" 

## PI/) 1-"1

Please make blank copies of this table for use as work sheets and/or for additional room.

OMB 2186.01 10

### IV. HAP·Containing Plating and Polishing Material Data Please provide the following infonnation for each HAP-containing plating or polishing material used in the Reporting Year that is a source of HAP emissions reported in Table I. If records for the full Reporting Year are not readily available, provide HAP-containing material information for a typical quarter in the Reporting Year and check 0 that data are for one quarter of the Reporting Year. For each material, either submit speciated HAP content data from the Material Safety Data Sheet [MSDS] or provide the speciated HAP content in Columns. 4 and 5 of this table. DO NOT report chromium material data from chromium electroplating operations regulated under 

### 40 CFR 

### 63, subpart N. 

### Reporting Year:

### £oo~**~** 

# t**~**



# < E-c

# ~**~** 0 ;>4 Data are for Full Reporting Year: 

### 0 Data are for One Quarter**~** 

### (Check the BOX that is applicable) 

### TABLE 6. HAP·CONTAINING MATERIAL DATA Manufacturer Material name or supplier Amount HAP or lOt name used2 

### Units 3 

### (From Table 1) Nickel anodes Acme 2.150 Ibs nickel Nickel sulfate Acme 628 Ibs nickel Cadmium anodes Industrial Chem 2.8/0 Ibs cadmium compound Potassium silver cyanide Industrial Chem 246 Ibs cyanide compounds Potassium cyanide Industrial Chem 1.227 Ibs cyanide compounds 

## #u

..ltll**cJ.lo~.** 

## Je. If,les 

## IIfS- Its**IJ,ck~1** 

# ICo,"-"- S"lnk.**~,I~J** }200 

# ILs COl!Jd'

.....

, I 7

I Indicate the generic name, trade name, or product name for any material that contains one or more HAP. 2 Indicate the total amount used during the reporting year. 

### LinelD No's." InNi-l. InNl-2 ENi-2. ENi-2

Cd-I. Cd-2 Ag-I. Ag-2 Ag-I. Ag-2 

## #.1> (1-'1) CIA..
- (.1- 

### :1)

J For example, gallons (ga1), pounds (lbs). 4 Use the same ID No's for all plating and polishing tanks listed in Tables 2 & 3, and thermal spraying lines in Table 4. 

### Please make blank copies of this table for use as work sheets and/or for additional room..

OMB2186.0I 

### 11

### V. Ventilation System and Emission Control System Information A. Ventilation Systems: For each ventilation system that exhausts one or more ofthe tanks listed in Tables 2 or 3, or thermal spraying operation listed in Table 4, please provide the following infonnation, if available. 

### TABLE 7. LOCAL VENTILATION SYSTEM DESIGN AND OPERATING DATA Tank and Type of Ventilation thermal sprar Exhaust flow Exhaust duct Hood emission system 

## ml line ID No's. rate (acfm)3 diameter (int locations control6**~** V-I InNi-l,lnNi-2 6,600 18 side none

### ~ V-2 EN-2 3,000 9 centerline MPME

## ~ V-5 CD-2 4.500 12 side WS



# 11-1 AI, 

# ° CI-'1) 

## 7,**~()** C> 

## zll**UI1ljc,J,,~** 

## c'" (1-1)**~1',AlE"**

. -<**~ ~** 

, "

..

.- :: , 

# <.0, ,E-c



# < 

# =:,

'" : 

# =f, ;;J, 

# 0':,' 

# >

I Indicate the name or Identlficatlon number for each mdependent ventdatlon system. 2 List the ID No's. from Tables 2 and 3 for all tanks or the thermal spray line ill No's from Table 4 for aU tanks and thermal

. spraying operations that are exhausted by the ventilation system. ' 3 Indicate the exhaust flow rate through the entire system in units of actual cubic feet per minute. 4 Provide the diameter of the duct in inches at the inlet to the control device or at the exhaust point. S For ventilation systems that exhaust tanks, indicate ifthe tank exhaust hood is located on the centerlines or sides ofthe tanks. 6 Identify the type of emission control system installed on the ventilation system. For example, composite mesh pad = CMP; mesh pad mist eliminator 

### = MPME; packed bed scrubber 

### = PBS; high efficiency particulate air filter 

### = HEPA; wet scrubber (other than packed bed) = WS; chevron-blade mist eliminator 

## =CBME. 

### Please make blank copies of this table for use as work sheets and/or for additional room.

OMB 2186.01

. 

### 12

### B. Surfactant or Wetting Agent Fume Suppressant: For each tank listed in Tables 2 or 3 in which a foam blanket, surfactant or wetting agent fume suppressant, or combination foam blanket/surfactant or wetting agent is used, please provide the following infonnation and submit the MSDS for each surfactant or wetting agent used. TABLE 8. SURFACTANT OR WETTING AGENT FUME SUPPRESSANTS Annual cost Bath Surfactant Amount used of surfactant surface Tank or wetting Manufacturerl in reportin§ or wetting tension

IDI 

### agent name supplier year (units) agent ($) 

### (dynes/em)] NiI-l FS-250 Electrochem l4gallons $1,840 

### 45**~** 

# t NiI-2 FS-250 Electrochem l4 gallons $1,840 

### 45**~** AgCN-l No Foam Ind. Chem 8 gallons $160 NA

'. 

# <**~** ..

# ~.

. . 

# ==**~** 

# 0 

# >

I List the ID No's. from Tables 2 and 3 for all tanks in which the surfactant or wetting agent is used. 2 Indicate the amount used during the reporting year and units (e.g., gallons, pounds). 3 If you monitor or periodically measure the bath surface tension, indicate the surface tension in units of dynes per centimeter. 

### Please make blank copies of this table for use as work sheets antVor for additional room.

OMB 2186.01 

### 13

# lob
C. Air Pollution Control Devices (APCD): For each ventilation system listed in Table 7 that is exhausted to an emission or air pollution control device, please provide the following information TABLE 9. AIR POLLUTION CONTROL DEVICE (APCD) INFORMATION Control Basis for VentUation efficiency control system Inl APCDTypeZ (%)3 efficiency·**~** V-2 Sure Control. Inc.. meshpad mist elimin 90 Manufocturer**~**

## ~ V-5 Whirlwind. Inc.• wet scrubber 85 Per/lest

.. 

# V

.. 1 DlAc..I '/ t1\tS" 

## 'P,J ,.,.,s).**eh"",,,,,~.,,,** 

# 'I'." /'4

... f 1i-(1

# ~

# ~**.~.**

# ~

I Indicate the ventilation system ID No or name from Table 7. 2 List the. type of air pollution control device. For example. composite mesh pad 

## =CMP; mesh pad mist eliminator 

## = MPME; packed bed scrubber 

### = PBS; high efficiency particulate air filter 

### =HEPA; wet scrubber (other than packed bed) = WS; chevron-blade mist eliminator = CBME. l Indicate the control efficiency or percent reduction in percent. 4 Identify the basis for the control efficiency. For example, manufacturer's guarantee, performance test, other (please specify). 

### Please make blank copies of this table for use as work sheets and/or for additional room.

OMB 2186.01 

### 14

### VI. Pollution Prevention· A. Steps used to minimize drag-out%: 

# o Surfactants 

## ot Drip time 0 Air blow down 0 Other: B. Describe any other pollution prevention measures (e.g., drain board between tanks angled to drain dragout back to the previous bath) or housekeeping activities that reduce air or water pollution, or solid waste. done



### C. Provide costs and cost basis (e.g., cost of developing and implementing work practices or cost of substituting a non-HAP plating finish for a HAP-containing plating finish) ofwork practices or pollution prevention (P2) measures currently being used:**d<Jyt~**



### D. Provide costs and cost basis for P2 measures evaluated but not implemented and reason(s) why they were not implemented:

### ~ svJ,s.},

### I-.JI-~$**t;~ C~("QoMl"""**  Ih 

### fl..so 

### Ci-Cb.,.

... I-'JC**CJ.~4. LJ~<Jc.«**  .J'



### I

I Pollution prevention means any practice that reduces or eliminates the creation ofpollutants through increased efficiency in the use ofraw materials, energy, water, or other resources. Examples include substituting a hazardous material with a non-hazardous material, or a process change that eliminates the use ofa hazardous material. 2 Oragout refers to residual plating or finishing bath solution that remains on parts or workpieces after they are removed from the tank.

OMB 2186.01 

### 15OMB2186.01 

### Attachment I List of Most Common Hazardous Air Pollutants (HAPs) Reported Emitted from Plating and Polishing Facilities in SIC Code 3471

CAS Chemical Name Number 

### 7782505 Chlorine 

### 50000 Fonnaldehyde 

### 7647010 Hydrochloric acid 

### 7664393 Hydrogen Fluoride 

### 67561 Methanol 

### 7723140 Phosphorus 

### 108883 Toluene 

### 1330207 Xylenes Cadmium Compounds Cobalt Compounds Chromium Compounds Cyanide Compounds Glycol Ethers Lead Compounds Manganese Compounds Nickel Compounds

16

### Attachment 2 Complete List of Hazardous Air Pollutants (HAPs)
CAS No. Chemical Dame CAS No. Chemical name 75070 Acetaldehyde 106467 1,4-Dichlorobenzene(p) 60355 Acetamide 91941 3,3-Dichlorobenzidene 75058 Acetonitrile 111444 Dichloroethyl ether (Bis(2-chloroethyl)ether) 98862 Acetophenone 542756 1,3-Dichloropropene 53963 2-Acetylaminofluorine 62737 Dicblorvos 107028 Acrolein 111422 Diethanolamine 79061 Acrylamide 121697 N,N-Diethyl aniline (N,N-Dimethylaniline) 79107 Acrylic acid 64675 Dietbyl sulfate 107131 Acrylonitrile 119904 3,3-Dimethoxybenzidine 107051 Allyl chloride 60117 Dimethyl aminoazobenzene 92671 4-Aminobiphenyl 119937 3,3'-Dimethyl benzidine 62533 Aniline 79447 Dimethyl carbamoyl chloride 90040 o-Anisidine 57147 I,I-Dimethyl hydrazine 1332214 Asbestos 68122 Dimethyl formamide 71432 Benzene (including benzene from gasoline) 131113 Dimethyl phthalate 92875 Benzidine 77781 Dimethyl sulfate 98077 Benzotrichloride 534521 4,6-Dinitro-o-cresol, and salts 100447 Benzyl chloride 51285 2,4-Dinitrophenol 92524 Biphenyl 121142 2,4-Dinitrotoluene 117817 Bis(2-ethylhexyl)phthalate (DEHP) 123911 1,4-Dioxane (1,4-Diethyleneoxide) 542881 Bis( chloromethyl)ether 122667 1,2-Diphenylhydrazine 75252 Bromofonn 106898 Epichlorohydrin (I-Chloro106990 1,3-Butadiene 2,3-epoxypropane) 156627 Calcium cyanamide

. 106887 1,2-Epoxybutane 133062 Caplan 140885 Ethyl acrylate 63252 Carbaryl 100414 Ethyl benzene 75150 Carbon disulfide 51796 Ethyl carbamate (Urethane) 56235 Carbon tetrachloride 75003 Ethyl chloride (Chloroethane) 463581 Carbonyl sulfide 106934 Ethylene dibromide (Dibromoethane) 120809 Catechol 107062 Ethylene dichloride (I ,2-Dichloroethane) 133904 Chloramben 107211 Ethylene glycol 57749 Chlordane 151564 Ethylene imine (Aziridine) 7782505 Chlorine 75218 Ethylene oxide 79118 Chloroacetic acid 96457 Ethylene thiourea 532274 2-Chloroacetophenone 75343 Ethylidene dichloride (l, 1-Dichloroethane) 108907 Chlorobenzene 50000 Fonnaldehyde 510156 Chlorobenzilate 76448 Heptachlor 67663 Chlorofonn 118741 Hexachlorobenzene 107302 Chloromethyl methyl ether 87683 Hexachlorobutadiene 126998 Chloroprene 77474 Hexachlorocyclopentadiene 1319773 CresolsiCresylic acid (isomers and mixture) 67721 Hexachloroethane 95487 o-Cresol 822060 Hexamethylene-I,6-diisocyanate 108394 m-Cresol 680319 Hexamethylphosphoramide 106445 p-Cresol 110543 Hexane 98828 Cumene 302012 Hydrazine 94757 2,4-D, salts and esters 7647010 Hydrochloric acid 3547044 DDE 7664393 Hydrogen fluoride (Hydrofluoric acid) 334883 Diazomethane 123319 Hydroquinone 132649 Dibenzofurans 78591 Isophorone 96128 1.4-Dibromo-3-chloropropane 58899 Lindane (all isomers) 84742 Dibutylphthalate 108316 Maleic anhydride OMS 2186.01 

### 17CAS No. 67561 72435 74839 74873 71556 78933 60344 101688 101779 91203 98953 92933 100027 79469 684935 62759 59892 56382 82688 87865 108952 106503 75445 7803512 7723140 85449 1336363 1120714 57578 123386 114261 78875

OMB 2186.01 

### List of Hazardous Air Pollutants (continued) Chemical name Methanol Methoxychlor Methyl bromide (Bromomethane) Methyl chloride (Chloromethane) Methyl ch1orofonn (1,1 , I-Trichloroethane) Methyl ethyl ketone (2-Butanone) Methyl hydrazine Methylene diphenyl diisocyanate (MOl) 4,4'-Methylenedianiline Naphthalene Nitrobenzene 4-Nitrobiphenyl 4-Nitrophenol 2-Nitropropane N-Nitroso-N-methylurea N-Nitrosodimethylamine N-Nitrosomorpholine Parathion Pentachloronitrobenzene (Quintobenzene) Pentachlorophenol Phenol p-Phenylenediamine Phosgene Phosphine Phosphorus Phthalic anhydride Polychlorinated biphenyls (Aroclors) 1,3-Propane sultone beta-Propiolactone Propionaldehyde Propoxur (Baygon) Propylene dichloride (l,2-Dichloropropane)



### 18 CAS No. 74884 108101 624839 80626 1634044 101144 75092 75569 75558 91225 106514 100425 96093 1746016 79345 127184 7550450 108883 95807 584849 95534 8001352 120821 79005 79016 95954 88062 121448 1582098 540841 108054 593602 75014 75354 1330207 95476 108383 106423 Chemical name Methyl iodide (Iodomethane) Methyl isobutyl ketone (Hexone) Methyl isocyanate Methyl methacrylate Methyl tert butyl ether 4,4-Methylene bis(2-chloroaniline) Methylene chloride (Dichloromethane) Propylene oxide 1,2-Propylenimine (2-Methyl aziridine) Quinoline Quinone Styrene Styrene oxide 2,3,7,8-Tetrachlorodibenzo-p-dioxin 1,1,2,2-Tetrachloroethane Tetrachloroethylene (Perchloroethylene) Titanium tetrachloride Toluene 2,4-Toluene diamine 2,4-Toluene diisocyanate 0-Toluidine Toxaphene (chlorinated camphene) 1,2,4- Trichlorobenzene 1, I ,2-Trichloroethane Trichloroethylene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Triethylamine Trifluralin 2,2,4-Trimethylpentane Vinyl acetate Vinyl bromide Vinyl chloride Vinylidene chloride (l,I-Dichloroethylene) Xylenes (isomers and mixture) o-Xylenes m-Xylenes p-Xylenes

# [W]**~.&JmATIONAL** TECHNOLOGY CORPORATION 

### ANALYSIS RECauJEST AND CHAIN OF CUSTODY RECORD 

### * Reference Document Nu. 

# 334 

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# . . Special Instructions: 23 Possible Hazard Identification: 24 Sample Disposal: 25 

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### ..J Flammable -J Skin Irritant -J Poison B .-J Unknown**~** Return to Client '-J Disposal.by. Lab 

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### o 

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## o 

## o o 

## o o o o 

## o o 

## o List of Hazardous Air Pollutants (continued) Chemical name Antimony Compounds Arsenic Compounds (inorganic including arsine) Beryllium Compounds Cadmium Compounds Chromium Compounds Cobalt Compounds Coke Oven Emissions Cyanide Compounds' Glycol ethers

. Lead Compounds Manganese Compounds Mercury Compounds Fine mineral fibers 3 Nickel Compounds Polycylic Organic Matter" Radionuclides (including radon)! Selenium Compounds NOTE: For aU listings above which contain the word "compounds" and for glycol ethers, the following applies: Unless otherwise specified, these listings are defined as including any unique chemical substance that contains the named chemical (i.e., antimony, arsenic, etc.) as part of that chemical's infrastructure. 'X'CN where X = H' or any other group where a formal dissociation may occur. For example KCN or Ca(CN)2. 2Includes mono- and di-ethers of ethylene glycol, diethylene glycol, and triethylene glycol R-(OCH2CH2),,-OR' where n 

## = 1,2, or 3 R ::: alkyl or aryl groups R' 

## =R, H, or groups which, when removed, yield glycol ethers with the structure: R-(OCH2CH),,-OH. Polymers are excluded from the glycol category. 3lncludes mineral fiber emissions from facilities manufacturing or processing glass, rock, or slag fibers (or

other mineral derived fibers) of average diameter I micrometer or less. 4lncludes organic compounds with more than one benzene ring, and which have a boiling point greater than or

equal to 100°C. sA type ofatom which spontaneously undergoes radioactive decay.

OMB 2186.01 

### 19

### Marinshaw, Richard From: Sent: To: Marinshaw, Richard Friday, August 04, 2006 11 :47 AM 'ecrdarrel@aol.com' Subject: Plating and Polishing Survey Response for Anaheim Plating Darrel Lewis Anaheim Plating & Polishing, Inc. Mr. Lewis, 

### Page 1 of 1

The response to the survey for the Plating and Polishing Source Category from Anaheim Plating & Polishing. Inc., included an emission test report, dated March 29. 1993. In the appendices to the test report is a diagram of the sampling train used for the emission test. That diagram is marked "Confidential.· It appears to be a standard sampling train schematic of the kind you find in any emission test report. Can you tell us whether or not that diagram is really meant to be confidential? Thank you,
Rick Marinshaw Richard 

### J. Marinshaw. P.E. RTI International 3040 Cornwallis Road PO Box 12194 Research Triangle Park, NC 27709-2194 (919) 316-3735



### 8/412006• -0-

-


### Marlnshaw, Richard From: Ecrdarrel@aol.com Sent: Sunday, August 06,20062:58 PM To: Marinshaw, Richard Subject: Re: Plating and Polishing Survey Response for Anaheim Plating
Mr. Marinshaw No this document is not confidential, the Engineering Firm that did the test marked it Confidential, but this information has been given to several of the local administrating agencies and is not classified by Anaheim Plating & Polishing as confidential. Darrel Lewis Environmental Compliance, Anaheim Plating



### Sn12006