ATC LABORATORY RESULTS 

PARTICULATE MATTER 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 221 
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Client: Filter Treatment: Desiccate 2: 24 hours 

Location: Test Date: 

Fraction #1: Filter Catch (If other, indicate here ) 

Analyst(s) .Initials g/{ giL ~t<- {J ll;fl wKf 

Date '1.2-e.ro 0. tl.m 1. ~Lio B'/11ho &'hila 

Time o1ts'" I.>(J-71 iS"~t:> O'too It., o~ . 

Desiccator Temp. (68±lO"F) i-1 "ft 1-s IS.b 7~ 

Desiccator %RH (15±8% RH) I> 1) )<. i.J. d 

Room Temperature (68±10'F) 1-?..- ·:ro 1'.:' 15' 11 

Room %RH (2So/o-50% RH) '1B t.f'i 7'1 -:? . .f 31 

Run# j Filter# / Final Weight (U 4'" wt. doesn't confirm, use Initial Weight (U 4 .. wt. doesn't confirm, use Net ···--···--~------·--------··--·-..,.-------··· I ·-·------·--·,------~--- -~ .. ------T-----~~---·-- . ! I 'l'il...&\ i #1 I #2 i #3 I #4 #l #2 #3 #4 i Gain 

Blank 'J c\.-:~J 0- 3~:>'-\3 D ·wt~ ~-'- 1 kY::3 ,..-- ¥ 

Run#! ·3os("RJt 0-31. ?'-/ /J. %;.1 (). %S' .U D · 3 t.;fd l(o .. JC.:iA ['\ -· - Run#2 '1o~ (.1. )4#1 I@.J?v~ f> .. nS'i (.'). 31>#1~ -- ~ 

Run#3 ·1 ostf1l o .31.1-i D. pt.of:; f-{1. ~bdj ) I).Jf:H t>-'J?:S ~ -·· 

Initial Tore Weights transferred from Lab Book No. 126, page _k.8. Filter Media Type (Circle): ~) (Weights must agree within 0.0005 (5) grams-40CFR60, app A, Method 5, section U.2.l, July 2004} C/ 

Teflon Quartz Other 

ATC Fmm 124~version 53 September 2009 Page 115 of200 Lab Book 124-MS 
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if 

f"i ~ '1/li.J IO II Project No.:--'- fi<>JJ.Y ..f 

Fraction #2: Residue from Front Half Acetone Rinse (or other as indicated ) 

Analyst(s) Initials BtL f3JC. W}\f_ wiN wjl:.f 

Date 't~. jO 1,1. '21 '1/24 10 t:z/Zi hv <1/ ?.:?>!u 

Time o?Y: orr< t'i:JA1 rtr~ _,. ()ifiJJ 

Desiccator Temp. (68±10°F) '\h> dO !"" !:> - 7'1/6 75"-1 

Desiccator %RH (15±8% RH) ·-;r- i(... LS'" IS 15 

Room Tempcr~ture (68±10QF) 1-0 ?il ~~ 15' {)' 

Room %RU {25%-50% RH) 'f~ L{'-{ ~ "3 3 3-:J 

Run# Vol. Beaker Final Wei~ht {!f 4th wt. doesn't confirm, use a;verage) Initial Weight Qf..'!~ ~--~ocsn't confirm, use ave~L._ Net 

l~ ····---·-·-----· ··--····--·~---~-

--·--;~--T - #2 #3 I #4 #.! #2 1 #3 ! #4 

r------------

(mQ No. Gain 

Blank lv» ILl 'RfJ-iJP>' l?t) ' () 16-1\ Sc.t.b 11 (1 ~ i:;f. -;i f# ~@ -- "" -' iJ. i:o - p _,.o;·s 

Run#! t<t:J. l)l in i-t>N 5).)~>3 7~.nn. 73, 17:71'# l2_1- )?]'II - G= Run#2 'o"l) If/ 'f.I;[J};j 1'![6'!51 /"J,C'f-:ri V'17 ,, j:'j '·).{ ...... ' 77. CliJh - Run#3 

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ro;;. J$,1 l.t1.S?et &1.r:'!S:3 k:.t s:ns 1/~ 1, .. !:?51:. )t.,"iJ, 516 I - · Combined ;Fractions, . 

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·R.un# · NfitGain,.gnims ·Net'Gilfn-, Warns_ . . : ·, :Filler: Brank Acetone I Total 

Fraction #l Ffaction-#2 QA.only Correction* :.Piirti~Uiftte,. gra~s 

Run#! o .. ooo"? tJ ... oe45 ( _f)_ J2!1 r:i ~D 

Run#2 o ,oos;tf {! ~'fJ<Mr ( _A .. OO[} .11_ .. {)01) J 

Run#3 D . 002.1 /) . DM f" ( _fJ. oO!? /) .. 003{ 

*Determine correction by multiplying the blank residue by the ratio of blank volume to run volume. 

Volume of Acetone (or oilier) Blank It{? Maximum Allowable Residue (MAR), _________ _ 

Blank Acceptable? , . ,(MAR (g)= VoL (ml) x density (glml) x 0.001%) Acetone~0.788, Water =1.00, MeC/2~1.3255 

Beaker Tare Weights have been transferred from Lab Book 125, page '3 ~ 3 'I 

(Weights must agree within 0 .. 0005 (:5) gram>-40CFR60, app A, Method 5, section 11 .. 2 .. 1, July Z004} 

ATC Fomll24-version 5,3 Scptember2009 Page 116 of200 Lab Book 124-MS 
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Client: Project No. : Treatment: Desiccate::>: 24 hours 

Location: Test Date: Balance Used: 

Fraction #1: Filter Catch (If other, indicate here _______________ -.J 

Ana!yst(s) Initials II ~ ~IL }S!( wi.f wJ .. :f 

Datejj q .].-'J ,Ill P'i· w 't )o.w E/r/lil} gf,g/Jr. I I 

Time n-is- ~t">>1 . i <;'i v 01oo /boo 

Desiccator Temp. (68±10"F) ri 1-1 '11-) 1C6 "18 

Desiccator %RH (15±8% RH) 13> !? tl... j;;t II 

Room Temperature (68±10'F) ?-2-- '111 ?5 ·I> 1-'L. 

Room %llli (25%-50% RH) </'8 y'-f 3"\ 35 3J 

I Final Weight (If 4"' wt. doesn't confirm, use Initial Weight (If 4"' wt. doesn't confirm, use I Net . - ---~--~·~--~--------~- ."'..,.-------------- - -~·-r·-------- --_--~·---r--·---... ·------···-- 1 #1 ! #2 1 #3 I #4 #1 . . ! · 1 #3 i #4 1 Gain 

Blank P. ")~~} /). ·- r I 

Run#! ~~~~--

i:J.)&?'t> ~-----·~~~ 

().]l,.'~o 631.R- -- ,.... 

Run#2 II }o~111"->":t.-rl& .. 3t.?(u/G.j-t.--i:DI !IP-1f._fl~Y- 1r 

Run#3 11 J.oAill o.H&i &J.fb;~) Uo.3(:,'>""1,2_l ~P.J~Jtt o.J~Q-D - ,_ 

Initial 

{Weights 

Tare 

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Weights 

agree 

trsnsferred 

within 0.0005 

~kb {5) 

Book No. 126, page£. Filter Media Typ~:~h';i grams40CFR60, appA, MethodS, section 11.2.1, July 2004} ']C7...-:::.~ ... ; "/ 

Teflon Quartz Other 

ATC Form _l24:..version 5.3 September 2009 Page 117 of ZOO Lab Book 124-M5 
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L- u.""""w- I ....... Client: '13 "''1:-t\ '13-1 '-i"- If Souree: I 1~ ]!Test Date: I Cit/f0J/JjlProjectNo.: !f.-joj,;;>i.:f• -ll 

Fraction #2: Residne from Front Half Acetone Rinse (or other as indicated 

Ana!yst(s) Initials PJIL p; 

_) 

f[ w_X_1'_ 

Date tf, 2-f> 

~..;Xf. W}(./f" 

,/0 '1-t-'l 

"t/2.; '"' Time OrK t/1-6 

"'~ Ju };i) _qj_'t.3~ 

,y_:#V lo'$3 {J uo $" Desiccator Temp. (68±10'11) -:ro· ·. '":"ff; . -~(§ 7'/, 8 "'7i),9 

Desiccator %RH (15±8% Rll) !1- j/, iO' IS' !:5 Room Temperature (68±lO'F) "ff 1-v 7S ~~ _25" 

Room %RH (25%-50% lUl) {( l(\.{ '3;l 

Run# Vol. Beaker 

·'"'3 5 3-:} 

____ !!_~~!;. W':~.~!(If 4u' wt.I~-~~~~~~~.f!.!:~, use R_!~ra~g-~L- __ ,,,;;;~-~r t'r :: wt. ~~~~ c:firmT ·v~;-tL ~-:.~: _ 1--------- --,·~--·-- -------~ 

O,Ai-tl (ml) No. #l··; #2 #3' #4 ' 

Blank j()u I J.'j. ,.........., )jt;, "".? ! 'fi-fJ-1;1>;; ,r I) h. ~;.:rr - Run#l il'io 101 -~.'f>M ~it.- <{3'12-"' f.-7 b. 'l$/2 7t,. '11)1/ -· - Run#2 No !v'il (l -·?51ft ~,qqq:-r_ l'i, 'l.S t. '~7 '~· "s:s·.r -- --- Run#3 i<f() I!UA 7-1- (f'63 1'1-. tfl5>' r"7 --pq '31 i1,e<13• , - --- .. 

Combined Fractions 

I Riln# Net;Gain,;grarits . · ~et Gain,.,_grams ·Filter :ma:nk Acetorre 'rota! .. 

I Fi-.actiOn '#1 Fi-action:#2 . • QAonly Corr·ection* 

Run 

· Pnrtil:rilat<; grams 

Ill -:.(), ouv :r ('). odto {J _(1-'.00 ('iii _,Q. bD{.,"l.-

Run#2 -o oD/7..- o . oo'N ( ~-oolf> 

i~n#3 ~ 

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(J-{}(JO i &-DOZ-'-f (/1 {)-00~~ _d_,ooo~ 

*Determine correction by multiplying the blank residue by the ratio of blank volume 

Volume of Acetone (or other) Blank 

to run volume. 

Maximum Allowable Residue (.MAR)·------=------

Hlank Acceptable? ~::> . ,(MAR (g)= Vol. (ml) x density (g/ml) x 0.001%) Acel0ne=0.788, Wafer ~roo, MeCl2~1.3255 

Beaker Tare Weights have been transferred from Lab Book 125, page 1 - {Weights must agree within 0..0905 (;::) grarns4-0CFR60, app A, Metho S, section 11.2.1, .July 2004} 

ATC Fohn 124-version 5.3 Septcmber2009 Page 1 IS of200 

Lab Book 124-M5 
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ATC Air Laboratory 

GRAVIMETRIC ANALYSIS 

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Ciielllt! lSd(.i£. Source: Project No. : I f'-/IJI"l</ ~ o ::;" II Filter Treatment: Desiccate~ 24 hours 

Location: Test Date: Balance Used! I .Precisa 303A SIN 43108 !!Acetone Residue Treatment: Natural 

Fraction #1: Filter Catch (If other, indicate here ) 

Analyst(s} Initials t:t .. Bit.. P,ll.: F;i:.- lvH wll.P .!JJ.i /11f 

Date ~-2 i Jo '1·2-'1, I 0 "/ .. ;;~ -1 ~ /b. I . /1> ¥)nJJ, i h8ho t:./.1~ """"J}J!Jpt; 

Time o::ns o "f:>o 1'5'"'-{" "'?"-'-' O'Jc;,; Ho~ f .1 ,·.1 l..b..£f' 

Desiccator Temp. (68±10"F) ""}( 1-i ~s 1-..... 1S". 6 7.B_ '11. ~ 'l_t. ~ 

Desiccator %RH (15±8% RH) ,, 13 ll.. 1> f:l. Jl :J:l II& 

Room Temperature (68±Hl''F) 'r't-· -:to 1t;' {-7.. j.{ 77 {, " 'I ..,: .. 1')-3 

Room %RH (25%-50% RH} '-1113 '-{if 3"\ ,H 3~ ;;:. Jj '-/{ '{;) 

Run# i Filter#~ I 

Final Weight (lf 4" wt. doesn't confirm, use Initial Weight (If 4th wt. doesn't confirm, use Net -"------·-·---·+·-~·~------- ' -----.--------·--· -~····r--- -------·--- ·----------r-·-·-·--·--, ----- I Pr;;- 11./~r , #1 i #2 #3 I #4 #1 #2 #3 i #4 Gain 

Blank 3o~co fi. 3/..<i"?. p . .:Jt.?'/). fl. ;JJ.:f_J - - Run#l ) C/,., l 

Rnn#2 

ll>, ·-q-2.-q-1{312)) p. JH1 IG:J~.U) - - 1o66 e;. ·wu. k }ht""i) - t>. :1 $'13 ~>fJ., _ ... .-

~ Run#3 QSr1 p- }jcj $ &- H% .J.3u't o .. )it<l'· ,.. .. ~ {), 1ui:l c. ~.1cM lL .... .,. }..;:, i!\1'\,)J..$ .. 

Initial Tare Weights transferred from Lab Book No. 126, page /..,!), .bd Filter Media Type (Circle): pnr:ss F_ib::) (Weigbls must agree within 0.0005 (5) grams-40CFR60, ap;A:;l!etbod 5, section 11.2.1, July 2004) ~ Teflon ¢$Other 

A TC Fonn J 24~version 5.3 September 2009 Page 119 of200 Lnb Book J24~M5 

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Fraction #2: Residue from Front Half Acetone Rinse (or other as indicated __________ _, 

• Hnitials II f.;K...- / fj IL 

Date~ i 11 ,'(~ I ''J.. 2.') tJ 

Time\\ cBs I n'h( 

Desiccator Temp. "fv I ~o ...... ~ " I ' 

r %RR (15±8% RHJII 11' _L p,. 16' 

RoomT, t> u.s.+ln-~nn {il I fp j;) ' -~ 

"3'3 ]. "1-

Room %RH -·~-----~ 

• Rfllll y:fm I n '-f'1 

Gain #3 

(!•.~v:•g_•LII_l_ll!;;l'Y.!'_ii~(lf_~wt. _<ll~~'t_<!firm, use ~-~;~~~~ __ y_ol: __ pe_a_~<_e_r ___ , __ Ei.~_IY'(~~~ht (If_<£~'!!: 

~~~ ... ~11(11 ;~~ I~ 1--- -I - _ L ___ li?o.:c~~JCw u4 3-i:l&b. D~1j 

Net 

#1 #2 114 

'1--

\Run#l \\ (D1.1\\ ll9 llbf-•l§bz.t'{;;:?-:~J I . _ ~1',3S"LkJ>~:f.q~,~· -~ .~ 

Run#2 1)\,; ~1-'{, { ~ - J 

·*/RlUI#3 .' 0 ~71-H& _ _ . 

Rtin:t# 

II Run#! 

Ho,,., -U'? 

!\Run #3 

Net. Gain; -~rams 

Fraction #1 

/} .. nhUl 

tJ . crntt 

01. Ot>1>~ 

Combined F----"'-'· 

NetcG9.in~·gnms I FilterJ}limk 

FractiOn #2 QA- only 

Acetone 

Correction* 

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D ·· 00<-i.r --~_.@l} 

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* Determine correction by multiplying tJi.e iJimikresidue by ~ratio OJ to run volume. 

Total 

Particulate, grams 

.11: QQi\ 

o.od7.-

D .oc£2.. 

Volume of Acetone (or other) Blank Maximum Allowable Residue (MAR), __________ _ 

Blank Acceptable? '"7~ .(1\'fAR (g)~ Vol. (ml) X density (glml) x 0.001%) Acetone~0.788, Water =1.00, MeC/2=13255 

Beaker Tare Weights have been transferred from Lab Book 125, page ::1;? ":f 

{Weights must agree witliin 0.0005 (:9 grams-40CFR60, app A, Metho 5, section ll.2.1, July 2004) 

ATC Fmm 124-version 5.3 Septembcr2009 Page 120 of200 Lab Book 124-MS 

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GRA VIMETJUC 

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f Client:. f 1<. .... . nA.. \ ·1<....-'f. .• •~ /{_ ~~ i AJ Proiect No. : /J..,..Joj ~ IJ.,. riJ .f. Filter Treatment: 

Location: Test Date: () Balance Used; I Precisa303ASIN43108 II Acetone 

[ Fraction #1: Filter Catch (If other, indicate here ) I 

Ana!yst(s) Initials ~-- t.> /t_. !)II- WKf vVk-f 

Date llH'5_1 II &i- fi .10 '1- 3" f 11111• gj,~ it~ 

Time o11> . t;,()o IS"'-i o D"'uu i b 0'-" 

Desiccator Temp. (68±1 O'F) +-\ '7i 1(' l§ .~. H 

Desiccator %RH (15±8% RH) n ;? . 1'- i,;). II 

Room Temperature (68±10"F) rZ :ro 15 ·-,5' 'r!:~/111 Room %RH (25%-50% RH) q~ '-1'-\ )'1 '"35" :Jl 

,_ -~~~:. .. t--O:!fi:J-- ·)--;;·~~rg~~~f 4'~f ~~;;'t corrm, ;;-~1·---_l~i~~-~W~ig~-;~~~~t:~d~:~~Oll~~!-;;.-~- :~:- _ 

Blank s,;, tn o II b - ~~<11:> {), J't.YJJ f).:JI,'f ;1 I - """ 

Run#l 

'·-·· .····~ 

"}~\:,;I J 0.~72-::_lf'. $~d?~3kl&. ' .• ·~. -""' I ~·~. J!!~ J ~It.. "''· 3 !.:1 'l 'I ·-· /" 

Run#2 3o"> I! o.'3t,zk.;n,~'c.\ {).:Jt.n-1(.;.). nli:4..1) - ··-· 

Run#3 )obfll o-3&40 \.<>. ~~>>i- ~Jell> iii[ t.\J't.'tJU) -

Initial Tare Weights transferred from Lab Book No. 126, page b fJ. FilterMedia Type ~c·· (Circle lass Fi~er ·, 

{Weights most agree within 0.0005 (!;) grams-40CFR60, app A, Method 5, section 11.2.1, July 2004} _ 

Teflon Quartz Other 

ATC .Fonn l24~version 5.3 September 2009 Page 12l of200 lab Book. 124-MS 
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I Client: I B"':1Jl "/JriU(., I/ source: I&_-/ J;J II Test Date: I 'I ln/1 J II Project No. : /""-NJ:J. 1'5 

Fraction #2: Residue from Front Half Acetone Rinse (or other as indicated ) 

Analyst(s) Initials P-1- HIL &!C g({_ u!Lf Wf..f i_,,J f.,f 

Date b9t2& -1~ o''! . l-'i ' l\7 I q ->a-'" lb. 1.1.:> "'{Uill~ cl['l-1 \I~ rtl2 Jli;,: 

Time al1< O'HS i ·0."'-1" 01'1. i) )1-g~ ! s::."'tl o t; o'i5 Se ~'- Lh13 p. ~~ 

Desiccator Temp. (68±lO'F) '(V .-;w 1o ··H ... .1 ..... :::. J '1.8 15';.; fv~ ,..·n;vo..t. ~ 

Desiccator %RH (15±8% RH) cr ilr r:r l'> ts- {~ '_..... [:;) Du "'"........,. M.., 

Room Temperature {68±10°~'} 11) ''.)v 43-o -rt.. "1..) I.? 1.1"' c.;.! if\.,~~· ?, 

Room %RH (25%~50%· lUJ) eft '-{'-{ '17 '{) "3J.. '")') '), 1 / j( 

Run# Vol. Beaker Final Weight (lf 4tb wt. doesn't confirm, use average) 1-!~it~"{_'\Y(lift:.(lf 4'" wt. do"!'.":t.~•n!'"::lll•-"'" ~~i-r--· Ne~---- ---·=- _______ .__ ·---------------·---- -.---~----·---------·---1-- ---·-----.--------·-·--.. ····------

~ (ml) No. #l ! #2 i #3 I #4 #1 #2 i #3 #4 i Gain ' ' 

Blank lee il~ !$tl. ~\,3 I eO~H \ 1 "./) i,:J'\1 . -It/ 

Run#! /00 l£,.1-' 51·m~>"1 5':&__~) Jld "i7.7il'-f'll ~·J_ n~~ 1's7:7rl't-:i >S7:nff.Y 

lvo lo'J t:f5.~S'b\. Run#2 - ~~, -:.r.i. "f(.¥6) IS>r:H'f. Cns.v.<w :::> . " 6 ·- - Run#3 f.•O 5) fll;} Is-vas;, '$--'ZA lH1 1/f;.<, '11'i ~J $~';;.. 'If,' .\> ' 

Combined Frictions· ...... 

Run# Ne't Gairi~ grams . Net: Gain.; grams Fllter Blank Acetone Tot.• I 

. Ftaction·#l FractiOn #2 QAonly Correction"' Pnrtictita~.grams 

Run#! - o.dfufi ().(})(;/'}.... ~· n- w·:<, ti 

Run#2 6. 0()()<( t'J • tll.! <--> tt 0 · Doi; 't~·-001'{ 

Run#3 -o-ooiv 0 • 00 1-c:r {/1 ()-O~>i? i) • (]Ill) ,_j -- ------- • Determine correction by multiplying the blank residue by tire ratio of blank volume to run volume. 

Volwne of Acetone (or other) Blank Maximum Allowable Residue (MAR); __________ _ 

Blank Acceptable? • ..,..--, T~(M.I)g-,(g) =VoL (ml) x density (g/ml) x 0.001%) Acetone~0.788. Water ~1.00, MeC/2~1.3255 

Beaker Tare Weights have been transferred ftom Lab Book 125, page "~ ,.,., i J'i' 

(Weights must agree within 0.0005(.:9 grams40CFR60, app A, Metbod 5, section 1 1.2.1, July 2004) 

ATC Fonn 124-version 5.3 September 2009 Page 122 of200 Lab Book 124-M5 

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ATC Air Laboratory 

ANALYSIS 

Client: 

Location: Test Date: 

Precisa303ASIN43108 fiACetone 

----·····----- -

Fraction #1: Filter Catch (If other, indicate here ) 

Analyst(s) Initials FJrt- f3 iL !f;,ILDate lif·t'if;w rJt§;/.rv I q!{;:§fo.i" 

Time /;7(:; n-5o f!)•{o 

Desiccator Temp. (68±10"F) '} \ ·r! .:r<; 

Desiccator %RH (15±8% RH) ! ~ 1 ·~ 12-. 

Room Temperature (68±10"F) 1 ?..-- _]-Q_ ':J<; 

Room %RH (25%-50% Jill) l{ f) i.f'-1 3 "\ 

Ron# ! Filter# i Final Weight (If 4'" wt doesn't confirm, use Initial Weight (If 4"' wt. doesn't confirm, use Net ---------··r· ---------- --------i·-------,--------1---------;------·------- ----------.-----------------T-·-·----·--r--------,--------.-

1 ifrj i./i..;'-1!~ i #.! 1 #2 i 113 1 #4 #l I #2 1 #3 I #4 · Gam 

Blank ') · JH,o t<~v 1{'$ 

Run#l ')-- S&<~l D~~t(f1& :;;;_?%'-/) IIi. fiS·:~.- bj}'tr<-(~oV • 

Run#2 5·- )a•"-f o. {':fill-- D· rfo'ff ;:'3~ n.':>!.-.71 D~bZ-V · Run #3 ') • ,_,-., p , )'?fl~ ~b. -~::,--~ o . ).!;,')'{ II 0 ?3~,;51) -· _1_ ---- - ----···-------·-----t~~--~-- -----··-------- ------------ -~-----··----·· --------- ---·-------

fnitial 

(Weights 

Tare 

must 

Weights 

agne 

transferred 

within 0.0005 

from Lab Book No. 126, page __ . Filter Media Type (Circle): Glass Fiber Teflon Quartz Other 

(:9 grams-40CFR60, app A, Method 5, section 11.2.l,July2004) 

ATC Fonn 124~version 5.3 September 2009 Page 123 of200 Lab Book 124-MS 
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Fraction #2: Residue fr!?!}l Front Half Acetone Rinse (or other as indicated j 

Analyst(s) Initials tJii. Us • I W tft 2'llg( Lv)Uf '...J}Vj W)Vr Lvl'-f 

Date nr1? · o 1--ts" "i lniJo •lll'""lli, <tl&t-;JJ. 0 _qj"t-d I o 

Time 1-o ~ti.? j oSS1u rcrl5 i<f~ t.n:t 

Desiccator Temp. (68±l0°F) !'1- I~ I "' ;5').( .::1_1 (,:( ' '] ...j, s 

Desiccator %lUI (15±8% RH) l-il 1-o ! j.) IY 15' 15' :.f:r .- I 

lS"' (5 lS -·u: Room l~empcrature (68±l0t.F} y'-1 i 

Uoom %RH (25%-50% RH) W' ~ >£" -:3')- ""3) T3 

ERun_LI Vol. Beaker '-Final \\'~rH!fj"'.:IV.~.;'!...es"'' confir_'!'•r"'~!'!.•!:~&"L .. !~~·~ wl~W :; wt:_!!_oesn't •:;firm,_r-~!!:~~L-+-· :.~: ----------------

(ml) No. #! #2 I 113 ! 114 

Blank lou {/;). 

Run#! /IJO -;:y· :r I) .. f?rrl. 9;>. 51-f;i.':'> . ~~ .. S1iJi$ {.'v. ,;.·Jo ,;'.;; Jil:' '5'1) .to 'HS 

Run#2 lo1J $~ "io.?i1~ in>' 113'f? £'~;>, "") no £~. 7i~ \2: "'' l 11~ l)~·o, "J n; .?6 f.. 

Run /13 · iff/::J hv sP .1lt; '.{-: 51'> ,'')-::c:-r .L :SD 7~:d!!J ~.1i."f'O .::>/). /lc!J) l $.1.1' ]i.f'~ I"" r~ 

Combined.F.ractions. ·i-

,R,ndt Net Gain;-~rams Net-Gain; grams Filter Blank Ac::etooe 'l'otai 

Fra-ction #1 F ... ction#2 QA only Correction* Pa.rticu~a~ grams 

' Run#J &-01'53 t'J •. 03< I d) e ood o .oq< 

Run#2 (j.of[.$ 11. on .. <: I! o.wi3> i! •.. ~ 

D·i,?l,!_ .... If; o-OOt?. li . o·l.A Rnn#3 f) .. en "2-S 

• Determine correction by multiplying the blank residue by the ratio of blank volume to run volume. 

Volume of Acetone (or other) Blank Maximum Allowable Residue (MAR)'-------'---

Beaker 

Blank Acceptable? ~--'JJMAR (g)= VoL (ml) X densily (g/ml) X 0.00!%) Acetone=0.788, Water ~1.00, MeC/2=1.3255 

Tare Weights have been u-ansferred from Lab Book 125, page c: . (Weights must agree within 0.0005 (:9 grams-40CJ1R60, app A, Metho 5, sc<tion U.2.l, July 2004) 

ATC 

. 

Form 124-version 5.3 Septcmber2009 Page 124 of200 Lab Book 124-M$ 
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ATC Air Laboratory 

GRAVIMETRIC ANALYSIS 

Project No. : 

~ fb-bvJ-Itr 

Filter Treatment Desiccate 2:. 24 hours 

Lvcation; S~!. oL 'fest Date: Balance Used: Precisa 303A SIN 43108 AcetQ:ne Residue Treatment: Natural 

Fraction #1: Filter Catch (If other, indicate here __ ) 

Analyst(s) Initial• II '/?,if-. gfl ~t.-

Date /I "J.V{>. 1 11 q,_,! 0 (3>·1• 

Time! t/}i5' 1j{5 iS'"'" 

Desiccator Temp. (68±10'F) '7f{ Jf~t I ·'fiS 

Desiccator %RH (15±8% RH) (!:. lt. If~ 

Room Temperature (68±Hl"F) {1. 1-0 15' 

Room %RH (25%-50% RH} r~£ '-1 't ;,., 

--~_"~_.'l __ j ' ' __ ~~lter. # ___ J ___ Fin~i Wei~t (lf 4"' ~ do~n't ~!'rm, use 1~ _ _!11~~1 W~!'_t (f_f_~"'.'V~-~{)"'.()'_t:_o."_li_.·~~~~-"."_ __ L '__ Net _ 

I ' I I ' ' I I i Ou+-·\e. r I #I I #2 i #3 : #4 #l i #2 I #3 l #4 . l Gain 

l3lani< <)- ~ci.-0 /)' -"7&•1 ?> ~-~ ~i}. ).f., . . ' ··••·· ~,.," I I 

Run#] s: " ~thi"- b3&;'2-;;~ I lif).%5'i..dj)-.·:~JI I 

Run#2 5 ·· ')cJVU o.~~sttllo.~o?-~;:~~o) ') ............ ::.::. ... --·-- '1-

v.'?>l·l% (I ,.<:::mt ./ 

Run113__j ~ .. )O()'t.j /)· '3£;~®~~-0~--- ·- () . i, to 51:(1 {J . -; if><;') 

" 

Initial Tare Weights transferred from Lab Book No. 126., page __ . Filter Media Type (Circle): Glass Fiber Teflon Quartz Other 

{Weights must agree within 0.0005 (::;;) grams-40CFR60, app A, Method 5, section li.Z.l, J•ly 2004) 

ATC Ponn l24~version 5.3 September 2009 Page 125 of200 Lab Book !24-M5 
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tG 1;./ IITest Date: I '1/ tl/lllljProjeetNo.: I 

Fraction #2: Residue from Front Half Acetone Rinse (or other :as indicated _) 

AnaJystfsJ Initials . 11 .. \L .. ~ l'tt<.. tH£. w lGlf 'W)'Vf wJVI vll:E_ 

Date j)_'j.'\\ • m 1!-l, ~~ 1-i~ ... lC,~~tC qfhh 'tlt11J \ '-f t U;IJ.> q/z,j Jio !I ·1 

Time v'l-~t; 1)"}1~ iN~ Ofl," 0$! D Ins: i 'f,).'.\) t_il_o 

Desiccator Temp. (68±10"1') }'> fll ?() "}-).. "1~8 -~., 7) ~!J 

Desictator %RH (15±8"/o. RH) !'1· lit? i:.r !? j s:· l'f 1r }'(' 

Room Temperature (68±10uF) '1"" ""ro '}o }1. If 1!" !) -IS' 

Room %lUi (25%-50% RH) ''-;)- '-\, '-~"i U) '-i'J ":. 5''" '"3;. 'J).. "JJ 

1--~'-'~-#-1 Voi. Beaker .Final Weight (If 4t1

' -wt. doesn't confirm, use av-etage) ____ }~-~!i.l!! w~! ht Qi£~ .. ~?~~-~E:.!_~~:mfirm,~r-~!~~~g~---! -~-- Net --·····-·- ·-·--··------··--- ··-----~,----··-··-·-· -------------· -·----~-

(ml) No, #li #2 #3 114 #1 #2 I #3 i #4, Gain 

Blank Jrro 1/'J. ~i,;lt.,')J (.l(-'ll 011' 'H j)~ Ci.:$.;1 -- Run#l /flO b$ f)_ ~i>Cfl 9-if?t.< lt,1-. "/'J.v- ~ "?'( l.f\1-l'i......., 'i /. '16-f " :ti-WtJ;. ..... ).'{~[1 •j '1;'1 'i'f,"' {, 

Run#2 I/CiD '1""' ;J 'I ~"'1- 8'.1:% l5'1·'5"1'ltl_) $1, S'l;J.'" £"~.\n (J ~ :;;t~.n I 'I '> 'f .,n li; 

Run !13 /t).} . 71 l$'1. I b&-2-- :,"i. /.t p_ >1- rJoz..( : :r:.-1./J,q-:[1 :s.'1./<d" $%) ./ 1.1.$" 1?-i.ll.'l.'i.. S'<J, I !>:I' 

Combined .Fractions 

Run# NetGain;··g:tams Net 'Giiin;:-:grams li'ilter Blnnk Acetone Total 

Fraction .#1 Ffaction #2 QAonly Correction* ·particulate:,. grams 

- ()·1;100 s JJ.Jt.'O?f! d; fi L'l{) i ~ I!- OCJi /,- i 

Run #1 

Run#2 - {).(J/I)i /) . «X?'i ~ CH)D!) - o · voo·..f 

Run#3 <"'" t) .I!}IJ~i 0 t: . z:z ,. l?Q ·:::> f; 0-0UI} /) • ""' i 0 - • Determine c01nction by multiplying the blank residue by the ratio of blank volume to run volume. 

Volume of Acetone (or other) Blank Maximum Allowable Residue (MAR)•-----------

Biank Acceptable?_ """:l.r:l .,(MAR (g)= Vol. (ml) X density (g/ml) X 0.001%) Acetone~0.788, Water ~I.OO, MeCI2-I,3&5S 

Beaker Tare Weights have been transferred from Lab Book 125, page -="'~+4"'- .1' 

{Weights must agree within 0.0005 (:5) grams40CFR60, app A, Method 5, section 11.2.1, July 2004) 

ATC Form 124-vcrsion 5.3 September 2009 Page 126 of200 Lab Book .124-M5 

- - - - - lllillll>1 

- - - - - - -·- - - l<!!i'iR Ill 
...., 

 'RiferUl~ i/J/1 - !_..., -- ~ r Exposed Fflter 

! 1"'v~ FH Acetone Rinse 

Run 1 FH CFA -100 ml fPMl 

FH Acetone Rinse 

Run 2 FH CFA -100 ml (PMl 

I 

' FH Acetone Rinse I 

Run 3 FH ' CFA -100 ml (PM) ! 

I 

"?.. 

fLJII 

R<!llllent lll"''k .-"' ...... " ' ~~ ~lfifi!Tl\1 r one 

- ~ "\ 

REL IS OBY , DATE RECE.1Vt'06Y DAtE T>IE ~//'[ --}-4 ]I 1(/{.,t- 'flo/ /!D !/Oft Jqt., I l~>: :;$>:> 

{." NOOT~Y DATE TIME RECEIVED BY DATE TlME I 

FIELD REMARKS: CF A: CLEAN Fl~l,D AREA 

NOTE: PLEASE MARK LIQUID LEVEL ON ALL SAMPLE BOTILES WITH GREASE PENCIL. 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAS PERSONNEL 

FORMNo.AiC 1 

C:'l8ora! !CR\COCs\MS COC\Piant 51n!e1 • M5 

Var 1.0 29 August 2003 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 234 
~ 

'~Blank ""\. I ..--T ~ILTER#_____-~ Ex 

! 

J 

! FH Acetone Rinse 

Run ' 1 FH ! CFA -100 mL (PM\ 

I FH Acetone Rinse Run 2 FH CFA -100ml (PM\ I 

I FH Acetone Rlnse 

Run 3 FH i CFA -100 ml !PM\ 

i 

Rli-ao~ 

--t--"--

-~ 

C--~ ' 1011fiffilnk 

,-----· 

UNQUI BY DATE. TIME RECEIV BY PATE TIME 

':Y1 

c&>L-/1~{ yq • v I 04.> 1.1!.-M. l'tli'f I lo_lv REUNQUISHEO BY 

FIELD REMARKS: 

NOTE: 

FORM No. AT¢ 1 

DATE TIME RECEIVEOSY DAE TIME 

I 

CFA: CLEAN FJELD AREA 

PLEASE MARK LIQUID LE:.VEL ON ALL SAMPLE BOTTLES VVHH GREASE PENCIL 

SEAL TIGHTLY AND RE-CHECK UPON DELIVERY TO LAB PERSONNEL 

C:\Boral !CR\COC'::1M5 COC\Piam S 0!11~( • M5 

~( / -( 

fV 

A~ 

-· < 

Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PlANTS 4 & 5, SALISBURY PlANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 235 
/ 

Filter Blank I CFA FILTER# 3o(,O Exposed Filter 

' 

I 

I FH Acetone Rlnse 

Run 1 FH I CFA ~100 mL {PM) 

j FH Acetone Rinse Run 2 FH ' CFA ~100 ml iPMl i FH Acetone Rinse 

Run 3FH ' CFA -100 rnL (PM) 

I 

Reaaent Blank '~ I CFA -100 ml Acetone Blank 

// .""' 

' eoav "'n' T!ME RECSVS)6Y DATE TIME f?Vi L /[ J'·L,J Jo3b.A itlJ- '1U11 {tJ: 'j:J 

Et!NOUI$HEO BY DATE T!ME RECfJI/ED6Y DATE TIME 

I 

FIELD REMARKS: CFA: CLEAN FIELD AREA 

NOTE: PlEASE MARK UQU!D LEVEL ON ALL SAMPLE BOTTLES WITH GREASE PENCIL. 

SEAl TIGHTlY AND RE¥CHECK UPON DELIVERY TO LAB PERSONNEL. 

f'ORM "~*' ATC 1 

C:\BotaJ lCRICOC'siMS COC\Plan{ 4 Inlet· M5 

ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUST A PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 236 
/ 

, 

1"- --cFA rxoos.d"F? · 

! r 

i FH Acetone Rinse Run 1 FH CFA -100 mL I PM\ 

! FH Acetone Rinse ' Run 2 FH I CFA -100 ml I PM\ 

!. FH Acetone Rinse 

Run 3 FH i CFA -100 mL (PM) 

I 

_/ 

lank ' --c=- .->1-99-ml::"'"" Ace'fl.ne 

I 

.,;.'<' 

----------!--""· 

E DBY DATE RECeiVED BY DATE TIME 

I Cl)f1,/D 1107{1 41141 I&}" 

EUNOUISHED BY 

FlELD REMARKS: NOTE: 

FORM N¢, ATC 1 

DATE TIME RECEIVED BY n; TIME 

T 

CFA: CLEAN FIELD AREA 

PLEASE MARK UOU!D LEVEL ON ALL SAMPLE BOTTLES WITH GREASE PENCIL 

SEAL TIGHTLY ANO RE..CHECK UPON DELIVERY TO LAB PERSONNEL 

I.Y' P':. 

f/ 

Ver 1.0 29 August 2003 

ATC PROJECT No. P-10142 EPA ICR EMISSION TEST PROJECT 

AUGUSTA PLANTS 4 & 5, SALISBURY PLANT 6 

SEPTEMBER 2010 

APPENDIX PAGE No. 237