CLEAN SITES 


Environmental Services, Inc. 

April 21 , 2009 

Mr. Ron Davis 

Remedial Project Manager 

U.S. Environmental Protection Agency 

Region III 

1650 Arch Street 

Philadelphia, PA 19103 

Subject: 2009 Monitoring Report 

Coker's Landfills 

Cheswold, Delaware 

Dear Mr. Davis: 

Clean Sites Environmental Services, Inc. (Clean Sites) hereby submits this monitoring report at the 

request ofEPA in conjunction with their on-going five-year review for the site. EPA Headquarters 

has requested that we also conduct monitoring events to coincide with future five-year reviews. This 

report includes a summary of the field and laboratory test results from the monitoring event 

conducted on March 21 and March 22, 2009. In addition, it was prepared in accordance with the 

Consent Decree and Part 4.C of the March 1993 Remedial Design submittal. 

Groundwater Sampling 

Prior to groundwater sampling, each ofthe wells to be sampled was inspected and the depth to water 

level was recorded. The water levels were used to calculate the well purge volumes and to create 

groundwater contour maps as detailed below. The wells were purged using a submersible pump and 

disposable poly-flow tubing. 

Groundwater samples were either collected using a submersible pump (decontaminated between 

wells) or disposable bailers if a well went dry while being purged. All Groundwater samples were 

sent to Test America in Pittsburgh, Pennsylvania for analysis. Groundwater samples for Coker's 1 

were analyzed for styrene, ethyl benzene, and total organic carbon (TOC). Groundwater samples for 

Coker's 2 were also sent to Test America and analyzed for styrene, ethylbenzene, 1,2,3­

trichloropropane, , total phenolics, total antimony, and TOC. Field measurements of pH, specific 

conductance, and temperature were recorded for each well. A trip blank accompanied the sample 

coolers and a rinse blank was collected from the submersible pump to verify it was being thoroughly 

decontaminated between wells. 

Surface Water and Sediment Sampling 

Surface water samples were collected from Willis Branch adjacent to Coker's 1 in accordance with 

the approved sampling plans. Sampling was conducted from downstream to upstream, with surface 

CLEAN SITES ENVIRONMENTAL SERVICES . INC . • 46161 WESTLAKE DRIVE, SUITE 230·B • POTOMAC FALLS, VIRGINIA 20165 

TEL : (703) 519·2140 • FAX: (703) 519-2141 0 
water samples being collected prior to sediment samples at each location. Samples were collected at 

the center of the stream using a pole sampler. Sediment samples were collected from likely 

depositional areas using decontaminated stainless steel scoops. Sediment samples were collected 

from the sediment bed surface to a maximum depth of 6 inches. 

Surface water and sediment sanlples were also sent to Test Alnerica and analyzed for styrene, 

ethyl benzene, total xylenes, and TOC. Field measurenlents of pH, temperature, specific 

conductance, and dissolved oxygen were recorded for the surface water samples. In addition, 

Froehling & Robertson in Dulles Virginia performed the grain size analysis on the sediment samples. 

Sampling Results 

Sampling locations for Coker's 1 and 2 are shown on Figures 1 and 2. Estimated groundwater 

contours for each landfill are also presented on the figures. These contours have been created using 

the March 21, 2009 water level data. A summary ofthe water elevation data is provided on Table 1. 

A summary of the groundwater analytical results and field measurements for both landfills is 

provided on Table 2. The surface water and sediment sampling information is provided on Table 3. 

The analytical results are provided in Appendix A. The results of the grain size analysis will be 

submitted under separate cover. 

No constituents were detected above the established trigger values. In fact, with the exception of 

TOC and estimated antimony hits « 1.0 !J,g/l) well below the trigger level of 6 !J,g/l, no other 

constituents were detected. These results are consistent with previous sampling events. Please 

note that while previous ERM antinl0ny results from the 1990s were non-detect, their reporting 

limit was much higher than what is currently being used today. 

Site Inspection 

A site inspection was conducted concurrently with the sampling activities. There were no problems 

noted with the exception offence repairs being needed at both landfills and an unlocked gate along 

the rear fence line at Coker's 1. A new lock has been installed on the gate and Pierce Fence in Dover 

Delaware will be completing the fence repairs later this month. 

Should you have any questions regarding this report or need additional information, please call me at 

(703) 519-2142. 
stt R~e~,~.~'--· Project Coordinator 

cc: 	 Sandra Guastaferro, Reichhold. Inc. 

Stephen Johnson, DNREC 

Lisa D. Krogman, P.E., Kraft Foods Global, Inc. 

Jeffrey Srulovitz, Esq., Kraft Foods Global, Inc. 


MARCH 2009

TOP OF CASING DEPTH TO GROUNDW

MONITORING WELL ELEVATION (FT, MSL) WATER (FT)(1) ELEVATI

L1-S1 41.73 8.03 33.70

L1-S3 42.41 13.51 28.90L1-S4 28.88 3.27 25.61

MW-1S 45.52 5.99 39.53

MW-3S 45.19 5.22 39.97

L2-S1 50.33 6.92 43.41

Notes:(1) Depth to water readings were measured on March 21, 2009.

Coker's 1Coker's 2

TABLE 1

GROUNDWATER ELEVATIONS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE
MARCH 2009

PARAMETER Trigger Level L1-S1 L1-S3 L1-S4 Trigger Level MW-1S 

Ethylbenzene 3,200 ND ND ND 700 ND 

Styrene 2,500 ND ND ND 100 ND 1,2,3-Trichloropropane - NA NA NA 5 ND 

Antimony - NA NA NA 6 0.62 B 

Phenolics (mg/l) - NA NA NA 22 ND 

Total Organic Carbon (mg/l) - 1.5 J 4.6 J 10.1 J - 7.0 J 

Temperature (oC) - 13.2 11.7 8.9 - 11.5 

pH - 5.48 5.66 5.81 - 5.83 

Specific Conductance (μmhos/cm) - 103.4 387.6 446.5 - 178.7 

Notes:ND indicates parameter was not detected.NA indicates parameter was not analyzed.Concentrations are reported in μg/l except where indicated otherwise.B indicates an estimated result below the reporting limit.J indicates method blank contamination.

Coker's 1 Coker's 

TABLE 2

SUMMARY OF GROUNDWATER SAMPLING RESULTS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE
MARCH 2009

PARAMETER Trigger Level SW-1 SW-2 SW-3 Trigger Level SED-1 

Ethylbenzene 1,600 ND ND ND - ND 

Styrene 1,250 ND ND ND - ND 

Xylenes (total) 615 ND ND ND - ND 

Total Organic Carbon (mg/l or mg/kg) - 3.4 J 3.4 J 3.4 J - 674 

Temperature (oC) - 9.6 7.7 6.3 - NA 

pH - 7.28 7.20 7.00 - NA 

Dissolved Oxygen (mg/l) - 11 11 9 - NA 

Specific Conductance (μmhos/cm) - 208.8 213.4 202.2 - NA 

Notes:ND indicates parameter was not detected.NA indicates parameter was not analyzed.Concentrations are reported in μg/l except where indicated otherwise.J indicates method blank contamination.

Surface Water Sedime

TABLE 3

SUMMARY OF WILLIS BRANCH SAMPLING RESULTS

COKER'S LANDFILLS SITE

CHESWOLD, DELAWARE
Appendix A 

 Analytical Results
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METHODS SUMMARY

C9C250123

ANALYTICAL PREPARATION

PARAMETER __________________________________________________ METHOD _______________ METHOD _______________

ICP-MS (6020) SW846 6020 SW846 3010

Phenolics SW846 9066 SW846 9066

Total Organic Carbon, TOC 5310B SM20 5310B

Total Residue as Percent Solids SM20 2540G

Volatile Organics by GC/MS SW846 8260B SW846 5030B

References:

EPA "EASTERN ENVIRONMENTAL RADIATION FACILITY RADIOCHEMISTRY

PROCEDURES MANUAL" US EPA EPA 520/5-84-006 AUGUST 1984

SM20 "STANDARD METHODS FOR THE EXAMINATION OF WATER AND

WASTEWATER", 20TH EDITION."

SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical

Methods", Third Edition, November 1986 and its updates.

TestAmerica Laboratories, Inc.

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SAMPLE SUMMARY

C9C250123

SAMPLED SAMP

WO #_____ SAMPLE# _______ CLIENT SAMPLE ID ________________________________________________________________ DATE ________ TIME _____

K84AL 001 L1-S1 03/21/09 13:35

K84A4 002 L1-S3 03/21/09 17:35

K84A7 003 L1-S4 03/21/09 17:50

K84CH 004 SW-1 03/22/09 12:00

K84CJ 005 SW-2 03/22/09 11:10

K84CL 006 SW-3 03/22/09 10:30

K84CM 007 SED-1 03/22/09 12:10

K84CN 008 SED-2 03/22/09 11:20

K84EM 009 SED-3 03/22/09 10:40

K84EQ 010 TRIP BLANK 03/22/09

K84E3 011 MW-1S 03/21/09 17:10

K84GK 012 MW-3S 03/21/09 16:50

K84GL 013 L2-S1 03/21/09 10:35

K84GN 014 RINSE BLANK-1 03/21/09 10:15

NOTE(S): _____________________________________________________________________________________________

- The analytical results of the samples listed above are presented on the following pages.

- All calculations are performed before rounding to avoid round-off errors in calculated results.

- Results noted as "ND" were not detected at or above the stated limit.

- This report must not be reproduced, except in full, without the written approval of the laboratory.

- Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitability, layers, odor,

paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight.

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-001 Work Order #...: Work Order #...: K84AL1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 13:18

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 89 (62 - 123)

Toluene-d8 95 (80 - 120)

4-Bromofluorobenzene 92 (75 - 120)

Dibromofluoromethane 89 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-002 Work Order #...: Work Order #...: K84A41AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 14:10

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 88 (62 - 123)

Toluene-d8 95 (80 - 120)

4-Bromofluorobenzene 90 (75 - 120)

Dibromofluoromethane 88 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-003 Work Order #...: Work Order #...: K84A71AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 14:37

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 88 (62 - 123)

Toluene-d8 99 (80 - 120)

4-Bromofluorobenzene 96 (75 - 120)

Dibromofluoromethane 90 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: SW-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-004 Work Order #...: Work Order #...: K84CH1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 15:04

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 105 (62 - 123)

Toluene-d8 115 (80 - 120)

4-Bromofluorobenzene 108 (75 - 120)

Dibromofluoromethane 108 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: SW-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-005 Work Order #...: Work Order #...: K84CJ1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 15:28

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 86 (62 - 123)

Toluene-d8 96 (80 - 120)

4-Bromofluorobenzene 88 (75 - 120)

Dibromofluoromethane 90 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: SW-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-006 Work Order #...: Work Order #...: K84CL1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 15:51

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 90 (62 - 123)

Toluene-d8 103 (80 - 120)

4-Bromofluorobenzene 95 (75 - 120)

Dibromofluoromethane 95 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: SED-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-007 Work Order #...: Work Order #...: K84CM1AC Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9091061

Prep Date......: Prep Date......: 04/01/09 Analysis Date..: Analysis Date..: 04/01/09

Prep Batch #...: Prep Batch #...: 9091101 Analysis Time..: Analysis Time..: 13:18

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 21 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 6.3 ug/kg

Styrene ND 6.3 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 96 (52 - 124)

Toluene-d8 106 (72 - 127)

4-Bromofluorobenzene 84 (63 - 120)

Dibromofluoromethane 102 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 14 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-008 Work Order #...: Work Order #...: K84CN1AC Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9091061

Prep Date......: Prep Date......: 04/01/09 Analysis Date..: Analysis Date..: 04/01/09

Prep Batch #...: Prep Batch #...: 9091101 Analysis Time..: Analysis Time..: 13:43

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 6.5 ug/kg

Styrene ND 6.5 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 95 (52 - 124)

Toluene-d8 100 (72 - 127)

4-Bromofluorobenzene 86 (63 - 120)

Dibromofluoromethane 101 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 15 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-009 Work Order #...: Work Order #...: K84EM1AC Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9091061

Prep Date......: Prep Date......: 04/01/09 Analysis Date..: Analysis Date..: 04/01/09

Prep Batch #...: Prep Batch #...: 9091101 Analysis Time..: Analysis Time..: 14:08

Dilution Factor: Dilution Factor: 1

% Moisture.....: % Moisture.....: 23 Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 6.5 ug/kg

Styrene ND 6.5 ug/kg

Xylenes (total) ND 19 ug/kg

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 96 (52 - 124)

Toluene-d8 105 (72 - 127)

4-Bromofluorobenzene 82 (63 - 120)

Dibromofluoromethane 100 (68 - 121)

NOTE(S): _______________________________________________________________________________________

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: TRIP BLANK

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-010 Work Order #...: Work Order #...: K84EQ1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 12:31

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

Xylenes (total) ND 15 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 89 (62 - 123)

Toluene-d8 93 (80 - 120)

4-Bromofluorobenzene 91 (75 - 120)

Dibromofluoromethane 88 (80 - 120)

TestAmerica Laboratories, Inc.

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Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-011 Work Order #...: Work Order #...: K84E31AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 16:14

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

1,2,3-Trichloropropane ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 95 (62 - 123)

Toluene-d8 105 (80 - 120)

4-Bromofluorobenzene 97 (75 - 120)

Dibromofluoromethane 99 (80 - 120)

TestAmerica Laboratories, Inc.

C9C250123 18 of 52
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-012 Work Order #...: Work Order #...: K84GK1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 16:37

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

1,2,3-Trichloropropane ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 104 (62 - 123)

Toluene-d8 113 (80 - 120)

4-Bromofluorobenzene 103 (75 - 120)

Dibromofluoromethane 102 (80 - 120)

TestAmerica Laboratories, Inc.

C9C250123 19 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-013 Work Order #...: Work Order #...: K84GL1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 17:01

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

1,2,3-Trichloropropane ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 82 (62 - 123)

Toluene-d8 91 (80 - 120)

4-Bromofluorobenzene 83 (75 - 120)

Dibromofluoromethane 86 (80 - 120)

TestAmerica Laboratories, Inc.

C9C250123 20 of 52
Clean Sites Environmental Services Inc

Client Sample ID: RINSE BLANK-1

GC/MS Volatiles

Lot-Sample #...: Lot-Sample #...: C9C250123-014 Work Order #...: Work Order #...: K84GN1AA Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 17:24

Dilution Factor: Dilution Factor: 1

Method.........: Method.........: SW846 8260B

REPORTING

PARAMETER ______________________________ RESULT _______________ LIMIT _________ UNITS __________

Ethylbenzene ND 5.0 ug/L

Styrene ND 5.0 ug/L

1,2,3-Trichloropropane ND 5.0 ug/L

PERCENT RECOVERY

SURROGATE ______________________________ RECOVERY _______________ LIMITS __________

1,2-Dichloroethane-d4 97 (62 - 123)

Toluene-d8 108 (80 - 120)

4-Bromofluorobenzene 99 (75 - 120)

Dibromofluoromethane 101 (80 - 120)

TestAmerica Laboratories, Inc.

C9C250123 21 of 52
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K9DGL1AA Matrix.........: Matrix.........: WATER

MB Lot-Sample #: MB Lot-Sample #: C9C310000-362

Prep Date......: Prep Date......: 03/31/09 Analysis Time..: Analysis Time..: 09:06

Analysis Date..: Analysis Date..: 03/31/09 Prep Batch #...: Prep Batch #...: 9090362

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Ethylbenzene ND 5.0 ug/L SW846 8260B

Styrene ND 5.0 ug/L SW846 8260B

Xylenes (total) ND 15 ug/L SW846 8260B

1,2,3-Trichloropropane ND 5.0 ug/L SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 76 (62 - 123)

Toluene-d8 112 (80 - 120)

4-Bromofluorobenzene 99 (75 - 120)

Dibromofluoromethane 96 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 22 of 52
METHOD BLANK REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K9D5G1AA Matrix.........: Matrix.........: SOLID

MB Lot-Sample #: MB Lot-Sample #: C9D010000-101

Prep Date......: Prep Date......: 04/01/09 Analysis Time..: Analysis Time..: 07:34

Analysis Date..: Analysis Date..: 04/01/09 Prep Batch #...: Prep Batch #...: 9091101

Dilution Factor: Dilution Factor: 1

REPORTING

PARAMETER _________________________ RESULT _______________ LIMIT _________ UNITS __________ METHOD _________________

Ethylbenzene ND 5.0 ug/kg SW846 8260B

Styrene ND 5.0 ug/kg SW846 8260B

Xylenes (total) ND 15 ug/kg SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 93 (52 - 124)

Toluene-d8 100 (72 - 127)

4-Bromofluorobenzene 98 (63 - 120)

Dibromofluoromethane 92 (68 - 121)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 23 of 52
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K9DGL1AC Matrix.........: Matrix.........: WATER

LCS Lot-Sample#: LCS Lot-Sample#: C9C310000-362

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 10:55

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

1,1-Dichloroethene 1,1-Dichloroethene 93 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 96 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Benzene Benzene 94 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

Toluene Toluene 99 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 103 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 88 (62 - 123)

Toluene-d8 100 (80 - 120)

4-Bromofluorobenzene 96 (75 - 120)

Dibromofluoromethane 92 (80 - 120)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

TestAmerica Laboratories, Inc.

C9C250123 24 of 52
LABORATORY CONTROL SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K9D5G1AC Matrix.........: Matrix.........: SOLID

LCS Lot-Sample#: LCS Lot-Sample#: C9D010000-101

Prep Date......: Prep Date......: 04/01/09 Analysis Date..: Analysis Date..: 04/01/09

Prep Batch #...: Prep Batch #...: 9091101 Analysis Time..: Analysis Time..: 08:23

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY

PARAMETER ________________________ RECOVERY ________ LIMITS __________ METHOD _________________

1,1-Dichloroethene 1,1-Dichloroethene 94 (59 - 129) (59 - 129) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 89 (76 - 119) (76 - 119) SW846 8260B SW846 8260B

Benzene Benzene 97 (77 - 120) (77 - 120) SW846 8260B SW846 8260B

Toluene Toluene 104 (78 - 124) (78 - 124) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 94 (79 - 120) (79 - 120) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 90 (52 - 124)

Toluene-d8 106 (72 - 127)

4-Bromofluorobenzene 101 (63 - 120)

Dibromofluoromethane 89 (68 - 121)

NOTE(S): _____________________________________________________________________________________ _____________________________________________________________________________________ 

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

TestAmerica Laboratories, Inc.

C9C250123 25 of 52
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K84AL1AD-MS Matrix.........: Matrix.........: WATER

MS Lot-Sample #: MS Lot-Sample #: C9C250123-001 K84AL1AE-MSD

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09 MS Run #.......: MS Run #.......: 9090218

Prep Date......: Prep Date......: 03/31/09 Analysis Date..: Analysis Date..: 03/31/09

Prep Batch #...: Prep Batch #...: 9090362 Analysis Time..: Analysis Time..: 10:03

Dilution Factor: Dilution Factor: 1

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

1,1-Dichloroethene 1,1-Dichloroethene 100 (69 - 127) (69 - 127) SW846 8260B SW846 8260B

92 (69 - 127) (69 - 127) 8.1 (0-20) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 97 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

96 (80 - 120) (80 - 120) 0.98 (0-20) SW846 8260B SW846 8260B

Benzene Benzene 97 (80 - 120) (80 - 120) SW846 8260B SW846 8260B

92 (80 - 120) (80 - 120) 5.2 (0-20) SW846 8260B SW846 8260B

Toluene Toluene 97 (80 - 124) (80 - 124) SW846 8260B SW846 8260B

97 (80 - 124) (80 - 124) 0.54 (0-20) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 101 (83 - 120) (83 - 120) SW846 8260B SW846 8260B

102 (83 - 120) (83 - 120) 1.2 (0-20) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 89 (62 - 123)

85 (62 - 123)

Toluene-d8 99 (80 - 120)

99 (80 - 120)

4-Bromofluorobenzene 97 (75 - 120)

97 (75 - 120)

Dibromofluoromethane 95 (80 - 120)

92 (80 - 120)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

TestAmerica Laboratories, Inc.

C9C250123 26 of 52
MATRIX SPIKE SAMPLE EVALUATION REPORT

GC/MS Volatiles

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K84871D5-MS Matrix.........: Matrix.........: SOLID

MS Lot-Sample #: MS Lot-Sample #: C9C250233-004 K84871D6-MSD

Date Sampled...: Date Sampled...: 03/24/09 Date Received..: Date Received..: 03/25/09 MS Run #.......: MS Run #.......: 9091061

Prep Date......: Prep Date......: 04/01/09 Analysis Date..: Analysis Date..: 04/01/09

Prep Batch #...: Prep Batch #...: 9091101 Analysis Time..: Analysis Time..: 08:47

Dilution Factor: Dilution Factor: 0.89 % Moisture.....: % Moisture.....: 100

PERCENT RECOVERY RPD

PARAMETER _________________________ RECOVERY _________ LIMITS __________ RPD ____ LIMITS _________ METHOD _________________

1,1-Dichloroethene 1,1-Dichloroethene 121 (59 - 129) (59 - 129) SW846 8260B SW846 8260B

111 (59 - 129) (59 - 129) 2.5 (0-25) SW846 8260B SW846 8260B

Trichloroethene Trichloroethene 105 (76 - 119) (76 - 119) SW846 8260B SW846 8260B

99 (76 - 119) (76 - 119) 0.05 (0-21) SW846 8260B SW846 8260B

Benzene Benzene 107 (77 - 120) (77 - 120) SW846 8260B SW846 8260B

102 (77 - 120) (77 - 120) 1.7 (0-20) SW846 8260B SW846 8260B

Toluene Toluene 119 (78 - 124) (78 - 124) SW846 8260B SW846 8260B

118 (78 - 124) (78 - 124) 6.1 (0-21) SW846 8260B SW846 8260B

Chlorobenzene Chlorobenzene 105 (79 - 120) (79 - 120) SW846 8260B SW846 8260B

101 (79 - 120) (79 - 120) 2.6 (0-20) SW846 8260B SW846 8260B

PERCENT RECOVERY

SURROGATE _________________________ RECOVERY ________ LIMITS __________

1,2-Dichloroethane-d4 76 (52 - 124)

72 (52 - 124)

Toluene-d8 109 (72 - 127)

114 (72 - 127)

4-Bromofluorobenzene 98 (63 - 120)

100 (63 - 120)

Dibromofluoromethane 88 (68 - 121)

87 (68 - 121)

NOTE(S): ___________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 27 of 52
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9C250123-011 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9089175

Antimony Antimony 0.62 B 2.0 ug/L SW846 6020 SW846 6020 03/30-03/31/09 03/30-03/31/09 K84E31AC K84E31AC

Dilution Factor: 1 Analysis Time..: 14:21 MS Run #.......: 9089103

NOTE(S): ___________________________________________________________________________________________

B Estimated result. Result is less than RL.

TestAmerica Laboratories, Inc.

C9C250123 28 of 52
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9C250123-012 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9089175

Antimony Antimony 0.33 B 2.0 ug/L SW846 6020 SW846 6020 03/30-03/31/09 03/30-03/31/09 K84GK1AC K84GK1AC

Dilution Factor: 1 Analysis Time..: 14:39 MS Run #.......: 9089103

NOTE(S): ___________________________________________________________________________________________

B Estimated result. Result is less than RL.

TestAmerica Laboratories, Inc.

C9C250123 29 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

TOTAL Metals

Lot-Sample #...: Lot-Sample #...: C9C250123-013 Matrix.......: Matrix.......: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

Prep Batch #...: Prep Batch #...: 9089175

Antimony Antimony 0.097 B 0.097 B 2.0 ug/L SW846 6020 SW846 6020 03/30-03/31/09 03/30-03/31/09 K84GL1AC K84GL1AC

Dilution Factor: 1 Analysis Time..: 14:44 MS Run #.......: 9089103

NOTE(S): ___________________________________________________________________________________________

B Estimated result. Result is less than RL.

TestAmerica Laboratories, Inc.

C9C250123 30 of 52
METHOD BLANK REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- WORK

PARAMETER _______________ RESULT _____________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ ORDER # ________

MB Lot-Sample #: MB Lot-Sample #: C9C300000-175 Prep Batch #...: Prep Batch #...: 9089175

Antimony ND 2.0 ug/L SW846 6020 03/30-03/31/09 K9AJ71AK

Dilution Factor: 1

Analysis Time..: 14:12

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 31 of 52
LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY PREPARATIONPARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ WORK ORDER # ____________

LCS Lot-Sample#: LCS Lot-Sample#: C9C300000-175 Prep Batch #...: Prep Batch #...: 9089175

Antimony 86 (80 - 120) SW846 6020 03/30-03/31/09 K9AJ71A0

Dilution Factor: 1 Analysis Time..: 14:16

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 32 of 52
MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/26/09 Date Received..: Date Received..: 03/27/09

PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ ORDER # _______

MS Lot-Sample #: MS Lot-Sample #: C9C270204-006 Prep Batch #...: Prep Batch #...: 9089175

Antimony 86 (75 - 125) SW846 6020 03/30-03/31/09 K88RN1CC

87 (75 - 125) 0.76 (0-20) SW846 6020 03/30-03/31/09 K88RN1CD

Dilution Factor: 1

Analysis Time..: 15:59

MS Run #.......: 9089103

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 33 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L1-S1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-001 Work Order #...: Work Order #...: K84AL Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 1.5 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089057 9089057

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 34 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L1-S3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-002 Work Order #...: Work Order #...: K84A4 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 4.6 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089057 9089057

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 35 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L1-S4

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-003 Work Order #...: Work Order #...: K84A7 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 10.1 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 36 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SW-1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-004 Work Order #...: Work Order #...: K84CH Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 3.4 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 37 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SW-2

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-005 Work Order #...: Work Order #...: K84CJ Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 3.4 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 38 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SW-3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-006 Work Order #...: Work Order #...: K84CL Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon 3.4 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 39 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SED-1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-007 Work Order #...: Work Order #...: K84CM Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

% Moisture.....: % Moisture.....: 21

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 79.3 1.0 % SM20 2540G SM20 2540G 03/26-03/27/09 03/26-03/27/09 9085144 9085144

Dilution Factor: 1 Analysis Time..: 07:56 MS Run #.......: 9085080

Total Organic Carbon Total Organic Carbon 3210 674 mg/kg EPA Lloyd Kahn EPA Lloyd Kahn 03/27/09 03/27/09 9086084 9086084

(TOC)

Dilution Factor: 1.07 Analysis Time..: 14:55 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 40 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SED-2

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-008 Work Order #...: Work Order #...: K84CN Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

% Moisture.....: % Moisture.....: 23

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 77.4 1.0 % SM20 2540G SM20 2540G 03/26-03/27/09 03/26-03/27/09 9085144 9085144

Dilution Factor: 1 Analysis Time..: 07:56 MS Run #.......: 9085080

Total Organic Carbon Total Organic Carbon 3580 1030 mg/kg EPA Lloyd Kahn EPA Lloyd Kahn 03/27/09 03/27/09 9086084 9086084

(TOC)

Dilution Factor: 1.6 Analysis Time..: 15:05 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 41 of 52
Clean Sites Environmental Services Inc

Client Sample ID: SED-3

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-009 Work Order #...: Work Order #...: K84EM Matrix.........: Matrix.........: SOLID

Date Sampled...: Date Sampled...: 03/22/09 Date Received..: Date Received..: 03/24/09

% Moisture.....: % Moisture.....: 23

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids Percent Solids 77.2 1.0 % SM20 2540G SM20 2540G 03/26-03/27/09 03/26-03/27/09 9085144 9085144

Dilution Factor: 1 Analysis Time..: 07:56 MS Run #.......: 9085080

Total Organic Carbon Total Organic Carbon 1840 608 mg/kg EPA Lloyd Kahn EPA Lloyd Kahn 03/27/09 03/27/09 9086084 9086084

(TOC)

Dilution Factor: 0.94 Analysis Time..: 15:15 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

Results and reporting limits have been adjusted for dry weight.

TestAmerica Laboratories, Inc.

C9C250123 42 of 52
Clean Sites Environmental Services Inc

Client Sample ID: MW-1S

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-011 Work Order #...: Work Order #...: K84E3 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 03/30/09 9089049

Phenolics

Dilution Factor: 1 Analysis Time..: 07:20 MS Run #.......: 9089030

Total Organic Carbon Total Organic Carbon 7.0 J 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

NOTE(S): ___________________________________________________________________________________________

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

TestAmerica Laboratories, Inc.

C9C250123 43 of 52
Clean Sites Environmental Services Inc

Client Sample ID: MW-3S

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-012 Work Order #...: Work Order #...: K84GK Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 03/30/09 9089049

Phenolics

Dilution Factor: 1 Analysis Time..: 07:20 MS Run #.......: 9089030

Total Organic Carbon Total Organic Carbon 5.7 1.0 mg/L SM20 5310B SM20 5310B 04/01/09 04/01/09 9091035 9091035

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

TestAmerica Laboratories, Inc.

C9C250123 44 of 52
Clean Sites Environmental Services Inc

Client Sample ID: L2-S1

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123-013 Work Order #...: Work Order #...: K84GL Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/21/09 Date Received..: Date Received..: 03/24/09

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable ND 0.010 mg/L SW846 9066 03/30/09 9089049

Phenolics

Dilution Factor: 1 Analysis Time..: 07:20 MS Run #.......: 9089030

Total Organic Carbon Total Organic Carbon 3.0 1.0 mg/L SM20 5310B SM20 5310B 04/01/09 04/01/09 9091035 9091035

(TOC)

Dilution Factor: 1 Analysis Time..: 00:00 MS Run #.......:

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METHOD BLANK REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: SOLID

REPORTING PREPARATION- PREP

PARAMETER __________________ RESULT __________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Work Order #: K872G1AA MB Lot-Sample #: C9C270000-084

(TOC)

ND 1250 mg/kg EPA Lloyd Kahn 03/27/09 9086084

Dilution Factor: 2.5

Analysis Time..: 13:44

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

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METHOD BLANK REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

REPORTING PREPARATION- PREP

PARAMETER __________________ RESULT __________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon Total Organic Carbon Work Order #: K9ADA1AA MB Lot-Sample #: C9C300000-057

(TOC)

0.20 B 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089057 9089057

Dilution Factor: 1

Analysis Time..: 00:00

Total Organic Carbon Total Organic Carbon Work Order #: K9A6T1AA MB Lot-Sample #: C9C300000-463

(TOC)

0.34 B 1.0 mg/L SM20 5310B SM20 5310B 03/30/09 03/30/09 9089463 9089463

Dilution Factor: 1

Analysis Time..: 00:00

Total Organic Carbon Work Order #: K9D201AA MB Lot-Sample #: C9D010000-035

(TOC)

ND 1.0 mg/L SM20 5310B 04/01/09 9091035

Dilution Factor: 1

Analysis Time..: 00:00

Total Recoverable Work Order #: K9AC11AA MB Lot-Sample #: C9C300000-049

Phenolics

ND 0.010 mg/L SW846 9066 03/30/09 9089049

Dilution Factor: 1

Analysis Time..: 07:12

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

B Estimated result. Result is less than RL.

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LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123 Matrix.........: Matrix.........: SOLID

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon WO#:K872G1AC-LCS/K872G1AD-LCSD LCS Lot-Sample#: C9C270000-084

(TOC)

103 (75 - 125) EPA Lloyd Kahn 03/27/09 9086084

96 (75 - 125) 6.5 (0-20) EPA Lloyd Kahn 03/27/09 9086084

Dilution Factor: 1.98 Analysis Time..: 13:54

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

C9C250123 48 of 52
LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Lot-Sample #...: Lot-Sample #...: C9C250123 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Organic Carbon WO#:K9ADA1AC-LCS/K9ADA1AD-LCSD LCS Lot-Sample#: C9C300000-057

(TOC)

92 (80 - 120) SM20 5310B 03/30/09 9089057

94 (80 - 120) 2.4 (0-10) SM20 5310B 03/30/09 9089057

Dilution Factor: 1 Analysis Time..: 00:00

Total Organic Carbon WO#:K9A6T1AC-LCS/K9A6T1AD-LCSD LCS Lot-Sample#: C9C300000-463

(TOC)

93 (80 - 120) SM20 5310B 03/30/09 9089463

94 (80 - 120) 0.85 (0-10) SM20 5310B 03/30/09 9089463

Dilution Factor: 1 Analysis Time..: 00:00

Total Organic Carbon WO#:K9D201AC-LCS/K9D201AD-LCSD LCS Lot-Sample#: C9D010000-035

(TOC)

93 (80 - 120) SM20 5310B 04/01/09 9091035

99 (80 - 120) 5.6 (0-10) SM20 5310B 04/01/09 9091035

Dilution Factor: 1 Analysis Time..: 00:00

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

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LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

PERCENT RECOVERY PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable Work Order #: K9AC11AC LCS Lot-Sample#: C9C300000-049

Phenolics

82 (75 - 125) SW846 9066 03/30/09 9089049

Dilution Factor: 1 Analysis Time..: 07:12

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

TestAmerica Laboratories, Inc.

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MATRIX SPIKE SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9C250123 Matrix.........: Matrix.........: WATER

Date Sampled...: Date Sampled...: 03/25/09 Date Received..: Date Received..: 03/26/09

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Total Recoverable WO#: K86JM1AC-MS/K86JM1AD-MSD MS Lot-Sample #: C9C260151-001

Phenolics

86 (75 - 125) SW846 9066 03/30/09 9089047

82 (75 - 125) 4.4 (0-20) SW846 9066 03/30/09 9089047

Dilution Factor: 1

Analysis Time..: 07:12

MS Run #.......: 9089030

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

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SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: C9C250123 Work Order #...: Work Order #...: K83RM-SMP Matrix.......: Matrix.......: SOLID

K83RM-DUP

Date Sampled...: Date Sampled...: 03/12/09 Date Received..: Date Received..: 03/13/09

% Moisture.....: % Moisture.....: 0.56

DUPLICATE RPD PREPARATION- PREP

PARAM_____ RESULT ___________ RESULT ___________ UNITS ________ RPD _____ LIMIT _______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Percent Solids SD Lot-Sample #: C9C240299-001

99.4 99.4 % 0.004 (0-20) SM20 2540G 03/26-03/27/09 9085144

Dilution Factor: 1 Analysis Time..: 07:56 MS Run Number..: 9085080

TestAmerica Laboratories, Inc.

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