## Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Test Date

7210 Cope COP1 6/8/2010

### Fuel Type 1 Fuel Type 2 Fuel Type 3

bitum inous

### Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte

7210 Cope COP1 As Received Higher Heating Value 7210 Cope COP1 As Received % Moisture 7210 Cope COP1 As Received % Ash 7210 Cope COP1 As Received % Sulfur 7210 Cope COP1 Dry basis Higher Heating Value 7210 Cope COP1 Dry basis % Moisture 7210 Cope COP1 Dry basis % Ash 7210 Cope COP1 Dry basis % Sulfur 7210 Cope COP1 Dry basis Antim ony 7210 Cope COP1 Dry basis Arsenic 7210 Cope COP1 Dry basis Beryllium 7210 Cope COP1 Dry basis Cadmium 7210 Cope COP1 Dry basis Chlorine 7210 Cope COP1 Dry basis Chromium 7210 Cope COP1 Dry basis Cobalt 7210 Cope COP1 Dry basis Fluorine 7210 Cope COP1 Dry basis Lead 7210 Cope COP1 Dry basis Manganese 7210 Cope COP1 Dry basis Mercury 7210 Cope COP1 Dry basis Nickel 7210 Cope COP1 Dry basis Selenium

### An alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D 5865-04 ASTM D 3173-03 ASTM D 3174 ASTM D 4239 ASTM D 5865-04 ASTM D 3173-03 ASTM D 3174 ASTM D 4239 ASTM D 6357-04 ASTM D 6357-04 ASTM D 6357-04 ASTM D 6357-04 ASTM D 6721-01 ASTM D 6357-04 ASTM D 6357-04 ASTM D 3761-96 ASTM D 6357-04 ASTM D 6357-04 ASTM D 6722-01 ASTM D 6357-04 SW -846-7740EIA Facility Code Facility Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M30B, M26A, M0031 wi th SW-846 M6260B) 7210 Cope COP1 OTM27,OTM28,M5,M6,M7e,M18,M25e,M26,M29,M3A,M10,M4

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units CO4388 6/8/2010 12689.00 Btu/lb 4.518 9.812 1.251 12972 Btu/lb CO4389 6/8/2010 12216.00 Btu/lb 6.161 11.005 0.96 13018 Btu/lb CO 4390 6/8/2010 12707.00 Btu/lb 4.391 9.132 1.146 13291 Btu/lb Fuel Testing Results% Moisture

(Dry Basis) % Ash (Dry Basis) % Sulfur (Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic

(Dry Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units 0 11.748 1.115 960 ug/g 0.08 μg/g 5 μg/g 2.2 μg/g <0.2 μg/g 0 11.728 1.022 930 ug/g 0.08 μg/g 4 μg/g 2.3 μg/g <0.2 μg/g 0 9.551 1.199 720 ug/g 0.07 μg/g 5 μg/g 1.9 μg/g <0.2 μg/gChromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt

Units 19 μg/g 7 μg/g 12 μg/g 14 μg/g 4 μg/g 79 ug/g 7 μg/g 21 μg/g 8 μg/g 12 μg/g 15 μg/g 4 μg/g 75 ug/g 8 μg/g 16 μg/g 6 μg/g 13 μg/g 13 μg/g 4 μg/g 69 ug/g 6 μg/gEIA Facility Code Facility

Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 7210 Cope COP1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 7210 Cope COP1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 7210 Cope COP1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm