### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC General Company and Facility** 

**Information**

**Instructions**

Please complete this worksheet for your parent company and PVC production facility

.

**Parent Company General Information**

Parent Company

Name:

Address:

City:
Country: USA

Size of Company

(approximate number of employees including all subsidiaries, branches, and related establishments owned):

**PVC Production Facility General Information**

Facility Name:

Facility Address:

Facility City:
Facility Technical Contact Name:

Technical Contact Telephone Number:

Technical Contact Email:

Number of employees attached to the PVC production facility: 90 Avon Lake 33587 Walker Rd PolyOne Corp

309-364-9108

Scott.Johnson@polyone.com PolyOne Henry

1546 County

Road, 1450N

Henry

Scott Johnson

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

State: OH Zip Code: 44012

Size of Company

(approximate number of employees including all subsidiaries, branches, and related establishments owned):

State: ILL Zip Code: 61537

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Treatment Sy** **stem Information Update**

**Instructions**

2. Also complete the additional supplemental questions to Form C-1-c.

**FORM C-1-c PROCESS EQUIPMENT - WA** **STEWA TER STEA** **M STRIPPER**

Process Unit ID: P-11

Process Equipment ID: U-2 Wastewater Feed Rate (lb/hr): 20000 Feed Temperature (°F): 200 Feed Inlet Pressure (psia): NA Liquid Loading Rate (liters/m2): NA SteamFeed Rate (lb/hr): NA Steamto Feed Ratio (kg steam/liter of wastewater): NA Operating Temperature (°F): 226 Operating Pressure (psig): 5 Total Number of Stages: 0 Overall Calculated Tray Efficiency: 0 Stripping Factor: NA Flow configuration (countercurrent, cocurrent): cocurrent Number of Actual Trays: 0 Column Height (meters): 6.1

Year Equipment Installed: 1978 Equipment Currently

Regulated Under (cite regulations): 61.65 b 9i 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary below.

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

**Form C-1-c Supplemental Questions**

Please also provide the stripper feed rate in liters per hour, or liters for batch strippers:

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values: 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessaryPlease also provide the stripper feed rate in liters per hour, or liters for batch strippers: 9463liters/hour liters

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values:

liters/hour (max design) liters (max design) 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Stream Information** 

**Instructions**

1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process wastewater treatment system. 2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wastewater treatment system. 3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC production facility

.

**Table 1. Process Wastewater Streams Not Treated by a PVC Process Wastewater Treatment System 1**  **3 4**  **5**

**Min Ma** **x** P1 W1 6048 8467 P2 W1 6221 8294 P4 W2 14976 22464 P5 W2 10368 15552 **PVC Process Unit ID**  **Name of PVC Process Wastewater Stream 2** 

Permeate **PVC Process Wastewater Stream Flow Rate (gallons per day)** 

Permeate

Centrate **PVC Process Wastewater**  **Stream ID**

Centrate**Table 2. Process Wastewater Streams Exiting a PVC Process Wastewater Treatment System 1**  **2 3**  **4 5**  **6 7**  **8**

**Min Ma** **x Av** **erage** P1,2,4,5 P-11 SteamStripping Continuous 720 1200 960

**Table 3. PVC Process Wastewater Destination Codes Table Ty** **pe of Process Wastewater**  **Treatment System PVC Process**  **Wastewater Treatment**  **System ID PVC Process**  **Unit ID PVC Process**  **Wastewater Stream ID**  **Is this process**  **wastewater treatment**  **system batch or continuous**  **operation? PVC Process Wastewater Stream Flow Rate**  **(gallons per day)**Wastewater treatment system

Discharge without treatment by pipeline, sewer, or other conveyance to surface water Discharge to POTW, no treatment Discharge to PrOTW, no treatment Zero discharge or alternative disposal method Recycle to process Other

**Table 4. Non-PVC Production Process Wastewater Streams Entering a PVC Process Wastewater Treatment System 2**  **3 4**  **5**

**Min Ma** **x Av** **erage Destination Description** 

**1**

**Process Wastewater Stream Flow Rate (gallons per day)**  **Source of Process Wastewater Stream Flow Rate**  **Determination Me** **thod**1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process wastewater treatment system. 2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wastewater treatment system. 3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC production facility

.

**6 7**  **8 9**  **10**

**Av erage**  7258Measured 305U3 Ultrafiltration 7258Measured 261 U5 Ultrafiltration 18720Measured 190U5 Centrifuge 12960Measured 132 U6 Centrifuge **Operating Days Per Year**  **Originating PVC Process Equipment Description**  **Flow Rate Determination**  **Me thod**  **Originating PVC Process Equipment ID**  **PVC Process Wastewater Stream Flow Rate 9**  **10 11**  **12 13** 

Measured 305WWT Yes **PVC Process Wastewater Stream**  **Destination Code**

(Refer to Table 3 below) **As sociated Destination**  **Information**

(Refer to Table 3 below) **Operating Days Per Year**  **Is this PVC process wastewater stream exposed to the atmosphere**  **at any point between the outlet of the PVC process wastewater**  **treatment system and its destination?**  **Flow Rate Determination**  **Me thod** **Code** WWT Provide name of the wastewater treatment system SW Provide name of outfall POTWRAW Provide name of POTW PrOTWRAW Provide name of PrOTW ZEROALT Describe method RECYC Describe where in the process the stream is recycled OTHER Describe

**6 7**  **Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2**

**PVC Process Wastewater**  **Treatment System ID**  **Operating Days Per Year** **11 12**  **13**

WWT Yes WWT Yes WWT Yes WWT Yes **Is this PVC process wastewater stream exposed to the atmosphere**  **at any point between the originating PVC process equipment**  **and its destination? PVC Process Wastewater Stream**  **Destination Code**

(Refer to Table 3 below) **As sociated Destination Information** **14**

**If your response in Column 3 is "Other" then please provide a description of the process wastewaetr treatment system** **Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2**

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

**Instructions**

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Complete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

**Company Facility**  **PVC Process Wastewater Treatment Sy stem ID** 

**CA S No.**  **HA P** 
107211 Ethylene glycol 67561 Methanol 75070Acetaldehyde 50000Formaldehyde 512852,4-dinitrophenol 98862Acetophenone 117817Bis(2-ethylhexyl) phthalate (DEHP) 123319Hydroquinone 108952Phenol 79345 1,1,2,2-tetrachloroethane 106990 1,3-butadiene 540841 2,2,4-trimethylpentane 71432Benzene 108907Chlorobenzene 67663Chloroform 126998Chloroprene 98828Cumene 75003Ethyl chloride (Chloroethane) 100414Ethylbenzene 107062 Ethylene dichloride (1,2-Dichloroethane) 75343Ethylidene dichloride (1,1-Dichloroethane) 74873Methyl chloride (Chloromethane) 75092Methylene chloride **Resin Type (suspension, dispersion, bulk, etc.) -->**110543n-Hexane 108883Toluene 71556Methyl chloroform (1,1,1-Trichloroethane) 79005 1,1,2-Trichloroethane 108054Vinyl acetate 593602Vinyl bromide 75014Vinyl chloride 75354Vinylidene chloride (1,1-Dichloroethylene) 1330207Xylenes (isomers and mixtures)

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Complete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

PolyOne Henry P-11

**An alysis M** **ethod Concentration**  **(ppmw) Non-Detect?** 
SW-846-8015C 10 Non-detect SW-846-8015C 0.045 Non-detect SW-846-8315A 0.149 SW-846-8315A 0.238 SW-846-8270D 0.017 Non-detect SW-846-8270D 0.0642 SW-846-8270D 0.001 SW-846-8270D 0.005 Non-detect SW-846-8270D 0.0013 Non-detect SW-846-8260B 0.00021 Non-detect SW-846-8260B 0.0019 Non-detect SW-846-8260B 0.00023 Non-detect SW-846-8260B 0.00036 SW-846-8260B 0.00023 Non-detect SW-846-8260B 0.0002 Non-detect SW-846-8260B 0.00021 Non-detect SW-846-8260B 0.00045 Non-detect SW-846-8260B 0.407 SW-846-8260B 0.00023 Non-detect SW-846-8260B 0.114 SW-846-8260B 0.00049 SW-846-8260B 0.908 SW-846-8260B 0.004 **Sample Date -->** Suspension/Blending/Dispersion **Stream Flow Rate (gallons per minute) --> Resin Type (suspension, dispersion, bulk, etc.) -->** 

**Lab Sample ID --> Lab Report ID -->**  **An alysis Date -->**  **Stream Temperature (degrees F) -->** 01/07/13

JB25203-1 JB25203 See Lab Report **Flow Rate Determination Method -->** MeasuredSW-846-8260B 0.00046 Non-detect

SW-846-8260B 0.00023 Non-detect SW-846-8260B 0.00024 Non-detect SW-846-8260B 0.0011 SW-846-8260B 0.0011 Non-detect SW-846-8260B 0.00027 Non-detect EPA Method 107 0.084 SW-846-8260B 0.00019 Non-detect SW-846-8260B 0.00024 Non-detect1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Complete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed.

4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column.

**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U U 5.18 0.179 0.321 U 0.017 Non-detect U 0.21 J 0.00059 U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.00021 Non-detect U U 0.0019 Non-detect U U 0.00023 Non-detect U J 0.00048 J U 0.00023 Non-detect U U 0.0002 Non-detect U U 0.00021 Non-detect U U 0.00053 J 1.28 U 0.00023 Non-detect U 0.304 J 0.0019 1.52 0.0007 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion

See Lab Report

JB25204-1 **1**

221 40 01/07/13 **2**

220 42

JB25203-1 JB25203 See Lab Report 01/08/13

JB25204 Measured MeasuredU 0.00046 Non-detect U U 0.00023 Non-detect U U 0.00024 U 0.0015 U 0.0011 Non-detect U U 0.00027 Non-detect U 0.896 U 0.00019 Non-detect U U 0.00024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 2 15.9 0.117 0.547 0.075 1.37 0.017 Non-detect U 0.017 Non-detect 0.0984 0.802 0.00059 Non-detect U 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.00021 Non-detect U 0.00021 Non-detect 0.0019 Non-detect U 0.0019 Non-detect 0.00023 Non-detect U 0.00023 Non-detect 0.00037 J 0.0004 0.00023 Non-detect U 0.00023 Non-detect 0.0002 Non-detect U 0.0002 Non-detect 0.00021 Non-detect U 0.00021 Non-detect 0.00045 Non-detect U 0.00061 0.526 0.521 0.00023 Non-detect U 0.00023 Non-detect 0.112 0.177 0.0006 J 0.00091 1.16 0.867 0.0032 0.0007 Non-detect

Suspension/Blending/Dispersion Suspension/Blending/Dispersion

See Lab Report

JB25205-1 JB25206-1 **3**

221 219.6 38 01/10/13 01/09/13

JB25205 JB25206 See Lab Report Measured Measured0.00049 J 0.00046 Non-detect

0.00029 J 0.00023 Non-detect 0.00024 Non-detect U 0.00024 Non-detect 0.0013 0.0011 0.0011 Non-detect U 0.0011 Non-detect 0.00027 Non-detect U 0.00027 Non-detect 13.185 7.601 0.00019 Non-detect U 0.00019 Non-detect 0.00024 Non-detect U 0.00024 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 0.847 0.123 0.0334 U 0.017 Non-detect U 0.0374 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0024 Non-detect U 0.0054 Non-detect U U 0.048 Non-detect U U 0.0056 Non-detect U J 0.0059 Non-detect U U 0.0057 Non-detect U U 0.0051 Non-detect U U 0.0052 Non-detect U J 0.011 Non-detect U 0.222 U 0.0057 Non-detect U 0.0679 J 0.0027 Non-detect U 0.425 U 0.018 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion

JB25206-1 JB25207-1 **4 5** 

219.6 221 39 40 01/10/13 01/11/13

JB25206 JB25207 See Lab Report See Lab Report Measured MeasuredU 0.012 Non-detect U U 0.0057 Non-detect U U 0.0059 Non-detect U 0.0072 Non-detect U U 0.028 Non-detect U U 0.0067 Non-detect U 0 6.841 0 U 0.0048 Non-detect U U 0.006 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 9.67 17.6 0.301 0.651 0.0243 0.793 0.017 Non-detect U 0.017 Non-detect 0.985 1.01 0.0011 J 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0054 Non-detect U 0.0054 Non-detect 0.048 Non-detect U 0.048 Non-detect 0.0056 Non-detect U 0.0056 Non-detect 0.0059 Non-detect U 0.0059 Non-detect 0.0057 Non-detect U 0.0057 Non-detect 0.0051 Non-detect U 0.0051 Non-detect 0.0052 Non-detect U 0.0052 Non-detect 0.011 Non-detect U 0.011 Non-detect 0.0527 1.24 0.0057 Non-detect U 0.0057 Non-detect 0.0723 0.549 0.0027 Non-detect U 0.0027 Non-detect 0.226 1.34 0.018 Non-detect U 0.018 Non-detect

Suspension/Blending/Dispersion Suspension/Blending/Dispersion

223 41

See Lab Report

JB25209-1 JB25210-1 01/15/13 01/16/13 **6**

JB25209 JB25210 See Lab Report Measured Measured0.012 Non-detect U 0.012 Non-detect

0.0057 Non-detect U 0.0057 Non-detect 0.0059 Non-detect U 0.0059 Non-detect 0.0072 Non-detect U 0.0072 Non-detect 0.028 Non-detect U 0.028 Non-detect 0.0067 Non-detect U 0.0067 Non-detect 6.793 0 7.205 0.0048 Non-detect U 0.0048 Non-detect 0.006 Non-detect U 0.006 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 0.045 Non-detect U 0.112 0.0371 U 0.017 Non-detect U 0.0389 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.0054 Non-detect U U 0.048 Non-detect U U 0.0056 Non-detect U U 0.0059 Non-detect U U 0.0057 Non-detect U U 0.0051 Non-detect U U 0.0052 Non-detect U U 0.011 Non-detect U 0.33 U 0.0057 Non-detect U 0.121 U 0.0027 Non-detect U 0.549 U 0.018 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion

42 38

See Lab Report See Lab Report

JB25210-1 01/16/13 01/17/13 **7 8** 

223 223

JB25210 JB25211 JB25211-1 Measured MeasuredU 0.012 Non-detect U U 0.0059 J U 0.0059 Non-detect U U 0.0072 Non-detect U U 0.028 Non-detect U U 0.0067 Non-detect U 6.565 U 0.0048 Non-detect U U 0.006 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 6.11 1.85 0.193 0.33 0.021 0.155 0.017 Non-detect U 0.017 Non-detect 0.591 0.0252 0.0015 J 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0054 Non-detect U 0.0054 Non-detect 0.048 Non-detect U 0.048 Non-detect 0.0056 Non-detect U 0.0056 Non-detect 0.0059 Non-detect U 0.0059 Non-detect 0.0057 Non-detect U 0.0057 Non-detect 0.0051 Non-detect U 0.0051 Non-detect 0.0052 Non-detect U 0.0052 Non-detect 0.011 Non-detect U 0.011 Non-detect 0.268 0.811 0.0057 Non-detect U 0.0057 Non-detect 0.073 0.415 0.0027 Non-detect U 0.0027 Non-detect 0.651 1.13 0.018 Non-detect U 0.018 Non-detect Suspension/Blending/Dispersion Suspension/Blending/Dispersion

Measured 39

See Lab Report Measured 01/18/13 01/21/13 **9**

224.5 See Lab Report JB25212 JB25212-1 JB25213-1 JB252130.012 Non-detect U 0.012 Non-detect

0.0057 Non-detect U 0.0057 Non-detect 0.0059 Non-detect U 0.0059 Non-detect 0.0072 Non-detect U 0.0072 Non-detect 0.028 Non-detect U 0.028 Non-detect 0.0067 Non-detect U 0.0067 Non-detect 6.479 4.861 0.0048 Non-detect U 0.0048 Non-detect 0.006 Non-detect U 0.006 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 0.01 Non-detect U 1.95 0.125 0.0477 U 0.017 Non-detect U 0.0581 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.0054 Non-detect U U 0.048 Non-detect U U 0.0056 Non-detect U U 0.0059 Non-detect U U 0.0057 Non-detect U U 0.0051 Non-detect U U 0.0052 Non-detect U U 0.011 Non-detect U 0.478 U 0.0057 Non-detect U 0.122 U 0.0027 Non-detect U 0.967 U 0.018 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion

Measured Measured 01/21/13 01/22/13 **11 10** 

222 See Lab Report 39 40

221 See Lab Report

JB25213-1 JB25214-1 JB25213 JB25214U 0.012 Non-detect U U 0.0057 Non-detect U U 0.0059 Non-detect U U 0.0072 Non-detect U U 0.028 Non-detect U U 0.0067 Non-detect U 7.447 U 0.0048 Non-detect U U 0.006 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 4.36 5.03 0.116 0.856 0.059 0.583 0.017 Non-detect U 0.017 Non-detect 0.595 0.0142 0.00059 U 0.0042 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.00021 Non-detect U 0.0021 Non-detect 0.0019 Non-detect U 0.019 Non-detect 0.00023 Non-detect U 0.0023 Non-detect 0.00086 J 0.0024 Non-detect 0.00023 Non-detect U 0.0023 Non-detect 0.0002 Non-detect U 0.002 Non-detect 0.00021 Non-detect U 0.0021 Non-detect 0.00095 J 0.0045 Non-detect 0.242 1.69 0.00023 Non-detect U 0.0023 Non-detect 0.0969 0.423 0.00011 Non-detect U 0.0011 Non-detect 0.565 1.77 0.0007 Non-detect U 0.007 Non-detect

Suspension/Blending/Dispersion Suspension/Blending/Dispersion

Measured Measured 01/28/13 **12** 02/04/13

37

223 See Lab Report See Lab Report

JB25215-1 JB25216-1 JB25216 JB252150.00046 Non-detect U 0.0046 Non-detect

0.00023 Non-detect U 0.0023 Non-detect 0.00024 Non-detect U 0.0024 Non-detect 0.00082 J 0.0029 Non-detect 0.0011 Non-detect U 0.011 Non-detect 0.00027 Non-detect U 0.0027 Non-detect 6.092 6.691 0.00019 Non-detect U 0.0019 Non-detect 0.00024 Non-detect U 0.0024 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 9.35 0.604 0.578 U 0.017 Non-detect U 0.38 0.0015 J U 0.005 Non-detect U U 0.0013 Non-detect U U 0.0021 Non-detect U U 0.019 Non-detect U U 0.0023 Non-detect U U 0.0024 Non-detect U U 0.0023 Non-detect U U 0.002 Non-detect U U 0.0021 Non-detect U U 0.0045 Non-detect U 0.675 U 0.0023 Non-detect U 0.184 U 0.0011 Non-detect U 1.01 U 0.007 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion

221 Measured Measured **13 14**  02/04/13 02/05/13

40 41

221 See Lab Report See Lab Report

JB25216-1 JB25217-1 JB25216 JB25217U 0.0046 Non-detect U U 0.0023 Non-detect U U 0.0024 Non-detect U U 0.0029 Non-detect U U 0.011 Non-detect U U 0.0027 Non-detect U 7.217 U 0.0019 Non-detect U U 0.0024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 0.045 Non-detect U 0.635 0.121 0.112 0.017 J 0.0558 0.017 Non-detect U 0.017 Non-detect 0.0247 0.04 0.001 J 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.011 Non-detect U 0.0043 Non-detect 0.095 Non-detect U 0.038 Non-detect 0.011 Non-detect U 0.0045 Non-detect 0.012 Non-detect U 0.0047 Non-detect 0.011 Non-detect U 0.0046 Non-detect 0.01 Non-detect U 0.0041 Non-detect 0.01 Non-detect U 0.0042 Non-detect 0.022 Non-detect U 0.0089 Non-detect 0.322 0.272 0.011 Non-detect U 0.0046 Non-detect 0.121 0.0962 0.0053 Non-detect U 0.0021 Non-detect 0.633 0.547 0.035 Non-detect U 0.014 Non-detect

Suspension/Blending/Dispersion Suspension/Blending/Dispersion

**15** 02/06/13 02/07/13

219 Measured Measured

See Lab Report JB25218 JB25219 JB25218-1 JB25219-1 See Lab Report 390.023 Non-detect U 0.0093 Non-detect 0.011 Non-detect U 0.0045 Non-detect 0.012 Non-detect U 0.0047 Non-detect 0.014 Non-detect U 0.0057 Non-detect 0.056 Non-detect U 0.022 Non-detect 0.013 Non-detect U 0.0054 Non-detect 7.831 9.898 0.0096 Non-detect U 0.0038 Non-detect 0.012 Non-detect U 0.0048 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 3.28 0.0422 0.0068 J U 0.017 Non-detect U 0.0418 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.00021 Non-detect U U 0.0019 Non-detect U U 0.00023 Non-detect U U 0.00073 J U 0.00023 Non-detect U U 0.0002 Non-detect U U 0.00021 Non-detect U U 0.00045 Non-detect U 0.619 U 0.00023 Non-detect U 0.184 U 0.001 Non-detect 0.946 U 0.0007 Non-detect U Suspension/Blending/Dispersion Suspension/Blending/Dispersion **17**

**16** 02/07/13 02/08/13

Measured Measured 221 222

JB25219 JB25220 JB25219-1 JB25220-1 See Lab Report See Lab Report 42 36U 0.00046 Non-detect U U 0.00023 Non-detect U U 0.00024 Non-detect U U 0.0009 Non-detect J U 0.0011 Non-detect U U 0.00027 Non-detect U 8.662 U 0.00019 Non-detect U U 0.00024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 4.4 7.14 0.952 0.217 0.492 0.0216 0.017 Non-detect U 0.017 Non-detect 0.0222 0.478 0.00059 Non-detect U 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0021 Non-detect U 0.0021 Non-detect 0.019 Non-detect U 0.019 Non-detect 0.0023 Non-detect U 0.0023 Non-detect 0.0024 Non-detect U 0.0024 Non-detect 0.0023 Non-detect U 0.0023 Non-detect 0.002 Non-detect U 0.002 Non-detect 0.0021 Non-detect U 0.0021 Non-detect 0.0045 Non-detect U 0.0045 Non-detect 1.84 0.769 0.0023 Non-detect U 0.0023 Non-detect 0.375 0.0961 0.0011 Non-detect U 0.0011 Non-detect 1.78 1.5 0.007 Non-detect U 0.007 Non-detect02/12/13 Suspension/Blending/Dispersion

Measured

See Lab Report JB25222 JB25222-1 Suspension/Blending/Dispersion

**18** 02/11/13

Measured 221 See Lab Report JB25221 JB25221-1 400.0046 Non-detect U 0.0046 Non-detect

0.0023 Non-detect U 0.0023 Non-detect 0.0024 Non-detect U 0.0024 Non-detect 0.0029 Non-detect U 0.0029 Non-detect 0.011 Non-detect U 0.011 Non-detect 0.0027 Non-detect U 0.0027 Non-detect 8.586 6.533 0.0019 Non-detect U 0.0019 Non-detect 0.0024 Non-detect U 0.0024 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 3.79 0.314 0.294 U 0.017 Non-detect U 0.0703 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.0021 Non-detect U U 0.019 Non-detect U U 0.0023 Non-detect U U 0.0024 Non-detect U U 0.0023 Non-detect U U 0.002 Non-detect U U 0.0021 Non-detect U U 0.0045 Non-detect U 0.797 U 0.0023 Non-detect U 0.225 U 0.0011 Non-detect U 1.24 U 0.007 Non-detect U **19** 02/12/13 Suspension/Blending/Dispersion

41 Measured 223 See Lab Report JB25222 JB25222-1 Suspension/Blending/Dispersion **20** 02/13/13

39 Measured 222 See Lab Report JB25223 JB25223-1U 0.0046 Non-detect U U 0.0023 Non-detect U U 0.0024 Non-detect U U 0.0029 Non-detect U U 0.011 Non-detect U U 0.0027 Non-detect U 9.583 U 0.0019 Non-detect U U 0.0024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 4.08 0.045 0.308 0.0972 0.274 0.0129 0.017 Non-detect U 0.017 Non-detect 0.021 0.0526 0.00059 Non-detect U 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0021 Non-detect U 0.0021 Non-detect 0.019 Non-detect U 0.019 Non-detect 0.0023 Non-detect U 0.0023 Non-detect 0.0024 Non-detect U 0.0024 Non-detect 0.0023 Non-detect U 0.0023 Non-detect 0.002 Non-detect U 0.002 Non-detect 0.0021 Non-detect U 0.0021 Non-detect 0.0045 Non-detect U 0.0045 Non-detect 1.06 0.307 0.0023 Non-detect U 0.0023 Non-detect 0.302 0.187 0.0011 Non-detect U 0.0011 Non-detect 1.3 0.713 0.007 Non-detect U 0.007 Non-detect JB25225-1 JB25224-1 Measured Measured 02/15/13 02/14/13

JB25225 Suspension/Blending/Dispersion Suspension/Blending/Dispersion

**21**

221

JB25224 See Lab Report See Lab Report 420.0046 Non-detect U 0.0046 Non-detect

0.0023 Non-detect U 0.0023 Non-detect 0.0024 Non-detect U 0.0024 Non-detect 0.0029 Non-detect U 0.0029 Non-detect 0.011 Non-detect U 0.011 Non-detect 0.0027 Non-detect U 0.0027 Non-detect 7.89 8.818 0.0019 Non-detect U 0.0019 Non-detect 0.0024 Non-detect U 0.0024 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U U 9.07 0.163 J 0.0221 U 0.017 Non-detect U 0.0644 U 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.00021 Non-detect U U 0.0019 Non-detect U U 0.00023 Non-detect U U 0.00059 J U 0.00023 Non-detect U U 0.0002 Non-detect U U 0.00021 Non-detect U U 0.00045 Non-detect U 0.196 U 0.00023 Non-detect U 0.0753 U 0.00011 Non-detect U 0.575 U 0.0007 Non-detect U JB25226-1 JB25225-1 Measured 220 02/15/13 02/19/13

JB25226 JB25225 Suspension/Blending/Dispersion Suspension/Blending/Dispersion

222 Measured

See Lab Report See Lab Report 39 40 **22 23** U 0.00046 Non-detect U U 0.00023 Non-detect U U 0.00024 Non-detect U U 0.00068 J U 0.0011 Non-detect U U 0.00027 Non-detect U 7.024 U 0.00019 Non-detect U U 0.00024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 25.2 12.2 0.607 0.138 0.912 0.0904 0.017 Non-detect U 0.017 Non-detect 0.188 0.569 0.00059 Non-detect U 0.00059 Non-detect 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0021 Non-detect U 0.0054 Non-detect 0.019 Non-detect U 0.048 Non-detect 0.0023 Non-detect U 0.0056 Non-detect 0.0024 Non-detect U 0.0059 Non-detect 0.0023 Non-detect U 0.0057 Non-detect 0.002 Non-detect U 0.0051 Non-detect 0.0021 Non-detect U 0.0052 Non-detect 0.0045 Non-detect U 0.011 Non-detect 0.726 0.67 0.0023 Non-detect U 0.0057 Non-detect 0.218 0.214 0.0011 Non-detect U 0.0027 Non-detect 0.67 0.86 0.007 Non-detect U 0.018 Non-detect JB25228-1 JB25227-1 Measured 223 02/25/13 02/20/13

37 Suspension/Blending/Dispersion Suspension/Blending/Dispersion

Measured

See Lab Report See Lab Report JB25227 JB25228 **24**0.0046 Non-detect U 0.012 Non-detect

0.0023 Non-detect U 0.0057 Non-detect 0.0024 Non-detect U 0.0059 Non-detect 0.0029 Non-detect U 0.0072 Non-detect 0.011 Non-detect U 0.028 Non-detect 0.0027 Non-detect U 0.0067 Non-detect 5.658 17.841 0.0019 Non-detect U 0.0048 Non-detect 0.0024 Non-detect U 0.006 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 0.01 Non-detect U 3.2 0.208 0.211 U 0.017 Non-detect U 0.0609 U 0.0012 J U 0.005 Non-detect U U 0.0013 Non-detect U U 0.00021 Non-detect U U 0.0019 Non-detect U U 0.00023 Non-detect U U 0.00093 J U 0.00023 Non-detect U U 0.0002 Non-detect U U 0.00021 Non-detect U U 0.00045 Non-detect U 0.638 U 0.00023 Non-detect U 0.377 U 0.0012 Non-detect 0.766 U 0.0007 Non-detect U JB25228-1 03/01/13 02/25/13

38 Suspension/Blending/Dispersion Suspension/Blending/Dispersion

Measured **26**

See Lab Report JB25228 **25**

39

222 221

JB25229-1 See Lab Report JB25229 MeasuredU 0.00046 Non-detect U U 0.00023 Non-detect U U 0.00024 Non-detect U U 0.0015 U 0.0011 Non-detect U U 0.00027 Non-detect U 7.874 U 0.00019 Non-detect U U 0.00024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 10 Non-detect 3.22 4.37 4.89 0.204 0.108 0.288 0.017 Non-detect U 0.017 Non-detect 0.0513 0.0832 0.0051 0.0011 0.005 Non-detect U 0.005 Non-detect 0.0013 Non-detect U 0.0013 Non-detect 0.0021 Non-detect U 0.00021 Non-detect 0.019 Non-detect U 0.0019 Non-detect 0.0023 Non-detect U 0.00023 Non-detect 0.0024 Non-detect U 0.00098 0.0023 Non-detect U 0.00023 Non-detect 0.002 Non-detect U 0.0002 Non-detect 0.0021 Non-detect U 0.00021 Non-detect 0.0076 J 0.00045 0.488 0.666 0.0023 Non-detect U 0.00023 Non-detect 0.245 0.338 0.0011 Non-detect U 0.0012 Non-detect 0.648 0.714 0.007 Non-detect U 0.0007 Non-detect

03/04/13 Suspension/Blending/Dispersion

38

223 03/05/13 Suspension/Blending/Dispersion

Measured

See Lab Report JB25231 JB25230-1 See Lab Report JB25230 Measured **27**

JB25231-10.0046 Non-detect U 0.00046 Non-detect

0.0023 Non-detect U 0.00023 Non-detect 0.0024 Non-detect U 0.00024 Non-detect 0.0029 Non-detect U 0.0015 0.011 Non-detect U 0.0011 Non-detect 0.0027 Non-detect U 0.00027 Non-detect 7.404 5.658 0.0019 Non-detect U 0.00019 Non-detect 0.0024 Non-detect U 0.00024 Non-detect**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

U 10 Non-detect U 2.38 0.163 0.0878 U 0.017 Non-detect U 0.0349 J 0.00059 Non-detect U U 0.005 Non-detect U U 0.0013 Non-detect U U 0.0021 Non-detect U U 0.019 Non-detect U U 0.0023 Non-detect U J 0.0024 Non-detect U U 0.0023 Non-detect U U 0.002 Non-detect U U 0.0021 Non-detect U U 0.0045 Non-detect U 0.457 U 0.0023 Non-detect U 0.179 0.0011 Non-detect U 0.606 U 0.007 Non-detect U 03/06/13 Suspension/Blending/Dispersion

39

222 **28** 03/05/13 Suspension/Blending/Dispersion

41 Measured 221 See Lab Report JB25231 JB25232-1 See Lab Report JB25232 Measured **29**

JB25231-1U 0.0046 Non-detect U U 0.0023 Non-detect U U 0.0024 Non-detect U 0.0029 Non-detect U U 0.011 Non-detect U U 0.0027 Non-detect U 6.653 U 0.0019 Non-detect U U 0.0024 Non-detect U**Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?** 

10 Non-detect U 1.97 0.209 0.0108 J 0.017 Non-detect U 0.0865 0.0014 J 0.005 Non-detect U 0.0013 Non-detect U 0.00021 Non-detect U 0.0019 Non-detect U 0.00023 Non-detect U 0.00055 J 0.00023 Non-detect U 0.0002 Non-detect U 0.00021 Non-detect U 0.00045 Non-detect U 0.232 0.00023 Non-detect U 0.0857 0.00011 Non-detect U 0.646 0.0007 Non-detect U

See Lab Report JB26507 Measured Suspension/Blending/Dispersion

JB26507-1 **30** 03/07/13

39

2210.00046 Non-detect U

0.00023 Non-detect U 0.00024 Non-detect U 0.00029 Non-detect U 0.0011 Non-detect U 0.00027 Non-detect U 7.069 0.00019 Non-detect U 0.00024 Non-detect U**Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s) 31**  **32 Concentration** 

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **33 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **34 35** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **36 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **37 38** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **39 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **40 41** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **42 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **43 44** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **45 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **46 47** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **48 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **49 50** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **51 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **52 53** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **54 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **55 56** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) Concentration**  **(ppmw) Non-Detect?**  **57 Note(s)**  **Concentration (ppmw)**  **Non-Detect? Note(s)**  **58 59** **Concentration**

**(ppmw) Non-Detect?**  **Note(s) 60**