08/04/09 PAGE: 1 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ AZ0022268 06 FREEPORT-MCMORAN BAGDAD, INC BAGDAD OPERATIONS COPPER CRK,MULHOLLAND WASH,MAMMOTH 01/31/13

001A BAGDAD NEW MILL - 001 +3436230 -11313049 P/F STATRE 96HR ACU DAPHNIA MAGNA DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN3C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 001A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 001A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 001A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 001A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 001A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 001A 12/31/08 01/26/09 E00 C PASS=0FAIL=1 9 0 001A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 001A 02/28/09 03/31/09 E00 C PASS=0FAIL=1 9 0 001A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 001A 04/30/09 05/29/09 E00 C PASS=0FAIL=1 9 0 001A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 001A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

P/F STATRE 96HR ACU PIMEPHALES PROMELAS DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN6C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 001A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 001A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 001A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 001A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 001A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 001A 12/31/08 01/26/09 E00 C PASS=0FAIL=1 9 0 001A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 001A 02/28/09 03/31/09 E00 C PASS=0FAIL=1 9 0 001A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 001A 04/30/09 05/29/09 E00 C PASS=0FAIL=108/04/09 PAGE: 2 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 001A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

TUC STAT 4DAY CHR SELEN. CAPRICORNUTUM DELMON ADDMON ADDMON CHRONCTOXCTY TTC1A 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 001A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 001A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 001A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 001A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 001A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 001A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 001A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 001A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 001A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 001A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 001A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 001A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STAT 7DAY CHR CERIODAPHNIA DUBIA DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTD3B 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 001A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 001A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 001A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 001A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 001A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 001A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 001A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 001A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 001A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 001A 04/30/09 05/29/09 E00 C CHRONCTOXCTY08/04/09 PAGE: 3 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 001A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STATRE 7DAY CHR PIMPHALES PROMELAS DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTP6C 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 001A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 001A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 001A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 001A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 001A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 001A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 001A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 001A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 001A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 001A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 001A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 001A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

PH DELMON DELMON 6.5 DELMON 9 SU 00400 1 EFFLUENT GROSS VALUE MINIMUM MAXIMUM 9 0 001A 06/30/08 07/25/08 E00 C SU 9 0 001A 07/31/08 08/29/08 E00 C SU 9 0 001A 08/31/08 09/29/08 E00 C SU 9 0 001A 09/30/08 10/24/08 E00 C SU 9 0 001A 10/31/08 11/24/08 E00 C SU 9 0 001A 11/30/08 12/19/08 E00 C SU 9 0 001A 12/31/08 01/26/09 E00 C SU 9 0 001A 01/31/09 02/27/09 E00 C SU 9 0 001A 02/28/09 03/31/09 E00 C SU 9 0 001A 03/31/09 04/20/09 E00 C SU 9 0 001A 04/30/09 05/29/09 E00 C SU08/04/09 PAGE: 4 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C SU 9 0 001A 06/30/09 07/24/09 E00 C SU

SOLIDS, TOTAL SUSPENDED DELMON DELMON DELMON 20 30 MG/L 00530 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C MG/L 9 0 001A 07/31/08 08/29/08 E00 C MG/L 9 0 001A 08/31/08 09/29/08 E00 C MG/L 9 0 001A 09/30/08 10/24/08 E00 C MG/L 9 0 001A 10/31/08 11/24/08 E00 C MG/L 9 0 001A 11/30/08 12/19/08 E00 C MG/L 9 0 001A 12/31/08 01/26/09 E00 C MG/L 9 0 001A 01/31/09 02/27/09 E00 C MG/L 9 0 001A 02/28/09 03/31/09 E00 C MG/L 9 0 001A 03/31/09 04/20/09 E00 C MG/L 9 0 001A 04/30/09 05/29/09 E00 C MG/L 9 0 001A 05/31/09 06/26/09 E00 C MG/L 9 0 001A 06/30/09 07/24/09 E00 C MG/L

CYANIDE, TOTAL (AS CN) DELMON DELMON DELMON ADDMON ADDMON UG/L 00720 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 5 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

SULFIDE, TOTAL (AS S) DELMON DELMON DELMON ADDMON ADDMON UG/L 00745 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

HARDNESS, TOTAL (AS CACO3) DELMON DELMON DELMON ADDMON ADDMON MG/L 00900 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C MG/L 9 0 001A 07/31/08 08/29/08 E00 C MG/L 9 0 001A 08/31/08 09/29/08 E00 C MG/L 9 0 001A 09/30/08 10/24/08 E00 C MG/L 9 0 001A 10/31/08 11/24/08 E00 C MG/L 9 0 001A 11/30/08 12/19/08 E00 C MG/L 9 0 001A 12/31/08 01/26/09 E00 C MG/L 9 0 001A 01/31/09 02/27/09 E00 C MG/L 9 0 001A 02/28/09 03/31/09 E00 C MG/L 9 0 001A 03/31/09 04/20/09 E00 C MG/L 9 0 001A 04/30/09 05/29/09 E00 C MG/L08/04/09 PAGE: 6 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C MG/L 9 0 001A 06/30/09 07/24/09 E00 C MG/L

ARSENIC, TOTAL RECOVERABLE DELMON DELMON DELMON 50 73 UG/L 00978 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

SELENIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00981 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 7 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

THALLIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00982 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

BERYLLIUM, TOTAL RECOVERABLE (AS BE) DELMON DELMON DELMON ADDMON ADDMON UG/L 00998 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 8 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

NICKEL TOTAL RECOVERABLE DELMON DELMON DELMON 85.2 171 UG/L 01074 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

SILVER TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01079 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 9 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

ZINC TOTAL RECOVERABLE DELMON DELMON DELMON 117 235 UG/L 01094 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

CADMIUM TOTAL RECOVERABLE DELMON DELMON DELMON 3.36 6.73 UG/L 01113 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 10 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

LEAD TOTAL RECOVERABLE DELMON DELMON DELMON 4.96 15.9 UG/L 01114 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM TOTAL RECOVERABLE DELMON DELMON DELMON 100 146 UG/L 01118 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 11 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

COPPER TOTAL RECOVERABLE DELMON DELMON DELMON 14.5 29.1 UG/L 01119 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM, HEXAVALENT DISSOLVED (AS CR) DELMON DELMON DELMON ADDMON ADDMON UG/L 01220 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L08/04/09 PAGE: 12 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

ANTIMONY, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01268 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

FLOW, IN CONDUIT OR THRU TREATMENT PLANT ADDMON ADDMON MGD DELMON DELMON DELMON 50050 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C MGD 9 0 001A 07/31/08 08/29/08 E00 C MGD 9 0 001A 08/31/08 09/29/08 E00 C MGD 9 0 001A 09/30/08 10/24/08 E00 C MGD 9 0 001A 10/31/08 11/24/08 E00 C MGD 9 0 001A 11/30/08 12/19/08 E00 C MGD 9 0 001A 12/31/08 01/26/09 E00 C MGD 9 0 001A 01/31/09 02/27/09 E00 C MGD 9 0 001A 02/28/09 03/31/09 E00 C MGD 9 0 001A 03/31/09 04/20/09 E00 C MGD 9 0 001A 04/30/09 05/29/09 E00 C MGD08/04/09 PAGE: 13 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 001A 05/31/09 06/26/09 E00 C MGD 9 0 001A 06/30/09 07/24/09 E00 C MGD

MERCURY TOTAL RECOVERABLE DELMON DELMON DELMON .01 .02 UG/L 71901 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 001A 06/30/08 07/25/08 E00 C UG/L 9 0 001A 07/31/08 08/29/08 E00 C UG/L 9 0 001A 08/31/08 09/29/08 E00 C UG/L 9 0 001A 09/30/08 10/24/08 E00 C UG/L 9 0 001A 10/31/08 11/24/08 E00 C UG/L 9 0 001A 11/30/08 12/19/08 E00 C UG/L 9 0 001A 12/31/08 01/26/09 E00 C UG/L 9 0 001A 01/31/09 02/27/09 E00 C UG/L 9 0 001A 02/28/09 03/31/09 E00 C UG/L 9 0 001A 03/31/09 04/20/09 E00 C UG/L 9 0 001A 04/30/09 05/29/09 E00 C UG/L 9 0 001A 05/31/09 06/26/09 E00 C UG/L 9 0 001A 06/30/09 07/24/09 E00 C UG/L

003A BAGDAD NEW MILL - 003 +3435020 -11315230 P/F STATRE 96HR ACU DAPHNIA MAGNA DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN3C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 003A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 003A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 003A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 003A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 003A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 003A 12/31/08 01/26/09 E00 C PASS=0FAIL=1 9 0 003A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 003A 02/28/09 03/31/09 E00 C PASS=0FAIL=108/04/09 PAGE: 14 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 003A 04/30/09 05/29/09 E00 C PASS=0FAIL=1 9 0 003A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 003A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

P/F STATRE 96HR ACU PIMEPHALES PROMELAS DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN6C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 003A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 003A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 003A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 003A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 003A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 003A 12/31/08 01/26/09 E00 C PASS=0FAIL=1 9 0 003A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 003A 02/28/09 03/31/09 E00 C PASS=0FAIL=1 9 0 003A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 003A 04/30/09 05/29/09 E00 C PASS=0FAIL=1 9 0 003A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 003A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

TUC STAT 4DAY CHR SELEN. CAPRICORNUTUM DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTC1A 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 003A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 003A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 003A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 003A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 003A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 003A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 003A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 003A 02/28/09 03/31/09 E00 C CHRONCTOXCTY08/04/09 PAGE: 15 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 003A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 003A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 003A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STAT 7DAY CHR CERIODAPHNIA DUBIA DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTD3B 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 003A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 003A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 003A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 003A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 003A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 003A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 003A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 003A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 003A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 003A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 003A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 003A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STATRE 7DAY CHR PIMPHALES PROMELAS DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTP6C 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 003A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 003A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 003A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 003A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 003A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 003A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 003A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 003A 02/28/09 03/31/09 E00 C CHRONCTOXCTY08/04/09 PAGE: 16 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 003A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 003A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 003A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

PH DELMON DELMON 6.5 DELMON 9 SU 00400 1 EFFLUENT GROSS VALUE MINIMUM MAXIMUM 9 0 003A 06/30/08 07/25/08 E00 C SU 9 0 003A 07/31/08 08/29/08 E00 C SU 9 0 003A 08/31/08 09/29/08 E00 C SU 9 0 003A 09/30/08 10/24/08 E00 C SU 9 0 003A 10/31/08 11/24/08 E00 C SU 9 0 003A 11/30/08 12/19/08 E00 C SU 9 0 003A 12/31/08 01/26/09 E00 C SU 9 0 003A 01/31/09 02/27/09 E00 C SU 9 0 003A 02/28/09 03/31/09 E00 C SU 9 0 003A 03/31/09 04/20/09 E00 C SU 9 0 003A 04/30/09 05/29/09 E00 C SU 9 0 003A 05/31/09 06/26/09 E00 C SU 9 0 003A 06/30/09 07/24/09 E00 C SU

SOLIDS, TOTAL SUSPENDED DELMON DELMON DELMON ADDMON ADDMON MG/L 00530 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C MG/L 9 0 003A 07/31/08 08/29/08 E00 C MG/L 9 0 003A 08/31/08 09/29/08 E00 C MG/L 9 0 003A 09/30/08 10/24/08 E00 C MG/L 9 0 003A 10/31/08 11/24/08 E00 C MG/L 9 0 003A 11/30/08 12/19/08 E00 C MG/L 9 0 003A 12/31/08 01/26/09 E00 C MG/L 9 0 003A 01/31/09 02/27/09 E00 C MG/L 9 0 003A 02/28/09 03/31/09 E00 C MG/L08/04/09 PAGE: 17 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C MG/L 9 0 003A 04/30/09 05/29/09 E00 C MG/L 9 0 003A 05/31/09 06/26/09 E00 C MG/L 9 0 003A 06/30/09 07/24/09 E00 C MG/L

CYANIDE, TOTAL (AS CN) DELMON DELMON DELMON ADDMON ADDMON UG/L 00720 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

SULFIDE, TOTAL (AS S) DELMON DELMON DELMON ADDMON ADDMON UG/L 00745 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 18 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

HARDNESS, TOTAL (AS CACO3) DELMON DELMON DELMON ADDMON ADDMON MG/L 00900 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C MG/L 9 0 003A 07/31/08 08/29/08 E00 C MG/L 9 0 003A 08/31/08 09/29/08 E00 C MG/L 9 0 003A 09/30/08 10/24/08 E00 C MG/L 9 0 003A 10/31/08 11/24/08 E00 C MG/L 9 0 003A 11/30/08 12/19/08 E00 C MG/L 9 0 003A 12/31/08 01/26/09 E00 C MG/L 9 0 003A 01/31/09 02/27/09 E00 C MG/L 9 0 003A 02/28/09 03/31/09 E00 C MG/L 9 0 003A 03/31/09 04/20/09 E00 C MG/L 9 0 003A 04/30/09 05/29/09 E00 C MG/L 9 0 003A 05/31/09 06/26/09 E00 C MG/L 9 0 003A 06/30/09 07/24/09 E00 C MG/L

ARSENIC, TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 00978 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 19 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

SELENIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00981 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

THALLIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00982 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 20 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

BERYLLIUM, TOTAL RECOVERABLE (AS BE) DELMON DELMON DELMON ADDMON ADDMON UG/L 00998 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

NICKEL TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01074 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 21 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

SILVER TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01079 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

ZINC TOTAL RECOVERABLE DELMON DELMON ADDMON UG/L 01094 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 22 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

CADMIUM TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01113 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

LEAD TOTAL RECOVERABLE DELMON DELMON DELMON 4.97 9.97 UG/L 01114 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 23 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01118 1 EFFLUENT GROSS VALUE DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

COPPER TOTAL RECOVERABLE DELMON DELMON DELMON 14.5 29.1 UG/L 01119 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 24 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM, HEXAVALENT DISSOLVED (AS CR) DELMON DELMON DELMON ADDMON ADDMON UG/L 01220 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

ANTIMONY, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01268 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 25 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

FLOW, IN CONDUIT OR THRU TREATMENT PLANT ADDMON ADDMON MGD DELMON DELMON DELMON 50050 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C MGD 9 0 003A 07/31/08 08/29/08 E00 C MGD 9 0 003A 08/31/08 09/29/08 E00 C MGD 9 0 003A 09/30/08 10/24/08 E00 C MGD 9 0 003A 10/31/08 11/24/08 E00 C MGD 9 0 003A 11/30/08 12/19/08 E00 C MGD 9 0 003A 12/31/08 01/26/09 E00 C MGD 9 0 003A 01/31/09 02/27/09 E00 C MGD 9 0 003A 02/28/09 03/31/09 E00 C MGD 9 0 003A 03/31/09 04/20/09 E00 C MGD 9 0 003A 04/30/09 05/29/09 E00 C MGD 9 0 003A 05/31/09 06/26/09 E00 C MGD 9 0 003A 06/30/09 07/24/09 E00 C MGD

MERCURY TOTAL RECOVERABLE DELMON DELMON DELMON .01 .02 UG/L 71901 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 003A 06/30/08 07/25/08 E00 C UG/L 9 0 003A 07/31/08 08/29/08 E00 C UG/L 9 0 003A 08/31/08 09/29/08 E00 C UG/L 9 0 003A 09/30/08 10/24/08 E00 C UG/L 9 0 003A 10/31/08 11/24/08 E00 C UG/L 9 0 003A 11/30/08 12/19/08 E00 C UG/L 9 0 003A 12/31/08 01/26/09 E00 C UG/L 9 0 003A 01/31/09 02/27/09 E00 C UG/L 9 0 003A 02/28/09 03/31/09 E00 C UG/L08/04/09 PAGE: 26 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 003A 03/31/09 04/20/09 E00 C UG/L 9 0 003A 04/30/09 05/29/09 E00 C UG/L 9 0 003A 05/31/09 06/26/09 E00 C UG/L 9 0 003A 06/30/09 07/24/09 E00 C UG/L

006A BAGDAD NEW MILL - 006 +3435070 -11317019 P/F STATRE 96HR ACU DAPHNIA MAGNA DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN3C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 006A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 006A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 006A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 006A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 006A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 006A 12/31/08 01/26/09 E00 C PASS=0FAIL=1 9 0 006A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 006A 02/28/09 03/31/09 E00 C PASS=0FAIL=1 9 0 006A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 006A 04/30/09 05/29/09 E00 C PASS=0FAIL=1 9 0 006A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 006A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

P/F STATRE 96HR ACU PIMEPHALES PROMELAS DELMON DELMON DELMON DELMON ADDMON PASS=0FAIL=1 TGN6C 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C PASS=0FAIL=1 9 0 006A 07/31/08 08/29/08 E00 C PASS=0FAIL=1 9 0 006A 08/31/08 09/29/08 E00 C PASS=0FAIL=1 9 0 006A 09/30/08 10/24/08 E00 C PASS=0FAIL=1 9 0 006A 10/31/08 11/24/08 E00 C PASS=0FAIL=1 9 0 006A 11/30/08 12/19/08 E00 C PASS=0FAIL=1 9 0 006A 12/31/08 01/26/09 E00 C PASS=0FAIL=108/04/09 PAGE: 27 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C PASS=0FAIL=1 9 0 006A 02/28/09 03/31/09 E00 C PASS=0FAIL=1 9 0 006A 03/31/09 04/20/09 E00 C PASS=0FAIL=1 9 0 006A 04/30/09 05/29/09 E00 C PASS=0FAIL=1 9 0 006A 05/31/09 06/26/09 E00 C PASS=0FAIL=1 9 0 006A 06/30/09 07/24/09 E00 C PASS=0FAIL=1

TUC STAT 4DAY CHR SELEN. CAPRICORNUTUM DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTC1A 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 006A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 006A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 006A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 006A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 006A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 006A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 006A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 006A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 006A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 006A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 006A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 006A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STAT 7DAY CHR CERIODAPHNIA DUBIA DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTD3B 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 006A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 006A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 006A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 006A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 006A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 006A 12/31/08 01/26/09 E00 C CHRONCTOXCTY08/04/09 PAGE: 28 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 006A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 006A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 006A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 006A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 006A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

TUC STATRE 7DAY CHR PIMPHALES PROMELAS DELMON DELMON DELMON ADDMON ADDMON CHRONCTOXCTY TTP6C 1 EFFLUENT GROSS VALUE MO MED DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C CHRONCTOXCTY 9 0 006A 07/31/08 08/29/08 E00 C CHRONCTOXCTY 9 0 006A 08/31/08 09/29/08 E00 C CHRONCTOXCTY 9 0 006A 09/30/08 10/24/08 E00 C CHRONCTOXCTY 9 0 006A 10/31/08 11/24/08 E00 C CHRONCTOXCTY 9 0 006A 11/30/08 12/19/08 E00 C CHRONCTOXCTY 9 0 006A 12/31/08 01/26/09 E00 C CHRONCTOXCTY 9 0 006A 01/31/09 02/27/09 E00 C CHRONCTOXCTY 9 0 006A 02/28/09 03/31/09 E00 C CHRONCTOXCTY 9 0 006A 03/31/09 04/20/09 E00 C CHRONCTOXCTY 9 0 006A 04/30/09 05/29/09 E00 C CHRONCTOXCTY 9 0 006A 05/31/09 06/26/09 E00 C CHRONCTOXCTY 9 0 006A 06/30/09 07/24/09 E00 C CHRONCTOXCTY

PH DELMON DELMON 6.5 DELMON 9 SU 00400 1 EFFLUENT GROSS VALUE MINIMUM MAXIMUM 9 0 006A 06/30/08 07/25/08 E00 C SU 9 0 006A 07/31/08 08/29/08 E00 C SU 9 0 006A 08/31/08 09/29/08 E00 C SU 9 0 006A 09/30/08 10/24/08 E00 C SU 9 0 006A 10/31/08 11/24/08 E00 C SU 9 0 006A 11/30/08 12/19/08 E00 C SU 9 0 006A 12/31/08 01/26/09 E00 C SU08/04/09 PAGE: 29 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C SU 9 0 006A 02/28/09 03/31/09 E00 C SU 9 0 006A 03/31/09 04/20/09 E00 C SU 9 0 006A 04/30/09 05/29/09 E00 C SU 9 0 006A 05/31/09 06/26/09 E00 C SU 9 0 006A 06/30/09 07/24/09 E00 C SU

SOLIDS, TOTAL SUSPENDED DELMON DELMON DELMON 20 30 MG/L 00530 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C MG/L 9 0 006A 07/31/08 08/29/08 E00 C MG/L 9 0 006A 08/31/08 09/29/08 E00 C MG/L 9 0 006A 09/30/08 10/24/08 E00 C MG/L 9 0 006A 10/31/08 11/24/08 E00 C MG/L 9 0 006A 11/30/08 12/19/08 E00 C MG/L 9 0 006A 12/31/08 01/26/09 E00 C MG/L 9 0 006A 01/31/09 02/27/09 E00 C MG/L 9 0 006A 02/28/09 03/31/09 E00 C MG/L 9 0 006A 03/31/09 04/20/09 E00 C MG/L 9 0 006A 04/30/09 05/29/09 E00 C MG/L 9 0 006A 05/31/09 06/26/09 E00 C MG/L 9 0 006A 06/30/09 07/24/09 E00 C MG/L

CYANIDE, TOTAL (AS CN) DELMON DELMON DELMON ADDMON ADDMON UG/L 00720 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 30 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

SULFIDE, TOTAL (AS S) DELMON DELMON DELMON ADDMON ADDMON UG/L 00745 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

HARDNESS, TOTAL (AS CACO3) DELMON DELMON DELMON ADDMON ADDMON MG/L 00900 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C MG/L 9 0 006A 07/31/08 08/29/08 E00 C MG/L 9 0 006A 08/31/08 09/29/08 E00 C MG/L 9 0 006A 09/30/08 10/24/08 E00 C MG/L 9 0 006A 10/31/08 11/24/08 E00 C MG/L 9 0 006A 11/30/08 12/19/08 E00 C MG/L 9 0 006A 12/31/08 01/26/09 E00 C MG/L08/04/09 PAGE: 31 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C MG/L 9 0 006A 02/28/09 03/31/09 E00 C MG/L 9 0 006A 03/31/09 04/20/09 E00 C MG/L 9 0 006A 04/30/09 05/29/09 E00 C MG/L 9 0 006A 05/31/09 06/26/09 E00 C MG/L 9 0 006A 06/30/09 07/24/09 E00 C MG/L

ARSENIC, TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 00978 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

SELENIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00981 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 32 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

THALLIUM, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 00982 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

BERYLLIUM, TOTAL RECOVERABLE (AS BE) DELMON DELMON DELMON ADDMON ADDMON UG/L 00998 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 33 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

NICKEL TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01074 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

SILVER TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01079 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 34 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

ZINC TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01094 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

CADMIUM TOTAL RECOVERABLE DELMON DELMON DELMON 3.25 7.01 UG/L 01113 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 35 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

LEAD TOTAL RECOVERABLE DELMON DELMON DELMON 4.97 9.97 UG/L 01114 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM TOTAL RECOVERABLE DELMON DELMON DELMON DELMON ADDMON UG/L 01118 1 EFFLUENT GROSS VALUE DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 36 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

COPPER TOTAL RECOVERABLE DELMON DELMON DELMON 15.3 28.2 UG/L 01119 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

CHROMIUM, HEXAVALENT DISSOLVED (AS CR) DELMON DELMON DELMON ADDMON ADDMON UG/L 01220 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L08/04/09 PAGE: 37 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

ANTIMONY, TOTAL RECOVERABLE DELMON DELMON DELMON ADDMON ADDMON UG/L 01268 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L

FLOW, IN CONDUIT OR THRU TREATMENT PLANT ADDMON ADDMON MGD DELMON DELMON DELMON 50050 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C MGD 9 0 006A 07/31/08 08/29/08 E00 C MGD 9 0 006A 08/31/08 09/29/08 E00 C MGD 9 0 006A 09/30/08 10/24/08 E00 C MGD 9 0 006A 10/31/08 11/24/08 E00 C MGD 9 0 006A 11/30/08 12/19/08 E00 C MGD 9 0 006A 12/31/08 01/26/09 E00 C MGD08/04/09 PAGE: 38 MEASUREMENT VIOLATION REPORT WITH LIMITS FOR AZ0022268 (EFVIOQL6) QL ***************************************************************************************************************************** QL NPID SUBR RDF5 NAM1 NAM2 RWAT PERE

--------- ---- ---- ------------------------------ ------------------------------ ----------------------------------- -------- DSDG PIPE PHBC PLAT PLON
---- ------------------------------ -------- -------- --------- PRAM LQAV LQMX LQUC LCMN LCAV LCMX LCUC
---------------------------------------- -------- -------- ------------ -------- -------- -------- ------------ PRAM MLOC MLOC LQAS LQXS LCMS LCAS LCXS
----- ---- -------------------- -------- -------- -------- -------- -------- VIPQ VSEA VDSG MVDT DMRR MVIO NODI MQAV MQMX LQUC MCMN MCAV MCMX LCUC
---- ---- ---- -------- -------- ---- ---- -------- -------- ------------ -------- -------- -------- ------------ 9 0 006A 01/31/09 02/27/09 E00 C MGD 9 0 006A 02/28/09 03/31/09 E00 C MGD 9 0 006A 03/31/09 04/20/09 E00 C MGD 9 0 006A 04/30/09 05/29/09 E00 C MGD 9 0 006A 05/31/09 06/26/09 E00 C MGD 9 0 006A 06/30/09 07/24/09 E00 C MGD

MERCURY TOTAL RECOVERABLE DELMON DELMON DELMON .01 .02 UG/L 71901 1 EFFLUENT GROSS VALUE MO AVG DAILY MX 9 0 006A 06/30/08 07/25/08 E00 C UG/L 9 0 006A 07/31/08 08/29/08 E00 C UG/L 9 0 006A 08/31/08 09/29/08 E00 C UG/L 9 0 006A 09/30/08 10/24/08 E00 C UG/L 9 0 006A 10/31/08 11/24/08 E00 C UG/L 9 0 006A 11/30/08 12/19/08 E00 C UG/L 9 0 006A 12/31/08 01/26/09 E00 C UG/L 9 0 006A 01/31/09 02/27/09 E00 C UG/L 9 0 006A 02/28/09 03/31/09 E00 C UG/L 9 0 006A 03/31/09 04/20/09 E00 C UG/L 9 0 006A 04/30/09 05/29/09 E00 C UG/L 9 0 006A 05/31/09 06/26/09 E00 C UG/L 9 0 006A 06/30/09 07/24/09 E00 C UG/L SUB-TOTAL QUICK LOOK PRINT LINES: 1129 TOTAL QUICK LOOK PRINT LINES: 1129