Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet If you choose "other" please provide a description of the fuel in the Other Fuel Description column

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

measure.
EIA Facility Code Facility Name Boiler ID Fuel Type 1

7213 Clover 2 bituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

7213 Clover 2 As Received Higher Heating Value

7213 Clover 2 As Received % Moisture

7213 Clover 2 As Received % Ash

7213 Clover 2 As Received % Sulfur

7213 Clover 2 Dry basis Higher Heating Value

7213 Clover 2 Dry basis % Ash

7213 Clover 2 Dry basis % Sulfur

7213 Clover 2 Dry basis Antimony

7213 Clover 2 Dry basis Arsenic

7213 Clover 2 Dry basis Beryllium

7213 Clover 2 Dry basis Cadmium

7213 Clover 2 Dry basis Chlorine

7213 Clover 2 Dry basis Chromium

7213 Clover 2 Dry basis Cobalt

7213 Clover 2 Dry basis Fluorine

7213 Clover 2 Dry basis Lead

7213 Clover 2 Dry basis Manganese

7213 Clover 2 Dry basis Mercury

7213 Clover 2 Dry basis Nickel

7213 Clover 2 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D2015

ASTM D‐3173

ASTM D‐3174

ASTM D 4239

ASTM D2015

ASTM D‐3174

ASTM D 4239

SW 846 7041

SW 846 7060A

SW 846 6010B

SW 846 6010B

ASTM D4208

SW 846 6010B

SW 846 6010B

ASTM D3761

SW 846 6010B

SW 846 6010B

EPA 7473

SW 846 6010B

SW 846 7740
EIA Facility Code Facility Name Boiler ID

7213 Clover 2

Sample Number (minimum of 

3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received)

Unit 2 Run 1 PM/MTL-1 4/1/2010 4/1/2010 12902.00

Unit 2 Run 2 PM/MTL-2 4/1/2010 4/1/2010 13100.00

Unit 2 Run 1 PM/MTL-3 4/2/2010 4/2/2010 12608.00

 Fuel Testing Results
HAPs Test Group

Mercury and non‐mercury metalic HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 4.03 10.54 1.1 13400

Btu/lb 2.85 10.05 0.99 13500

Btu/lb 4 10.31 0.95 13100
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 10.98 1.15 240 ppm 0.079 ppm

Btu/lb 10.35 1.01 108 ppm 0.074 ppm

Btu/lb 10.74 0.99 1266 ppm 0.064 ppm
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

1.27 ppm 8.71 ppm < 5.00 ppm < 1.00 ppm 20.3

1.09 ppm 4.88 ppm < 5.00 ppm < 1.00 ppm 19.6

1.49 ppm 3.88 ppm < 5.00 ppm < 1.00 ppm 25
Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

ppm 11.7 ppm 25.7 ppm 16.7 ppm 2.7 ppm

ppm 10.1 ppm 25.4 ppm 14.5 ppm 2.38 ppm

ppm 12.1 ppm 18.9 ppm 20.3 ppm 2.76 ppm
Note the Proximate/Ultimate data below

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

93.8 ppm 8.95 ppm 3.55 10.98

61.6 ppm 8.41 ppm 2.4 10.35

54.3 ppm 12.5 ppm 3 10.74

Proximate Analyses, % by wt
w should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

78.99 5.13 1.47 1.15 2.28

78.96 5.11 1.45 1.01 3.11

77.1 5.19 1.41 0.99 4.57

Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID

7213 Clover 2

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

Unit 2 NDF-1 3/29/2010 3/29/2010 12278.00

Unit 2 Run 1 NDF‐AG(1)‐2 3/30/2010 3/30/2010 12570.00

Unit 2 Run 2 NDF‐AG(2)‐3 3/30/2010 3/30/2010 12291.00

Unit 2 Run 2 NDF‐4 4/1/2010 4/1/2010 12908.00

Unit 2 Run 2 NDF‐5 4/2/2010 4/2/2010 12671.00

 Fuel Testing Results
HAPs Test Group

Non‐dioxin/furan organic HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 7.69 9.91 1.01 13300

Btu/lb 6.04 9.22 1.08 13400

Btu/lb 7.22 10.23 1.14 13200

Btu/lb 4.69 9.47 1.07 13500

Btu/lb 4.18 9.91 0.93 13200
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 10.74 1.09 696 ppm 0.098 ppm

Btu/lb 9.82 1.15 1148 ppm 0.089 ppm

Btu/lb 11.03 1.23 1090 ppm 0.106 ppm

Btu/lb 9.94 1.12 318 ppm 0.07 ppm

Btu/lb 10.34 0.97 1017 ppm 0.052 ppm
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

1.34 ppm 10 ppm < 5.00 ppm < 1.00 ppm 21.3 ppm

0.92 ppm 11.2 ppm < 5.00 ppm < 1.00 ppm 20.2 ppm

1.16 ppm 10.9 ppm < 5.00 ppm < 1.00 ppm 20.4 ppm

1.41 ppm 7.09 ppm < 5.00 ppm < 1.00 ppm 20.4 ppm

1.55 ppm 4.25 ppm < 5.00 ppm < 1.00 ppm 24.6 ppm
Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

10.8 ppm 22.1 ppm 19.1 ppm 3.2 ppm 46.5 ppm

13.1 ppm 25.8 ppm 18.2 ppm 2.54 ppm 61.9 ppm

11.3 ppm 26 ppm 16.6 ppm 2.74 ppm 62.6 ppm

7.75 ppm 20.8 ppm 15.8 ppm 1.76 ppm 69.1 ppm

10.8 ppm 7.44 ppm 21.4 ppm 2.71 ppm 45.8 ppm
Note the Proximate/Ultimate data below should be rec

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen

10.8 ppm 6.75 10.74 78.29 5.09

9.98 ppm 5.2 9.82 78.6 5.1

9.34 ppm 6.4 11.03 77.78 5.09

9.32 ppm 3.85 9.94 79.39 5.2

13.1 ppm 2.7 10.34 76.16 5.12

Proximate Analyses, % by wt Ultim
corded on a dry basis (including ash).

Nitrogen Total Sulfur Oxygen

1.47 1.09 3.31

1.46 1.15 3.87

1.42 1.23 3.44

1.47 1.12 2.89

1.37 0.97 6.04

mate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID

7213 Clover 2

Sample Number (minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received)

Unit 2 Run 1 NDF-AG (1)-2 3/30/2010 3/30/2010 12570.00

Unit 2 Run 2 NDF-AG (2)-3 3/30/2010 3/30/2010 12291.00

Unit 2 Run 1 AG‐3 3/31/2010 3/31/2010 12584.00

 Fuel Testing Results
HAPs Test Group

Acid gas HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 6.04 9.22 1.08 13400

Btu/lb 7.22 10.23 1.14 13200

Btu/lb 6.62 9.17 1.22 13500
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 9.82 1.15 1148 ppm 0.089 ppm

Btu/lb 11.03 1.23 1090 ppm 0.106 ppm

Btu/lb 9.82 1.3 714 ppm 0.108 ppm
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

0.92 ppm 11.2 ppm < 5.00 ppm < 1.00 ppm 20.2 ppm

1.16 ppm 10.9 ppm < 5.00 ppm < 1.00 ppm 20.4 ppm

1.13 ppm 11 ppm < 5.00 ppm < 1.00 ppm 18.8 ppm
Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

13.1 ppm 25.8 ppm 18.2 ppm 2.54 ppm 61.9 ppm

11.3 ppm 26 ppm 16.6 ppm 2.74 ppm 62.6 ppm

7.91 ppm 23.8 ppm 15.7 ppm 2.18 ppm 47.3 ppm
Note the Proximate/Ultimate data below should be recorded on a

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen

9.98 ppm 5.2 9.82 78.6 5.1 1.46

9.34 ppm 6.4 11.03 77.78 5.09 1.42

9.22 ppm 5.55 9.82 79.19 5.08 1.46

Proximate Analyses, % by wt Ultimate Analys
a dry basis (including ash).

Total Sulfur Oxygen

1.15 3.87

1.23 3.44

1.3 3.15

ses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

7213 Clover 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the Proximate/U

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash

Proximate Analyses, % by w
ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

wt Ultimate Analyses, % by wt
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

ppm
re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm