# 2vo7053/ YIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIMIIIIIIIIIMI 

# ETAD

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Ecological and Toxicological Association of Dyes and Organic Pigments Manufacturers U .S. DYE MANUFACTURERS OPERATING COMMITTEE OF ETAD March 9, 2011 Document Control Office (7407 M) Office of Pollution Prevention and Toxics (OPPT) Environmental Protection Agency C.3 EPA East Building, RoomE6428 (202-564-8930) 1201 Constitution Avenue, NW -p -= `-'' Washington, DC 20460 Attention: TSCASection 4 Do 40 CFR 799

.5087 171%) Docket ID Number EPA-HQ-OPPT-2007-0531 To Whom

It May Concern: RE: Testing of Certain High Production Volume Chemicals; Second Group of Chemicals. Federal Register 76 (5), 1067-1093, January 7, 2011 . C .I . Leu__co Sulphur Black_11C AS No . 66241-11-0) . N co

On behalf of Clariant Corporation, ETAD submits this letter of intent to comply with the subject test rule for C

.I . Leuco Sulphur Black 1 (CAS No. 66241-11-0) . Clariant Corporation will supply test results data for the following required tests in compliance with the test rule and according to current OPPTS Harmonized Guidelines: 1 . Melting point: ASTM E 324-99 (capillary tube) or, if a freezing point: OECD 102 (melting point/melting range) . 2 . Boiling point : ASTM E 1719-05 (ebulliometry) . 3 . Vapor pressure: ASTME 1782-08 (thermal analysis) . 4 . N-Octanollwater partition coefficient (log 10 basis) or logKow by appropriate method as specified as Method A, 40 CRFR 799.6755 (shake flask) ; Method B, ASTN1 E 1147-92 (reapproved 2005) (liquid chromatography) ; or Method C, 40 CFR 799 .6756 (generator column) . 5 . Water solubility: By appropriate test method as specified as Method A, ASTM E 1148- 02 (reapproved 2008) (shake flask) ; Method B, 40 CFR 799.6784 (shake flask) ; Method C, 40 CFR 799.6784 (column elution) ; or Method D, 40 CFR 799.6786 (generator column) . 6. Environmental fate and pathways - ready biodegradation: According to ISO 10634:1995(E) guidance by one of the following: 1) ASTM E 1720-01 (reapproved 2008) (sealed vessel C02 production test) ; 2) ISO 14593:1999(E) (COZ headspace test) ; 3) ISO 7827:1994(E) (analysis of DOC) ; 4) ISO9408:1999(E) (determination of oxygen demand in a closed respirometer) ; 5) ISO 9439:1999(E) (C02 evolution test) ; 6) ISO 10707:1994(E) (closed bottle test) ; or 7) ISO 10708:1997(E) (two-phased closed bottle test) .

1850 M Street, N .W

., Suite 700 - Washington, D.C. 20036 " (202) 721-4100 " Fax (202) 296-8120 

## CONTAINS NOCBI7. Aquatic toxicity, depending on whether Test Group 1 or Test Group 2, as defined in the test rule. Test Group 1 : 1) Acute toxicity to fish, ASTM E 729-96 (reapproved 2007) ; 2) Acute toxicity to Daphnia, ASTME 729-96 (reapproved 2007) ; 3) Toxicity to plants (algae), ASTM

E 1218-04e' . Test Group 2 : 1) Chronic toxicity to Daphnia ASTME 1193-97 (reapproved 2004) ; 2) Toxicity to plants (algae), ASTM E 1218-04e' . 8 . Mammalian toxicity-acute, by either: 1 . Acute (up/down) oral toxicity (rat), ASTM E 1163-98 (reapproved 2002) or 2 . Acute (up/down) oral toxicity (rat), 40 CFR 799 .9110(d)(1)(i)(A) . 9 . Mammalian toxicity - genotoxicity: Bacterial reverse mutation test (in vitro), 40 CFR 799.9510 . 10 . Mammalian toxicity - genotoxicity (chromosomal damage) by any one of: 1 . !n vitro mammalian chromosome aberration, 40 CFR 799.9537 ; 2 . Mammalian bone marrow chromosomal aberration (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR 799.9538 ; or 3 . Mammalian erythrocyte microneucleus test (sampled in bone marrow) (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR 799 .9539 . 11 . Mammalian toxicity - repeated dose/reproduction/developmental by either: Combined repeated dose toxicity study with reproduction/developmental toxicity screening test, 40 CFR 799 .9365 or Reproduction/developmental toxicity screening test, 40 CFR 799.9355 and Repeated dose 28-day oral toxicity study in rodents, 40 CFR 799 .9305 . The Ecological and Toxicological Association of Dyes and Organic Pigments Manufactures (ETAD) is an international technical organization that addresses the health, environmental and safety aspects of the global colorants industry. Headquartered in Basel, Switzerland, its members include the leading colorant manufacturers in Europe, Asia, and North America. In North America, ETAD represents only the dyes industry. Clariant Corporation is a member of ETAD

. For further information concerning these plans to satisfy the requirements of the subject test rule, please contact the undersigned directly at 202-721-4154 or helmestCcr?_socma.com . 

# t 1 C . Tucker Helmes, Ph .D. Executive Director ETAD North America

# Clariant Clarient Corporation 4000 Monroe Road ChaHotbe, NC 28205 704.331 .7715 March 9, 2011 Dr. C . T . Helmes Executive Director ETAD North America 1850 M Street, NW

Suite 700 Washington, DC 20036 Tel 202-721-4154 / Fax 202-296-8120 helmestfto_c_ma.com Re: Testing of Certain High Production Volume Chemicals; Second Group of Chemicals. Federal Register 76 (5),1067-1093, January 7, 2011 . C .I . Leuco Sulphur Black 1 (CAS No. 66241-11-0) . 

### Dear Tucker : Clariant commits to comply with the subject test rule for C .I . Leuco Sulphur Black 1 (CAS No. 66241-11-0) . Please proceed with submitting the letter to EPA on behalf of Clariant Corporation. Sincerely, - 

# (A~O k- ~ Daria Church Head of Product Stewardship-NAp. 4



# ~SOCnnA Society of Chemical Manufacturers & Affiliates March 9, 2011 Document Control Office (7407 M) Office of Pollution Prevention and Toxics (OPPT) Environmental Protection Agency EPA East Building, RoomE6428 (202-564-8930) 1201 Constitution Avenue, NW Washington, DC 20460 Attention: TSCA Section 4 40 CFR 799

.5087 Docket ID Number EPA-HQ-OPPT-2007-0531 To WhomIt May Concern: RE : Testing of Certain High Production Volume Chemicals; Second Group of Chemicals. Federal Register 76 (5), 1067-1093, January 7, 2011 . C .I . Leuco Sulphur Black 1 (CAS No. 66241-11-0) . . . +

ru s .10

On behalf of C

.H. Patrick &Company, Inc., the Society of Chemical Manufacturers & Affiliates (SOCMA) submits this letter of intent to comply with the subject test rule for C .I . Leuco Sulphur Black 1 (CAS No. 66241-11-0) . C .H. Patrick & Company will supply test results data for the following required tests in compliance with the test rule and according to current OPPTS Harmonized Guidelines: 1 . Melting point : ASTME 324-99 (capillary tube) or, if a freezing point: OECD 102 (melting point/melting range) . 2 . Boiling point: ASTME 1719-05 (ebulliometry) . 3 . Vapor pressure: ASTM E 1782-08 (thermal analysis) . 4 . N-Octanol/water partition coefficient (log 10 basis) or logKo by appropriate method as specified as Method A, 40 CRFR 799 .6755 (shake flask) ; Method B, ASTM E 1147-92 (reapproved 2005) (liquid chromatography) ; or Method C, 40 CFR 799 .6756 (generator column) . 5 . Water solubility: By appropriate test method as specified as Method A, ASTM E 1148- 02 (reapproved 2008) (shake flask) ; Method B, 40 CFR 799.6784 (shake flask) ; Method C, 40 CFR 799.6784 (column elution) ; or Method D, 40 CFR 799 .6786 (generator column) . 6. Environmental fate and pathways - ready biodegradation: According to ISO 10634:1995(E) guidance by one of the following: 1) ASTM E 1720-01 (reapproved 2008) (sealed vessel COZ production test) ; 2) ISO 14593:1999(E) (COZ headspace test) ; 3) ISO 7827 :1994(E) (analysis of DOC) ; 4) ISO9408:1999(E) (determination of oxygen demand in a closed respirometer) ; 5) ISO 9439:1999(E) (COZ evolution test) ; 6) ISO 10707:1994(E) (closed bottle test) ; or 7) ISO 10708:1997(E) (two-phased closed bottle test) .

ChemStewards"

. 202-296-8556 - www .socma.com '"Im"'ISOCMA 1850 M St NW Suite 700 " Washington, DC 20036-5810 -Tel' . 202-721-4100 " Fax

.p. 5 

# SQCMA 7. Aquatic toxicity, depending on whether Test Group 1 or Test Group 2, as defined in the test rule. Test Group 1 : 1) Acute toxicity to fish, ASTM E 729-96 (reapproved 2007) ; 2) Acute toxicity to Daphnia, ASTM E 729-96 (reapproved 2007) ; 3) Toxicity to plants (algae), ASTM

E 1218-048' . Test Group 2 : 1) Chronic toxicity to Daphnia ASTM E 1193-97 (reapproved 2004) ; 2) Toxicity to plants (algae), ASTME 1218-04e' . 8 . Mammalian toxicity - acute, by either : 1 . Acute (up/down) oral toxicity (rat), ASTME 1163-98 (reapproved 2002) or 2. Acute (up/down) oral toxicity (rat), 40 CFR 799 .9110(d)(1)(i)(A) . 9 . Mammalian toxicity - genotoxicity: Bacterial reverse mutation test (in vitro), 40 CFR 799.9510

. 10. Mammalian toxicity - genotoxicity (chromosomal damage) by any one of: 1 . In vitro mammalian chromosome aberration, 40 CFR 799.9537; 2. Mammalian bone marrow chromosomal aberration (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR 799.9538; or 3

. Mammalian erythrocyte microneucleus test (sampled in bone marrow) (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR 799 .9539 . 11 . Mammalian toxicity - repeated dose/reproduction/developmental by either : Combined repeated dose toxicity study with reproduction/developmental toxicity screening test, 40 CFR 799.9365 or Reproduction/developmental toxicity screening test, 40 CFR 799.9355 and Repeated dose 28-day oral toxicity study in rodents, 40 CFR 799.9305 . Forfurther information concerning these plans to satisfy the requirements of the subject test rule, please contact the undersigned directly at 301-987-0924 or diloretoia-socma .com . Sincerely,

John DiLoreto Executive Director

(:ikemStewarcis .ow3PAO ;S,' ;rCMA 1850 N

¬ Sc Nb°V S<. .ic.c 700 " VV'ashmgcor, . DC "GOv6-S810 » ic1 ; 202-721 A100 - Fax : 202-296-8124 " wwv*~.s~cn,a .c~m

# C . N . PATRICK & CO

. . INC .

March 8 20?' Society of Chemical Manufacturers &Affiliates 1850 M Street NW

. Suite 700 

### Wasf7mgton DC 20036 Attention: TSCA Section 4 

### Docket ID Number EPA-HQ-OPPT-2007-0531 To Whom

It May Concern RE: Testing of Certain High Production Volume Chemicals: Second Group of Chemicals . Federal Register 76 (5) . 1067-1093 . January 7, 2011 . 

### L+euco Sulphur Btack 1 jCA3 No. 66241-11-0) This letter is to confirmthe intention of C H Patrick 8 Company Inc to compiy with the subject test rule for Leuco Sulphur Black (CAS No 6624' - s 1-0; as a member of a consortiumbeing formed and managed under the Society of Chemical Manufacturers and Affiliates (SOCIVIA) Stnc,erety Steven .t Mresbauer V P Chemicals & Environmental Control C H Patrick & Company Inc

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Document Control Office (7407 M) Office of Pollution Prevention and Toxics (OPPT) Environmental Protection Agency EPA East Building, RoomE6428 (202-564-8930) 1201 Constitution Avenue, NW Washington, DC 20460 Attention : TSCA Section 4 40 CFR 799.5087 Docket ID Number EPA-HQ-OPPT-2007-0531 To WhomIt May Concern: RE: Testing of Certain High Production Volume Chemicals; Second Group of Chemicals. Federal Register 76 (5), 1067-1093, January 7, 2011 . Castor oil, sutfated, sodiumsalt (CAS No. 68187-76-8) r ;

On behalf of the companies listed below, SOCMAsubmits this letter of intent to comply with the subject test rule for castor oil, sulfated, sodiumsalt (CAS No. 68187-76-8) . The listed companies have agreed to forma consortiumfor purposes of satisfying the testing requirements of the test rule. The consortiumis formed and managed under the Society of Chemical Manufacturers and Affiliates (SOCMA) . The consortiumwill conduct the following studies in compliance with the test rule and according to current OPPTS Harmonized Guidelines 1 . Melting point: ASTME 324-99 (capillary tube) or, if a freezing point : OECD 102 (melting point/melting range) . 2 . Boiling point: ASTM E 1719-05 (ebulliometry) . 3 . Aquatic toxicity, depending on whether Test Group 1 or Test Group 2, as defined in the test rule. Test Group 1 : 1) Acute toxicity to fish, ASTM E 729-96 (reapproved 2007) ; 2) Acute toxicity to Daphnia, ASTM E 729-96 (reapproved 2007) ; 3) Toxicity to plants (algae), ASTME 1218-04°' . Test Group 2 : 1) Chronic toxicity to Daphnia ASTM E 1193-97 (reapproved 2004) ; 2) Toxicity to plants (algae), ASTM E 1218-04e' . 4 . Mammalian toxicity - acute, by either : 1 . Acute (up/down) oral toxicity (rat), ASTM E 1163-98 (reapproved 2002) or 2 . Acute (up/down) oral toxicity (rat), 40 CFR 799 .9110(d)(1)(i)(A) . 5 . Mammalian toxicity - genotoxicity: Bacterial reverse mutation test (in vitro), 40 CFR 799.9510

. 6 . Mammalian toxicity - genotoxicity (chromosomal damage) by any one of: 1 . In vitro mammalian chromosome aberration, 40 CFR 799.9537; 2 . Mammalian bone marrow chromosomal aberration (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR

emStevvarii ; . " ranc~a .a.r SC

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# : SOCMA Soc+ety o' Chemical AffirIate.. March 9, 2011

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# SQCMA - 799.9538; or 3. Mammalian erythrocyte microneucleus test (sampled in bone marrow) (in vivo in mouse (preferred), rat, or Chinese hamster), 40 CFR 799.9539 . 7. Mammalian toxicity - repeated dose/reproduction/developmental by either: Combined repeated dose toxicity study with reproduction/developmental toxicity screening test, 40 CFR 799.9365 or Reproduction/developmental toxicity screening test, 40 CFR 799.9355 and Repeated dose 28-day oral toxicity study in rodents, 40 CFR 799.9305. The participating companies in the consortiumfor sulfated castor oil are: Emerald Performance Materials, LLC Manufacturers Chemicals, LLC Acopy of each company's letter of intent to participate in the consortiumis attached for reference. For further information about the consortiumor its plans to satisfy the requirements of the subject test rule, please contact the undersigned directly at 202-721-4154 or helmesta-socma .com

. Sincerely, 

## c~ ~ l.v~/61~v~~ C . Tucker Helmes, Ph .D. Executive Director

Chc r-r5tr'War tts P"' ; sr~sc 5~}CNMa 8~

.0 N' sr .'";~1v ~,a;rc 700 `v`Va~!iingt :~e . i~C2C}036-St~ i 0~ ~ic : ; : 202-7- I -4 10~ ~ Fax. 2'J?-296 8120 " v.rww .s~zcn,a. :.on-

# EmmW

Performance MateHab

James D . Tanzilli Director, Product Compliance Emerald Performance Materials, 2020 Front Street, Suite 100, Cuyahoga Falls, OH 44221 Telephone: 330.916.6725, Fax 330.916.6734, James .TanziIliMEmeraIdMater[sis .com 7 March 2011 Document Control officer (7407 M) Office of Pollution Prevention and Toxics (OPPT) Environmental Protection Agency 1200 Pennsylvania Ave., NW Washington, DC 20430-0001 Attention: TSCA Section 4 Docket ID Number EPA-HQ-OPPT-2007-0631 To WhomIt May Concern: RE: Testing of Certain High Production Volume Chemicals; Second Group of Chemicals. Federal Register 76 (6),1067-1093, January 7, 2011 . C astor oil, sulfated, sodium salt (CAS No. 68187-76-8) This letter is to confirmthe intention of Emerald Performance Materials, LLCto comply with the subject test rule for castor oil, sulfated, sodiumsalt (CAS No. 68187-76-8) as a member of a consortiumbeing formed and managed under the Society of Chemical Manufacturers and Affiliates (SOCMIA) . Sincerely,

James D . Tanzilli* Pt} . Boat 2'!!rd " TWO . (+1i8) !'T&8618 " ram(00) 4?S.'Ts"

-sow or wrwW

srsrti" .e+am March 7, 2011 Document Control officer (7407 M) Office ofPollution Prevention and Toxics (OPPT) Environmental Protection Agency 1200 Pennsylvania Ave

., NW Washington, DC 20430-0001 Attention: TSCA Section 4 Docket ID Number EPA-NO-OPPT-2007-)531 To Whom

It May Concem

: RE: Testing of Certain Nigh Production Volume Chemicals; Second Groupof Chemicals

. Federal Register 78(5), 1067-1093, January 7, 201! . Cestor ON, sWfaW

sodium salt (CAS No U187

, 7 0-8) This letter is to confirmthe intention of Manufacturers Chemicals, LLCto comply with the subject test nrle for castoror7, sulfated, sodfum soft (CAS No

. 68187-76-8) as a member ofa consortiumbeingformed and managed under the Society of Chemical Manufadumrs and Affiliates (SOCMA) .

Chuck Stieg President



## 100 ON SNIViNOO