Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2451 San Juan Unit 4 subbituminousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

2451 San Juan Unit 4 As Received Higher Heating Value 2451 San Juan Unit 4 As Received % Moisture 2451 San Juan Unit 4 Dry basis Higher Heating Value 2451 San Juan Unit 4 Dry basis Antim ony 2451 San Juan Unit 4 Dry basis Arsenic 2451 San Juan Unit 4 Dry basis Beryllium 2451 San Juan Unit 4 Dry basis Cadmium 2451 San Juan Unit 4 Dry basis Chlorine 2451 San Juan Unit 4 Dry basis Chromium 2451 San Juan Unit 4 Dry basis Cobalt 2451 San Juan Unit 4 Dry basis Fluorine 2451 San Juan Unit 4 Dry basis Lead 2451 San Juan Unit 4 Dry basis Manganese 2451 San Juan Unit 4 Dry basis Mercury 2451 San Juan Unit 4 Dry basis Nickel 2451 San Juan Unit 4 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D-5865 ASTM D-5865 ASTM D-5865 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010 ASTM D-6010EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2451 San Juan Unit 4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 5/19/2010 5/19/2010 9748.00 Btu/lb 2 5/19/2010 5/19/2010 9862.00 Btu/lb 3 5/20/2010 5/20/2010 10075.00 Btu/lb 4 5/20/2010 5/20/2010 10034.00 Btu/lb 5 5/21/2010 5/21/2010 9675.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Mercury (Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic

Units 5.67 10334 Btu/lb 0.065 mg/Kg 0.816 mg/Kg 8.6 10790 Btu/lb 0.09 mg/Kg 0.46 mg/Kg 8.46 11006 Btu/lb 0.04 mg/Kg 0.528 mg/Kg 9.12 11040 Btu/lb 0.041 mg/Kg 0.258 mg/Kg 7.82 10496 Btu/lb 0.048 mg/Kg 0.701 mg/KgBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 0.373 mg/Kg 0.037 mg/Kg 1.02 mg/Kg 4.81 mg/Kg 10.6 0.309 mg/Kg 0.051 mg/Kg 0.949 mg/Kg 4.09 mg/Kg 8.53 0.303 mg/Kg 0.036 mg/Kg 0.89 mg/Kg 3.79 mg/Kg 8.67 0.308 mg/Kg 0.048 mg/Kg 1.05 mg/Kg 3.73 mg/Kg 6.98 0.346 mg/Kg 0.04 mg/Kg 1.01 mg/Kg 4.29 mg/Kg 13.9Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units mg/Kg 1.4 mg/Kg 1.16 mg/Kg mg/Kg 1.07 mg/Kg 0.864 mg/Kg mg/Kg 1.18 mg/Kg 0.822 mg/Kg mg/Kg 1.13 mg/Kg 0.726 mg/Kg mg/Kg 1.26 mg/Kg 0.955 mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm