Method321TestingforHClatPortlandCementManufacturingPlantsAugust6,2010e Oconcentrillion voare belowthe dete10]).ExhaustStream%Moisture007680085700765%Worksheet Title:HCl Emission Test Results Template Using Method 321Who Should Complete this Spreadsheet?Facilities that use Method 321 to test for HClCompany Name:Lehigh Southwest Cement CompanyFacility Name:TehachapiAddress:13578 Tehachapi BlvdCity:TehachapiState:CAKiln ID:Kiln Type:PH/PCIn-line Raw Mill:YESControl Device Configuration:BaghouseParameter p le #1 Samp l p le #2 p le #3

Samp l Samp l erageUnits O ther

i ptionTest Method Used

Test Av Units Descri pEnter HClparts per mtest resultsplease note(e.g., [< 0.0ation value in drylume (ppmvd). If thedetection limit,ction limit in bracketsSelect appropriate unitfrom list. If other isselected please describeunits in column H at right.Enter the name of the Test Method used.Sample Date (mm/dd/yyyy)3/25/2010 3/27/2010 3/27/2010HCl Concentration - as measured - dry basis2.83 2.310.88ppmvdOxygen Concentration - dry basis13.38 11.7711.97%CO2 Concentration - dry basis13.96 16.4715.84%HCl Concentration - correctedto 7% oxygen5.243.52 1.363.37ppmvd@7% O2Method 321ExhaustStream%Moisture00768.0085700765%..Exhaust Flowrate168536177917 166377dscfmExhaust Temperature157.2165.5 160.4FSample Date(mm/dd/yyyy)3/25/2010 3/25/2010HCl Concentration - as measured - drybasis0.91 0.62ppmvdOxygen Concentration - drybasis12.62 13.28%CO2 Concentration - drybasis15.06 13.96%HCl Concentration - correctedto 7% oxygen1.531.131.33ppmvd@7% O2Method 321Exhaust Stream %Moisture0.02640.0311%Exhaust Flowrate178441167033dscfmExhaust Temperature278.5277.4FNotes:Peach shaded cells indicate areas where the user will enter a responseOnly two (2) runs were completed during Raw Mill Off condition due to numerousFTIR monitor and process problems.MillOnTest LocationNoteIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.Downstream; BaghouseMill OnMillOnMill OnMill OnDownstream; BaghouseMill OffMill OffMill OffMill Off# gParameter # #Units oTestUsedncentratiolume (plow detection lim0]).HCld7%d@321Worksheet Title:HCl Emission Test Results Template Using Method 321Who Should Complete this Spreadsheet?Facilities that use Method 321 to test for HClCompany Name:Lehigh Southwest Cement CompanyFacility Name:ReddingAddress:15390 Wonderland BlvdCity:ReddingState:CAKiln ID:1Kiln Type:PHIn-line Raw Mill:YesControl Device Configuration:In line Raw Mill/Kiln Baghouse (S260)Parameter # 1 Sample 2 Sample # 3 Sample e Test AveraUnits er o nTest Method Used

Units Oth e DescriptiMethodEnter HCl coper million vresults are benote the dete(e.g., [< 0.01on value in dry partspmvd). If the testction limit, pleaseit in bracketsSelect appropriate unitfrom list. If other isselected please describeunits in column H at right.Enter the name of the Test Method used.Sample Date (mm/dd/yyyy)3/16/2010 3/16/2010 3/16/2010HCl Concentration - as measured - drybasis3.00 1.671.60ppmvdOxygen Concentration - dry basis11.07 10.7211.60%CO2 Concentration - dry basis16.62 17.1815.92%HCloncentrationtedConcentration - correco7%ygentox4 2.42 22 3.9.92 9ppmvd@Method321.77%O2Exhaust Stream %Moisture14.015.3 15.5%Exhaust Flowrate133,025 135,639 133,951dscfmExhaust Temperature228.4227.9 218.0degrees FSample Date(mm/dd/yyyy)3/17/2010 3/17/2010 3/17/2010HCl Concentration - as measured - drybasis35.29 16.9815.91ppmvdOxygen Concentration - drybasis9.236 8.9148.966%CO2 Concentration - drybasis19.74 20.1620.29%HCl Concentration42.0519.69 18.5326.76ppmvd@7% O2Mthod 321Exhaust Stream %Moisture14.814.5 5.5%Exhaust Flowrate115,358 111,530 108,519dscfmExhaust Temperature280.0281.7 284.3degrees FNotes:Peach shaded cells indicate areas where the user will enter a responseTestNoteousTest LocationLocationIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.Downstream;aghouseDownstream;BaghRaw mill onRaw mill onRaw mill onRaw mill onDownstream; BaghouseRaw mill offRaw mill offRaw mill offRaw mill off# gParameter # #Units oTestUsedncentratiolume (pelow detection lim0]).HCld7%d@USEPA321Worksheet Title:HCl Emission Test Results Template Using Method 321Who Should Complete this Spreadsheet?Facilities that use Method 321 to test for HClCompany Name:Lafarge North AmericaFacility Name:Ravena Cement PlantAddress:1916 Route 9W, PO Box 3City:RavenaState:New YorkKiln ID:Kiln 1Kiln Type:WetIn-line Raw Mill:NoControl Device Configuration:Electrostatic PrecipitatorsParameter # 1 Sample 2 Sample # 3 Sample e TestUnits er o nTest Method Used

Avera Units Oth e DescriptiMethodEnter HCl coper million vresults are bnote the dete(e.g., [< 0.01on value in dry partspmvd). If the testction limit, pleaseit in bracketsSelect appropriate unitfrom list. If other isselected please describeunits in column H at right.Enter the name of the Test Method used.Sample Date (mm/dd/yyyy)3/12/2010 3/12/2010 3/12/2010HCl Concentration - as measured - drybasis30.2 26.9 33.5ppmvdOxygen Concentration - dry basis4.9 4.9 4.9%CO2 Concentration - dry basis18.6 18.3 17.9%HCloncentrationtedConcentration - correco7%toxygen26.223.4 29.1 2ppmvd@7%O2USEPAMethod3216.2ppmv7%O2MethodExhaust Stream %Moisture26.4 25.2 24.7%Exhaust Flowrate577,108 575,859 590,980acfmExhaust Temperature261,756 263,979 272,533dscfmNotes:Oxygen measurements were conducted at two locations - in the stackwhere the volumetric flow rate testing was conducted and in thebreaching, where the HCl testing was conducted. Oxygen data collected at the breachinglocation were used to correct HCl data to 7% O2. See report text for further detailsTestNoteLocationLocationIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.DownstreamDownstreamNASamples collected in stackbreaching. See report text for details.oncentratllion volure belowthe detec0]).Worksheet Title:HCl Emission Test Results Template Using Method 321Who Should Complete this Spreadsheet?Facilities that use Method 321 to test for HClCompany Name:Lafarge North AmericaFacility Name:AlpenaAddress:1435 Ford AvenueCity:AlpenaState:MichiganKiln ID:K23Kiln Type:Long DryIn-line Raw Mill:NoControl Device Configuration:Fabric FilterParameter Sample #1 Sample #2 Sample #3 Test AverageUnits Units Other Descriptio nTest Method UsedEnter HCl cparts per mitest results aplease note(e.g., [< 0.01ion value in dryme (ppmvd). If thedetection limit,tion limit in bracketsSelect appropriate unitfrom list. If other isselected please describeunits in column H at right.Enter the name of the Test Method used.Sample Date(mm/dd/yyyy)3/25/2010 3/25/2010 3/25/2010HCl Concentration - as measured - drybasis34.84 33.79 29.55ppmvdOxygen Concentration - drybasis6.22 5.96 6.18% (dry)CO2 Concentration - drybasis23.35 23.63 23.24% (dry)HCl Concentration - correctedto 7% oxygen32.9931.43 27.91 30.78ppmvd @ 7% O2Method 321Exhaust Stream %Moisture5.87 5.56 5.25%Exhaust Flowrate146090 144187 145502SCFMExhaust Temperature~ 400 ~ 400 ~ 400degrees FSample Date(mm/dd/yyyy)HCl Concentration - as measured - drybasisN/A N/dA N/AppmvdOxygen Concentration - drybasisN/A N/A N/A%CO2 Concentration - drybasisN/A N/A N/A%HCl ConcentrationN/A N/A N/Appmvd@7% O2Exhaust Stream %MoistureN/A N/A N/A%Exhaust FlowrateN/A N/A N/A(select flowrate units)Exhaust TemperatureN/A N/A N/A(select temperature units)Notes:Peach shaded cells indicate areas where the user will enter a responseTest LocationNoteIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.DownstreamNABased on preliminary Velocity Traverse on 3/24/2010oncentratllion volure belowthe detec0]).Worksheet Title:HCl Emission Test Results Template Using Method 321Who Should Complete this Spreadsheet?Facilities that use Method 321 to test for HClCompany Name:Lafarge North AmericaFacility Name:AlpenaAddress:1435 Ford AvenueCity:AlpenaState:MichiganKiln ID:K23Kiln Type:Long DryIn-line Raw Mill:NoControl Device Configuration:Fabric FilterParameter Sample #1 Sample #2 Sample #3 Test AverageUnits Units Other Descriptio nTest Method UsedEnter HCl cparts per mitest results aplease note(e.g., [< 0.01ion value in dryme (ppmvd). If thedetection limit,tion limit in bracketsSelect appropriate unitfrom list. If other isselected please describeunits in column H at right.Enter the name of the Test Method used.Sample Date(mm/dd/yyyy)3/25/2010 3/25/2010 3/25/2010HCl Concentration - as measured - drybasis34.84 33.79 29.55ppmvdOxygen Concentration - drybasis6.22 5.96 6.18% (dry)CO2 Concentration - drybasis23.35 23.63 23.24% (dry)HCl Concentration - correctedto 7% oxygen32.99 31.43 27.91ppmvd @ 7% O2Method 321Exhaust Stream %Moisture5.87 5.56 5.25%Exhaust Flowrate146090 144187 145502SCFMExhaust Temperature~ 400 ~ 400 ~ 400degrees FSample Date(mm/dd/yyyy)HCl Concentration - as measured - drybasisN/A N/dA N/AppmvdOxygen Concentration - drybasisN/A N/A N/A%CO2 Concentration - drybasisN/A N/A N/A%HCl ConcentrationN/A N/A N/Appmvd@7% O2Exhaust Stream %MoistureN/A N/A N/A%Exhaust FlowrateN/A N/A N/A(select flowrate units)Exhaust TemperatureN/A N/A N/A(select temperature units)Notes:Peach shaded cells indicate areas where the user will enter a responseTest LocationNoteIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.DownstreamNABased on preliminary Velocity Traverse on 3/24/2010concentravolume (. If the temit, pleasckets10]).000 79133TABLE 1.2 EPA REPORTING SPREADSHEETCompany Name:Lone Star Industries Inc.Facility Name:PRYOR CEMENT PLANTAddress:5 Mi E on 20 2 Mi S Co RdCity:PRYORState:OklahomaKiln ID:Kiln Number 3Kiln Type:Long DryIn-line Raw Mill:NoControl Device Configuration:BaghouseParameter a mple #1 Sa m a mple #2 a mple #3

Sa m Sa m Avg.UnitsTest Method UsedEnter HClper million7% oxygendetection lilimit in bra(e.g., [< 0.0tion value in dry pappmvd) corrected tost results are belowe note the detectionSelect appropriate unitfrom list. If other isselected please describeunits in column H at right. Enter the name of the Test Method used.rtsSample Date (mm/dd/yyyy)2/24/2010 2/24/2010 2/24/2010HCl Concentration - as measured - WetBasis7.86.5 5.96.7ppmv WetM321HCl Concentration Dry Basis8.26.8 6.27.1ppm v DryM321Oxygen Concentration - dry basis12.112.7 12.412.4 %M3ACO2 Concentration - dry basis13.712.6 13.213.2 %M3AHCl Concentration - dry corrected to 7%oxygen13.011.5 10.111.5ppm v dryat 7% O2M321Exhaust Stream %Moisture4.94.6 4.64.7 %M320 and M4E hFlxaust Flowrate77,800280000,4 77,279133M123Ad4dscfm1, 2, 3A and 4Exhaust Temperature372370 389377 FT/CNotes:Method 320 data used for moisture results reporting.Test LocationNoteIndicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyother information supportinginformation you think is necessaryabout this test report.Downstream of BaghouseOff Line Raw MillDownstream of BaghouseOff Line Raw MillDownstream of BaghouseOff Line Raw MillDownstream of BaghouseOff Line Raw MillDownstream of BaghouseOff Line Raw MillDownstream of BaghouseOff Line Raw MillD tfBhownsream of BaghouseOffLiRMillLine Raw MillDownstream of BaghouseOff Line Raw Millncentratme (ppmtfit t uls arebldlilction lim0]).HClConcentrationdrycorrectedto7%oxygen96910809551001ppmvdryat7%O2M321TABLE 1.2 EPA REPORTING SPREADSHEETCompany Name:California Portland Cement Co.Facility Name:Mojave FacilityAddress:9350 Oak Creek Rd Mojave CA 93501City:Mojave FacilityState:CaliforniaKiln ID:Kiln 1Kiln Type:Pre-Heater/ Pre-CalcinerIn-line Raw Mill:YesControl Device Configuration:BaghouseParameter Sam ple #1 Sam ple #2 Sam ple #3 Avg .UnitsTest Method UsedEPA InstructionsEnter HCl comillion voluIfhttte es resnote the dete(e.g., [< 0.01ion value in dry parvd) corrected to 7%bldttilie ow etecton mit in bracketsSelect appropriate unitflitIfthits peroxygen.itlromlist. Ifother sselected please describeunits in column H at right. Enter the name of the Test Method used.it, p easeSample Date(mm/dd/yyyy)3/30/2010 3/30/2010 3/30/2010HCl Concentration - as measured - WetBasis6.36.35.8 6.1ppmv WetM321HCl Concentration Dry Basis6.96.96.3 6.7ppm v DryM321Oxygen Concentration - dry basis12.4212.07 11.92 12.1 %M3ACO2 Concentration - dry basis19.119.119.1 19.1 %M3AHCl Concentration - dry corrected to 7% oxygen11.210.89.8 10.6ppm v dryat 7% O2M321Exhaust Stream %Moisture8.28.28.2 8.2 %M320Exhaust Flowrate259,488259,249 253,513 257,417 dscfmM1, 2, 3A, 320Exhaust Temperature219230230226 FT/CSample Date(mm/dd/yyyy)3/31/2010 3/31/2010 3/31/2010HCl Concentration - as measured - WetBasis57.366.868.1 64.1ppmv WetM321HCl Concentration Dry Basis59.969.971.0 67.0ppm v DryM321Oxygen Concentration - dry basis12.311.9 10.56 11.6 %M3ACO2 Concentration - dry basis21.716.719.7 19.3 %M3AHClConcentrationdrycorrectedto-7%oxygen969.1080.9551001ppmvdryat7%O2M321..Exhaust Stream %Moisture4.44.54.1 4.3 %M320Exhaust Flowrate218,776200,306 214,974 211,352 dscfmM1, 2, 3A, 320Exhaust Temperature354411410392 FT/CNotes:Method 320 data used for moisture and CO2 results reporting.flifDownstreamofBaghouseTest LocationNoteIndicate whether the testoccurred upstream ord tflownsream o a controdevice(s); list the controldevice(s)If kiln has an in-line raw mill, indicateraw mill status during tests (i.e., rawmill on or raw mill off). Provide anyhifiioter n ormaton supportnginformation you think is necessaryabout this test report.Downstream of BaghouseRaw Mill OnDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseRaw Mill OffDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseDownstreamofBaghouseDownstream of BaghouseDownstream of BaghouseDownstream of BaghouseMethod321TestLonestar,Pryor,OKAugust6,2010ter HClmillionoxygenection liit in bra., [< 0.0TABLE 1.2 EPA REPORTINGSPREADSHEETCompanyName:Lone Star Industries Inc.FacilityName:PRYOR CEMENT PLANTAddress:5 Mi E on 20 2 Mi S Co RdCity:PRYORState:OklahomaKiln ID:Kiln Number 3Kiln Type:Long DryIn-line Raw Mill:NoControl Device Configuration:BaghouseParameter Sample #1 Sample #2 Sample #3 Avg.UnitsTest Method UsedTest LocationNoteEnper7%detlim(e.gconcentration valuvolume (ppmvd). If the test resultsmit, please note thckets10]).e in dry partscorrected toare belowe detectionSelect appropriatefrom list. If otherselected please deunits in column Hunitisscribeat right. Enter the name of the Test Method used.Indicate whether the testoccurred upstream ordownstream of a controldevice(s); list the controldevice(s)If kiln has an in-line raw mill,indicate raw mill status during tests(i.e., raw mill on or raw mill off).Provide any other informationsupporting information you think isnecessary about this test report.Sample Date (mm/dd/yyyy)2/24/2010 2/24/2010 2/24/2010HCl Concentration - as measured -Wet Basis7.86.55.9 6.7ppmv WetM321Downstream of BaghouseOff Line Raw MillHCl Concentration DryBasis8.26.86.2 7.1ppm v DryM321Downstream of BaghouseOff Line Raw MillOxygen Concentration - drybasis12.112.712.4 12.4%M3ADownstream of BaghouseOff Line Raw MillCO2 Concentration - drybasis13.712.613.2 13.2%M3ADownstream of BaghouseOff Line Raw MillHCl Concentration - drycorrectedto 7% oxygen13.011.510.1 11.5ppm v dryat 7% O2M321Downstream of BaghouseOff Line Raw MillExhaust Stream %Moisture4.94.64.6 4.7%M320 and M4Downstream of BaghouseOff Line Raw MillExhaust Flowrate77,80082,40077,200 79133dscfmM1, 2, 3A and 4Downstream of BaghouseOff Line Raw MillExhaust Temperature372370389377FT/CDownstream of BaghouseOff Line Raw MillNotes:Method 320 data used for moisture results reporting.